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JCAR35061 1-0815204r01
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TITLE 35: ENVIRONMENTAL
PROTECTION
SUBTITLE F: PUBLIC WATER
SUPPLIES
CHAPTER I: POLLUTION
CONTROL BOARD
PART 611
PRIMARY DRiNKING
WATER STANDARDS
SUBPART A: GENERAL
CVD
CL<’
OFFICE
10
Section
SEP ‘
11
13
12
611.101
611.100611.102
DefinitionsPurpose,
Incorporations
Scope,
by
and
Reference
Applicability
?oHtjo
STATE
OF
Control
ILIJN
Boa%
14
611.103
Severability
15
611.105
Electronic
Reporting
16
611.107
Agency Inspection of PWS Facilities
17
611.108
Delegation
to Local Government
18
611.109
Enforcement
19
611.110
Special
Exception Permits
20
611.111
Relief Equivalent to SDWA
Section 1415(a) Variances
21
611.112
Relief Equivalent to SDWA Section
1416 Exemptions
22
611.113
Alternative Treatment Techniques
23
611.114
Siting
Requirements
24
611.115
Source Water Quantity
25
611.120
Effective Dates
26
61 1.12 1
Maximum Contaminant Levels and Finished
Water Quality
27
611.125
Fluoridation Requirement
28
611.126
Prohibition
on Use of Lead
29
611.130
Special Requirements for Certain
Variances and Adjusted Standards
30
61 1.13 1
Relief Equivalent
to SDWA Section 1415(e) Small
System Variance
31
611.160
Composite Correction Program
32
611.161
Case-by-Case Reduced Subpart
Y Monitoring for Wholesale
and Consecutive
33
Systems
34
35
SUBPART B:
FILTRATION AND
DISINFECTION
36
37
Section
38
611.201
Requiring a Demonstration
39
611.202
Procedures for Agency Determinations
40
611.211
Filtration Required
41
611.212
Groundwater under Direct
Influence of Surface
Water
42
611.213
No Method of HPC Analysis
43
611.220
General Requirements
JCAR35O61
1-0815204r01
Point-of-Entry
Devices
Use
of
Point-of-Use
Devices
or Bottled
Water
63
64
SUBPART
D:
TREATMENT
TECHNIQUES
65
General
Requirements
Acrylamide
and Epichlorohydrin
Corrosion
Control
SUBPART
F:
MAXIMUM
CONTAMINANT
LEVELS
(MCLs)
AN])
MAXIMUM
RESIDUAL
DISINFECTANT
LEVELS
(MRDLs)
Old
MCLs for
Inorganic
Chemical
Contaminants
Revised
MCLs
for
Inorganic
Chemical
Contaminants
State-Only
Maximum
Contaminant
Levels (MCLs)
for
Organic Chemical
Contaminants
Revised
MCLs
for Organic
Chemical
Contaminants
Maximum
Contaminant
Levels
(MCLs)
for
Disinfection
Byproducts
(DBPs)
Maximum
Residual
Disinfectant
Levels
(MRDLs)
Turbidity
(Repealed)
Microbiological
Contaminants
Maximum
Contaminant
Levels
for Radionuclides
Beta Particle
and Photon
Radioactivity
(Repealed)
44
611.230
45
611.231
46
611.232
47
611.233
48
611.240
49
611.241
50
611.242
51
611.250
52
611.261
53
611.262
54
611.271
55
611.272
56
611.276
57
Filtration
Effective
Dates
Source
Water
Quality
Conditions
Site-Specific
Conditions
Treatment
Technique
Violations
Disinfection
Unfiltered
PWSs
Filtered
PWSs
Filtration
Unfiltered
PWSs:
Reporting
and
Recordkeeping
Filtered
PWSs:
Reporting
and Recordkeeping
Protection
during
Repair
Work
Disinfection
Following
Repair
Recycle
Provisions
60
Section
61
611.280
62
611.290
58
SUBPART
C:
USE
OF NON-CENTRALIZED
TREATMENT
DEVICES
59
66
Section
67
611.295
68
611.296
69
611.297
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
Section
611.300
6
11.301
611.3
10
611.3
11
611.3
12
611.3
13
611.320
611.325
611.330
611.33 1
JCAR35O61 1-0815204r01
87
SUBPART G: LEAD ANT)
COPPER
88
89
Section
90
611.350
General
Requirements
91
611.351
Applicability of Corrosion
Control
92
611.352
Corrosion Control Treatment
93
611.353
Source
Water
Treatment
94
611.354
Lead Service Line Replacement
95
611.355
Public Education and Supplemental
Monitoring
96
611.356
Tap
Water Monitoring
for Lead and Copper
97
611.357
Monitoring for Water Quality
Parameters
98
611.358
Monitoring for Lead
and Copper in Source Water
99
611.359
Analytical
Methods
100
611.360
Reporting
101
611.361
Recordkeeping
102
103
SUBPART
I: DISiNFECTANT
RESIDUALS, DISINFECTION
BYPRODUCTS,
104
AND DISINFECTION BYPRODUCT
PRECURSORS
105
106
Section
107
611.380
General Requirements
108
611.381
Analytical
Requirements
109
611.382
Monitoring Requirements
110
611.383
Compliance Requirements
111
611.384
Reporting and Recordkeeping Requirements
112
611.385
Treatment Technique
for Control of Disinfection Byproduct
(DBP) Precursors
113
114
SUBPART K:
GENERAL
MONITORING AND ANALYTICAL
REQUIREMENTS
115
116
Section
117
611.480
Alternative
Analytical
Techniques
118
611.490
Certified Laboratories
119
611.491
Laboratory Testing Equipment
120
611.500
Consecutive
PWSs
121
611.510
Special Monitoring for Unregulated
Contaminants (Repealed)
122
123
SUBPART L:
MICROBIOLOGICAL
MONITORING
124
AND ANALYTICAL
REQUIREMENTS
125
126
Section
127
611.521
Routine Coliform Monitoring
128
611.522
Repeat Coliform Monitoring
129
611.523
Invalidation of
Total Coliform Samples
JCAR35O61 10815204r01
130
611.524
Sanitary Surveys
131
611.525
Fecal Coliform
and E. Coli Testing
132
611.526
Analytical Methodology
133
611.527
Response to Violation
134
611.531
Analytical
Requirements
135
611.532
UnfilteredPWSs
136
611.533
FilteredPWSs
137
138
SUBPART M: TURBIDITY
MONITORING ANT)
ANALYTICAL REQUIREMENTS
139
140
Section
141
611.560
Turbidity
142
143
SUBPART
N: INORGANIC
MONITORING AND
ANALYTICAL
REQUIREMENTS
144
145
Section
146
611.591
Violation
of a State MCL
147
611.592
Frequency of State
Monitoring
148
611.600
Applicability
149
611.601
Monitoring
Frequency
150
611.602
Asbestos Monitoring
Frequency
151
611.603
Inorganic Monitoring Frequency
152
6
11.604
Nitrate
Monitoring
153
611.605
Nitrite Monitoring
154
611.606
Confirmation Samples
155
611.607
More Frequent Monitoring and
Confirmation Sampling
156
611.608
Additional Optional
Monitoring
157
6 11.609
Determining Compliance
158
611.610
Inorganic Monitoring
Times
159
611.611
Inorganic
Analysis
160
611.612
Monitoring Requirements
for Old Inorganic MCLs
161
611.630
Special Monitoring
for Sodium
162
611.631
Special
Monitoring for Inorganic
Chemicals (Repealed)
163
164
SUBPART 0:
ORGANIC MONITORING AND
ANALYTICAL REQUIREMENTS
165
166
Section
167
611.640
Definitions
168
611.641
OldMCLs
169
611.645
Analytical
Methods for Organic
Chemical Contaminants
170
611.646
Phase I, Phase
II, and Phase V Volatile Organic
Contaminants
171
611.647
Sampling for Phase I
Volatile Organic Contaminants
(Repealed)
172
611.648
Phase
II, Phase JIB, and Phase
V Synthetic Organic Contaminants
JCAR35O61 1-0815204r01
173
611.650
Monitoring
for
36 Contaminants
(Repealed)
174
611.657
Analytical Methods
for 36 Contaminants
(Repealed)
175
611.658
Special Monitoring
for Organic
Chemicals (Repealed)
176
177
SUBPART P: THM
MONITORING
AND
ANALYTICAL
REQUREMENTS
178
179
Section
180
611.680
Sampling,
Analytical,
and
other Requirements
181
611.683
Reduced
Monitoring Frequency
(Repealed)
182
611.684
Averaging
(Repealed)
183
611.685
AnalyticalMethods
184
6 11.686
Modification
to
System
(Repealed)
185
611.687
Sampling for
THM Potential
(Repealed)
186
611.688
Applicability
Dates (Repealed)
187
188
SUBPART
Q: RADIOLOGICAL
MONITORING
AND ANALYTICAL
REQUIREMENTS
189
190
Section
191
611.720
Analytical Methods
192
611.731
Gross Alpha
193
611.732
Beta Particle
and Photon Radioactivity
194
611.733
General Monitoring
and
Compliance
Requirements
195
196
SUBPART
R: ENHANCED
FILTRATION
AND
DISINFECTION:
197
SYSTEMS THAT
SERVE
10,000 OR MORE PEOPLE
198
199
Section
200
611.740
General
Requirements
201
611.741
Standards for Avoiding
Filtration
202
611.742
Disinfection
Profiling
and Benchmarking
203
611.743
Filtration
204
611.744
Filtration
Sampling Requirements
205
611.745
Reporting
and Recordkeeping
Requirements
206
207
SUBPARTS:
GROUNDWATER
RULE
208
Section
209
611.800
General
Requirements
and Applicability
210
611.801
Sanitary
Surveys for
GWS Suppliers
211
611.802
Groundwater
Source
Microbial Monitoring
and Analytical
Methods
212
611.803
Treatment
Technique
Requirements for
GWS Suppliers
213
611.804
Treatment Technique
Violations
for
GWS
Suppliers
214
611.805
Reporting
and Recordkeeping
for
GWS Suppliers
215
JCAR35O61 1-0815204r01
216
SUBPART
T:
REPORTING
AND RECORDKEEPING
217
218
Section
219
611.830
Applicability
220
611.831
Monthly Operating
Report
221
611.832
Notice by Agency
(Repealed)
222
611.833
Cross
Connection
Reporting
223
611.840
Reporting
224
611.851
Reporting MCL,
MRDL, and other
Violations (Repealed)
225
611.852
Reporting other
Violations (Repealed)
226
611.853
Notice to New
Billing Units (Repealed)
227
611.854
General Content
of Public Notice (Repealed)
228
611.855
Mandatory
Health Effects Language
(Repealed)
229
611.856
Fluoride Notice
(Repealed)
230
611.858
Fluoride Secondary
Standard (Repealed)
231
611.860
Record
Maintenance
232
611.870
List of 36 Contaminants
(Repealed)
233
234
SUBPART
U: CONSUMER
CONFIDENCE REPORTS
235
236
Section
237
611.881
Purpose and Applicability
238
611.882
Compliance Dates
239
611.883
ContentoftheReports
240
611.884
Required
Additional
Health Information
241
611.885
Report
Delivery and Recordkeeping
242
243
SUBPART
V: PUBLIC NOTIFICATION
OF DRINKING
WATER
VIOLATIONS
244
245
Section
246
611.901
General
Public Notification
Requirements
247
611.902
Tier
1 Public
Notice:
Form,
Manner,
and Frequency of Notice
248
611.903
Tier 2 Public Notice:
Form, Manner, and
Frequency of
Notice
249
611.904
Tier
3
Public Notice:
Form, Manner,
and Frequency of Notice
250
611.905
Content of the Public
Notice
251
611.906
Notice
to
New
Billing Units or New
Customers
252
611.907
Special Notice of the
Availability of Unregulated
Contaminant
Monitoring
253
Results
254
611.908
Special Notice for Exceedence
of the Fluoride
Secondary Standard
255
611.909
Special
Notice for Nitrate
Exceedences above
the MCL by a
Non-Community
256
Water
System
257
611.910
Notice by the
Agency on
Behalf of a PWS
258
611.911
Special
Notice for Cryptosporidium
JCAR35O61
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259
260
SUBPART
W: INITIAL DISTRIBUTION SYSTEM EVALUATIONS
261
Section
262
611.920
General Requirements
263
611.921
Standard
Monitoring
264
611.922
System-Specific Studies
265
611.923
40/30 Certification
266
611.924
Very Small
System Waivers
267
611.925
Subpart Y Compliance Monitoring Location Recommendations
268
269
SUBPART X: ENHANCED FILTRATION AND DISiNFECTION -
270
SYSTEMS
SERVING FEWER THAN 10,000 PEOPLE
271
Section
272
611.950
General
Requirements
273
611.951
Finished
Water Reservoirs
274
611.952
Additional Watershed Control Requirements for Unfiltered
Systems
275
611.953
Disinfection
Profile
276
611.954
Disinfection Benchmark
277
611.955
Combined Filter
Effluent Turbidity Limits
278
611.956
Individual Filter Turbidity Requirements
279
611.957
Reporting and Recordkeeping Requirements
280
281
SUBPART Y-
STAGE 2 DISINFECTION BYPRODUCTS REQUIREMENTS
282
Section
283
611.970
General Requirements
284
611.971
Routine
Monitoring
285
611.972
Subpart YMonitoring Plan
286
611.973
Reduced
Monitoring
287
611.974
Additional Requirements for Consecutive Systems
288
611.975
Conditions
Requiring Increased Monitoring
289
611.976
Operational
Evaluation Levels
290
611.977
Requirements for Remaining on Reduced TTHM and HAA5
Monitoring Based
291
on Subpart I
Results
292
611.978
Requirements for Remaining on Increased
TTHM and HAA5 Monitoring Based
293
on Subpart
I Results
294
611.979
Reporting and Recordkeeping Requirements
295
296
SUBPART Z: ENHANCED TREATMENT FOR CRYPTOSPORIDIUM
297
Section
298
611.1000
General
Requirements
299
611.1001
Source Water Monitoring Requirements: Source Water Monitoring
300
611.1002
Source Water Monitoring Requirements: Sampling Schedules
301
611.1003
Source
Water Monitoring Requirements: Sampling Locations
JCAR35O61
1-0815204r01
302
611.1004
Source
Water Monitoring Requirements:
Analytical
Methods
303
611.1005
Source Water
Monitoring
Requirements:
Approved Laboratories
304
611.1006
Source
Water Monitoring Requirements:
Reporting Source
Water Monitoring
305
Results
306
611.1007
Source
Water
Monitoring
Requirements:
Grandfathering
Previously
Collected
307
Data
308
611.1008
Disinfection Profiling
and Benchmarking
Requirements:
Requirements
When
309
Making
a
Significant
Change in Disinfection
Practice
310
611.1009
Disinfection Profiling
and Benchmarking
Requirements:
Developing
the
311
Disinfection
Profile
and Benchmark
312
611.1010
Treatment Technique
Requirements:
Bin Classification
for Filtered
Systems
313
611.1011
Treatment
Technique
Requirements:
Filtered System
Additional
314
Cryptosporidium Treatment
Requirements
315
611.1012
Treatment
Technique
Requirements:
Unfiltered
System
Cryptosporidium
316
Treatment
Requirements
317
611.1013
Treatment
Technique Requirements:
Schedule for
Compliance with
318
Cryptosporidium
Treatment
Requirements
319
611.1014
Treatment
Technique Requirements:
Requirements
for Uncovered Finished
320
Water
Storage
Facilities
321
611.1015
Requirements
for Microbial
Toolbox
Components:
Microbial Toolbox
Options
322
for Meeting Cryptosporidium
Treatment
Requirements
323
611.1016
Requirements
for
Microbial Toolbox
Components:
Source Toolbox
Components
324
611.1017
Requirements
for Microbial Toolbox
Components:
Pre-Filtration Treatment
325
Toolbox Components
326
611.1018
Requirements
for Microbial
Toolbox Components:
Treatment
Performance
327
Toolbox
Components
328
611.1019
Requirements
for Microbial
Toolbox Components:
Additional
Filtration Toolbox
329
Components
330
611.1020
Requirements
for Microbial Toolbox
Components:
Jiiactivation
Toolbox
331
Components
332
611.1021
Reporting
and Recordkeeping Requirements:
Reporting Requirements
333
611.1022
Reporting and Recordkeeping
Requirements: Recordkeeping
Requirements
334
611.1023
Requirements to Respond
to Significant
Deficiencies
Identified in Sanitary
335
Surveys
Performed
by USEPA or
the Agency
336
337
61 1.APPENDIX
A
Regulated
Contaminants
338
61
1.APPENDIX
B
Percent Inactivation
of
G.
Lamblia
Cysts
339
61
1.APPENDIX
C
Common
Names
of Organic
Chemicals
340
611
.APPENDJX
D
Defined
Substrate Method
for the Simultaneous
Detection
of Total
341
Coliforms
and Eschericia
Coli
from
Drinking Water
342
611
.APPENDIX E
Mandatory
Lead
Public Education Information
for
Community Water
343
Systems
344
61
1.APPENDIX
F
Mandatory
Lead
Public Education
Information for Non-Transient
Non-
JCAR35O61 1-0815204r01
Community Water
Systems
NPDWR Violations and
Situations Requiring Public Notice
Standard Health
Effects Language for Public Notification
Acronyms Used in
Public Notification Regulation
Total Coliform Monitoring
Frequency
Fecal or
Total Coliform Density
Measurements
Frequency of
RDC Measurement
Number of Lead and
Copper Monitoring Sites
Lead and
Copper Monitoring Start Dates
Number of Water
Quality Parameter Sampling Sites
Summary
of
Section
611.357 Monitoring Requirements
for Water Quality
Parameters
CT Values (mgminte)
for Cryptosporidium Inactivation
by Chlorine
Dioxide
CT Values (mgmin!e)
for Cryptosporidium Inactivation
by
Ozone
UV
Dose
Table for Cryptosporidium, Giardia lamblia,
and Virus
Inactivation Credit
Federal Effective
Dates
364
AUTHORITY: Implementing Sections 7.2, 17, and 17.5 and
authorized by Section 27 of the
365
Environmental
Protection Act
[415 ILCS 5/7.2, 17, 17.5, and 27].
SOURCE: Adopted in R88-26 at 14 Ill. Reg.
16517, effective September 20, 1990; amended
in
R90-21 at 14 Ill. Reg.
20448,
effective December 11, 1990; amended
in R90-13 at 15 Ill. Reg.
1562,
effective January 22, 1991;
amended in R91-3 at 16 Ill. Reg. 19010,
effective December
1,
1992; amended in R92-3 at 17 Ill. Reg.
7796, effective May 18, 1993; amended in R93-1
at 17
Ill. Reg.
12650,
effective July
23,
1993; amended in R94-4 at 18 Ill.
Reg.
12291,
effective July
28, 1994;
amended in R94-23 at 19 Ill. Reg.
8613, effective June 20, 1995; amended in
R95-17
at 20 Ill. Reg.
14493, effective
October 22, 1996; amended in R98-2 at 22
Ill. Reg. 5020,
effective March 5, 1998; amended in R99-6 at 23 Ill. Reg. 2756,
effective February 17, 1999;
amended in R99-12 at 23 Ill. Reg. 10348,
effective August 11, 1999; amended in
R00-8 at 23 Ill.
Reg. 14715, effective December 8, 1999; amended in R00-10 at 24 Ill.
Reg. 14226, effective
September
11, 2000; amended in R01-7 at 25
Iii. Reg.
1329,
effective January 11, 2001;
amended
in R01-20 at 25 Ill. Reg.
13611, effective October
9,
2001; amended
in
R02-5
at 26 Ill.
Reg.
3522, effective February
22,
2002; amended in R03-4 at
27 Ill. Reg. 1183, effective January
10, 2003;
amended
in
R03-15 at 27 Ill.
Reg. 16447, effective October
10,
2003;
amended in
R04-3 at 28 Ill. Reg. 5269, effective March 10,
2004; amended in R04-13 at 28 Ill. Reg. 12666,
effective August
26,
2004; amended in R05-6 at 29 Ill. Reg. 2287,
effective January 28, 2005;
amended
in R06-15 at
30
Ill. Reg. 17004,
effective October 13, 2006; amended
in R07-2/R07-1 1
at
31111. Reg. 11757, effective July 27, 2007;
amended in R08-5/R08-7/R08-13 at 33 Ill.
Reg.
effective
345
346
347
348
349
350
351
352
353
354
355
356
357
358
359
360
361
362
363
611.APPENDIX
G
611 .APPENDIX H
611 .APPENDJX I
611.TABLE A
611.TABLE B
611.TABLE C
611.TABLE D
611.TABLE E
61 1.TABLE
F
611.TABLE
G
61 1.TABLE H
611.TABLE I
611.TABLE J
611.TABLE
Z
366
367
368
369
370
371
372
373
374
375
376
377
378
379
380
381
382
383
384
385
386
387
SUBPART A: GENERAL
JCAR35O61
1-0815204r01
388
389
Section 611.101
Definitions
390
391
As used in
this Part,
the
following terms
have
the
given meanings:
392
393
“Act”
means
the Environmental
Protection
Act [415
ILCS
5].
394
395
“Agency”
means
the Illinois
Environmental
Protection
Agency.
396
BOARD
NOTE:
The Department
of Public
Health
(Public Health
or DPH)
397
regulates
non-community
water
supplies
(“non-C
WSs,”
including
non-transient,
398
non-community
water
supplies
(“NTNCWSs”)
and
transient non-community
399
water
supplies
(“transient
non-CWSs”)).
For the
purposes
of regulation
of
400
supplies
by Public
Health
by
reference to
this Part,
“Agency”
will mean the
401
Department
of Public
Health.
402
403
“Approved
source of
bottled water,”
for the
purposes
of
Section
6 11.130(d)
(4),
404
means
a
source of
water
and
the
water
therefrom,
whether
it be from
a spring,
405
artesian well,
drilled
well, municipal
water
supply, or
any
other
source, that
has
406
been inspected
and
the
water sampled,
analyzed,
and
found
to be
a
safe and
407
sanitary
quality
according
to
applicable
laws
and
regulations
of
State and local
408
government
agencies
having jurisdiction,
as evidenced
by
the
presence in
the
409
plant
of current
certificates
or
notations
of approval
from
each
government
410
agency
or
agencies
having
jurisdiction
over the
source, the
water
it bottles,
and
411
the
distribution
of
the water
in
commerce.
412
BOARD
NOTE:
Derived
from
40
CFR
142.62(g)(2)
and
21 CFR 129.3(a)
413
QQ7)(2006).
The Board
cannot
compile
an
exhaustive
listing
of all federal,
414
State,
and local
laws to which
bottled
water and
bottling
water
may be
subjected.
415
However,
the
statutes and
regulations
of which
the Board
is
aware are
the
416
following:
the
Illinois Food,
Drug and
Cosmetic
Act
[410
ILCS 620],
the Bottled
417
Water
Act [815
ILCS
310],
the
DPH Water
Well
Construction
Code (77
Iii.
Adm.
418
Code
920),
the
DPH Water
Well
Pump
Installation
Code
(77
Ill.
Adm.
Code 925),
419
the
federal
bottled
water quality
standards
(21
CFR 103.35),
the federal
drinking
420
water
processing
and bottling
standards
(21
CFR
129), the
federal
Current
Good
421
Manufacturing
Practice
in Manufacturing,
Packing,
or Holding
Human
Food (21
422
CFR
110),
the federal
Fair
Packaging
and
Labeling
Act (15
USC
1451 et
seq.),
423
and
the
federal Fair
Packaging
and Labeling
regulations
(21
CFR
201).
424
425
“Bag
filters” means
pressure-driven
separation
devices
that
remove particulate
426
matter
larger
than
one
micrometer
using
an engineered
porous
filtration
media.
427
They
are typically
constructed
of
a non-rigid,
fabric
filtration
media housed
in
a
428
pressure
vessel
in which
the
direction
of flow is
from
the
inside of the
bag to
429
outside.
430
JCAR35O61 1-0815204r01
431
“Bank
filtration”
means a water treatment
process that uses a well to recover
432
surface water that has naturally infiltrated
into groundwater through
a
river
bed or
433
banks.
Infiltration
is typically enhanced
by the hydraulic gradient imposed
by a
434
nearby
pumping water supply
or other wells.
435
436
“Best available technology” or “BAT”
means the best technology, treatment
437
techniques,
or
other means that USEPA has found are available
for the
438
contaminant in question. BAT is
specified in Subpart F of this Part.
439
440
“Bin
classification”
or “bin” means, for the purposes of Subpart Z
of this Part, the
441
appropriate of the four treatment categories
(Bin 1, Bin 2, Bin 3, or Bin 4) that
is
442
assigned to a filtered system
supplier pursuant to Section 611.1010 based
on the
443
results
of the
source water Cryptosporidium monitoring
described in the previous
444
section. This bin classification determines
the degree of additional
445
Cryptosporidium treatment,
if any, the filtered PWS must provide.
446
BOARD NOTE: Derived from 40 CFR 141.7
10
and
the preamble discussion
at
447
71 Fed. Reg. 654, 657 (Jan.
5,
2006).
448
449
“Board” means the Illinois
Pollution Control Board.
450
451
“Cartridge filters” means pressure-driven separation devices
that remove
452
particulate matter
larger than 1 micrometer using an engineered
porous filtration
453
media. They are typically constructed
as rigid or semi-rigid, self-supporting
filter
454
elements housed in pressure vessels in which
flow is from the outside of the
455
cartridge to the
inside.
456
457
“CAS No.” means “Chemical Abstracts Services
Number.”
458
459
“CT” or
“CTcaic”
is the product of “residual disinfectant
concentration” (RDC or
460
C)
in mg!e determined before or at the
first customer, and the corresponding
461
“disinfectant contact
time” (T) in minutes. If a supplier applies disinfectants
at
462
more than one point prior to the first customer,
it must determine the CT of each
463
disinfectant sequence before or at
the first customer to determine the total
percent
464
inactivation
or “total inactivation ratio.” In determining the
total inactivation
465
ratio, the supplier must determine the
RDC of each disinfection sequence and
466
corresponding
contact time before any subsequent disinfection
application points.
467
(See “CT
999
.”)
468
469
9
99.
“CT”is the
CT value required for
99.9
percent (3-log) inactivation
of Giardia
470
lamblia cysts. CT
99.9for
a variety of disinfectants and conditions appear in
Tables
471
1.1-1.6, 2.1 and 3.1 of Appendix B
of this Part. (See “Inactivation Ratio.”)
472
BOARD
NOTE: Derived from the definition of”CT” in4O
CFR
141.2
473
(2007)(2006).
JCAR35O61
1-0815204r01
474
475
“Coagulation” means a process using coagulant chemicals and mixing by which
476
colloidal and suspended
materials
are destabilized and agglomerated
into
flocs.
477
478
“Combined distribution system” means the interconnected distribution system
479
consisting of the distribution systems of wholesale systems and of the consecutive
480
systems that
receive finished water.
481
482
“Community water system” or “CWS” means a public water system (PWS) that
483
serves at least 15
service connections used
by
year-round residents or regularly
484
serves at least 25 year-round
residents.
485
BOARD NOTE: This definition differs slightly from that of Section 3.05 of the
486
Act.
487
488
“Compliance
cycle” means the nine-year calendar year cycle during which public
489
water systems (PWSs) must monitor. Each compliance cycle
consists of three
490
three-year compliance periods. The first calendar cycle began January 1, 1993,
491
and ended December31,
2001;
the second began
January 1, 2002, and ends
492
December
31,
2010; the third begins January 1, 2011, and ends December 31,
493
2019.
494
495
“Compliance
period” means a three-year calendar year period within a
496
compliance cycle. Each compliance cycle has three three-year compliance
497
periods. Within the first compliance cycle, the first compliance period ran from
498
January 1, 1993to
December 31, 1995; the second from January 1, 1996 to
499
December 31, 1998; the third from January 1, 1999to December 31, 2001.
500
501
“Comprehensive performance evaluation” or “CPE” is a thorough review and
502
analysis of a treatment plant’s
performance-based capabilities and associated
503
administrative, operation, and maintenance practices. It is conducted to identify
504
factors that may be
adversely impacting a plant’s capability to achieve compliance
505
and emphasizes approaches that can be implemented
without significant capital
506
improvements.
507
BOARD NOTE: The
final sentence of the definition of “comprehensive
508
performance evaluation” in 40 CFR 141.2 is codified as Section 611. 160(a)(2),
509
since it contains
substantive elements that are more appropriately codified in a
510
substantive provision.
511
512
“Confluent growth”
means
a
continuous bacterial growth covering the entire
513
filtration area of a membrane filter or a portion thereof, in which bacterial
514
colonies are not discrete.
515
JCAR35O61 1-0815204r01
516
“Consecutive system” means a public
water system that receives some or all
of its
517
finished water from one or more wholesale systems. Delivery
may be through a
518
direct connection or through the
distribution system of one or more consecutive
519
systems.
520
521
“Contaminant” means any physical, chemical, biological, or radiological
522
substance or matter in water.
523
524
“Conventional
filtration treatment”
means a series of processes including
525
coagulation, flocculation, sedimentation, and
filtration resulting in substantial
526
particulate removal.
527
528
“Diatomaceous earth filtration”
means a process resulting in substantial
529
particulate removal in which the following occur:
530
531
A precoat cake of diatomaceous
earth filter media is deposited on
a
532
support membrane (septum); and
533
534
While the water is filtered
by
passing through
the cake on the septum,
535
additional filter media known as body feed is continuously added
to the
536
feed water to maintain
the permeability of the filter cake.
537
538
“Direct filtration” means a series of processes including coagulation
and filtration
539
but excluding sedimentation resulting in substantial particulate removal.
540
541
“Disinfectant” means any oxidant, including but not limited
to chlorine, chlorine
542
dioxide,
chioramines, and
ozone added to water in any part of the treatment
or
543
distribution process, that is intended to kill or inactivate
pathogenic
544
microorganisms.
545
546
“Disinfectant contact time” or
“T”
means
the time
in
minutes that it takes for
547
water
to
move
from
the
point of disinfectant application or the previous point
of
548
RDC measurement to a point before or at the point where RDC
is measured.
549
550
Where only one RDC is measured, T is the time in minutes that
it takes for
551
water to move from
the point of disinfectant application to a point before
552
or at the point where RDC is measured.
553
554
Where more than one
RDC is measured, T is as follows:
555
556
For the first measurement of RDC, the time in minutes
that it takes
557
for water to
move from the first or only point of disinfectant
558
application to a point
before or at the point where the first RDC
is
JCAR35O61
1-0815204r01
559
measured;
and
560
561
For subsequent
measurements
of RDC, the
time in
minutes
that it
562
takes
for water to move from
the previous
RDC measurement
563
point to the RDC measurement
point
for which the particular
T is
564
being
calculated.
565
566
T in pipelines
must be calculated
based
on “plug flow” by dividing
the
567
internal
volume of the pipe
by the maximum
hourly
flow
rate through that
568
pipe.
569
570
T within
mixing basins and
storage reservoirs
must be determined
by
571
tracer studies
or an equivalent
demonstration.
572
573
“Disinfection”
means a process that inactivates
pathogenic
organisms in
water
by
574
chemical oxidants or
equivalent agents.
575
576
“Disinfection byproduct”
or “DBP”
means a chemical
byproduct that
forms when
577
disinfectants
used
for microbial control
react with
naturally occurring compounds
578
already present in source
water.
DBPs include, but are
not limited to,
579
bromodichloromethane,
bromoform,
chloroform, dichloroacetic
acid, bromate,
580
chlorite, dibromochloromethane,
and certain halo
acetic acids.
581
582
“Disinfection
profile” is a summary
of daily Giardia
lamblia inactivation
through
583
the treatment
plant. The procedure
for
developing
a disinfection
profile is
584
contained in
Section 611.742.
585
586
“Distribution
system”
includes
all points downstream
of an
“entry point” to the
587
point of
consumer ownership.
588
589
“Domestic
or other non-distribution
system
plumbing problem”
means a coliform
590
contamination
problem in a PWS
with
more than
one service connection
that is
591
limited to the specific
service
connection from which
the
coliform-positive
592
sample was
taken.
593
594
“Dose equivalent”
means the product
of
the absorbed
dose from ionizing
radiation
595
and such factors
as account
for
differences in biological
effectiveness
due to the
596
type of radiation
and its distribution
in the body
as specified
by
the
International
597
Commission
on Radiological
Units and
Measurements
(ICRU).
598
599
“Dual
sample set” means a
set of two samples
collected at the same
time
and
600
same location,
with one
sample analyzed
for TTHM and the
other sample
601
analyzed
for HAA5. Dual
sample sets are
collected
for
the purposes of conducting
JCAR35O61
1-0815204r01
602
an
DSE under Subpart
W of this Part
and determining
compliance with
the
603
TTHM and HAA5
MCLs under Subpart
Y of this Part.
604
605
“Enhanced coagulation”
means the
addition of sufficient
coagulant
for improved
606
removal of disinfection
byproduct
(DBP) precursors
by conventional
filtration
607
treatment.
608
609
“Enhanced
softening” means the
improved
removal
of disinfection
byproduct
610
(DBP) precursors
by
precipitative
softening.
611
612
“Entry point” means
a
point
just downstream
of the final treatment
operation,
but
613
upstream of
the first user and upstream
of any
mixing with other water.
If raw
614
water is used without
treatment,
the “entry point”
is the raw
water
source. If
a
615
PWS
receives treated
water from
another PWS,
the “entry point” is
a point
just
616
downstream of
the other PWS,
but upstream of the
first user on
the receiving
617
PWS, and upstream
of
any mixing
with other water.
618
619
“Filter profile” is a
graphical
representation
of individual
filter performance,
620
based on continuous
turbidity
measurements or total
particle counts
versus time
621
for
an
entire filter
run, from startup
to backwash
inclusively, that includes
an
622
assessment of filter
performance
while another filter
is being backwashed.
623
624
“Filtration”
means a process
for removing
particulate matter from
water
by
625
passage
through
porous
media.
626
627
“Finished
water” means
water that
is
introduced into the distribution
system
of
a
628
public
water system
which is intended for
distribution
and consumption without
629
further
treatment, except
that treatment
which is necessary
to maintain
water
630
quality
in the distribution
system (e.g., booster
disinfection,
addition of corrosion
631
control
chemicals,
etc.).
632
633
“Flocculation”
means
a
process to enhance agglomeration
or collection of
smaller
634
floc particles
into larger, more
easily
settleable
particles through
gentle
stirring
by
635
hydraulic or
mechanical
means.
636
637
“Flowing stream”
means
a course of running
water
flowing
in a definite channel.
638
639
“40/30 certification”
means
the certification,
submitted by
the supplier to the
640
Agency
pursuant to Section
611.923, that
the supplier had
no TTHM or HAA5
641
monitoring
violations, and
that
no individual
sample from
its system
exceeded
642
0.040
mg/i?
TTHM
or 0.030 mg/2
HAA5 during eight
consecutive calendar
643
quarters.
644
BOARD NOTE: Derived
from
40
CFR 141.603(a) (2007)(2006).
JCAR35O61
1-0815204r01
645
646
“GAC1O”
means
granular
activated
carbon
(GAC)
filter
beds with
an empty-bed
647
contact time
of 10 minutes
based
on average
daily flow
and a carbon
reactivation
648
frequency
of every
180 days,
except
that
the reactivation
frequency
for
GAC1O
649
that is
used
as a
best
available technology
for
compliance
with the
MCLs set
forth
650
in SubpartY
of this
Part pursuant
to Section
611.312(b)(2)
is
120 days.
651
652
“GAC2O”
means
granular
activated
carbon
filter
beds with
an
empty-bed
contact
653
time
of 20 minutes
based
on
average daily
flow and
a carbon
reactivation
654
frequency
of every
240 days.
655
656
“GC”
means
“gas
chromatography”
or “gas-liquid
phase
chromatography.”
657
658
“GC/MS”
means gas
chromatography
(GC)
followed
by
mass
spectrometry
(MS).
659
660
“Gross
alpha particle
activity”
means
the
total radioactivity
due
to alpha particle
661
emission
as inferred
from
measurements
on
a dry
sample.
662
663
“Gross
beta
particle
activity”
means
the total
radioactivity
due to
beta particle
664
emission
as inferred
from measurements
on a dry sample.
665
666
“Groundwater
system” or
“GWS”
means
a public
water
supply
(PWS) that
uses
667
only
groundwater
sources,
including a
consecutive
system
that
receives
finished
668
groundwater.
669
BOARD
NOTE:
Derived
from
40
CFR 141.23(b)(2)
and
141.24(f)(2)
note
670
(2006)
and 40
CFR 141.400(b)
(2007),
as added
at 71
Fed.
Reg. 65576
ov.
8,
671
2006).
672
673
“Groundwater
under the
direct
influence
of surface
water”
means
any
water
674
beneath
the surface
of
the
ground with
significant
occurrence
of insects
or other
675
macroorganisms,
algae,
or
large-diameter
pathogens,
such
as
Giardia lamblia
or
676
Cryptosporidium,
or significant
and
relatively
rapid shifts
in water
characteristics,
677
such
as
turbidity,
temperature,
conductivity,
or pH,
that closely
correlate
to
678
climatological
or surface
water
conditions.
“Groundwater
under
the direct
679
influence
of surface
water”
is as
determined
in Section
611.212.
680
681
“Haloacetic
acids
(five)”
or
“HAA5” means
the
sum of
the
concentrations
in
682
milligrams
per
liter (mg/i)
of
five haloacetic
acid
compounds
(monochioroacetic
683
acid,
dichioroacetic
acid,
trichloroacetic
acid,
monobromoacetic
acid, and
684
dibromoacetic
acid),
rounded to
two
significant
figures
after
addition.
685
686
“Halogen”
means one
of the
chemical
elements
chlorine,
bromine,
or iodine.
687
JCAR35O61
1-0815204r01
688
“HPC”
means “heterotrophic
plate count,” measured as
specified in Section
689
611.531(c).
690
691
“Hydrogeologic sensitivity assessment,”
for the purposes of
Subpart S of this Part,
692
means a determination of whether a
GWS supplier obtains water from a
693
hydrogeologically sensitive
setting.
694
BOARD NOTE: Derived
from
40
CFR 141.400(c)(5) (2007),
as added at 71 Fed.
695
Reg.
65574
(Nov. 8, 2006).
696
697
“Inactivation ratio” or “Ai” means as
follows:
698
699
Ai
= CTcac/CT
999
700
701
The
sum of the inactivation ratios or
“total inactivation ratio” (B) is
702
calculated by adding together
the inactivation ratio for each disinfection
703
sequence
as follows:
704
705
B=E(Ai)
706
707
A
total
inactivation ratio equal to or greater
than 1.0 is assumed to provide
708
a 3-log inactivation
of Giardia lamblia cysts.
709
710
BOARD NOTE: Derived from the definition
of”CT” in 40 CFR 141.2
711
(2007)(2006).
712
713
“Initial compliance period” means the
three-year compliance period that
begins
714
January 1, 1993,
except for the MCLs for dichioromethane, 1,2,4-
715
trichlorobenzene, 1,1 ,2-trichloroethane,
benzo(a)pyrene, dalapon, di(2-
716
ethylhexyl)adipate,
di(2-ethylhexyl)phthalate, dinoseb, diquat,
endothall, endrin,
717
glyphosate, hexachlorobenzene, hexachiorocyclopentadiene,
oxamyl, picloram,
718
simazine, 2,3,7,8-TCDD,
antimony, beryllium, cyanide, nickel, and thallium,
as
719
they
apply to a
supplier whose system has fewer than
150 service connections,
for
720
which it means the three-year compliance
period that began on January 1, 1996.
721
722
“Initial distribution system evaluation” or “IDSE”
means the evaluation,
723
performed by the
supplier pursuant to Section 611.921(c), to
determine the
724
locations in a distribution system that are
representative of high TTHM and
725
HAA5 concentrations
throughout the distribution
system. An IDSE is used in
726
conjunction with,
but is distinct from, the compliance monitoring
undertaken to
727
identify and select monitoring locations
used to determine compliance with
728
Subpart I of this PartX.
729
BOARD NOTE: Derived
from 40 CFR 141 .601(c) (2007)611.601(c)
(2006).
730
JCAR35O61 1-0815204r01
731
“Inorganic contaminants” or “lOCs” refers to that group
of contaminants
732
designated
as such
in United
States Environmental Protection Agency
(USEPA)
733
regulatory discussions and guidance documents.
lOCs include antimony, arsenic,
734
asbestos, barium, beryllium, cadmium, chromium, cyanide,
mercury, nickel,
735
nitrate, nitrite, selenium,
and thallium.
736
BOARD NOTE: The IOCs are derived
from
40
CFR 141.23(a)(4) (2007)(2006).
737
738
“e”
means
“liter.”
739
740
“Lake or reservoir” means a natural or man made basin or hollow on the Earth’s
741
surface in which water collects or is stored that
may or may not have a current or
742
single direction
of flow.
743
744
“Legionella” means a genus of bacteria,
some species of which have caused a type
745
of pneumonia called Legionnaires Disease.
746
747
“Locational
running
annual average”
or “LRAA” means the average of sample
748
analytical results for samples taken at a particular monitoring
location during the
749
previous four calendar quarters.
750
751
“Man-made beta particle and photon emitters” means all radionuclides
emitting
752
beta particles or photons listed in “Maximum Permissible Body Burdens and
753
Maximum Permissible
Concentrations of Radionuclides in Air and in Water
for
754
Occupational Exposure,” NCRP Report
Number
22,
incorporated by reference in
755
Section 611.102, except the daughter products of thorium-232, uranium-235
and
756
uranium-238.
757
758
“Maximum contaminant level” or “MCL” means the maximum permissible
level
759
of a contaminant in water that is delivered to any user of a public water
system.
760
(See Section 611.121.)
761
762
“Maximum contaminant level goal”
or “MCLG”
means
the maximum level of a
763
contaminant in drinking water at
which no known or anticipated adverse effect
on
764
the health of persons would occur, and which allows an adequate margin
of
765
safety. MCLGs are nonenforceable
health goals.
766
BOARD NOTE: The Board has not routinely adopted the regulations
relating to
767
the federal MCLGs because
they are outside the scope of the Board’s identical-in
768
substance mandate under Section 17.5
of
the
Act [415 ILCS 5/17.5].
769
770
“Maximum residual
disinfectant level” or “MRDL” means the maximum
771
permissible level of a disinfectant
added for water treatment that may not be
772
exceeded at the consumer’s tap without an unacceptable
possibility of adverse
773
health effects. MRDLs
are enforceable in the same manner as are MCLs.
(See
JCAR35O61 1-0815204r01
774
Section
611.313 and Section 611.383.)
775
776
“Maximum residual disinfectant level
goal??
or “MRDLG” means the maximum
777
level of a disinfectant added for water treatment at which no known or anticipated
778
adverse effect on the health of persons would occur, and which allows an
779
adequate
margin
of
safety. MRDLGs
are
nonenforceable
health goals
and
do not
780
reflect the benefit of the addition of the chemical for control of waterbome
781
microbial contaminants.
782
783
“Maximum total trihalomethane potential” or “MTP” means the maximum
784
concentration of total trihalomethanes (TTHMs) produced in a given water
785
containing a disinfectant residual after seven days at a temperature of
250
C
or
786
above.
787
788
“Membrane filtration” means a pressure or vacuum driven separation process in
789
which particulate matter larger than one micrometer is rejected
by
an engineered
790
barrier, primarily through a size exclusion mechanism, and which has a
791
measurable removal efficiency of a target organism that can be verified through
792
the application of a direct integrity test. This definition includes the common
793
membrane
technologies of microfiltration, ultrafiltration, nanofiltration,
and
794
reverse osmosis.
795
796
“MFL” means millions of fibers per liter larger than 10 micrometers.
797
BOARD
NOTE: Derived from 40
CFR
141.23(a)(4)(i) (2007)(2006).
798
799
“mg” means milligrams (1/1000 of a gram).
800
801
“mg/C “means milligrams per liter.
802
803
“Mixed system” means a PWS that uses both groundwater and
surface water
804
sources.
805
BOARD
NOTE: Drawn from 40 CFR 141.23(b)(2) and
141.24(0(2)
note
806
(2007)(2006).
807
808
“MUG” means
4-methyl-umbelliferyl-beta-d-glucuronide.
809
810
“Near the first service connection” means at one of the 20 percent of all service
811
connections in the entire system that
are
nearest the
public
water
system (PWS)
812
treatment facility, as measured by water transport time within the distribution
813
system.
814
815
“nm” means nanometer (1/1,000,000,000 of a meter).
816
JCAR35O61 1-0815204r01
817
“Non-community
water
system”
or
“NCWS”
or “non-CWS” means
a public water
818
system (PWS)
that is not a community
water system
(CWS). A
non-community
819
water
system
is
either
a “transient
non-community
water system (TWS)”
or a
820
“non-transient non-community
water system (NTNCWS).”
821
822
“Non-transient
non-community
water
system”
or “NTNCWS” means
a public
823
water system
(PWS)
that
is not a community water
system
(CWS) and that
824
regularly
serves at least 25 of
the
same persons
over six months
per year.
825
826
“NPDWR”
means “national
primary drinking
water regulation.”
827
828
“NTU”
means “nephelometric
turbidity
units.”
829
830
“Old MCL”
means one of the
inorganic
maximum
contaminant
levels
(MCLs),
831
codified at
Section 611.300, or
organic MCLs,
codified at Section
611.310,
832
including any marked
as “additional
State requirements.”
833
BOARD NOTE:
Old MCLs are
those derived
prior to the implementation
of the
834
USEPA
“Phase
II” regulations.
The Section 611.640
definition
of this term,
835
which applies
only to Subpart
0 of this Part, differs
from this
definition in that the
836
definition
does not include the
Section
611.300
inorganic MCLs.
837
838
“P-A Coliform
Test” means
“Presence-Absence
Coliform
Test.”
839
840
“Paired sample” means
two samples
of
water
for Total
Organic Carbon
(TOC).
841
One
sample is of raw water
taken prior
to any treatment.
The other sample
is
842
taken after the point
of combined
filter effluent and is representative
of the treated
843
water. These
samples
are taken at the
same time.
(See Section 611.382.)
844
845
“Performance
evaluation
sample” or
“PE sample” means
a reference sample
846
provided to a laboratory
for the
purpose
of demonstrating
that the laboratory
can
847
successfully
analyze the
sample
within
limits of performance
specified by
the
848
Agency; or,
for bacteriological
laboratories,
Public
Health;
or, for radiological
849
laboratories,
the Illinois
Department
of
Nuclear Safety. The
true value
of
the
850
concentration
of the reference
material is
unknown to
the
laboratory at the time
of
851
the
analysis.
852
853
“Person”
means an individual,
corporation,
company, association,
partnership,
854
state, unit of
local
government,
or federal
agency.
855
856
“Phase I” refers to that
group
of chemical
contaminants
and the
accompanying
857
regulations promulgated
by USEPA
on July 8, 1987,
at 52 Fed. Reg. 25712.
858
859
“Phase II” refers
to that group
of chemical contaminants
and the
accompanying
JCAR35O61
1-0815204r01
860
regulations
promulgated by USEPA
on January
30, 1991,
at 56 Fed. Reg. 3578.
861
862
“Phase JiB”
refers to that group
of chemical contaminants
and the accompanying
863
regulations
promulgated by
USEPA on
July
1, 1991, at 56 Fed.
Reg. 30266.
864
865
“Phase
V” refers to that group
of chemical
contaminants
promulgated
by USEPA
866
on
July 17,
1992,
at 57
Fed. Reg. 31776.
867
868
“Picocurie”
or “pCi” means
the
quantity
of radioactive
material producing
2.22
869
nuclear
transformations
per minute.
870
871
“Plant
intake” means the
works or structures
at
the head
of a conduit through
872
which water
is diverted
from a source
(e.g., a river or lake)
into
the treatment
873
plant.
874
875
“Point
of disinfectant application”
is the point
at which the
disinfectant is applied
876
and downstream
of
which
water is not subject
to recontamination
by
surface
water
877
runoff.
878
879
“Point-of-entry
treatment device”
or “POE”
is a treatment
device applied to
the
880
drinking
water entering
a house or
building
for the purpose
of reducing
881
contaminants
in the
drinking water distributed
throughout
the house
or building.
882
883
“Point-of-use treatment
device”
or “POU” is a treatment
device applied
to a
single
884
tap
used for the
purpose of reducing
contaminants
in drinking
water
at that one
885
tap.
886
887
“Presedimentation”
means a preliminary
treatment
process used to remove
gravel,
888
sand,
and
other
particulate material
from the source
water through
settling before
889
the water enters the
primary
clarification
and filtration
processes in
a treatment
890
plant.
891
892
“Public
Health” or “DPH”
means the
Illinois Department
of Public Health.
893
BOARD
NOTE:
The
Department
of Public Health (“Public
Health”)
regulates
894
non-community
water
supplies (“non-C
WSs,” including
non-transient, non-
895
community
water
supplies
(“NTNCWSs”)
and transient
non-community
water
896
supplies
(“transient
non-CWSs”)). For
the purposes
of regulation of supplies
by
897
Public Health by reference
to this
Part, “Agency” must
mean Public
Health.
898
899
“Public water system”
or “PWS”
means a
system
for the provision to
the
public of
900
water for human
consumption
through pipes or
other constructed
conveyances,
if
901
such
system
has at least 15 service
connections
or regularly
serves an average
of
902
at least 25 individuals
daily
at least
60
days
out of the year. A PWS
is either
a
JCAR35O61
1-0815204r01
903
community
water
system (CWS)
or a non-community
water system
(non-CWS).
904
A PWS
does
not
include any
facility
defined
as “special
irrigation
district.”
Such
905
term
includes
the following:
906
907
Any collection,
treatment,
storage,
and
distribution
facilities
under control
908
of the operator
of such
system
and
used
primarily
in
connection
with
such
909
system;
and
910
911
Any collection
or
pretreatment
storage
facilities not
under such
control
912
that
are used primarily
in
connection
with such
system.
913
914
BOARD
NOTE:
Where
used in
Subpart
F of
this Part,
“public
water
supply”
915
means
the same
as “public
water system.”
916
917
“Radioactive
contaminants”
refers to
that group
of
contaminants
designated
918
“radioactive
contaminants”
in
USEPA
regulatory
discussions
and guidance
919
documents.
“Radioactive
contaminants”
include
tritium,
strontium-89,
strontium-
920
90,
iodine-131,
cesium-134,
gross beta
emitters,
and other nuclides.
921
BOARD
NOTE:
Derived
from
40
CFR
141.25(c)
Table B
(2007)(2006).
These
922
radioactive
contaminants
must
be reported
in Consumer
Confidence
Reports
923
under
Subpart
U
of this Part
when they
are detected
above
the levels
indicated
in
924
Section
611.720(c)(3).
925
926
“Reliably
and
consistently”
below
a specified
level
for a
contaminant
means
an
927
Agency
determination
based
on
analytical
results following
the
initial detection
of
928
a
contaminant
to determine
the
qualitative
condition
of
water from
an
individual
929
sampling
point or source.
The
Agency must
base this
determination
on the
930
consistency
of analytical
results,
the
degree
below
the MCL,
the
susceptibility
of
931
source
water
to variation,
and
other
vulnerability
factors
pertinent
to the
932
contaminant
detected
that may
influence
the
quality
of
water.
933
BOARI) NOTE:
Derived
from
40
CFR 141.23(b)(9),
141.24(f)(11)(ii),
and
934
141.24(f)(1
1)(iii) (2007)(2006).
935
936
“Rem”
means
the unit
of dose equivalent
from
ionizing
radiation to
the total body
937
or any
internal
organ
or organ
system.
A
“millirem
(mrem)”
is 1/1000
of
a
rem.
938
939
“Repeat
compliance
period”
means
a compliance
period
that
begins
after the
940
initial
compliance
period.
941
942
“Representative”
means
that a
sample must
reflect
the
quality
of
water that
is
943
delivered
to consumers
under
conditions
when
all
sources
required
to supply
944
water under
normal
conditions
are in use
and all treatment
is properly
operating.
945
JCAR35O61 1-0815204r01
946
“Residual disinfectant concentration”
(“RDC” or
“C”
in CT calculations) means
947
the concentration of disinfectant measured in mg! in a representative sample
of
948
water. For purposes
of
the requirement
of Section 611.241(d) of maintaining a
949
detectable RDC in the distribution system, “RDC”
means a
residual
of free or
950
combined chlorine.
951
952
“Safe Drinking Water Act” or “SDWA”
means the Public Health Service Act, as
953
amended by the Safe Drinking Water Act, Pub. L. 93-523, 42
USC
300f et
seq.
954
955
“Sanitary survey” means an onsite review of the delineated WHPAs (identifying
956
sources of contamination within
the WHPAs and evaluations or the hydrogeologic
957
sensitivity of the delineated WHPAs conducted under source water assessments
or
958
utilizing other relevant information where available),
facilities, equipment,
959
operation, maintenance, and monitoring compliance of a public water system
960
(PWS) to evaluate the adequacy of the system, its sources, and operations
for the
961
production and distribution
of
safe
drinking water.
962
BOARD NOTE: Derived from 40 CFR 141.2 (2006) and 40 CFR 142.16(o)(2)
963
(2007),
as added
at
71 Fed. Reg. 65574
(Nov. 8,
2006).
964
965
“Sedimentation” means a process for removal of solids before filtration by gravity
966
or
separation.
967
968
“SEP” means special exception permit (Section 611.110).
969
970
“Service connection,” as used in the definition
of public water
system,
does not
971
include a connection to a system that delivers water by a constructed conveyance
972
other
than a pipe
if any of
the following
is true:
973
974
The water is used exclusively
for purposes other than
residential
use
975
(consisting of drinking, bathing, and cooking, or other similar uses);
976
977
The Agency determines
by
issuing
a SEP that alternative water for
978
residential use or similar uses for drinking and cooking is provided to
979
achieve the equivalent level of public health
protection
provided
by the
980
applicable
national primary drinking water regulations; or
981
982
The Agency determines by issuing a SEP that the water provided for
983
residential
use or similar uses for drinking, cooking, and bathing is
984
centrally treated or treated at the point
of entry by the
provider,
a pass
985
through entity, or the user to achieve the equivalent level of protection
986
provided
by the applicable national primary drinking water regulations.
987
BOARD NOTE: See sections
1401(4)(B)(i)(II) and (4)(B)(i)(III) of SDWA (42
988
USC
300f(4)(B)(i)(II) and (4)(B)(i)(III) (2000)).
JCAR35O61
1-0815204r01
989
990
“Significant
deficiency” means a
deficiency identified
by the
Agency in a
991
groundwater system
pursuant
to Section
611.803.
A significant
deficiency might
992
include, but
is not limited
to, a defect in
system design, operation,
or
maintenance
993
or a failure
or malfunction of
the
sources,
treatment, storage,
or distribution
994
system
that the Agency
determines
to
be causing or have
potential for causing
the
995
introduction
of contamination
into the water
delivered
to consumers.
996
BOARD
NOTE: Derived
from 40 CFR
142.16(o)(2)(iv)
(2007), as added
at 71
997
Fed. Reg.
65574
(Nov.
8, 2006). The
Agency must submit
to USEPA
a definition
998
and
description of at least
one significant
deficiency
in each of the eight
sanitary
999
survey
elements listed
in Section
611.801(c) as part of
the
federal primacy
1000
requirements.
The Board
added
the general
description
of what a significant
1001
deficiency
might include
in non-limiting
terms, in order
to provide
this
important
1002
definition
within the body
of the
Illinois
rules. No Agency
submission to
USEPA
1003
can provide
definition within
the context
of Board
regulations.
1004
1005
“Slow
sand filtration” means
a process involving
passage
of raw water through
a
1006
bed of sand
at low velocity
(generally
less than 0.4 meters
per
hour (mlh))
1007
resulting
in substantial
particulate removal
by
physical
and biological
1008
mechanisms.
1009
1010
“SOC”
or “Synthetic
organic chemical
contaminant”
refers to that
group of
1011
contaminants designated
as “SOCs,”
or “synthetic
organic chemicals”
or
1012
“synthetic organic
contaminants,”
in USEPA regulatory
discussions
and guidance
1013
documents.
“SOCs” include alachlor,
aldicarb,
aldicarb sulfone,
aldicarb
1014
sulfoxide, atrazine,
benzo(a)pyrene,
carbofuran,
chlordane, dalapon,
1015
dibromoethylene
(ethylene dibromide
or EDB),
dibromochloropropane
(DBCP),
1016
di(2-ethylhexyl)adipate,
di(2-ethylhexyl)phthalate,
dinoseb, diquat,
endothall,
1017
endrin, glyphosate,
heptachlor, heptachlor
epoxide,
hexachlorobenzene,
1018
hexachlorocyclopentadiene,
lindane,
methoxychlor,
oxamyl,
pentachiorophenol,
1019
picloram, simazine,
toxaphene, polychlorinated
biphenyls (PCBs), 2,4-D,
2,3,7,8-
1020
TCDD,
and
2,4,5-TP.
1021
BOARD NOTE: See
the
Board note
appended to
Section 611.3 11 for
1022
information
relating
to implementation
of requirements
relating to
aldicarb,
1023
aldicarb sulfone, and
aldicarb
sulfoxide.
1024
1025
“Source” means a well,
reservoir,
or other source
of raw water.
1026
1027
“Special irrigation
district” means
an irrigation
district in existence
prior to May
1028
18,
1994
that provides
primarily
agricultural
service through a piped
water
system
1029
with only
incidental
residential
use or similar
use, where
the
system or the
1030
residential users
or similar users
of the system
comply with
either of the following
1031
exclusion conditions:
JCAR35O61 1-0815204r01
1032
1033
The Agency determines
by issuing a SEP that alternative
water is
1034
provided for residential use or similar
uses for drinking or cooking
to
1035
achieve
the equivalent level of public health
protection provided by the
1036
applicable national primary
drinking water regulations;
or
1037
1038
The Agency determines by issuing a
SEP that the water provided for
1039
residential use
or
similar
uses for drinking, cooking,
and bathing is
1040
centrally treated or treated at the
point of entry by the provider, a
pass-
1041
through entity,
or the user to achieve the equivalent
level of protection
1042
provided by the applicable national
primary drinking water regulations.
1043
BOARD NOTE: Derived
from
40
CFR 141.2 (2007)(2006)
and sections
1044
1401(4)(B)(i)(II)
and (4)(B)(i)(III) of SDWA (42
USC 300f(4)(B)(i)(II) and
1045
(4)(B)(i)(III) (2007)(2000)).
1046
1047
“Standard monitoring” means the monitoring,
performed by the supplier pursuant
1048
to Section 611.921(a) and
(b), at various specified locations
in a distribution
1049
system including near entry points, at points
that represent the average residence
1050
time in the distribution system,
and at points in the distribution
system that are
1051
representative of high TTHM and
HAA5 concentrations throughout the
1052
distribution system.
1053
BOARD NOTE: Derived
from 40 CFR 141.601(a)
and (b) (2007)(2006).
1054
1055
“Standard sample” means the aliquot
of finished drinking water that is examined
1056
for the
presence
of coliform bacteria.
1057
1058
“Subpart B system” means a public water
system that uses surface water or
1059
groundwater under the direct
influence of surface water
as a source and which is
1060
subject to
the
requirements of Subpart
B of this Part and the analytical and
1061
monitoringrequirements of
Sections 611.531, 611.532, 611.533,
Appendix B of
1062
this Part, and Appendix
C
of this Part.
1063
1064
“Subpart I compliance monitoring”
means monitoring required
to demonstrate
1065
compliance
with disinfectant residuals, disinfection
byproducts, and disinfection
1066
byproduct precursors requirements
of Subpart I of this Part.
1067
1068
“Subpart I system” means
a public water system that
uses surface water or
1069
groundwater as a source and which
is subject to the disinfectant residuals,
1070
disinfection
byproducts, and disinfection
byproduct precursors requirements
of
1071
Subpart I of this Part.
1072
JCAR35O61 1-0815204r01
1073
“Subpart
Y
compliance monitoring” means monitoring
required to demonstrate
1074
compliance with Stage 2 disinfection
byproducts requirements of Subpart
Y of
1075
this Part.
1076
1077
“Supplier of water” or “supplier”
means any person who owns or operates a
public
1078
water system (PWS). This term includes the “official
custodian.”
1079
1080
“Surface water” means all water
that is open to the atmosphere and subject
to
1081
surface runoff.
1082
1083
“SUVA” means specific ultraviolet absorption at 254
nanometers (nm), which is
1084
an indicator of the humic content
of water. It is a calculated parameter obtained
1085
by
dividing
a
sample’s ultraviolet
absorption at a wavelength
of
254
nm (UV
254)
1086
(in m’) by its concentration of dissolved organic carbon
(in mg/e).
1087
1088
“SWS” means
“surface
water system,” a public water supply
(PWS) that uses only
1089
surface water sources, including “groundwater
under the direct influence of
1090
surface water.”
1091
BOARD NOTE: Derived from 40
CFR
141.23(b)(2)
and
141.24(0(2)
note
1092
(2007)(2006).
1093
1094
“System-specific study plan”
means the plan, submitted by the supplier to
the
1095
Agency pursuant to Section 611.922,
for studying the occurrence of TTHM
and
1096
HAA5 in a supplier’s distribution system based on either
monitoring results or
1097
modelling of
the
system.
1098
BOARD NOTE: Derived from 40
CFR
141.602
(2007)(2006).
1099
1100
“System with a single service connection”
means a system that supplies drinking
1101
water to
consumers via
a single service line.
1102
1103
“Too numerous to count” means
that the total number of bacterial colonies
1104
exceeds 200 on a
47-mm
diameter membrane filter used for coliform
detection.
1105
1106
“Total organic carbon”
or “TOC” means total organic carbon (in
mg/f?)
measured
1107
using heat, oxygen, ultraviolet irradiation, chemical
oxidants, or combinations
of
1108
these oxidants that convert
organic carbon to carbon dioxide, rounded
to
two
1109
significant figures.
1110
1111
“Total trihalomethanes”
or “TTHM” means the sum of the concentration
of
1112
trihalomethanes (THMs), in milligrams
per liter (mg/f?), rounded to two
1113
significant figures.
1114
BOARD NOTE: See
the definition of” trihalomethanes”
for
a listing
of the four
1115
compounds that
US
EPA considers
TTHMs to comprise.
JCAR35O61
1-0815204r01
1116
1117
“Transient,
non-community
water system”
or
“transient
non-CWS” means a
non-
1118
CWS
that does not regularly
serve at
least 25 of the same
persons over six
months
1119
oftheyear.
1120
BOARD
NOTE:
The federal regulations
apply
to
all “public water systems,”
1121
which are defined as
all
systems
that have at least 15
service connections
or which
1122
regularly serve
water to at least 25
persons. (See 42
USC 300f(4).)
The Act
1123
mandates that
the Board and the
Agency regulate
“public water supplies,”
which
1124
it defines as having
at least 15
service connections
or
regularly
serving 25 persons
1125
daily at least
60 days per year. (See
Section
3.28
of the Act [415 ILCS
5/3.28].)
1126
The Department
of Public
Health
regulates transient,
non-community
water
1127
systems.
1128
1129
“Treatment” means
any process that
changes the physical,
chemical,
1130
microbiological,
or radiological properties
of water,
is under the control
of the
1131
supplier, and is not
a point-of-use
treatment device or a
point-of-entry
treatment
1132
device
as defined
in this Section. Treatment
includes,
but is not limited
to,
1133
aeration, coagulation,
sedimentation,
filtration, activated
carbon
treatment,
1134
disinfection,
and
fluoridation.
1135
1136
“Trihalomethane”
or “THM”
means one of the family
of organic compounds,
1137
named as derivatives
of methane,
in which
three
of the four hydrogen
atoms
in
1138
methane are each
substituted
by a halogen atom
in the molecular
structure.
The
1139
THMs are the
following
compounds:
1140
1141
Trichloromethane
(chloroform),
1142
Dibromochloromethane,
1143
Bromodichioromethane,
and
1144
Tribromomethane
(bromofonn)
1145
1146
“Two-stage
lime softening” means
a
process
in which chemical
addition and
1147
hardness precipitation
occur
in each of two distinct
unit clarification
processes in
1148
series prior to filtration.
1149
1150
“pg”
means micrograms
(1/1,000,000
of a gram).
1151
1152
“USEPA” means
the
U.S.
Environmental
Protection Agency.
1153
1154
“Uncovered
finished water
storage facility”
is a tank, reservoir,
or other facility
1155
that is used
to
store water
which will
undergo no further treatment
to reduce
1156
microbial
pathogens
except residual disinfection
and which
is directly open to
the
1157
atmosphere.
1158
JCAR35O61 1-0815204r01
1159
“Very small system waiver” means the conditional waiver from the requirements
1160
of Subpart W of
this Part applicable
to a supplier that serves
fewer than 500
1161
persons
and which has taken TTHM and HAA5 samples pursuant to Subpart
I
of
1162
this Part.
1163
BOARD
NOTE: Derived
from
40
CFR
141.604 (2007)(2006).
1164
1165
“Virus” means a virus of fecal origin that is infectious to humans by waterborne
1166
transmission.
1167
1168
“VOC”
or “volatile organic chemical contaminant” refers to that group of
1169
contaminants designated as “VOCs,” “volatile organic chemicals,” or “volatile
1170
organic
contaminants,”
in USEPA regulatory discussions and guidance
1171
documents. “VOCs” include benzene, dichioromethane, tetrachioromethane
1172
(carbon
tetrachioride), trichioroethylene, vinyl chloride, 1,1,1 -trichloroethane
1173
(methyl chloroform), 1,1 -dichioroethylene, 1 ,2-dichloroethane, cis-
1,2-
1174
dichioroethylene, ethylbenzene, monochlorobenzene, o-dichlorobenzene, styrene,
1175
1 ,2,4-trichlorobenzene, 1,1 ,2-trichloroethane,
tetrachioroethylene, toluene, trans..
1176
1
,2-dichloroethylene, xylene, and 1 ,2-dichloropropane.
1177
1178
“Waterbome
disease outbreak” means the significant occurrence of acute
1179
infectious illness, epidemiologically associated with the ingestion of water from a
1180
public water system (PWS) that is deficient in treatment, as determined by the
1181
appropriate local or State agency.
1182
1183
“Welihead protection area” or “WHPA” means the surface and subsurface
1184
recharge area surrounding a community water supply well or
well field,
1185
delineated outside of any applicable setback zones (pursuant to Section
1186
17J1-7-2 of the Act {415 ILCS
5/17.15/17.2)1)
pursuant to
Illinois’
1187
Wellhead Protection Program, through which contaminants are reasonably
1188
likely to
move toward
such well or
well
field.
1189
BOARD NOTE: The Agency uses two guidance documents for
1190
identification of WHPAs:
1191
1192
“Guidance Document for Groundwater Protection Needs Assessments,”
1193
Illinois Environmental Protection
Agency,
Illinois State Water Survey,
1194
and Illinois State Geologic Survey joint report, January 1995; and
1195
1196
“The Illinois Wellhead Protection Program Pursuant to Section 1428 of
1197
the Federal Safe Drinking Water Act,” Illinois Environmental Protection
1198
Agency, No.
22480,
October 1992.
1199
1200
“Welihead protection program” means the welihead protection program for the
1201
State of Illinois, approved by USEPA under Section 1428 of the
SDWA, 42
USC
JCAR35O61 1-0815204r01
1202
300h-7.
1203
BOARD NOTE: Derived from 40 CFR 141.71(b) (2007)(2006). The welihead
1204
protection program includes the “groundwater
protection needs assessment” under
1205
Section 17.1 of the Act [415 ILCS 5/17.1] and 35111. Adm.
Code
615-617.
1206
1207
“Wholesale system”
means a
public water
system that treats source water as
1208
necessary to produce finished water, which then
delivers some or all of that
1209
finished water to another public water system. Delivery
by
a wholesale
system
1210
may be through a direct connection or through
the distribution system of one or
1211
more consecutive systems.
1212
1213
BOARD NOTE: Derived from
40
CFR
141.2 (2007)(2006).
1214
1215
(Source: Amended at
33
Ill.
Reg.
effective
1216
1217
Section 611.102 Incorporations
by
Reference
1218
1219
a)
Abbreviations and short-name listing
of
references.
The following names and
1220
abbreviated names, presented in alphabetical order, are used in this Part to refer
to
1221
materials incorporated
by
reference:
1222
1223
“ASTM Method” means a method published
by
and available
from the
1224
American Society for Testing and Materials (ASTM).
1225
1226
“Colisure Test” means “Colisure
Presence/Absence Test for Detection and
1227
Identification of Coliform Bacteria and Escherichia Coli in Drinking
1228
Water,” available from Millipore
Corporation, Technical Services
1229
Department.
1230
1231
“Colitag®
Test” means “Colitag® Product as a Test for Detection and
1232
Identification
of Coliforms and E. coli Bacteria in Drinking Water and
1233
Source Water as Required in National Primary Drinking Water
1234
Regulations,” available from CPI
International.
1235
1236
“Determination of Inorganic Oxyhalide”
means
“Determination
of
1237
Inorganic
Oxyhalide Disinfection By-Products in Drinking Water Using
1238
Ion Chromatography with the
Addition of a Postcolumn Reagent for Trace
1239
Bromate Analysis,” available from NTIS.
1240
1241
“Dioxin and Furan Method
1613” means “Tetra- through Octa-Chlorinated
1242
Dioxins and Furans by Isotope-Dilution
HRGC/HRMS,”
available from
1243
NTIS.
1244
JCAR35O61
1-0815204r01
1245
t
E*Colite
Test”
means “Charm
E*Colite
Presence/Absence
Test for
1246
Detection and Identification
of Coliform Bacteria and Escherichia coli
in
1247
Drinking Water,” available from
Charm
Sciences,
Inc. and USEPA, Water
1248
Resource Center.
1249
1250
“EC-MUG” means “Method 9221
F: Multiple-Tube Fermentation
1251
Technique
for Members of the Coliform Group, Escherichia
coli
1252
Procedure (Proposed),” available
from American Public Health
1253
Association and American Waterworks
Association.
1254
1255
“Enterolert” means “Evaluation
of
Enterolert
for Enumeration of
1256
Enterococci in Recreational
Waters,” available from American Society
for
1257
Microbiology.
1258
1259
“Georgia Radium
Method” means “The Determination of Radium-226
and
1260
Radium-228 in Drinking Water
by
Gamma-ray
Spectrometry Using HPGE
1261
or
Ge(Li)
Detectors,”
Revision 1.2, December 2004, available from
the
1262
Environmental Resources Center, Georgia Institute
of Technology.
1263
1264
“GLI Method 2” means GLI
Method
2,
“Turbidity,” Nov. 2, 1992,
1265
available from Great Lakes Instruments, Inc.
1266
1267
“Hach FilterTrak
Method 10133” means “Determination of Turbidity
by
1268
Laser Nephelometry,” available
from Hach Co.
1269
1270
“HASL Procedure
Manual” means HASL Procedure Manual, HASL
300,
1271
available from ERDA Health and Safety Laboratory.
1272
1273
“ITS Method D99-003” means Method D99-003, Revision
3.0, “Free
1274
Chlorine Species
(HOCF
and
OCR
by Test Strip,” available from
1275
Industrial
Test Systems, Inc.
1276
1277
“Kelada 01” means
“Kelada Automated Test Methods for Total Cyanide,
1278
Acid Dissociable Cyanide, And Thiocyanate,” Revision 1.2,
August 2001,
1279
EPA 8211B-0l/009, available
from the National Technical Information
1280
Service (NTIS).
1281
1282
“m-ColiBlue24 Test” means
“Total Coliforms and E. coli Membrane
1283
Filtration
Method with m-ColiBlue24® Broth,” available
from Hach
1284
Company and USEPA,
Water Resource Center.
1285
1286
“Membrane Filter Technique using
Chromocult Doliform Agar” means
1287
“Chromocult Coliform
Agar Presence/Absence Membrane Filter
Test
JCAR35O61
1-0815204r01
1288
Method for Detection and Identification of Coliform Bacteria
and
1289
Escherichia coli in Finished Waters,” available from EMD Chemicals Inc.
1290
1291
“NA-MUG” means “Method
9222
G:
Membrane Filter Technique for
1292
Members of the Coliform Group, MF Partition Procedures,” available
1293
from American Public Health Association and American Waterworks
1294
Association.
1295
1296
“NCRP” means “National Council on Radiation Protection.”
1297
1298
“NTIS” means “National Technical Infonnation Service.”
1299
1300
“New Jersey Radium Method” means
“Determination
of
Radium 228 in
1301
Drinking Water,” available from the New Jersey Department of
1302
Environmental Protection.
1303
1304
“New York Radium Method” means “Determination of Ra-226 and Ra
1305
228 (Ra-02),” available from the New York Department of
Public
Health.
1306
1307
“01 Analytical Method OIA-1677” means “Method OIA-1677, DW
1308
Available Cyanide by Flow
Injection,
Ligand Exchange, and
1309
Amperometry,” available from
ALPKEM, Division of 01 Analytical.
1310
1311
“ONPG-MUG Test” (meaning “minimal medium ortho-nitrophenyl-beta
1312
d-galactopyranoside-4-methyl-umbelliferyl
-beta-d-glucuronide test”),
1313
also called
the “Autoanalysis Colilert System,” is Method 9223, available
1314
in “Standard Methods for the Examination of Water and
Wastewater,”
1315
18
th
19
th 20
th
or
21st
ed., from American Public Health Association and
1316
the American Water Works Association.
1317
1318
“Palintest Method 1001” means “Method
Number 1001,” available from
1319
Palintest, Ltd. or the Hach Company.
1320
1321
“QuikChem Method 10-204-00-1-X” means “Digestion and
distillation
of
1322
total
cyanide in drinking and wastewaters using MICRO DIST and
1323
determination of cyanide by flow injection analysis,”
available from
1324
Lachat
Instruments.
1325
1326
“Readycult Coliforms 100 Presence/Absence Test” means
“Readycult
1327
Coliforms
100 Presence/Absence
Test for
Detection and Identification of
1328
Coliform Bacteria and Escherichia coli in Finished Waters,” available
1329
from EMD Chemicals Inc.
1330
JCAR35O61
1-0815204r01
1331
“SimPlate
Method!!
means “LDEXX
SimPlate
TM HPC Test Method
for
1332
Heterotrophs
in Water,”
available
from IDEXX
Laboratories,
Inc.
1333
1334
“Radiochemical
Methods”
means “Interim Radiochemical
Methodology
1335
for Drinking
Water,”
available from NTIS.
1336
1337
“Standard
Methods”
means “Standard
Methods for the Examination
of
1338
Water
and Wastewater,”
available from
the American
Public Health
1339
Association or the American
Waterworks
Association.
1340
1341
“Standard
Methods
Online!!
means
the website maintained
by
the
Standard
1342
Methods
Organization
(at
www.standardmethods.org)
for purchase of
the
1343
latest versions
of methods
in an electronic
format.
1344
1345
“Syngenta
AG-625”
means “Atrazine in Drinking
Water
by
1346
Immunoassay,”
February
2001
is available
from Syngenta Crop
1347
Protection,
Inc.
1348
1349
“Technical
Bulletin
601”
means “Technical
Bulletin
601,
Standard
1350
Method
of Testing for
Nitrate in Drinking
Water,” July 1994,
available
1351
from
Analytical
Technology,
Inc.
1352
1353
“Technical Notes on
Drinking Water
Methods” means the
USEPA
1354
document by that
title,
October
1994,
USEPA document
number
EPA
1355
600/R-94/173,
available from NTIS.
1356
1357
“Technicon
Methods” means
“Fluoride in Water
and Wastewater,”
1358
available from Bran
& Luebbe.
1359
1360
“USDOE Manual”
means
“EML
Procedures Manual,”
available
from the
1361
United State Department
of Energy.
1362
1363
“USEPA Asbestos
Methods-100.1”
means Method 100.1,
“Analytical
1364
Method
for Determination
of Asbestos
Fibers in Water,”
September
1983,
1365
available from NTIS.
1366
1367
“USEPA Asbestos
Methods-100.2”
means Method 100.2,
“Determination
1368
of Asbestos Structures
over 10-mm
in Length in Drinking
Water,”
June
1369
1994, available from
NTIS.
1370
1371
“USEPA Environmental
Inorganics Methods” means
“Methods
for the
1372
Determination
of Inorganic
Substances in Environmental
Samples,”
1373
August 1993,
available
from
NTIS.
JCAR35O61
1-0815204r01
1374
1375
“USEPA
Environmental
Metals
Methods”
means
“Methods for
the
1376
Determination
of Metals
in Environmental
Samples,”
available
from
1377
NTIS.
1378
1379
“USEPA
Inorganic
Methods”
means
“Methods
for
Chemical
Analysis
of
1380
Water
and
Wastes,”
March
1983, available
from
NTIS.
1381
1382
“USEPA
Interim
Radiochemical
Methods”
means
“Interim
Radiochemical
1383
Methodology
for Drinking
Water,”
EPA 600/4-75/008
(revised),
March
1384
1976.
Available
from
NTIS.
1385
1386
“USEPA
Method
1600”
means
“Method
1600:
Enterococci
in Water
by
1387
Membrane
Filtration
Using
Membrane-Enterococcus
Indoxyl-b-D
1388
Glucoside
Agar
(mET),” available
from
USEPA,
Water Resource
Center.
1389
1390
“USEPA
Method
1601” means
“Method
1601:
Male-specific
(Fj and
1391
Somatic
Coliphage
in
Water
by Two-step
Enrichment
Procedure,”
1392
available
from
USEPA, Water
Resource
Center.
1393
1394
“USEPA
Method
1602”
means
“Method
1602:
Male-specific
(F) and
1395
Somatic
Coliphage
in
Water
by Single
Agar Layer
(SAL)
Procedure,”
1396
available from
USEPA,
Water Resource
Center.
1397
1398
“USEPA Method
1604”
means “Method
1604:
Total Coliforms
and
1399
Escherichia
coli in
Water by Membrane
Filtration
Using
a Simultaneous
1400
Detection
Technique
(MI
Medium),”
available
from
USEPA,
Water
1401
Resource
Center.
1402
1403
“USEPA
NERL Method
200.5
(rev.
4.2)”
means
Method
200.5,
Revision
1404
4.2, “Determination
of
Trace Elements
in Drinking
Water
by Axially
1405
Viewed
Inductively-Coupled Plasma
— Atomic
Emission
Spectrometry,”
1406
October 2003,
EPA 600/R-06/1
15.
Available
from USEPA,
Office
of
1407
Research
and
Development.
1408
1409
“USEPA
Method
1622
(05)” means
“Method
1622: Ctosporidium
in
1410
Water
by Filtratiom’IMS/FA,”
December
2005,
available
from USEPA,
1411
Office
of Ground
Water
and Drinking
Water.
1412
1413
“USEPA
Method 1622
(01)” means
“Method
1622:
Cryytosporidium
in
1414
Water
by FiltrationiiMS/FA,”
April
2001,
available
from
USEPA,
Office
1415
of Ground
Water
and
Drinking
Water.
1416
1445
1446
1447
1448
1449
1450
1451
1452
1453
1454
1455
1456
1457
1458
JCAR35O61 1-0815204r01
“USEPA Method 1622
(99)” means “Method 1622: Crtosporidium
in
Water by FiltrationilMS/FA,” January
1999,
available
from USEPA,
Office
of
Ground
Water and Drinking Water.
“USEPA Method 1623 (05)” means “Method 1623:
Crtosporidium
and
Giardia in
Water by Fi1tration’DS/FA,” December 2005,
available from
the USEPA, Office of Ground
Water and Drinking Water.
r,r;\
A KL.-1
‘.‘ir, II U
1
n/
fC1i
I)
iri;,ji “1{efhnc1 1 621
rntnnnric1um
nnrl
Giardia in
1rby
FiltrationifMS,PA,”
April2001, available from
USEPA, Office
of Ground Water and Drinking Water.
“USEPA Method 1623
(99)” means “Method 1623: Crtosporidium
and
Giardia in Water
by Filtratiom{S!FA,” April 1999, available
from the
USEPA, Office of Ground Water
and Drinking Water.
“USEPA NERL Method 415.3 (rev. 1.1)”
means Method 415.3, Revision
1.1, “Determination
of Total Organic Carbon and Specific
UV Absorbance
at 254 nm in Source Water and
Drinking Water,” USEPA, February 2005,
EPA 600/R-05/055. Available from the USEPA,
Office of Research and
Development.
“USEPA OGWDW Methods” means
one of the methods listed as
available
from the USEPA, Office of Ground Water and
Drinking Water
(Methods 317.0 (rev. 2.0),
326.0 (rev. 1.0), 327.0 (rev. 1.1), 515.4
(rev.
1.0), 531.2 (rev. 1.0), and-552.3 (rev.
1.0),
1622
(99),
1622
(01), 1622
(05),
1623
(99),
1623
(01).
and 1623 (05)).
1417
1418
1419
1420
1421
1422
1423
1424
1425
1426
1427
1428
1429
1430
1431
1432
1433
1434
1435
1436
1437
1438
1439
1440
1441
1442
1443
1444
“USEPA Organic
Methods” means “Methods for the Determination
of
Organic Compounds in Drinking Water,”
July 1991, for Methods 502.2,
505, 507, 508, 508A, 515.1,
and 531.1; “Methods for the Determination
of
Organic Compounds
in Drinking Water — Supplement I,” July
1990, for
Methods 506, 547, 550, 550.1, and
551; “Methods for the Determination
of Organic Compounds
in Drinking Water — Supplement II,” August
1992, for Methods 504.1, 508.1, 515.2, 524.2, 525.2, 548.1,
549.1, 552.1,
552.2, and 555; and
“Methods for the Determination of Organic
Compounds in Drinking Water
— Supplement III,” August 1995, for
Methods 502.2, 524.2,
551.1, and 552.2. Method 515.4,
“Determination
of Chlorinated Acids
in Drinking Water by Liquid Liquid
Microextraction, Derivatization
and Fast Gas Comatography with
Electron Capture
Detection,” Revision 1.0, April 2000,
EPA 815
00/00 1, and Method
531.2, “Measurement of
N
methylcarbamoyloximes
1459
and N methylcarbamates in
Water by Direct Aqueous Injection HPLC
JCAR35O61 1-0815204r01
1460
with Postcolumn
Derivatization,”
Revision
1.0, September
2001, EPA
1461
815/B
01/002, are
both
available
on line
from USEPA,
Office of Ground
1462
Water
and Drinking
Water.
1463
1464
“USEPA Organic
and Inorganic Methods”
means “Methods
for the
1465
Determination
of
Organic and
Inorganic Compounds
in Drinking
Water,
1466
Volume
1,”
EPA 815/R-00/014, PB2000-106981,
August 2000. Available
1467
from NTIS.
1468
1469
“USEPA
Radioactivity Methods”
means “Prescribed
Procedures
for
1470
Measurement
of Radioactivity in Drinking
Water,”
EPA 600/4-80/032,
1471
August 1980. Available
from
NTIS.
1472
1473
“USEPA Radiochemical
Analyses”
means “Radiochemical
Analytical
1474
Procedures
for
Analysis of Environmental
Samples,”
March 1979.
1475
Available
from NTIS.
1476
1477
“USEPA Radiochemistry
Methods”
means “Radiochemistry
Procedures
1478
Manual,” EPA 520/5-84/006,
December
1987. Available
from NTIS.
1479
1480
“USEPA Technical
Notes” means
“Technical
Notes
on Drinking Water
1481
Methods,” available
from NTIS.
1482
1483
“USGS
Methods” means “Methods
of Analysis
by the
U.S.
Geological
1484
Survey National
Water Quality
Laboratory
— Determination
of Inorganic
1485
and Organic
Constituents
in Water and Fluvial
Sediments,”
available from
1486
NTIS
andUSGS.
1487
1488
“Waters
Method B-101 1”
means “Waters
Test Method for the
1489
Determination
of Nitrite/Nitrate
in Water Using
Single Column
Ion
1490
Chromatography,”
available
from Waters
Corporation, Technical
Services
1491
Division.
1492
1493
b)
The
Board incorporates
the following
publications
by reference:
1494
1495
ALPKEM,
Division of 01 Analytical,
P.O.
Box 9010, College Station,
TX
1496
77842-9010,
telephone:
979-690-1711,
Internet:
www.oico.com.
1497
1498
“Method
OIA-1677
DW, Available
Cyanide by Flow
Injection,
1499
Ligand
Exchange,
and Amperometry,”
EPA 821/R-04/001,
1500
January
2004 (referred
to as “01
Analytical Method OIA-1677”),
1501
referenced
in
Section 611.611.
JCAR35O61 1-0815204r01
1502
BOARD NOTE:
Also available online
for download from
1503
www.epa.
gov/waterscience/methods/methodlcyanide/1
677-
1504
2004.pdf.
1505
1506
APHA. American Public Health
Association, 1015 Fifteenth
Street NW,
1507
Washington,
DC 20005 202-777-2742.
1508
1509
“Standard Methods for
the Examination of Water and
1510
Wastewater,”
17
th
Edition, 1989 (referred
to as “Standard Methods,
1511
17
th
ed.”). See the methods
listed separately for the
same
1512
references
under American Waterworks
Association.
1513
1514
“Standard Methods
for the Examination of
Water and
1515
Wastewater,”
18
th
Edition, 1992,
including “Supplement to the
18
th
1516
Edition of Standard
Methods for the Examination
of Water and
1517
Wastewater,”
1994 (collectively referred
to as “Standard Methods,
1518
ed.”). See the methods
listed separately for the same
1519
references
under American Waterworks
Association.
1520
1521
“Standard Methods for the Examination
of Water and
1522
Wastewater,”
Edition, 1995 (referred
to as “Standard
1523
Methods,
19
th
ed.”).
See the methods listed separately
for the
1524
same references under
American Waterworks Association.
1525
1526
“Standard
Methods for the Examination of
Water and
1527
Wastewater,”
20
th
Edition,
1998 (referred to as “Standard
Methods,
1528
20
th
ed.”).
See the methods listed
separately for the same
1529
references under
American Waterworks Association.
1530
1531
“Standard
Methods for the
Examination of Water and
1532
Wastewater,”
21
St
Edition, 2005 (referred to as “Standard
Methods,
1533
21
st
ed.”).
See the methods listed
separately for the same
1534
references under American
Waterworks Association.
1535
1536
American
Society for Microbiology,
1752 N Street
N.W.,
Washington,
1537
DC 20036, 202-737-3600:
1538
1539
“Evaluation
of Enterolert for Enumeration
of Enterococci in
1540
Recreational
Waters,” Applied and Environmental
Microbiology,
1541
Oct. 1996, vol. 62,
no. 10,
p.
3881 (referred to as “Enterolert”),
1542
referenced
in Section 611.802.
1543
JCAR35O61 1-0815204r01
1544
BOARD NOTE:
At the table to 40 CFR 141 .402(c)(2),
USEPA
1545
approved the method as described in the
above literature review.
1546
The method
itself
is embodied in the printed instructions to
the
1547
proprietary kit available
from JDEXX Laboratories, Inc.
1548
(accessible on-line and available
by
download
from www.asm.org,
1549
as
“EnterolertTM
Procedure”). ASTM approved
the method as
1550
“Standard Test
Method for Enterococci in Water Using
1551
EnterolertTM,
which
is
available in two versions
from ASTM:
1552
ASTM D 6503-99 (superceded) and ASTM D 6503-99 (2005).
1553
While it is more conventional
to incorporate the method as
1554
presented in the kit instructions or as approved by ASTM
by
1555
reference, the Board is constrained to
incorporate the version that
1556
appears in the technical
literature by reference, which is the
1557
version that USEPA has explicitly approved.
1558
1559
AWWA.
American Water Works Association et al.,
6666
West
Quincy
1560
Ave., Denver,
CO
80235 (303-794-7711).
1561
1562
“National Field Evaluation
of a Defined Substrate Method for the
1563
Simultaneous Enumeration of Total Coliforms and Escherichia
coli
1564
for Drinking Water: Comparison with the Standard Multiple
Tube
1565
Fermentation
Method,” S.C. Edberg, M.J. Allen
&
D.B. Smith,
1566
Applied Environmental
Microbiology, vol.
54,
iss. 6,
pp
1595-
1567
1601 (1988), referenced in Appendix D to this Part.
1568
1569
“Standard Methods for
the Examination of Water and
1570
Wastewater,”l
3
th
Edition, 1971 (referred to as “Standard
Methods,
1571
13thed.).
1572
1573
Method 302, Gross Alpha
and
Gross
Beta Radioactivity in
1574
Water
(Total, Suspended, and Dissolved), referenced in
1575
Section 611.720.
1576
1577
Method 303, Total Radioactive Strontium and Strontium
90
1578
in Water, referenced
in Section
611.720.
1579
1580
Method 304,
Radium in Water by Precipitation, referenced
1581
in Section 611.720.
1582
1583
Method
305, Radium 226 by Radon in Water (Soluble,
1584
Suspended, and Total),
referenced in Section 611.720.
1585
1586
Method
306, Tritium in Water, referenced in Section
JCAR35O61
1-0815204r01
1587
611.720.
1588
1589
“Standard Methods
for the Examination of
Water and
1590
Wastewater,”
17
th
Edition,
1989 (referred to as “Standard
Methods,
1591
l7thed.I?).
1592
1593
Method 7110
B, Gross Alpha and Gross Beta
Radioactivity
1594
in
Water (Total, Suspended, and
Dissolved), referenced
in
1595
Section 611.720.
1596
1597
Method
7500-Cs B, Radioactive Cesium,
Precipitation
1598
Method, referenced in Section
611.720.
1599
1600
Method
7500-
3
HB, Tritium in Water,
referenced in Section
1601
611.720.
1602
1603
Method 7500-I B, Radioactive
Iodine, Precipitation
1604
Method, referenced
in Section 611.720.
1605
1606
Method
7500-I C, Radioactive Iodine,
Ion-Exchange
1607
Method, referenced
in Section 611.720.
1608
1609
Method 7500-I D, Radioactive
Iodine, Distillation Method,
1610
referenced
in Section 611.720.
1611
1612
Method 7500-Ra B, Radium in
Water by Precipitation,
1613
referenced
in Section 611.720.
1614
1615
Method
7500-Ra C, Radium 226 by Radon in
Water
1616
(Soluble,
Suspended, and Total),
referenced in Section
1617
611.720.
1618
1619
Method 7500-Ra D, Radium,
Sequential Precipitation
1620
Method (Proposed),
referenced in Section 611.720.
1621
1622
Method 7500-Sr
B, Total Radioactive Strontium and
1623
Strontium 90 in Water, referenced
in Section 611.720.
1624
1625
Method 7500-U B,
Uranium, Radiochemical Method
1626
(Proposed), referenced in
Section 611.720.
1627
1628
Method 7500-U
C, Uranium, Isotopic Method
(Proposed),
1629
referenced
in Section 611.720.
JCAR35O61
1-0815204r01
1630
1631
“Standard
Methods for
the Examination
of
Water and
1632
Wastewater,”
18
th
Edition,
1992
(referred
to as “Standard
Methods,
1633
18thed.).
1634
1635
Method 2130
B, Turbidity,
Nephelometric
Method,
1636
referenced
in
Section
611.531.
1637
1638
Method
2320
B, Alkalinity,
Titration Method,
referenced
in
1639
Section6ll.611.
1640
1641
Method
2510
B, Conductivity,
Laboratory
Method,
1642
referenced
in
Section
611.611.
1643
1644
Method
2550,
Temperature,
Laboratory
and
Field
Methods,
1645
referenced
in
Section
611.611.
1646
1647
Method
3111
B, Metals
by Flame
Atomic
Absorption
1648
Spectrometry,
Direct Air-Acetylene
Flame Method,
1649
referenced
in Sections
611.611
and 611.612.
1650
1651
Method
3111
D,
Metals by
Flame
Atomic
Absorption
1652
Spectrometry,
Direct
Nitrous
Oxide-Acetylene
Flame
1653
Method,
referenced
in Section
611.611.
1654
1655
Method
3112 B,
Metals
by
Cold-Vapor
Atomic
Absorption
1656
Spectrometry,
Cold-Vapor
Atomic
Absorption
1657
Spectrometric
Method,
referenced
in
Section
611.611.
1658
1659
Method
3113 B,
Metals
by
Electrothermal
Atomic
1660
Absorption
Spectrometry,
Electrothermal
Atomic
1661
Absorption
Spectrometric
Method, referenced
in
Sections
1662
611.611
and 611.612.
1663
1664
Method
3114 B, Metals
by Hydride
GenerationlAtomic
1665
Absorption
Spectrometry,
Manual
Hydride
1666
GenerationlAtomic
Absorption
Spectrometric
Method,
1667
referenced
in Section
611.611.
1668
1669
Method
3120 B,
Metals
by Plasma
Emission
Spectroscopy,
1670
Inductively-Coupled
Plasma
(ICP)
Method, referenced
in
1671
Sections
611.611
and
611.612.
1672
JCAR35O61 1-0815204r01
1673
Method 3500-Ca D, Calcium, EDTA Titrimetric
Method,
1674
referenced in Section
611.611.
1675
1676
Method 3500-Mg E, Magnesium, Calculation Method,
1677
referenced in Section
611.611.
1678
1679
Method 4110 B, Determination of Anions
by
Ion
1680
Chromatography, Ion
Chromatography with Chemical
1681
Suppression of Eluent Conductivity, referenced
in Section
1682
611.611.
1683
1684
Method 4500-CN
C, Cyanide, Total Cyanide after
1685
Distillation, referenced in Section 611.611.
1686
1687
Method
4500-CN
B, Cyanide, Colorimetric Method,
1688
referenced in Section 611.611.
1689
1690
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
1691
Method, referenced
in Section 611.611.
1692
1693
Method 4500-CN
G,
Cyanide, Cyanides Amenable
to
1694
Chlorination
after Distillation, referenced in Section
1695
611.611.
1696
1697
Method 4500-Cl D, Chlorine, Amperometric Titration
1698
Method, referenced in
Section 611.53 1.
1699
1700
Method 4500-Cl E,
Chlorine, Low-Level Amperometric
1701
Titration Method, referenced in Section 611.531.
1702
1703
Method
4500-Cl
F, Chlorine, DPD Ferrous Titrimetric
1704
Method, referenced in Section
611.53 1.
1705
1706
Method 4500-Cl
G,
Chlorine, DPD Colorimetric Method,
1707
referenced in Section 611.53
1.
1708
1709
Method 4500-Cl
H, Chlorine, Syringaldazine (FACTS)
1710
Method, referenced in Section
611.53 1.
1711
1712
Method 4500-Cl
I, Chlorine, lodometric Electrode Method,
1713
referenced in Section 611.531.
1714
1715
Method 4500-Cl02
C, Chlorine Dioxide, Amperometric
JCAR35O61
1-0815204r01
1716
Method I,
referenced
in
Section 611.531.
1717
1718
Method 4500-dO2
D, Chlorine
Dioxide,
DPD Method,
1719
referenced
in Section 611.53
1.
1720
1721
Method
4500-dO
2
E, Chlorine Dioxide,
Amperometric
1722
Method
II (Proposed), referenced
in
Section 611.531.
1723
1724
Method
4500-V
B, Fluoride, Preliminary
Distillation
Step,
1725
referenced
in Section
611.611.
1726
1727
Method
4500-V
C,
Fluoride, Ion-Selective
Electrode
1728
Method,
referenced in
Section 611.611.
1729
1730
Method 4500-V
D, Fluoride,
SPADNS
Method, referenced
1731
in Section
611.611.
1732
1733
Method
4500-V E,
Fluoride, Complexone
Method,
1734
referenced
in Section 611.611.
1735
1736
Method
4500-Hf B,
pH Value, Electrometric
Method,
1737
referenced in Section
611.611.
1738
1739
Method 4500-N0
2
B, Nitrogen
(Nitrite),
Colorimetric
1740
Method, referenced
in Section
611.611.
1741
1742
Method 4500-N0
3
D, Nitrogen
(Nitrate),
Nitrate Electrode
1743
Method,
referenced
in Section
611.611.
1744
1745
Method
4500-N03
E, Nitrogen
(Nitrate), Cadmium
1746
Reduction Method,
referenced
in Section 611.611.
1747
1748
Method
4500-N0
3
F, Nitrogen
(Nitrate), Automated
1749
Cadmium Reduction
Method, referenced
in Section
1750
611.611.
1751
1752
Method
4500-03
B, Ozone
(Residual)
(Proposed),
Indigo
1753
Colorimetric
Method, referenced
in
Section 611.531.
1754
1755
Method 4500-P
E, Phosphorus,
Ascorbic Acid
Method,
1756
referenced
in Section 611.611.
1757
1758
Method
4500-P F, Phosphorus,
Automated
Ascorbic
Acid
JCAR35061 1-0815204r01
1759
Reduction Method, referenced
in Section 611.6 11.
1760
1761
Method 4500-Si D,
Silica, Molybdosilicate
Method,
1762
referenced in Section
611.611.
1763
1764
Method 4500-Si E,
Silica, Heteropoly Blue
Method,
1765
referenced in Section
611.611.
1766
1767
Method 4500-Si F,
Silica, Automated Method
for
1768
Molybdate-Reactive Silica, referenced
in Section 611.611.
1769
1770
Method
6651, Glyphosate Herbicide
(Proposed), referenced
1771
in Section 611.645.
1772
1773
Method 7110 B, Gross Alpha
and Beta Radioactivity
1774
(Total, Suspended, and
Dissolved), Evaporation
Method for
1775
Gross
Alpha-Beta, referenced in Section
611.720.
1776
1777
Method 7110
C,
Gross Alpha
and Beta Radioactivity
1778
(Total, Suspended,
and Dissolved),
Coprecipitation Method
1779
for Gross Alpha Radioactivity
in Drinking Water
1780
(Proposed), referenced in
Section 611.720.
1781
1782
Method 7500-Cs
B, Radioactive Cesium,
Precipitation
1783
Method, referenced in
Section 611.720.
1784
1785
Method H
3
7500-
B, Tritium, Liquid Scintillation
1786
Spectrometric
Method, referenced
in Section 611.720.
1787
1788
Method
7500-I B, Radioactive Iodine,
Precipitation
1789
Method, referenced in Section
611.720.
1790
1791
Method
7500-I
C,
Radioactive
Iodine, Ion-Exchange
1792
Method, referenced in
Section 611.720.
1793
1794
Method 7500-I D, Radioactive
Iodine, Distillation
Method,
1795
referenced
in Section 611.720.
1796
1797
Method 7500-Ra B,
Radium, Precipitation Method,
1798
referenced
in Section 611.720.
1799
1800
Method 7500-Ra
C, Radium, Emanation Method,
1801
referenced
in Section
611.720.
JCAR35O61
1-0815204r01
1802
1803
Method 7500-Ra D,
Radium, Sequential Precipitation
1804
Method (Proposed), referenced in Section
611.720.
1805
1806
Method 7500-Sr
B, Total Radioactive Strontium and
1807
Strontium 90, Precipitation Method,
referenced in Section
1808
611.720.
1809
1810
Method 7500-U B, Uranium, Radiochemical
Method
1811
(Proposed),
referenced in Section 611.720.
1812
1813
Method 7500-U
C, Uranium, Isotopic Method (Proposed),
1814
referenced
in Section 611.720.
1815
1816
Method 9215
B, Heterotrophic Plate Count, Pour Plate
1817
Method, referenced in Section 611.531.
1818
1819
Method 9221 A, Multiple-Tube Fermentation
Technique
1820
for Members
of the Coliform Group, Introduction,
1821
referenced in Sections 611.526
and 611.531.
1822
1823
Method 9221
B, Multiple-Tube Fermentation Technique
1824
for Members
of
the
Coliform Group, Standard Total
1825
Coliform Fermentation Technique,
referenced in Sections
1826
611.526and611.531.
1827
1828
Method 9221
C,
Multiple-Tube Fermentation
Technique
1829
for Members
of
the
Coliform Group, Estimation of
1830
Bacterial Density, referenced in Sections 611.526
and
1831
611.531.
1832
1833
Method 9221 D, Multiple-Tube
Fermentation Technique
1834
for Members of the
Coliform Group, Presence-Absence
(P
1835
A) Coliform Test, referenced in Section 611.526.
1836
1837
Method 9221 E, Multiple-Tube Fermentation
Technique
1838
for Members
of
the
Coliform Group, Fecal Coliform
1839
Procedure, referenced in
Sections 611.526 and 611.53 1.
1840
1841
Method 9222
A, Membrane Filter Technique for Members
1842
of the Coliform Group,
Introduction, referenced in Sections
1843
611.526and611.531.
1844
JCAR35O61 1-0815204r01
1845
Method 9222
B, Membrane Filter Technique for Members
1846
of the Coliform Group, Standard
Total Colifonn Membrane
1847
Filter Procedure,
referenced in Sections 611.526 and
1848
611.531.
1849
1850
Method
9222
C,
Membrane Filter Technique
for Members
1851
of the Coliform Group,
Delayed-Incubation Total Coliform
1852
Procedure, referenced in Sections
611.526 and 611.531.
1853
1854
Method 9222 D, Membrane
Filter Technique for Members
1855
of the
Coliform Group, Fecal Coliform Membrane Filter
1856
Procedure, referenced in Section
611.531.
1857
1858
Method 9223, Chromogenic Substrate Coliform
Test
1859
(Proposed) (also referred to as
the variations “Autoanalysis
1860
Colilert
System!!
and “Colisure
Test??),
referenced in
1861
Sections 611.526, and 611.531.
1862
1863
Method 9223 B, Chromogenic
Substrate Coliform Test
1864
(Proposed), referenced in Section 611.1004.
1865
1866
“Supplement to the
18
th
Edition
of Standard Methods for the
1867
Examination of Water and Wastewater,”
American Public Health
1868
Association,
1994.
1869
1870
Method 6610, Carbamate Pesticide
Method, referenced in
1871
Section6ll.645.
1872
1873
“Standard Methods
for the Examination of Water and
1874
Wastewater,”
19
th
Edition, 1995 (referred to
as “Standard Methods,
1875
19thed.?).
1876
1877
Method 2130 B, Turbidity, Nephelometric
Method,
1878
referenced in Section
611.53 1.
1879
1880
Method 2320
B,
Alkalinity,
Titration Method, referenced in
1881
Section6ll.611.
1882
1883
Method 2510
B, Conductivity, Laboratory Method,
1884
referenced in Section 611.611.
1885
1886
Method 2550,
Temperature, Laboratory, and Field
1887
Methods, referenced in
Section 611.611.
JCAR35O61
1-0815204r01
1888
1889
Method
3111
B, Metals
by
Flame Atomic
Absorption
1890
Spectrometry,
Direct
Air-Acetylene
Flame
Method,
1891
referenced
in
Sections
611.611
and
611.612.
1892
1893
Method
3111
D,
Metals
by
Flame
Atomic
Absorption
1894
Spectrometry,
Direct
Nitrous
Oxide-Acetylene
Flame
1895
Method,
referenced
in Section
611.611.
1896
1897
Method
3112
B,
Metals
by Cold-Vapor
Atomic
Absorption
1898
Spectrometry, Cold-Vapor
Atomic
Absorption
1899
Spectrometric
Method,
referenced
in Section
611.611.
1900
1901
Method
3113
B,
Metals
by
Electrothermal
Atomic
1902
Absorption
Spectrometry,
Electrothermal
Atomic
1903
Absorption
Spectrometric
Method,
referenced
in
Sections
1904
611.611
and6ll.612.
1905
1906
Method
3114
B,
Metals
by
Hydride
Generation/Atomic
1907
Absorption
Spectrometry,
Manual
Hydride
1908
Generation/Atomic
Absorption
Spectrometric
Method,
1909
referenced
in Section
611.611.
1910
1911
Method
3120 B,
Metals
by
Plasma
Emission
Spectroscopy,
1912
Inductively=Coupled
Plasma
(ICP)
Method,
referenced
in
1913
Sections
611.611
and
611.612.
1914
1915
Method
3500-Ca
D, Calcium,
EDTA
Titrimetric
Method,
1916
referenced
in
Section
611.611.
1917
1918
Method
3500-Mg
E, Magnesium,
Calculation
Method,
1919
referenced
in Section
611.611.
1920
1921
Method
4110
B,
Determination
of Anions
by
Ion
1922
Chromatography,
Ion Chromatography
with
Chemical
1923
Suppression
of
Eluent
Conductivity,
referenced
in Section
1924
611.611.
1925
1926
Method
4500-Cl
D,
Chlorine,
Amperometric
Titration
1927
Method,
referenced
in
Sections
611.381
and
611.531.
1928
1929
Method
4500-Cl
E,
Chlorine,
Low-Level
Amperometric
1930
Titration
Method,
referenced
in
Sections
611.381
and
JCAR35O61 1-0815204r01
1931
611.531.
1932
1933
Method 4500-Cl F,
Chlorine, DPD Ferrous Titrimetric
1934
Method, referenced in Sections
611.381 and 611.53 1.
1935
1936
Method 4500-Cl
G, Chlorine, DPD Colorimetric Method,
1937
referenced in Sections 611.381
and 611.531.
1938
1939
Method 4500-Cl
H, Chlorine, Syringaldazine (FACTS)
1940
Method, referenced in Sections 611.381 and
611.531.
1941
1942
Method 4500-Cl I, Chlorine, Jodometric Electrode
Method,
1943
referenced in Sections 611.381
and 611.531.
1944
1945
Method 4500-C102
C,
Chlorine Dioxide, Amperometric
1946
Method I, referenced
in Section 611.531.
1947
1948
Method 4500-C102
D, Chlorine Dioxide, DPD Method,
1949
referenced in Sections 611.381 and 611.531.
1950
1951
Method 4500-C102E,
Chlorine Dioxide, Amperometric
1952
Method II, referenced in Sections
611.381 and 611.531.
1953
1954
Method
4500-CN
C, Cyanide, Total Cyanide after
1955
Distillation, referenced in
Section 611.611.
1956
1957
Method 4500-CN
E, Cyanide, Colorimetric Method,
1958
referenced in Section 611.611.
1959
1960
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
1961
Method, referenced in Section
611.611.
1962
1963
Method 4500-CN
G,
Cyanide, Cyanides Amenable to
1964
Chlorination after Distillation,
referenced in Section
1965
611.611.
1966
1967
Method 4500-F B, Fluoride, Preliminary Distillation
Step,
1968
referenced
in Section 611.611.
1969
1970
Method 4500-F
C,
Fluoride, Ion-Selective Electrode
1971
Method, referenced in Section 611.611.
1972
1973
Method 4500-F D, Fluoride, SPADNS Method,
referenced
JCAR35O61
1-0815204r01
1974
in Section
611.611.
1975
1976
Method 4500-F
E, Fluoride, Complexone
Method,
1977
referenced in Section
611.611.
1978
-
1979
Method 4500-H
B, pH
Value, Electrometric Method,
1980
referenced in
Section 611.611.
1981
1982
Method
4500-N0
2B, Nitrogen
(Nitrite), Colorimetric
1983
Method, referenced
in Section 611.611.
1984
1985
Method 4500-N03
D, Nitrogen (Nitrate), Nitrate Electrode
1986
Method, referenced
in Section 611.611.
1987
1988
Method 4500-N03
E, Nitrogen (Nitrate), Cadmium
1989
Reduction
Method, referenced in Section
611.611.
1990
1991
Method 45
3
00-N0 F, Nitrogen (Nitrate),
Automated
1992
Cadmium Reduction
Method, referenced in Section
1993
611.611.
1994
1995
Method
4500-03 B, Ozone (Residual) (Proposed),
Indigo
1996
Colorimetric Method,
referenced in Section 611.53
1.
1997
1998
Method 4500-P
E, Phosphorus, Ascorbic
Acid Method,
1999
referenced in Section
611.611.
2000
2001
Method 4500-P F,
Phosphorus, Automated Ascorbic
Acid
2002
Reduction
Method, referenced in Section
611.611.
2003
2004
Method 4500-Si
D, Silica, Molybdosilicate
Method,
2005
referenced
in Section 611.611.
2006
2007
Method 4500-Si
E, Silica, Heteropoly
Blue Method,
2008
referenced in Section
611.611.
2009
2010
Method 4500-Si F,
Silica, Automated Method for
2011
Molybdate-Reactive
Silica,
referenced in Section 611.611.
2012
2013
Method 5910 B,
UV Absorbing Organic Constituents,
2014
Ultraviolet Absorption
Method, referenced in Section
2015
611.381.
2016
JCAR35O61 1-0815204r01
2017
Method
6251 B, Disinfection
Byproducts:
Haloacetic
2018
Acids
and Trichiorophenol,
Micro Liquid-Liquid
2019
Extraction
Gas Chromatographic
Method, referenced
in
2020
Section6ll.381.
2021
2022
Method
6610, Carbamate Pesticide
Method, referenced
in
2023
Section 611.645.
2024
2025
Method 6651,
Glyphosate Herbicide
(Proposed), referenced
2026
in Section
611.645.
2027
2028
Method
7110 B, Gross Alpha
and Gross Beta
2029
Radioactivity,
Evaporation Method
for Gross
Alpha-Beta,
2030
referenced
in Section 611.720.
2031
2032
Method
7110
C,
Gross Alpha
and Beta Radioactivity
2033
(Total,
Suspended, and
Dissolved), Coprecipitation
Method
2034
for Gross
Alpha Radioactivity
in Drinking Water
2035
(Proposed),
referenced
in Section 611.720.
2036
2037
Method 7120
B, Gamma-Emitting
Radionuclides, Gamma
2038
Spectrometric
Method,
referenced
in Section 611.720.
2039
2040
Method 7500-Cs
B, Radioactive Cesium,
Precipitation
2041
Method, referenced
in Section
611.720.
2042
2043
Method H
3
7500- B,
Tritium, Liquid Scintillation
2044
Spectrometric
Method, referenced in
Section 611.720.
2045
2046
Method 7500-I
B, Radioactive Iodine,
Precipitation
2047
Method, referenced
in Section
611.720.
2048
2049
Method
7500-I
C,
Radioactive Iodine,
Ion-Exchange
2050
Method, referenced
in Section
611.720.
2051
2052
Method 7500-I
D, Radioactive Iodine,
Distillation
Method,
2053
referenced
in Section 611.720.
2054
2055
Method 7500-Ra B,
Radium, Precipitation
Method,
2056
referenced
in Section
611.720.
2057
2058
Method
7500-Ra
C,
Radium,
Emanation Method,
2059
referenced
in Section
611.720.
JCAR35O61
1-0815204r01
2060
2061
Method
7500-Ra D,
Radium, Sequential
Precipitation
2062
Method, referenced
in Section 611.720.
2063
2064
Method
7500-Sr B, Total
Radiactive
Strontium and
2065
Strontium
90,
Precipitation
Method, referenced
in Section
2066
611.720.
2067
2068
Method
7500-U B, Uranium,
Radiochemical
Method,
2069
referenced
in Section
611.720.
2070
2071
Method
7500-U C, Uranium,
Isotopic Method,
referenced
2072
in
Section 611.720.
2073
2074
Method
9215 B, Heterotrophic
Plate
Count, Pour Plate
2075
Method, referenced
in Section 611.531.
2076
2077
Method 9221 A, Multiple-Tube
Fermentation
Technique
2078
for
Members of the Coliform
Group,
Introduction,
2079
referenced in Sections
611.526 and 611.531.
2080
2081
Method
9221 B, Multiple-Tube
Fermentation Technique
2082
for Members
of the Coliform Group,
Standard
Total
2083
Coliform
Fermentation Technique,
referenced in Sections
2084
611.526and611.531.
2085
2086
Method 9221
C,
Multiple-Tube
Fermentation Technique
2087
for Members of
the Coliform Group,
Estimation of
2088
Bacterial Density,
referenced in
Sections 611.526 and
2089
611.531.
2090
2091
Method
9221 D, Multiple-Tube
Fermentation Technique
2092
for Members
of the Coliform Group,
Presence-Absence
(P
2093
A) Coliform
Test, referenced
in Section 611.526.
2094
2095
Method
9221 E, Multiple-Tube
Fermentation Technique
2096
for Members
of the Coliform Group,
Fecal Coliform
2097
Procedure,
referenced in Sections
611.526 and 611.53
1.
2098
2099
Method 9222 A,
Membrane Filter Technique
for
Members
2100
of the Coliform Group,
Introduction,
referenced in Sections
2101
611.526and611.531.
2102
JCAR35O611-0815204r01
2103
Method 9222
B, Membrane Filter Technique for Members
2104
of
the Coliform Group, Standard Total
Colifomi Membrane
2105
Filter
Procedure, referenced in Sections 611.526 and
2106
611.531.
2107
2108
Method
9222
C,
Membrane Filter Technique
for Members
2109
of the Coliform
Group, Delayed-Incubation Total Coliform
2110
Procedure, referenced in Sections 611.526
and 611.531.
2111
2112
Method 9222 D, Membrane
Filter Technique for Members
2113
of the
Coliform Group, Fecal Coliform Membrane Filter
2114
Procedure, referenced in Section
611.531.
2115
2116
Method 9222
G,
Membrane Filter Technique for
Members
2117
of the Coliform Group,
MF
Partition
Procedures,
2118
referenced
in Section 611.526.
2119
2120
Method 9223,
Chromogenic Substrate Coliform Test
(also
2121
referred to as the variations “Autoanalysis
Colilert System”
2122
and “Colisure Test”), referenced in Sections 611.526,
and
2123
611.531.
2124
2125
Method 9223 B, Chromogenic Substrate Coliform
Test
2126
(Proposed), referenced in Section 611.1004.
2127
2128
“Supplement to the
19
th
Edition of Standard
Methods for the
2129
Examination
of Water and Wastewater,” American Public Health
2130
Association, 1996.
2131
2132
Method 5310 B, TOC, Combustion-Infrared
Method,
2133
referenced in Section 611.381.
2134
2135
Method 5310
C,
TOC, Persulfate-Ultraviolet
Oxidation
2136
Method, referenced
in Section 611.381.
2137
2138
Method
5310 D, TOC, Wet-Oxidation Method, referenced
2139
inSection6ll.381.
2140
2141
“Standard Methods
for the Examination of Water and
2142
Wastewater,”
Edition, 1998 (referred
to as “Standard Methods,
2143
20
th
ed.”).
2144
JCAR35O61
1-0815204r01
2145
Method
2130 B, Turbidity,
Nephelometric
Method,
2146
referenced
in Section
61 1.531.
2147
2148
Method
2320
B,
Alkalinity, Titration
Method,
referenced
in
2149
Section 611.611.
2150
2151
Method 2510
B, Conductivity, Laboratory
Method,
2152
referenced in Section
611.611.
2153
2154
Method 2550,
Temperature,
Laboratory, and Field
2155
Methods,
referenced in Section
611.611.
2156
2157
Method 3120
B, Metals by Plasma
Emission
Spectroscopy,
2158
Inductively-Coupled
Plasma
(ICP) Method, referenced
in
2159
Sections 611.611
andSection6ll.612.
2160
2161
Method 3500-Ca
B,
Calcium,
EDTA
Titrimetric
Method,
2162
referenced
in Section
611.611.
2163
2164
Method 3500-Mg
B, Magnesium,
EDTA Titrimetric
2165
Method,
referenced
in Section 611.611.
2166
2167
Method 4110
B, Determination
of Anions
by
Ion
2168
Chromatography,
Ion Chromatography
with
Chemical
2169
Suppression
of Eluent Conductivity,
referenced in Section
2170
611.611.
2171
2172
Method
4500-CN
C, Cyanide, Total Cyanide
after
2173
Distillation,
referenced
in Section
611.611.
2174
2175
Method 4500-CN
E, Cyanide,
Colorimetric
Method,
2176
referenced
in Section 611.611.
2177
2178
Method 4500-CN
F, Cyanide,
Cyanide-Selective
Electrode
2179
Method, referenced
in
Section
611.611.
2180
2181
Method 4500-CN
G, Cyanide,
Cyanides Amenable
to
2182
Chlorination
after Distillation,
referenced
in Section
2183
611.611.
2184
2185
Method
4500-Cl D,
Chlorine, Amperometric
Titration
2186
Method,
referenced
in Section
611.531.
2187
JCAR35O61 1-0815204r01
2188
Method 4500-Cl
E, Chlorine, Low-Level Amperometric
2189
Titration Method, referenced
in Section 611.531.
2190
2191
Method 4500-Cl
F, Chlorine, DPD Ferrous Titrimetric
2192
Method, referenced in Section
611.53 1.
2193
2194
Method 4500-Cl
G,
Chlorine, DPD Colorimetric
Method,
2195
referenced in Section
611.531.
2196
2197
Method 4500-Cl
H, Chlorine, Syringaldazine (FACTS)
2198
Method,
referenced in Section 611.53 1.
2199
2200
Method 4500-Cl
I, Chlorine, lodometric Electrode
Method,
2201
referenced
in Section 611.531.
2202
2203
Method
4500-C102
C,
Chlorine Dioxide, Amperometric
2204
Method I, referenced in Section
611.531.
2205
2206
Method 4500-C10
2
D, Chlorine Dioxide, DPD Method,
2207
referenced
in Section 611.531.
2208
2209
Method 4500-C10
2
E, Chlorine Dioxide, Arnperometric
2210
Method II (Proposed), referenced
in Section an4-611.531.
2211
2212
Method 4500-F
B, Fluoride, Preliminary Distillation
Step,
2213
referenced in Section 611.611.
2214
2215
Method 4500-F
C,
Fluoride,
Ion-Selective Electrode
2216
Method,
referenced in Section 611.611.
2217
2218
Method 4500-F D,
Fluoride, SPADNS Method, referenced
2219
in Section
611.611.
2220
2221
Method 4500-F
E, Fluoride, Complexone
Method,
2222
referenced
in Section 611.611.
2223
2224
Method 4500-H B,
pH Value, Electrometric Method,
2225
referenced
in Section 611.611.
2226
2227
Method 4500-N02
B, Nitrogen (Nitrite), Colorimetric
2228
Method, referenced in Section
611.611.
2229
JCAR35O61 1-0815204r01
2230
Method
4500-N0
3D, Nitrogen
(Nitrate), Nitrate Electrode
2231
Method, referenced
in Section 611.611.
2232
2233
Method
4500-N0
3E, Nitrogen (Nitrate),
Cadmium
2234
Reduction
Method, referenced in Section 611.611.
2235
2236
Method 4500-N0
3F, Nitrogen (Nitrate),
Automated
2237
Cadmium
Reduction Method, referenced in Section
2238
611.611.
2239
2240
Method 4500-03 B, Ozone
(Residual) (Proposed), Indigo
2241
Colorimetric
Method, referenced in Section 611.531.
2242
2243
Method 4500-P E,
Phosphorus, Ascorbic Acid Method,
2244
referenced
in Section 611.611.
2245
2246
Method 4500-P
F, Phosphorus, Automated Ascorbic
Acid
2247
Reduction Method, referenced
in Section 611.611.
2248
2249
Method 4500-Si
C, Silica, Molybdosilicate Method,
2250
referenced in Section 611.611.
2251
2252
Method 4500-Si
D, Silica, Heteropoly Blue Method,
2253
referenced in Section
611.611.
2254
2255
Method 4500-Si
E, Silica, Automated Method for
2256
Molybdate-Reactive Silica,
referenced in Section 611.611.
2257
2258
Method 5910 B, UV-Absorbing
Organic Constituents,
2259
Ultraviolet Absorption
Method, referenced in Sections
2260
611.381
and 611.382.
2261
2262
Method 6251,
Disinfection By-Products: Haloacetic
Acids
2263
and Trichlorophenol, referenced
in Section 611.381.
2264
2265
Method 6610, Carbamate
Pesticide Method, referenced
in
2266
Section
611.645.
2267
2268
Method 6651, Glyphosate
Herbicide (Proposed), referenced
2269
in
Section 611.645.
2270
JCAR35O61 1-0815204r01
2271
Method
7110 B, Gross Alpha and Gross Beta
2272
Radioactivity, Evaporation
Method for Gross Alpha-Beta,
2273
referenced
in Section 611.720.
2274
2275
Method 7110
C,
Gross
Alpha and Beta Radioactivity
2276
(Total, Suspended, and Dissolved),
Coprecipitation Method
2277
for Gross
Alpha Radioactivity in Drinking Water
2278
(Proposed), referenced
in Section 6 11.720.
2279
2280
Method 71207120
B, Gamma-Emitting Radionuclides,
2281
Gamma
Spectrometric Method, referenced
in Section
2282
611.720.
2283
2284
Method 7500-Cs B, Radioactive Cesium,
Precipitation
2285
Method, referenced
in Section 611.720.
2286
2287
Method H
3
7500-
B, Tritium, Liquid Scintillation
2288
Spectrometric Method, referenced in Section
6
11.720.
2289
2290
Method 7500-I B, Radioactive Iodine,
Precipitation
2291
Method, referenced in Section 611.720.
2292
2293
Method 7500-I
C, Radioactive Iodine, Ion-Exchange
2294
Method, referenced in Section 611.720.
2295
2296
Method 7500-I
D, Radioactive Iodine, Distillation Method,
2297
referenced in Section 611.720.
2298
2299
Method 7500-Ra B, Radium, Precipitation Method,
2300
referenced in Section 611.720.
2301
2302
Method 7500-Ra
C,
Radium, Emanation Method,
2303
referenced in Section
611.720.
2304
2305
Method 7500-Ra D, Radium,
Sequential Precipitation
2306
Method, referenced in Section 611.720.
2307
2308
Method 7500-Sr B, Total
Radiactive Strontium and
2309
Strontium 90, Precipitation Method, referenced
in Section
2310
611.720.
2311
2312
Method 7500-U B, Uranium, Radiochemical
Method,
2313
referenced in
Section 611.720.
JCAR35O61
1-0815204r01
2314
2315
Method
7500-U
C,
Uranium, Isotopic
Method,
referenced
2316
in Section 611.720.
2317
2318
Method 9215
B, Heterotrophic
Plate
Count,
Pour Plate
2319
Method, referenced
in
Section 611.53 1.
2320
2321
Method 9221
A, Multiple-Tube
Fermentation
Technique
2322
for Members
of the
Colifonn Group, Introduction,
2323
referenced
in Sections
611.526 and
611.531.
2324
2325
Method 9221
B, Multiple-Tube
Fermentation
Technique
2326
for Members
of the Coliform
Group, Standard
Total
2327
Coliform
Fermentation
Technique, referenced
in
Sections
2328
611.526and611.531.
2329
2330
Method 9221
C,
Multiple-Tube
Fermentation
Technique
2331
for Members
of the
Coliform
Group, Estimation
of
2332
Bacterial
Density, referenced
in Sections
611.526 and
2333
611.531.
2334
2335
Method 9221
D, Multiple-Tube
Fermentation
Technique
2336
for Members
of the
Coliform Group, Presence-Absence
(P
2337
A)
Coliform
Test,
referenced in Sections
611.526.
2338
2339
Method
9221
E,
Multiple-Tube Fermentation
Technique
2340
for Members of
the Coliform Group,
Fecal Coliform
2341
Procedure,
referenced
in Sections 611.526
and 611.53
1.
2342
2343
Method
9221
F,
Multiple-Tube Fermentation
Technique
for
2344
Members
of the Coliform
Group,
Escherichia Coli
2345
Procedure
(Proposed),
referenced in
Section 611.802.
2346
2347
Method
9222 A, Membrane
Filter Technique
for Members
2348
of the
Coliform
Group,
Introduction, referenced
in Sections
2349
611.526and611.531.
2350
2351
Method
9222
B,
Membrane Filter Technique
for Members
2352
of the Coliform Group,
Standard
Total Coliform Membrane
2353
Filter
Procedure,
referenced in
Sections 611.526 and
2354
611.531.
2355
JCAR35O61 1-0815204r01
2356
Method
9222
C, Membrane Filter Technique for
Members
2357
of the
Coliform Group, Delayed-Incubation
Total Coliform
2358
Procedure, referenced
in Sections 611.526 and
611.531.
2359
2360
Method 9222
D, Membrane Filter
Technique for Members
2361
of the Coliform
Group, Fecal Coliform Membrane
Filter
2362
Procedure, referenced
in Section 611.531.
2363
2364
Method 9222
G, Membrane Filter Technique for
Members
2365
of the
Coliform Group,
ME
Partition
Procedures,
2366
referenced in
Section 611.526.
2367
2368
Method 9223, Chromogenic
Substrate Coliform Test
(also
2369
referred to
as the variations “Autoanalysis
Colilert System”
2370
and
“Colisure Test”), referenced in
Sections 611.526,
2371
611.531.
2372
2373
Method 9223 B,
Chromogenic Substrate Coliform
Test
2374
(also
referred to as the variations
“Autoanalysis Colilert
2375
System” and
“Colisure Test”), referenced in
Sections
2376
611.802 and 611.1004.
2377
2378
Method 9230
B, Fecal Streptococcus
and Enterococcus
2379
Groups, Multiple
Tube Techniques, referenced
in Section
2380
611.802.
2381
2382
Method 9230
C, Fecal Streptococcus and Enterococcus
2383
Groups,
Membrane Filter Techniques,
referenced in
2384
Section 611.802.
2385
2386
“Standard
Methods for the Examination
of Water and
2387
Wastewater,”
21
st
Edition, 2005
(referred to as “Standard
Methods,
2388
21st
ed.).
2389
2390
Method 2130
B,
Turbidity,
Nephelometric
Method,
2391
referenced in Section
611.53 1.
2392
2393
Method 2320 B,
Alkalinity. Titration Method, referenced
in
2394
Section6ll.611.
2395
2396
Method 2510
B, Conductivity, Laboratory
Method,
2397
referenced in Section
611.611.
2398
JCAR35O61
1-0815204r01
2399
Method
2550,
Temperature,
Laboratory,
and
Field
2400
Methods,
referenced
in Section
611.611.
2401
2402
Method
3111 B, Metals
by
Flame
Atomic
Absorption
2403
pçctrometry,
Direct
Air-Acetylene
Flame
Method,
2404
referenced
in
Sections 611.611
and
611.612.
2405
2406
Method
3111
D, Metals
by Flame Atomic
Absorption
2407
Spectrometry,
Direct
Nitrous
Oxide-Acetylene
Flame
2408
Method,
referenced
in Section
611.611.
2409
2410
Method
3112
B, Metals
by
Cold-Vapor
Atomic
Absorption
2411
Spectrometry,
Cold-Vapor
Atomic
Absorption
2412
Spectrometric
Method, referenced
in
Section
611.611.
2413
2414
Method
3113 B, Metals
by
Electrothermal
Atomic
2415
Absorption
Spectrometry,
Electrothermal
Atomic
2416
Absorption
Spectrometric
Method,
referenced
in Sections
2417
611.611
and 611.612.
2418
2419
Method
3114 B,
Metals
by Hydride
GenerationlAtomic
2420
Absorption
Spectrometry,
Manual
Hydride
2421
GenerationlAtomic
Absorption
Spectrometric
Method,
2422
referenced
in Section
611.611.
2423
2424
Method 3120
B, Metals
by Plasma
Emission
Spectroscopy,
2425
Inductively-Coupled
Plasma
(ICP)
Method,
referenced
in
2426
Sections
611.611 and
611.612.
2427
2428
Method 3500-Ca
B,
Calcium, EDTA
Titrimetric
Method,
2429
referenced
in Section
611.611.
2430
2431
Method
3500-Ca
D, Calcium,
EDTA
Titrimetric
Method,
2432
referenced
in
Section 611.611.
2433
2434
Method
3500-Mg
B, Magnesium,
Calculation
Method,
2435
referenced
in Section
611.611.
2436
2437
Method
4110
B, Determination
of
Anions
by
Ion
2438
Chromatography,
Ion
Chromatography
with
Chemical
2439
Suppression
of Eluent
Conductivity,
referenced
in
Section
2440
611.611.
2441
JCAR35O61 1-0815204r01
2442
Method
4500-Cl D, Chlorine,
Amperometric
Titration
2443
Method, referenced
in
Section 611.381.
2444
2445
Method 4500-Cl
E, Chlorine,
Low-Level Amperometric
2446
Titration
Method, referenced
in Section
611.381.
2447
2448
Method
4500-Cl
F,
Chlorine, DPD Ferrous
Titrimetric
2449
Method,
referenced
in Section 611.381.
2450
2451
Method
4500-Cl
G, Chlorine, DPD
Colorimetric
Method,
2452
referenced
in Section
611.381.
2453
2454
Method
4500-Cl
H,
Chlorine, Syringaldazine
(FACTS)
2455
Method,
referenced in Section
611.381.
2456
2457
Method
4500-Cl I, Chlorine,
Jodometric
Electrode Method,
2458
referenced
in Section
611.381.
2459
2460
Method
4500-C10
2
C, Chlorine Dioxide,
Amperometric
2461
Method
I, referenced in
Section
611.53
1.
2462
2463
Method
4500-C10
2
E, Chlorine Dioxide,
Amperometric
2464
Method II (Proposed),
referenced
in Section and-611.381.
2465
2466
Method 4500-CN
E,
Cyanide,
Colorimetric
Method,
2467
referenced in Section
611.611.
2468
2469
Method 4500-CN
F, Cyanide,
Cyanide-Selective
Electrode
2470
Method, referenced
in Section 611.611.
2471
2472
Method 4500-CN
G, Cyanide,
Cyanides
Amenable
to
2473
Chlorination
after
Distillation,
referenced in Section
2474
611.611.
2475
2476
Method 4500-V B,
Fluoride,
Preliminary
Distillation
Step,
2477
referenced
in Section
611.611.
2478
2479
Method
4500-V
C,
Fluoride,
Ion-Selective Electrode
2480
Method, referenced
in Section 611.611.
2481
2482
Method 4500-V
D, Fluoride,
SPADNS Method,
referenced
2483
inSection6ll.611.
2484
JCAR35O61
1-0815204r01
2485
Method
4500-V
E,
Fluoride,
Complexone Method,
2486
referenced
in Section
611.611.
2487
+
2488
Method
4500-H
B,
pH
Value,
Electrometnc Method,
2489
referenced
in Section
611.611.
2490
2491
Method
4500-N0
B,
Nitrogen
(Nitrite),
Colorimetric
2492
Method,
referenced
in
Section
611.611.
2493
2494
Method
4500-N0
D,
Nitrogen
(Nitrate),
Nitrate
Electrode
2495
Method,
referenced
in
Section
611.611.
2496
2497
Method
4500-N0
E, Nitrogen
(Nitrate).
Cadmium
2498
Reduction
Method,
referenced
in
Section
611.611.
2499
2500
Method
4500-NOr
F,
Nitrogen
(Nitrate),
Automated
2501
Cadmium
Reduction
Method,
referenced
in Section
2502
611.611.
2503
2504
Method
4500-03
B, Ozone
(Residual)
(Proposed),
Indigo
2505
Colorimetric
Method,
referenced
in Section
611.53
1.
2506
2507
Method
4500-P
F, Phosphorus,
Ascorbic
Acid
Method,
2508
referenced
in
Section
611.611.
2509
2510
Method
4500-P
F, Phosphorus,
Automated
Ascorbic
Acid
2511
Reduction
Method,
referenced
in
Section
611.611.
2512
2513
Method
4500-SjQ
C, Silica,
Molybdosilicate
Method,
2514
referenced
in
Section
611.611.
2515
2516
Method
4500-jQ
2
D,
Silica,
Heteropoly
Blue
Method,
2517
referenced
in Section
611.611.
2518
2519
Method
4500-SiQ
E,
Silica,
Automated
Method
for
2520
Molybdate-Reactive
Silica,
referenced
in Section
611.611.
2521
2522
Method
5310
B,
TOC,
Combustion-Infrared
Method,
2523
referenced
in Section
611.381.
2524
2525
Method
5310 C,
TOC,
Persulfate-Ultraviolet
Oxidation
2526
Method,
referenced
in Section
611.381.
2527
JCAR35O61
1-0815204r01
2528
Method
5310 D, TOC, Wet-Oxidation Method,
referenced
2529
in Section 611.381.
2530
2531
Method 5910
B, IJV-Absorbing Organic Constituents,
2532
Ultraviolet Absorption
Method, referenced in Sections
2533
611.381 and 611.382.
2534
2535
Method 6251,
Disinfection By-Products: Haloacetic
Acids
2536
and Trichiorophenol, referenced
in
Section
611.381.
2537
2538
Method 6610, Carbamate Pesticide Method,
referenced in
2539
Section 611.645.
2540
2541
Method 7110 B, Gross Alpha
and Gross Beta
2542
Radioactivity,
Evaporation Method for Gross Alpha-Beta,
2543
referenced
in Section 611.720.
2544
2545
Method 7110
C,
Gross Alpha and Beta Radioactivity
2546
(Total, Suspended,
and
Dissolved),
Coprecipitation
Method
2547
for Gross Alpha Radioactivity in Drinking
Water
2548
(Proposed),
referenced in Section 611.720.
2549
2550
Method 7120, Gamma-Emitting
Radionuclides, referenced
2551
in Section 611.720.
2552
2553
Method 7500-Cs B, Radioactive
Cesium, Precipitation
2554
Method, referenced in Section 611.720.
2555
2556
Method
H
3
7500- B, Tritium, Liquid Scintillation
2557
Spectrometric Method,
referenced in Section 611.720.
2558
2559
Method 7500-I B, Radioactive Iodine,
Precipitation
2560
Method, referenced
in Section 611.720.
2561
2562
Method 7500-I
C, Radioactive Iodine, Ion-Exchange
2563
Method,
referenced in Section 611.720.
2564
2565
Method 7500-I D, Radioactive
Iodine, Distillation Method,
2566
referenced
in Section 611.720.
2567
2568
Method 7500-Ra
B,
Radium,
Precipitation Method,
2569
referenced
in Section
6
11.720.
2570
JCAR35O61
1-0815204r01
2571
Method
7500-Ra
C,
Radium,
Emanation
Method,
2572
referenced
in Section 611.720.
2573
2574
Method
7500-Ra
D, Radium,
Sequential Precipitation
2575
Method,
referenced in
Section 611.720.
2576
2577
Method
7500-Sr
B,
Total Radioactive Strontium
and
2578
Strontium
90, Precipitation
Method,
referenced in
Section
2579
611.720.
2580
2581
Method
7500-U B,
Uranium, Radiochemical
Method,
2582
referenced
in Section
611.720.
2583
2584
Method
7500-U
C,
Uranium,
Isotopic
Method, referenced
2585
in
Section
611.720.
2586
2587
Method
9221 A, Multiple-Tube
Fermentation
Technique
2588
for Members
of the Coliform
Group, Introduction,
2589
referenced
in Sections
611.526 and 611.531.
2590
2591
Method
9221
B, Multiple-Tube
Fermentation
Technique
2592
for
Members
of
the
Coliform
Group,
Standard
Total
2593
Coliform Fermentation
Technique,
referenced in
Sections
2594
611.526and611.531.
2595
2596
Method 9221
C,
Multiple-Tube
Fermentation Technique
2597
for Members
of the Coliform Group,
Estimation
of
2598
Bacterial Density,
referenced
in Sections 611.526
and
2599
611.531.
2600
2601
Method 9221 D,
Multiple-Tube
Fermentation
Technique
2602
for
Members
of
the Coliform Group,
Presence-Absence
(P
2603
A)
Coliform Test, referenced
in
Section 611.526.
2604
2605
Method 9221 E, Multiple-Tube
Fermentation Technique
2606
for
Members
of
the Coliform Group,
Fecal Coliform
2607
Procedure, referenced
in
Sections
611.526 and
611.53 1.
2608
2609
Method 9221 F,
Multiple-Tube
Fermentation
Technique
for
2610
Members of the
Coliform Group,
Escherichia
Coli
2611
Procedure
(Proposed),
referenced
in Section 611.802.
2612
JCAR35O61 1-0815204r01
2613
Method 9222
A, Membrane
Filter Technique
for Members
2614
of the
Coliform Group,
Introduction, referenced
in Sections
2615
611.526and611.531.
2616
2617
Method
9222 B, Membrane
Filter Technique
for Members
2618
of the
Coliform
Group,
Standard Total
Coliform Membrane
2619
Filter
Procedure, referenced
in Sections
611.526 and
2620
611.531.
2621
2622
Method 9222
C,
Membrane
Filter
Technique for Members
2623
of
the Coliform
Group, Delayed-Incubation
Total
Coliform
2624
Procedure,
referenced
in Sections
611.526 and 611.531.
2625
2626
Method
9222
D, Membrane
Filter
Technique for Members
2627
of
the Coliform Group,
Fecal Coliform
Membrane Filter
2628
Procedure,
referenced
in Section 611.53 1.
2629
2630
Method
9222
G, Membrane
Filter Technique
for Members
2631
of
the Coliform Group,
MF Partition
Procedures,
2632
referenced
in Section
611.526.
2633
2634
Method 9223, Chromogenic
Substrate
Coliform Test
(also
2635
referred
to as the
variations
“Autoanalysis Colilert
System”
2636
and “Colisure
Test”),
referenced
in
Sections 611.526
and
2637
611.531.
2638
2639
Method 9223
B, Chromogenic
Substrate Coliform
Test
2640
(also
referred
to as the variations
“Autoanalysis
Colilert
2641
System”
and
“Colisure
Test”),
referenced in
Sections
2642
611.802
and
611.1004.
2643
2644
BOARD
NOTE: Individual
Methods from
Standard
Methods areis
2645
available
online at www.standardmethods.org.
2646
2647
Analytical Technology,
Inc. ATI
Orion, 529
Main Street, Boston,
MA
2648
02129.
2649
2650
Technical
Bulletin
601, “Standard Method
of Testing
for Nitrate in
2651
Drinking
Water,” July,
1994,
PN 221890-001
(referred
to as
2652
“Technical
Bulletin
601”), referenced
in Section 611.611.
2653
2654
ASTM.
American Society
for Testing
and Materials,
100 Barr Harbor
2655
Drive,
West Conshohocken,
PA 19428-2959
(610-832-9585).
JCAR35O61 1-0815204r01
2656
2657
ASTM Method
D51 1-93 A and
B,
“Standard
Test
Methods
for
2658
Calcium
and Magnesium
in Water,”
“Test Method
A —
2659
Complexometric
Titration”
& “Test Method B —
Atomic
2660
Absorption Spectrophotometric,”
approved
1993, referenced
in
2661
Section6ll.611.
2662
2663
ASTM Method
D51 1-03 A
and B, “Standard
Test Methods
for
2664
Calcium
and Magnesium
in Water,” “Test Method
A —
2665
Complexometric
Titration”
&
“Test
Method
B — Atomic
2666
Absorption
Spectrophotometric,”
approved
2003,
referenced
in
2667
Section 611.611.
2668
2669
ASTM Method
D515-88 A,
“Standard Test
Methods for
2670
Phosphorus
in Water,” “Test Method
A — Colorimetric
Ascorbic
2671
Acid
Reduction,”
approved
August 19, 1988, referenced
in Section
2672
611.611.
2673
2674
ASTM
Method
D859-94D859
88, “Standard
Test Method
for
2675
Silica in Water,”
approved
l994August 19,
1988, referenced
in
2676
Section6ll.611.
2677
2678
ASTM Method
D859-00,
“Standard
Test Method for Silica
in
2679
Water,”
approved 2000,
referenced in Section
611.611.
2680
2681
ASTM
Method
D859-05,
“Standard
Test Method for
Silica
in
2682
Water,”
approved 2005,
referenced
in Section
611.611.
2683
2684
ASTM
Method D1067-92
B, “Standard
Test Methods
for Acidity
2685
or Alkalinity
in Water,”
“Test Method
B — Electrometric
or
Color-
2686
Change
Titration,” approved
May 15,
1992, referenced
in Section
2687
611.611.
2688
2689
ASTM
Method D1067-02
B, “Standard
Test Methods
for Acidity
2690
or Alkalinity
in Water,”
“Test Method
B — Electrometric
or
Color-
2691
Change
Titration,” approved
in
2002,
referenced
in
Section
2692
611.611.
2693
2694
ASTM
Method D1125-95
(1999)D1125
91 A,
“Standard
Test
2695
Methods
for Electrical
Conductivity
and Resistivity of
Water,”
2696
“Test
Method
A — Field and Routine
Laboratory
Measurement
of
2697
Static (Non-Flowing)
Samples,”
approved 1995,
reapproved
2698
l999June
15,
1991, referenced in
Section 611.611.
JCAR35O61
1-0815204r01
2699
2700
ASTM
Method Dl 179-93
B, “Standard Test
Methods for Fluoride
2701
in Water,”
“Test Method
B — Ion Selective
Electrode,” approved
2702
1993,
referenced in Section
611.611.
2703
2704
ASTM Method Dl 179-99
B, “Standard
Test Methods for
Fluoride
2705
in Water,” “Test Method
B
— Ion
Selective
Electrode,”
approved
2706
1999, referenced
in Section 611.611.
2707
2708
ASTM
Method
Dl 179-04 B, “Standard
Test Methods for
Fluoride
2709
in Water,” “Test Method
B — Ion
Selective Electrode,”
approved
2710
2004, referenced
in Section 611.611.
2711
2712
ASTM Method D1253-86,
“Standard
Test Method for Residual
2713
Chlorine
in Water,”
reapproved 1992, referenced
in Section
2714
611.381.
2715
2716
ASTM Method D1253-96,
“Standard
Test Method for Residual
2717
Chlorine
in Water,”
reapproved 1996, referenced
in Section
2718
611.381.
2719
2720
ASTM Method
D1253-03, “Standard
Test Method
for Residual
2721
Chlorine
in Water,” reapproved
2003, referenced in
2722
SectionsSection
611.381 and
611.531.
2723
2724
ASTM
Method D1293-95
A or BD1293 84, “Standard
Test
2725
Methods
for pH of Water,”
“Test Method A
— Precise Laboratory
2726
Measurement”
& “Test Method
B — Routine or Continuous
2727
Measurement,”
approved l995October
26, 1984,
referenced in
2728
Section6ll.611.
2729
2730
ASTM Method
D1293-99
A or B, “Standard Test
Methods for pH
2731
of
Water,”
“Test Method A — Precise
Laboratory
Measurement”
&
2732
“Test Method
B — Routine
or Continuous Measurement,”
approved
2733
1999, referenced
in Section 611.611.
2734
2735
ASTM
Method
D1688-95D 1688
90
A or
C,
“Standard
Test
2736
Methods for Copper
in
Water,”
“Test Method A
— Atomic
2737
Absorption,
Direct”
&
“Test Method
C
—Atomic
Absorption,
2738
Graphite
Furnace,” approved
1 995March 15, 1990,
referenced
in
2739
Section6ll.611.
2740
JCAR35O61 1-0815204r01
2741
ASTM
Method
D1688-02
A or
C,
“Standard
Test
Methods
for
2742
Copper
in Water,”
“Test
Method
A
—
Atomic
Absorption, Direct”
2743
&
“Test
Method
C
—
Atomic
Absorption,
Graphite
Furnace,”
2744
approved 2002,
referenced
in
Section
611.611.
2745
2746
ASTM
Method
D2036-98D2036
91
A
or
B, “Standard Test
2747
Methods
for
Cyanide
in
Water,”
“Test
Method
A
— Total
Cyanides
2748
after
Distillation”
&
“Test
Method
B
— Cyanides Amenable
to
2749
Chlorination
by
Difference,”
approved
l998September
15,
1991,
2750
referenced
in
Section
611.611.
2751
2752
ASTM
Method
D2036-06
A
or B,
“Standard
Test
Methods
for
2753
Cyanide
in
Water,”
“Test
Method
A
— Total
Cyanides
after
2754
Distillation”
&
“Test
Method
B
— Cyanides Amenable
to
2755
Chlorination
by
Difference,” approved
2006,
referenced
in Section
2756
611.611.
2757
2758
ASTM
Method
D2459-72,
“Standard
Test
Method
for
Gamma
2759
Spectrometry in
Water,”
approved
July
28,
1972,
discontinued
2760
1988,
referenced
in Section
611.720.
2761
2762
ASTM
Method
D2460-90,
“Standard Test
Method
for
2763
Radionuclides
of
Radium
in
Water,”
approved
1990,
referenced
in
2764
Section
611.720.
2765
2766
ASTM
Method
D2907-91,
“Standard
Test
Methods for
2767
Microquantities
of
Uranium
in Water
by
Fluorometry,”
“Test
2768
Method
A
— Direct
Fluorometric”
&
“Test
Method
B
—
2769
Extraction,”
approved
June
15, 1991,
referenced
in
Section
2770
611.720.
2771
2772
ASTM
Method
D2972-97D2972
93
B
or
C,
“Standard
Test
2773
Methods
for
Arsenic
in Water,”
“Test
Method
B
— Atomic
2774
Absorption,
Hydride
Generation”
&
“Test
Method
C
— Atomic
2775
Absorption, Graphite
Furnace,”
approved
19974-993, referenced
in
2776
Section
611.611.
2777
2778
ASTM
Method
D2972-03
B
or
C, “Standard Test
Methods
for
2779
Arsenic
in
Water,”
“Test
Method
B —
Atomic
Absorption,
Hydride
2780
Generation”
& “Test
Method
C
—
Atomic
Absorption,
Graphite
2781
Furnace,”
approved
2003,
referenced
in Section
611.611.
2782
2783
ASTM
Method
D3223-97D3223
91,
“Standard
Test
Method
for
JCAR35O61
1-0815204r01
2784
Total Mercury
in Water,”
approved
l997September
23,
1991,
2785
referenced
in
Section 611.611.
2786
2787
ASTM Method
D3223-02,
“Standard
Test
Method
for Total
2788
Mercury in
Water,”
approved
2002,
referenced
in Section
611.611.
2789
2790
ASTM
Method
D3454-91,
“Standard Test
Method for
Radium-226
2791
in Water,”
approved
1991,
referenced
in Section
611.720.
2792
2793
ASTM
Method
D3559-96
D, “Standard
Test Methods
for Lead
in
2794
Water,”
“Test Method
D — Atomic
Absorption,
Graphite
Furnace,”
2795
approved
August
6,
1990, referenced
in
Section 611.611.
2796
2797
ASTM Method
D3559-03
D,
“Standard
Test Methods
for Lead
in
2798
Water,”
“Test
Method
D
— Atomic
Absorption,
Graphite
Furnace,”
2799
approved
2003,
referenced
in
Section 611.611.
2800
2801
ASTM Method
D3645-97
B,
“Standard
Test
Methods
for
2802
Beryllium
in
Water,”
“Method
B — Atomic
Absorption,
Graphite
2803
Furnace,”
approved
19971993,
referenced
in Section
611.611.
2804
2805
ASTM
Method
D3645-03
B, “Standard
Test
Methods
for
2806
Beryllium
in
Water,”
“Method
B
— Atomic
Absorption,
Graphite
2807
Furnace,”
approved
2003,
referenced
in Section
611.611.
2808
2809
ASTM Method
D3649-91,
“Standard
Test
Method
for High-
2810
Resolution
Gamma-Ray
Spectrometry
of
Water,”
approved
1991,
2811
referenced
in Section
611.720.
2812
2813
ASTM
Method
D3649-98a,
“Standard
Test
Method
for High-
2814
Resolution
Gamma-Ray
Spectrometry
of
Water,”
approved
1998,
2815
referenced
in Section
611.720.
2816
2817
ASTM
Method
D3697-92,
“Standard
Test Method
for Antimony
in
2818
Water,”
approved
June 15,
1992,
referenced
in Section
611.611.
2819
2820
ASTM
Method
D3697-02,
“Standard
Test
Method
for Antimony
in
2821
Water,”
approved
2002, referenced
in
Section 611.611.
2822
2823
ASTM Method
D3859-98D3859
93 A, “Standard
Test Methods
2824
for
Selenium
in
Water,”
“Method
A
— Atomic
Absorption,
Hydride
2825
Method,”
approved 19981993,
referenced
in
Section 611.611.
2826
JCAR3 506 11-081 5204r01
2827
ASTM Method D3859-03
A, “Standard Test Methods for
2828
Selenium
in Water,” “Method A — Atomic Absorption,
Hydride
2829
Method,” approved 2003,
referenced in Section 611.611.
2830
2831
ASTM
Method D3867-90 A and B, “Standard Test Methods
for
2832
Nitrite-Nitrate in Water,”
“Test Method A — Automated Cadmium
2833
Reduction”
&
“Test Method
B
— Manual Cadmium
Reduction,”
2834
approved
January 10, 1990, referenced in Section 611.611.
2835
2836
ASTM Method D3972-90, “Standard Test Method for
Isotopic
2837
Uranium in Water
by Radiochemistry,” approved 1990, referenced
2838
in
Section 611.720.
2839
2840
ASTM Method D3972-02,
“Standard Test Method for Isotopic
2841
Uranium in Water by Radiochemistry,” approved 2002, referenced
2842
in Section 611.720.
2843
2844
ASTM Method D4107-91,
“Standard Test Method for Tritium in
2845
Drinking Water,” approved 1991, referenced in Section
611.720.
2846
2847
ASTM Method D4107-98,
“Standard Test Method for Tritium in
2848
Drinking Water,” approved 1998
(reapproved
2002),
referenced in
2849
Section
611.720.
2850
2851
ASTM Method D4327-97D4327
91, “Standard Test Method for
2852
Anions in Water by Ion Chromatography,” approved l997October
2853
15, 1991, referenced
in Section 611.611.
2854
2855
ASTM Method D4327-03,
“Standard Test Method for Anions in
2856
Water
by Ion Chromatography,” approved 2003, referenced in
2857
Section6ll.611.
2858
2859
ASTM Method D4785-88, “Standard Test Method for Low-Level
2860
Iodine-131 in Water,” approved
1988, referenced in Section
2861
611.720.
2862
2863
ASTM Method D4785-OOa, “Standard Test Method
for
Low-Level
2864
Iodine-13 1 in Water,”
approved 2000, referenced in Section
2865
611.720.
2866
2867
ASTM Method D5174-91, “Standard Test Method for Trace
2868
Uranium in
Water by Pulsed-Laser Phosphorimetry,” approved
2869
1991, referenced in Section 611.720.
JCAR35O61
1-0815204r01
2870
2871
ASTM Method D5174-02,
“Standard
Test Method for
Trace
2872
Uranium in Water
by
Pulsed-Laser
Phosphorimetry,”
approved
2873
2002,
referenced
in Section 611.720.
2874
2875
ASTM Method
D5317-93,
“Standard Test Method
for
2876
Determination
of Chlorinated
Organic Acid
Compounds
in
Water
2877
by Gas Chromatography
with an Electron Capture
Detector,”
2878
approved
1993, referenced
in
Section
611.645.
2879
2880
ASTM
Method D5317-98,
“Standard
Test
Method for
2881
Determination
of Chlorinated
Organic Acid
Compounds in Water
2882
by Gas
Chromatography with
an Electron Capture
Detector,”
2883
approved
1998 (reapproved 2003),
referenced
in Section 611.645.
2884
2885
ASTM Method
D5673-03, “Standard
Test
Method
for Elements in
2886
Water
by
Inductively-Coupled
Plasma — Mass Spectrometry,”
2887
approved
2003, referenced in Section
611.720.
2888
2889
ASTM Method
D5673-05,
“Standard Test Method
for Elements in
2890
Water
by Inductively-Coupled
Plasma — Mass
Spectrometry,”
2891
approved
2005,
referenced
in Section 611.720.
2892
2893
ASTM
Method D6508-00(2005)e2
(rev.
2),
“Standard Test
2894
Method for Determination
of Dissolved
Inorganic Anions
in
2895
Aqueous
Matrices
Using Capillary
Ion Electrophoresis and
2896
Chromate Electrolyte,”
approved 2000
(revised 2005),
referenced
2897
in
Section
611.611.
2898
2899
ASTM
Method D6581-00,
“Standard
Test Method for Bromate,
2900
Bromide, Chlorate,
and Chlorite in Drinking
Water
by
Chemically
2901
Suppressed
Ion Chromatography,”
approved
2000,
referenced
in
2902
Section6ll.381.
2903
2904
ASTM
Method D6919-03,
“Standard Test
Method for
2905
Determination
of Dissolved
Alkali and Alkaline
Earth Cations
and
2906
Ammonium
in Water
and Wastewater by
Ion Chromatography,”
2907
approved
2003, referenced
in Section
611.611.
2908
2909
ASTM
Method
D6888-04, “Standard
Test Method for Available
2910
Cyanide with Ligand
Displacement
and Flow
Injection
Analysis
2911
(FIA)
Utilizing
Gas Diffusion Separation
and
Amperometric
2912
Detection,”
approved 2004, referenced
in Section 611.611.
JCAR35O61
1-0815204r01
2913
2914
Bran
& Luebbe, 1025
Busch
Parkway,
Buffalo Grove, IL
60089.
2915
2916
“Fluoride in Water
and Wastewater,”
Industrial
Method #129-
2917
71W, December
1972
(referred to as “Technicon
Methods:
Method
2918
#129-71W”).
See 40 CFR
141.23(k)(1),
footnote 11
(2007)(2006),
2919
referenced
in
Section
611.611.
2920
2921
“Fluoride
in
Water and
Wastewater,”
#380-75 WE, February
1976
2922
(referred
to as “Technicon
Methods: Method
#380-75WE”).
See
2923
40 CFR
141.23(k)(1),
footnote
11
(2007)(2006),
referenced
in
2924
Section
611.611.
2925
2926
Charm Sciences,
Inc., 659 Andover
St., Lawrence,
MA 01843-1032:
2927
2928
“Charm
E*Colite
Presence/Absence
Test
for Detection and
2929
Identification
of Coliform
Bacteria and Escherichia
coli in
2930
Drinking
Water,” January
9,
1998
(referred
to as
E*Colite
Test”),
2931
referenced
in Section
611.802 (also available
from
USEPA,
Water
2932
Resource
Center).
2933
2934
CPI International,
Inc.,
5580
Skylane Blvd., Santa
Rosa, CA
95403
2935
(800-878-7654
/fax: 707-545-7901/Internet
address:
2936
www.cpiinternationa1.com).
2937
2938
“Colitag®
Product
as a Test for Detection
and Identification
of
2939
Coliforms
and
B. coli
Bacteria in Drinking Water
and Source
2940
Water as
Required in National
Primary
Drinking Water
2941
Regulations,”
August
2001, referenced in Section
611.526.
2942
2943
EMD
Chemicals
Inc. (an affiliate
of Merck KGgA,
Darmstadt,
Germany),
2944
480
5.
Democrat Road,
Gibbstown,
NJ 08027—1297.
(800-222-0342/e-
2945
mail:adellenbusch@emscience.com).
2946
2947
“Chromocult
Coliform Agar Presence/Absence
Membrane Filter
2948
Test Method
for Detection
and Identification of
Coliform Bacteria
2949
and Escherichia
coli in Finished
Waters,” November
2000,
Version
2950
1.0, referenced
in Section
611.526.
2951
2952
“Readycult
Coliforms
100 Presence/Absence
Test for Detection
2953
and Identification
of Coliform
Bacteria
and Escherichia coli
in
2954
Finished
Waters,”
November 2000, Version
1.0, referenced
in
2955
Section 611.526.
JCAR35O61 1-0815204r01
2956
2957
Environmental
Resources
Center, Georgia
Institute
of Technology,
620
2958
Cherry
Street,
Atlanta,
GA
30332-0335
(404-894-3776).
2959
2960
“The Determination
of Radium-226
and Radium-228
in
Drinkiig
2961
Water
by Gamma-ray
Spectrometry
Using HPGE
or Ge(Li)
2962
Detectors,”
Revision 1.2, December
2004
(called
“Georgia
Radium
2963
Method”), referenced
in Section
611.720.
2964
2965
ERDA
Health and
Safety Laboratory,
New York,
NY.
2966
2967
HASL Procedure
Manual,
HASL 300, 1973.
See
40
CFR
2968
141 .25(b)(2)
(2007)(2006), referenced
in Section
611.720.
2969
2970
Great
Lakes Instruments,
Inc., 8855 North
55
th
Street,
Milwaukee, WI
2971
53223.
2972
2973
GLI Method
2, “Turbidity,” Nov.
2, 1992, referenced
in Section
2974
611.531.
2975
2976
The
Hach Company,
P.O. Box 389, Loveland,
CO
80539-03 89
(800-227-
2977
4224).
2978
2979
“Lead
in Drinking Water
by Differential
Pulse Anodic
Stripping
2980
Voltammetry,”
Method
1001, August
1999, referenced in
Section
2981
611.611.
2982
2983
“Determination
of
Turbidity by Laser
Nephelometry,”
January
2984
2000,
Revision 2.0 (referred
to as
“Hach
FilterTrak Method
2985
10133”),
referenced
in Section 611.53 1.
2986
2987
“Total
Coliforms and E.
coli Membrane
Filtration Method
with m
2988
ColiBlue24®
Broth,”
Method No. 10029,
Revision 2, August
17,
2989
1999 (referred
to as “m-ColiBlue24
Test”),
referenced in
Section
2990
611.802 (also
available
from USEPA, Water
Resource Center).
2991
2992
[DEXX Laboratories,
Inc., One
IDEXX Drive,
Westbrook, Maine
04092
2993
(800-321-0207).
2994
2995
“IDEXX
SimPlate
TM HPC Test
Method for Heterotrophs
in
2996
Water,”
November 2000
(referred to
as “SimPlate
method”),
2997
referenced
in Section
611.531.
2998
JCAR35O61
1-0815204r01
2999
Industrial Test Systems,
Inc., 1875 Langston St.,
Rock Hill,
SC
29730.
3000
3001
Method
D99-003, Revision 3.0, “Free Chlorine
Species
(HOCF
3002
and
OCF) by
Test Strip,”
November
21, 2003 (referred to as
“ITS
3003
Method
D99-003”),
referenced in Section 611.381.
3004
3005
Lachat Instruments, 6645
W. Mill Rd., Milwaukee, WI
53218 (414-358-
3006
4200).
3007
3008
“Digestion and distillation of
total
cyanide in drinking and
3009
wastewaters
using MICRO DIST and
determination
of
cyanide
by
3010
flow injection analysis,” Revision 2.1, November 30, 2000
3011
(referred
to as “QuikChem Method
10-204-00-1-X”), referenced
in
3012
Section6ll.611.
3013
3014
Millipore Corporation, Technical Services Department, 80
Ashby
Road,
3015
Milford, MA 01730 (800-654-5476).
3016
3017
Colisure Presence/Absence Test for Detection and Identification
of
3018
Coliform Bacteria and Escherichia Coli in Drinking Water,
3019
February
28, 1994
(referred to as “Colisure
Test”), referenced
in
3020
Section 611.526.
3021
3022
NCRP. National Council on Radiation Protection, 7910 Woodmont Ave.,
3023
Bethesda, MD
(301-657-2652).
3024
3025
“Maximum Permissible Body Burdens and Maximum Permissible
3026
Concentrations of Radionuclides in Air and in Water for
3027
Occupational Exposure,” NCRP Report Number
22,
June 5, 1959,
3028
referenced in Section 611.101.
3029
3030
NSF. National Sanitation Foundation International,
3475
Plymouth Road,
3031
P0 Box 130140, Ann Arbor, Michigan 48113-0140 (734-769-8010).
3032
3033
NSF Standard 61, section
9,
November 1998, referenced in
3034
Sections 611.126 and 611.356.
3035
3036
NTIS. National Technical Information Service,
U.S.
Department of
3037
Commerce, 5285 Port Royal Road, Springfield, VA
22161
(703-487-4600
3038
or
800-553-6847).
3039
3040
“Interim Radiochemical Methodology for Drinking Water,” EPA
3041
600/4-75-008 (revised),
March 1976 (referred
to as “USEPA
JCAR35O61 1-0815204r01
3042
Interim
Radiochemical Methods”), referenced
in
Section
6 11.720.
3043
(Pages 1, 4,
6, 9, 13, 16, 24, 29, 34)
3044
3045
“Kelada
Automated Test Methods for Total Cyanide, Acid
3046
Dissociable
Cyanide, andAn4 Thiocyanate,” Revision 1.2, August
3047
2001, EPA 821/B-01-009
(referred to as “Kelada 01”), referenced
3048
in
Section 611.611.
3049
3050
“Maximum Permissible
Body Burdens and Maximum Permissible
3051
Concentrations
of Radionuclides in Air and in Water for
3052
Occupational Exposure,”
NBS (National Bureau of Standards)
3053
Handbook
69, as amended August 1963,
U.S.
Department of
3054
Commerce, referenced in Section 611.330.
3055
3056
Method
100.1, “Analytical Method for Determination of Asbestos
3057
Fibers in Water,” EPA 600/4-83-043,
September 1983, Doc. No.
3058
PB83-260471
(referred to as “USEPA Asbestos Methods-100.1”),
3059
referenced in Section 611.611.
3060
3061
Method 100.2, “Determination
of Asbestos Structures over 10-mm
3062
in Length in Drinking Water,” EPA 600/R-94-134,
June 1994,
3063
Doc.
No. PB94-201902 (referred to as “USEPA Asbestos
3064
Methods-100.2”),
referenced in Section 611.611.
3065
3066
“Methods for Chemical Analysis of Water and Wastes,”
March
3067
1983,
EPA
600/4-79-020,
Doc. No. PB84-128677 (referred to
as
3068
“USEPA Inorganic Methods”).
(Methods 150.1, 150.2, and 245.2,
3069
which
formerly appeared in this reference, are available from
3070
USEPA EMSL.), referenced in Section
611.611.
3071
3072
“Methods for the Determination of Inorganic Substances
in
3073
Environmental Samples,”
August 1993, EPA 600/R-93-100, Doc.
3074
No. PB94-120821
(referred to as “USEPA Environmental
3075
Inorganic Methods”), referenced
in Sections 611.381, 611.531, and
3076
611.611.
(Formethods 180.1, 300.0, 335.4, 353.2, and 365.1.)
3077
3078
“Methods
for the Determination of Metals in Environmental
3079
Samples,” June 1991, EPA 600/4-91-010,
Doc. No. PB91-231498
3080
and “Methods for the Determination
of Metals in Environmental
3081
Samples — Supplement I,” May 1994, EPA 600/R-94-1 11,
Doc.
3082
No. PB95-125472
(referred to as “USEPA Environmental Metals
3083
Methods”), referenced in
Sections 611.611,
611.612,
and 611.720.
3084
(For methods 200.7, 200.8, 200.9, and 245.1.)
JCAR35O61
l-0815204r01
3085
3086
“Methods
for
the
Determination
of Organic
and Inorganic
3087
Compounds
in
Drinking
Water,
Volume
1”
August
2000,
EPA
3088
815/R-00/014,
Doc. No.
PB2000-106981
(referred
to
as “USEPA
3089
Organic
and Inorganic
Methods”),
referenced
in Section
611.381.
3090
(Formethods
300.1
and 321.8.)
3091
3092
“Methods
for
the
Determination
of Organic
Compounds
in
3093
Drinking
Water,”
December
1988, revised
July 1991,
EPA
600/4-
3094
88/039,
Doc.
No.
PB91-23 1480
(referred
to
as “USEPA
Organic
3095
Methods”),
referenced
in
Sections 611.645
and 611.648.
(For
3096
methods
502.2, 505,
507, 508,
508A, 515.1,
and 531.1.)
3097
3098
“Methods
for the
Determination
of Organic
Compounds
in
3099
Drinking
Water
—
Supplement
I,” July
1990,
EPA 600/4-90/020,
3100
Doc. No.
PB91-146027
(referred
to as
“USEPA
Organic
3101
Methods”),
referenced
in Section
611.645.
(For methods
506, 547,
3102
550,550.1,and5Sl.)
3103
3104
“Methods
for the
Determination
of Organic
Compounds
in
3105
Drinking
Water
— Supplement
II,” August
1992, EPA
600/R-
3106
92/129,
Doc.
No.
PB92-207703
(referred
to
as “USEPA
Organic
3107
Methods”),
referenced
in
Sections 611.381
and
611.645. (For
3108
methods
515.2,
524.2,
548.1, 549.1,
552.1,
and 555.)
3109
3110
“Methods
for the
Determination
of
Organic Compounds
in Drinking
3111
Water— Supplement
III,” August
1995, EPA
6001R-95/131,
Doc.
3112
No.
PB95-261616,
(referred
to as
“USEPA
Organic
Methods”),
3113
referenced
in Sections
611.381
and 611.645.
(For
methods
502.2,
3114
524.2,
551.1,
and
552.2.)
3115
3116
“Prescribed
Procedures
for Measurement
of
Radioactivity
in
3117
Drinking
Water,”
EPA 600/4-80/032,
August 1980;
(Doc.
No.
PB
3118
8
0-224744)
(referred
to
as “USEPA
Radioactivity
Methods”),
3119
referenced
in
Section
611.720.
(For
methods 900,
901, 901.1,
902,
3120
903,
903.1, 904,
905,
906,
908, 908.1)
3121
3122
“Procedures
for Radiochemical
Analysis
of
Nuclear
Reactor
3123
Aqueous Solutions,”
H.L. Krieger
and
S.
Gold,
EPA-R4-73-014,
3124
May 1973,
Doc.
No. PB222-154/7BA,
referenced
in Section
3125
611.720.
3126
3127
“Radiochemical
Analytical
Procedures
for
Analysis of
JCAR35O61 1-0815204r01
3128
Environmental Samples,”
March
1979, Doc.
No.
EMSL
LV
3129
053917 (referred
to as “USEPA Radiochemical
Analyses”),
3130
referenced in Section
611.720.
(Pages 1, 19, 33, 65,
87, 92)
3131
3132
“Radiochemistry
Procedures Manual,”
EPA
520/5-84-006, August
3133
1984, Doc. No.
PB84-215581
(referred to as
“USEPA
3134
Radiochemistry
Methods”),
referenced in Section
611.720.
3135
(Methods
00-01, 00-02, 00-07,
H-02, Ra-03,
Ra-04, Ra-05, Sr-04)
3136
3137
“Technical
Notes on Drinking
Water Methods,”
EPA 600/R-
3138
94/173,
October
1994,
Doe. No. PB95-104766
(referred
to as
3139
“USEPA Technical
Notes”),
referenced in
Sections 611.531,
3140
611.611,and6ll.685.
3141
3142
BOARD
NOTE: USEPA made
the
following
assertion with
3143
regard to this
reference
at
40 CFR 141.23(k)(1)
and 141.24(e)
and
3144
(n)(11) (2007)(2006):
“This document
contains
other analytical
3145
test
procedures
and approved
analytical methods
that
remain
3146
available
for compliance monitoring
until
July
1, 1996.” Also
3147
available online
at http://nepis.epa.gov/EPA/html/Pubs/
3148
pubtitleORD.htm
under
the document designation
“600R94173.”
3149
3150
“Method
1613:
Tetra-
through Octa-Chlorinated
Dioxins
and
3151
Furans
by Isotope
Dilution HRGCIHRMS,”
October
1994, EPA
3152
821/B-94/005,
Doc.
No.
94-104774
(referred to as “Dioxin
and
3153
Furan
Method
1613”),
referenced in Section
611.645.
3154
3155
USEPA
Method 326.0,
Revision 1.0,
“Determination
of Inorganic
3156
Oxyhalide Disinfection
By-Products
in Drinking Water
Using Ion
3157
Chromatography
Incorporating the Addition
of a Suppressor
3158
Acidified
Postcolumn
Reagent
for Trace
Bromate Analysis,”
3159
USEPA,
June 2002,
EPA 815/R-03/007,
Doc.
No. PB2003-107402
3160
(referred
to as “OGWDW
Methods, Method
326.0,
rev. 1.0”),
3161
referenced
in Sections
611.381 and 611.382.
3162
3163
BOARD
NOTE: Also
available from United
States Environmental
3164
Protection
Agency, Office
of Ground
Water and Drinking
Water.
3165
3166
New Jersey
Department of Environment,
Division
of Environmental
3167
Quality, Bureau
of Radiation
and Inorganic
Analytical Services,
9
Ewing
3168
Street, Trenton,
NJ
08625.
3169
3170
“Determination
of Radium 228 in
Drinking Water,”
August 1990
JCAR35O61
1-0815204r01
3171
(referred
to
as “New Jersey
Radium Method”),
referenced
in
3172
Section
611.720.
3173
3174
New
York Department
of
Health, Radiological
Sciences
Institute,
Center
3175
for Laboratories
and Research,
Empire State
Plaza, Albany,
NY 12201.
3176
3177
“Determination
of Ra-226 and Ra-228
(Ra-02),”
January 1980,
3178
Revised June 1982
(referred to
as “New York Radium
Method”),
3179
referenced
in
Section 611.720.
3180
3181
Palintest,
Ltd., 21
Kenton
Lands Road,
P.O. Box 18395,
Erlanger,
KY
3182
(800-835-9629).
3183
3184
“Lead
in Drinking
Water
by Differential
Pulse Anodic
Stripping
3185
Voltamrnetry,”
Method 1001, August
1999 (referred
to as
3186
“Palintest
Method
1001”), referenced
in Section 611.611.
3187
3188
Standard Methods
Online,
available online
from the Standard
Methods
3189
Organization
at www.standardmethods.org.
3190
3191
Method
6610
B-04, Carbamate Pesticides,
High-Performance
3192
Liquid Chromatographic
Method,
referenced
in Section 611.645.
3193
3194
Method
9230
B-04, Fecal
Streptococcus and
Enterococcus
Groups,
3195
Multiple
Tube
Techniques,
referenced
in
Section 611.802.
3196
3197
Syngenta Crop
Protection, Inc., 410
Swing Road,
Post Office Box
18300,
3198
Greensboro, NC
27419
(336-632-6000).
3199
3200
“Atrazine
in Drinking
Water by Immunoassay,”
February
2001
3201
(referred to as
“Syngenta AG-625”),
referenced
in Section
3202
611.645.
3203
3204
United
States Department
of Energy, available
at the
Environmental
3205
Measurements
Laboratory,
U.S. Department
of Energy,
376 Hudson
3206
Street,
New York,
NY 10014-3621.
3207
3208
“EML
Procedures
Manual,”
27
th
Edition, Volume
1, 1990
(referred
3209
to as
“USDOE Manual”), referenced
in
Section 611.720.
3210
3211
United States
Environmental Protection
Agency,
Office of
Ground
Water
3212
and Drinking
Water (accessible
on-line
and
available by download
from
3213
http
://www.epa.gov/safewater/methods/).
JCAR35O61 1-0815204r01
3214
3215
USEPA
OGWDW Methods, Method 317.0, Revision 2.0,
3216
“Determination
of Inorganic Oxyhalide Disinfection By-Products
3217
in
Drinking Water Using
Ion Chromatography with the Addition of
3218
a Postcolunin
Reagent for Trace Bromate Analysis,”
USEPA, July
3219
2001, EPA
815/B-01/001 (referred to as “OGWDW Methods,
3220
Method 317.0, rev. 2.0”),
referenced in SectionsSection 611.381
3221
and 611.382.
3222
3223
USEPA OGWDW Methods, Method 326.0, Revision
1.0,
3224
“Determination
of Inorganic Oxyhalide Disinfection By-Products
3225
in Drinking
Water Using Ion Chromatography Incorporating
the
3226
Addition of a Suppressor
Acidified Postcolumn Reagent for Trace
3227
Bromate
Analysis,” USEPA, June 2002, EPA 815/R-03/007
3228
(referred
to as “OGWDW Methods, Method 326.0, rev.
1.0”),
3229
referenced in Sections
611.381 and 611.382.
3230
3231
BOARD NOTE:
Also available from NTIS.
3232
3233
USEPA
OGWDW Methods, Method 327.0, Revision 1.1,
3234
“Determination
of Chlorine Dioxide and Chlorite Ion in Drinking
3235
Water Using Lissamine Green
B and Horseradish Peroxidase with
3236
Detection
by Visible Spectrophotometry,” USEPA, May 2005,
3237
EPA 815/R-05/008
(referred to as “OGWDW Methods, Method
3238
327.0, rev. 1.1”),
referenced in SectionsSection 61 1.381 and
3239
611.531.
3240
3241
USEPA OGWDW Methods, Method 515.4,
Revision 1.0,
3242
“Determination
of Chlorinated Acids in Drinking Water by Liquid-
3243
Liquid
Microextraction, Derivatization and Fast Gas
3244
Chromatography with Electron
Capture Detection,” April 2000,
3245
EPA 81513-00/001
(document file name “met5lS_4.pdf’)
3246
(referred to as “OGWDW Methods, Method 515.4, rev.
1.0”),
3247
referenced in
Section
611.645.
3248
3249
USEPA OGWDW
Methods, Method 531.2, Revision 1.0,
3250
“Measurement of N-methylcarbamoyloximes
and N-
3251
methylcarbamates
in Water by Direct Aqueous Injection HPLC
3252
with Postcolumn Derivatization,”
September 2001, EPA 8 15/B-
3253
01/002 (document file name “metS3l_2.pdf’)
(referred to as
3254
“OGWDW Methods, Method 531.2, rev. 1.0”), referenced
in
3255
Section 611.645.
3256
JCAR35O61
1-0815204r01
3257
USEPA
OGWDW Methods, Method 552.3, Revision
1.0,
3258
“Determination
of Haloacetic
Acids and Dalapon in Drinking
3259
Water
by Liquid-liquid Microextraction, Derivatization,
and Gas
3260
Chromatography with
Electron Capture Detection,” USEPA,
July
3261
2003,
EPA 815/B-03/002
(referred to as “OGWDW Methods,
3262
Method
552.3, rev. 1.0”), referenced in SectionsSection
611.381
3263
and 611.645.
3264
3265
USEPA
OGWDW Methods, Method 1622
(05),
“Method
1622:
3266
Cryptosporidium in Water
by FiltrationlfMS!FA,” December 2005,
3267
EPA 815/R-05/001
(referred to as “USEPA Method 1622
(05)”),
3268
referenced in Sections 611.1004
and 611.1007.
3269
3270
USEPA
OGWDW Methods, Method 1622
(01), “Method 1622:
3271
Cryptosporidium in Water
by FiltrationllMS/FA,” April 2001,
3272
EPA 821/R-01/026,
(referred to as “USEPA Method 1622
(01)”),
3273
referenced in Section 611.1007.
3274
3275
USEPA OGWDW Methods,
Method 1622 (99), “Method 1622:
3276
Cryptosporidium
in Water
by
Filtration/IMS/FA,”
April 1999,
3277
EPA 821/R-99/001,
(referred to as “USEPA Method 1622
(99)”),
3278
referenced in
Section 611.1007.
3279
3280
USEPA OGWDW Methods, Method 1623
(05), “Method 1623:
3281
Cryptosporidium
and Giardia in Water
by
Filtration/IMS/FA,”
3282
December 2005, EPA
81 5/R-05/002 (referred to as “USEPA
3283
Method
1623 (05)”), referenced in Sections 611.1004
and
3284
611.1007.
3285
3286
USEPA OGWDW Methods,
Method 1623 (01), “Method 1623:
3287
Cryptosporidium
and Giardia in Water
by
FiltrationllMS/FA,”
3288
April 2001,
EPA 821/R-01/025 (referred
to as “USEPA Method
3289
1623 (01)”), referenced
in Section 611.1007.
3290
3291
USEPA OGWDW Methods,
Method 1623 (99), “Method 1623:
3292
Cryptosporidium
and Giardia in Water
by
Filtration/IMS/FA,”
3293
January 1999, EPA 821/R-99/006
(referred to as “USEPA Method
3294
1623
(99)”), referenced in Sections
611.1007.
3295
3296
United States Environmental
Protection Agency, EMSL, Cincinnati,
OH
3297
45268
(513-569-7586).
3298
3299
“Interim Radiochemical
Methodology for Drinking Water,” EPA
JCAR35O61
1-0815204r01
3300
600/4-75/008 (revised), March
1976
(referred to as “USEPA
3301
Interim
Radiochemical Methods”), referenced in Section 611.720.
3302
See NTIS.
3303
3304
“Methods for the Determination of Organic Compounds in
3305
Drinking
Water,” December 1988, revised July 1991,
EPA
600/4-
3306
88/039 (referred
to
as
“USEPA
Organic Methods”), referenced in
3307
Sections 611.645 and 611.648. (Formethods 504.1, 508.1, and
3308
525.2
only.) See NTIS.
3309
3310
“Procedures
for Radiochemical Analysis of
Nuclear Reactor
3311
Aqueous Solutions,” referenced in Section 611.720. See NTIS.
3312
3313
USEPA, Office of Research and Development,
National Exposure
3314
Research Laboratory, Microbiological
&
Chemical Exposure Assessment
3315
Research Division
(accessible on-line and
available
by
download from
3316
http ://www.epa.gov/nerlcwww/ordmeth.htm).
3317
3318
USEPA Method 200.5, Revision 4.2, “Determination of Trace
3319
Elements in Drinking Water by Axially Viewed
Inductively-
3320
Coupled
Plasma
— Atomic Emission Spectrometry,” October 2003,
3321
EPA 600/R-06/1 15
(referred
to as “USEPA NERL Method
3322
200.5”),
referenced in Sections 611.611 and 611.612.
3323
3324
USEPA Method
415.3, Revision
1.1,
“Determination of Total
3325
Organic Carbon and Specific UV Absorbance at 254 nm in Source
3326
Water and Drinking Water,” February
2005,
EPA 600/R-05/055
3327
(referred to as “USEPA NERL Method 415.3 (rev. 1.1)”),
3328
referenced in Section 611.381.
3329
3330
USEPA, Science and Technology Branch, Criteria and Standards
3331
Division, Office of Drinking Water, Washington, D.C.
20460.
3332
3333
“Guidance Manual for
Compliance
with
the Filtration and
3334
Disinfection Requirements for Public Water Systems using Surface
3335
Water Sources,” October 1989, referenced
in Sections 611.111
and
3336
611.212.
3337
3338
USEPA Water Resource
Center (RC-4100T), 1200 Pennsylvania Avenue,
3339
NW,
Washington, DC 20460:
3340
3341
“Charm
E*Colite
Presence/Absence Test for
Detection and
3342
Identification of Coliform Bacteria and Escherichia coli in
JCAR35O61 1-0815204r01
3343
Drinking Water,” January
9,
1998 (referred to as
E*Colite
Test”),
3344
referenced in Section 611.802
(also
available from Charm
3345
Sciences, Inc.).
3346
3347
“Total Coliforms and E.
coli
Membrane Filtration Method with
m
3348
ColiBlue24® Broth,” Method
No.
10029, Revision 2, August 17,
3349
1999 (referred to as “m-ColiBlue24 Test”), referenced in Section
3350
611.802
(also
available
from The Hach
Company).
3351
3352
“EPA
Method
1600: Enterococci
in Water by
Membrane Filtration
3353
Using Membrane-Enterococcus Indoxyl-b-D-Glucoside Agar
3354
(mEl),” September 2002,
EPA
821/R-02/022 (referred to as
3355
“USEPA Method 1600”) is an approved variation of Standard
3356
Methods, Method 9230
C,
“Fecal Streptococcus and Enterococcus
3357
Groups,
Membrane Filter Techniques”
(which has not itself
been
3358
approved for use by USEPA) (accessible on-line and available
by
3359
download from http ://www.epa.gov/nerlcwww/1 600sp02
.pdf),
3360
referenced in Section 611.802.
3361
3362
“Method 1601: Male-specific
(F)
and Somatic Coliphage in
3363
Water by Two-step Enrichment Procedure,” April 2001, EPA
3364
821/R-01/030
(referred to as “USEPA Method 1601”) (accessible
3365
on-line and available
by download from
3366
http ://www.epa.gov/nerlcwww/1 601 apO 1 .pdf), referenced in
3367
Section 611.802.
3368
3369
“Method 1602: Male-specific (Fj and Somatic Coliphage in
3370
Water by Single Agar Layer (SAL)
Procedure,” April 2001, EPA
3371
8211R-01/029 (referred to as “USEPA Method 1602”) (accessible
3372
on-line and available
by download
from
3373
http ://www.epa.gov/nerlcwww!1 602ap0 1 .pdf), referenced in
3374
Section 611.802.
3375
3376
“Method 1604: Total Coliforrns and Escherichia coli in Water
by
3377
Membrane Filtration Using
a Simultaneous
Detection Technique
3378
(MI Medium),” September 2002, EPA 821/R-02/024 (referred to
3379
as “USEPA Method 1604”) (accessible on-line and
available
by
3380
download from http ://www.epa.gov/nerlcwww/1 604sp02.pdf),
3381
referenced in Section 611.802.
3382
3383
USGS.
Books and Open-File Reports Section, United States Geological
3384
Survey, Federal Center, Box 25286, Denver,
CO
80225-0425.
3385
JCAR35O61
1-0815204r01
3386
Methods
available
upon request by method
number
from
“Methods
3387
for Analysis
by the
U.S. Geological
Survey National Water
3388
Quality
Laboratory
— Determination of
Inorganic
and
Organic
3389
Constituents in Water
and Fluvial Sediments,”
Open File
Report
3390
93-125,
1993, or Book
5,
Chapter
A-i, “Methods for
3391
Determination
of Inorganic Substances
in
Water
and Fluvial
3392
Sediments,” 3rd ed.,
Open-File
Report 85-495, 1989,
as
3393
appropriate
(referred
to as
“USGS Methods”).
3394
3395
1-1030-85,
referenced
in Section 611.611.
3396
3397
1-1601-85,
referenced in
Section 611.611.
3398
3399
1-1700-85,
referenced in Section
611.611.
3400
3401
1-2598-85,
referenced in Section
611.611.
3402
3403
1-2601-90,
referenced in Section
611.611.
3404
3405
1-2700-85,
referenced in Section
611.611.
3406
3407
1-3300-85,
referenced
in Section 611.611.
3408
3409
Methods
available upon request
by
method
number from “Methods
3410
for Determination
of Radioactive
Substances
in Water
and
Fluvial
3411
Sediments,”
Chapter AS in
Book 5 of “Techniques
of Water-
3412
Resources
Investigations
of the United States
Geological
Survey,”
3413
1997.
3414
3415
R-1110-76, referenced
in Section
611.720.
3416
3417
R-liii-76, referenced
in Section 611.720.
3418
3419
R-1120-76,
referenced
in Section 611.720.
3420
3421
R-1140-76,
referenced
in Section 611.720.
3422
3423
R-1
141-76,
referenced
in Section 611.720.
3424
3425
R-1142-76, referenced
in Section
611.720.
3426
3427
R-1160-76,
referenced in Section
611.720.
3428
JCAR35O61 1-0815204r01
3429
R-1171-76,
referenced in
Section
611.720.
3430
3431
R-1
180-76,
referenced in
Section 611.720.
3432
3433
R-1181-76,
referenced
in Section 611.720.
3434
3435
R-1182-76,
referenced
in Section 611.720.
3436
3437
Waters
Corporation,
Technical Services
Division,
34
Maple St., Milford,
3438
MA 01757
(800-252-4752
or 508-482-2131,
fax: 508-482-3625).
3439
3440
“Waters
Test
Method for
Determination
of Nitrite/Nitrate
in Water
3441
Using Single Column
Ion Chromatography,”
Method B-101 1,
3442
August 1987
(referred to as
“Waters Method B-loll”),
referenced
3443
in
Section 611.611.
3444
3445
c)
The Board incorporates
the following
federal
regulations by reference:
3446
3447
40 CFR 3.2
(2007)(2006)
(How
Does
This Part Provide for
Electronic
3448
Reporting?),
referenced
in Section 611.105.
3449
3450
40
CFR 3.3 (2007)(2006)
(What Definitions
Are Applicable
to This
3451
Part?),
referenced
in Section 611.105.
3452
3453
40
CFR 3.10 (2007)(2006)
(What
Are the Requirements
for Electronic
3454
Reporting
to
EPA?), referenced
in Section 611.105.
3455
3456
40
CFR
3.2000
(2007)(2006)
(What Are the Requirements
Authorized
3457
State, Tribe, and
Local
Programs’
Reporting
Systems Must Meet?),
3458
referenced in
Section 611.105.
3459
3460
40
CFR 136.3(a) (2007)(2006),
referenced
in Section
611.1004.
3461
3462
Appendix B to 40 CFR
136 (2007)(2006),
referenced
in Sections 611.359,
3463
611.609,
and
611.646.
3464
3465
d)
This Part incorporates
no
later amendments
or editions.
3466
3467
(Source:
Amended at 33 Ill. Reg.
effective
3468
3469
SUBPART
G: LEAD
AND
COPPER
3470
3471
Section
611.350 General
Requirements
JCAR35O611-0815204r01
3472
3473
a)
Applicability and Scope
3474
3475
1)
Applicability.
The requirements
of this Subpart
G
constitute
national
3476
primary drinking
water regulations
for lead and copper.
This Subpart
G
3477
applies to all community
water
systems (CWSs) and non-transient,
non-
3478
community water systems
(NTNCWSs).
3479
3480
2)
Scope. This Subpart
G
establishes
a treatment technique that includes
3481
requirements
for corrosion
control treatment, source water
treatment,
lead
3482
service line replacement,
and public
education. These requirements
are
3483
triggered, in
some cases,
by lead and copper action levels
measured in
3484
samples collected at
consumers’ taps.
3485
3486
b)
Definitions. For the purposes of
only this Subpart
G,
the following
terms have
the
3487
following meanings:
3488
3489
“Action level” means
that concentration
of
lead
or copper in water
3490
computed pursuant to
subsection (c) of this Section that determines,
in
3491
some cases, the
treatment requirements
of this Subpart
G
that a
supplier
3492
must complete. The
action level for lead is
0.0
15
mg/f. The action
level
3493
for copper is 1.3 mg/f.
3494
3495
“Corrosion inhibitor”
means a
substance capable of reducing
the
3496
corrosivity of water
toward metal plumbing materials,
especially lead
and
3497
copper, by forming a protective
film on the interior surface
of those
3498
materials.
3499
3500
“Effective corrosion
inhibitor residual” means
a concentration of
inhibitor
3501
in the drinking water sufficient
to form a passivating film
on the interior
3502
walls of a pipe.
3503
3504
“Exceed,” as this term is
applied to either the lead or the
copper action
3505
level, means
that the 90th percentile level
of
the
supplier’s samples
3506
collected during a six-month
monitoring period is greater than
the action
3507
level for that contaminant.
3508
3509
“First draw
sample” means a one-liter
sample of tap water, collected
in
3510
accordance with
Section 61 1.356(b)(2), that has
been standing in
3511
plumbing pipes for at least
six hours and which is collected
without
3512
flushing
the tap.
3513
3514
“Large system” means
a water system that regularly serves
water to
more
JCAR35O61
1-0815204r01
3515
than 50,000
persons.
3516
3517
“Lead
service line” means
a service line
made of lead that
connects
the
3518
water main
to the building
inlet, including
any lead pigtail, gooseneck,
or
3519
other
fitting that is
connected to such lead
line.
3520
3521
“Maximum
permissible
concentration”
or “MPC” means that
3522
concentration
of
lead
or copper for
finished water entering
the supplier’s
3523
distribution
system,
designated
by
the
Agency by a
SEP pursuant to
3524
Sections 611.110
and 611.353(b)
that reflects the contaminant
removal
3525
capability
of the
treatment properly
operated and maintained.
3526
BOARD NOTE:
Derived from
40
CFR 141.83(b)(4) (2007)(2002).
(See
3527
Section
611.353(b)(4)(B).)
3528
3529
“Medium-sized
system”
means a water
system that regularly
serves water
3530
to more
than 3,300 up
to 50,000 or fewer persons.
3531
3532
“Meet,”
as this term is
applied to either the
lead
or the copper
action level,
3533
means
that the
90
th
percentile level of
the supplier’s samples
collected
3534
during a six-month monitoring
period
is less than or equal
to the action
3535
level
for that contaminant.
3536
3537
“Method detection
limit” or “MDL”
is as defined at
Section 611.646(a).
3538
The MDL for
lead is
0.00
1
mg!?.
The MDL for
copper is 0.00 1 mg!E,
or
3539
0.020
mg/i
by atomic absorption
direct aspiration
method.
3540
BOARD NOTE:
Derived
from
40
CFR 141.89(a)(1)(iii)
(2007)(2002).
3541
3542
“Monitoring
period” means
any of the six-month
periods of time during
3543
which a
supplier must complete
a cycle
of
monitoring
under
this
Subpart
3544
G.
3545
BOARD
NOTE: USEPA refers
to these as “monitoring
periods.”
The
3546
Board uses “six-month
monitoring
period” to avoid
confusion with
3547
“compliance
period,” as used
elsewhere in this Part
and defined at Section
3548
611.101.
3549
3550
“Multiple-family
residence” means
a building
that
is currently used as
a
3551
multiple-family
residence, but
not one that is also a
“single-family
3552
structure.”
3553
3554
,,
90
th
percentile
level” means
that concentration
of lead or copper
3555
contaminant
exceeded
by ten percent or fewer
of all samples collected
3556
during
a six-month monitoring
period pursuant
to Section 611.356
(i.e.,
3557
that concentration
of
contaminant greater than
or equal
to
the
results
JCAR35O61 1-0815204r01
3558
obtained
from 90 percent
of the samples).
The
90
th
percentile
levels for
3559
copper and
lead
must be
determined
pursuant
to subsection
(c)(3)
of this
3560
Section.
3561
BOARD
NOTE: Derived
from
40
CFR
141.80(c) (2007)(2002).
3562
3563
“Optimal
corrosion
control treatment”
means
the corrosion
control
3564
treatment
that minimizes
the lead
and copper concentrations
at users’
taps
3565
while
ensuring
that
the treatment
does not cause the
water system
to
3566
violate any national primary
drinking
water
regulations.
3567
3568
“Practical quantitation
limit” or “PQL”
means
the
lowest concentration
of
3569
a contaminant
that
a well-operated
laboratory can reliably
achieve
within
3570
specified limits of precision
and accuracy
during routine
laboratory
3571
operating
conditions.
The PQL for lead
is 0.005 mg/f.
The PQL for
3572
copper
is 0.050 mg/f.
3573
BOARD
NOTE: Derived
from 40 CFR
141.89(a)(1)(ii)
and (a)(1)(iv)
3574
(2007)(2002).
3575
3576
“Service
line sample”
means
a one-liter
sample of water,
collected
in
3577
accordance
with
Section 611
.356(b)(3),
that
has been
standing for at
least
3578
six hours in a service
line.
3579
3580
“Single-family
structure” means
a building that
was constructed
as a
3581
single-family
residence and which
is
currently
used as either a residence
3582
or a place of
business.
3583
3584
“Small system”
means a water
system that regularly
serves water
to
3,300
3585
or
fewer
persons.
3586
BOARD NOTE:
Derived
from 40 CFR 141.2
(2007)(2002).
3587
3588
c)
Lead and Copper Action
Levels.
3589
3590
1)
The
lead
action
level is exceeded
if the
90
th
percentile
lead level
is greater
3591
than 0.015 mg/f.
3592
3593
2)
The copper action
level is exceeded
if the
90
th
percentile copper
level
is
3594
greater than
1.3 mg/f.
3595
3596
3)
Suppliers must
compute
the
percentile lead
and copper levels
as
3597
follows:
3598
3599
A)
List
the results
of all lead or copper
samples taken
during a six
3600
month monitoring
period in ascending
order, ranging
from the
JCAR35O61
1-0815204r01
3601
sample
with the lowest concentration first
to
the sample with the
3602
highest concentration
last. Assign each sampling result a number,
3603
ascending by single integers
beginning with
the number 1
for the
3604
sample
with the lowest contaminant level. The number assigned to
3605
the sample
with
the
highest contaminant level must be equal to the
3606
total number of samples taken.
3607
3608
B)
Determine
the number for the
90
th
percentile sample by
3609
multiplying the total number
of samples taken
during the six-
3610
month
monitoring period by 0.9.
3611
3612
C)
The contaminant
concentration in the sample with the number
3613
yielded by the calculation in subsection (c)(3)(B) of this Section is
3614
the
90
th
percentile contaminant
level.
3615
3616
D)
For suppliers that collect five samples
per
six-month monitoring
3617
period,the
90
th
percentile
is computed by taking the average of the
3618
highest and second highest concentrations.
3619
3620
)
For a supplier that has been allowed
by the Agency to collect fewer
3621
than five samples in accordance with Section 611.356(c), the
3622
sample result with the highest concentration is considered the
90
th
3623
percentile
value.
3624
3625
d)
Corrosion Control Treatment Requirements.
3626
3627
1)
All suppliers must install and operate optimal corrosion control treatment.
3628
3629
2)
Any supplier that complies with the applicable corrosion control treatment
3630
requirements
specified by
the
Agency pursuant to Sections 611.351 and
3631
611.352 is deemed in compliance with the treatment requirement of
3632
subsection (d)(1) of this Section.
3633
3634
e)
Source water treatment requirements. Any supplier whose system exceeds the
3635
lead
or copper action
level must implement all applicable source water treatment
3636
requirements specified by the Agency pursuant to Section 611.353.
3637
3638
f)
Lead service line replacement requirements.
Any supplier whose system exceeds
3639
the lead action level after implementation of applicable corrosion control and
3640
source
water
treatment requirements must complete the lead service line
3641
replacement requirements contained
in Section 611.354.
3642
3643
g)
Public education requirements. Pursuant to Section 611.355, the supplier must
JCAR35O61
l-0815204r01
3644
provide
a consumer
notice
of the
lead
tap water
monitoring
results
to the persons
3645
served
at each
site (tap) that
is tested.
Any supplier
whose
system exceeds
the
3646
lead
action
level
must
implement
the
public
education
requirements
contained
in
3647
Section
611.355.
3648
3649
h)
Monitoring
and analytical
requirements.
Suppliers
must
complete
all tap water
3650
monitoring
for lead
and copper,
monitoring
for water
quality
parameters,
source
3651
water
monitoring
for
lead and copper,
and
analyses
of
the monitoring
results
3652
under this
Subpart
Gin compliance
with
Sections 611.356,
611.357,
611.358,
and
3653
611.359.
3654
3655
i)
Reporting
requirements.
Suppliers
must report
to
the
Agency any
information
3656
required
by
the
treatment
provisions
of this
Subpart
G
and
Section
6 11.360.
3657
3658
j)
Recordkeeping
requirements.
Suppliers
must
maintain
records in
accordance
with
3659
Section 611.361.
3660
3661
k)
Violation
of national
primary
drinking
water
regulations.
Failure to
comply
with
3662
the
applicable
requirements
of
this
Subpart
G,
including
conditions
imposed
by
3663
the
Agency
by SEP pursuant
to
these provisions
and
Section 611.110,
will
3664
constitute
a violation
of the
national
primary
drinking
water
regulations
for
lead
3665
or
copper.
3666
3667
BOARD
NOTE:
Derived
from 40
CFR
141.80
(2007),
as amended
at 72 Fed.
Reg.
3668
57782
(October
10, 2007)(2002).
3669
3670
(Source:
Amended
at
33 Ill. Reg.
effective
3671
3672
Section 611.351
Applicability
of Corrosion
Control
3673
3674
a)
Corrosion
control
required.
Suppliers
must complete
the
applicable
corrosion
3675
control
treatment
requirements
described
in Section
6
11.352
on or before
the
3676
deadlines
set forth
in this
Section.
3677
3678
1)
Large systems.
Each
large system
supplier
(one regularly
serving
more
3679
than 50,000
persons)
must
complete
the corrosion
control
treatment
steps
3680
specified in
subsection
(d)
of this
Section, unless
it is deemed
to have
3681
optimized
corrosion
control
under
subsection
(b)(2)
or
(b)(3) of
this
3682
Section.
3683
3684
2)
Medium-sized
and
small systems.
Each
small system
supplier
(one
3685
regularly
serving
3,300
or fewer
persons)
and each
medium-sized
system
3686
(one regularly
serving
more
than
3,300
up to
50,000
persons)
must
JCAR35O61
1-0815204r01
3687
complete
the corrosion
control
treatment
steps
specified in subsection
(e)
3688
of this
Section,
unless
it is deemed
to have optimized
corrosion control
3689
under
one of subsections
(b)(1), (b)(2),
or
(b)(3)
of this Section.
3690
3691
b)
Suppliers
deemed to have
optimized corrosion
control.
A supplier is deemed
to
3692
have
optimized corrosion
control,
and
is not required
to complete the applicable
3693
corrosion
control
treatment
steps identified
in this Section,
if
the supplier
satisfies
3694
one
of the criteria
specified in subsections
(b)(1) through
(b)(3) of this
Section.
3695
Any
such
system deemed
to have
optimized corrosion
control under
this
3696
subsection,
and which
has treatment
in
place, must
continue to operate
and
3697
maintain optimal corrosion
control
treatment and meet
any requirements
that the
3698
Agency
determines are
appropriate to
ensure
optimal
corrosion control
treatment
3699
is maintained.
3700
3701
1)
Small-
or medium-sized
system
meeting action
levels.
A small
system or
3702
medium-sized system
supplier
is deemed to have
optimized corrosion
3703
control if the
system meets the lead
and copper
action levels
during each
3704
of two consecutive
six-month
monitoring periods with
monitoring
3705
conducted
in
accordance with
Section 611.356.
3706
3707
2)
SEP for equivalent
activities
to corrosion control.
The Agency
must,
by a
3708
SEP
granted
pursuant to Section
611.110, deem
any supplier
to have
3709
optimized
corrosion control
treatment
if it determines that the
supplier has
3710
conducted
activities
equivalent to the corrosion
control
steps applicable
3711
under
this Section. fri making
this determination,
the
Agency must specify
3712
the water
quality control
parameters
representing optimal
corrosion
3713
control
in accordance with
Section 611.352(f).
A water
supplier that
is
3714
deemed
to have optimized
corrosion
control under this subsection
(b)(2)
3715
must
operate in compliance
with the Agency-designated
optimal water
3716
quality control
parameters
in accordance
with Section 611.352(g)
and
3717
must
continue to conduct
lead
and copper
tap and water
quality parameter
3718
sampling
in accordance
with Sections 611.356(d)(3)
and
611.357(d),
3719
respectively.
A supplier
must provide
the Agency with the
following
3720
information
in order to support
an Agency
SEP
determination
under this
3721
subsection
(b)(2):
3722
3723
A)
The results of all test
samples
collected
for each
of the water
3724
quality
parameters
in Section 61
1.352(c)(3);
3725
3726
B)
A report explaining
the
test
methods the supplier
used to evaluate
3727
the
corrosion
control treatments
listed in Section
61 1.352(c)(1),
the
3728
results
of all tests conducted,
and
the basis
for the supplier’s
3729
selection
of optimal
corrosion
control treatment;
JCAR35O61 1-0815204r01
3730
3731
C)
A report explaining
how the supplier has installed
corrosion
3732
control and how the supplier
maintains it to insure minimal lead
3733
and copper
concentrations
at consume?s taps; and
3734
3735
D)
The results of tap water
samples collected in accordance with
3736
Section
611.356 at least
once every six months for one year after
3737
corrosion control
has been installed.
3738
3739
3)
Results less than
practical quantitation level
(PQL) for lead. Any supplier
3740
is deemed to have optimized corrosion
control if it submits results
of tap
3741
water monitoring conducted
in accordance with Section
611.356 and
3742
source
water
monitoring conducted
in accordance with Section 611.358
3743
that demonstrate that for
two consecutive six-month monitoring
periods
3744
the difference between
the 90th percentile tap water
lead level, computed
3745
pursuant to Section 611
.350(c)(3), and the highest source water lead
3746
concentration is less
than the practical quantitation level
for lead specified
3747
in Section 611.359(a)(1)(B)(i).
3748
3749
A)
Those systems whose
highest source water lead level is below
the
3750
method detection limit
(MDL) may also be deemed to have
3751
optimized corrosion control under this
subsection (b) if the 90th
3752
percentile tap water
lead level is less than or equal
to the PQL for
3753
lead for two consecutive
six-month monitoring periods.
3754
3755
B)
Any water
system deemed to have optimized
corrosion control in
3756
accordance with this
subsection (b) must continue monitoring
for
3757
lead and copper
at the tap no less frequently
than once every three
3758
calendar years using the
reduced number of sites specified in
3759
Section 611.356(c)
and collecting the samples at times
and
3760
locations specified in Section 61 1.356(d)(4)(D).
Any such
system
3761
that has not conducted
a round of monitoring pursuant to
Section
3762
611.356(d)
since September 30, 1997, must have
completed a
3763
round of monitoring
pursuant to this subsection (b) no later than
3764
September
30,
2000.
3765
3766
C)
Any water
system deemed to have optimized
corrosion control
3767
pursuant to this
subsection (b) must notify the Agency
in writing
3768
pursuant to Section 61 1.360(a)(3)
of any upcoming long-term
3769
change in treatment or the addition of a
new source, as described
in
3770
that Section. The
Agency must review and approve
the addition of
3771
a new source or any
long-term change in water treatment before
3772
the addition or long-term change is
implemented
by the water
JCAR35O61 l-0815204r01
3773
system
require
any
such system to conduct
additional
monitoring
3774
or to take
other action
if the
Agency
deteines that the
additional
3775
monitoring
is necessary
and appropriate
to ensure that
the supplier
3776
maintains
minimal
levels of corrosion
in its distribution
system.
3777
3778
D)
AAs
of
July
12,
2001, a supplier
is not deemed to
have optimized
3779
corrosion control
under this subsection
(b),
and must implement
3780
corrosion
control
treatment
pursuant to subsection
(b)(3)(E) of
this
3781
Section,
unless
it meets the copper
action level.
3782
3783
E)
Any supplier
triggered into corrosion
control
because it is no
3784
longer
deemed
to have optimized
corrosion control
under
this
3785
subsection must
implement corrosion
control
treatment in
3786
accordance
with
the deadlines in
subsection (e) of
this Section.
3787
Any such large system
supplier
must adhere to the
schedule
3788
specified
in
that
subsection (e) for a
medium-sized
system supplier,
3789
with
the time periods
for completing
each step being
triggered
by
3790
the
date the
supplier
is no longer deemed
to have
optimized
3791
corrosion control
under
this subsection
(b).
3792
3793
c)
Suppliers not
required to complete
corrosion control
steps for
having met both
3794
action
levels.
3795
3796
1)
Any small
system
or medium-sized
system supplier,
otherwise required
to
3797
complete the corrosion
control
steps due to its
exceedence of the
lead or
3798
copper action
level, may cease
completing the treatment
steps
after the
3799
supplier has fulfilled
both of the
following
conditions:
3800
3801
A)
It has met
both the copper
action level
and the lead action
level
3802
during
each of two consecutive
six-month
monitoring periods
3803
conducted
pursuant
to
Section 611.356; and
3804
3805
B)
The supplier
has submitted
the results for those
two
consecutive
3806
six-month
monitoring periods
to the
Agency.
3807
3808
2)
A supplier that has
ceased completing
the corrosion
control steps pursuant
3809
to subsection (c)(1)
of this
Section
(or the Agency,
if appropriate)
must
3810
resume completion
of the applicable
treatment
steps, beginning with
the
3811
first treatment step
that the supplier
previously
did not complete
in its
3812
entirety, if the
supplier
thereafter
exceeds the lead
or
copper
action level
3813
during any
monitoring period.
3814
3815
3)
The Agency
may,
by
SEP, require a supplier
to
repeat
treatment
steps
JCAR35O61 1-0815204r01
3816
previously completed
by the supplier
where it determines that this is
3817
necessary to properly implement
the treatment requirements of this
3818
Section.
Any such SEP must explain
the basis for this decision.
3819
3820
4)
The requirement for any
small- or medium-sized system supplier to
3821
implement corrosion control treatment
steps in accordance with subsection
3822
(e)
of
this Section
(including systems
deemed to have
optimized
corrosion
3823
control under subsection
(b)(1) of this Section) is triggered whenever
any
3824
small- or medium-sized system supplier
exceeds the lead or copper action
3825
level.
3826
3827
d)
Treatment steps and deadlines
for large systems. Except as provided in
3828
subsections
(b)(2)
and (b)(3) of this Section, large
system
suppliers
must complete
3829
the following corrosion control treatment
steps (described in the referenced
3830
portions of Sections 611.352,
611.356, and 611.357) on or before the indicated
3831
dates.
3832
3833
1)
Step 1: The supplier must have conducted
initial monitoring (Sections
3834
611.356(d)(1) and
611.357(b)) during two consecutive six-month
3835
monitoring periods on or before
January 1, 1993.
3836
3837
2)
Step
2: The
supplier must have completed corrosion control studies
3838
(Section 611.352(c))
on or before July 1, 1994.
3839
3840
3)
Step 3: The Agency must have approved
optimal corrosion control
3841
treatment (Section
611.352(d)) by a SEP issued pursuant to Section
3842
611.110 on orbefore January
1, 1995.
3843
3844
4)
Step
4:
The supplier must have installed
optimal corrosion control
3845
treatment (Section 611.352(e))
by January 1, 1997.
3846
3847
5)
Step 5: The supplier must have
completed follow-up sampling (Sections
3848
611.356(d)(2) and
611.357(c)) by January 1, 1998.
3849
3850
6)
Step 6: The Agency
must have reviewed installation of treatment and
3851
approve optimal water quality control parameters
(Section 611.352(f))
by
3852
July 1, 1998.
3853
3854
7)
Step 7: The supplier must operate in compliance with
the Agency-
3855
specified optimal
water quality control parameters (Section
611.352(g))
3856
and continue to conduct tap
sampling (Sections 61 1.356(d)(3) and
3857
611.357(d)).
3858
JCAR35O61
l-0815204r01
3859
e)
Treatment
steps and
deadlines for
small- and
medium-sized
system
suppliers.
3860
Except
as provided
in subsection
(b) of this
Section,
small- and
medium-sized
3861
system
suppliers
must
complete
the following
corrosion
control
treatment
steps
3862
(described
in
the referenced
portions
of
Sections
611.352,
611.356,
and 611.357)
3863
by
the
indicated
time periods.
3864
3865
1)
Step
1:
The supplier
must conduct
initial
tap
sampling
(Sections
3866
611.356(d)(l)
and
611.357(b))
until the
supplier either
exceeds
the lead
3867
action level
or
the copper
action
level
or it becomes
eligible
for reduced
3868
monitoring
under
Section 611.356(d)(4).
A
supplier
exceeding
the lead
3869
action level
or
the copper
action
level
must
recommend
optimal
corrosion
3870
control
treatment
(Section
611.352(a))
within
six
months
after
the end
of
3871
the monitoring
period
during which
it
exceeds one
of
the action
levels.
3872
3873
2)
Step
2:
Within
12 months
after
the end of
the monitoring
period
during
3874
which a supplier
exceeds
the lead
action
level or
the copper
action
level,
3875
the
Agency
may require
the
supplier
to perform
corrosion
control
studies
3876
(Section 611.352(b)).
If
the Agency
does
not
require the
supplier
to
3877
perform
such studies,
the Agency
must,
by
a
SEP
issued
pursuant
to
3878
Section
611.110,
specify
optimal
corrosion
control
treatment
(Section
3879
611.352(d))
within
the
appropriate
of
the following
timeframes:
3880
3881
A)
Forfef
medium-sized
systems,
within 18
months after
the end
of
3882
the monitoring
period
during
which such
supplier
exceeds the
lead
3883
action level
or
the
copper action
level
3884
3885
B)
Forfef
small
systems,
within
24 months
after the end
of the
3886
monitoring
period
during which
such supplier
exceeds
the lead
3887
action
level or
the
copper action
level.
3888
3889
3)
Step
3: If the Agency
requires
a supplier
to
perform
corrosion
control
3890
studies
under
step 2
(subsection
(e)(2)
of this
Section),
the
supplier
must
3891
complete
the studies
(Section
611.352(c))
within
18 months
after the
3892
Agency
requires
that
such studies
be
conducted.
3893
3894
4)
Step 4:
If the
supplier
has performed
corrosion
control
studies
under
step
3895
2
(subsection
(e)(2)
of this
Section), the
Agency
must, by a
SEP issued
3896
pursuant
to Section
611.110,
approve
optimal
corrosion
control
treatment
3897
(Section
611.352(d))
within
six months
after
completion
of
step 3
3898
(subsection
(e)(3)
of
this
Section).
3899
3900
5)
Step
5: The
supplier
must
install
optimal
corrosion
control
treatment
3901
(Section 611.352(e))
within
24 months
after
the
Agency
approves
such
JCAR35O61 1-0815204r01
3902
treatment.
3903
3904
6)
Step
6: The supplier must complete
follow-up sampling (Sections
3905
611.356(d)(2)
and 611.357(c)) within
36 months after the Agency
3906
approves optimal corrosion
control treatment.
3907
3908
7)
Step 7:
The Agency must review the
supplier’s installation of treatment
3909
and, by a SEP issued
pursuant to Section 611.110, approve optimal
water
3910
quality
control parameters
(Section 611.352(f)) within six months after
3911
completion
of
step
6 (subsection (e)(6) of this
Section).
3912
3913
8)
Step 8: The supplier
must operate in compliance with the
Agency-
3914
approved
optimal water quality control
parameters (Section 611.352(g))
3915
and continue to conduct tap
sampling (Sections 61 1.356(d)(3) and
3916
611.357(d)).
3917
3918
BOARD NOTE: Derived from 40
CFR 141.81
(2007),
as amended at 72 Fed.
Reg.
3919
57782
(October
10,
2007)(2003).
3920
3921
(Source: Amended at 33 Ill. Reg.
effective
3922
3923
Section 611.353
Source Water Treatment
3924
3925
Suppliers must complete the applicable source
water monitoring and treatment requirements
3926
(described in the referenced portions of subsection
(b) of this Section, and in Sections 611.356
3927
and 611.358) by
the following deadlines.
3928
3929
a)
Deadlines for completing
source water treatment steps.
3930
3931
1)
Step 1: A supplier exceeding
the lead action level or the copper action
3932
level must
complete lead and copper
and
source water
monitoring (Section
3933
611.358(b)) and make a treatment
recommendation to the Agency
3934
(subsection (b)(1)
of this Section) within 180 dayssix months
after the end
3935
of the monitoring period during
which the supplier exceeded exceeding
3936
the pertinent action
level.
3937
3938
2)
Step 2: The Agency
must, by a SEP issued pursuant to
Section 611.110,
3939
make a determination regarding
source water treatment (subsection
(b)(2)
3940
of this Section) within six months
after submission of monitoring results
3941
under step 1.
3942
3943
3)
Step 3: If the Agency requires
installation of source water treatment, the
3944
supplier must
install that treatment (subsection
(b)(3) of this Section)
JCAR35O61
1-0815204r01
3945
within
24 months
after completion
of step 2.
3946
3947
4)
Step
4: The supplier
must
complete
follow-up
tap water
monitoring
3948
(Section
611
.356(d)(2))
and source
water
monitoring
(Section 611.358(c))
3949
within 36 months
after
completion
of
step
2.
3950
3951
5)
Step 5: The
Agency must,
by
a SEP issued
pursuant
to Section
611.110,
3952
review the
supplier’s
installation
and
operation of
source
water
treatment
3953
and specify
MPCs
for lead and
copper
(subsection
(b)(4) of this
Section)
3954
within six
months after
completion
of
step 4.
3955
3956
6)
Step 6: The
supplier
must operate
in
compliance
with
the Agency-
3957
specified lead
and
copper
MPCs
(subsection
(b)(4)
of this Section)
and
3958
continue
source water
monitoring
(Section
611.358(d)).
3959
3960
b)
Description
of Source
Water
Treatment
Requirements.
3961
3962
1)
System
treatment
recommendation.
Any
supplier that
exceeds
the lead
3963
action level
or the
copper
action
level
must
recommend
in writing
to the
3964
Agency the
installation
and operation
of one
of
the source
water
3965
treatments
listed in
subsection
(b)(2) of
this Section.
A supplier
may
3966
recommend
that
no
treatment
be installed
based
on
a
demonstration
that
3967
source
water treatment
is
not
necessary
to
minimize
lead and
copper
levels
3968
at users’
taps.
3969
3970
2)
Agency
determination
regarding
source water
treatment.
3971
3972
A)
The
Agency
must
complete
an evaluation
of the results
of
all
3973
source
water samples
submitted
by
the
supplier to
determine
3974
whether
source
water
treatment
is necessary
to minimize
lead
or
3975
copper
levels in
water
delivered
to users’
taps.
3976
3977
B)
If the
Agency
determines
that
treatment
is
needed,
the Agency
3978
must, by
a SEP issued
pursuant
to Section
611.110,
either require
3979
installation
and
operation
of the
source
water
treatment
3980
recommended
by
the
supplier
(if any) or
require the
installation
3981
and
operation
of
another
source
water treatment
from
among
the
3982
following:
3983
3984
i)
ion
exchange;
3985
3986
ii)
reverse
osmosis;
3987
JCAR35O61 1-0815204r01
3988
iii)
lime softening; or
3989
3990
iv)
coagulationlfiltration.
3991
3992
C)
The Agency may
request and the supplier must submit
such
3993
additional information,
on or before a certain date, as the Agency
3994
determines
is necessary to aid in its
review.
3995
3996
D)
The Agency must notify
the supplier in writing of its determination
3997
and set forth
the basis for its decision.
3998
3999
3)
Installation of source
water treatment. Each supplier must properly
install
4000
and operate the
source water treatment
approved by the Agency under
4001
subsection (b)(2) of this Section.
4002
4003
4)
Agency review of source water treatment
and specification of maximum
4004
permissible source water
levels (MPC5).
4005
4006
A)
The Agency
must review the source water samples taken
by the
4007
supplier both before
and after the supplier installs source water
4008
treatment,
and determine whether
the supplier has properly
4009
installed and
operated the approved
source
water
treatment.
4010
4011
B)
Based on its review,
the Agency must, by a SEP issued pursuant
to
4012
Section 611.110, approve the lead
and copper MPCs for finished
4013
water entering
the supplier’s distribution system.
Such levels must
4014
reflect the contaminant removal
capability of the treatment
4015
properly operated
and maintained.
4016
4017
C)
The Agency must
explain the basis for its decision under
4018
subsection
(b)(4)(B) of this Section.
4019
4020
5)
Continued operation
and maintenance. Each supplier must
maintain lead
4021
and copper levels below the MPCs
approved by the Agency at each
4022
sampling point monitored
in accordance with Section 611.358.
The
4023
supplier is out of compliance with this
subsection if the level of lead
or
4024
copper at any sampling
point is greater than the
MPC
approved
by the
4025
Agency pursuant to subsection
(b)(4)(B) of this Section.
4026
4027
6)
Modification
of Agency treatment decisions.
4028
4029
A)
On its own initiative, or
in response to a request by a supplier,
the
4030
Agency
may, by a SEP issued pursuant
to Section 611.110, modify
JCAR35O61 1-0815204r01
4031
its
determination
of
the
source water treatment under subsection
4032
(b)(2)
of this Section, or the lead and
copper MPCs under
4033
subsection
(b)(4) of this Section.
4034
4035
B)
A request
for modification
by a
supplier
must be in writing,
4036
explain why the
modification is appropriate,
and
provide
4037
supporting documentation.
4038
4039
C)
The Agency may,
by a SEP issued pursuant to Section 611.110,
4040
modify its determination where it
concludes that such change is
4041
necessary to ensure
that the supplier continues to minimize lead
4042
and
copper concentrations in source water.
4043
4044
D)
A revised determination
made pursuant to subsection
(b)(6)(C) of
4045
this Section must set forth the new
treatment requirements, explain
4046
the basis for the
Agency’s decision, and provide an implementation
4047
schedule
for completing the treatment modifications.
4048
4049
E)
Any interested person may submit information
to the Agency, in
4050
writing, that
bears on whether the Agency should, within its
4051
discretion, issue
a SEP to modify its determination pursuant to
4052
subsection (h)(1)
of this Section. An Agency determination not to
4053
act on a submission of such information
by an interested person is
4054
not an Agency
determination for the purposes of Sections
39 and
4055
40 of the Act
[415 ILCS 5/39 and 40].
4056
4057
7)
Treatment decisions
by USEPA. Pursuant to the procedures in 40
CFR
4058
142.19,
the USEPA Regional Administrator
reserves the prerogative to
4059
review treatment determinations
made by the Agency under subsections
4060
(b)(2),
(b)(4), or (b)(6) of this Section and issue
federal treatment
4061
determinations consistent
with the requirements of 40 CFR 141.83(b)(2),
4062
(b)(4),
and
(b)(6), where the Administrator finds that the following is
true:
4063
4064
A)
the Agency has
failed to issue a treatment determination by the
4065
applicable deadline contained in subsection
(a) of this Section;
4066
4067
B)
the Agency has abused its discretion in
a substantial number of
4068
cases or
in cases affecting a substantial population; or
4069
4070
C)
the technical aspects
of the
Agency’s
determination would be
4071
indefensible
in an expected federal enforcement action taken
4072
against a supplier.
4073
JCAR35O61
1-0815204r01
4074
BOARD
NOTE:
Derived
from
40 CFR
141.83
(2007),
as amended
at 72 Fed.
Reg.
4075
57782 (October
10, 2007)(2002).
4076
4077
(Source:
Amended
at 33 Ill. Reg.
effective
4078
4079
Section
611.354
Lead
Service Line
Replacement
4080
4081
a)
Suppliers
required
to replace
lead
service
lines.
4082
4083
1)
If
the results
from tap
samples taken
pursuant
to Section
61 1.356(d)(2)
4084
exceed
the lead
action level
after the
supplier
has
installed
corrosion
4085
control
or source
water
treatment
(whichever
sampling
occurs
later),
the
4086
supplier
must
recommence
replacing
lead
service
lines in
accordance
with
4087
the requirements
of
subsection
(b)
of this Section.
4088
4089
2)
If a
supplier is
in violation
of Section
611.351
or Section
611.353
for
4090
failure
to install
source
water
or corrosion
control
treatment,
the
Agency
4091
may,
by a SEP
issued pursuant
to Section
611.110,
require
the supplier
to
4092
commence
lead
service
line
replacement
under
this
Section
after the
date
4093
by which
the supplier
was
required
to conduct
monitoring
under
Section
4094
611.356(d)(2)
has passed.
4095
4096
b)
Annual replacement
of lead
service
lines.
4097
4098
fl
Initiation
of a lead service
line
replacement
program.
4099
4100
A1-)
A
supplier
that is
required
to commence
lead
service line
4101
replacement
pursuant
to subsection
(a)
of
this
Section
must
4102
annually
replace
at least
seven
percent of
the
initial number
of
lead
4103
service lines
in its
distribution
system.
4104
4105
B2)
The
initial number
of lead
service
lines is
the number
of lead
lines
4106
in
place at the
time
the
replacement
program
begins.
4107
4108
3)
The
supplier
must
identify
the initial
number
of lead
service
lines
4109
in its
distribution
system,
including
an
identification
of the
portions
4110
of
the system
owned
by
the supplier,
based on
a materials
4111
evaluation,
including
the
evaluation
required under
Section
4112
6
11.356(a) and
relevant
legal authorities
(e.g.,
contracts,
local
4113
ordinances)
regarding
the portion
owned
by
the system.
4114
4115
4)
The first year
of
lead
service line
replacement
must begin
on
the
4116
first
day
following
the end of
the monitoring
period
in which date
JCAR35O61
1-0815204r01
4117
the
supplier
exceeded
the
action level
pursuant
to in tap
sampling
4118
referenced
in subsection
(a) of this
Section.
4119
4120
If monitoring
is
required
annually
or less
frequently,
the
end of the
4121
monitoring
period
is September
30 of the
calendar
year
in which
4122
the sampling
occurs.
4123
4124
If the
Agency has
established
an alternate
monitoring
period
by a
4125
SEP issued
pursuant
to Section
611.110,
then the end
of the
4126
monitoring
period will
be the
last day
of
that
period.
4127
4128
Resumption
of a lead
service
line replacement
program
after
cessation.
4129
4130
)
A supplier
that is resuming
a program
after
cessation
of its lead
4131
service
line
replacement
program,
as
allowed
pursuant
to
4132
subsection
(f)
of this
Section, must
update
its inventory
of lead
4133
service
lines
to
include
those sites
that it
had
previously
4134
determined
did not require
replacement
pursuant
to the
sampling
4135
provision
of
subsection
(c)
of
this Section.
4136
4137
The supplier
will then
divide
the updated
number of
remaining
4138
lead service
lines
by the number
of remaining
years
in the program
4139
to determine
the
number
of lines
that
must
be replaced
per
year
4140
(seven
percent lead
service
line replacement
is based
on a 15-year
4141
replacement
program,
so
that, for example,
a supplier
resuming
4142
lead
service
line
replacement
after
previously
conducting
two years
4143
of replacement
would divide
the
updated
inventory
by
13).
4144
4145
For
a supplier
that has
completed
a
15-year
lead
service line
4146
replacement
program,
the Agency
must, by
a SEP
issued
pursuant
4147
to Section
611.110,
determine
a schedule
for replacing
or
retesting
4148
lines that
were previously
tested
out
under
the completed
4149
replacement
program,
whenever
the
supplier
has re-exceeded
the
4150
action
level.
4151
4152
c)
Service
lines
not needing
replacement.
A supplier
is not
required
to replace
any
4153
individual
lead
service
line for
which
the
lead
concentrations
in all
service
line
4154
samples taken
from that
line pursuant
to Section
61 1.356(b)(3)
are
less than
or
4155
equalto0.OlSmg!E.
4156
4157
d)
A
water
supplier must
replace
that portion
of the
lead
service line
that it owns.
In
4158
cases
where the
supplier does
not own
the entire
lead service
line, the supplier
4159
must
notify
the
owner
of
the line, or
the owner’s
authorized
agent,
that
the
JCAR35O61 1-0815204r01
4160
supplier will
replace
the portion of the service line that it owns and must offer to
4161
replace the owner’s portion of the line. A supplier
is
not required to bear the cost
4162
of replacing the
privately-owned
portion of the line, nor is it required to replace
4163
the
privately-owned portion where the
owner chooses not to pay the cost of
4164
replacing the privately-owned portion of the line,
or
where replacing the
4165
privately-owned portion would be precluded by State, local, or common law. A
4166
water
supplier that
does not replace the entire length of the service line also must
4167
complete the following tasks:
4168
4169
1)
Notice Prior to Commencement of
Work.
4170
4171
A)
At least 45 days priorto commencing the partial replacement of
a
4172
lead
service line, the water supplier must provide notice to
the
4173
residents of all buildings served by the line explaining that they
4174
may experience a temporary increase
of
lead levels in their
4175
drinking water, along with guidance on measures consumers can
4176
take to minimize their exposure to lead.
4177
4178
B)
The Agency,
by
issuing an appropriate SEP, may allow the water
4179
supplier to provide notice under the previous sentence less than 45
4180
days prior to commencing partial lead service line replacement
4181
where it determines
that such replacement is in
conjunction
with
4182
emergency repairs.
4183
4184
C)
In addition, the water supplier must inform the residents served by
4185
the line that the supplier will, at the supplier’s expense, collect a
4186
sample from each partially-replaced lead service line that is
4187
representative of the water in the service line for analysis of lead
4188
content, as prescribed by Section 611.356(b)(3), within 72 hours
4189
afler the completion of the partial replacement of the service line.
4190
The supplier must collect the sample and report
the results
of the
4191
analysis to the owner and the residents served by the line within
4192
three business days
of
receiving the results.
4193
4194
D)
Mailed notices post-marked within three business days of receiving
4195
the results must be considered “on time.”
4196
4197
2)
The water supplier must provide the information required by subsection
4198
(d)(1) of this Section to the residents of individual dwellings by mail or by
4199
other methods approved
by the
Agency
by a
SEP issued pursuant to
4200
Section 611.110. In instances where multi-family dwellings are served
by
4201
the service line, the water supplier must have the option to post the
4202
information at
a conspicuous location.
JCAR35O61
1-0815204r01
4203
4204
e)
Agency
determination of shorter
replacement
schedule.
4205
4206
1)
The Agency must,
by a SEP issued
pursuant to
Section 611.110, require
a
4207
supplier to replace
lead service
lines on a
shorter
schedule than that
4208
otherwise
required
by this Section
if it determines,
taking
into
account
the
4209
number of lead
service lines in
the
system,
that such a shorter replacement
4210
schedule is feasible.
4211
4212
2)
The Agency
must notify
the supplier
of
its finding pursuant
to subsection
4213
(e)( 1) of
this Section within six
months after
the supplier
is triggered into
4214
lead service
line replacement
based on monitoring,
as referenced
in
4215
subsection
(a) of this Section.
4216
4217
f)
Cessation
of service line
replacement.
4218
4219
1)
Any supplier may
cease
replacing
lead service
lines whenever it
fulfills
4220
both
of the following
conditions:
4221
4222
A)
First
draw tap samples
collected pursuant
to
Section
611.356(b)(2)
4223
meet
the lead action
level during each
of two consecutive
six-
4224
month
monitoring
periods;
and
4225
4226
B)
The supplier has
submitted those
results to the
Agency.
4227
4228
2)
If any
of the supplier’s
first draw tap samples
thereafter
exceed the lead
4229
action level, the supplier
must recommence
replacing lead
service lines
4230
pursuant
to subsection
(b) of this Section.
4231
4232
g)
To demonstrate
compliance with
subsections
(a)
through
(d)
of this Section,
a
4233
supplier must
report to the Agency
the
information
specified in
Section
4234
611.360(e).
4235
4236
BOARD
NOTE:
Derived
from 40 CFR
141.84
(2007),
as amended at 72
Fed. Reg.
4237
57782
(October
10, 2007)(2003).
4238
4239
(Source:
Amended at
33
Ill. Reg.
effective
4240
4241
Section 611.355
Public
Education
and Supplemental
Monitoring
4242
4243
A
supplier that exceeds
the lead action level
based on tap
water
samples
collected in accordance
4244
with Section 611.356
must deliver the public
education
materials required
by
4245
subsectionsubsections
(a) and
(b) of
this Section in
accordance with the
requirements
of
4246
4247
4248
4249
4250
4251
4252
4253
4254
4255
4256
4257
4258
4259
4260
4261
4262
4263
4264
4265
4266
4267
4268
4269
4270
4271
4272
4273
4274
4275
4276
4277
4278
4279
4280
4281
4282
4283
4284
4285
4286
4287
4288
JCAR35O61 1-0815204r01
subsection
ci2)Ee
of this Section.
A supplier that exceeds
the lead action level must sample
the
tap
water of any customer who
reciuests
it in
accordance with subsection
(c)
of
this
Section. A
supplier must deliver a consumer
notice of lead tap water
monitoring results to persons who
are
served by the supplier at each site that the
supplier has tested, as
specified in subsection
(d)
of
this
Section.
a)
Content of written
public education materials.
1)
Community
water systems and non-transient
non-community water
systems. A
CWS or NTNCWS supplier must include
the following
elements in
printed materials (e.g.,
brochures and pamphlets) in the
same
order as listed in subsections
(a)(1)(A)
through (a)(1)(F).
In addition, the
supplier must
include the language set forth
in subsections
(a)(1)(A),
(a)(l)(B),
and (a)(1)(F) of this
Section in the materials, exactly
as written,
except for the text
in brackets in these subsections,
for which the supplier
must include
system-specific information.
Any additional information
presented by a supplier
must be consistent with the information
set forth in
subsections
(a)(1)(A)
through (a)(l)(F),
and the supplier must present
the
additional information
in plain language that can be
understood by the
general public. The supplier
must submit all written public education
materials
to the Agency prior to delivery,
as required
by
subsection
(a)(3)
of this Section.text
Get forth in Appendix E
of
this
Part in all of the printed
materials it distributes
through its lead public education
program. A
supplier may delete information
pertaining to lead service lines,
upon
approval
by the Agency by a SEP issued
pursuant to Section 611.110,
if
no lead service lines
exist anvhere in the water system service
area.
Public education language at
paragraphs (4)(B)(5) and (4)(D)(2)
of
Appendix E of this
Part may be modified regarding
building permit record
availability
and consumer access
to
these
records, if approved
by
the
Agency
by
a SEP issued
pursuant to Section 61 1.110. A
supplier may
also continue
to utilize pre printed materials
that meet the public education
language
requirements in 40
CFR
141.85
(1991). Any additional
information presented
by a supplier must be consistent
with the
information
in Appendix E
of
this Part
and be in plain English that can
be
understood by lay persons.
BO NOTE:
At coffesponding 40 CFR 141.85
(a(1) (2002), USEPA
allowed
the use of pre
printed copies of the public notices whose
content
met the requirements
of the original lead
and copper rule adopted on
June
7, 1991
(56
Fed.
Reg. 26548). Rather than reference aprior version
of this
Section of the Illinois
rules, the Board has retained the federal
reference to
the
prior requirements.
JCAR35O61
1-0815204r01
4289
IMPORTANT
INFORMATION
ABOUT
LEAD
IN YOUR
4290
DRiNKING
WATER.
[INSERT
NAME
OF SUPPLIER]
found
4291
elevated
levels
of
lead
in
drinking water
in some
homes/buildings.
4292
Lead
can cause serious
health
problems,
especially
for pregnant
4293
women
and young
children.
Please
read
this information
closely
to
4294
see
what
you
can
do
to
reduce lead
in your drinking
water.
4295
4296
BOARD
NOTE:
The supplier
must use
the
verbatim
text set forth
4297
in
this subsection
(a)(1)(A),
with
the exception
that the
supplier
4298
must
insert its
name in
place
of
the
bracketed
text.
4299
4300
Health
effects
of
lead.
Lead can
cause
serious
health
problems
if
4301
too
much
enters
your body
from
drinking
water
or other
sources.
4302
It
can cause
damage
to
the brain and
kidneys,
and can interfere
4303
with
the production
of red
blood
cells that
carry
oxygen
to all parts
4304
of
your body.
The
greatest
risk of
lead exposure
is to infants,
4305
young
children,
and pregnant
women.
Scientists
have linked
the
4306
effects
of lead
on
the
brain
with lowered
IQ
in
children.
Adults
4307
with
kidney problems
and
high blood
pressure
can be
affected
by
4308
low
levels
of
lead more
than healthy
adults.
Lead is stored
in
the
4309
bones, and
it can
be released
later
in life.
During
pregnancy,
the
4310
child
receives
lead from
the
mother’s
bones,
which
may affect
4311
brain development.
4312
4313
BOARD
NOTE:
The
supplier
must use
the
verbatim
text set
forth
4314
in this subsection
(a)(1)(B).
4315
4316
)
Sources
of Lead.
4317
4318
j)
Explain
what
lead is.
4319
4320
II
Explain
possible
sources
of lead in
drinking
water and
how
4321
lead
enters drinking
water.
Include
information
on home
4322
and
building
plumbing
materials
and
service
lines that
may
4323
contain
lead.
4324
4325
jjj
Discuss
other
important
sources
of
lead exposure
in
4326
addition
to
drinking
water
(e.g., paint).
4327
4328
BOARD
NOTE:
The
supplier
must
use
text that provides
the
4329
information
described
in this
subsection
(a)(1)(C).
4330
JCAR35O61 l-0815204r01
4331
]
Discuss
the steps the consumer can take to reduce his or her
4332
exposure to lead in drinking water.
4333
4334
Encourage running the water
to flush out the
lead.
4335
4336
ii)
Explain concerns with using hot water from the tap and
4337
specifically
caution
against the use of hot water for
4338
preparing baby formula.
4339
4340
jj)
Explain that boiling water does not reduce lead levels.
4341
4342
jy
Discuss other options consumers can take to reduce
4343
exposure to lead in
drinking
water, such as
alternative
4344
sources or treatment of water.
4345
4346
y)
Suggest that parents have their child’s blood tested for lead.
4347
4348
BOARD NOTE: The supplier must use text that provides the
4349
information described in this subsection
(a)(1)(D).
4350
4351
j)
Explain
why there are elevated
levels
of lead in the supplier’s
4352
drinking water
(if
known) and what the supplier
is
doing to reduce
4353
the lead levels in homes and buildings in this area.
4354
4355
BOARD NOTE: The supplier must use text that provides the
4356
information described in this subsection (a)(1)(E).
4357
4358
For more information, call us at
[iNSERT
THE SUPPLIER’S
4359
NUMBER] [(IF
APPLICABLE),
or visit our Web site at
[INSERT
4360
THE SUPPLIER’S WEB SITE
HERE]].
For more information on
4361
reducing
lead exposure around your home/building and
the
health
4362
effects of lead, visit USEPA’s Web site at http://www.epa.gov/lead
4363
or contact
your
health care provider.
4364
4365
BOARD NOTE: The supplier must use the verbatim text set forth
4366
in this subsection
(a)(1)(F),
with the exception that the supplier
4367
must insert
its name in
place of the first segment of bracketed text,
4368
and it must add the second segment of bracketed text and substitute
4369
its
Web address for the internal bracketed text.
4370
4371
2)
Community Non transient non community water systems. In addition to
4372
including the elements A NTNCWS must either include the text specified
4373
in subsection
(a)(1) of this Sections
or
must include the
text set forth in
JCAR35O61 1-0815204r01
4374
Appendix
F of this Part
in all
of the printed
materials it distributes
through
4375
its lead public education program. A water supplier may delete
4376
information
pertaining to
lead
service lines upon
approval
by the Agency
4377
by a SEP issued pursuant to Section
611.110 if no
lead service lines exist
4378
anywhere in the water system service area. Any additional information
4379
presented by a supplier must be consistent with the information below and
4380
be in plain English
that
can be understood
by lay
persons. a
CWS supplier
4381
must do both of the following:
4382
4383
It must tell consumers how to get their water
tested:
and
4384
4385
It must discuss lead in plumbing components and the difference
4386
between low-lead and lead-free
components.
4387
4388
Agency review and approval of written public education materials.
4389
4390
The supplier must submit all written public education materials
to
4391
the Agency for
review
at least 60 days prior to its planned date for
4392
delivery of the materials to the public.
4393
4394
If the Agency
determines
that the form and
content
of the
4395
supplier’s written
public
education materials is adequate, it may
4396
issue a SEP pursuant to Section 611.110 that expressly approves
of
4397
the materials.
4398
4399
A
supplier
may immediately distribute its written public education
4400
materials after receipt of a SEP or a revised SEP that expressly
4401
approves those materials.
4402
4403
If the Agency determines that the form or content of the written
4404
public
education materials
submitted by the
supplier does not
4405
comply with the requirements of this Section, it must issue a SEP
4406
pursuant to Section 611.110. The Agency may issue a revised
SEP
4407
that expressly
supercedes
a SEP previously issued under this
4408
subsection
(a)(1).
Any SEP or revised SEP issued by the Agency
4409
must identify any deficiencies in the written
public
education
4410
materials with specificity sufficient
to
guide the supplier to correct
4411
the deficiencies in a way that would address the Agency’s
4412
concerns.
4413
4414
The Agency must issue any SEP or revised SEP under subsection
4415
(a)(3)(D)
of this Section no later than 30 days after the date on
4416
which it received a copy
of the supplier’s
prospective written
JCAR35O61 1-0815204r01
4417
public education materials,
unless
the Agency
and
the
supplier
4418
have agreed
to a later date pursuant to subsection (a)(3)(F) of this
4419
Section. The Agency and
the supplier may agree to a longer time
4420
within which the Agency may issue a SEP or a revised SEP, in
4421
which case
the Agency must issue the SEP or revised SEP before
4422
expiration
of
the agreed longer
time.
4423
4424
BOARD
NOTE: The Board has provided that the Agency and the
4425
supplier may agree to a longer time before
the Agency issues a
4426
SEP and for the Agency to issue a revised SEP that supercedes
an
4427
already-issued SEP, in order
to
allow for negotiation
of any issues
4428
and
the quickest possible distribution of the materials.
4429
4430
If the supplier
has not
received
a SEP from the Agency within 45
4431
days after the date on which the Agency received its written
public
4432
education materials, those materials are deemed approved,
and the
4433
supplier may immediately proceed to distribute them.
4434
4435
Once the supplier has revised its written public education materials
4436
exactly
as described by the Agency in a SEP issued under
4437
subsection (a)(3)(D) of this Section, those materials are
deemed
4438
approved, and the supplier may
immediately
proceed to distribute
4439
them.
4440
BOARD NOTE: At corresponding 40 CFR 141.85(a’)(1) (2007),
USEPA
allowed the State to require prior approval of written public infonnation
materials. Rather than
require prior Agency approval, the Board has
chosen to require submission to the Agency for review sufficiently in
advance of distribution
to
allow
the
Agency
to
raise any deficiencies
that it
may perceive. The Board has used the mechanism of the SEP for the
Agency to communicate its concerns, as this would allow the supplier
to
petition the Board
for
review
of the Agency’s determination pursuant to
Section
611.110(c).
b
Content of broadcast materials. A supplier must include the following
information in all public service announcements
submitted
under its lead
public
education program to television and radio stations for broadcast:
Why should everyone want
to
imow
the facts about lead and
drinking
water? Because unhealthy amounts of lead can enter drinking water
through the plumbing
in your home. That’s why I urge you to do what I
did. I had my water tested for (insert
“free” or the cost per
sample).
You
can contact the (insert the name of the city or supplier) for information on
4441
4442
4443
4444
4445
4446
4447
4448
4449
4450
4451
4452
4453
4454
4455
4456
4457
4458
4459
JCAR35O61
1-0815204r01
testing
and
on simple
ways
to reduce
your
exposure
to lead
in drinking
water.
2)
To have your
water J
for lead,
r to get
nir
information
about
this
public health
concern,
please
call
(insert the
phone
number
of
the
city or
supplier).
be)
Delivery
of a-public
education
materialsprogram.
1)
The
public
education
materials
of a supplier
that
serves
In communities
where
a largesignificant
proportion
of
the
population
speaks a language
other than
non-English
speaking
consumers,
public
education
materials
must
contain information
be communicated
in
the appropriate
languages
regarding
the importance
of the
notice,
or it must
contain
a telephone
number or
address where
a person
served
may
contact
the supplier
to
obtain
a translated
copy
of the public
education
materials
or to request
assistance
in the appropriate
language.
2)
A
CWS
supplier that
exceeds the
lead action
level
on
the basis
of tap
water samples
collected
in
accordance
with
Section
611.356
and which
is
not already
conducting
repeating
public
education
tasks
pursuant
to
subsection
(c)(3),
(c)(7),
or (c)(S)
of this
Section must,
within
60 days
after
the end of
the monitoring
period
in which the
exceedance
occuned,
do
each of the
following
complete
the public
education
tasks
according
to
the following
requirements:
The
CWS
supplier
must
deliver
printed
materials
that
meet the
content
requirements
of subsection
(a)
of
this
Section
to all of
its
bill-paying
customers.
])
Methods
of
delivery
for a
CWS supplier.
The
CWS
supplier
must
contact customers
who
are most
at
risk by
delivering
education
materials
that meet
the content
requirements
of subsection
(a)
of
this
Section
to
local
public
health
agencies, even
if
the
agencies
are
not located
within
the supplier’s
service
area,
along with
an
informational
notice
that encourages
distribution
to all
of
the
agencies’
potentially
affected
customers
or the supplier’s
users. The
supplier
must contact
the local
public health
agencies
directly
by
phone or
in
person.
The
local
public
health
agencies
may
provide
a
specific list
of additional
community-based
organizations
that
serve
the target
t”_,t,i
4460
4461
4462
4463
4464
4465
4466
4467
4468
4469
4470
4471
4472
4473
4474
4475
4476
4477
4478
4479
4480
4481
4482
4483
4484
4485
4486
4487
4488
4489
4490
4491
4492
4493
4494
4495
4496
4497
4498
4499
4500
4501
4502
1CAR35061 1-0815204r01
4503
populations, which
may
include
organizations outside the
4504
service area of the supplier. If such lists are
provided,
the
4505
supplier
must deliver education materials that meet the
4506
content requirements
of
subsection (a)
of
this Section
to
4507
each
of the organizations on the provided lists.
4508
4509
jj)
The
CWS supplier must
contact customers
who are most at
4510
risk by delivering materials that meet the content
4511
requirements
of subsection
(a)
of this Section to the
4512
organizations listed in subsections
(b)(2)(H)(i)
through
4513
(b)(2)(H)(vi)
that are located within the supplier’s service
4514
area, along with an informational notice that encourages
4515
distribution
to all the
organization’s potentially
affected
4516
customers or supplier’s users.
4517
4518
BOARD
NOTE: The Board found it necessary to move the
4519
text of 40 CFR
141.85(b)(2)(ii)(B)(1)
through
4520
(b)(2)(ii)(B)(6) (2007),
as added at
72
Fed. Reg. 57782
4521
(Oct.
10,
2007),
to appear as subsection
(b)(2)(H)(i)
4522
through subsection
(b)(2)(H)(vi)
of this Section, in order
to
4523
comport
with Illinois
Administrative
Code codification
4524
requirements relating
to
allowed indent levels in rules.
4525
4526
jjfl
The CWS supplier must make a good faith effort to locate
4527
the
organizations listed in
subsections b)(2)(I)(i)
through
4528
(b)(2)(I)(iii) of this Section that are located within the
4529
service area and deliver materials that meet the content
4530
requirements of subsection
(a)
of this Section to them,
4531
along with an informational notice that encourages
4532
distribution to all potentially affected customers or users.
4533
The
good
faith
effort
to contact
at-risk
customers
may
4534
include requesting a specific contact list of these
4535
organizations from the local public health agencies, even
if
4536
the agencies are not located within the supplier’s service
4537
4538
4539
BOARD NOTE: The Board found it necessary to move
the
4540
text of 40 CFR
141.85(b)(2)(ii)(C)(])
through
4541
(b)(2)(ii)(C)(3)
(2007),
as added at 72 Fed. Reg. 57782
4542
(Oct.
10,
2007),
to appear as subsection
(b)(2X1)(i)
through
4543
subsection
(b)(2)(I)(iii)
of this Section, in order to comport
4544
with Illinois Administrative Code codification requirements
4545
relating to allowed indent levels in
rules.
JCAR35O61
1-0815204r01
4546
4547
)
No less oflen than quarterly,
the
CWS
supplier
must
provide
4548
information
on or in
each water bill as long
as the system exceeds
4549
the action level for lead.
The message on the
water bill must
4550
include
the following
statement exactly
as written, except for
the
4551
text in brackets
for which the supplier
must include system-
4552
specific information:
4553
4554
[INSERT
NAME
OF
SUPPLIER]
found high
levels of lead
4555
in drinking
water in some homes.
Lead can cause
serious
4556
health problems.
For
more
information please
call
4557
[INSERT
NAME OF
SUPPLIER]
For
visit
(INSERT
4558
SUPPLIER’S
WEB
SITE
HERE)!.
The message or
4559
delivery
mechanism can be
modified in consultation
with
4560
the Illinois
Environmental Protection
Agency, Division
of
4561
Public Water
Supply specifically,
the Agency may
allow a
4562
separate mailing
of public education
materials to customers
4563
if the water
system cannot place
the information on
water
4564
bills.
4565
4566
The
CWS
supplier
must
post material
meeting the
content
4567
requirements
of subsection (a) of this
Section on the supplier’s
4568
Web site
if the
CWS
supplier serves
a population greater
than
4569
100,000.
4570
4571
j)
The
CWS supplier must submit
a press release to
newspaper,
4572
television,
and radio
stations.
4573
4574
In addition
to subsections (b)(2)(A)
through
(b)(2)(E)
of this
4575
Section,
the CWS supplier
must implement at least
three activities
4576
from one
or more of the categories
listed below. The
educational
4577
content and selection
of these
activities must be
determined in
4578
consultation
with the Agency.
4579
4580
Public
Service Announcements.
4581
4582
jj)
Paid
advertisements.
4583
4584
jjj)
Public
Area Information
Displays.
4585
4586
jy)
E-mails
to customers.
4587
4588
y
Public Meetings.
JCAR35O61
1-0815204r01
4589
4590
yj
Household
Deliveries.
4591
4592
yji
Targeted
Individual Customer
Contact.
4593
4594
yjji
Direct material distribution
to all
multi-family homes
and
4595
institutions.
4596
4597
j
2)
Other methods
approved by the
State.
4598
4599
For
a CWS supplier that
is required to
conduct monitoring
4600
annually
or less frequently,
the end of the monitoring
period is
4601
September
30 of
the calendar year
in which the sampling
occurs,
4602
or, if
the Agency has established
an alternate
monitoring
period,
by
4603
a SEP issued
pursuant to Section
611.110, the last day
of that
4604
period.
4605
4606
Organizations
that the CWS
supplier
must contact when
required
4607
to do so pursuant
to subsection
(b)(2)(B)(ii)
of this Section.
4608
4609
j)
Public and private
schools
or
school boards.
4610
4611
jj
Women, Infants
and Children
(WIC)
and Head Start
4612
programs.
4613
4614
jjj
Public and
private hospitals and
medical clinics.
4615
4616
yj).
Pediatricians.
4617
4618
y)
Family planning
clinics.
4619
4620
yj)
Local welfare
agencies.
4621
4622
BOARD
NOTE:
This
subsection
(b)(2)(H) corresponds
with 40
4623
CFR
141.85(b)(2)(ii)(B)(1)
through
(b)(2)(ii)(B)(6)
(2007).
as
4624
added at 72 Fed. Reg.
57782
(Oct.
10,
2007). The
Board found
it
4625
necessary
to move the
text of those federal provisions
to comport
4626
with Illinois Administrative
Code codification
requirements
4627
relating
to allowed
indent
levels in rules.
4628
4629
j)
Organizations
that the
CWS
supplier
must contact when
required
4630
to do so pursuant
to subsection
(b)(2)(B)(iii)
of this
Section.
4631
JCAR35O61
1-0815204r01
4632
Licensed
childcare centers.
4633
4634
j)
Public
and
private preschools.
4635
4636
jj
Obstetricians,
gynecologists
and midwives.
4637
4638
BOARD
NOTE:
This
subsection
(b)(2)(H)
corresponds
with 40
4639
CFR 141
.85(b)(2)(ii)(C)(1)
through
(b)(2)(ii)(C)(3)
(2007), as
4640
added at 72
Fed. Reg. 57782
(Oct.
10, 2007).
The Board found it
4641
necessary
to move
the text
of those federal provisions
to comport
4642
with Illinois Administrative
Code
codification requirements
4643
relating
to allowed
indent levels
in rules.
4644
4645
)
As long
as a
CWS supplier
exceeds the action
level, it must
repeat the
4646
activities described
in subsection
(b)(2)
of this Section, as described
in
4647
subsections
(b)(3)(A)
through (b)(3)(D) of
this Section.
4648
4649
A
CWS
supplier
must repeat the tasks
contained in
subsections
4650
(b)(2)(A),
(b)(2)(B)
and (b)(2)(D)
of this Section every
12 months.
4651
4652
J
A
CWS
supplier
must repeat tasks
contained in subsection
4653
(b)(2)(C) of this
Section with
each billing cycle.
4654
4655
A
CWS
supplier serving a
population
greater
than 100,000 must
4656
post and
retain
material
on a publicly accessible
Web site
pursuant
4657
to
subsection
(b)(2)(D) of
this
Section.
4658
4659
The
CWS supplier must repeat
the task
in subsection (b)(2)(E)
of
4660
this Section
twice
every
12 months on a schedule
agreed
upon with
4661
the Agency
by a SEP issued
pursuant to
Section 611.110. The
4662
Agency must,
on a
case-by-case
basis, by a
SEP issued pursuant
to
4663
Section
611.110, extend the
time for the
supplier to complete
the
4664
public education
tasks set forth
in subsection
(b)(2)
of this
Section
4665
beyond the
60-day limit if
it determines that the
extended
time
is
4666
needed
for
implementation
purposes;
however,
the Agency must
4667
issue the SEP
granting any
extension prior
to
expiration
of the
60-
4668
day deadline.
4669
4670
A)
Insert notices
in
each
customers water utility
bill
or
disseminate
to
4671
each
customer
by
separately
mailing a notice
containing the
4672
information
required by
subsection
(a(1) of this Section,
along
4673
with
the
following
alert in large print on
the water bill
itself:
4674
“SOME HOMES IN THIS
COMMUNITY
HAVE ELEVATED
V
r
-J
-4
r
c
I
a
C
4-
C
C
C
-
--
-
J
4-
t
•-•1
‘-4
I
JCAR35O61
1-0815204r01
4718
4719
Those of
subsections (c)(2)(A)
tlough
(c)(2)(C) of this Section,
4720
every 12
months; and
4721
4722
B
Those of
subsection (c)(2)(D)
of this
Section,
eve
six months.
4723
4724
4)
Within
60 days after the end of
the
monitoring
period in which a
4725
NTNCWS supplier
it-exceeds
the lead action
level (unless it
already is
4726
repeating
public education tasks
pursuant to
subsection
(b)(5)(c)(5) of this
4727
Section),
a NTNCWS supplier
must
deliver the public education
4728
materials
specified
by
subsection
(a) of this
Sectioncontained in
Appendix
4729
E or F of this
Part,
as in subsections
(b)(4)(A)
and
(b)(4)(B)
of this
4730
Section,
subject to the limitation
set forth in
subsection
(b)(4)(C) of this
4731
Sectionfollows:
4732
4733
A)
The
NTNCWS
supplier
must post Post
informational
posters on
4734
lead in
drinking water
in a public
place
or common area in
each
of
4735
the buildings
served
by the supplier; and
4736
4737
B)
The
NTNCWS supplier
must distribute
Distribute
informational
4738
pamphlets
or brochures
on lead in drinking
water
to each person
4739
served by the NTNCWS
supplier.
The Agency may,
by
a SEP
4740
granted
pursuant
to Section 611.110,
allow the system
to utilize
4741
electronic transmission
in lieu
of or combined
with printed
4742
materials as long
as it achieves
at least the same
coverage.
4743
4744
)
For a NTNCWS
supplier that
is required to conduct
monitoring
4745
annually
or less frequently, the
end of the monitoring
period is
4746
September 30
of the
calendar
year in which the
sampling occurs,
4747
or, if
the
Agency has established
an
alternate
monitoring
period,
by
4748
a SEP issued
pursuant
to
Section
611.110, the last
day of that
4749
period.
4750
4751
5)
A NTNCWS
supplier must
repeat the tasks
set forthcontained
in
4752
subsection
(he)(4)
of
this Section at least
once during each
calendar year
4753
in which
the supplier exceeds
the lead
action level. The Agency
must, on
4754
a case-by-case
basis,
by a SEP issued
pursuant
to Section
611.110, extend
4755
the
time for the
supplier
to complete the
public
education
tasks set forth in
4756
subsection
(b)(2)
of this
Section
beyond
the 60-day limit
if it
determines
4757
that
the extended
time is needed for
implementation
purposes; however,
4758
the Agency must
issue the SEP granting
any
extension
prior to expiration
4759
of the 60-day deadline.
4760
JCAR35O61
1-0815204r01
4761
6)
A supplier
may
discontinue
delivery
of public education
materials
after
it
4762
has met
the lead action
level
during
the most
recent
six-month
monitoring
4763
period
conducted
pursuant
to Section
611.356.
Such a supplier
must
begin
4764
public
education
anew
in
accordance
with this
Section
if
it subsequently
4765
exceeds
the lead
action level
during any
six-month
monitoring
period.
4766
4767
7)
A CWS supplier
may
apply
to the
Agency,
in writing,
to use only
the text
4768
specified
in subsection
(a)(l)
of this
Section
Appendix
F
of this
Part in
4769
lieu of the
text in subsections
(a)(1)
and (a)(2)
of this Section
Appendix
E
4770
of
this Part
and
to
perform
the tasks
listed
in
subsections
(b)(4)(c)(4)
and
4771
(b)(5)(c)(5)
of this Section
in lieu
of the tasks
in subsections
(b)(2)(c)(2)
4772
and
(b’)(3)(c)(3)
of
this Section
if the
following
are
true:
4773
4774
A)
The supplier
is a
facility, such
as a
prison
or a hospital,
where
the
4775
population
served
is not capable
of or
is
prevented from
making
4776
improvements
to
plumbing
or installing
point of use
treatment
4777
devices;
and
4778
4779
B)
The system
provides
water
as part of
the
cost of services
provided,
4780
and it
does not separately
charge
for water
consumption.
4781
4782
A
CWS
supplier
that
serves
3,300
or fewer
people
may limit
certain
4783
aspects of its
public education
programs
as
follows:
4784
4785
)
With respect
to
the requirements
of subsection
(b)(2)(F)
of this
4786
Section,
a
supplier
that
serves
3,300
or fewer
people must
4787
implement
at least one
of the activities
listed
in that subsection.
4788
4789
With respect
to
the
requirements
of subsection
(b)(2)(B)
of this
4790
Section,
a supplier
that
serves
3,300 or
fewer
people may
limit
the
4791
distribution
of the
public
education
materials
required
under that
4792
subsection
to
facilities
and organizations
that
it serves which
are
4793
most
likely
to be
visited regularly
by
pregnant women
and
4794
children.
4795
4796
With
respect
to the requirements
of
subsection
(b)(2)(E)
of this
4797
Section,
the Agency
may,
by a SEP
issued
pursuant
to Section
4798
611.110,
waive
this requirement
for
a
supplier
that serves
3,300
or
4799
fewer
persons,
as
long
as the supplier
distributes
notices
to every
4800
household
that it
serves.
4801
4802
)
Reduced
requirements
for
certain smaller
CWS
suppliers.
4803
4804
4805
4806
4807
4808
4809
4810
4811
4812
4813
4814
4815
4816
4817
4818
4819
4820
4821
4822
4823
4824
4825
4826
4827
4828
4829
4830
4831
4832
4833
4834
4835
4836
4837
4838
4839
4840
4841
4842
4843
4844
4845
4846
JCAR35O61
1-0815204r01
A
A CWS
supplier
serving 3,300
or
fewer people
ffly
contained
in
subsection
(c)(2)(D)
of this
Section. As
long as it
distributes
notices
containing
the
information
contained
in
Appendix
E of
this
Part
to
every household
served
by
the system,
such
a supplier
may
further
limit its public
education
proams
as
follows:
A
supplier
serving
500 or fewer
people
may forego
the task
contained
in subsection
(c)(2)(B)
of
this
Section.
Such a
system
may
limit
the
distribution
of
the
public education
materials
required
under subsection
(c)(2)(C
nth
Section
to
facilities
and organizations
served
by the
supplier
‘
are
most likely
to be
visited regularly
by
pregnant
women and
children,
unless
it
is notified
by the
Agency
in
writing that
it
must
make
a broader
distribution.
If
approved
by the Agency
by
a
SEP issued
pursuant
to
Section
611.110, a
system serving
501 to
3,300
people
may
omit
the
task
in subsection
(c)(2)(B)
of this
Section or
limit
the distribution
of
the public
education materials
required
under
subsection
(c)(2)(C)
of this Section
to
facilities
and
organizations
served by
the system
that
are most likely
to
be
visited
regularly
by
pregnant
women
and children.
A
CWS
supplier serving
3,300
or
fewer people
that delivers
public
education
in
accordance
with subsection
(c)(8)(A)
of this
Section
must repeat
the
required
public
education
tasks
at
least
during
each calendar
year in
which
the supplier
exceeds
the lead
action
level.
c4)
Supplemental
monitoring
and notification
of
results. A
supplier
that fails
to
meet
the lead action
level
on the basis
of tap
samples
collected
in accordance
with
Section
611.356
must offer
to
sample
the tap
water
of any
customer
who
requests
it. The
supplier
is not required
to pay
for collecting
or
analyzing
the
sample,
nor
is the
supplier
required
to collect
and analyze
the
sample itself.
ç)
Requirement
for consumer
notice
of
tap
water
monitoring
results.
jJ
Consumer
notice
requirement.
A supplier
must
provide
a notice
of the
individual
tap
results from
lead
tap
water
monitoring
carried out
under the
requirements
of
Section
611.356
to the
persons served
by the
water system
at
the specific
sampling
site from which
the sample
was
taken
(e.g.,
the
occupants
of
the
residence
where
the tap was
tested).
JCAR35O61
1-0815204r01
4847
4848
)
Timing
of
consumer notice.
The
supplier
must
provide
the
consumer
4849
notice as
soon as practical,
but
no later than
30
days
after it learns
of the
4850
tap
monitoring
results.
4851
4852
)
Content
of consumer
notice.
The consumer
notice
must include
the
results
4853
of lead
tap water
monitoring
for the tap
that was
tested, an
explanation
of
4854
the health
effects
of lead,
steps
consumers
can
take
to reduce
exposure
to
4855
lead
in drinking
water,
and
contact information
for
the water
utility.
The
4856
notice
must also
provide
the
maximum
contaminant
level
goal and the
4857
action
level for
lead
and
the
definitions
for
these
two terms
from
Section
4858
611.883(c).
4859
4860
4)
Delivery
of consumer
notice.
The consumer
notice
must be provided
to
4861
persons
served
at the tap
that
was tested,
either by
mail
or by
another
4862
method
approved
by
the Agency,
by
a SEP
issued
pursuant to
Section
4863
611.110.
For example,
upon approval
by the
Agency,
a NTNCWS
4864
supplier
could post
the results
on a bulletin
board
in the facility
to allow
4865
users
to
review
the
information.
The
supplier must
provide
the notice
to
4866
customers
at sample
taps
tested,
including
consumers
who do
not receive
4867
water
bills.
4868
4869
BOARD
NOTE:
Derived
from
40
CFR
141.85 (2007),
as
amended
at 72
Fed. Reg.
4870
57782
(October
10,
2007)(2002).
4871
4872
(Source:
Amended
at 33
Ill. Reg.
effective
4873
4874
Section
611.356
Tap
Water
Monitoring
for Lead
and Copper
4875
4876
a)
SamplingSample
site
location.
4877
4878
1)
Selecting
a pool
of
targeted
sampling
sites.
4879
4880
A)
By the
applicable
date for commencement
of monitoring
under
4881
subsection
(d)(1)
of
this
Section,
each
supplier
must
complete
a
4882
materials
evaluation
of its distribution
system in order
to identify
a
4883
pool
of targeted
sampling
sites that meets
the
requirements
of this
4884
Section.
4885
4886
B)
The
pool of
targeted sampling
sites
must be sufficiently
large to
4887
ensure
that
the
supplier
can collect
the
number
of lead
and copper
4888
tap
samples
required by
subsection
(c) of
this
Section.
4889
JCAR35O61
1-0815204r01
4890
C)
The supplier
must
select
the sites
for collection
of first
draw
4891
samples
from this
pool of
targeted
sampling
sites.
4892
4893
D)
The
supplier must
not
select as sampling
sites
any faucets
that
have
4894
point-of-use
or point-of-entry
treatment
devices designed
to
4895
remove
or
capable of
removing
inorganic contaminants.
4896
4897
2)
Materials
evaluation.
4898
4899
A)
A
supplier
must
use the
information
on
lead, copper,
and
4900
galvanized
steel collected
pursuant
to
40
CFR
141.42(d)
(special
4901
monitoring
for corrosivity
characteristics)
when conducting
a
4902
materials
evaluation.
4903
4904
B)
When
an evaluation
of
the
information
collected
pursuant
to
40
4905
CFR
141.42(d)
is
insufficient
to
locate
the
requisite
number
of
lead
4906
and
copper sampling
sites
that
meet the targeting
criteria
in
4907
subsection
(a) of
this
Section, the
supplier
must review
the
4908
following
sources
of information
in order
to identify
a sufficient
4909
number
of
sampling sites:
4910
4911
i)
All
plumbing
codes,
permits, and
records
in the files
of the
4912
building
departments
that indicate
the plumbing
materials
4913
that are installed
within
publicly-
and
privately-owned
4914
structures
connected
to the distribution
system;
4915
4916
ii)
All inspections
and
records
of the
distribution
system
that
4917
indicate the
material
composition
of
the
service
4918
connections
which
connect
a
structure to
the
distribution
4919
system;
4920
4921
iii)
All existing
water quality
information,
which includes
the
4922
results
of
all
prior
analyses of
the system
or individual
4923
structures
connected
to the
system,
indicating
locations
that
4924
may
be
particularly
susceptible
to high lead
or copper
4925
concentrations;
and
4926
4927
iv)
The supplier
must
seek to collect
such
information
where
4928
possible
in the course
of its
normal
operations
(e.g.,
4929
checking
service
line materials
when
reading water
meters
4930
or performing
maintenance
activities).
4931
4932
3)
Tiers
of sampling
sites.
Suppliers
must
categorize
the sampling
sites
JCAR35O61
1-0815204r01
4933
within their
pool
according
to
the
following
tiers:
4934
4935
A)
CWS
Tier
1 sampling
sites. ‘CWS
Tier
1
sampling
sites” must
4936
include
the
following
single-family
structures:
4937
4938
i)
Those that
contain copper
pipes
with
lead
solder installed
4939
after 1982
or
which
contain lead
pipes; or
4940
4941
ii)
Those
that are served
by a lead
service
line.
4942
4943
BOARD
NOTE:
Subsection
(a)(3)(A)
was
derived
from segments
4944
of 40
CFR
141.86(a)(3)
(2007)(2003).
This
allows
the pool
of
4945
CWS
tier 1 sampling
sites
to consist
exclusively
of
structures
4946
served
by lead
service
lines.
4947
4948
B)
CWS
Tier 2
sampling
sites.
??cwS
Tier
2
sampling
sites??
must
4949
include
the
following
buildings,
including
multiple-family
4950
structures:
4951
4952
i)
Those that
contain copper
pipes
with
lead
solder installed
4953
after 1982
or
contain
lead pipes;
or
4954
4955
ii)
Those
that are served
by a lead
service line.
4956
4957
BOARD NOTE:
Subsection
(a)(3)(B)
was derived
from
segments
4958
of
40
CFR
141
.86(a)(4)
(2007)(2003).
This
allows the pool
of
4959
CWS tier
2 sampling
sites to consist
exclusively
of
structures
4960
served
by
lead
service lines.
4961
4962
C)
CWS
Tier
3
sampling sites.
??CWS
Tier
3
sampling
sites??
must
4963
include
the
following
single-family
structures:
those that
contain
4964
copper
pipes
with lead
solder installed
before
1983.
4965
4966
BOARD
NOTE:
Subsection
(a)(3)(C)
was
derived
from
segments
4967
of 40
CFR 141
.86(a)(5) (2007)(2003).
4968
4969
D)
NTNCWS
Tier 1
sampling
sites.
??NTNCWS
Tier
1 sampling
4970
sites??
must include
the
following buildings:
4971
4972
i)
Those
that contain
copper
pipes
with
lead solder
installed
4973
after
1982 or
which contain
lead pipes;
or
4974
4975
ii)
Those
that are
served
by a lead
service
line.
JCAR35O61
1-0815204r01
4976
4977
BOARD
NOTE: Subsection
(a)(3)(D)
was derived from segments
4978
of 40 CFR
141.86(a)(6)
(2007)(2003). This
allows
the pool
of
4979
NTNCWS
tier 1 sampling
sites to consist
exclusively of
buildings
4980
served
by
lead
service
lines.
4981
4982
E)
Alternative
NTNCWS
sampling sites.
“Alternative
NTNCWS
4983
sampling
sites”
must
include the following
buildings:
those that
4984
contain
copper
pipes with lead solder
installed
before
1983.
4985
4986
BOARD
NOTE:
Subsection (a)(3)(E)
was derived
from segments
4987
of 40
CFR 141.86(a)(7)
(2007)(2003).
4988
4989
4)
Selection
of
sampling
sites.
Suppliers must select
sampling
sites for their
4990
sampling pooi as
follows:
4991
4992
A)
CWS
Suppliers.
CWS
suppliers must
use CWS tier 1 sampling
4993
sites,
except that the
supplier may include
CWS
tier 2 or
CWS tier
4994
3 sampling
sites in its
sampling pooi as
follows:
4995
4996
i)
If multiple-family
residences
comprise at least 20
percent
4997
of the structures
served
by a supplier, the supplier
may
use
4998
CWS
tier 2 sampling sites in
its sampling
pool; or
4999
5000
BOARD
NOTE:
Subsection
(a)(4)(A)(i)
was derived
from
5001
a
segment of 40 CFR 141.86(a)(3)(ii)
(2007)(2003).
5002
5003
ii)
If
the CWS supplier has
an insufficient
number of
CWS tier
5004
1 sampling
sites
on
its distribution system,
the supplier
may
5005
use
CWS tier 2 sampling
sites in its sampling
pool; or
5006
5007
BOARD NOTE:
Subsection
(a)(4)(A)(ii) was
derived from
5008
a segment
of 40 CFR 141.86(a)(4)
(2007)(2003).
5009
5010
iii)
If the
CWS supplier has an
insufficient
number
of
CWS
tier
5011
1 and
CWS
tier 2
sampling
sites on its distribution
system,
5012
the
supplier
may complete its
sampling
pool
with
CWS
tier
5013
3 sampling
sites.
5014
5015
BOARD
NOTE: Subsection
(a)(4)(A)(iii)
was derived
5016
from a
segment of 40
CFR 141.86(a)(5) (2007)(2003).
5017
5018
iv)
If the
CWS supplier
has an
insufficient
number of
CWS tier
JCAR35O61
1-0815204r01
5019
1
sampling sites,
CWS
tier 2
sampling sites, and
CWS tier
5020
3 sampling sites,
the supplier must
use those
CWS tier 1
5021
sampling sites,
CWS tier
2
sampling sites, and
CWS tier 3
5022
sampling
sites that it has and complete
its sampling
pool
5023
with representative
sites throughout
its distribution
system
5024
for the balance
of its
sampling
sites. For the
purpose
of this
5025
subsection
(a)(4)(A)(iv), a representative
site is a site
in
5026
which the
plumbing
materials
used at that
site would be
5027
commonly
found at other
sites served by
the water
system.
5028
5029
BOARD
NOTE: Subsection
(a)(4)(A)(iv)
was derived
5030
from segments
of
40
CFR
141.86(a)(5) (2007)(2003).
5031
5032
B)
NTNCWS
suppliers.
5033
5034
i)
An
NTNCWS
supplier must select
NTNCWS
tier 1
5035
sampling sites
for
its sampling
pool.
5036
5037
BOARD NOTE:
Subsection
(a)(4)(B)(i) was
derived from
5038
segments
of 40 CFR 141.86(a)(6)
(2007)(2003).
5039
5040
ii)
If the NTNCWS
supplier
has an insufficient
number
of
5041
NTNCWS
tier 1 sampling
sites, the supplier
may complete
5042
its
sampling pooi with
alternative
NTNCWS
sampling
5043
sites.
5044
5045
BOARD
NOTE: Subsection
(a)(4)(B)(ii)
was derived
from
5046
segments
of 40 CFR
141.86(a)(7) (2007)(2003).
5047
5048
iii)
If
the NTNCWS supplier
has an insufficient
number
of
5049
NTNCWS
tier
1 sampling
sites and
NTNCWS alternative
5050
sampling
sites, the supplier
must use
representative sites
5051
throughout
its distribution
system. For the
purpose of
this
5052
subsection
(a)(4)(B)(ii),
a representative
site is a site in
5053
which
the plumbing
materials used at that
site would
be
5054
commonly
found at other
sites served
by the water system.
5055
5056
BOARD
NOTE: Subsection
(a)(4)(B)(iii)
was derived
5057
from segments
of
40
CFR 141.86(a)(7) (2007)(2003).
5058
5059
C)
Suppliers with
lead service
lines.
Any supplier
whose
distribution
5060
system contains
lead
service
lines must
draw samples during
each
5061
six-month
monitoring period
from sampling
sites
as
follows:
JCAR35O61 1-0815204r01
5062
5063
i)
50 percent
of the samples from
sampling
sites that contain
5064
lead
pipes
or from
sampling
sites that have copper
pipes
5065
with lead
solder; and
5066
5067
ii)
50 percent
of those
samples from sites served
by a lead
5068
service
line.
5069
5070
iii)
A
supplier that cannot
identify a sufficient
number
of
5071
sampling
sites served
by a lead service
line must collect
5072
first-draw
samples from
all of the sites
identified as
being
5073
served
by such lines.
5074
5075
BOARD
NOTE:
Subsection
(a)(4)(C) was derived
from
segments
5076
of 40 CFR 141.86(a)(8)
(2007)(2003).
This allows
the pool of
5077
sampling
sites
to consist exclusively
of structures
or buildings
5078
served by lead service
lines.
5079
5080
b)
Sample
collection
methods.
5081
5082
1)
All
tap samples for lead
and copper collected
in accordance
with this
5083
Subpart
G,
with the exception
of lead
service line
samples collected under
5084
Section
611.354(c)
and samples
collected under subsection
(b)(5)
of this
5085
Section, must be
first-draw samples.
5086
5087
2)
First-draw
tap
samples.
5088
5089
A)
Each
first-draw tap
sample for lead and
copper must
be one liter
in
5090
volume and
have
stood
motionless in the
plumbing system
of
each
5091
sampling
site for at least six
hours.
5092
5093
B)
First-draw samples
from residential
housing
must be collected
5094
from the
cold water kitchen
tap or bathroom
sink
tap.
5095
5096
C)
First-draw
samples from a
non-residential building
must be
one
5097
liter in volume
and
must be
collected
at
an interior tap from which
5098
water
is typically
drawn
for consumption.
5099
5100
D)
Non-first-draw
samples
collected in lieu
of first-draw samples
5101
pursuant
to subsection
(b)(5) of this Section
must be
one liter in
5102
volume and
must be collected
at an
interior tap from which
water
5103
is typically
drawn
for consumption.
5104
JCAR35O61
l-0815204r01
5105
E)
First-draw
samples
may
be collected
by
the
supplier
or
the supplier
5106
may allow
residents
to collect
first-draw
samples
after
instructing
5107
the
residents
of the
sampling
procedures
specified
in
this
5108
subsection
(b).
5109
5110
i)
To
avoid
problems
of residents
handling
nitric
acid,
5111
acidification
of
first-draw
samples
may be
done
up
to 14
5112
days
after
the sample
is collected.
5113
5114
ii)
After
acidification
to resolubilize
the
metals,
the
sample
5115
must
stand
in
the original
container
for the
time
specified
in
5116
the
approved
USEPA
method
before
the
sample
can
be
5117
analyzed.
5118
5119
F)
If
a
supplier
allows
residents
to perform
sampling
under
subsection
5120
(b)(2)(D)
of
this Section,
the
supplier
may
not challenge
the
5121
accuracy
of
sampling
results
based
on
alleged
errors
in
sample
5122
collection.
5123
5124
3)
Service
line
samples.
5125
5126
A)
Each
service
line
sample
must be
one
liter
in volume
and
have
5127
stood
motionless
in the
lead
service
line
for at least
six
hours.
5128
5129
B)
Lead
service
line
samples
must
be collected
in
one of
the
following
5130
three ways:
5131
5132
i)
At the tap
after
flushing
that
volume
of
water calculated
as
5133
being
between
the
tap and
the
lead service
line
based
on the
5134
interior
diameter
and
length of
the
pipe
between
the tap
and
5135
the
lead
service
line;
5136
5137
ii)
Tapping
directly
into the
lead
service
line;
or
5138
5139
iii)
If
the sampling
site
is a single-family
structure,
allowing
5140
the
water
to
run until
there
is a significant
change
in
5141
temperature that
would
be
indicative
of
water
that
has been
5142
standing
in the
lead
service
line.
5143
5144
4)
Follow-up
first-draw
tap
samples.
5145
5146
A)
A
supplier
must
collect
each
follow-up
first-draw
tap
sample
from
5147
the
same
sampling
site
from
which
it
collected
the
previous
JCAR35O61
1-0815204r01
5148
samples.
5149
5150
B)
If,
for any reason,
the supplier
cannot
gain
entry
to
a sampling
site
5151
in order
to collect
a follow-up
tap
sample,
the supplier
may
collect
5152
the
follow-up
tap
sample
from another
sampling
site in
its
5153
sampling
pool,
as
long
as the new
site meets
the same
targeting
5154
criteria
and is
within reasonable
proximity
of
the original
site.
5155
5156
5)
Substitute
non-first-draw
samples.
5157
5158
A)
A NTNCWS
supplier
or a CWS
supplier
that
meets
the criteria
of
5159
Sections 611.355(be)(7)(A)
and
(be)(7)(B),
that does
not have
5160
enough
taps that
can supply
first-draw
samples,
as defined
in
5161
Section 611.102,
may
apply to the
Agency
in writing
to substitute
5162
non-first-draw
samples
by a SEP
granted
under
Section
611.110.
5163
5164
B)
A
supplier approved
to
substitute
non-first-draw
samples
must
5165
collect
as
many
first-draw
samples
from
appropriate
taps
as
5166
possible
and
identify sampling
times
and
locations
that
would
5167
likely result
in the longest
standing
time for
the
remaining
sites.
5168
5169
C)
The Agency
may
grant
a SEP that
waives the
requirement
for
prior
5170
Agency
approval of
non-first-draw
samplingsample
sites selected
5171
bythesystem.
5172
5173
c)
Number of
samples.
5174
5175
1)
Suppliers
must
collect
at
least one
sample
from the
number
of sites
listed
5176
in the
first
column of
Table
D
of
this Part (labelled
“standard
monitoring”)
5177
during
each six-month
monitoring
period specified
in subsection
(d)
of
5178
this
Section.
5179
5180
2)
A supplier
conducting
reduced
monitoring
pursuant
to subsection
(d)(4)
of
5181
this Section
must
collect
one
sample
from the
number
of sites
specified
in
5182
the second
column
of Table
D of this
Part (labelled
“reduced
monitoring”)
5183
during
each reduced
monitoring
period
specified
in
subsection
(d)(4)
of
5184
this
Section. Such
reduced
monitoring
sites must
be representative
of the
5185
sites
required
for standard
monitoring.
A supplier
whose
system has
fewer
5186
than
five drinking
water
taps
that
can be used
for
human consumption
and
5187
which
can meet
the sampling
site criteria
of subsection
(a)
of this Section
5188
to reach the
required number
of sampling
sites
listed in
this subsection
(c)
5189
must
collect multiple
samples
from
individual
taps.
To accomplish
this,
5190
the supplier
must collect
at least
one sample
from
each
tap, then it
must
JCAR35O61 1-0815204r01
5191
collect additional
samples
from those same taps
on different
days during
5192
the monitoring
period,
in order to collect a
total number of samples
that
5193
meets the
required number
of sampling
sites. Alternatively,
the Agency
5194
must, by
a SEP
issued
pursuant to Section
611.110, allow a
supplier
5195
whose
system has fewer
than five drinking
water taps to collect
a number
5196
of samples
that is fewer
than the number
of sites specified
in this
5197
subsection
(c)
if
it determines that 100
percent
of all
taps that can be used
5198
for human consumption
are sampled
and that the reduced
number of
5199
samples
will produce
the same results
as
would the
collection of multiple
5200
samples from some
taps. Any Agency
approval of a reduction
of the
5201
minimum
number
of samples must be
based
on a request
from the supplier
5202
or on on-site verification
by the Agency.
The Agency may,
by a SEP
5203
issued
pursuant
to Section 611.110, specify
sampling locations
when
a
5204
system
is conducting
reduced monitoring.
5205
5206
d)
Timing
of monitoring.
5207
5208
1)
Initial tap
sampling.
5209
5210
The first six-month monitoring
period
for small, medium-sized
and large
5211
system
suppliers
must begin on the dates
specified in Table
B of this Part.
5212
5213
A)
All large
system suppliers
must monitor during
each of two
5214
consecutive
six-month periods.
5215
5216
B)
All small-
and medium-sized
system suppliers
must monitor
during
5217
each
consecutive six-month
monitoring
period until the following
5218
is true:
5219
5220
i)
The supplier exceeds
the
lead action
level or the copper
5221
action
level and
is therefore required
to implement the
5222
corrosion control treatment
requirements
under Section
5223
611.351,
in which case
the supplier must
continue
5224
monitoring in accordance
with subsection
(d)(2)
of this
5225
Section;
or
5226
5227
ii)
The
supplier
meets
the
lead action level
and the copper
5228
action level during
each of two
consecutive six-month
5229
monitoring periods,
in which case the
supplier may
reduce
5230
monitoring in
accordance with subsection
(d)(4) of this
5231
Section.
5232
5233
2)
Monitoring
after installation
of corrosion control
and source water
JCAR35O61
1-0815204r01
5234
treatment.
5235
5236
A)
Any large system supplier that installs optimal
corrosion
control
5237
treatment pursuant
to Section 611.351 (d)(4) must have monitored
5238
during each of two consecutive
six-month monitoring periods
5239
before January 1, 1998.
5240
5241
B)
Any small- or medium-sized
system supplier that installs optimal
5242
corrosion control treatment pursuant
to
Section 61
1.35
1(e)(5)
must
5243
monitor during each
of two consecutive six-month monitoring
5244
periods before 36 months after the Agency approves optimal
5245
corrosion control treatment,
as specified in Section 611.35 1(e)(6).
5246
5247
C)
Any supplier that installs source water treatment
pursuant to
5248
Section 61 1.353(a)(3)
must monitor during each of two
5249
consecutive six-month monitoring periods before 36 months
after
5250
completion of step 2,
as specified in Section 611.353(a)(4).
5251
5252
3)
Monitoring after the Agency
specification of water quality parameter
5253
values for optimal corrosion control.
5254
After the Agency specifies the values for water quality control parameters
5255
pursuant to Section 611.352(f),
the supplier must monitor during each
5256
subsequent six-month monitoring
period, with the first six-month
5257
monitoring period to begin on the date the Agency specifies the
optimal
5258
values.
5259
5260
4)
Reduced monitoring.
5261
5262
A)
Reduction
to annual for small- and medium-sized system suppliers
5263
meeting the lead and copper action
levels. A small- or medium-
5264
sized system
supplier that meets the lead and copper action levels
5265
during each of two consecutive six-month monitoring periods
may
5266
reduce the number of samples
in accordance with subsection (c) of
5267
this Section,
and reduce the frequency of sampling to once per
5268
year. A small- or medium-sized
system
supplier that
collects
5269
fewer
than five samples as specified in subsection
(c)
of this
5270
Section and which meets the
lead and copper action levels during
5271
each of two consecutive six-month monitoring periods may
reduce
5272
its frequency
of sampling to once per year. In no case can the
5273
supplier reduce the
number of samples required below the
5274
minimum of one sample per available
tap.
This reduced
sampling
5275
may only begin during the calendar year
immediately
following
5276
the end of the second
consecutive six-month monitoring period.
JCAR35O61
1-0815204r01
5277
5278
B)
SEP
allowing
reduction to
annual for
suppliers
maintaining
water
5279
quality
control
parameters.
5280
5281
i)
Any
supplier that
meets the
lead action
level and
which
5282
maintains
the
range of values
for the
water quality
control
5283
parameters
reflecting
optimal
corrosion
control
treatment
5284
specified
by the
Agency
under Section
611.352(f)
during
5285
each of
two consecutive
six-month
monitoring
periods
may
5286
reduce
the frequency
of
monitoring
to once per
year and
the
5287
number of
lead
and
copper
samples
to
that
specified
by
5288
subsection
(c)
of this Section
if
it
receives
written
approval
5289
from the
Agency
in the
form of a
SEP
granted
pursuant
to
5290
Section
611.110.
This reduced
sampling
may
only begin
5291
during
the calendar
year immediately
following
the end
of
5292
the
second
consecutive
six-month
monitoring
period.
5293
5294
ii)
The
Agency
must
review
monitoring,
treatment,
and
other
5295
relevant
information
submitted
by
the
water system
in
5296
accordance
with
Section
611.360, and
must notify
the
5297
system in
writing
by a
SEP granted
pursuant
to Sections
5298
611.110
when
it determines
the system
is eligible
to reduce
5299
its monitoring
frequency
to once
every three
years pursuant
5300
to this
subsection
(d)(4).
5301
5302
iii)
The Agency
must review,
and
where appropriate,
revise
its
5303
determination
under
subsection
(d)(4)(B)(i)
of
this
Section
5304
when the
supplier submits
new
monitoring
or treatment
5305
data, or
when
other data
relevant
to
the number
and
5306
frequency
of tap sampling
becomes
available
to the
5307
Agency.
5308
5309
C)
Reduction
to triennial
for small-
and medium-sized
system
5310
suppliers.
5311
5312
i)
Small-
and medium-sized
system
suppliers
meeting
lead
5313
and copper
action levels.
A small-
or medium-sized
system
5314
supplier
that meets
the
lead action
level
and which
meets
5315
the
lead
and
copper action
levels
during three
consecutive
5316
years of monitoring
may reduce
the frequency
of
5317
monitoring
for
lead
and copper
from
annually
to once
every
5318
three
years.
5319
JCAR35O61
1-0815204r01
5320
ii)
SEP
for
suppliers
meeting
optimal
corrosion
control
5321
treatment.
Any
supplier
that
maintains
the
range
of values
5322
for the
water
quality
control
parameters
reflecting optimal
5323
corrosion
control
treatment
specified
by
the
Agency
under
5324
Section
611.352(f)
during
three consecutive
years
of
5325
monitoring
may reduce
its
monitoring
frequency from
5326
annual
to
once
every
three
years
if
it receives
written
5327
approval
from
the
Agency
in the
form of
a SEP
granted
5328
pursuant
to Section
6 11.110.
Samples
collected
once every
5329
three
years
must
be collected
no
later than
every
third
5330
calendar
year.
5331
5332
iii)
The
Agency
must review,
and
where
appropriate,
revise
its
5333
determination
under
subsection
(d)(4)(C)(ii)
of
this
Section
5334
when
the supplier
submits
new monitoring
or treatment
5335
data,
or when
other
data
relevant
to
the
number
and
5336
frequency
of tap
sampling
becomes
available
to
the
5337
Agency.
5338
5339
D)
Sampling
at a reduced
frequency.
A
supplier
that
reduces
the
5340
number
and
frequency
of sampling
must
collect
these samples
5341
from
representative
sites
included
in
the
pool of
targeted
sampling
5342
sites
identified
in
subsection
(a)
of this
Section,
preferentially
5343
selecting
those
sampling
sites
from the
highest
tier
first.
Suppliers
5344
sampling
annually
or
less
frequently
must
conduct
the
lead
and
5345
copper
tap sampling
during
the
months
of June,
July,
August,
or
5346
September,
unless
the
Agency
has
approved
a
different
sampling
5347
period in
accordance
with
subsection
(d)(4)(D)(i)
of
this
Section.
5348
5349
i)
The Agency
may
grant
a SEP
pursuant
to Section
611.110
5350
that
approves
a
different
period
for conducting
the lead
and
5351
copper
tap sampling
for
systems
collecting
a
reduced
5352
number
of
samples.
Such
a period
must
be no
longer
than
5353
four
consecutive
months
and
must
represent
a
time of
5354
normal
operation
where
the
highest
levels
of
lead
are
most
5355
likely
to
occur.
For
a
NTNCWS
supplier
that
does not
5356
operate
during
the
months
of June
through
September
and
5357
for which
the period
of
normal
operation
where
the highest
5358
levels
of lead
are
most
likely
to
occur
is not known,
the
5359
Agency
must
designate
a period
that
represents
a
time
of
5360
normal
operation
for
the system.
This
reduced
sampling
5361
may
only begin
during
the
period
approved
or designated
5362
by the
Agency
in the
calendar
year
immediately
following
JCAR35O61
1-0815204r01
5363
the end
of
the
second consecutive
six-month
monitoriflg
5364
period
for systems initiating
annual monitoring
and
during
5365
the three-year
period following
the end
of the third
5366
consecutive
calendar
year of annual monitoring
for a
5367
supplier
initiating triennial
monitoring.
5368
5369
ii)
A
supplier monitoring
annually that
has
been collecting
5370
samples during the
months
of June
through September
and
5371
which
receives
Agency approval
to alter its sample
5372
collection period under
subsection
(d)(4)(D)(i)
of
this
5373
Section
must collect
its next round
of samples during
a time
5374
period that ends no
later than
21
months after the previous
5375
round
of sampling.
A supplier monitoring
once every
three
5376
years
that has been
collecting samples
during the months
of
5377
June
through September
and which receives
Agency
5378
approval
to alter
the
sampling collection
period as provided
5379
in
subsection (d)(4)(D)(i)
of this Section
must collect
its
5380
next round
of samples
during a time period
that ends no
5381
later
than 45 months after
the previous
round of sampling.
5382
Subsequent
rounds
of sampling
must be collected annually
5383
or
once every
three
years, as required
by
this
Section.
A
5384
small system supplier
with
a waiver
granted pursuant
to
5385
subsection
(g)
of this Section
that has been collecting
5386
samples
during
the months of June
through September
and
5387
which receives
Agency approval
to alter its
sample
5388
collection
period under subsection
(d)(4)(D)(i)
of this
5389
Section must
collect its next
round
of samples
before the
5390
end of the
nine-year compliance
cycle (as that
term is
5391
defined in
Section 611.101).
5392
5393
E)
Any water
system that
demonstrates
for two consecutive
six-month
5394
monitoring
periods
that the tap water lead
level
computed
under
5395
Section
611.350(c)(3)
is less than or
equal to 0.005 mg!
and
that
5396
the tap
water copper level
computed under
Section 611
.350(c)(3) is
5397
less than
or
equal to 0.65
mg/i may reduce
the number of
samples
5398
in accordance
with
subsection (c) of this
Section and reduce
the
5399
frequency
of sampling
to once every
three calendar years.
5400
5401
F)
Resumption
of standard
monitoring.
5402
5403
i)
Small-
or medium-sized suppliers
exceeding
lead or copper
5404
action level.
A small- or
medium-sized
system supplier
5405
subject
to reduced monitoring
that exceeds
the lead action
JCAR35O61
1-0815204r01
5406
level
or the copper
action level
must resume
sampling
in
5407
accordance
subsection
(d)(3)
of this
Section and
collect the
5408
number
of
samples
specified
for
standard
monitoring
under
5409
subsection
(c)
of this Section.
Such
a supplier
must also
5410
conduct
water
quality
parameter
monitoring
in accordance
5411
with
Section
611.357(b),
(c), or
(d)
(as appropriate)
during
5412
the six-month
monitoring
period
in
which it
exceeded
the
5413
action
level.
Any such
supplier
may resume
annual
5414
monitoring
for lead and
copper
at
the tap at
the reduced
5415
number of
sites specified
in subsection
(c)
of this Section
5416
after it
has
completed
two subsequent
consecutive
six-
5417
month
rounds
of monitoring
that
meet
the
criteria of
5418
subsection
(d)(4)(A) of
this
Section.
Any such
supplier
5419
may
resume monitoring
once every
three years
for lead
and
5420
copper at
the
reduced
number of
sites after it
demonstrates
5421
through
subsequent
rounds
of
monitoring
that
it meets
the
5422
criteria of
either
subsection
(d)(4)(C)
or (d)(4)(E)
of this
5423
Section.
5424
5425
ii)
Suppliers
failing
to operate
within
water
quality
control
5426
parameters.
Any supplier
subject
to
reduced
monitoring
5427
frequency
that fails
to meet the
lead action
level during
any
5428
four-month
monitoring
period
or
that fails
to operate
within
5429
the
range
of values
for the
water
quality control
parameters
5430
specified
pursuant
to Section
611.352(f)
for more than
nine
5431
days
in any
six-month
period
specified
in
Section
5432
611.357(d)
must conduct
tap water
sampling
for lead
and
5433
copper
at
the
frequency
specified
in
subsection
(d)(3)
of
5434
this Section,
must
collect the
number of
samples specified
5435
for
standard
monitoring
under
subsection
(c) of this
5436
Section,
and must
resume monitoring
for
water quality
5437
parameters
within the
distribution
system
in accordance
5438
with
Section
611.357(d).
This
standard
tap water sampling
5439
must begin
no later
than the six-month
period
beginning
5440
January
1
of
the calendar
year
following
the
lead
action
5441
level exceedance
or
water quality
parameter
excursion.
A
5442
supplier
may
resume
reduced
monitoring
for lead and
5443
copper
at
the tap and
for water
quality parameters
within
5444
the distribution
system
only if
it fulfills
the conditions
set
5445
forth
in
subsection
(d)(4)(H)
of this
Section.
5446
5447
BOARD
NOTE:
The Board
moved
the
material
from the
last
5448
sentence
of
40 CFR 141.86(d)(4)(vi)(B)
and
40
CFR
JCAR35O61
l-0815204r01
5449
141.86(d)(4)(vi)(B)(1)
through (d)(4)(vi)(B)(3)
(2007)
to
5450
subsections
(d)(4)(H)
and
(d)(4)(H)(i)
through (d)(4)(H)(iii),
since
5451
Illinois
Administrative
Code codification
requirements
allow
5452
subsections
only to four
indent levels.
5453
5454
G)
Any water supplier
subject to a reduced
monitoring
frequency
5455
under
subsection
(d)(4) of this
Section that either
adds a new
5456
source
of water
or changes any water
treatment
must notify
inform
5457
the Agency in writing
in accordance
with
Section
611.360(a)(3)of
5458
any
upcoming
long-term change
in treatment or
addition
of a
new
5459
source as described
in that Section.
The
Agency
must review
and
5460
approve
the addition
of a new
source or long-term
change in
water
5461
treatment
before it
is
implemented
by the supplier.
The Agency
5462
may,
by
a
SEP
granted pursuant to
Section
611.110,
require the
5463
system
to resume
sampling in
accordance with subsection
(d)(3) of
5464
this Section and
collect the number
of samples
specified
for
5465
standard
monitoring
under subsection
(c) of this Section
or take
5466
other appropriate
steps such as increased
water
quality
parameter
5467
monitoring
or re-evaluation
of
its corrosion control treatment
given
5468
the potentially
different water quality
considerations.
5469
5470
H)
A
supplier required
under
subsection (d)(4)(F) of
this
Section
to
5471
resume
monitoring
in accordance
with Section
611.357(d)
may
5472
resume reduced
monitoring
for lead
and
copper at the tap and
for
5473
water quality
parameters
within the distribution
system under
the
5474
following
conditions:
5475
5476
i)
The supplier may resume
annual
monitoring for lead
and
5477
copper
at the tap
at the reduced number
of sites specified
in
5478
subsection (c) of this
Section
after
it has completed two
5479
subsequent
six-month
rounds of monitoring
that meet
the
5480
criteria
of subsection
(d)(4)(B)
of
this Section and the
5481
supplier
has received written
approval
from the Agency
by
5482
a SEP
pursuant to Section
611.110 that it
is
appropriate
to
5483
resume
reduced monitoring
on an annual
frequency.
This
5484
sampling
must begin
during the calendar
year immediately
5485
following
the end of the
second consecutive
six-month
5486
monitoring
period.
5487
5488
ii)
The supplier may resume
monitoring
for lead and
copper
5489
once
every three
years at the
tap at the reduced number
of
5490
sites after
it demonstrates through
subsequent
rounds of
5491
monitoring that
it
meets the
criteria of either
subsection
JCAR35O61
1-0815204r01
5492
(d)(4)(C)
or (d)(4)(E)
of
this Section
and the system
has
5493
received
a
SEP
under Section
611.110
from the
Agency
5494
that
it is
appropriate
to resume
monitoring
once
every three
5495
years.
5496
5497
iii)
The
supplier
may reduce
the number
of water
quality
5498
parameter
tap
water
samples
required
in
accordance
with
5499
Section
61
1.357(e)(1)
and
the
frequency
with
which
it
5500
collects
such
samples
in accordance
with
Section
5501
611.357(e)(2).
Such a
system
may
not resume
monitoring
5502
once every
three
years
for water
quality parameters
at
the
5503
tap
until
it
demonstrates,
in accordance
with
the
5504
requirements
of
Section
611
.357(e)(2),
that
it has re
5505
qualified
for
monitoring
once every
three years.
5506
5507
BOARD
NOTE:
Subsections
(d)(4)(H)
and (d)(4)(H)(i)
through
5508
(d)(4)(H)(iii)
are
derived
from the
last sentence
of 40
CFR
5509
141.86(d)(4)(vi)(B)
and
40
CFR
141.86
(d)(4)(vi)(B)(1)
through
5510
(d)(4)(vi)(B)(3)
(2007)(2003),
since
Illinois
Administrative
Code
5511
codification
requirements
allow
only four
indent levels
of
5512
subsections.
5513
5514
e)
Additional
monitoring.
The results
of any
monitoring
conducted
in addition
to
5515
the
minimum
requirements
of
this
Section
must be
considered
by the supplier
and
5516
the
Agency
in making
any
determinations
(i.e., calculating
the
90
th
percentile
lead
5517
action
level
or the
copper level)
under this
Subpart
G.
5518
5519
f)
Invalidation
of lead
or copper
tap
water
samples.
A
sample invalidated
under
this
5520
subsection
does not
count
toward
determining
lead
or
copper
90
th
percentile
levels
5521
under
Section
611.3
50(c)(3)
or
toward meeting
the
minimum
monitoring
5522
requirements
of subsection
(c) of
this Section.
5523
5524
1)
The
Agency must
invalidate
a lead
or copper
tap
water sample
if it
5525
determines
that
one of
the
following
conditions
exists:
5526
5527
A)
The laboratory
establishes
that improper
sample analysis
caused
5528
erroneous
results;
5529
5530
B)
The sample
was
taken from
a site
that did
not meet
the
site
5531
selection
criteria
of this Section;
5532
5533
C)
The
sample container
was
damaged
in
transit;
or
5534
JCAR35O61 1-0815204r01
5535
D)
There
is substantial reason to
believe that the sample was subject
5536
to tampering.
5537
5538
2)
The supplier
must report the results
of
all samples
to the Agency and all
5539
supporting documentation
for samples the supplier believes
should be
5540
invalidated.
5541
5542
3)
To invalidate a
sample under subsection (f)(1) of this
Section, the decision
5543
and the rationale
for the decision
must be documented in writing. The
5544
Agency may
not invalidate a sample solely
on the grounds that a follow-
5545
up sample
result is higher or lower
than that of the original sample.
5546
5547
4)
The water
supplier must collect replacement
samples for any samples
5548
invalidated
under this Section
if, after the invalidation of one or more
5549
samples, the
supplier has too few samples to meet the
minimum
5550
requirements
of subsection (c) of this
Section. Any such replacement
5551
samples must
be taken as soon as possible, but no later than 20
days after
5552
the date
the Agency invalidates the sample
or by the end of the applicable
5553
monitoring period,
whichever occurs later. Replacement
samples taken
5554
after
the end of the applicable
monitoring period must not also be used
to
5555
meet the
monitoring requirements of
a subsequent monitoring period.
The
5556
replacement
samples must be taken at the same locations
as the
5557
invalidated samples
or, if that is not possible, at locations other
than those
5558
already
used for sampling
during the monitoring period.
5559
5560
g)
Monitoring waivers for
small system suppliers. Any small system
supplier that
5561
meets the
criteria of this subsection
(g)
may
apply to the Agency to reduce the
5562
frequency of monitoring
for lead and copper under this Section
to once every nine
5563
years (i.e., a
“full waiver”) if it meets all of the
materials criteria specified in
5564
subsection (g)(1) of this Section
and all of the monitoring criteria specified
in
5565
subsection (g)(2)
of this Section. Any small system supplier
that meets the
5566
criteria in
subsections (g)(1) and (g)(2)
of
this
Section only for lead, or only
for
5567
copper, may apply to the State
for a waiver to reduce the frequency
of tap water
5568
monitoring to once
every nine years for that contaminant
only (i.e., a “partial
5569
waiver”).
5570
5571
1)
Materials criteria. The
supplier must demonstrate that its distribution
5572
system
and service lines and all drinking
water supply plumbing,
5573
including plumbing
conveying drinking water
within all residences and
5574
buildings connected
to the system, are free of lead-containing
materials or
5575
copper-containing
materials,
as those terms are defined in this subsection
5576
(g)(1), as
follows:
5577
JCAR35O61
1-0815204r01
5578
A)
Lead. To qualify
for a full waiver,
or a waiver
of
the
tap
water
5579
monitoring
requirements
for lead
(i.e., a “lead waiver”),
the
water
5580
supplier must provide
certification
and supporting
documentation
5581
to the Agency that
the
system is
free of all lead-containing
5582
materials,
as
follows:
5583
5584
i)
It contains
no plastic
pipes that contain lead
plasticizers,
or
5585
plastic
service lines that
contain lead
plasticizers; and
5586
5587
ii)
It
is free of lead service
lines, lead pipes,
lead soldered
pipe
5588
joints,
and
leaded brass
or bronze alloy
fittings and fixtures,
5589
unless
such fittings and
fixtures
meet
the specifications
of
5590
NSF Standard
61, section
9, incorporated
by
reference
in
5591
Section6ll.102.
5592
5593
BOARD
NOTE: Corresponding
40
CFR
5594
141.
86(g)(
1 )(i)(B) specifies
“any standard
established
5595
pursuant
to
42
USC 300g-6(e)
(SDWA section
1417(e)).”
5596
USEPA
has stated that
the NSF standard
is that standard.
5597
See 62
Fed. Reg. 44684
(Aug. 22,
1997).
5598
5599
B)
Copper.
To qualify for a
full waiver, or a waiver
of the tap
water
5600
monitoring
requirements for
copper (i.e.,
a “copper waiver”),
the
5601
water supplier
must provide
certification
and supporting
5602
documentation
to the
Agency that the system
contains
no copper
5603
pipes or
copper service
lines.
5604
5605
2)
Monitoring criteria
for waiver
issuance.
The
supplier must have
completed
5606
at least one
six-month round
of standard tap water
monitoring
for lead and
5607
copper at sites approved
by the
Agency and
from the number of
sites
5608
required
by
subsection (c) of this
Section and demonstrate
that the
90
th
5609
percentile levels
for any and
all
rounds of monitoring
conducted
since the
5610
system became
free of all lead-containing
or copper-containing
materials,
5611
as appropriate, meet
the following
criteria:
5612
5613
A)
Lead levels.
To qualify
for a full waiver, or
a lead waiver,
the
5614
supplier must
demonstrate
that
the
percentile lead level
does
5615
not exceed
0.005
mgLe.
5616
5617
B)
Copper levels.
To qualify
for a full
waiver, or a copper waiver,
the
5618
-
supplier
must
demonstrate
that the
90
th
percentile copper
level
does
5619
not
exceed 0.65 mg/.
5620
JCAR35O61
1-0815204r01
5621
3)
State approval
of waiver application.
The Agency
must notify
the supplier
5622
of its waiver
determination
by a SEP
issued
pursuant
to Section
611.110,
5623
in writing,
setting
forth the
basis of its
decision
and any condition
of
the
5624
waiver.
As a
condition
of
the waiver,
the Agency
may require
the supplier
5625
to perform
specific
activities
(e.g.,
limited monitoring,
periodic
outreach
5626
to
customers
to remind
them to avoid
installation
of materials
that
might
5627
void
the waiver)
to avoid
the risk
of lead or
copper
concentration
of
5628
concern
in tap
water.
The
small
system supplier
must continue
monitoring
5629
for
lead and
copper at
the tap as
required
by
subsections
(d)(1) through
5630
(d)(4)
of this
Section,
as
appropriate,
until
it
receives
written
notification
5631
from
the Agency
that
the waiver
has been approved.
5632
5633
4)
Monitoring
frequency
for
suppliers
with waivers.
5634
5635
A)
A
supplier
with
a
full
waiver
must conduct
tap water
monitoring
5636
for lead
and copper
in accordance
with
subsection
(d)(4)(D)
of this
5637
Section
at the
reduced
number
of sampling
sites identified
in
5638
subsection
(c) of
this Section
at least once
every nine
years and
5639
provide
the
materials
certification
specified
in subsection
(g)(1)
of
5640
this Section
for both
lead and
copper to
the Agency
along with
the
5641
monitoring
results.
Samples
collected
every
nine
years must
be
5642
collected
no
later
than every
ninth
calendar
year.
5643
5644
B)
A
supplier with
a
partial
waiver must
conduct
tap water
monitoring
5645
for the waived
contaminant
in accordance
with
subsection
5646
(d)(4)(D)
of this
Section
at the reduced
number
of sampling
sites
5647
specified
in subsection
(c) of this
Section at
least
once
every
nine
5648
years
and
provide
the materials
certification
specified in
subsection
5649
(g)(1) of this
Section
pertaining
to the
waived
contaminant
along
5650
with
the monitoring
results.
Such
a
supplier
also must continue
to
5651
monitor
for
the
non-waived
contaminant
in
accordance
with
5652
requirements
of subsections
(d)( 1)
through (d)(4)
of this
Section,
5653
as appropriate.
5654
5655
C)
pyIf-a
supplier
with a full
or partial
waiver adds
a new source
of
5656
water
or changes
any
water
treatment,
the
supplier
must
notify
the
5657
Agency
in writing
in accordance
with
Section
61
1.360(a)(3)
of any
5658
upcoming
long-term
change
in treatment
or addition
of
a new
5659
source, as
described
in
that Section.
The
Agency
must
review and
5660
approve
the
addition of
a new source
or
long-term
change
in
water
5661
treatment
before it is
implemented
by
the supplier.
The
Agency
5662
has the
authority to
require the
supplier to
add or modify
waiver
5663
conditions
(e.g.,
require
recertification
that
the supplier’s
system
is
JCAR35O61
1-0815204r01
5664
free of
lead-containing
or copper-containing
materials,
require
5665
additional
rounds
of
monitoring),
if
it deems such
modifications
5666
are necessary
to
address treatment
or
source
water
changes at
the
5667
system.
5668
5669
D)
If a
supplier with
a full or
partial
waiver
becomes
aware that
it is
5670
no
longer
free of
lead-containing
or copper-containing
materials,
5671
as appropriate
(e.g.,
as a result of
new
construction
or
repairs), the
5672
supplier
must
notify the
Agency in
writing
no
later than
60
days
5673
after becoming
aware
of such a
change.
5674
5675
5)
Continued
eligibility.
If the
supplier continues
to
satisfy
the
requirements
5676
of subsection
(g)(4)
of
this Section,
the waiver
will be
renewed
5677
automatically,
unless
any
of the
conditions
listed in
subsection
(g)(5)(A)
5678
through
(g)(5)(C)
of
this Section
occur. A
supplier
whose
waiver
has been
5679
revoked may
re-apply
for a waiver
at such time
as
it again
meets
the
5680
appropriate
materials
and
monitoring
criteria
of
subsections
(g)(1)
and
5681
(g)(2) of this
Section.
5682
5683
A)
A supplier
with a
full waiver
or a lead
waiver no
longer satisfies
5684
the
materials
criteria of
subsection
(g)(1)(A)
of this Section
or
has
5685
a
90
th
percentile
lead
level greater
than 0.005
mg!e.
5686
5687
B)
A
supplier
with
a
full
waiver or
a copper waiver
no longer
satisfies
5688
the materials
criteria
of subsection
(g)(1)(B)
of this
Section or
has
5689
a
90
th
percentile
copper level
greater than
0.65
mg/e.
5690
5691
C)
The State
notifies
the
supplier,
in writing,
that
the waiver
has
been
5692
revoked,
setting forth
the basis
of its decision.
5693
5694
6)
Requirements
following
waiver
revocation.
A supplier
whose
flu or
5695
partial
waiver has
been
revoked
by
the
Agency
is
subject to the
corrosion
5696
control
treatment
and
lead and
copper
tap
water monitoring
requirements,
5697
as follows:
5698
5699
A)
If the supplier
exceeds
the lead
or copper action
level,
the supplier
5700
must implement
corrosion
control
treatment
in
accordance
with
the
5701
deadlines
specified in
Section 611.351(e),
and any other
applicable
5702
requirements
of this
Subpart
G.
5703
5704
B)
If the
supplier
meets
both the
lead
and
the
copper action
level,
the
5705
supplier
must monitor
for lead
and copper
at the tap
no less
5706
frequently
than
once every
three years
using the
reduced number
of
JCAR35O61
1-0815204r01
5707
samplingsample
sites
specified in subsection
(c)
of this
Section.
5708
5709
7)
Pre-existing
waivers. Small
system supplier waivers
approved
by the
5710
Agency in writing
prior to April
11,
2000 must
remain in effect
under the
5711
following
conditions:
5712
5713
A)
If the
supplier has
demonstrated
that it is both free of
lead-
5714
containing and
copper-containing
materials, as required
by
5715
subsection (g)(1)
of
this
Section
and that its
90
th
percentile lead
5716
levels and
90th
percentile copper
levels meet the
criteria
of
5717
subsection (g)(2)
of this
Section,
the waiver remains
in effect
so
5718
long as the
supplier
continues to
meet the waiver
eligibility criteria
5719
of
subsection (g)(5)
of this
Section.
The first round
of tap
water
5720
monitoring conducted
pursuant to subsection
(g)(4)
of this Section
5721
must
be completed
no later than
nine years after the
last time
the
5722
supplier
monitored for
lead and copper
at the tap.
5723
5724
B)
If
the supplier has met
the materials
criteria of subsection
(g)(1)
of
5725
this
Section
but has
not met the
monitoring criteria of
subsection
5726
(g)(2) of this Section,
the supplier must
conduct
a round of
5727
monitoring
for lead
and
copper
at the tap demonstrating
that it
met
5728
the
criteria
of
subsection (g)(2)
of this Section no
later than
5729
September
30, 2000. Thereafter,
the waiver
must remain in
effect
5730
as long as the
supplier
meets
the continued eligibility
criteria
of
5731
subsection
(g)(5) of this
Section. The first round
of tap
water
5732
monitoring
conducted pursuant
to
subsection
(g)(4) of this
Section
5733
must be completed
no
later than nine years after
the
round
of
5734
monitoring
conducted pursuant
to
subsection
(g)(2) of this
Section.
5735
5736
BOARD NOTE:
Derived from 40
CFR
141.86
(2007),
as
amended
at 72 Fed. Reg.
5737
57782 (October 10,
2007)(2003).
5738
5739
(Source: Amended
at 33 Ill. Reg.
effective
5740
5741
Section 611.357
Monitoring
for Water
Quality
Parameters
5742
5743
All large
system suppliers,
and all small- and
medium-sized
system suppliers
that exceed the
5744
lead action
level or the copper
action level,
must monitor
water quality
parameters in addition
to
5745
lead
and copper in accordance
with this
Section. The requirements
of this
Section
are
5746
summarized in Table
G of this Part.
5747
5748
a)
General
Requirements.
5749
JCAR35O61 1-0815204r01
5750
1)
Sample
collection
methods.
5751
5752
A)
Use
of tap samples.
The
totality
of all tap samples collected
by a
5753
supplier must
be representative
of water quality
throughout the
5754
distribution
system
taking into
account the
number
of persons
5755
served,
the different
sources
of water, the different
treatment
5756
methods
employed by the supplier,
and seasonal
variability.
5757
Although a supplier
may conveniently
conduct
tap sampling for
5758
water
quality
parameters at
sites used for coliform
sampling
5759
performed
pursuant to Subpart
L of this
Part, it is not required
to
5760
do so,
and
a supplier is not required
to perform
tap sampling
5761
pursuant to this
Section at
taps targeted for
lead and copper
5762
sampling
under Section 611.356(a).
5763
5764
B)
Use of entry
point samples. Each
supplier
must
collect samples
at
5765
entry
points to
the distribution
system from locations
5766
representative
of each source after
treatment.
If a supplier draws
5767
water
from more
than one source
and the sources
are combined
5768
before distribution,
the supplier
must sample
at an entry point
to
5769
the
distribution
system
during
periods of normal
operating
5770
conditions
(i.e., when water is representative
of all sources
being
5771
used).
5772
5773
2)
Number
of samples.
5774
5775
A)
Tap
samples. Each
supplier must collect
two
tap samples
for
5776
applicable
water quality
parameters
during each six-month
5777
monitoring
period
specified under subsections
(b) through
(e)
of
5778
this Section
from the number
of sites
indicated in the first
column
5779
of Table
E of this Part.
5780
5781
B)
Entrypoint
samples.
5782
5783
i)
Initial monitoring.
Except
as provided
in subsection
(c)(3)
5784
of
this Section,
each supplier must collect
two samples
for
5785
each
applicable water
quality
parameter
at each entry
point
5786
to
the distribution
system during
each six-month
5787
monitoring period
specified in subsection
(b)
of this
5788
Section.
5789
5790
ii)
Subsequent monitoring.
Each
supplier
must
collect one
5791
sample for
each applicable
water quality parameter
at each
5792
entry
point
to the distribution
system during
each six-month
JCAR35O61
1-0815204r01
5793
monitoring
period
specified
in
subsections
(c)
through
(e)
5794
of this
Section.
5795
5796
b)
Initial
Sampling.
5797
5798
1)
Large
systems.
Each
large
system supplier
must
measure
the
applicable
5799
water
quality parameters
specified
in subsection
(b)(3) of this
Section
at
5800
taps
and
at each
entry
point
to
the
distribution
system
during
each
six-
5801
month
monitoring
period
specified
in
Section
61
1.356(d)(1).
5802
5803
2)
Small-
and medium-sized
systems.
Each
small-
and
medium-sized
system
5804
supplier
must
measure
the
applicable
water
quality
parameters
specified
in
5805
subsection
(b)(3)
of this
Section
at
the
locations
specified
in
this
5806
subsection
during
each
six-month
monitoring
period
specified
in
Section
5807
61
1.356(d)(1)
during
which
the
supplier
exceeds
the
lead
action
level
or
5808
the
copper
action
level.
5809
5810
3)
Water
quality
parameters.
5811
5812
A)
pH;
5813
5814
B)
Alkalinity;
5815
5816
C)
Orthophosphate,
when
an
inhibitor
containing
a
phosphate
5817
compound
is
used;
5818
5819
D)
Silica,
when
an
inhibitor
containing
a
silicate
compound
is
used;
5820
5821
E)
Calcium;
5822
5823
F)
Conductivity;
and
5824
5825
G)
Water
temperature.
5826
5827
c)
Monitoring
after
installation
of
corrosion
control.
5828
5829
1)
Large
systems.
Each
large
system
supplier
that
installs
optimal
corrosion
5830
control
treatment
pursuant
to
Section
611.351
(d)(4)
must
measure
the
5831
water
quality
parameters
at
the locations
and
frequencies
specified
in
5832
subsections
(c)(4)
and
(c)(5)
of
this
Section
during
each
six-month
5833
monitoring
period
specified
in Section
611
.356(d)(2)(A).
5834
5835
2)
Small-
and
medium-sized
systems.
Each
small-
or medium-sized
system
JCAR35O61
1-0815204r01
5836
that
installs optimal
corrosion
control
treatment
pursuant to Section
5837
611.35 1(e)(5)
must measure
the water quality parameters
at
the locations
5838
and frequencies
specified in subsections
(c)(4)
and (c)(5) of this
Section
5839
during
each
six-month
monitoring
period
specified in Section
5840
611
.356(d)(2)(B)
in which
the supplier exceeds
the lead
action level or
the
5841
copper action
level.
5842
5843
3)
Any groundwater
system
can limit entry
point sampling
described in
5844
subsection
(c)(2)
of this
Section to
those entry points that
are
5845
representative
of water
quality and treatment
conditions
throughout the
5846
system.
If water
from
untreated
groundwater
sources mixes
with
water
5847
from treated
groundwater
sources, the
system must monitor
for water
5848
quality
parameters
both
at representative
entry points receiving
treatment
5849
and representative
entry points
receiving
no treatment. Prior
to the start
of
5850
any
monitoring
under this
subsection, the system
must provide
to the
5851
Agency written
infonnation
identifying
the selected entry points
and
5852
documentation,
including
information on seasonal
variability,
sufficient
to
5853
demonstrate
that
the sites
are representative
of water quality
and
treatment
5854
conditions
throughout the
system.
5855
5856
4)
Tap water
samples,
two
samples at each
tap for each of
the following
5857
water
quality parameters:
5858
5859
A)
PH;
5860
5861
B)
Alkalinity;
5862
5863
C)
Orthophosphate,
when
an inhibitor containing
a phosphate
5864
compound
is used;
5865
5866
D)
Silica, when
an inhibitor containing
a silicate
compound is used;
5867
and
5868
5869
E)
Calcium, when
calcium carbonate
stabilization
is used
as
part
of
5870
corrosion control.
5871
5872
5)
Entry
point samples,
except
as provided
in subsection
(c)(3) of this
5873
Section,
one
sample
at each entry
point to the distribution
system
every
5874
two
weeks (bi-weekly)
for each of
the
following
water quality
parameters:
5875
5876
A)
pH;
5877
5878
B)
When
alkalinity
is
adjusted as part
of optimal corrosion
control,
a
JCAR35O61
1-0815204r01
5879
reading
of
the dosage rate
of the chemical used
to adjust
alkalinity,
5880
and the alkalinity
concentration;
and
5881
5882
C)
When a corrosion
inhibitor
is
used as part
of optimal corrosion
5883
control, a
reading
of the
dosage rate
of
the inhibitor
used,
and
the
5884
concentration
of orthophosphate
or silica
(whichever
is applicable).
5885
5886
d)
Monitoring
after the
Agency specifies
water quality parameter
values
for optimal
5887
corrosion
control.
5888
5889
1)
Large system
suppliers. After
the
Agency
has specified the values
for
5890
applicable
water
quality
control
parameters reflecting
optimal
corrosion
5891
control treatment
pursuant to
Section
611.352(f),
each large system
5892
supplier
must
measure the applicable
water quality
parameters
in
5893
accordance with
subsection
(c)
of this Section and
determine compliance
5894
with the requirements
of Section
611.352(g) every
six months with
the
5895
first six-month period
to
begin
on either January 1 or
July 1, whichever
5896
comes first,
afterthe date the AgencyState
specifies
the optimal values
5897
under Section 611.352(f).
5898
5899
2)
Small- and medium-sized
system
suppliers.
Each small- or medium-sized
5900
system supplier
must
conduct
such monitoring
during each six-month
5901
monitoring
period specified
in this subsection
(d) in
which
the supplier
5902
exceeds
the lead action level
or the copper
action level.
For any such
5903
small and
medium-size
system that
is subject to a reduced
monitoring
5904
frequency
pursuant to
Section 611 .356(d)(4)
at the
time
of the action
level
5905
exceedence,
the starte+i4
of the
applicable
six-month monitoring
period
5906
under
this subsection
fl
must coincide
with the starte4
of the applicable
5907
monitoring
period under
Section 61 1.356(d)(4).
5908
5909
3)
Compliance
with
Agency-designated
optimal
water quality
parameter
5910
values
must be determined
as
specified
under Section 611.352(g).
5911
5912
e)
Reduced monitoring.
5913
5914
1)
Reduction in
tap monitoring.
A supplier
that has maintained
the
range of
5915
values for
the water quality
parameters reflecting
optimal
corrosion
5916
control treatment
during each
of two consecutive
six-month
monitoring
5917
periods
under
subsection
(d) of this Section
must continue
monitoring
at
5918
the
entry points to the
distribution system
as
specified
in subsection
(c)(4)
5919
of this
Section. Such
a supplier
may
collect two samples
from each tap
for
5920
applicable
water
quality parameters
from the reduced
number of
sites
5921
indicated in the second
coluirm of
Table E of this
Part during each
JCAR35O61
1-0815204r01
5922
subsequent
six-month
monitoring
period.
5923
5924
2)
Reduction
in monitoring
frequency.
5925
5926
A)
Staged
reductions
in monitoring
frequency.
5927
5928
i)
Annual monitoring.
A
supplier
that
maintains
the range
of
5929
values
for
the
water
quality
parameters
reflecting
optimal
5930
corrosion control
treatment
specified
pursuant
to Section
5931
611.352(f)
during three
consecutive
years
of monitoring
5932
may reduce
the frequency
with which
it collects
the number
5933
of tap
samples
for applicable
water
quality
parameters
5934
specified in
subsection
(e)(1)
of
this
Section
from every
six
5935
months to
annually.
This reduced
sampling
may
only
begin
5936
during the
calendar
year
immediately
following
the end
of
5937
the
monitoring
period in
which
the
third consecutive
year
5938
of
six-month
monitoring
occurs.
5939
5940
ii)
Triennial
monitoring.
A supplier
that
maintains
the range
5941
of
values for
the water quality
parameters
reflecting
5942
optimal corrosion
control
treatment
specified
pursuant
to
5943
Section 611.352(f)
during
three
consecutive
years of
annual
5944
monitoring
under
subsection
(e)(2)(A)(i)
of this Section
5945
may reduce
the frequency
with
which it collects
the
number
5946
of tap samples
for
applicable
water quality
parameters
5947
specified
in
subsection
(e)(1)
of this
Section
from
annually
5948
to
once
every three
years. This
reduced
sampling
may
only
5949
begin
no
later
than
the third
calendar
year
following
the
end
5950
of the monitoring
period in which
the third
consecutive
5951
year
of
monitoring
occurs.
5952
5953
B)
A water
supplier
may reduce
the frequency
with which
it
collects
5954
tap
samples for
applicable
water quality
parameters
specified
in
5955
subsection
(e)(1)
of this Section
to every
three years
if it
5956
demonstrates
that
it
has fulfilled
the
conditions
set forth
in
5957
subsections
(e)(2)(B)(i)
through
(e)(2)(B)(iii)
of this
Section-the
5958
following
during
two
consecutive
monitoring
periods,
subject
to
5959
the limitation
of
subsection
(e)(2)(B)(iv)
of
this Section.
5960
5961
i)
The
supplier
must
demonstrate
thatThat
its tap
water
lead
5962
level
at
the
90
th
percentile
is less
than or
equal to
the PQL
5963
for lead
specified
in Section
611.359(a)(1)(B);
5964
JCAR35O61
1-0815204r01
5965
ii)
The supplier
must
demonstrate
thatThft
its tap
water
5966
copper
level
at
the
90
th
percentile
is less
than or
equal
to
5967
0.65
mg/i
for copper
in
Section 61
1.350(c)(2);
and
5968
5969
iii)
The
supplier
must demonstrate
thatfhat
it also
has
5970
maintained
the
range
of
values
for
the water
quality
5971
parameters
reflecting
optimal
corrosion
control
treatment
5972
specified by
the
Agency
under Section
611.352(f);
and
7
5973
5974
jy)
Monitoring
conducted
every
three
years must
be
done
no
5975
later
than
every
third
calendar
year.
5976
5977
3)
A
supplier
that conducts
sampling
annually
or
every
three
years must
5978
collect these
samples
evenly throughout
the calendar
year so
as to reflect
5979
seasonal variability.
5980
5981
4)
Any supplier
subject
to a
reduced
monitoring
frequency
pursuant
to
this
5982
subsection
that fails
to
operate
at or above
the
minimum
value
or within
5983
the range
of
values
for the water
quality
parameters
specified
pursuant
to
5984
Section 611.352(f)
for
more than
nine
days in any
six-month
period
5985
specified
in Section
611.352(g)
must
resume tap
water
sampling
in
5986
accordance
with
the number
and frequency
requirements
of
subsection
(d)
5987
of this
Section.
Such a
system
may
resume annual
monitoring
for water
5988
quality
parameters
at
the
tap
at
the
reduced
number of
sites specified
in
5989
subsection
(e)(1)
of this
Section after
it
has
completed
two
subsequent
5990
consecutive
six-month
rounds of
monitoring
that meet
the criteria
of that
5991
subsection
or
may resume
monitoring
once
every
three
years for
water
5992
quality
parameters
at
the
tap
at the
reduced
number of
sites after
it
5993
demonstrates
through subsequent
rounds
of
monitoring
that
it meets
the
5994
criteria
of either
subsection
(e)(2)(A)
or (e)(2)(B)
of this
Section.
5995
5996
f)
Additional
monitoring
by
suppliers.
The
results of
any
monitoring
conducted
in
5997
addition
to the
minimum
requirements
of this
Section
must be considered
by the
5998
supplier
and
the Agency
in making
any determinations
(i.e.,
determining
5999
concentrations
of water
quality
parameters)
under this
Section or
Section 611.352.
6000
6001
BOARD
NOTE:
Derived
from
40
CFR
141.87
(2007),
as
amended
at 72 Fed. Reg.
57782
6002
(October
10,
2007)(2002).
6003
6004
(Source:
Amended
at
33 fli.
Reg.
effective
6005
6006
Section
611.358
Monitoring
for Lead
and Copper
in Source
Water
6007
JCAR35O61
1-0815204r01
6008
a)
Sample
location,
collection
methods,
and
number
of
samples.
6009
6010
1)
A
supplier
that
fails
to
meet
the
lead
action
level
or
the
copper
action
level
6011
on
the
basis
of
tap
samples
collected
in
accordance
with
Section
6 11.356
6012
must
collect
lead
and
copper
source
water
samples
in accordance
with
the
6013
following
requirements
regarding
sample
location,
number
of
samples,
6014
and
collection
methods:
6015
6016
A)
A
groundwater
supplier
must
take
a minimum
of one
sample
at
6017
every
entry
point
to
the distribution
system
that
is
representative
of
6018
each
well
after
treatment
(hereafter
called
a sampling
point).
The
6019
supplier
must
take
one
sample
at
the same
sampling
point
unless
6020
conditions
make
another
sampling
point
more
representative
of
6021
each
source
or
treatment
plant.
6022
6023
B)
A
surface
water
supplier
must
take
a
minimum
of one
sample
at
6024
every
entry
point
to the
distribution
system
after
any
application
of
6025
treatment
or in
the
distribution
system
at a
point
that
is
6026
representative
of
each
source
after
treatment
(hereafter
called
a
6027
sampling
point). The
system
must
take
each
sample
at
the same
6028
sampling
point
unless
conditions
make
another
sampling
point
6029
more
representative
of each
source
or
treatment
plant.
6030
6031
BOARD
NOTE:
For
the
purposes
of
this
subsection
(a)(1)(B),
6032
surface
water
systems
include
systems
with
a combination
of
6033
surface
and
ground
sources.
6034
6035
C)
If
a
supplier
draws
water
from
more
than
one
source
and
the
6036
sources
are
combined
before
distribution,
the
supplier
must
sample
6037
at an
entry
point
to
the
distribution
system
during
periods
of
6038
normal
operating
conditions
(i.e.,
when
water
is representative
of
6039
all
sources
being
used).
6040
6041
D)
The
Agency
may,
by
a
SEP
issued
pursuant
to
Section
611.110,
6042
reduce
the
total
number
of samples
that
must
be analyzed
by
6043
allowing
the
use
of compositing.
Compositing
of
samples
must
be
6044
done
by
certified
laboratory
personnel.
Composite
samples
from
a
6045
maximum
of
five
samples
are
allowed,
provided
that
if the
lead
6046
concentration
in
the
composite
sample
is
greater
than
or equal
to
6047
0.00
1
mg/R
or
the copper
concentration
is
greater
than
or
equal
to
6048
0.160
mg!e,
then
the
supplier
must
do either
of
the
following:
6049
6050
i)
The
supplier
must
take
and
analyze
a
follow-up
sample
JCAR35O61
1-0815204r01
6051
within
14
days
at
each
sampling
point
included
in
the
6052
composite;
or
6053
6054
ii)
If
duplicates
of
or
sufficient
quantities
from
the
original
6055
samples
from
each
sampling
point
used
in
the
composite
6056
are
available,
the
supplier
may
use
these
instead
of
6057
resampling.
6058
6059
2)
SEP
requiring
an
additional
sample.
6060
6061
A)
When
the
Agency
determines
that
the
results
of
sampling
indicate
6062
an
exceedence
of
the
lead
or
copper
MPC
established
under
6063
Section
61
1.353(b)(4),
it must,
by
a SEP
issued
pursuant
to
Section
6064
611.110,
require
the
supplier
to
collect
one
additional
sample
as
6065
soon
as
possible
after
the
initial
sample
at
the
same
sampling
point,
6066
but
no
later
than
two
weeks
after
the
supplier took
the
initial
6067
sample.
6068
6069
B)
If
a supplier
takes
an Agency-required
confirmation
sample
for
6070
lead
or
copper,
the
supplier
must
average
the
results
obtained
from
6071
the
initial
sample
with
the
results
obtained
from
the
confirmation
6072
sample
in determining
compliance
with
the
Agency-specified
lead
6073
and
copper
MPCs.
6074
6075
i)
Any
analytical
result
below
the
MDL
must
be
considered
6076
as
zero
for
the
purposes
of
averaging.
6077
6078
ii)
Any
value
above
the
MDL
but
below
the
PQL
must
either
6079
be
considered
as
the
measured
value
or
be
considered
one-
6080
half
the
PQL.
6081
6082
b)
Monitoring
frequency
after
system
exceeds
tap
water
action
level.
A supplier
that
6083
exceeds the
lead
action
level
or the
copper
action
level
in
tap
sampling
must
6084
collect
one
source
water
sample
from
each
entry
point
to
the
distribution
system
6085
no
later
thanwithin
six
months
after
the
end
of
the
monitoring
period
during
6086
which
the
lead
or
copper
action
level
was
exceeded.
For
monitoring
periods
that
6087
are
annual or
less
frequent,
the
end
of
the
monitoring
period
is September
30
of
6088
the
calendar
year
in
which
the
sampling
occurs,
or
if
the
Agency
has
established
6089
an
alternate
monitoring
period
by a
SEP
issued
pursuant
to
Section 611.110,
the
6090
last
day
of
that
period.
exceedence.
6091
6092
c)
Monitoring
frequency
after
installation
of
source
water
treatment.
A
supplier
that
6093
installs
source
water
treatment
pursuant
to
Section
611.353(a)(3)
must
collect
an
JCAR35O61
1-0815204r01
6094
additional source
water sample
from each entry
point
to the
distribution
system
6095
during each of
two
consecutive
six-month
monitoring periods
on or before 36
6096
months
after
completion
of
step
2, as specified
in Section 61
1.353(a)(4).
6097
6098
d)
Monitoring
frequency
after
the Agency
has specified the lead
and copper
MPCs
6099
or has
determined that
source water treatment
is not needed.
6100
6101
1)
A supplier
must
monitor at the
frequency specified
by subsection
6102
(d)(1)(A) or (d)(1)(B)
of this
Section
where
the Agency has
specified the
6103
MPCs
pursuant
to Section
61 1.353(b)(4) or has
determined
that
the
6104
supplier is not
required to install
source
water
treatment pursuant
to
6105
Section
611.353(b)(2).
6106
6107
A)
GWS
suppliers.
6108
6109
i)
A
GWS supplier required
to sample
by subsection
(d)(1) of
6110
this
Section
must
collect samples once
during the
three-
6111
year
compliance period
(as that
term is defined in
Section
6112
611.101)
during
which the Agency
makes its determination
6113
pursuant to Section
611 .353(b)(4)
or 611
.353(b)(2).
6114
6115
ii)
A
GWS supplier
required to
sample by subsection
(d)(1)
of
6116
this Section must
collect samples
once
during
each
6117
subsequent
compliance
period.
6118
6119
ffi)
Triennial
samples must
be collected every
third calendar
6120
year.
6121
6122
B)
A
SWS
or
mixed
system supplier
must collect samples
once
during
6123
each
calendar yearannually,
the
first annual monitoring
period
to
6124
begin
during
the
year mon the date
on which
the
Agency makes
its
6125
determination
pursuant
to Section
61 1.353(b)(4) or 61
1.353(b)(2).
6126
6127
2)
A supplier is
not required
to conduct source
water sampling
for lead
or
6128
copper if
the supplier meets
the action level
for the specific
contaminant
in
6129
all tap water
samples
collected
during the
entire source water
sampling
6130
period
applicable
under
subsection (d)(1)(A)
or (d)(1)(B)
of this Section.
6131
6132
e)
Reduced monitoring
frequency.
6133
6134
1)
A
GWS
supplier
may
reduce the
monitoring
frequency for
lead and copper
6135
in source
water
to
once during each nine-year
compliance
cycle
(as
that
6136
term is defined
in Section
611.101),
provided that
the samples are
JCAR35O61 1-0815204r01
6137
collected no
later than
every
ninth calendar
year, and only if
the supplier
6138
meets one
of the following criteria:
6139
6140
A)
The
supplier
demonstrates that finished
drinking
water entering
the
6141
distribution system
has
been maintained
below
the maximum
6142
pennissible lead
and copper
concentrations specified
by the State
6143
in
Section
61 1.353(b)(4) during
at least three
consecutive
6144
compliance periods
under
subsection (d)(1)
of this Section; or
6145
6146
B)
The
Agency has determined,
by
a SEP issued
pursuant to Section
6147
611.110,
that source water
treatment is not needed
and the
system
6148
demonstrates
that,
during at
least three consecutive
compliance
6149
periods in
which sampling was
conducted under
subsection
(d)(1)
6150
of this Section,
the concentration
of lead in source
water
was
less
6151
than or
equal
to 0.005 mg!€ and
the concentration
of copper in
6152
source water
was less than
or equal to 0.65 mg!e.
6153
6154
2)
A
SWS or mixed system
supplier
may reduce the monitoring
frequency
in
6155
subsection
(d)(1)
of this Section to once
during
each
nine-year
6156
compliance cycle (as
that term
is defined
in Section 611.101),
provided
6157
that
the samples
are collected no later
than every ninth
calendar year,
and
6158
çpy
if the
supplier
meets one of the
following
criteria:
6159
6160
A)
The
supplier demonstrates
that finished
drinking water
entering the
6161
distribution
system has
been
maintained
below the maximum
6162
permissible
lead and
copper concentrations
specified
by the
6163
Agency
under Section
61
1.353(b)(4)
for at least three consecutive
6164
years;
or
6165
6166
B)
The Agency
has
determined,
by a SEP issued
pursuant
to Section
6167
611.110,
that source water
treatment
is not needed and the
supplier
6168
demonstrates
that, during
at least three consecutive
years, the
6169
concentration
of lead in
source water was less
than or equal
to
6170
0.005
mg/C and the concentration
of copper
in source water was
6171
less than
or equal
to 0.65
mg/C.
6172
6173
3)
A supplier that uses
a new source
of water is not eligible
for reduced
6174
monitoring for
lead or copper until
it demonstrates
by samples collected
6175
from the
new source during three
consecutive
monitoring periods,
of
the
6176
appropriate duration
provided
by subsection
(d)( 1) of this Section,
that
6177
lead or copper
concentrations
are
below the
MPC as specified
by the
6178
Agency
pursuant to Section
611
.353(a)(4).
6179
JCAR35O61 1-0815204r01
6180
BOARD NOTE: Derived from 40
CFR 141.88 (2007),
as amended at 72 Fed.
Reg.
6181
57782
(October
10,
2007)(2003).
6182
6183
(Source: Amended at 33 Iii. Reg.
effective
6184
6185
Section 611.359 Analytical
Methods
6186
6187
Analyses
for lead, copper, pH, conductivity, calcium,
alkalinity, orthophosphate,
silica, and
6188
temperature must be conducted
using the methods set forth
in Section 611.611(a).
6189
6190
a)
Analyses for
lead and copper performed for
the purposes of compliance
with this
6191
Subpart
G
must only be conducted
by laboratories that have
been certified by
6192
USEPA or the Agency.
To obtain certification
to conduct analyses for lead
and
6193
copper, laboratories
must do the following:
6194
6195
1)
Analyze
performance evaluation samples
that include lead and copper
6196
provided by USEPA Environmental
Monitoring and
Support Laboratory
6197
or equivalent
samples provided
by the Agency; and
6198
6199
2)
Achieve quantitative acceptance
limits as follows:
6200
6201
A)
For lead:
±30
percent of the actual amount
in the performance
6202
evaluation sample
when the actual amount is greater
than or equal
6203
to 0.005 mg! (the PQL
for lead is 0.005 mg/i);
6204
6205
B)
For copper:
±10
percent of the actual amount
in the performance
6206
evaluation sample when
the actual amount is greater than
or equal
6207
to 0.050 mg/e
(the PQL for copper is 0.050 mg!E);
6208
6209
C)
Achieve the method
detection limit (MDL) for lead
(0.00 1 mg/i,
6210
as defined
in Section 611.350(a)) according
to the procedures
in 35
6211
Ill. Adm. Code 186 and
appendix B to 40 CFR 136: “Definition
6212
and Procedure
for the Determination of the Method
Detection
6213
Limit
— Revision 1.11(2005)”,
incorporated by reference in
6214
Section 611.102(c).
This need only be accomplished
if the
6215
laboratory
will be processing
source water composite samples
6216
under Section
611.358(a)(1)(D)611.358(a)(1)(C);
and
6217
6218
D)
Be
currently certified
by USEPA or the Agency to perform
6219
analyses to
the specifications described in
subsection (a)(1)(a)(2)
6220
of this Section.
6221
6222
BOARD NOTE: Subsection
(a) is derived from 40
CFR 141.89(a) and (a)(1)
JCAR35O61
1-0815204r01
6223
(2007).
as amended
at 72
Fed.
Reg. 57782
(October
10, 2007)(2005).
6224
6225
b)
The
Agency
must,
by a SEP
issued
pursuant
to
Section
611.110,
allow a
supplier
6226
to
use
previously
collected
monitoring
data for the
purposes
of monitoring
under
6227
this
Subpart
G
if the data
were collected
and analyzed
in
accordance
with
the
6228
requirements
of this Subpart
G.
6229
6230
BOARD
NOTE:
Subsection
(b)
is
derived from
40 CFR
141.89(a)(2)
6231
(2007)(2005).
6232
6233
c)
Reporting
lead
and copper
levels.
6234
6235
1)
All lead
and
copper
levels greater
than
or equal
to
the lead and
copper
6236
PQL
(Pb 0.005
mg!
and
Cu
0.050
mg/C) must
be
reported
as
6237
measured.
6238
6239
2)
All lead
and copper
levels measured
less
than the PQL
and
greater
than
6240
the MDL
(0.005
mg/C> Pb>
MDL
and
0.050
mg/C >
Cu > MDL)
must
be
6241
either reported
as
measured
or as one-half
the PQL
set
forth in
subsection
6242
(a)
of
this Section
(i.e.,
reported
as
0.0025
mg/C
for
lead
or 0.025
mg/C
for
6243
copper).
6244
6245
3)
All
lead and copper
levels
below the
lead and
copper
MDL
(MDL >
Pb)
6246
must be reported
as zero.
6247
6248
BOARD
NOTE: Subsection
(c) is
derived from
40
CFR
141.89(a)(3)
and (a)(4)
(2007)(2005).
6249
6250
(Source:
Amended
at 33 Ill.
Reg.
effective
6251
6252
Section
611.360
Reporting
6253
6254
A supplier
must
report
all of the following
infonnation
to
the Agency
in
accordance
with
this
6255
Section.
6256
6257
a)
Reporting
for tap, lead,
and copper,
and water
quality
parameter
monitoring.
6258
6259
1)
Except
as provided
in subsection
(a)(1)(viii)
of
this Section,
a supplier
6260
must
report
the
following
information
for all
samples
specified
in
Section
6261
611.356
and for
all
water
quality parameter
samples
specified
in Section
6262
611.357 within
ten days
of the end
of each applicable
sampling
period
6263
specified
in Sections
611.356 and
611.357
(i.e.,
every six
months,
6264
annually, every
three
years,
or every
nine
years).
For a
monitoring
period
6265
with a duration
less
than
six months,
the end
of the monitoring
period
is
JCAR35O61
1-0815204r01
6266
the
last
date on
which samples
can be
collected
during
that
period, as
6267
specified
in Sections
611.356
and 611.357.
6268
6269
A)
The results
of all
tap
samples
for lead
and copper,
including
the
6270
location
of each
site
and
the
criteria
under Section
611.356(a)(3)
6271
through
(a)(7) under
which
the site was
selected for
the
supplier’s
6272
sampling
pool;
6273
6274
B)
Documentation
for each tap
water lead
or
copper
sample for
which
6275
the
water supplier
requests
invalidation
pursuant
to Section
6276
61 1.356(f)(2);
6277
6278
C)
This
subsection
(a)(1)(C)
corresponds
with
40
CFR
6279
141.90(a)(1)(iii),
a provision
that
USEPA
removed
and marked
6280
“reserved.”
This
statement
preserves
structural
parity with
the
6281
federal
rules;
6282
6283
D)
The
90
th
percentile
lead and
copper concentrations
measured
from
6284
among
all lead
and copper
tap samples
collected
during each
6285
sampling
period
(calculated
in accordance
with Section
6286
611
.350(c)(3)),
unless the
Agency calculates
the
system’s
90
th
6287
percentile
lead
and copper
levels under
subsection
(h) of
this
6288
Section;
6289
6290
E)
With the exception
of
initial tap
sampling conducted
pursuant
to
6291
Section
611 .356(d)(1),
the supplier
must
designate
any site that
6292
was not sampled
during
previous
sampling
periods, and
include
an
6293
explanation
of why
sampling
sites have
changed;
6294
6295
F)
The
results
of all
tap samples
for pH, and
where
applicable,
6296
alkalinity,
calcium, conductivity,
temperature,
and orthophosphate
6297
or
silica collected
pursuant
to Section
611.357(b)
through
(e);
6298
6299
G)
The
results
of
all samples
collected
at entry points
for applicable
6300
water
quality
parameters
pursuant
to Section
611.357(b)
through
6301
(e).
6302
6303
H)
A
water
supplier
must report
the results
of
all
water quality
6304
parameter
samples collected
under
Section
6 11.357(c)
through
(f)
6305
during each
six-month
monitoring
period
specified
in
Section
6306
611.357(d)
within
the
first
10 days following
the end
of the
6307
monitoring
period,
unless the
Agency has
specified,
by a SEP
6308
granted
pursuant
to Section
611.110, a
more frequent
reporting
JCAR35O61
1-0815204r01
6309
requirement.
6310
6311
2)
For a NTNCWS
supplier, or a
CWS
supplier
meeting the criteria
of
6312
Sections
61
1.355(be)(7)(A)
and (be)(7)(B), that
does not have
enough
taps
6313
which can
provide first-draw
samples,
the
supplier must
do either of the
6314
following:
6315
6316
A)
Provide written documentation
to the Agency that
identifies
6317
standing
times
and locations for enough
non-first-draw
samples
to
6318
make up its sampling
pool under
Section 611.356(b)(5)
by the start
6319
of the
first applicable
monitoring
period under Section
611.356(d)
6320
that
commenced after
April
11,
2000, unless the
Agency has
6321
waived
prior
Agency approval of non-first-draw
samplingsample
6322
sites
selected by the
supplier pursuant
to Section 61 1.356(b)(5);
or
6323
6324
B)
If the
Agency
has
waived prior approval
of non-first-draw
6325
samplingsample sites
selected
by the
supplier, identify,
in writing,
6326
each
site
that did not
meet the six-hour
minimum standing
time
6327
and the length of standing
time for
that particular
substitute sample
6328
collected
pursuant
to Section
611
.356(b)(5) and include
this
6329
information
with
the lead and copper
tap sample
results required
to
6330
be submitted pursuant
to subsection
(a)(1)(A)
of this Section.
6331
6332
3)
At a
time
specified
by the Agency,
by a SEP issued
pursuant
to Section
6333
611.110, or if no specific
time is designated
by
the Agency, then as early
6334
as
possible prior
toNo later than
60 days after the addition
of a new
source
6335
or any change in
water treatment,
unless the
Agency
requires earlier
6336
notification,
a water
supplier deemed
to have optimized
corrosion
control
6337
under Section 61 1.35
1(b)(3), a water
supplier
subject
to reduced
6338
monitoring
pursuant
to Section 61 1.356(d)(4),
or a water
supplier
subject
6339
to a monitoring waiver
pursuant
to
Section 611.356(g),
must submit&en4
6340
written
documentation
to the Agency describing
the
change or addition.
6341
In those
instances
where
prior Agency
approval of the treatment
change
or
6342
new
source is not required,
USEPA has
stated that
it
encourages water
6343
systems
to
provide the
notification to
the Agency beforehand
to minimize
6344
the
risk the treatment change
or new source
will
adversely
affect optimal
6345
corrosion
control.
6346
6347
4)
Any small system
supplier applying
for a monitoring
waiver under Section
6348
611.356(g),
or subject
to a waiver
granted pursuant
to
Section
6349
61 1.356(g)(3),
must provide the following
information
to the Agency
in
6350
writing by the specified
deadline:
6351
JCAR35O61
1-0815204r01
6352
A)
By
the
start
of
the
first
applicable
monitoring
period
in
Section
6353
611.356(d),
any
small
water
system
supplier
applying
for
a
6354
monitoring
waiver
must
provide
the
documentation
required
to
6355
demonstrate
that
it meets
the
waiver
criteria
of
Sections
6356
611.356(g)(1)
and
(g)(2).
6357
6358
B)
No
later
than
nine
years
after
the monitoring
previously
conducted
6359
pursuant
to
Section
611.356(g)(2)
or
Section
611.356(g)(4)(A),
6360
each
small
system
supplier
desiring to
maintain
its monitoring
6361
waiver
must
provide
the
information
required
by
Sections
6362
611
.356(g)(4)(A)
and
(g)(4)(B).
6363
6364
C)
No
later
than
60
days
after
it becomes
aware
that
it
is
no
longer
6365
free
of lead-containing
or
copper-containing
material,
as
6366
appropriate,
each
small
system
supplier
with
a
monitoring
waiver
6367
must
provide
written
notification
to
the
Agency,
setting
forth
the
6368
circumstances
resulting
in
the
lead-containing
or
copper-containing
6369
materials
being
introduced
into
the
system
and
what
corrective
6370
action,
if
any,
the
supplier
plans
to
remove
these
materials.
6371
6372
D)
By
October
10,
2000,
any
small
system
supplier
with
a
waiver
6373
granted
prior
to
April
11,
2000
and
that
had
not
previously
met
the
6374
requirements
of
Section
611
.356(g)(2)
must
have
provided
the
6375
information
required
by
that
subsection.
6376
6377
5)
Each
GWS
supplier
that
limits
water
quality
parameter
monitoring
to
a
6378
subset
of
entry
points
under
Section
611
.357(c)(3)
must
provide,
by the
6379
commencement
of
such
monitoring,
written
correspondence
to the
Agency
6380
that
identifies
the
selected
entry
points
and
includes
information
sufficient
6381
to
demonstrate
that
the
sites
are
representative
of
water
quality
and
6382
treatment
conditions
throughout
the
system.
6383
6384
b)
Reporting for
source
water
monitoring.
6385
6386
1)
A
supplier must
report
the
sampling
results
for
all
source
water
samples
6387
collected
in
accordance
with
Section
611.358
within
ten
days
of
the
end
of
6388
each
source
water
sampling
period
(i.e.,
annually,
per
compliance
period,
6389
per
compliance
cycle)
specified
in
Section
611.358.
6390
6391
2)
With
the
exception
of
the
first
round
of
source
water
sampling
conducted
6392
pursuant
to Section
611.358(b),
a
supplier
must
specify
any
site
that
was
6393
not sampled
during
previous
sampling
periods,
and
include
an
explanation
6394
of
why
the sampling
point
has
changed.
JCAR35O61
1-0815204r01
6395
6396
c)
Reporting
for corrosion
control
treatment.
6397
6398
By
the
applicable
dates
under Section
611.351, a
supplier must
report the
6399
following
information:
6400
6401
1)
For a supplier
demonstrating
that
it
has already
optimized
corrosion
6402
control,
the information
required
by Section
611
.352(b)(2)
or (b)(3).
6403
6404
2)
For
a supplier
required
to
optimize corrosion
control,
its recommendation
6405
regarding
optimal
corrosion
control
treatment
pursuant
to
Section
6406
611.352(a).
6407
6408
3)
For
a supplier required
to
evaluate the
effectiveness
of corrosion
control
6409
treatments
pursuant
to Section
611.352(c),
the information
required
by
6410
Section
611.352(c).
6411
6412
4)
For
a supplier required
to
install
optimal
corrosion
control
approved
by
the
6413
Agency
pursuant
to
Section
611.352(d),
a copy of
the Agency
permit
6414
letter,
which acts
as certification
that
the supplier
has
completed
installing
6415
the
permitted
treatment.
6416
6417
d)
Reporting
for source
water treatment.
On
or before the
applicable
dates in
6418
Section
611.353, a
supplier must
provide
the following
information
to the
6419
Agency:
6420
6421
1)
If required
by Section
611 .353(b)(1),
its
recommendation
regarding
source
6422
water treatment;
or
6423
6424
2)
For suppliers
required
to
install source
water
treatment
pursuant to
Section
6425
61 1.353(b)(2),
a copy
of
the Agency
permit
letter,
which
acts as
6426
certification
that the
supplier
has
completed
installing
the
treatment
6427
approved
by
the
Agency
within 24
months after
the Agency
approved
the
6428
treatment.
6429
6430
e)
Reporting
for lead
service line
replacement.
A supplier
must report
the following
6431
information
to the Agency
to
demonstrate
compliance
with the requirements
of
6432
Section
611.354:
6433
6434
1)
No later than
12
months
after the
end of a monitoring
period
in
6435
whichWithin
12 months
after a
supplier exceeds
the
lead action
level in
6436
sampling
referred
to in Section
611.354(a),
the
supplier
must submitreport
6437
each of the
following
to
the Agency
in
writing:
JCAR35O61
1-0815204r01
6438
6439
A)
The
materialA
demonstration
that it
has
conducted
a materials
6440
evaluation,
including
the
evaluation
conducted
as required
by
6441
Section
611.356(a);
6442
6443
B)
Theldentify
the initial
number
of lead
service
lines in
its
6444
distribution
system
at the time
the supplier
exceeds
the lead
action
6445
level; and
6446
6447
C)
TheProvide
the
Agency
with
the supplier’s
schedule
for annually
6448
replacing
at least seven
percent
of the
initial
number
of
lead
6449
service lines
in its
distribution
system.
6450
6451
2)
Action
by the supplier.
6452
6453
A
No
later thanWithin
12 months
after the end
of a monitoring
period
6454
in
which
a supplier
exceeds
the
lead action
level
in
sampling
6455
referred
to
in Section
611.354(a),
and every
12 months
thereafter,
6456
the
supplier
must
demonstrate
to the Agency
in
writing
that the
6457
supplier has
done either
of the following:
6458
6459
iA)
Replaced
in the
previous
12 months
at least
seven percent
6460
of
the initial
number
of lead service
lines
in its distribution
6461
system (or
any greater
number
of
lines specified
by the
6462
Agency
pursuant
to
Section
6
11.354(e));
or
6463
6464
iiR)
Conducted
sampling
that demonstrates
that
the lead
6465
concentration
in all
service
line
samples
from individual
6466
lines,
taken
pursuant
to Section
61
1.356(b)(3),
is
less than
6467
or equal
to
0.015 mg!E.
6468
6469
WhenWhere
the
supplier makes
a demonstration
under
subsection
6470
(e)(2)(AB)jj
of
this
Section,
the total
number
of lines that
the
6471
supplier
has
replaced,
combined
with the
total number
that
meet
6472
the criteria
of Section
61 1.354(c)611.354(b),
must
equal at
least
6473
seven
percent of
the
initial number
of lead
lines identified
pursuant
6474
to subsection
(e)(1)Ea
of this
Section
(or the percentage
specified
6475
by the
Agency pursuant
to Section
611.354(e)).
6476
6477
3)
The
annual letter
submitted
to the
Agency
pursuant
to
subsection
(e)(2)
of
6478
this
Section
must contain
the following
information:
6479
6480
A)
The
number
of
lead service
lines
originally
scheduled
to be
JCAR35O61
1-0815204r01
6481
replaced
during
the previous
year
of the
supplier’s
replacement
6482
schedule;
6483
6484
B)
The
number
and location
of each
lead service
line actually
replaced
6485
during
the
previous
year of the
supplier’s
replacement
schedule;
6486
and
6487
6488
C)
If
measured,
the
water lead
concentration
from each
lead service
6489
line sampled
pursuant
to Section
611.356(b)(3)
and
the location
of
6490
each
lead
service
line sampled,
the sampling
method
used, and
the
6491
date of sampling.
6492
6493
4)
Any
supplier that
collects
lead service
line
samples
following
partial
lead
6494
service
line replacement
required
by
Section
611.354
must
report the
6495
results
to the Agency
within
the first
ten days of
the month
following
the
6496
month
in which the
supplier
receives the
laboratory
results,
or as specified
6497
by the Agency.
The
Agency
may, by
a SEP granted
pursuant
to Section
6498
611.110,
eliminate
this requirement
to report
these
monitoring
results.
A
6499
supplier
must also
report any
additional
information
as specified
by
the
6500
Agency,
and in
a time
and manner
prescribed
by
the
Agency,
to verify
that
6501
all partial
lead service
line
replacement
activities
have taken
place.
6502
6503
f)
Reporting
for
public
education
program.
6504
6505
1)
Any
water
supplier that
is subject
to the
public
education
requirements
in
6506
Section
611.355
must,
within
ten
days after
the end of
each period
in
6507
which
the supplier
is
required
to
perform
public
education
tasks
in
6508
accordance
with Section
61
1.355(b)61
1.355(c),
send
written
6509
documentation
to
the
Agency
that
contains
the
following:
6510
6511
A)
A demonstration
that the
supplier has
delivered
the public
6512
education
materials
that
meet the content
requirements
in
6513
SectionSections
611.355(a)
and
(b)
and
the delivery
requirements
6514
in Section
611.355(b)611.355(c);
and
6515
6516
B)
A list
of all
the
newspapers,
radio
stations,
television
stations,
and
6517
facilities
and organizations
to which
the supplier
delivered
public
6518
education
materials
during
the period
in
which
the supplier
was
6519
required
to perform
public
education
tasks.
6520
6521
2)
Unless
required
by
the
Agency,
by a SEP
issued pursuant
to Section
6522
611.110,
a supplier
that
previously
has
submitted
the
information
required
6523
by subsection
(f)(1)(B)
of this
Section need
not
resubmit
the information
JCAR35O61
1-0815204r01
6524
required
by
subsection
(f)(1)(B)
of this
Section,
as long as
there have
been
6525
no changes
in the
distribution
list and the
supplier
certifies
that the public
6526
education
materials
were
distributed
to the same
list submitted
previously.
6527
6528
.j
No later
than three
months
following
the
end
of the
monitoring
period,
6529
each supplier
must mail
a sample copy
of
the
consumer notification
of
tap
6530
results
to the Agency,
along
with
a certification
that the
notification
has
6531
been
distributed
in
a
manner
consistent
with
the
requirements
of
Section
6532
611.355(d).
6533
6534
g)
Reporting
of
additional
monitoring
data.
Any supplier
that collects
sampling
data
6535
in
addition
to that required
by
this
Subpart
G must
report
the results
of
that
6536
sampling
to
the Agency
within
the
first
ten
days following
the
end of the
6537
applicable
sampling
periods specified
by Sections
611.356
through
611.358
6538
during
which
the samples
are collected.
6539
6540
h)
Reporting
of
90th percentile
lead
and copper
concentrations
where
the Agency
6541
calculates
a system’s
90th
percentile
concentrations.
A
water supplier
is
not
6542
required
to report
the 90th
percentile
lead
and copper
concentrations
measured
6543
from
among
all lead
and copper
tap water
samples collected
during
each
6544
monitoring
period,
as required
by subsection
(a)(1)(D)
of this
Section if
the
6545
following
is true:
6546
6547
1)
The
Agency
has previously
notified
the water
supplier
that it
will calculate
6548
the water
system’s
90
th
percentile
lead and
copper
concentrations,
based
on
6549
the lead and
copper
tap results
submitted
pursuant
to subsection
(h)(2)(A)
6550
of this Section,
and
has specified
a date
before
the
end of the
applicable
6551
monitoring
period
by
which the
supplier
must
provide
the results
of
lead
6552
and copper
tap
water
samples;
6553
6554
2)
The supplier
has provided
the following
information
to the Agency
by the
6555
date
specified
in subsection
(h)(1)
of this
Section:
6556
6557
A)
The results
of
all
tap
samples
for lead
and copper
including
the
6558
location
of each
site and the
criteria
under
Section 61 1.356(a)(3),
6559
(a)(4),
(a)(5),
(a)(6), or
(a)(7) under
which the
site was selected
for
6560
the
system’s sampling
pooi,
pursuant
to
subsection
(a)(1)(A)
of this
6561
Section;
and
6562
6563
B)
An
identification
of sampling
sites utilized
during the
current
6564
monitoring
period that
were not
sampled during
previous
6565
monitoring
periods,
and an explanation
why
sampling
sites
have
6566
changed;
and
JCAR35O61
1-0815204r01
6567
6568
3)
The Agency
has provided
the results
of
the
90
th
percentile
lead
and
copper
6569
calculations,
in
writing,
to the
water
supplier before
the end of the
6570
monitoring
period.
6571
6572
BOARD
NOTE: Derived
from 40
CFR
141.90 (2007),
as amended
at 72 Fed. Reg. 57782
6573
(October
10,
2007)(2003).
6574
6575
(Source: Amended
at 33 Ill.
Reg.
effective
6576
6577
SUBPART
I:
DISINFECTANT
RESIDUALS,
DISINFECTION
6578
BYPRODUCTS,
AND
DISINFECTION
BYPRODUCT
PRECURSORS
6579
6580
Section 611.381
Analytical
Requirements
6581
6582
a)
A supplier
must use
only
the analytical
methods specified in
this Section
or
6583
alternative
methodstheir equivalents
as approved
by the
Agency pursuant
to
6584
Section 611.480
to
demonstrate
compliance
with the requirements
of this
Subpart
I
6585
and with
the requirements
of Subparts
W
and
Y of this
Part.
6586
6587
b)
Disinfection
byproducts
(DBPs).
6588
6589
1)
A supplier must
measure
disinfection byproducts
(DBPs)
by the appropriate
6590
of the
following
methods:
6591
6592
A)
TTHM:
6593
6594
i)
By
purge
and trap, gas chromatography,
electrolytic
6595
conductivity
detector, and
photoionization
detector:
6596
USEPA
Organic Methods,
Method 502.2.
If TTHMs
are
6597
the only analytes
being
measured in the
sample, then a
6598
photoionization
detector is not
required.
6599
6600
ii)
By purge and trap,
gas chromatography,
mass
6601
spectrometer:
USEPA Organic
Methods, Method
524.2.
6602
6603
iii)
By
liquid-liquid
extraction,
gas chromatography,
electron
6604
capture detector:
USEPA Organic
Methods,
Method
551.1.
6605
6606
B)
HAA5:
6607
JCAR35O61
1-0815204r01
6608
i)
By
liquid-liquid
extraction
(diazomethane),
gas
6609
chromatography,
electron
capture
detector:
Standard
6610
Methods,
19
th
or
21st
ed.,
Method
6251
B.
6611
6612
BOARD
NOTE:
On January
4,
2006
(at
71 Fed.
Reg.
6613
388),
USEPA
amended
the entry
for HAA5
by
liquid-liquid
6614
extraction
(diazomethane),
gas
chromatography,
electron
6615
capture
detector,
in the
table
at
corresponding
40 CFR
6616
14l.131(b)(l)
to allow
the use
of Standard
Methods
Online
6617
(at
www.standardmethods.org),
Method
6251
B (as
6618
approved
in 1994).
The
Board
has instead
cited
to the
21st
6619
edition
of
Standard
Methods
for
the Examination
of
Water
6620
and
Wastewater
(the
printed
version
of
Standard
Methods),
6621
since
the
version
of Method
6251
that
appears
in
that
6622
printed
volume
is
that cited
by
USEPA
as acceptable
for
6623
use.
USEPA
later
added
Method
6251
B from
the
21st
6624
edition
of Standard
Methods
as
an approved
alternative
6625
method
in
appendix
A
to subpart
C, added
on
June
3, 2008
6626
(at
73 Fed.
Reg.
31616).
6627
6628
ii)
By solid
phase
extractor
(acidic
methanol),
gas
6629
chromatography,
electron
capture
detector:
USEPA
6630
Organic
Methods,
Method
552.1.
6631
6632
iii)
By
liquid-liquid
extraction
(acidic
methanol),
gas
6633
chromatography,
electron
capture
detector:
USEPA
6634
Organic
Methods,
Method
552.2
or 552.3.
6635
6636
C)
Bromate:
6637
6638
i)
By ion
chromatography:
USEPA
Organic
and
Inorganic
6639
Methods,
Method
300.1.
6640
6641
ii)
By ion
chromatography
and
post-column
reaction:
USEPA
6642
OGWDW
Methods,
Method
317.0,
rev 2.0,
or 326.0,
rev.
6643
1.0.
6644
6645
iii)
By inductively-coupled
plasma—?mass spectrometer:
6646
USEPA
Organic
and
Inorganic
Methods,
Method
321.8.
6647
6648
BOARD
NOTE:
Ion
chromatography
and
post
column
reaction
or
6649
inductively-coupled
plasma—mass
spectrometry
must
be
used
for
6650
monitoring
of bromate
for
purposes
of
demonstrating
eligibility
of
JCAR35O61 1-0815204r01
6651
reduced
monitoring,
as prescribed
in Section
611
.382(b)(3)(B).
6652
For inductively-coupled
plasma—mass
spectrometry,
samples
6653
must be preserved
at the time
of sampling with
50 mg
6654
ethylenediamine
(EDA) per liter
of sample, and the
samples
must
6655
be analyzed within
28 days.
6656
6657
D)
Chlorite:
6658
6659
i)
By amperometric titration:
Standard
Methods,
19
th
or
21
st
6660
ed.,
Method
4500-C102
E.
6661
6662
BOARD
NOTE:
On January 4, 2006
(at
71 Fed. Reg.
6663
388),
USEPA amended
the entry for chlorite
by
6664
amperometric
titration,
in the table at
corresponding 40
6665
CFR
141.23(k)(1)
to allow the use of Standard
Methods
6666
Online
(at
www.standardmethods.org),
Method 4500-C1O
2
6667
E (as
approved
in
2000).
The Board has
instead cited
to the
6668
21St
edition of Standard
Methods
for
the Examination
of
6669
Water
and Wastewater
(the printed version
of Standard
6670
Methods),
since the version
of Method
4500-dO
2that
6671
appears in that printed
volume is that
cited by USEPA
as
6672
acceptable
for
use. USEPA later added
Method
4500-C1O
2
6673
E fromthe
21
St
edition of Standard
Methods as an
approved
6674
alternative method
in
appendix
A to subpart
C,
added
on
6675
June 3, 2008
(at
73 Fed. Reg. 31616).
6676
6677
ii)
By spectrophotometry:
USEPA OGWDW Methods,
6678
Method
327.0, rev. 1.1.
6679
6680
iii)
By ion
chromatography: USEPA
Environmental
Inorganic
6681
Methods,
Method
300.0;
USEPA Organic and
Inorganic
6682
Methods,
Method 300.1; USEPA
OGWDW Methods,
6683
Method 317.0,
rev. 2.0, or 326.0,
rev. 1.0; or
ASTM
6684
Method D6581-00.
6685
6686
BOARD NOTE: Amperometric
titration
or spectrophotometry
6687
may
be used for
routine
daily monitoring
of chlorite
at
the
entrance
6688
to the distribution system,
as prescribed
in Section
6689
611
.382(b)(2)(A)(i).
Ion chromatography
must be used
for routine
6690
monthly
monitoring
of chlorite and
additional monitoring
of
6691
chlorite in the distribution
system,
as prescribed in Section
6692
611.382(b)(2)(A)(ii)
and (b)(2)(B).
6693
JCAR35O61
1-0815204r01
6694
2)
Analyses
under this Section
for DBPs
must
be conducted
by laboratories
6695
that
have received
certification
by USEPA or the Agency
except as
6696
specified under
subsection (b)(3) of
this
Section.
To receive certification
6697
to conduct
analyses
for
the DBP
contaminants listed
in Sections 611.312
6698
and 611.381
and Subparts
W
andY
of this Part,
the laboratory
must fulfill
6699
the requirements
of subsections
(b)(2)(A),
(b)(2)(C),
and (b)(2)(D)
of
this
6700
Section.
6701
6702
A)
The
laboratory
must
analyze
performance
evaluation
(PE) samples
6703
that
are acceptable
to USEPA or the
Agency
at least
once during
6704
each
consecutive
12-month period
by each method for
which
the
6705
laboratory
desires
certification.
6706
6707
B)
This
subsection corresponds
with 40
CFR 141.131 (b)(2)(ii),
which
6708
has expired
by
its
own terms. This statement
maintains
structural
6709
consistency
with the corresponding
federal rule.
6710
6711
C)
The laboratory
must achieve
quantitative
results on the PE
sample
6712
analyses
that are
within
the acceptance limits
set forth
in
6713
subsections
(b)(2)(C)(i)
through
(b)(2)(B)(xi)
of this Section,
6714
subject
to
the conditions
of subsections
(b)(2)(C)(xii)
and
6715
(b)(2)(C)(xiii)
of this Section:
6716
6717
i)
Chloroform
(a THM):
± 20% of true value;
6718
6719
ii)
Bromodichloromethane
(a THM):
± 20% of true value;
6720
6721
iii)
Dibromochloromethane
(a THM):
± 20% of true value;
6722
6723
iv)
Bromoform
(a
THM):
± 20% of true value;
6724
6725
v)
Monochloroacetic
Acid
(an HAA5):
± 40%
of true value;
6726
6727
vi)
Dichloroacetic
Acid (an
HAA5): + 40%
of true value;
6728
6729
vii)
Trichloroacetic
Acid (an HAA5):
± 40%
of true value;
6730
6731
viii)
Monobromoacetic
Acid
(an HAA5):
± 40%
of
true value;
6732
6733
ix)
Dibromoacetic
Acid
(an HAA5):
± 40% of true value;
6734
6735
x)
Chlorite:
±
30%
of
true
value; and
6736
JCAR35O61 1-0815204r01
6737
xi)
Bromate:
±
30% of true
value.
6738
6739
xii)
The laboratory must
meet all four of the individual THM
6740
acceptance
limits set forth
in
subsections
(b)(2)(B)(i)
6741
through (b)(2)(B)(iv)
of this Section in order
to
6742
successfully pass
a PE sample for TTHM.
6743
6744
xiii)
The laboratory
must meet the acceptance limits
for four out
6745
of the five HAA5
compounds set forth in subsections
6746
(b)(2)(B)(v)
through (b)(2)(B)(ix) of this
Section in order
to
6747
successfully pass
a PE sample for HAA5.
6748
6749
D)
The laboratory must report quantitative
data for concentrations
at
6750
least as low as the minimum
reporting levels (MRLs) listed in
6751
subsections
(b)(2)(D)(i) through (b)(2)(D)(xi)
of
this
Section,
6752
subject to the limitations
of subsections (b)(2)(D)(xii) and
6753
(b)(2)(D)(xiii)
of this Section, for all DBP samples analyzed
for
6754
compliance with Sections
611.312 and 611.385 and Subparts
W
6755
and Y of
this
Part:
6756
6757
i)
Chloroform (a THM):
0.0010 mg/i;
6758
6759
ii)
Bromodichloromethane
(a THM): 0.0010 mg!;
6760
6761
iii)
Dibromochloromethane
(a THM): 0.0010 mg/i;
6762
6763
iv)
Bromoform (a THM):
0.00 10 mg/e;
6764
6765
v)
Monochloroacetic
Acid (an HAA5): 0.0020 mg!e;
6766
6767
vi)
Dichloroacetic Acid (an HAA5): 0.0010
mgJ;
6768
6769
vii)
Trichloroacetic
Acid (an HAA5): 0.00 10 mg/e;
6770
6771
viii)
Monobromoacetic
Acid (an HAA5): 0.00 10 mg/2;
6772
6773
ix)
Dibromoacetic
Acid (an HAA5): 0.00 10 mg/i;
6774
6775
x)
Chlorite: 0.020 mg/e,
applicable to monitoring as required
6776
by Section 611.382(b)(2)(A)(ii) and (b)(2)(B);
and
6777
6778
xi)
Bromate: 0.0050,
or 0.0010 mg/C if the laboratory uses
6779
USEPA OGWDW Methods, Method 317.0,
rev. 2.0, or
JCAR35O61 1-0815204r01
6780
326.0
or USEPA Organic
and Inorganic Methods, Method
6781
321.8.
6782
6783
xii)
The calibration
curve must encompass
the regulatory MRL
6784
concentration.
Data may be reported for
concentrations
6785
lower than the regulatory
MRL as long as the precision
and
6786
accuracy
criteria are met
by analyzing an MRL check
6787
standard at the
lowest reporting limit chosen
by the
6788
laboratory. The laboratory
must verify the accuracy
of the
6789
calibration
curve at the MRL concentration
by analyzing
an
6790
MRL check standard with
a concentration less than
or
6791
equal to
110% of the MRL with each batch
of samples.
6792
The measured concentration
for the MRL check standard
6793
must be
±50%
of the
expected value, if any field
sample in
6794
the batch
has a concentration less than
five times the
6795
regulatory MRL. Method
requirements to analyze higher
6796
concentration
check standards and meet
tighter acceptance
6797
criteria for them must be
met in addition to the MRL
check
6798
standard
requirement.
6799
6800
xiii)
When adding the individual
trihalomethane or haloacetic
6801
acid
concentrations, for the compounds
listed in
6802
subsections
(b)(2)(D)(v) through (b)(2)(D)(ix)
of this
6803
Section, to calculate
the TTHM or HAA5 concentrations,
6804
respectively, a zero is used for
any analytical result that
is
6805
less than
the MRL concentration for
that DBP, unless
6806
otherwise specified
by
the
Agency.
6807
6808
3)
A party approved
by USEPA or the Agency must measure
daily chlorite
6809
samples at the
entrance to the distribution
system.
6810
6811
c)
Disinfectant residuals.
6812
6813
1)
A supplier must
measure residual disinfectant
concentrations for free
6814
chlorine, combined chlorine
(chloramines), and chlorine
dioxide by the
6815
appropriate of
the methods listed in subsections
(c)(1)(A) through (c)(1)(D)
6816
of this Section, subject
to the provisions of subsection
(c)(1)(E) of this
6817
Section:
6818
6819
A)
Free Chlorine:
6820
6821
i)
Amperometric titration using
Standard Methods,
19
th,
20
th
6822
or
21
st
ed., Method 4500-Cl D,
or ASTM Method 1253-86,
6823
1253-96,
or 1253-03;
JCAR35O61 l-0815204r01
6824
6825
ii)
DPD ferrous
titration using
Standard
Methods,
19
th, 20
th
or
6826
21st
ed., Method
4500-Cl
F;
6827
6828
iii)
DPD colorimetric
using
Standard Methods,
19
t,20
th
or
6829
21st
ed.,
Method
4500-Cl
G;
or
6830
6831
iv)
Syringaldazine
(FACTS)
using Standard
Methods,
19
th,
6832
20
th
or
21st
ed.,
Method 4500-Cl H.
6833
6834
B)
Combined
Chlorine:
6835
6836
i)
Amperometric
titration
using Standard
Methods,
19
th
20
th
6837
or
21st
ed.,
Method
4500-Cl D, or ASTM
Method 1253-86,
6838
1253-96,
or 1253-03;
6839
6840
ii)
DPD ferrous
titration using
Standard
Methods,
19
th 20
th
or
6841
21st
ed.,
Method 4500-Cl
F; or
6842
6843
iii)
DPD
colorimetric
using
Standard Methods,
19
th
20
th
or
6844
21
st
ed., Method 4500-Cl
G.
6845
6846
C)
Total Chlorine:
6847
6848
i)
Amperometric
titration
using
Standard Methods,
19
th
20
th
6849
or
21
st
ed.,
Method 4500-Cl D, or
ASTM
Method
1253-86,
6850
1253-96, or 1253-03;
6851
6852
ii)
Low-level amperometric
titration
using Standard
Methods,
6853
19
th
20
th
or
21st
ed., Method 4500-Cl
E;
6854
6855
iii)
DPD ferrous titration
using Standard
Methods,
19
th,
20
th,
or
6856
21st
ed.,
Method
4500-Cl F;
6857
6858
iv)
DPD
colorimetric
using Standard Methods,
19
th, 20
th
or
6859
21st
ed., Method 4500-Cl
G;
or
6860
6861
v)
lodometric electrode
using Standard
Methods, 19”,
20
th
or
6862
2l5t
ed.,
Method
4500-Cl
I.
6863
6864
D)
Chlorine Dioxide:
6865
JCAR35O61
1-0815204r01
6866
i)
DPD
using Standard
Methods,
19
th,
20
th
or
21st
ed.,
6867
Method 4500-dO
2
D;
6868
6869
ii)
Amperometric
Method
II using Standard
Methods,
19
th,
6870
20
th
or
21st
ed., Method
4500-dO
2
E; or
6871
6872
iii)
Lissamine
Green spectrophotometric
using
USEPA
6873
OGWDW
Method
327.0 (rev.
1.1).
6874
6875
E)
The
methods listed
are approved
for
measuring
the specified
6876
disinfectant
residual.
The
supplier
may
measure
free chlorine
or
6877
total
chlorine
for demonstrating
compliance
with
the chlorine
6878
MRDL
and
combined
chlorine,
or
total
chlorine may
be
measured
6879
for
demonstrating
compliance
with
the
chioramine
MRDL.
6880
6881
BOARD NOTE:
On
January
4, 2006
(at
71
Fed.
Reg.
388),
USEPA
6882
amended
the
entries for
free chlorine,
combined
chlorine,
and chlorine
6883
dioxide
in
the
table at
corresponding
40 CFR 141.23(k)(1)
to allow
the use
6884
of
Standard Methods
Online
(at
www.standardmethods.org),
Method
6885
4500-Cl D,
E, F,
G,
H,
or
I or
Method
4500-C10
2
E
(as approved
in 2000).
6886
The Board
has
instead
cited
to the
21st
edition
of Standard
Methods
for the
6887
Examination
of
Water
and Wastewater
(the
printed version
of Standard
6888
Methods),
since the
versions of
Method 4500-Cl
and
Method 4500-C1O
2
6889
that appear
in that
printed
volume
is that
cited by
USEPA as
acceptable
6890
for
use.
USEPA
later
added Method
4500-Cl
D,
E,
F,
G,
H, or
I
or
6891
Method
4500-C10
2
E
from the
21st
edition
of Standard
Methods
as an
6892
approved
alternative
method in
appendix
A to
subpart
C,
added
on June
3,
6893
2008 (at
73 Fed.
Reg.
31616).
6894
6895
2)
Test strips.
6896
6897
ITS Method
D99-003.
6898
6899
BOARD
NOTE:
USEPA
added
ITS
Method D99-003
as
an
6900
approved
alternative
method
in appendix
A to
subpart
C,
added
on
6901
June 3,
2008
(at
73 Fed.
Reg.
31616).
6902
6903
j)
If approved
by
the Agency,
a supplier
may
also
measure
residual
6904
disinfectant
concentrations
for
chlorine,
chioramines,
and
chlorine
6905
dioxide
by using
DPD
colorimetric
test
kits.
6906
6907
3)
A
party approved
by USEPA
or the
Agency must
measure
residual
6908
disinfectant
concentration.
JCAR35O61
1-0815204r01
6909
6910
d)
A
supplier
required
to analyze
parameters
not included
in
subsections
(b)
and (c)
of
6911
this
Section
must
use
the
methods
listed below.
A party
approved
by
USEPA
or
6912
the
Agency
must
measure
the
following
parameters:
6913
6914
6915
1)
Alkalinity.
All
methods
allowed
in Section
611.611
(a)(2
1) for
measuring
6916
alkalinity.
6917
6918
2)
Bromide:
6919
6920
A)
USEPA
Inorganic
Methods,
Method
300.0;
6921
6922
B)
USEPA
Organic
and
Inorganic
Methods,
Method
300.1;
6923
6924
C)
USEPA
OGWDW
Methods,
Method
317.0
(rev.
2.0)
or
Method
6925
326.0
(rev.
1.0);
or
6926
6927
D)
ASTM
Method
D6581-00.
6928
6929
3)
Total Organic
Carbon
(TOC),
by
any of
the
methods
listed
in
subsection
6930
(d)(3)(A)(i),
(d)(3)(A)(ii),
(d)(3)(A)(iii),
or (d)(3)(B)
of this
Section,
subject
6931
to the
limitations
of subsection
(d)(3)(C)
of
this Section:
6932
6933
A)
Standard
Methods,
19
th,
20
th
or
21
st
ed.,
using
one
of the
following
6934
methods:
6935
6936
i)
Method
5310
B
(High-Temperature
Combustion
Method);
6937
6938
ii)
Method
5310
C (Persulfate-Ultraviolet
or
Heated-
6939
Persulfate
Oxidation
Method);
or
6940
6941
iii)
Method
5310
D (Wet-Oxidation
Method).
6942
6943
BOARD
NOTE:
On
January
4, 2006
(at
71
Fed.
Reg.
388),
6944
USEPA
amended
the
entries
for
total
organic
carbon,
high
6945
temperature
combustion,
persulfate-ultraviolet
or
heated
persulfate,
6946
and wet
oxidation
at
corresponding
40
CFR
141.131
(d)(3)
to allow
6947
the
use of
Standard
Methods
Online
(at
6948
www.standardmethods.org),
Method
5310
B,
C,
or D (as
approved
6949
in 2000).
The Board
has
instead
cited to
the
21
st
edition
of
6950
Standard
Methods
for
the
Examination
of
Water
and
Wastewater
6951
(the
printed
version
of
Standard
Methods),
since
the
version
of
JCAR35O61 l-0815204r01
6952
Method
5310 B,
C,
or D that
appears in that printed volume is
that
6953
cited by USEPA as
acceptable for use. USEPA later
added
6954
Method 5310 B,
C,
orD
from the
21st
edition of Standard Methods
6955
as an approved
alternative method in appendix
A to subpart
C,
6956
added on June
3,
2008
(at 73 Fed. Reg. 31616).
6957
6958
B)
USEPA NERL Method 415.3
(rev. 1.1).
6959
6960
C)
Inorganic
carbon must be removed from the samples
prior to
6961
analysis. TOC samples
may not be filtered prior to analysis.
TOC
6962
samples
must be acidified at the time of sample
collection to
6963
achieve pH less than or equal
to
2
with minimal addition of the
6964
acid specified in
the method or by the instrument manufacturer.
6965
Acidified
TOC samples must be analyzed
within 28 days.
6966
6967
4)
Specific Ultraviolet
Absorbance (SUVA). SUVA is equal
to the UV
6968
absorption at 254 nm )
254
(UV (measured
in m’) divided by the dissolved
6969
organic carbon
(DOC) concentration (measured as mg/i).
In order to
6970
detennine SUVA, it is necessary to
separately measure UV
254 and DOC.
6971
When determining
SUVA, a supplier must use the
methods stipulated in
6972
subsection (d)(4)(A)
of this Section to measure DOC and the
method
6973
stipulated in subsection
(d)(4)(B) of this Section to measure UV
254.
SUVA
6974
must be determined on water prior to the
addition of disinfectants/oxidants
6975
by the
supplier.
DOC and 254
UV samples used to
determine a SUVA value
6976
must be taken
at the same time and at the same location.
6977
6978
A)
Dissolved
Organic Carbon (DOC). Standard Methods,
19
th
ed.,
20
th
6979
ed., or
21st
ed., Method
5310 B (High-Temperature Combustion
6980
Method),
Method 5310
C
(Persulfate-Ultraviolet or
Heated-
6981
Persulfate Oxidation Method),
or Method 5310 D (Wet-Oxidation
6982
Method) or
USEPA NERL Method 415.3 (rev. 1.1). Prior
to
6983
analysis, DOC samples must be filtered through
the
0.45
tm
6984
pore-diameter
filter as soon as practical after sampling,
not to
6985
exceed 48 hours. After filtration,
DOC samples must be acidified
6986
to achieve
pH less than or equal to 2 with minimal addition
of the
6987
acid specified in the method
or by the instrument manufacturer.
6988
Acidified
DOC samples must be analyzed within 28
days after
6989
sample collection.
Inorganic carbon must be removed from the
6990
samples prior to analysis.
Water passed through the filter prior
to
6991
filtration
of the sample must serve as the filtered
blank. This filtered
6992
blank must be analyzed
using procedures identical to those used
for
6993
analysis of the samples and
must meet the following standards:
6994
DOC less
than 0.5 mg/er; and
6995
JCAR35O61 1-0815204r01
6996
BOARD NOTE:
On January 4, 2006
(at
71 Fed. Reg.
388),
6997
USEPA amended the entries for
specific ultraviolet absorbance
6998
dissolved
organic carbon at corresponding 40 CFR
6999
141.131 (d)(4)(i) to allow
the use of Standard Methods Online
(at
7000
www.standardmethods.org),
Method 5310 B,
C,
or D
(as
approved
7001
in
2000).
The Board has instead cited to the
21
st
edition of
7002
Standard
Methods for the Examination of Water and Wastewater
7003
(the printed version of Standard
Methods),
since the version of
7004
Method 5310 B,
C,
or D that appears in that
printed
volume
is that
7005
cited by USEPA as acceptable
for use. USEPA later added
7006
Method 5310 B, C, or D from the
21
st
edition
of Standard Methods
7007
as an approved alternative
method in appendix A to subpart
C,
7008
added
on June 3,
2008
(at
73 Fed. Reg.
31616).
7009
7010
B)
Ultraviolet Absorption at 254
nm (TJV
254
).Method 5910 B
7011
(Ultraviolet Absorption Method). U’! absorption
must be measured
7012
at 253.7 nm (may be rounded
off to
254
nm). Prior to analysis,
7013
UV
254 samples must be filtered through a 0.45
im pore-diameter
7014
filter. The pH of 254
UV samples may not be
adjusted. Samples
7015
must be analyzed as
soon as practical after sampling, not to exceed
7016
48 hours; and
7017
7018
BOARD
NOTE: On January 4, 2006 (at 71 Fed.
Reg.
388),
7019
USEPA amended
the entries for specific ultraviolet absorbance
7020
ultraviolet absorption at 254
nm at corresponding 40 CFR
7021
141.131(d)(4)(ii) to allow the use of Standard
Methods Online (at
7022
www.standardmethods.org),
Method 5910 B (as approved in
7023
2000).
The Board has instead cited to the
21
st
edition of Standard
7024
Methods for the Examination
of Water and Wastewater
(the
7025
printed version
of Standard
Methods),
since the version
of Method
7026
5910 B that appears in that printed volume
is that cited by USEPA
7027
as acceptable for use.
USEPA later added Method 5910 B from
7028
the
21
St
edition of Standard Methods as an approved alternative
7029
method in appendix A to
subpart
C,
added on June 3, 2008
(at
73
7030
Fed. Reg.
31616).
7031
7032
5)
pH. All methods allowed in Section 611.61 1(a)(17)
for measuring pH.
7033
7034
6)
Magnesium. All methods allowed in
Section 611.611(a) for measuring
7035
magnesium.
7036
7037
BOARD
NOTE: Derived
from 40 CFR 141.131 (2007) and
appendix A to
40
CFR 141,
7038
as
added at 73 Fed. Reg. 31616
(June
3,
2008)(2006).
7039
JCAR35O61
1-0815204r01
7040
(Source: Amended
at 33 Ill. Reg.
effective
7041
7042
SUBPART K: GENERAL
MONITORING
AND ANALYTICAL
REQUIREMENTS
7043
7044
Section 611.480
Alternative Analytical
Techniques
7045
7046
The
Agency
mustma approve, by
a SEP
issued
pursuant to Section
611.110, an
7047
alternativealternate
analytical
technique
if it determines
that USEPA
has approved
the method
as
7048
an alternative
method by adding it
to 4OCFR
141
and the Board
has not incorporated
the
federal
7049
approval
into this
Part
611. The
Agency must
not approve an alternativealternate
analytical
7050
technique without
the concurrence
of USEPA.
The Agency
must
approve an alternate
technique
7051
if it is substantially
equivalent
to the prescribed
test in both precision
and accuracy
as it relates
to
7052
the-determination
of compliance with
any
MCL.
The use of the altemativealtemate
analytical
7053
technique must not
decrease the
frequency of monitoring
required
by this Part.
7054
7055
BOARD NOTE:
Derived from 40
CFR
141.27
(2007)(2002).
7056
7057
(Source:
Amended at 33 Ill.
Reg.
effective
7058
7059
SUBPART
L: MICROBIOLOGICAL
MONITORING
7060
AND
ANALYTICAL
REQUIREMENTS
7061
7062
Section 611.526
Analytical
Methodology
7063
7064
a)
The standard
sample volume
required for total
coliform
analysis,
regardless
of
7065
analytical
method used, is 100
mf.
7066
7067
b)
Suppliers
need only determine
the presence
or absence of
total coliforms; a
7068
determination
of total
coliform
density is not required.
7069
7070
c)
Suppliers must
conduct
total coliform analyses
in accordance
with one of the
7071
following analytical
methods,
incorporated
by reference in Section
611.102,
or in
7072
accordance
with an alternative
method approved
by
the Agency
pursuant to
7073
Section 611.480
(the
time from
sample collection
to initiation of
analysis
may
not
7074
exceed
30 hours,
and the supplier
is encouraged
but not required
to hold samples
7075
below 10°
C
during
transit):
7076
7077
1)
Total Coliform
Fermentation
Technique,
as set forth in
Standard Methods,
7078
18
th, 19
th
20
th
or
21
st
ed.: Methods
9221
A and B,
as follows:
7079
7080
A)
Lactose broth,
as
commercially
available,
may be used in
lieu
of
7081
lauryl
tryptose broth if the
supplier conducts
at least 25
parallel
7082
tests between
this medium
and lauryl
tryptose broth using
the
JCAR35O61
l-0815204r01
7083
water normally tested
and this comparison
demonstrates that the
7084
false-positive
rate and false-negative
rate for total coliforms,
using
7085
lactose broth, is less
than 10 percent;
7086
7087
B)
If inverted
tubes are used to detect
gas production, the
media
7088
should cover
these tubes at least one-half
to two-thirds after the
7089
sample is added;
and
7090
7091
C)
No requirement
exists to run the completed
phase on 10 percent
of
7092
all total colifonn-positive
confirmed tubes.
7093
7094
2)
Total Coliform
Membrane Filter
Technique, as set forth in Standard
7095
Methods,
18
th 19
th
20
th
or
21st
ed.: Methods 9222
A, B, and
C.
7096
7097
3)
Presence-Absence
(P-A) Coliform
Test, as set forth in: Standard
Methods,
7098
18
th 19
th 20
th
or
21st
ed.: Method 9221 D,
as follows:
7099
7100
A)
No requirement
exists to run the completed
phase on 10 percent
of
7101
all total coliform-positive
confirmed tubes; and
7102
7103
B)
Six-times formulation
strength may be used
if the medium is filter-
7104
sterilized rather than autoclaved.
7105
7106
4)
ONPG-MUG
test: Standard Methods,
18
th
19
th20
th
or
21st
ed.:-of
7107
from Standard Methods
outlined Method 9223.
(The ONPG-MUG test
is
7108
also known as the Autoanalysis Colilert
System).
7109
7110
5)
Colisure Test (Autoanalysis Colilert
System). (The Colisure Test
may be
7111
read after an incubation
time of 24 hours.)
7112
7113
BOARD NOTE: USEPA
included the P-A Coliform
and Colisure Tests
7114
for testing finished
water under the coliform
rule, but did not include
them
7115
for the purposes of the surface water
treatment rule, under Section
7116
611.531, for which
quantitation of total coliforms
is necessary. For these
7117
reasons,
USEPA included Standard
Methods: Method 9221
C
for
the
7118
surface water treatment
rule, but did not include
it for the purposes of
the
7119
total coliform rule, under this Section.
7120
7121
6)
E*Colite®
Test (Charm
Sciences, Inc.).
7122
7123
7)
m-ColiBlue24®
Test (Hatch Company).
7124
7125
8)
Readycult Coliforms 100
Presence/Absence Test.
JCAR35O61 1-0815204r01
7126
7127
9)
Membrane
Filter Technique
using Chromocult
Coliform
Agar.
7128
7129
10)
Colitag®
Test.
7130
7131
BOARD
NOTE: On March
12, 2007
(at
72 Fed. Reg.
11200),
USEPA
amended
7132
note ito
the table at corresponding
40 CFR
141 .21(f)(3)
to allow the use of
7133
Standard
Methods Online
(at
www.standardmethods.org),
Method 9221
A, B,
and
7134
D
(as
approved
in
1999)
or Method 9222
A, B, and
C
(as
approved in 1997);
and
7135
9223
B
(as
approved in
1997).
The Board
has cited to the
21
st
edition of
Standard
7136
Methods
for the Examination
of Water
and Wastewater
(the printed version
of
7137
Standard
Methods)
for Methods
9221
and 9223, since the cited
versions
of the
7138
methods
appears in that
reference. USEPA
later
added
Method 9221 A, B,
and
D:
7139
Method
9222
A, B, and
C;
Method 9223
from the
21st
edition
of Standard
7140
Methods
as an approved alternative
method
in appendix
A to subpart
C,
added
on
7141
June
3,
2008
(at
73 Fed.
Reg.
31616).
7142
7143
d)
This subsection
corresponds
with 40
CFR
141.21(f)(4),
which
USEPA
has
7144
marked
“reserved.” This
statement maintains
structural consistency
with the
7145
federal
regulations.
7146
7147
e)
Suppliers
must conduct
fecal coliform
analysis in accordance
with the following
7148
procedure:
7149
7150
1)
When
the
MTF Technique
or P-A
Coliform
Test is used to test
for
total
7151
coliforms,
shake the
lactose-positive presumptive
tube or
P-A vigorously
7152
and
transfer the growth with
a sterile 3-mm
loop or sterile applicator
stick
7153
into brilliant
green lactose
bile broth and EC
medium, defined
below,
to
7154
determine
the presence of
total
and fecal
coliforms, respectively.
7155
7156
2)
For approved
methods
that
use a membrane
filter, transfer the
total
7157
coliform-positive
culture
by one of the following
methods: remove
the
7158
membrane containing
the
total coliform colonies
from the substrate
with
7159
sterile forceps
and carefully curl
and insert
the membrane into a
tube of
7160
EC medium;
(the laboratory
may first remove
a
small portion
of selected
7161
colonies for
verification); swab
the entire membrane
filter surface
with a
7162
sterile cotton
swab
and transfer
the inoculum
to EC medium
(do not leave
7163
the cotton
swab in the EC
medium); or inoculate
individual
total coliform
7164
positive colonies
into EC
medium.
Gently
shake the inoculated
tubes of
7165
EC medium
to insure
adequate mixing and
incubate in a
waterbath at
44.5
7166
±0.2°
C
for 24
±2
hours.
Gas production
of any amount
in the inner
7167
fermentation
tube of
the EC
medium
indicates a positive
fecal
coliform
7168
test.
JCAR35O61 1-0815204r01
7169
7170
3)
EC
medium is described
in Standard Methods,
18
th
ed.,
19
th
ed., and
20
th
7171
ed.: Method
9221E.
7172
7173
4)
Suppliers
need
only determine the
presence or absence
of fecal coliforms;
7174
a determination
of fecal coliform
density is not required.
7175
7176
f)
Suppliers
must conduct
analysis of E.
coli in accordance with
one of the
following
7177
analytical
methods,
incorporated
by
reference
in Section
611.102:
7178
7179
1)
EC
medium
supplemented with
50
pg/f
of MUG
(final concentration).
7180
EC medium is as
described in
subsection (e)
of
this
Section. MIJG
may
7181
be added to
BC medium before autoclaving.
BC
medium supplemented
7182
with
50 tg!f MUG
is commercially
available. At least
10 me
of
BC
7183
medium supplemented
with MUG
must be used.
The inner inverted
7184
fermentation
tube
may be omitted.
The procedure for
transferring a
total
7185
coliform-positive
culture to BC medium
supplemented
with MUG is
as in
7186
subsection
(e) of
this Section for
transferring a total
coliform-positive
7187
culture to BC medium.
Observe fluorescence
with
an ultraviolet light
(366
7188
urn) in the dark after
incubating
tube at 44.5 ±2°
C
for 24±2 hours;
or
7189
7190
2)
Nutrient agar
supplemented with
100 ig/2
MUG (final concentration),
as
7191
described in
Standard
Methods,
l9t
ed. and
20
th
ed.:
Method
9222
G.
7192
This test
is used to determine
if a total coliform-positive
sample,
as
7193
determined
by the MF technique,
contains
B. coli. Alternatively,
Standard
7194
Methods,
18
th
ed.:
Method
9221 B may be
used
if the membrane
filter
7195
containing
a total coliform-positive
colony
or colonies is transferred
to
7196
nutrient
agar,
as described
in Method 9221
B (paragraph
3), supplemented
7197
with
100 Lg/€ MUG. If Method
9221
B is used, incubate the
agar plate
at
7198
35° Celsius
for four hours,
then observe the
colony
or colonies
under
7199
ultraviolet
light (366-nm)
in the dark
for
fluorescence. If fluorescence
is
7200
visible,
B. coli are present.
7201
7202
3)
Minimal
Medium ONPG-MUG
(MMO-MUG)
Test, as set forth
in
7203
Appendix D
of
this
Part.
(The Autoanalysis Colilert
System
is a MMO
7204
MUG test.)
If the MMO-MUG
test
is total
coliform positive after
a
24-
7205
hour incubation,
test the medium
for fluorescence
with a 366-nm
7206
ultraviolet
light (preferably
with a six-watt
lamp) in the
dark. If
7207
fluorescence
is observed,
the sample
is
B. coli-positive. If fluorescence
is
7208
questionable
(cannot
be definitively read)
after 24 hours
incubation,
7209
incubate
the culture for
an additional four
hours
(but
not to exceed 28
7210
hours
total), and again
test the medium
for fluorescence.
The
MMO-MUG
7211
test
with hepes
buffer
is the only approved
formulation
for the detection
of
JCAR35O61 1-0815204r01
7212
E.coli.
7213
7214
4)
The Colisure
Test (Autoanalysis
Colilert System).
7215
7216
5)
The membrane
filter
method with
MI agar.
7217
7218
6)
The
E*Colite®
Test.
7219
7220
7)
The
m-ColiBlue24®
Test.
7221
7222
8)
Readycult
Coliforms
100
Presence/Absence
Test.
7223
7224
9)
Membrane
Filter Technique
using
Chromocult Coliform
Agar.
7225
7226
10)
Colitag®
Test.
7227
7228
g)
As an option to
the method
set
forth in subsection
(f)(3) of this
Section,
a supplier
7229
with
a
total coliform-positive,
MUG-negative,
MMO-MUG
test may further
7230
analyze the culture
for
the presence
of
E.
coli
by transferring a
0.1
me,
28-hour
7231
MMO-MIJG
culture to EC
medium + MIJG with
a
pipet. The
formulation
and
7232
incubation conditions
of the
EC
medium
+
MUG, and observation
of the results,
7233
are described
in subsection
(f)(1) of this
Section.
7234
7235
h)
This
subsection corresponds
with 40
CFR 141.21
(f)(8),
a central listing
of
all
7236
documents
incorporated
by reference
into the federal microbiological
analytical
7237
methods.
The corresponding
Illinois
incorporations
by reference are
located at
7238
Section
611.102.
This
statement
maintains structural
parity with USEPA
7239
regulations.
7240
7241
BOARD NOTE:
Derived from
40
CFR 141.21(f)
(2007)
and appendix A to 40
CFR 141,
7242
as
added
at
73
Fed. Reg.
31616
(June
3, 2008)(2003).
7243
7244
(Source: Amended
at 33 Ill.
Reg.
effective
7245
7246
Section 611.531
Analytical Requirements
7247
7248
The
analytical methods
specified in
this Section, or alternative
methods
approved
by
the Agçpçy
7249
pursuant to Section
611.480, must be used
to demonstrate
compliance
with the requirements
of
7250
only 61 1.Subpart
B;
they
do not apply
to analyses
performed for the
purposes of Sections
7251
611.521
through 611.527
of this Subpart
L. Measurements
for pH,
temperature,
turbidity, and
7252
RDCs
must be
conducted under the
supervision
of a certified
operator. Measurements
for total
7253
coliforms,
fecal coliforms and
HPC must be conducted
by a laboratory
certified
by
the
Agency
to
7254
do such
analysis.
The following
procedures must
be performed
by the following
methods,
JCAR35O61
1-0815204r01
7255
incorporated
by
reference in Section
611.102:
7256
7257
a)
A
supplier shall do
as
follows:
7258
7259
1)
Conduct
analyses of pH in
accordance
with one of the methods
listed at
7260
Section
611.611; and
7261
7262
2)
Conduct analyses of
total coliforms,
fecal coliforms, heterotrophic
7263
bacteria,
and turbidity
in accordance with
one of
the following
methods,
7264
and by using analytical
test procedures
contained in USEPA
Technical
7265
Notes,
incorporated
by reference in Section
611.102, as follows:
7266
7267
A)
Total
Coliforms.
7268
7269
BOARD NOTE:
The time from
sample collection to
initiation
of
7270
analysis for source
(raw) water samples
required
by Sections
7271
611.521 and 611.532
and
Subpart
B of this Part only
must not
7272
exceed eight
hours. The supplier is
encouraged
but not required to
7273
hold samples below
10°
C during
transit.
7274
7275
i)
Total
coliform fermentation
technique: Standard
Methods,
7276
18
th 19
th
20
th
or
21
st
ed.: Method 9221
A, B, and
C.
7277
7278
BOARD NOTE: Lactose
broth,
as commercially available,
7279
may be used in
lieu of lauryl tryptose
broth if
the
supplier
7280
conducts
at
least 25
parallel tests
between this medium
and
7281
lauryl tryptose
broth using the water
normally tested
and
7282
this comparison
demonstrates that
the false-positive rate
7283
and false-negative
rate for total coliforms,
using lactose
7284
broth, is less than
10 percent. If
inverted tubes are used
to
7285
detect gas production,
the media should
cover these
tubes at
7286
least one-half to two-thirds
after
the sample is added. No
7287
requirement
exists
to run the completed
phase on 10
7288
percent of all total
coliform-positive
confirmed tubes.
7289
7290
ii)
Total coliform membrane
filter technique:
Standard
7291
Methods,
18
th
19
th
20
th
or
21st
ed.:
Method 9222
A, B,
7292
and
C.
7293
7294
iii)
ONPG-MIJG
test (also known as
the Autoanalysis
Colilert
7295
System): Standard
Methods,
th
18
19
th20
th
or
21st
ed.:
7296
Method 9223.
7297
JCAR35O61
1-0815204r01
7298
BOARD
NOTE: USEPA included the
P-A Coliform and
7299
Colisure Tests
for testing finished water under the coliform
7300
rule,
under Section
6
11.526,
but did
not
include them for
7301
the purposes
of the surface water treatment rule,
under this
7302
Section, for which
quantitation of total coliforms is
7303
necessary. For these
reasons, USEPA included Standard
7304
Methods:
Method 9221
C
for the surface water
treatment
7305
rule, but did
not include it for the purposes of the total
7306
coliform rule, under Section 611.526.
7307
7308
B)
Fecal
Coliforms.
7309
7310
BOARD
NOTE: The time from sample collection
to
initiation
of
7311
analysis for source (raw)
water samples required by Sections
7312
611.521 and6ll.532
and SubpartBofthisPartonlymustnot
7313
exceed
eight hours. The supplier is encouraged
but not required
to
7314
hold samples below
100
C
during transit.
7315
7316
i)
Fecal coliform
procedure: Standard Methods,
18
th
19
th
7317
20t
,or21St
ed.:Method9221E.
7318
7319
BOARD
NOTE: A-i broth maybe held up
to
seven
7320
ythree months
in a tightly closed screwcap tube at 4°
C
7321
(39° F).
7322
7323
ii)
Fecal
Colifonu Membrane Filter Procedure: Standard
7324
Methods,
18
th 19
th
20
th
or
21
st
ed.: Method 9222 D.
7325
7326
C)
Heterotrophic bacteria.
7327
7328
i)
Pour plate method: Standard Methods,
18
t},
l9tI,ef
20
th
7329
21ed.: Method 9215
B.
7330
7331
BOARD NOTE: The time from
sample collection to
7332
initiation
of analysis must not exceed eight hours.
The
7333
supplier is encouraged
but not required to hold samples
7334
below
10°
C
during transit.
7335
7336
ii)
SiinPlate method.
7337
7338
D)
Turbidity.
JCAR35O61 1-0815204r01
7339
BOARD
NOTE:
Styrene
divinyl
benzene
beads
(e.g.,
AMCO
7340
AEPA-1
or equivalent)
and stabilized
formazin
(e.g.,
Hach
7341
StablCalTM
or
equivalent)
are
acceptable
substitutes
for
formazin.
7342
7343
7344
i)
Nephelometric
method:
Standard
Methods,
18
th
19
th
7345
2Oth,or2lsted.:
Method
2130 B.
7346
7347
ii)
Nephelometric
method:
USEPA
Environmental
Inorganic
7348
Methods:
Method
180.1
7349
7350
iii)
GLI
Method
2.
7351
7352
iv)
Hach
FilterTrak
Method
10133.
7353
7354
E)
Temperature:
Standard
Methods,
18
th
19
th
20
th
or
21
St
ed.:
7355
Method
2550.
7356
7357
BOARD
NOTE:
On
March
12,
2007
(at 72
Fed.
Reg.
11200),
USEPA
amended
7358
the
entries
for
total
coliforms,
fecal
coliforms,
heterotrophic
bacteria,
turbidity,
7359
and
temperature
at
corresponding
40 CFR
141
.74(a)(1)
to
allow
the use
of
7360
Standard
Methods
Online
(at
www.standardmethods.org),
Method
2130
B (as
7361
approved
in
2001);
Method
9215
B
(as
approved
in
2000);
Method
9221
A,
B,
7362
and C
(as
approved
in 1999);
Method
9222 A.
B,
C,
and D
(as
approved
in
1997);
7363
and
Method
9223
B
(as
approved
in
1997).
The Board
has
instead
cited
to the
7364
21
st
edition
of
Standard
Methods
for
the
Examination
of Water
and
Wastewater
7365
(the
printed
version
of
Standard
Methods),
since
the
versions
of Method
2130,
7366
Method
9215,
Method
9221,
Method
9222,
and
Method
9223
that appear
in
that
7367
printed
volume
are
those
cited
by
USEPA
as
acceptable
for
use. USEPA
later
7368
added
Method
2130
B;
Method
9215
B;
Method
9221
A, B,
C,
and
E:
Method
7369
9222
A,
B,
C,
and
D; and
Method
9223
from
the
21st
edition
of Standard
Methods
7370
as
an
approved
alternative
method
in appendix
A to subpart
C,
added
on
June
3,
7371
2008
(at
73 Fed.
Reg.
31616).
7372
7373
b)
A
supplier
must
measure
residual
disinfectant
concentrations
with one
of the
7374
following
analytical
methods
from
Standard
Methods,
18
th_
19
th,
or
20
th
ed.
(the
7375
method
for ozone,
Method
4500
3
O
B,
appears
only
in
the
18
th
and
19
th
editions):
7376
7377
1)
Free
chlorine.
7378
7379
A)
Amperometric
Titration:
Method
4500
Cl D.
7380
JCAR35O61 1-0815204r01
7381
j)
Standard
Methods,
th,
18 19
th 20
th
or
21
st
ed.: Method
7382
4500-C1D.
7383
7384
jj)
ASTMMethodD1253-03.
7385
7386
B)
DPD Ferrous
Titrimetric: Standard
Methods,
18
th,
19th,
20
th
or
7387
21st
ed.: Method
4500-Cl F.
7388
7389
C)
DPD Colimetric:
Standard Methods,
18
th, 19
th
20
th
or
21
st
ed.:
7390
Method 4500-Cl
G.
7391
7392
D)
Syringaldazine
(FACTS):
Standard Methods,
18
th, 19
th 20
th
or
7393
2l5t
ed.: Method 4500-Cl
H.
7394
7395
2)
Total chlorine.
7396
7397
A)
Amperometric
Titration: Method 4500
Cl D.
7398
7399
j)
Standard Methods,
t1i,
18
19
th 20
th
or
21st
ed.: Method
7400
4500-C1D.
7401
7402
j
ASTM Method
D 1253-03.
7403
7404
B)
Amperometric
Titration (low level
measurement): Standard
7405
Methods,
18
th, 19
th
20
th
or
21st
ed.: Method 4500-Cl
B.
7406
7407
C)
DPD Ferrous
Titrimetric: Standard Methods,
18
th, 19
th, 20
th
or
7408
21st
ed.: Method 4500-Cl
F.
7409
7410
D)
DPD
Colimetric: Standard Methods,
18
th, 19
th 20
th
or
21st
ed.:
7411
Method 4500-Cl
G.
7412
7413
E)
lodometric Electrode:
Standard Methods,
18
th 19
th 20
th
or
21
st
7414
ed.: Method 4500-Cl
I.
7415
7416
3)
Chlorine dioxide.
7417
7418
A)
Amperometric
Titration: Standard
Methods,
18
th 19
th 20
th
or
21
st
7419
ed.: Method
4500-C10
2
C
or E.
7420
7421
B)
DPD Method: Standard Methods,
18
th, 19
th
or
20t1
ed.: Method
7422
4500-C1O
2
D.
7423
JCAR35O61
1-0815204r01
7424
c)
Spectrophotometric:
USEPA
OGWDW
Methods,
Method
327.0.
7425
7426
4)
Ozone:
Indigo
Method:
Standard
Methods,
18
th
19
th 20
th
or
21st
ed.:
7427
Method
45 00-03
B.
7428
7429
5)
Alternative
test methods:
The
Agency
may grant
a SEP pursuant
to
7430
Section 611.110
that
allows a supplier
to use
alternative
chlorine
test
7431
methods as
follows:
7432
7433
A)
DPD
colorimetric
test
kits: Residual
disinfectant
concentrations
7434
for
free chlorine
and
combined
chlorine
may also be
measured
by
7435
using
DPD
colorimetric
test kits.
7436
7437
B)
Continuous
monitoring
for free
and total chlorine:
Free
and total
7438
chlorine
residuals
may
be measured
continuously
by adapting
a
7439
specified
chlorine
residual
method
for use
with
a continuous
7440
monitoring
instrument,
provided the
chemistry,
accuracy,
and
7441
precision
remain
the same.
Instruments
used for
continuous
7442
monitoring
must
be calibrated
with
a grab
sample
measurement
at
7443
least
every five
days
or as otherwise
provided
by the Agency.
7444
7445
BOARD NOTE:
Suppliers
may
use
a
five-tube
test or
a 10-tube
7446
test.
7447
7448
BOARD
NOTE:
On
March 12,
2007
(at 72
Fed. Reg.
11200),
USEPA amended
7449
the
entries
for free chlorine,
total
chlorine,
chlorine dioxide,
and
ozone
at
7450
corresponding
40
CFR
141.74(a)(2)
to allow
the use
of Standard
Methods
Online
7451
(at
www.standardmethods.org),
Method 4500-Cl
D, E, F, G,
and
H
(as
approved
7452
in
2000);
Method
4500-C1O
2
C
and
E
(as
approved
in
2000);
and
Method
4500-
7453
03 B
(as approved
in
1997).
The
Board has
instead
cited
to the
21st
edition
of
7454
Standard
Methods
for the
Examination
of
Water and
Wastewater
(the
printed
7455
version
of Standard
Methods),
since
the versions
of Method
4500-Cl,
Method
7456
4500-CJQ
2
,
and Method
4500-03
that appear
in that printed
volume
are
those
7457
cited
by
USEPA
as
acceptable
for use.
USEPA
later
added Method
4500-Cl
D,
E,
7458
F,
G,
and
H;
Method 4500-C1O
2
C
and
E:
and
Method 4500-03
B
from the
21st
7459
edition
of Standard
Methods
as
an approved
alternative
method
in appendix
A
to
7460
subpart
C, added
on June
3, 2008
(at
73 Fed.
Reg. 31616).
7461
7462
BOARD
NOTE: Derived
from
40
CFR
141.74(a)
(2007)
and
appendix
A to 40
CFR
7463
141,
as
added at 73
Fed. Reg.
31616 (June
3, 2008)(2002).
7464
7465
(Source:
Amended
at 33
Iii. Reg.
effective
7466
JCAR35O61 1-0815204r01
7467
SUBPART
N: INORGANIC
MONITORING AN])
ANALYTICAL REQUIREMENTS
7468
7469
Section 611.600
Applicability
7470
7471
The following types of suppliers must conduct
monitoring to determine
compliance with the old
7472
MCLs in Section 6 11.300 and the revised MCLs in 611.301,
as appropriate, in accordance with
7473
this
Subpart N:
7474
7475
a)
CWS suppliers.
7476
7477
b)
NTNCWS suppliers.
7478
7479
c)
Transient non-CWS
suppliers to determine compliance
with the nitrate and nitrite
7480
MCLs.
7481
7482
d)
Detection limits. The following are detection
limits for purposes of this Subpart
7483
N
(MCLs from Section
611.301 are set forth for information
purposes only):
7484
Detection
MCL (mg/i,
Limit
Contaminant
except
asbestos) Method
(mg!’)
Antimony
0.006
Atomic
absorption-furnace
0.003
technique
Atomic absorption-furnace
0.0008
technique
(stabilized
temperature)
Inductively-coupled
plasma 0.0004
— mass
spectrometry
Atomic absorption-gaseous
0.001
hydride technique
Arsenic
0.0106
Atomic absorption-furnace
0.001
technique
Atomic
absorption-furnace
0.00005
technique
(stabilized
temperature)
JCAR35O61
1-0815204r01
Atomic
absorption-gaseous
0.001
hydride
technique
Inductively-coupled
plasma
0.0014
— mass spectrometry
Asbestos
7 MFL’
Transmission
electron
0.01
microscopy
MFL
Barium
2
Atomic
absorption-furnace
0.002
technique
Atomic
absorption-direct
0.1
aspiration
technique
Inductively-coupled
plasma
0.002
arc
furnace
Inductively-coupled
plasma
0.001
Beryllium
0.004
Atomic
absorption-furnace
0.0002
technique
Atomic
absorption-furnace
0.00002
technique
(stabilized
temperature)
Inductively-coupled
0.0003
plasma2
Inductively-coupled
plasma
0.0003
—
mass
spectrometry
Cadmium
0.005
Atomic
absorption-furnace
0.0001
technique
Inductively-coupled
plasma
0.001
Chromium
0.1
Atomic
absorption-furnace
0.001
technique
Inductively-coupled
plasma
0.007
Inductively-coupled
plasma
0.001
JCAR35O61
l-0815204r01
Cyanide
0.2
Distillation,
0.02
spectrophotometric
3
Automated
distillation,
0.005
spectrophotometric
3
Distillation, selective
0.05
electrode3
Distillation,
amenable,
0.002
spectrophotometric4
UV, distillation,
0.0005
spectrophotometric
Micro distillation,
flow
0.0006
ml
ection,Distillation,
spectrophotometric
Ligand
exchange with
0.0005
amperometry4
Mercury
0.002
Manual cold vapor
0.0002
technique
Automated cold vapor
0.0002
technique
Nickel
No MCL
Atomic absorption-furnace
0.001
technique
Atomic absorption-furnace
0.0006
technique (stabilized
temperature)
Inductively-coupled
0.005
plasma2
Inductively-coupled plasma 0.0005
— mass
spectrometry
Nitrate (as
N)
10
Manual cadmium
reduction 0.01
JCAR35O61 1-0815204r01
Automated
hydrazine
0.01
reduction
Automated cadmium
0.05
reduction
Ion-selective electrode
1
Ion chromatography
0.01
Capillary ion
0.076
electrophoresis
Nitrite (as N)
1
Spectrophotometric
0.01
Automated cadmium
0.05
reduction
Manual
cadmium reduction 0.01
Ion chromatography
0.004
Capillary
ion
0.103
electrophoresis
Selenium
0.05
Atomic absorption-furnace
0.002
technique
Atomic
absorption-gaseous 0.002
hydride technique
Thallium
0.002
Atomic absorption-furnace
0.00 1
technique
Atomic absorption-furnace
0.0007
technique (stabilized
temperature)
Inductively-coupled plasma
0.0003
— mass spectrometry
Footnotes.
“MFL” means millions
of fibers per liter less than 10 tm.
2
Using a 2x preconcentration
step as noted in Method 200.7.
Lower MDLs
may be achieved when
using a
4x
preconcentration.
Screening
method for total cyanides.
Measures
“fre&’
cyanides when distillation, digestion,
or ligand exchange
JCAR35O61
1-0815204r01
is omitted.
Lower MDLs
are reported
using
stabilized
temperature
graphite
furnace
atomic absorbtion.
6
The value
for arsenic
is
effective
January
23,
2006.
Until then,
the MCL
is 0.05
mg/2.
The MDL
reported
for USEPA
Method
200.9 (atomic
absorption-
platform
furnace
(stabilized
temperature))
was
determined
using a
2x
concentration
step during
sample digestion.
The
MDL determined
for
samples
analyzed
using
direct analyses
(i.e.,
no sample
digestion) will
be
higher.
Using
multiple
depositions,
USEPA
Method
200.9
is capable
of
obtaining
an
MDL of 0.0001
mg/i.
8
Using
selective
ion monitoring,
USEPA
Method
200.8 (ICP-MS)
is
capable
of
obtaining
an
MDL
of
0.0001
mg/i.
Measures
total
cyanides when
-digestor
is used,
and free”
cyanides
when
UV-digestor
is
bypassed.
7485
7486
BOARD
NOTE:
Subsections
(a) through
(c)
of
this Section
are derived
from 40
CFR 141.23
7487
preamble
(2007)(2003),
and
subsection
(d) of
this
Section
is
derived
from
40
CFR
141.23
7488
(a)(4)(i)
(2007)
and
appendix
A to 40
CFR
141,
as added at
73 Fed.
Reg.
31616 (June
3,
7489
2008)(2003).
See
the Board
Note at
Section 611.301(b)
relating
to the
MCL for
nickel.
7490
7491
(Source:
Amended
at 33 Ill.
Reg.
effective
7492
7493
Section
611.611
Inorganic
Analysis
7494
7495
Analytical
methods
are
from documents
incorporated
by reference
in Section
611.102.
These are
7496
mostly
referenced
by
a
short name
defined
by Section
611.102(a).
Other
abbreviations
are
7497
defined
in Section
611.101.
7498
7499
a)
Analysis
for
the
following
contaminants
must be
conducted
using the following
7500
methods
or an alternative
method
approved
pursuant
to
Section
611.480.
Criteria
7501
for
analyzing
arsenic,
chromium,
copper, lead,
nickel,
selenium,
sodium,
and
7502
thallium
with digestion
or directly
without
digestion,
and other
analytical
7503
procedures,
are contained
in
USEPA
Technical
Notes,
incorporated
by
reference
7504
in Section
611.102.
(This
document
also
contains approved
analytical
test
7505
methods that
remained
available
for compliance
monitoring
until
July 1, 1996.
7506
These
methods
are
not available
for use
after July 1,
1996.)
7507
7508
BOARD
NOTE: Because
MDLs
reported
in USEPA
Environmental
Metals
7509
Methods
200.7
and 200.9
were
determined
using a
2x
preconcentration
step
7510
during
sample
digestion,
MDLs
determined
when samples
are
analyzed by
direct
7511
analysis (i.e.,
no sample
digestion)
will be
higher.
For
direct analysis
of cadmium
7512
and
arsenic
by USEPA
Environmental
Metals
Method
200.7, and
arsenic
by
JCAR35O61 1-0815204r01
7513
Standard Methods,
18t1,
19
th 20
th
or
21st
ed., Method 3120 B sample
7514
preconcentration using pneumatic nebulization
may be required
to achieve lower
7515
detection
limits.
Preconcentration may also
be required for direct analysis
of
7516
antimony, lead,
and thallium by USEPA Environmental
Metals Method 200.9;
7517
antimony and lead
by
Standard
Methods, l8t
’-or
19
th,
or
21st
ed., Method 3113 B;
7518
and lead by ASTM Method D3559-96
D or D3559-03 D unless multiple
in-
7519
furnace depositions
are made.
7520
7521
1)
Alkalinity.
7522
7523
A)
Titrimetric.
7524
7525
i)
ASTM Method D1067-92
B or D1067-02 B; or
7526
7527
ii)
Standard Methods,
19
th
20
th
or
21st
ed.: Method
7528
2320 B.
7529
7530
BOARD NOTE:
On March 12, 2007
(at
72 Fed.
Reg.
7531
11200),
USEPA amended
the entry for alkalinity by
7532
titrimetric alkalinity
in the table at corresponding 40
CFR
7533
141.23(k)(1)
to allow the use of Standard Methods
Online
7534
(at
www.standardmethods.org),
Method 2320 B (as
7535
approved
in
1997).
The Board has
instead cited to the
21
st
7536
edition
of Standard Methods for the Examination
of Water
7537
and Wastewater
(the
printed version of Standard
Methods),
7538
since
the
version
of Method 2320
that appears in that
7539
printed volume
is that cited by USEPA as acceptable
for
7540
use. USEPA later added Method
2320 B from the
21
st
7541
edition of Standard
Methods as an approved alternative
7542
method
in appendix A to subpart
C, added on June 3, 2008
7543
(at
73 Fed. Reg.
31616).
7544
7545
B)
Electrometric
titration:
USGS Methods: Method 1-1030-85.
7546
7547
2)
Antimony.
7548
7549
A)
Inductively-coupled
plasma
— mass spectrometry: USEPA
7550
Environmental
Metals Methods: Method 200.8.
7551
7552
B)
Atomic
absorption, hydride
technique: ASTM Method D3697-92
7553
or D3697-02.
7554
JCAR35O61 1-0815204r01
7555
C)
Atomic
absorption,
platform furnace
technique:
USEPA
7556
Environmental
Metals Methods:
Method 200.9.
7557
7558
D)
Atomic
absorption,
furnace technique:
Standard
Methods,
18
t1Øf
7559
19
t
,or21s
t
ed.:
Method3ll3B.
7560
7561
BOARD
NOTE: On March
12, 2007
(at
72
Fed. Reg. 11200),
7562
USEPA
amended the
entry for antimony
by
atomic absorption,
7563
furnace
technique, in the table
at corresponding
40 CFR
7564
141 .23(k)(1)
to allow
the use of Standard Methods
Online
(at
7565
www.standardmethods.org),
Method
3113
B (as approved in
7566
1999).
The
Board has
instead cited to the
21st
edition
of
Standard
7567
Methods
for the Examination
of Water
and Wastewater (the
7568
printed version
of Standard
Methods),
since
the version of Method
7569
3113 that
appears in that printed
volume is
that
cited
by USEPA
as
7570
acceptable
for use. USEPA later
added Method
3113 B from the
7571
2lS
edition
of Standard Methods
as an approved
alternative
7572
method in
appendix A
to
subpart
C, added on
June 3, 2008
(at
73
7573
Fed. Reg.
31616).
7574
7575
)
Axially
viewed inductively-coupled
plasma
— atomic emission
7576
spectrometry
(AVICP-AES):
USEPA Methods:
Method
200.5.
7577
7578
BOARD
NOTE:
USEPA added this
method as an approved
7579
alternative method
in appendix A to
subpart
C
of 40
CFR 141,
7580
added
on
June
3,2008
(at
73 Fed. Reg.
31616).
7581
7582
3)
Arsenic.
7583
7584
BOARD
NOTE:
If ultrasonic
nebulization
is used in the determination
of
7585
arsenic
by Methods 200.7,
200.8, or Standard
Methods,
18
th 19
th
20
th
7586
or
21
st
ed.,
3120 B, the
arsenic must be in the
pentavalent state to
provide
7587
uniform signal
response.
For methods 200.7 and
3120
B, both
samples
7588
and standards
must be diluted
in
the
same
mixed
acid matrix concentration
7589
of nitric and
hydrochloric
acid with the addition
of 100 ji2 of
30%
7590
hydrogen
peroxide per 100 m2
of
solution.
For direct analysis of
arsenic
7591
with method
200.8
using
ultrasonic nebulization,
samples
and
standards
7592
must contain
one mg!e
of sodium hypochlorite.
7593
7594
A)
Inductively-coupled
plasma.
7595
7596
BOARD NOTE:
Effective
January 23, 2006, a supplier
may
no
7597
longer
employ
analytical methods
using the
ICP-AES technology
JCAR35O61
1-0815204r01
7598
because the detection
limits for these methods are
0.008 mg/C or
7599
higher.
This restriction means
that the two ICP-AES methods
7600
(USEPA Environmental
Metals Method 200.7
and Standard
7601
Methods, Method 3120
B) approved for use for the MCL
of 0.05
7602
mg/C may not be used for compliance
determinations for the
7603
revised
MCL of 0.010
mg/i?.
However,
prior to the 2005 through
7604
2007 compliance period,
a supplier may have compliance
samples
7605
analyzed
with these less sensitive
methods.
7606
7607
i)
USEPA Environmental
Metals Methods: Method 200.7;
or
7608
7609
ii)
Standard Methods,
th,
18 19
th, 20
th
or
21St
ed.: Method
7610
3120 B.
7611
7612
BOARD NOTE:
On March 12, 2007
(at
72 Fed. Reg.
7613
11200),
USEPA amended the entry for arsenic
by
7614
inductively-coupled
plasma in the table at corresponding
40
7615
CFR 141.23(k)(1)
to allow the use
of Standard Methods
7616
Online
(at
www.standardmethods.org),
Method 3120
B
(as
7617
approved in 1999). The Board
has instead cited to the
21
st
7618
edition
of Standard Methods for the Examination
of Water
7619
and Wastewater
(the
printed version of Standard Methods),
7620
since the version
of Method
3120
that appears in that
7621
printed volume is that cited
by USEPA as acceptable for
7622
use.
USEPA later added Method 3120
B from the
21St
7623
edition of Standard
Methods as an approved alternative
7624
method for several other metals in
appendix A to subpart
C,
7625
added on June
3,
2008
(at
73 Fed. Reg.
31616).
USEPA,
7626
however,
did not specifically add
Method
2130
B as to
7627
arsenic in the June
3, 2008 action.
7628
7629
B)
Inductively-coupled
plasma
— mass spectrometry: USEPA
7630
Environmental Metals
Methods: Method 200.8.
7631
7632
C)
Atomic
absorption, platform
furnace technique: USEPA
7633
Environmental
Metals Methods: Method 200.9.
7634
7635
D)
Atomic
absorption, furnace
technique.
7636
7637
i)
ASTM
Method D2972-97
C
or 2972-03
C;
or
7638
7639
ii)
Standard
Methods,
18
th.Ø
19
th
or
21
st
ed.: Method 3113
7640
B.
JCAR35O61
1-0815204r01
7641
7642
BOARD
NOTE:
On March 12, 2007
(at 72
Fed.
Reg.
7643
11200),
USEPA amended
the entry
for arsenic by atomic
7644
absorption,
furnace
technique, in the
table at corresponding
7645
40 CFR 141.23(k)(1)
to allow the
use of Standard
Methods
7646
Online
(at
www.standardmethods.org),
Method 3113
B (as
7647
approved in
1999).
The Board
has instead cited
to the
21
st
7648
edition
of Standard Methods
for the Examination
of Water
7649
and Wastewater
(the printed
version of Standard
Methods),
7650
since
the version of Method
3113 that
appears
in that
7651
printed volume
is that cited
by USEPA as acceptable
for
7652
use.
USEPA
later added Method
3113 B from
the
21St
7653
edition of
Standard Methods
as an approved alternative
7654
method in appendix
A to subpart
C,
added on June
3, 2008
7655
(at
73 Fed.
Reg. 31616).
7656
7657
E)
Atomic
absorption,
hydride technique.
7658
7659
i)
ASTM Method
D2972-97 B or 2972-03
B; or
7660
7661
ii)
Standard Methods,
18
th
19
th
or
21St
ed.: Method
3114
7662
B.
7663
7664
BOARD
NOTE: On
March 12, 2007
(at
72 Fed.
Reg.
7665
11200),
USEPA amended
the entry for
antimony by atomic
7666
absorption, hydride
technique,
in the
table at corresponding
7667
40
CFR 141.23(k)(1)
to allow the use
of Standard Methods
7668
Online
(at
www.standardmethods.org),
Method 3114 B
(as
7669
approved
in 1997). The
Board has instead
cited to the
21St
7670
edition
of Standard
Methods for the Examination
of Water
7671
and
Wastewater
(the printed
version
of Standard Methods),
7672
since the
version
of
Method 3114 that appears
in that
7673
printed
volume is that cited
by
USEPA
as acceptable for
7674
use. USEPA
later
added
Method 3114 B
from the
21St
7675
edition
of Standard Methods
as an approved alternative
7676
method
in appendix
A to subpart
C,
added
on June
3,
2008
7677
(at
73 Fed. Reg.
31616).
7678
7679
Axially viewed
inductively-coupled
plasma
— atomic emission
7680
spectrometry
(AVICP-AES):
USEPA
Methods:
Method 200.5.
7681
JCAR35O61
1-0815204r01
7682
BOARD
NOTE:
USEPA
added this
method
as an approved
7683
alternative
method
in
appendix A
to subpart
C of 40 CFR
141,
7684
added
on
June
3,2008
(at
73 Fed.
Reg.
31616).
7685
7686
4)
Asbestos:
Transmission
electron
microscopy:
USEPA
Asbestos
7687
Methods-l00.1
and USEPA
Asbestos Methods-l00.2.
7688
7689
5)
Barium.
7690
7691
A)
Inductively-coupled
plasma.
7692
7693
i)
USEPA Environmental
Metals
Methods:
Method 200.7;
or
7694
7695
ii)
Standard
Methods,
18
th
19
th
20
th
or
21st
ed.: Method
7696
3120
B.
7697
7698
BOARD
NOTE:
On March
12, 2007
(at
72
Fed. Reg.
7699
11200),
USEPA
amended
the entry
for barium
by
7700
inductively-coupled
plasma
in the
table at corresponding
40
7701
CFR
141.23(k)(1)
to
allow the
use
of
Standard
Methods
7702
Online
(at
www.standardmethods.org),
Method
3120
B
(as
7703
approved
in
1999).
The Board
has
instead
cited to the
21st
7704
edition
of Standard
Methods
for the Examination
of
Water
7705
and
Wastewater
(the
printed
version of
Standard
Methods),
7706
since
the
version of
Method
3120
that appears
in that
7707
printed
volume
is that cited
by
USEPA
as acceptable
for
7708
use.
USEPA
later
added
Method
3120 B
from
the
21st
7709
edition
of Standard
Methods
as an
approved
alternative
7710
method
in
appendix
A to
subpart
C,
added
on June
3, 2008
7711
(at
73
Fed. Reg.
31616).
7712
7713
B)
Inductively-coupled
plasma
— mass
spectrometry:
USEPA
7714
Environmental
Metals Methods:
Method
200.8.
7715
7716
C)
Atomic
absorption,
direct
aspiration
technique:
Standard Methods,
7717
18t19th,or21sted.:
Method 3111
D.
7718
7719
BOARD
NOTE:
On
March
12, 2007
(at 72
Fed.
Reg.
11200),
7720
USEPA
amended
the entry
for barium
by
atomic
absorption,
direct
7721
aspiration
technique,
in
the table at
corresponding
40 CFR
7722
141.23(k)(1)
to
allow
the use of
Standard Methods
Online
(at
7723
www.standardmethods.org),
Method
3111
D
(as
approved
in
7724
1999).
The
Board has
instead cited
to
the
21st
edition
of Standard
JCAR35O61
1-0815204r01
7725
Methods for
the Examination
of
Water and
Wastewater
(the
7726
printed
version
of
Standard
Methods),
since
the
version
of Method
7727
3111 that
appears in
that printed
volume is
that cited
by
USEPA
as
7728
acceptable
for use.
USEPA later
added
Method
3111
D from the
7729
2lS
edition
of Standard
Methods
as an
approved
alternative
7730
method
in appendix
A
to
subpart C,
added
on June
3,
2008
(at
73
7731
Fed. Reg.
31616).
7732
7733
D)
Atomic
absorption,
furnace
technique:
Standard
Methods,
18
th,
7734
l9th,or2lsted.:
Method3ll3B.
7735
7736
BOARD
NOTE:
On March
12, 2007
(at
72
Fed.
Reg. 11200),
7737
USEPA
amended
the
entry
for barium
by
atomic
absorption,
7738
furnace
technique,
in the
table at
corresponding
40
CFR
7739
141.23(k)(l)
to allow
the use
of Standard
Methods
Online
(at
7740
www.standardmethods.org),
Method
3113 B
(as
approved
in
7741
1999).
The Board
has instead
cited to
the
21st
edition
of Standard
7742
Methods
for the
Examination
of Water and
Wastewater
(the
7743
printed
version
of
Standard
Methods),
since the
version
of Method
7744
3113
that appears
in
that
printed volume
is
that cited
by
USEPA
as
7745
acceptable
for
use.
USEPA
later added
Method 3113
B from
the
7746
2lS
edition
of
Standard Methods
as
an approved
alternative
7747
method
in appendix
A
to subpart
C,
added on
June 3,
2008
(at
73
7748
Fed. Reg.
31616).
7749
7750
)
Axially viewed
inductively-coupled
plasma
— atomic
emission
7751
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
7752
7753
BOARD
NOTE:
USEPA
added
this
method
as an approved
7754
alternative
method in
appendix
A to subpart
C of
40
CFR
141,
7755
added
on
June
3,2008
(at
73 Fed.
Reg. 31616).
7756
7757
6)
Beryllium.
7758
7759
A)
Inductively-coupled
plasma.
7760
7761
i)
USEPA
Environmental
Metals
Methods:
Method
200.7;
or
7762
7763
ii)
Standard
Methods,
18
th
19
th
20
th
or
21st
ed.:
Method
7764
3120
B.
7765
7766
BOARD
NOTE:
On
March 12,
2007
(at
72 Fed.
Reg.
7767
11200),
USEPA
amended
the entry
for beryllium
by
JCAR35O61
l-0815204r01
7768
inductively-coupled
plasma
in the
table
at corresponding
40
7769
CFR
141
.23(k)(1)
to allow
the use of
Standard Methods
7770
Online
(at
www.standardmethods.org),
Method
3120
B
(as
7771
approved
in 1999).
The
Board has
instead
cited
to the
21st
7772
edition
of
Standard
Methods
for the
Examination
of Water
7773
and Wastewater
(the
printed
version
of Standard
Methods),
7774
since the
version
of
Method 3120
that
appears
in
that
7775
printed
volume
is that
cited
by
USEPA
as acceptable
for
7776
use. USEPA
later added
Method
3120
B
from the
21st
7777
edition
of
Standard
Methods
as an
approved
alternative
7778
method in
appendix
A to subpart
C,
added
on June 3,
2008
7779
(at
73 Fed.
Reg. 31616).
7780
7781
B)
Inductively-coupled
plasma —
mass spectrometry:
USEPA
7782
Environmental
Metals
Methods:
Method
200.8.
7783
7784
C)
Atomic absorption,
platform
furnace
technique:
USEPA
7785
Environmental
Metals
Methods:
Method
200.9.
7786
7787
D)
Atomic
absorption,
furnace technique.
7788
7789
i)
ASTM
Method
D3645-97
B
or
D3645-03
B;
or
7790
7791
ii)
Standard
Methods,
l8tef
19
th
or
21st
ed.: Method
3113
7792
B.
7793
7794
BOARD
NOTE:
On March
12, 2007
(at
72
Fed.
Reg.
7795
11200),
USEPA
amended
the entry
for
beryllium
by atomic
7796
absorption,
furnace
technique,
in the table
at corresponding
7797
40
CFR
141.23(k)(1)
to
allow the
use of
Standard
Methods
7798
Online
(at
www.standardmethods.org),
Method
3113 B (as
7799
approved
in 1999).
The Board
has instead
cited to
the
21
st
7800
edition
of
Standard
Methods
for the
Examination
of
Water
7801
and Wastewater
(the
printed
version
of
Standard Methods),
7802
since
the
version of
Method
3113
that appears
in that
7803
printed
volume is
that cited by
USEPA
as acceptable
for
7804
use.
USEPA
later added
Method
3113 B
from the
21
st
7805
edition
of Standard
Methods
as an approved
alternative
7806
method
in appendix
A to
subpart
C,
added
on June
3, 2008
7807
(at
73 Fed.
Reg. 31616).
7808
7809
Axially viewed
inductively-coupled
plasma
— atomic
emission
7810
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
JCAR35O61 1-0815204r01
7811
7812
BOARD
NOTE: USEPA added
this method as
an
approved
7813
alternative method
in
appendix
A to subpart
C
of
40 CFR 141,
7814
added
on
June 3,2008
(at
73
Fed.
Reg.
31616).
7815
7816
7)
Cadmium.
7817
7818
A)
Inductively-coupled
plasma
arc furnace: USEPA
Environmental
7819
Metals
Methods:
Method 200.7.
7820
7821
B)
Inductively-coupled
plasma — mass spectrometry:
USEPA
7822
Environmental
Metals
Methods: Method 200.8.
7823
7824
C)
Atomic absorption,
platform
furnace technique:
USEPA
7825
Environmental
Metals Methods:
Method 200.9.
7826
7827
D)
Atomic
absorption, furnace
technique: Standard
Methods,
18
tØf
7828
l9th,or2lsted.:
Method3ll3B.
7829
7830
BOARD
NOTE: On March
12, 2007
(at
72
Fed. Reg. 11200),
7831
USEPA
amended
the entry for cadmium
by atomic absorption,
7832
furnace
technique, in the
table
at corresponding
40 CFR
7833
141.23(k)(1)
to allow
the use of Standard
Methods Online
(at
7834
www.standardmethods.org),
Method
3113 B (as approved
in
7835
1999).
The
Board has instead cited
to the
21st
edition
of Standard
7836
Methods for the
Examination of Water
and Wastewater
(the
7837
printed
version
of Standard
Methods),
since the version
of
Method
7838
3113 that appears
in that printed volume
is that cited
by USEPA
as
7839
acceptable
for use. USEPA later
added Method 3113
B from
the
7840
21
5t
edition of
Standard Methods as
an approved
alternative
7841
method in appendix
A to subpart
C, added on June 3,
2008
(at
73
7842
Fed.
Reg.
31616).
7843
7844
)
Axially
viewed
inductively-coupled
plasma — atomic emission
7845
spectrometry (AVICP-AES):
USEPA
Methods: Method
200.5.
7846
7847
BOARD NOTE:
USEPA
added
this method as an approved
7848
alternative
method
in appendix A to
subpart
C of
40
CFR
141,
7849
added on
June 3,
2008
(at
73 Fed.
Reg.
31616).
7850
7851
8)
Calcium.
7852
7853
A)
EDTA titrimetric.
JCAR35O61 1-0815204r01
7854
7855
i)
ASTM Method
D511-93
AorD5ll-03 A; or
7856
7857
ii)
Standard
Methods,
18thor 19t1,
or 20th ed.:
Method
3500-
7858
Ca D
or Standard
Methods,
20t11
or
21st
ed.:
Method
3
500-
7859
CaB.
7860
7861
BOARD
NOTE:
On March 12, 2007
(at
72 Fed. Reg.
7862
11200),
USEPA amended
the entry
for calcium by EDTA
7863
titrimetric
in the
table at corresponding
40 CFR
7864
141.23(k)(1) to allow
the use of
Standard Methods Online
7865
(at
www.standardmethods.org),
Method
3500-Ca D
(as
7866
approved
in
1997).
The Board
has
instead cited to the
21
st
7867
edition
of Standard
Methods for the
Examination of
Water
7868
and
Wastewater (the
printed version of Standard
Methods),
7869
since
the version of
Method 3500-Ca
that appears in that
7870
printed
volume
is that
cited
by
USEPA as
acceptable
for
7871
use.
USEPA later added
Method 3500-Ca
B from the
21
st
7872
edition
of Standard
Methods as an approved
alternative
7873
method
in appendix
A to subpart
C,
added on June 3, 2008
7874
(at
73 Fed. Reg. 31616).
7875
7876
B)
Atomic
absorption,
direct aspiration.
7877
7878
i)
ASTM Method
D511-93 B
orD5ll-03 B; or
7879
7880
ii)
Standard Methods,
18
tØf
19
th
or
21st
ed.: Method
3111
7881
B.
7882
7883
BOARD
NOTE: On March
12, 2007
(at
72 Fed.
Reg.
7884
11200),
USEPA
amended the
entry for calcium
by atomic
7885
absorption, direct
aspiration,
in the table at corresponding
7886
40
CFR
141 .23(k)(1)
to allow the
use
of
Standard
Methods
7887
Online
(at
www.standardmethods.org),
Method 3111
B
(as
7888
approved
in
1999).
The Board has
instead cited to the
21st
7889
edition of Standard
Methods
for the Examination
of
Water
7890
and
Wastewater
(the
printed version
of Standard
Methods),
7891
since the version
of Method
3111 that appears in that
7892
printed volume
is that
cited
by USEPA as acceptable
for
7893
use.
USEPA
later added Method
3111 B
from the
21st
7894
edition of
Standard Methods
as an approved alternative
7895
method
in appendix
A to subpart
C,
added
on June 3, 2008
7896
(at
73 Fed. Reg. 31616).
JCAR35O61 1-0815204r01
7897
7898
C)
Inductively-coupled
plasma.
7899
7900
i)
USEPA Environmental Metals Methods: Method 200.7;
or
7901
7902
ii)
Standard
Methods, l8,
19
th, 20
th
or
21St
ed.: Method
7903
3120 B.
7904
7905
BOARD
NOTE: On March
12,
2007
(at
72 Fed. Reg.
7906
11200),
USEPA amended the entry for calcium
by
7907
inductively-coupled
plasma in the table at corresponding 40
7908
CFR
141
.23(k)(1)
to allow the use of Standard Methods
7909
Online
(at
www.standardmethods.org),
Method 3120 B (as
7910
approved
in
1999).
The Board has instead cited to the
21
st
7911
edition of Standard Methods for the Examination
of Water
7912
and Wastewater (the
printed
version
of Standard Methods),
7913
since the version of Method 3120 that appears in that
7914
printed volume is
that cited by USEPA as acceptable for
7915
use. USEPA later added Method 3120 B from the
21St
7916
edition of Standard Methods as an approved alternative
7917
method in appendix
A to subpart C, added on June 3, 2008
7918
(at 73 Fed. Reg.
31616).
7919
7920
j
Ion chromatography:
ASTM Method D6919-03.
7921
7922
j
Axially viewed
inductively-coupled plasma — atomic emission
7923
spectrometry
(AVICP-AES):
USEPA Methods: Method 200.5.
7924
7925
BOARD
NOTE: USEPA added this method as an approved
7926
alternative
method in appendix A to subpart
C
of 40 CFR 141,
7927
added on June
3,
2008
(at
73
Fed.
Reg.
31616).
7928
7929
9)
Chromium.
7930
7931
A)
Inductively-coupled plasma.
7932
7933
i)
USEPA Environmental Metals
Methods: Method 200.7; or
7934
7935
ii)
Standard
Methods,
th
18 19
th 20
th
or
21St
ed.: Method
7936
3120 B.
7937
7938
BOARD
NOTE: On March 12, 2007
(at
72 Fed. Reg.
7939
11200),
USEPA amended
the entry for chromium by
JCAR35O61
1-0815204r01
7940
inductively-coupled
plasma
in the table
at corresponding
40
7941
CFR 141.23(k)(1)
to allow the use
of Standard Methods
7942
Online
(at
www.standardmethods.org),
Method 3120
B
(as
7943
approved in
1999).
The Board has
instead cited to the
21st
7944
edition of Standard
Methods
for the Examination
of
Water
7945
and Wastewater
(the
printed
version of Standard
Methods),
7946
since
the
version
of Method
3120 that
appears
in that
7947
printed volume
is that cited
by USEPA as acceptable
for
7948
use. USEPA
later
added Method
3120
B
from the
21st
7949
edition of
Standard Methods
as an approved alternative
7950
method
in appendix A to
subpart
C,
added
on June 3, 2008
7951
(at
73 Fed.
Reg.
31616).
7952
7953
B)
Inductively-coupled
plasma
— mass
spectrometry: USEPA
7954
Environmental
Metals Methods: Method
200.8.
7955
7956
C)
Atomic
absorption,
platform furnace
technique: USEPA
7957
Environmental
Metals
Methods:
Method 200.9.
7958
7959
D)
Atomic
absorption,
furnace
technique:
Standard Methods,
181
-er
7960
l9th,or2lsted.:
Method3ll3B.
7961
7962
BOARD NOTE:
On
March
12, 2007
(at
72 Fed.
Reg. 11200),
7963
USEPA amended
the entry for
chromium by
atomic absorption,
7964
furnace technique,
in the table
at corresponding 40
CFR
7965
141
.23(k)(1)
to allow
the
use of Standard Methods
Online
(at
7966
www.standardmethods.org),
Method
3113
B (as approved in
7967
1999). The
Board
has
instead cited to the
21St
edition of
Standard
7968
Methods
for the Examination
of
Water and
Wastewater (the
7969
printed version
of Standard
Methods), since
the version
of
Method
7970
3113 that appears
in that printed
volume is that
cited by USEPA
as
7971
acceptable
for use. USEPA later
added Method
3113 B from the
7972
21
5t
edition of
Standard
Methods
as an approved
alternative
7973
method in
appendix A to subpart
C, added on
June 3, 2008 (at 73
7974
Fed. Reg. 31616).
7975
7976
Axially viewed
inductively-coupled
plasma — atomic
emission
7977
spectrometry
(AVICP-AES):
USEPA Methods:
Method 200.5.
7978
7979
BOARD
NOTE:
USEPA
added this method
as an
approved
7980
alternative
method in appendix
A to subpart
C
of 40 CFR 141,
7981
added
on June 3,2008
(at
73 Fed.
Reg.
31616).
7982
JCAR35O61
1-0815204r01
7983
10)
Copper.
7984
7985
A)
Atomic absorption,
furnace technique.
7986
7987
i)
ASTM
Method
D1688-95
C
orD1688-02
C;
or
7988
7989
ii)
Standard
Methods,
18
t1
,-ef
19
th
or
21
st
ed.: Method
3113
7990
B.
7991
7992
BOARD
NOTE:
On March 12,
2007
(at
72 Fed.
Reg.
7993
11200),
USEPA
amended
the
entry for copper by
atomic
7994
absorption,
furnace
techniciue,
in
the table
at
corresponding
7995
40
CFR
141.23(k)(1)
to allow
the use of Standard
Methods
7996
Online
(at
www.standardmethods.org),
Method 3113
B
(as
7997
approved
in 1999).
The Board has instead
cited to
the
21st
7998
edition of Standard
Methods for
the Examination of
Water
7999
and
Wastewater
(the
printed version
of
Standard
Methods),
8000
since the version of
Method 3113
that appears in that
8001
printed
volume
is that cited
by USEPA as acceptable
for
8002
use. USEPA later
added Method
3113 B from the
21st
8003
edition of Standard
Methods
as an approved alternative
8004
method
in
appendix A to
subpart C, added on
June 3, 2008
8005
(at
73
Fed. Reg. 31616).
8006
8007
B)
Atomic
absorption,
direct aspiration.
8008
8009
i)
ASTM
Method
D1688-95
A or 1688-02
A; or
8010
8011
ii)
Standard
Methods,
18
t11
0
f
19
th
or
21st
ed.:
Method
3111
8012
B.
8013
8014
BOARD NOTE:
On March
12, 2007
(at
72 Fed.
Reg.
8015
11200),
USEPA amended the
entry
for copper
by atomic
8016
absorption,
direct aspiration,
in the table at corresponding
8017
40 CFR
141.23(k)(1) to allow
the
use of
Standard Methods
8018
Online
(at
www.standardmethods.org),
Method
3111
B (as
8019
approved
in 1999). The Board
has instead
cited to the
21st
8020
edition of
Standard
Methods
for
the
Examination
of Water
8021
and Wastewater
(the
printed version of Standard
Methods),
8022
since
the version of Method
3111 that
appears in that
8023
pçjjited
volume
is that
cited
by
USEPA
as acceptable for
8024
use.
USEPA later
added Method 3111
B from the
21
st
8025
edition of Standard
Methods
as
an approved alternative
JCAR35O61
1-0815204r01
8026
method in appendix
A
to
subpart
C,
added on June 3,
2008
8027
(at
73
Fed.
Reg.
31616).
8028
8029
C)
Inductively-coupled
plasma.
8030
8031
i)
USEPA Environmental
Metals
Methods: Method
200.7;
or
8032
8033
ii)
Standard
Methods,
l8t,
19
th 20
th
or
21
st
ed.:
Method
8034
3120 B.
8035
8036
BOARD NOTE:
On March
12, 2007 (at 72 Fed.
Reg.
8037
11200),
USEPA amended the
entry for
copper
by
8038
inductively-coupled
plasma
in the table at corresponding
40
8039
CFR 141.23(k)(1)
to allow
the use of Standard Methods
8040
Online
(at
www.standardmethods.org),
Method
3120 B
(as
8041
approved in 1999).
The Board
has instead cited to
the
21st
8042
edition
of
Standard Methods for
the
Examination
of Water
8043
and Wastewater
(the
printed
version of Standard Methods),
8044
since the version
of Method 3120
that appears
in that
8045
printed volume
is that cited
by USEPA
as
acceptable
for
8046
use. USEPA
later
added
Method 3120 B from
the
21st
8047
edition
of Standard Methods
as an approved
alternative
8048
method
in appendix A to
subpart
C,
added on June 3, 2008
8049
(at 73
Fed.
Reg.
31616).
8050
8051
D)
Inductively-coupled
plasma
— mass spectrometry:
USEPA
8052
Environmental
Metals
Methods: Method 200.8.
8053
8054
B)
Atomic absorption,
platform
furnace technique:
USEPA
8055
Environmental
Metals Methods:
Method 200.9.
8056
8057
Axially viewed
inductively-coupled
plasma — atomic
emission
8058
spectrometry
(AVICP-AES):
USEPA
Methods:
Method 200.5.
8059
8060
BOARD
NOTE: USEPA added
this method
as an approved
8061
alternative method
in appendix
A to subpart
C
of
40 CFR 141,
8062
added
on
June 3, 2008
(at
73 Fed.
Reg.
31616).
8063
8064
11)
Conductivity; Conductance.
8065
8066
A)
ASTM
Method Dl
125-95(1999)_A;
or
8067
8068
B)
Standard
Methods,
th
18 19
th
20
th
or
21st
ed.: Method
2510
B.
JCAR35O61
1-0815204r01
8069
8070
BOARD
NOTE: On
March
12,2007
(at
72 Fed.
Reg. 11200),
8071
USEPA
amended
the
entry
for
conductivity
by conductance
in the
8072
table at
corresponding
40 CFR
141.23(k)(l)
to
allow the
use of
8073
Standard
Methods
Online
(at
www.standardmethods.org),
Method
8074
2510
B
(as
approved
in
1997).
The
Board
has instead
cited to
the
8075
21
St
edition of
Standard
Methods
for the
Examination
of Water
and
8076
Wastewater
(the
printed version
of Standard
Methods),
since
the
8077
version
of
Method
2510
that appears
in that
printed
volume
is that
8078
cited
by USEPA
as acceptable
for use.
USEPA
later
added
8079
Method
2510
B
from
the
215t
edition
of Standard
Methods as
an
8080
approved
alternative
method
in appendix
A
to subpart
C, added
on
8081
June
3,
2008
(at
73 Fed. Reg.
31616).
8082
8083
12)
Cyanide.
8084
8085
A)
Manual
distillation
(ASTM
Method
D2036-98
A or Standard
8086
Methods,
18
th,
19
th
or
20
th
ed.:
Method
4500-CN
C),
followed
by
8087
spectrophotometric,
amenable.
8088
8089
i)
ASTM
Method
D2036-98
B or
2036-06 B;
or
8090
8091
BOARD
NOTE:
USEPA
added ASTM
Method
2036-06
A
8092
as
an approved
alternative
method in
appendix
A to
subpart
8093
C
of 40 CFR
141,
added
on
June
3,
2008
(at
73 Fed.
Reg.
8094
31616).
8095
8096
ii)
Standard
Methods,
18t1,
19
th
20
th
or
21
st
ed.:
Method
8097
4500-CNG.
8098
8099
BOARD
NOTE:
On March
12, 2007
(at
72 Fed.
Reg.
8100
11200),
USEPA
amended
the entry
for
cyanide
by
8101
spectrophotometric,
amenable,
in
the table
at corresponding
8102
40
CFR
141.23(k)(1)
to
allow
the use of
Standard Methods
8103
Online
(at
www.standardmethods.org),
Method
4500-CN
8104
G
(as
approved
in
1999).
The
Board has
instead cited
to
8105
the
21
St
edition
of Standard
Methods
for
the Examination
of
8106
Water
and Wastewater
(the
printed
version
of Standard
8107
Methods),
since
the
version
of
Method
4500-CN
that
8108
appears
in
that
printed volume
is that
cited
by
US EPA as
8109
acceptable
for use. USEPA
later
added
Method
4500-CN
8110
G
fromthe
21
St
edition
of Standard
Methods as
an approved
JCAR35O61
1-0815204r01
8111
alternative method
in
appendix
A to subpart
C,
added
on
8112
June 3,2008
(at
73 Fed. Reg. 31616).
8113
8114
B)
Manual
distillation
(ASTM Method D2036-98
A or
Standard
8115
Methods,
18th,
19th, or 20th ed.: Method
4500-CN
C),
followed
8116
by spectrophotometric,
manual.
8117
8118
i)
ASTM
Method D2036-98
A or 2036-06
A;
8119
8120
ii)
Standard
Methods,
th,
18 19
th,
20
th
or
21St
ed.: Method
8121
4500-CNE;or
8122
8123
BOARD
NOTE: On
March 12, 2007
(at
72 Fed. Reg.
8124
11200),
USEPA
amended
the entry for
cyanide by
8125
spectrophotometric,
manual,
in the table
at corresponding
8126
40
CFR 141
.23(k)(1)
to
allow the use of Standard
Methods
8127
Online
(at
www.standardmethods.org),
Method
4500-CN
8128
E
(as
approved
in 1999).
The Board has instead
cited
to the
8129
21
5t
edition
of Standard Methods
for the Examination
of
8130
Water and
Wastewater
(the
printed
version
of Standard
8131
Methods),
since the
version of Method 4500-CN
that
8132
appears
in that printed volume
is that
cited by
US
EPA
as
8133
acceptable
for use.
USEPA later
added Method 4500-CN
8134
E
from
the
21
5t
edition of Standard Methods
as an
approved
8135
alternative method
in appendix
A
to subpart
C,
added
on
8136
June
3,
2008
(at
73 Fed. Reg. 31616).
8137
8138
iii)
USGS Methods:
Method 1-3300-85.
8139
8140
C)
Spectrophotometric,
semiautomated:Manual
distillation (ASTM
8141
Method D2036
98 A or Standard
Methods,
18th, 19th, or 20th
ed.:
8142
Method 4500
CN C),
followed by semiautomated
8143
spectrophotometric:
USEPA
Environmental
Inorganic Methods:
8144
Method 335.4.
8145
8146
D)
Selective
electrode:
Standard
Methods,
18
th 19
th
20
th
or
8147
ed.:
Method 4500-CN F.
8148
8149
BOARD
NOTE: On March
12,
2007
(at
72 Fed. Reg. 11200),
8150
USEPA
amended the entry
for
cyanide
by selective electrode
in the
8151
table
at corresponding
40 CFR 141.23(k)(1)
to allow
the use of
8152
Standard
Methods Online
(at
www.standardmethods.org),
Method
8153
4500-CN
F
(as
approved
in
1999).
The Board has instead
cited
to
JCAR35O61
1-0815204r01
8154
the
2l
edition
of
Standard
Methods
for
the Examination
of Water
8155
and
Wastewater
(the
printed
version
of
Standard
Methods),
since
8156
the
version
of Method
4500-CN
that
appears
in that
printed
8157
volume
is
that
cited by
TJSEPA
as
acceptable
for
use.
USEPA
8158
later
added
Method
4500-CN
F from
the
21St
edition
of Standard
8159
Methods
as an
approved
alternative
method
in appendix
A
to
8160
subpart
C, added
on
June
3, 2008
(at
73
Fed.
Reg. 31616).
8161
8162
E)
UV/DistillationlSpectrophotometric:
Kelada
01.
8163
8164
F)
MicrodistillationlFlow
IniectionlSpectrophotometric:
8165
DiGtillationlSpectrophotometric:
QuickChem
10-204-00-1
-X.
8166
8167
Ligand
exchange
and
amperometry.
8168
8169
ASTMMethodD6888-03.
8170
8171
jI
01 Analytical
Method
OIA-1677
DW.
8172
8173
13)
Fluoride.
8174
8175
A)
Ion
Chromatography.
8176
8177
i)
USEPA
Environmental
Inorganic
Methods:
Method
300.0
8178
or
Method
300.1;
8179
8180
ii)
ASTM
Method
D4327-97
or
D4327-03;
or
8181
8182
iii)
Standard
Methods,
18
th,
19
th,
0
f
20
th,
or
21St
ed.:
Method
8183
4110B.
8184
8185
BOARD
NOTE:
On
March
12, 2007
(at
72 Fed.
Reg.
8186
11200),
USEPA
amended
the
entry
for fluoride
by
ion
8187
chromatography
in
the table
at corresponding
40
CFR
8188
141.23(k)(1)
to
allow
the
use of
Standard
Methods
Online
8189
(at
www.standardmethods.org),
Method
4110 B
(as
8190
approved
in
2000).
The
Board
has
instead
cited to
the
21St
8191
edition
of
Standard
Methods
for
the
Examination
of Water
8192
and
Wastewater
(the
printed
version
of
Standard
Methods),
8193
since
the
version
of Method
4110
that
appears
in
that
8194
printed
volume
is
that
cited by
USEPA
as
acceptable
for
8195
use.
USEPA
later
added
Method
4110
B from
the
21
st
8196
edition
of
Standard
Methods
as an
approved
alternative
JCAR35O61
1-0815204r01
8197
method
in appendix
A to subpart
C,
added
on June
3, 2008
8198
(at
73
Fed.
Reg. 31616).
8199
8200
B)
Manual
distillation,
colorimetric
SPADNS:
Standard Methods,
8201
18
th
19
th
20
th
or
21st
ed.:
Method
4500-V B
and D.
8202
8203
BOARD NOTE:
On
March 12,
2007 (at 72
Fed. Reg.
11200),
8204
USEPA
amended
the entry
for
fluoride by
manual
distillation,
8205
colorimetry
SPADNS,
in the table
at
corresponding
40
CFR
8206
141.23(k)(1)
to
allow the
use
of Standard
Methods
Online
(at
8207
www.standardmethods.org),
Method
4500-V
B and D
(as
8208
approved
in
1997).
The
Board
has instead
cited
to
the
21st
edition
8209
of Standard
Methods
for the Examination
of
Water and
8210
Wastewater
(the
printed
version
of Standard
Methods),
since
the
8211
version of
Method
4500-V
that
appears in
that printed
volume is
8212
that
cited
by
USEPA as
acceptable
for
use.
USEPA
later
added
8213
Method
4500-V
B
and
D from the
21St
edition
of
Standard
8214
Methods
as
an approved
alternative
method
in
appendix
A to
8215
subpart
C,
added
on
June 3,2008
(at
73 Fed.
Reg.
31616).
8216
8217
C)
Manual electrode.
8218
8219
i)
ASTMMethodD1179-93B,D1179-99B,orDll79-04B;
8220
or
8221
8222
BOARD
NOTE:
USEPA added
ASTM
Method Dl
179-04
8223
B as
an
approved
alternative
method
in appendix
A
to
8224
subpart
C
of
40
CFR
141, added
on
June
3,
2008
(at
73
8225
Fed.
Reg.
31616).
8226
8227
ii)
Standard
Methods,
19
th
20
th
or
21St
ed.: Method
8228
4500-V
C.
8229
8230
BOARD
NOTE:
On March
12, 2007
(at
72
Fed. Reg.
8231
11200),
USEPA
amended
the entry
for fluoride
by manual
8232
electrode
in
the table at
corresponding
40 CFR
8233
141.23(k)(1)
to allow
the use of
Standard
Methods Online
8234
(at
www.standardmethods.org),
Method
4500-V
C
(as
8235
approved
in
1997).
The Board
has
instead
cited to the
21
st
8236
edition
of Standard
Methods
for the Examination
of
Water
8237
and
Wastewater
(the
printed
version
of Standard
Methods),
8238
since
the
version of
Method
4500-F that
appears in
that
8239
printed
volume
is that cited
by
USEPA
as acceptable
for
JCAR35O61
1-0815204r01
8240
use.
USEPA
later added
Method 4500-V
C from
the
21st
8241
edition
of Standard
Methods
as an
approved
alternative
8242
method
in
appendix
A to
subpart
C,
added on
June 3, 2008
8243
(at
73 Fed.
Reg.
31616).
8244
8245
D)
Automated
electrode:
Technicon
Methods:
Method
380-75WE.
8246
8247
E)
Automated
alizarin.
8248
8249
i)
Standard
Methods,
18
th 19
th
20
th
or
21
st
ed.: Method
8250
4500-V
E;
or
8251
8252
BOARD
NOTE: On
March 12,
2007
(at
72
Fed. Reg.
8253
11200),
USEPA
amended
the
entry
for fluoride
by
8254
automated
alizarin
in
the table
at
corresponding
40
CFR
8255
141.23(k)(1)
to allow
the use
of
Standard
Methods
Online
8256
(at
www.standardmethods.org),
Method
4500-V
E (as
8257
approved in
1997).
The
Board has
instead cited
to the
21
st
8258
edition of
Standard
Methods for
the
Examination
of
Water
8259
and
Wastewater
(the printed
version
of Standard
Methods),
8260
since the
version of
Method 4500-V
that appears
in that
8261
printed
volume
is
that cited by
USEPA
as
acceptable
for
8262
use.
USEPA
later
added Method
4500-V
E from the
21st
8263
edition
of
Standard
Methods
as an
approved
alternative
8264
method
in appendix
A to subpart
C,
added
on June
3, 2008
8265
(at
73 Fed.
Reg.
31616).
8266
8267
ii)
Technicon
Methods:
Method
129-71W.
8268
8269
Capillary
ion
electrophoresis:
ASTM
Method
D6508-00(2005)e2
8270
(rev.
2).
8271
8272
BOARD
NOTE:
On
March
12, 2007
(at
72
Fed.
Reg. 11200),
8273
USEPA
amended
the entry
for fluoride
to
add capillary
ion
8274
electrophoresis
in
the table
at corresponding
40 CFR
141.23(k)(1)
8275
to allow
the
use
of “Waters
Method
D6508, Rev.
2.” The
Board
8276
attempt
to locate
a
copy
of the method
disclosed that
it
is
an
8277
ASTM
method
originally
approved
in 2000
and
revised in
2005.
8278
The
Board
has
cited to
the ASTM
Method
D6508-00(2005)e2.
8279
8280
14)
Lead.
8281
8282
A)
Atomic
absorption,
furnace technique.
JCAR35O61
1-0815204r01
8283
8284
i)
ASTM
Method
D3559-96
D or
D3559-03
D; or
8285
8286
ii)
Standard
Methods,
18tef
19
th
or
21st
ed.:
Method
3113
8287
B.
8288
8289
BOARD
NOTE:
On March
12, 2007
(at
72
Fed.
Reg.
8290
11200),
USEPA
amended
the entry
for
lead
by
atomic
8291
absorption,
furnace
technique,
in
the
table at corresponding
8292
40
CFR
141.23(k)(1)
to
allow the
use
of Standard
Methods
8293
Online
(at
www.standardmethods.org),
Method
3113 B
(as
8294
approved
in 1999).
The
Board has
instead
cited
to
the
21st
8295
edition
of
Standard
Methods
for the
Examination
of Water
8296
and
Wastewater
(the printed
version of
Standard
Methods),
8297
since
the
version
of Method
3113
that appears
in that
8298
printed
volume
is that cited
by
USEPA
as acceptable
for
8299
use.
USEPA
later
added
Method
3113
B from the
21
st
8300
edition
of
Standard
Methods
as an approved
alternative
8301
method
in appendix
A to
subpart C,
added
on June
3, 2008
8302
(at
73 Fed.
Reg.
31616).
8303
8304
B)
Inductively-coupled
plasma —
mass
spectrometry:
USEPA
8305
Environmental
Metals
Methods:
Method
200.8.
8306
8307
C)
Atomic
absorption,
platform
furnace technique:
USEPA
8308
Environmental
Metals Methods:
Method
200.9.
8309
8310
D)
Differential
Pulse
Anodic
Stripping
Voltammetry:
Palintest
8311
Method
1001.
8312
8313
,)
Axially
viewed inductively-coupled
plasma
— atomic
emission
8314
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
8315
8316
BOARD
NOTE:
US
EPA added
this method
as an approved
8317
alternative
method
in
appendix
A to subpart
C
of 40 CFR
141,
8318
added
on
June
3,2008
(at
73 Fed.
Reg. 31616).
8319
8320
15)
Magnesium.
8321
8322
A)
Atomic
absorption.
8323
8324
i)
ASTM
Method D511-93
B
orD5ll-03
B; or
8325
JCAR35O61
1-0815204r01
8326
ii)
Standard
Methods,
18tT. e19th
or
21st
ed.:
Method
3111
8327
B.
8328
8329
BOARD
NOTE: On
March 12,
2007
(at
72 Fed. Reg.
8330
11200),
USEPA amended
the
entry for
magnesium
by
8331
atomic
absorption
in the table
at corresponding
40
CFR
8332
141.23(k)(1)
to allow
the
use of Standard
Methods
Online
8333
(at
www.standardmethods.org),
Method
3111 B
(as
8334
approved
in 1999).
The
Board has
instead
cited
to the
21
st
8335
edition of
Standard
Methods
for
the
Examination
of Water
8336
and
Wastewater
(the
printed
version
of
Standard
Methods),
8337
since the
version
of Method
3111
that
appears in
that
8338
printed
volume is
that cited
by USEPA
as acceptable
for
8339
use.
USEPA later
added Method
3111
B from the
21
st
8340
edition
of
Standard
Methods
as an
approved
alternative
8341
method
in
appendix
A to subpart
C,
added
on June
3, 2008
8342
(at
73 Fed.
Reg. 31616).
8343
8344
B)
Inductively-coupled
plasma.
8345
8346
i)
USEPA
Environmental
Metals
Methods:
Method
200.7;
or
8347
8348
ii)
Standard
Methods,
18
th 19
th
20
th
or
21st
ed.:
Method
8349
3120
B.
8350
8351
BOARD
NOTE:
On
March
12, 2007
(at
72
Fed. Reg.
8352
11200), USEPA
amended
the entry
for
magnesium
by
8353
inductively-coupled
plasma
in the
table at corresponding
40
8354
CFR
141.23(k)(1)
to
allow the
use
of Standard
Methods
8355
Online
(at
www.standardmethods.org’),
Method
3120 B
(as
8356
approved
in 1999).
The Board
has
instead cited
to
the
21
st
8357
edition
of
Standard
Methods
for
the Examination
of Water
8358
and
Wastewater
(the
printed
version
of Standard
Methods),
8359
since
the version
of Method
3120
that
appears
in that
8360
printed
volume
is that cited
by
USEPA
as acceptable
for
8361
use.
USEPA
later added
Method
3120
B from
the
21st
8362
edition of
Standard
Methods as
an
approved alternative
8363
method
in appendix
A
to subpart
C,
added on
June 3, 2008
8364
(at
73 Fed.
Reg.
31616).
8365
8366
C)
Complexation
titrimetric.
8367
8368
i)
ASTM
Method
D511-93
AorD5ll-03
A;
or
JCAR35O61 1-0815204r01
8369
8370
ii)
Standard Methods,
18
th
or
19
th
ed.: Method
3500-Mg Eor
8371
Standard Methods,
20’ or
21st
ed.: Method 3500-Mg
B.
8372
8373
BOARD NOTE:
On March
12, 2007 (at 72 Fed.
Reg.
8374
11200),
USEPA amended
the entry for magnesium
by
8375
complexation
titrimetric
in the table
at corresponding 40
8376
CFR 141.23(k)(1)
to
allow the use of Standard
Methods
8377
Online
(at
www.standardmethods.org),
Method
3500-Mg
B
8378
(as approved
in
1997).
The Board has
instead cited to
the
8379
21st
edition of Standard
Methods
for
the Examination
of
8380
Water
and
Wastewater
(the printed version
of Standard
8381
Methods),
since the version
of
Method
3500-Mg that
8382
appears
in that printed
volume is that cited
by
USEPA
as
8383
acceptable
for use. USEPA
later added
Method 3500-Mg
8384
B from
the
21
st
edition
of Standard Methods
as an approved
8385
alternative
method in appendix
A to subpart
C, added on
8386
June 3,
2008
(at
73
Fed. Reg.
31616).
8387
8388
i44)
Standard
Methods, 20th
ed.: Method 3500
Mg B.
8389
8390
)
Ion
chromatography:
ASTM
Method D6919-03.
8391
8392
Axially
viewed inductively-coupled
plasma
— atomic emission
8393
spectrometry
(AVICP-AES):
USEPA
Methods: Method
200.5.
8394
8395
BOARD
NOTE: USEPA
added
this
method as an approved
8396
alternative
method
in appendix A to subpart
C of 40
CFR 141,
8397
added
on June 3,2008
(at 73
Fed. Reg.
31616).
8398
8399
16)
Mercury.
8400
8401
A)
Manual cold
vapor technique.
8402
8403
i)
USEPA
Environmental
Metals Methods:
Method
245.1;
8404
8405
ii)
ASTM Method
D3223-97 or D3223-02;
or
8406
8407
iii)
Standard Methods,
18
t1
0
f
19
th
or
21st
ed.: Method
3112
8408
B.
8409
8410
BOARD NOTE:
On March
12, 2007
(at
72 Fed.
Reg.
8411
11200),
USEPA amended the
entry for mercury
by
manual
JCAR35O61
1-0815204r01
8412
cold vapor
technique in the table
at corresponding
40 CFR
8413
141.23(k)(1)
to
allow the
use
of Standard Methods
Online
8414
(at www.standardmethods.org),
Method 3112
B
(as
8415
approved in
1999).
The Board
has instead cited to
the
21st
8416
edition of
Standard
Methods
for the Examination
of
Water
8417
and Wastewater
(the
printed
version
of Standard
Methods),
8418
since the version
of Method
3112 that appears
in that
8419
printed
volume is that cited
by USEPA as
acceptable
for
8420
use.
USEPA later added
Method 3112
B from the
21st
8421
edition
of Standard
Methods as an approved
alternative
8422
method
in appendix A to
subpart
C,
added on June 3, 2008
8423
(at
73
Fed. Reg. 31616).
8424
8425
B)
Automated cold
vapor technique:
USEPA Inorganic
Methods:
8426
Method 245.2.
8427
8428
C)
Inductively-coupled
plasma
— mass
spectrometry: USEPA
8429
Environmental
Metals Methods: Method
200.8.
8430
8431
17)
Nickel.
8432
8433
A)
Inductively-coupled
plasma.
8434
8435
i)
USEPA Environmental
Metals Methods:
Method 200.7;
or
8436
8437
ii)
Standard
Methods,
th
18 19
th 20
th
or
21st
ed.:
Method
8438
3120 B.
8439
8440
BOARD NOTE:
On March 12, 2007
(at
72 Fed.
Reg.
8441
11200),
USEPA
amended the
entry
for nickel
by
8442
inductively-coupled
plasma in the table
at corresponding
40
8443
CFR 141.23(k)(1) to
allow the use
of Standard Methods
8444
Online
(at www.standardmethods.org),
Method 3120
B
(as
8445
approved in
1999).
The Board
has
instead cited to the
21
st
8446
edition
of Standard
Methods for the
Examination
of Water
8447
and Wastewater
(the
printed version
of Standard Methods),
8448
since
the version
of Method 3120 that
appears in
that
8449
printed volume is
that cited by USEPA
as acceptable
for
8450
use. USEPA later
added Method
3120 B from the
21st
8451
edition
of
Standard Methods as
an approved
alternative
8452
method in
appendix A to subpart
C,
added on June
3,
2008
8453
(at
73 Fed.
Reg. 31616).
8454
JCAR35O61
1-0815204r01
8455
B)
Inductively-coupled
plasma
— mass spectrometry:
USEPA
8456
Environmental
Metals
Methods:
Method
200.8.
8457
8458
C)
Atomic
absorption,
platform
furnace
technique:
USEPA
8459
Environmental
Metals
Methods: Method
200.9.
8460
8461
D)
Atomic
absorption,
direct
aspiration
technique:
Standard
Methods,
8462
l8teEr19th,or2lsted.:
Method
3111 B.
8463
8464
BOARD NOTE:
On
March 12,
2007
(at
72
Fed.
Reg.
11200),
8465
USEPA
amended
the entry
for nickel
by
atomic
absorption,
direct
8466
aspiration
technique,
in
the table
at
corresponding
40
CFR
8467
141.23(k)(1)
to
allow the
use of Standard
Methods
Online
(at
8468
www.standardmethods.org),
Method
3111
B
(as
approved
in
8469
1999).
The
Board
has
instead cited
to the
21st
edition
of
Standard
8470
Methods
for
the
Examination
of Water
and Wastewater
(the
8471
printed
version
of
Standard
Methods),
since
the version
of Method
8472
3111
that appears
in that
printed volume
is that
cited
by
USEPA
as
8473
acceptable
for
use.
USEPA
later
added
Method
3111 B
from the
8474
2lS
edition
of Standard
Methods
as
an
approved
alternative
8475
method
in appendix
A
to subpart
C,
added on
June 3, 2008
(at
73
8476
Fed. Reg.
31616).
8477
8478
E)
Atomic absorption,
furnace
technique:
Standard
Methods,
18
t
0
f
8479
l9th,or2lsted.:
Method3ll3B.
8480
8481
BOARD
NOTE:
On
March 12,
2007
(at
72 Fed. Reg.
11200),
8482
USEPA
amended
the
entry
for nickel
by
atomic
absorption,
8483
furnace
technique,
in the table
at corresponding
40
CFR
8484
141.23(k)(1)
to
allow
the use
of Standard
Methods
Online
(at
8485
www.standardmethods.org),
Method
3113 B
(as
approved
in
8486
1999).
The
Board has
instead
cited to
the
21st
edition
of Standard
8487
Methods
for the
Examination
of Water and
Wastewater
(the
8488
printed version
of
Standard
Methods),
since
the version
of Method
8489
3113
that
appears
in that
printed
volume
is
that
cited
by US EPA
as
8490
acceptable
for
use. USEPA
later
added
Method
3113
B from
the
8491
21
St
edition
of Standard
Methods
as an
approved
alternative
8492
method in
appendix A
to
subpart
C,
added
on June 3,
2008
(at
73
8493
Fed. Reg.
31616).
8494
8495
Axially
viewed inductively-coupled
plasma
— atomic
emission
8496
spectrometry
(AVICP-AES):
USEPA
Methods:
Method 200.5.
8497
JCAR35O61 1-0815204r01
8498
BOARD
NOTE: USEPA added this
method as an approved
8499
alternative
method
in appendix A to subpart
C of
40
CFR
141,
8500
added
on June 3, 2008
(at
73 Fed.
Reg. 31616).
8501
8502
18)
Nitrate.
8503
8504
A)
Ion chromatography.
8505
8506
i)
USEPA Environmental
Inorganic Methods: Method
300.0
8507
or
Method 300.1;
8508
8509
ii)
ASTM
Method D4327-97 or D4327-03;
8510
8511
iii)
Standard Methods,
th
18 19
th 20
th
or
21
st
ed.:
Method
8512
4110B;or
8513
8514
BOARD
NOTE: On March 12, 2007
(at
72
Fed. Reg.
8515
11200),
USEPA amended
the entry for nitrate by ion
8516
chromatography
in the table at corresponding
40 CFR
8517
141.23(k)(1)
to
allow
the use of Standard Methods
Online
8518
(at
www.standardmethods.org),
Method 4110 B (as
8519
approved in 2000). The Board
has instead cited to the
21
st
8520
edition
of Standard Methods for the
Examination of Water
8521
and Wastewater
(the
printed version of Standard
Methods),
8522
since the version of Method
4110 that appears in that
8523
printed
volume is that cited
by USEPA as acceptable for
8524
use. USEPA later
added Method 4110 B from the
21st
8525
edition
of Standard Methods
as an approved alternative
8526
method in appendix
A to subpart
C,
added on June
3, 2008
8527
(at
73 Fed. Reg.
31616).
8528
8529
iv)
Waters Test
Method B-lU 1 1, available from Millipore
8530
Corporation.
8531
8532
B)
Automated
cadmium reduction.
8533
8534
i)
USEPA Environmental Inorganic
Methods: Method 353.2;
8535
8536
ii)
ASTM Method D3867-90
A; or
8537
8538
iii)
Standard
Methods,
18t,
19
th
20
th
or
21
st
ed.: Method
8539
4500-NO3
F.
8540
JCAR35O61
1-0815204r01
8541
BOARD
NOTE:
On
March
12, 2007
(at
72 Fed. Reg.
8542
11200),
USEPA
amended
the entry
for nitrate
by
8543
automated
cadmium
reduction
in
the table
at corresponding
8544
40 CFR
141 .23(k)(1)
to allow
the
use of
Standard
Methods
8545
Online
(at www.standardmethods.org),
Method
4500-NO
8546
F
(as
approved
in
2000).
The Board
has instead
cited
to
the
8547
21
St
edition of
Standard
Methods for
the Examination
of
8548
Water and
Wastewater
(the
printed
version
of Standard
8549
Methods),
since
the
version of
Method
4500-NOr
that
8550
appears
in
that
printed
volume is
that
cited
by
USEPA
as
8551
acceptable
for
use.
USEPA later
added
Method
4500-NO
8552
F fromthe
21
st
edition
of Standard
Methods
as an approved
8553
alternative
method
in appendix
A
to
subpart
C,
added
on
8554
June 3, 2008
(at
73 Fed.
Reg.
31616).
8555
8556
C)
Ion selective
electrode.
8557
8558
i)
Standard
Methods,
18
th,
19
th
20
th
or
21st
ed.:
Method
8559
4500-NO
3
D;or
8560
8561
BOARD
NOTE:
On
March
12, 2007
(at
72 Fed.
Reg.
8562
11200), USEPA
amended
the entry
for nitrate
by ion
8563
selective
electrode in
the table
at
corresponding
40
CFR
8564
141.23(k)(1)
to allow
the use
of Standard
Methods
Online
8565
(at
www.standardmethods.org),
Method 4500-NO
D
(as
8566
approved
in 2000).
The Board
has instead
cited to
the
21
st
8567
edition
of
Standard
Methods
for the
Examination
of Water
8568
and
Wastewater
(the
printed
version of
Standard Methods),
8569
since
the
version
of Method
4500-NOr
that
appears
in
that
8570
printed
volume is
that cited
by
USEPA
as acceptable
for
8571
use.
USEPA
later added
Method
4500-NO
D from
the
8572
21
st
edition
of Standard
Methods
as
an approved
alternative
8573
method
in
appendix
A to subpart
C,
added
on June 3,
2008
8574
(at
73 Fed.
Reg.
31616).
8575
8576
ii)
Technical
Bulletin
601.
8577
8578
D)
Manual
cadmium
reduction.
8579
8580
i)
ASTM
Method D3867-90
B; or
8581
8582
ii)
Standard
Methods,
18
th, 19
th
20
th
or
21st
ed.:
Method
8583
4500-NO
3
E.
JCAR35O61
1-0815204r01
8584
8585
BOARD
NOTE: On
March 12,
2007 (at 72
Fed. Reg.
8586
11200),
USEPA amended
the
entry for
nitrate by manual
8587
cadmium
reduction
in the table
at
corresponding
40
CFR
8588
141.23(k)(1)
to allow
the
use of
Standard
Methods
Online
8589
(at
www.standardmethods.org),
Method
4500-NOr
E (as
8590
approved
in 2000).
The
Board has
instead cited
to the
21st
8591
edition of
Standard
Methods
for the
Examination
of
Water
8592
and
Wastewater
(the printed
version
of Standard
Methods),
8593
since the
version
of Method
4500-NOr
that appears
in
that
8594
printed
volume
is that cited
by
USEPA
as acceptable
for
8595
use.
USEPA
later
added
Method
4500-NOr
E from
the
8596
21
st
edition of
Standard Methods
as
an
approved
alternative
8597
method
in appendix
A to
subpart
C,
added
on June
3, 2008
8598
(at
73 Fed.
Reg.
31616).
8599
8600
Capillary
ion
electrophoresis:
ASTM
Method D6508-00(2005)e2
8601
(rev.
2).
8602
8603
BOARD
NOTE:
On March
12, 2007
(at
72 Fed.
Reg. 11200),
8604
USEPA amended
the
entry for nitrate
to
add
capillary
ion
8605
electrophoresis
in
the
table at
corresponding
40
CFR
141.23(k)(1)
8606
to
allow
the use
of “Waters
Method D6508,
Rev. 2.”
The Board
8607
attempt
to locate
a
copy of the
method disclosed
that
it is an
8608
ASTM
method originally
approved
in
2000 and revised
in 2005.
8609
The
Board has
cited
to the
ASTM Method
D6508-00(2005)e2.
8610
8611
19)
Nitrite.
8612
8613
A)
Ion
chromatography.
8614
8615
i)
USEPA
Environmental
Inorganic
Methods:
Method
300.0
8616
or Method
300.1;
8617
8618
ii)
ASTM
Method
D4327-97
or D4327-03;
8619
8620
iii)
Standard
Methods,
18
th
19
th
20
th
or
21
st
ed.: Method
8621
4110B;or
8622
8623
BOARD
NOTE:
On March
12, 2007
(at
72
Fed. Reg.
8624
11200),
USEPA
amended
the entry
for nitrite
by
ion
8625
chromatography
in
the
table
at
corresponding
40 CFR
8626
141.23(k)(l)
to
allow the use
of
Standard
Methods
Online
JCAR35O61 1-0815204r01
8627
(at
www.standardmethods.org),
Method
4110
B (as
8628
approved in 2000).
The Board
has instead
cited to the
21
st
8629
edition
of
Standard
Methods
for the Examination
of
Water
8630
and Wastewater
(the
printed
version
of Standard
Methods),
8631
since the version
of Method
4110 that appears
in
that
8632
printed
volume is
that
cited by USEPA as
acceptable
for
8633
use.
USEPA later added
Method 4110
B from the
21
st
8634
edition
of
Standard
Methods as an approved
alternative
8635
method
in appendix
A to subpart C,
added on June
3,
2008
8636
(at
73
Fed.
Reg.
31616).
8637
8638
iv)
Waters
Test
Method
B-101 1, available from
Millipore
8639
Corporation.
8640
8641
B)
Automated cadmium
reduction.
8642
8643
i)
USEPA Environmental
Inorganic Methods:
Method 353.2;
8644
8645
ii)
ASTM
Method D3867-90
A; or
8646
8647
iii)
Standard
Methods,
t1,
18 19
th 20
th
or
21st
ed.: Method
8648
4500-N0
3
F.
8649
8650
BOARD
NOTE:
On March 12,
2007
(at
72
Fed.
Reg.
8651
11200),
USEPA
amended
the
entry for nitrite
by
automated
8652
cadmium
reduction
in the table at
corresponding
40 CFR
8653
141.23(k)(1)
to allow the use
of Standard Methods
Online
8654
(at
www.standardmethods.org),
Method
4500-NO
F
(as
8655
approved in 2000).
The Board
has instead cited to
the
21St
8656
edition
of
Standard Methods for
the Examination
of Water
8657
and Wastewater
(the
printed
version of Standard Methods),
8658
since the version
of Method 4500-NOr
that
appears
in that
8659
printed volume
is that cited
by
USEPA
as acceptable
for
8660
use. USEPA later
added Method
4500-NOr
F from the
8661
21
5t
edition
of Standard
Methods as an
approved alternative
8662
method in appendix
A to subpart
C,
added on
June 3, 2008
8663
(at
73 Fed. Reg.
31616).
8664
8665
C)
Manual
cadmium reduction.
8666
8667
i)
ASTM
Method D3867-90 B;
or
8668
JCAR35O61
1-0815204r01
8669
ii)
Standard
Methods,
18tI,
19
th
ef20th,
01.21St
ed.:
Method
8670
4500-N0
3
E.
8671
8672
BOARD
NOTE:
On March
12, 2007
(at
72 Fed. Reg.
8673
11200),
USEPA
amended
the entry for
nitrite
by
manual
8674
cadmium
reduction
in the
table at
corresponding
40
CFR
8675
141.23(k)(1)
to
allow
the use of
Standard
Methods
Online
8676
(at
www.standardmethods.org),
Method
4500-NOr
E
(as
8677
approved
in 2000).
The
Board has
instead
cited
to the
21
5t
8678
edition
of
Standard
Methods
for
the
Examination
of
Water
8679
and
Wastewater
(the
printed
version
of
Standard
Methods),
8680
since
the
version
of Method
4500NO
that appears
in
that
8681
printed
volume
is that
cited by USEPA
as acceptable
for
8682
use.
USEPA
later added
Method 4500-NOr
E
from the
8683
21
St
edition
of Standard
Methods
as
an
approved
alternative
8684
method
in
appendix
A to
subpart
C,
added
on
June
3, 2008
8685
(at
73
Fed. Reg.
31616).
8686
8687
D)
Spectrophotometric:
Standard
Methods,
18
th 19
th
20
th
or
21
st
8688
ed.: Method
4500-NO
2
B.
8689
8690
BOARD NOTE:
On
March 12,
2007
(at
72
Fed. Reg.
11200),
8691
USEPA
amended the
entry for
nitrite
by
spectrophotometric
in
the
8692
table
at corresponding
40 CFR
141.23(k)(1)
to allow
the use
of
8693
Standard
Methods
Online
(at
www.standardmethods.org),
Method
8694
4500-NO
B
(as
approved
in 2000). The
Board has
instead
cited
8695
to the
21
5t
edition
of Standard
Methods
for
the
Examination
of
8696
Water
and Wastewater
(the
printed version
of Standard
Methods),
8697
since
the version
of
Method
4500-NO,
that
appears
in that
printed
8698
volume
is
that
cited
by USEPA
as acceptable
for
use. USEPA
8699
later
added
Method
4500-NOr
B from
the
21St
edition
of Standard
8700
Methods
as an approved
alternative
method
in appendix
A to
8701
subpart
C, added
on
June 3,2008
(at
73 Fed.
Reg.
31616).
8702
8703
Capillary
ion electrophoresis:
ASTM Method
D6508-00(2005)e2
8704
(rev. 2).
8705
8706
BOARD
NOTE:
On March
12, 2007
(at
72
Fed.
Reg. 11200),
8707
USEPA
amended
the
entry
for nitrite
to add capillary
ion
8708
electrophoresis
in
the table
at corresponding
40 CFR
141.23(k)(1)
8709
to allow
the
use
of “Waters
Method
D6508,
Rev.
2.” The
Board
8710
attempt
to locate
a copy
of the method
disclosed
that it is
an
JCAR35O61
1-0815204r01
8711
ASTM
method
originally
approved
in
2000
and revised
in
2005.
8712
The
Board has
cited
to
the
ASTM
Method
D6508-00(2005)e2.
8713
8714
20)
Orthophosphate
(unfiltered,
without
digestion
or
hydrolysis).
8715
8716
A)
Automated
colorimetric,
ascorbic
acid.
8717
8718
i)
USEPA
Environmental
Inorganic
Methods:
Method
365.1;
8719
or
8720
8721
ii)
Standard
Methods,
18
th
19
th
20
th
or
21St
ed.:
Method
8722
4500-P
F.
8723
8724
BOARD
NOTE:
USEPA
added
Method
4500-P
F
from
the
8725
21
st
edition
of
Standard
Methods
as an
approved
alternative
8726
method
in
appendix
A
to
subpart
C
of 40
CFR
141,
added
8727
on
June
3,
2008
(at
73 Fed.
Reg.
31616).
USEPA
also
8728
added
Method
4500-P
F (as
approved
in
1999)
as
available
8729
from
Standard
Methods
Online
(at
8730
www.standardmethods.org).
The
Board
has
instead
cited
8731
only to
the
21St
edition
of Standard
Methods
for
the
8732
Examination
of
Water
and
Wastewater
(the
printed
version
8733
of Standard
Methods),
since
the
version
of Method
4500-P
8734
F that
appears
in the
printed
volume
is the
1999
version
8735
available
from
the
online
source.
8736
8737
B)
Single
reagent
colorimetric,
ascorbic
acid.
8738
8739
i)
ASTMMethodD5l5-88
A;
or
8740
8741
ii)
Standard
Methods,
18
th,
19
th,
20
th
or
21
5t
ed.: Method
8742
4500-PE.
8743
8744
BOARD
NOTE:
USEPA
added
Method
4500-P
E
from
8745
the
21
5t
edition
of Standard
Methods
as an
approved
8746
alternative
method
in
appendix
A
to
subpart
C of
40
CFR
8747
141, added
on
June 3,2008
(at
73 Fed.
Reg.
31616).
8748
USEPA
also
added Method
4500-P
E
(as
approved
in
8749
1999)
as
available
from Standard
Methods
Online
(at
8750
www.standardmethods.org).
The Board
has
instead
cited
8751
only
to the
21St
edition
of
Standard
Methods
for
the
8752
Examination
of Water
and
Wastewater
(the
printed
version
8753
of
Standard
Methods),
since the
version
of Method
4500-P
JCAR35O61
1-0815204r01
8754
E that
appears in the printed volume
is the 1999
version
8755
available from the
online source.
8756
8757
C)
Colorimetric,
phosphomolybdate:
USGS
Methods: Method
I-
8758
1601-85.
8759
8760
D)
Colorimetric,
phosphomolybdate, automated-segmented
flow:
8761
USGS Methods: Method 1-2601-90.
8762
8763
E)
Colorimetric,
phosphomolybdate, automated discrete:
USGS
8764
Methods:
Method 1-2598-85.
8765
8766
F)
Ion Chromatography.
8767
8768
i)
USEPA
Environmental Inorganic Methods: Method
300.0
8769
or Method 300.1;
8770
8771
ii)
ASTM Method D4327-97
or
D4327-03;
or
8772
8773
iii)
Standard Methods,
th,
18 19
th 20
th
or
21st
ed.: Method
8774
4110B.
8775
8776
BOARD NOTE:
On March 12, 2007 (at 72 Fed.
Reg.
8777
11200),
USEPA
amended the entry for orthophosphate
by
8778
ion chromatography in the table
at corresponding 40
CFR
8779
141.23(k)(1)
to allow the use of Standard
Methods Online
8780
(at
www.standardmethods.org),
Method 4110 B
(as
8781
approved
in
2000).
The Board has instead
cited to the
21
st
8782
edition of Standard Methods
for the Examination of
Water
8783
and Wastewater
(the
printed version of Standard
Methods),
8784
since the version of Method 4110
that appears in that
8785
printed volume is that
cited by USEPA as acceptable
for
8786
use. USEPA
later added Method 4110
B from the
21st
8787
edition of Standard Methods
as an approved alternative
8788
method in
appendix A to subpart
C,
added
on June 3, 2008
8789
(at
73 Fed. Reg. 31616).
8790
8791
Capillary ion electrophoresis:
Waters Method D6508, rev. 2.
8792
8793
BOARD
NOTE: On March 12, 2007 (at
72 Fed. Reg.
11200),
8794
USEPA amended the
entry for orthophosphate to add
capillary ion
8795
electrophoresis
in the table
at corresponding 40 CFR 141 .23(k)(1)
8796
to allow
the use of “Waters Method
D6508, Rev. 2.” The Board
JCAR35O61
1-0815204r01
8797
attempt
to locate
a copy
of the method
disclosed that
it
is
an
8798
ASTM
method
originally
approved
in 2000 and
revised in
2005.
8799
The Board
has
cited
to
the ASTM
Method
D6508-00(2005)e2.
8800
8801
21)
pH:
electrometric.
8802
8803
A
Electrometric.
8804
8805
4)
USEPA
Inorganic
Methods:
Method 150.1
or
Method
150.2;
8806
8807
Bi4)
ASTM Method
D1293-95
or
D1293-99;
or
8808
8809
Ciii)
Standard
Methods,
1
gth
19
th,
20
th
or
21st
ed.:
Method
4500-
8810
H4500H+B.
8811
8812
BOARD NOTE:
On
March 12,
2007
(at
72
Fed.
Reg. 11200),
8813
USEPA
amended
the entry
for
pH by
electrometnc
in the
table
at
8814
corresponding
40
CFR
141.23(k)(1)
to
allow
the use of
Standard
8815
Methods
Online
(at www.standardmethods.org),
Method
4500-H
8816
B
(as
approved
in
2000).
The Board
has instead
cited
to the
21st
8817
edition of
Standard
Methods for
the
Examination
of
Water and
8818
Wastewater
(the
printed
version
of Standard
Methods),
since
the
8819
version
of
Method
4500-H that
appears
in
that printed
volume
is
8820
that cited
by
USEPA
as acceptable
for
use. USEPA
later added
8821
Method
4500-H
B
from
the
21st
edition
of
Standard
Methods
as
8822
an
approved
alternative
method
in
appendix
A to
subpart
C, added
8823
on June
3, 2008
(at 73 Fed.
Reg. 31616).
8824
8825
B
USEPA
Inorganic
Methods:
Method
150.2.
8826
8827
22)
Selenium.
8828
8829
A)
Atomic
absorption,
hydride.
8830
8831
i)
ASTM
Method
D3859-98
A
or
D3859-03
A;
or
8832
8833
ii)
Standard
Methods,
l8tl_ef
19
th
or
21st
ed.:
Method
3114
8834
B.
8835
8836
BOARD
NOTE:
On March
12,
2007 (at 72
Fed.
Reg.
8837
11200),
USEPA
amended
the entry
for
selenium
by atomic
8838
absorption,
hydride,
in the
table
at
corresponding
40
CFR
8839
141.23(k)(1)
to allow the
use of Standard
Methods
Online
JCAR35O61
1-0815204r01
8840
(at www.standardmethods.org),
Method
3114
B
(as
8841
approved
in
1997).
The Board
has instead
cited
to the
21st
8842
edition
of Standard
Methods
for
the
Examination
of
Water
8843
and Wastewater
(the
printed
version
of Standard
Methods),
8844
since
the
version
of
Method
3114
that
appears
in that
8845
printed
volume
is that
cited
by
USEPA
as
acceptable
for
8846
use.
USEPA
later
added Method
3114 B
from the
21
st
8847
edition
of
Standard
Methods
as
an
approved
alternative
8848
method
in
appendix
A to subpart
C,
added
on June
3, 2008
8849
(at
73 Fed.
Reg. 31616).
8850
8851
B)
Inductively-coupled
plasma
— mass
spectrometry:
USEPA
8852
Environmental
Metals
Methods:
Method
200.8.
8853
8854
C)
Atomic
absorption,
platform
furnace
technique:
USEPA
8855
Environmental
Metals
Methods:
Method
200.9.
8856
8857
D)
Atomic
absorption,
furnace
technique.
8858
8859
i)
ASTM
Method
D3859-98
B or
D3859-03
B; or
8860
8861
ii)
Standard
Methods,
18
th
19
th
or
21st
ed.:
Method
3113
8862
B.
8863
8864
BOARD
NOTE:
On March
12,
2007
(at
72 Fed.
Reg.
8865
11200),
USEPA
amended
the
entry
for
selenium
by
atomic
8866
absorption,
furnace
technique,
in
the table
at
corresponding
8867
40 CFR
141.23(k)(1)
to allow
the use
of Standard
Methods
8868
Online
(at
www.standardmethods.org),
Method
3113
B (as
8869
approved
in
1999).
The
Board
has
instead
cited
to
the
21
st
8870
edition
of
Standard
Methods
for
the Examination of
Water
8871
and Wastewater
(the
printed
version
of
Standard
Methods),
8872
since
the
version
of Method
3113
that
appears
in
that
8873
printed
volume
is
that cited
by
USEPA
as acceptable
for
8874
use.
USEPA
later
added
Method
3113
B
from
the
21st
8875
edition
of Standard
Methods
as an
approved
alternative
8876
method
in
appendix
A to
subpart
C,
added
on
June
3, 2008
8877
(at 73 Fed.
Reg.
31616).
8878
8879
Axially
viewed
inductively-coupled
plasma
— atomic
emission
8880
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
8881
JCAR35O61
1-0815204r01
8882
BOARD
NOTE: USEPA
added
this
method
as an approved
8883
alternative
method in
appendix
A to subpart
C of 40 CFR
141,
8884
added on
June 3, 2008
(at
73
Fed. Reg.
31616).
8885
8886
23)
Silica.
8887
8888
A)
Colorimetric,
molybdate
blue:
USGS
Methods:
Method
1-1700-
8889
85.
8890
8891
B)
Colorimetric,
molybdate
blue,
automated-segmented
flow:
USGS
8892
Methods:
Method
1-2700-85.
8893
8894
C)
Colorimetric:
ASTM Method
D859-94,
D859-00, or
D859-
8895
05D859
95.
8896
8897
BOARD
NOTE:
USEPA added
ASTM
Method
D859-05 as
an
8898
approved
alternative
method in
appendix
A
to subpart
C
of 40
CFR
8899
141, added
on June
3,2008
(at
73 Fed.
Reg.
31616).
8900
8901
D)
Molybdosilicate:
Standard
Methods,
18
th
or
19
th
ed.: Method
8902
4500-Si
D or Standard
Methods,
20
th
or
21st
ed.:
Method
4500-
8903
$jQ24500
Si
C.
8904
8905
BOARD
NOTE:
On March
12, 2007
(at
72 Fed.
Reg. 11200),
8906
USEPA amended
the
entry for silica
by
molybdosilicate
in the
8907
table at
corresponding
40
CFR
141.23(k)(1)
to
allow the
use
of
8908
Standard Methods
Online
(at
www.standardmethods.org),
Method
8909
4500-SiO
2
C
(as
approved
in
1997).
The
Board
has instead
cited
8910
to the
21
st
edition of
Standard Methods
for
the
Examination
of
8911
Water and
Wastewater
(the
printed
version
of
Standard
Methods),
8912
since the version
of Method
4500-SiO
2
that
appears
in
that printed
8913
volume
is
that
cited
by
USEPA
as
acceptable
for use. USEPA
8914
later added
Method 4500-Si0
2
C
from the
21st
edition
of Standard
8915
Methods
as
an approved
alternative
method
in
appendix
A to
8916
subpart
C,
added
on June
3,2008
(at
73 Fed.
Reg.
31616).
8917
8918
E)
Heteropoly
blue: Standard
Methods,
18
th
or
19
th
ed.:
Method
8919
4500-Si
E or Standard
Methods,
20
th
or
21
st
ed.:
Method
4500-
8920
SjQ24500
Si
D.
8921
8922
BOARD
NOTE:
On
March 12.
2007
(at
72
Fed. Reg.
11200),
8923
USEPA
amended the
entry for
silica
by
heteropoly
blue in the
8924
table at
corresponding
40 CFR
141.23(k)(1)
to allow
the use
of
JCAR35O61
1-0815204r01
8925
Standard Methods
Online
(at
www.standardmethods.org),
Method
8926
4500-SiO2
D (as approved in
1997).
The Board
has instead cited
8927
to the
21
st
edition
of Standard
Methods for the
Examination of
8928
Water and
Wastewater
(the
printed version
of Standard Methods),
8929
since
the version of Method
4500-Si0
2
that appears in that printed
8930
volume
is that cited by
USEPA
as
acceptable
for use. USEPA
8931
later
added Method
2
4500-Si0 D from the
21
st
edition
of
Standard
8932
Methods as an approved
alternative
method in appendix A
to
8933
subpart
C, added
on June 3, 2008 (at
73 Fed. Reg.
31616).
8934
8935
F)
Automated
method
for molybdate-reactive
silica:
Standard
8936
Methods,
18
th
or
19
th
ed.:
Method
4500-Si F or Standard
Methods,
8937
20
th
or
21
St
ed.:
Method
4500
Si 4500-SiO2
E.
8938
8939
BOARD
NOTE: On March
12,
2007
(at
72 Fed. Reg. 11200),
8940
USEPA amended
the
entry for silica
by
automated
method
for
8941
molybdate-reactive
silica in
the
table at
corresponding 40 CFR
8942
141.23(k)(1)
to allow
the use of Standard Methods
Online
(at
8943
www.standardmethods.org),
Method 2
4500-Si0
E
(as
approved
in
8944
1997).
The Board has
instead cited
to the
21
st
edition of
Standard
8945
Methods
for the Examination
of Water
and
Wastewater
(the
8946
printed
version
of Standard Methods),
since the version
of Method
8947
4500-SiO
2that appears
in
that
printed volume is that
cited
by
8948
USEPA as
acceptable
for use.
USEPA later added
Method 45
00-
8949
$iQ2
E from
the
21
st
edition of
Standard Methods
as an approved
8950
alternative method
in appendix
A to subpart
C,
added
on June
3,
8951
2008
(at
73 Fed. Reg.
31616).
8952
8953
G)
Inductively-coupled
plasma.
8954
8955
i)
USEPA
Environmental
Metals Methods:
Method 200.7; or
8956
8957
ii)
Standard
Methods, l8,
19
th
20
th
or
21
st
ed.:
Method
8958
3120 B.
8959
8960
BOARD
NOTE: On March
12, 2007
(at
72 Fed. Reg.
8961
11200),
USEPA amended
the entry for silica
by
8962
inductively-coupled
plasma in the table at
corresponding 40
8963
CFR
141.23(k)(1)
to allow
the use of
Standard Methods
8964
Online
(at
www.standardmethods.org),
Method 3120 B
(as
8965
approved
in
1999).
The Board has instead
cited to the
21st
8966
edition of Standard
Methods for
the Examination of
Water
8967
and Wastewater
(the
printed
version
of
Standard
Methods),
JCAR35O61
1-0815204r01
8968
since
the version
of
Method
3120
that appears
in
that
8969
printed
volume
is that
cited
by USEPA
as
acceptable
for
8970
use.
USEPA
later
added Method
3120
B
from the
21st
8971
edition
of
Standard
Methods
as
an
approved
alternative
8972
method
in
appendix
A to
subpart
C,
added
on June
3, 2008
8973
(at
73
Fed.
Reg.
31616).
8974
8975
Axially
viewed
inductively-coupled
plasma
— atomic
emission
8976
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
8977
8978
BOARD
NOTE:
USEPA
added
this method
as an
approved
8979
alternative
method
in
appendix
A
to
subpart
C
of 40 CFR
141,
8980
added
on
June 3,2008
(at
73 Fed.
Reg.
31616).
8981
8982
24)
Sodium.
8983
8984
A)
Inductively-coupled
plasma:
USEPA
Environmental
Metals
8985
Methods:
Method
200.7.
8986
8987
B)
Atomic
absorption,
direct
aspiration:
Standard
Methods,
l8th1ef
8988
l9th,or2lsted.:
Method3lllB.
8989
8990
BOARD
NOTE:
On
March
12,
2007
(at 72 Fed.
Reg.
11200),
8991
USEPA
amended
the
entry for
sodium
by
atomic
absorption,
direct
8992
aspiration,
in
the table
at corresponding 40
CFR
141.23(k)(l)
to
8993
allow
the use
of Standard
Methods
Online
(at
8994
www.standardmethods.org), Method
3111
B (as
approved
in
8995
1999).
The
Board has
instead
cited
to
the
21
st
edition
of
Standard
8996
Methods
for the
Examination
of Water
and
Wastewater
(the
8997
printed
version
of Standard
Methods),
since
the version
of
Method
8998
3111
that
appears
in
that printed
volume
is that
cited
by USEPA
as
8999
acceptable
for
use.
USEPA
later
added
Method
3111
B from
the
9000
21
st
edition
of
Standard
Methods
as
an
approved
alternative
9001
method
in appendix
A
to subpart
C,
added
on
June
3, 2008
(at
73
9002
Fed. Reg.
31616).
9003
9004
c)
Ion
chromatography:
ASTM
Method
D6919-03.
9005
9006
J)
Axially
viewed
inductively-coupled
plasma
— atomic
emission
9007
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
9008
JCAR35O61 1-0815204r01
9009
BOARD
NOTE:
USEPA added
this method
as an
approved
9010
alternative
method in
appendix A to
subpart
C
of
40 CFR 141,
9011
added
on
June 3,2008
(at
73 Fed.
Reg. 31616).
9012
9013
25)
Temperature;
thermometric:
Standard
Methods,
1
gth 19
th
20
th
or
9014
ed.: Method
2550.
9015
9016
BOARD
NOTE: On
March 12,
2007
(at
72 Fed.
Reg.
11200),
USEPA
9017
amended
the entry
for temperature
by thermometric
in
the table
at
9018
corresponding 40
CFR 141.23(k)(1)
to allow
the
use of Standard
Methods
9019
Online
(at
www.standardmethods.org),
Method 2550
(as
approved
in
9020
2000).
The Board has
instead
cited
to the
21
st
edition of Standard
9021
Methods
for the Examination
of Water
and Wastewater
(the
printed
9022
version
of Standard Methods),
since
the version of
Method 2550 that
9023
appears
in that printed volume
is that cited
by USEPA
as acceptable
for
9024
use. USEPA
later added
Method 2550
from the
21
st
edition
of Standard
9025
Methods
as an approved
alternative method
in
appendix
A to subpart
C,
9026
added on
June 3, 2008
(at
73 Fed.
Reg. 31616).
9027
9028
26)
Thallium.
9029
9030
A)
Inductively-coupled
plasma
— mass
spectrometry:
USEPA
9031
Environmental
Metals
Methods: Method
200.8.
9032
9033
B)
Atomic
absorption, platform
furnace
technique:
USEPA
9034
Environmental
Metals
Methods:
Method 200.9.
9035
9036
b)
Sample collection for
antimony,
arsenic (effective
January 22, 2004),
asbestos,
9037
barium,
beryllium,
cadmium, chromium,
cyanide,
fluoride,
mercury,
nickel,
9038
nitrate, nitrite, selenium,
and
thallium
pursuant to
Sections 611.600
through
9039
611.604
must be conducted
using the
following
sample
preservation,
container,
9040
and maximum holding
time procedures:
9041
9042
BOARD
NOTE:
For
cyanide determinations
samples
must
be adjusted
with
9043
sodium
hydroxide to pH
12
at the time
of collection.
When chilling is indicated
9044
the sample must
be shipped
and stored
at
4°
C
or less.
Acidification of nitrate
or
9045
metals samples
may be with a concentrated
acid
or a
dilute
(50% by volume)
9046
solution of the applicable
concentrated
acid.
Acidification
of samples for metals
9047
analysis is
encouraged and
allowed at the laboratory
rather
than at the time
of
9048
sampling
provided the shipping
time and
other instructions
in Section 8.3 of
9049
USEPA Environmental
Metals Method
200.7, 200.8, or 200.9
are followed.
9050
9051
1)
Antimony.
JCAR35O61 1-0815204r01
9052
9053
A)
Preservative:
Concentrated
nitric acid to pH less than 2.
9054
9055
B)
Plastic or glass (hard or
soft).
9056
9057
C)
Holding time:
Samples must be analyzed
as soon after collection
9058
as possible, but in any
event within six
months.
9059
9060
2)
Arsenic.
9061
9062
A)
Preservative:
Concentrated nitric
acid to pH less than 2.
9063
9064
B)
Plastic or glass (hard
or soft).
9065
9066
C)
Holding time: Samples
must be analyzed as
soon after collection
9067
as possible, but in
any event within
six months.
9068
9069
3)
Asbestos.
9070
9071
A)
Preservative:
Cool to 4°
C.
9072
9073
B)
Plastic or glass (hard
or soft).
9074
9075
C)
Holding
time: Samples must
be analyzed as soon after
collection
9076
as possible, but
in any event within 48
hours.
9077
9078
4)
Barium.
9079
9080
A)
Preservative:
Concentrated nitric
acid to pH less than 2.
9081
9082
B)
Plastic or glass
(hard or soft).
9083
9084
C)
Holding time: Samples
must be analyzed
as soon after collection
9085
as possible,
but in any event within
six months.
9086
9087
5)
Beryllium.
9088
9089
A)
Preservative:
Concentrated
nitric acid to pH less
than 2.
9090
9091
B)
Plastic or glass
(hard or soft).
9092
9093
C)
Holding
time: Samples
must be analyzed as soon after
collection
9094
as possible,
but in any event within
six months.
JCAR35O61 1-0815204r01
9095
9096
6)
Cadmium.
9097
9098
A)
Preservative:
Concentrated nitric acid
to pH less
than 2.
9099
9100
B)
Plastic
or glass
(hard or soft).
9101
9102
C)
Holding time:
Samples must
be analyzed as
soon after collection
9103
as
possible,
but in any event within
six months.
9104
9105
7)
Chromium.
9106
9107
A)
Preservative:
Concentrated nitric
acid
to pH
less than 2.
9108
9109
B)
Plastic or
glass (hard or soft).
9110
9111
C)
Holding time:
Samples must be
analyzed
as
soon after collection
9112
as
possible, but
in any event within
six months.
9113
9114
8)
Cyanide.
9115
9116
A)
Preservative:
Cool to 4°
C.
Add sodium
hydroxide to pH greater
9117
than 12.
See the analytical
methods for information
on sample
9118
preservation.
9119
9120
B)
Plastic
or
glass (hard
or soft).
9121
9122
C)
Holding
time: Samples
must be analyzed
as soon after
collection
9123
as
possible, but in any
event within
14 days.
9124
9125
9)
Fluoride.
9126
9127
A)
Preservative:
None.
9128
9129
B)
Plastic or
glass (hard or
soft).
9130
9131
C)
Holding
time: Samples
must be analyzed
as soon after collection
9132
as possible,
but in
any event within one
month.
9133
9134
10)
Mercury.
9135
9136
A)
Preservative:
Concentrated nitric
acid to pH less than
2.
9137
JCAR35O61
l-0815204r01
9138
B)
Plastic or glass (hard
or
soft).
9139
9140
C)
Holding time: Samples
must be
analyzed
as
soon after collection
9141
as possible, but
in any event
within 28 days.
9142
9143
11)
Nickel.
9144
9145
A)
Preservative:
Concentrated
nitric acid to
pH less than 2.
9146
9147
B)
Plastic
or glass (hard or
soft).
9148
9149
C)
Holding
time: Samples must
be analyzed
as soon after
collection
9150
as possible,
but in any
event within six months.
9151
9152
12)
Nitrate,
chlorinated.
9153
9154
A)
Preservative:
Cool to 4°
C.
9155
9156
B)
Plastic or
glass (hard or
soft).
9157
9158
C)
Holding time:
Samples
must be analyzed
as soon after collection
9159
as possible,
but in any
event within 14 days.
9160
9161
13)
Nitrate, non-chlorinated.
9162
9163
A)
Preservative: Concentrated
sulfuric
acid to pH less
than 2.
9164
9165
B)
Plastic or glass (hard
or soft).
9166
9167
C)
Holding time: Samples
must be
analyzed as soon after
collection
9168
as
possible,
but
in
any
event within
14 days.
9169
9170
14)
Nitrite.
9171
9172
A)
Preservative:
Cool to
4°
C.
9173
9174
B)
Plastic
or glass (hard
or soft).
9175
9176
C)
Holding
time:
Samples must
be analyzed as soon
after collection
9177
as possible, but in
any
event within
48
hours.
9178
9179
15)
Selenium.
9180
JCAR35O61
1-0815204r01
9181
A)
Preservative:
Concentrated
nitric
acid to pH
less
than 2.
9182
9183
B)
Plastic
or glass
(hard or
soft).
9184
9185
C)
Holding
time:
Samples
must be analyzed
as
soon after collection
9186
as possible,
but in any
event within
six months.
9187
9188
16)
Thallium.
9189
9190
A)
Preservative:
Concentrated
nitric acid
to pH
less than
2.
9191
9192
B)
Plastic
or glass
(hard
or soft).
9193
9194
C)
Holding time:
Samples
must be
analyzed as
soon after
collection
9195
as
possible,
but in
any event
within
six
months.
9196
9197
c)
Analyses
under this
Subpart
N
must be
conducted
by
laboratories
that received
9198
approval
from
USEPA or
the Agency.
The Agency
must
certify laboratories
to
9199
conduct
analyses
for
antimony,
arsenic
(effective
January
23,
2006),
asbestos,
9200
barium,
beryllium,
cadmium,
chromium,
cyanide,
fluoride,
mercury,
nickel,
9201
nitrate,
nitrite,
selenium,
and
thallium
if the laboratory
does
as follows:
9202
9203
1)
It analyzes
performance
evaluation
(PE) samples,
provided
by
the
Agency
9204
pursuant
to 35
Ill.
Adm.
Code 186,
that include
those substances
at levels
9205
not
in excess
of levels
expected in
drinking
water; and
9206
9207
2)
It
achieves
quantitative
results on
the analyses
within the
following
9208
acceptance
limits:
9209
9210
A)
Antimony:
±
30%
at greater
than
or equal
to
0.006 mg!e.
9211
9212
B)
Arsenic: ±
30%
at greater
than
or equal
to
0.003 mg!e.
9213
9214
C)
Asbestos:
2
standard
deviations
based on
study
statistics.
9215
9216
D)
Barium: ±
15%
at greater
than or
equal to
0.15
mgfl.
9217
9218
E)
Beryllium:
± 15% at
greater than
or equal
to 0.001 mg/i.
9219
9220
F)
Cadmium:
± 20%
at
greater than
or equal
to
0.002 mg/2.
9221
9222
G)
Chromium:
± 15%
at greater
than or equal
to 0.01
mg!2.
9223
JCAR35O61
1-0815204r01
9224
H)
Cyanide:
± 25%
at
greater
than or equal to
0.1 mg!.
9225
9226
I)
Fluoride:
± 10% at 1 to 10
mg!e.
9227
9228
J)
Mercury:
± 30% at greater
than
or equal
to 0.0005 mg!E.
9229
9230
K)
Nickel:
± 15% at greater
than or equal
to
0.01 mg/t
9231
9232
L)
Nitrate:
±
10% at
greater than or equal
to
0.4
mg/i.
9233
9234
M)
Nitrite:
± 15% at
greater than or equal
to
0.4
mg/i.
9235
9236
N)
Selenium:
± 20%
at greater than or equal
to
0.01 mg/e.
9237
9238
0)
Thallium:
± 30% at
greater than or equal
to 0.002 mg!8.
9239
9240
BOARD NOTE: Derived
from 40
CFR 141.23(k) (2007)
and appendix
A to 40
CFR
141,
as
9241
added at 73 Fed. Reg.
31616
(June
3. 2008)(2003).
9242
9243
(Source:
Amended at 33 Ill. Reg.
effective
9244
9245
Section
611.612
Monitoring
Requirements
for
Old Inorganic
MCLs
9246
9247
a)
Analyses for the
purpose
of
determining compliance
with the old
inorganic
9248
MCLs of Section
611.300 are
required as follows:
9249
9250
1)
Analyses
for all
CWSs utilizing surface
water
sources
must be repeated
at
9251
yearly intervals.
9252
9253
2)
Analyses
for
all CWSs
utilizing
only
groundwater sources
must be
9254
repeated
at three-year intervals.
9255
9256
3)
This
subsection (a)(3) corresponds
with
40 CFR 141.23(1)(3),
which
9257
requires
monitoring
for
the repealed old
MCL for nitrate
at a frequency
9258
specified
by the state. The
Board
has followed
the USEPA
lead and
9259
repealed
that old MCL.
This statement maintains
structural
consistency
9260
with
USEPA rules.
9261
9262
4)
This
subsection (a)(4)
corresponds with
40
CFR 141.23(1)(4)
,which
9263
authorizes the state to
determine
compliance
and
initiate enforcement
9264
action.
This
statement
maintains
structural consistency
with
USEPA
9265
rules.
9266
JCAR35O61
1-0815204r01
9267
b)
If the result
of an analysis
made under subsection
(a) of
this Section indicates
that
9268
the level of
any contaminant
listed
in
Section 611.300 exceeds
the old MCL,
the
9269
supplier
must report
to the Agency within
seven days
and initiate three
additional
9270
analyses
at the same
sampling point within
one
month.
9271
9272
c)
When
the average
of four analyses
made pursuant
to subsection
(b) of this
9273
Section, rounded to
the same number
of significant
figures as the old
MCL for the
9274
substance in question,
exceeds
the old MCL, the supplier
must
notify the Agency
9275
and give notice to
the public pursuant
to Subpart
V of this Part.
Monitoring after
9276
public notification
must be at
a frequency designated
by the Agency
by
a SEP
9277
granted pursuant to
Section 611.110
and
must
continue until the
old MCL has not
9278
been exceeded
in two successive
samples or until
a different
monitoring
schedule
9279
becomes effective
as a condition
to a variance,
an adjusted standard,
a site
9280
specific
rule,
an
enforcement action,
or another SEP
granted
pursuant
to Section
9281
611.110.
9282
9283
d)
This subsection (d)
corresponds
with
40 CFR 141.23(o),
which pertains
to
9284
monitoring
for
the
repealed old MCL
for nitrate.
This statement
maintains
9285
structural consistency
with
USEPA
rules.
9286
9287
e)
This subsection (e)
corresponds with
40
CFR
141
.23Q), which pertains
to the use
9288
of existing data
up
until a date
long since expired.
This statement
maintains
9289
structural consistency
with
USEPA rules.
9290
9291
f)
Except
for
arsenic,
for which
analyses
must be made in accordance
with
Section
9292
611.611,
analyses
conducted
to determine
compliance
with the old MCLs
of
9293
Section
611.300 must be
made in accordance
with the following
methods,
9294
incorporated
by
reference
in Section 611.102,
or
alternative
methods approved
by
9295
the
Agency
pursuant to Section
611.480.
9296
9297
1)
Fluoride:
The methods
specified in
Section 611.611(c)
must
apply
for the
9298
purposes of this Section.
9299
9300
2)
Iron.
9301
9302
A)
Standard Methods.
9303
9304
i)
Method
3111 B,
18tlor19th,or21sted.;
9305
9306
ii)
Method 3113 B,
18
th,
19
th
or
21st
ed.;
9307
9308
iii)
Method 3120
B,
l8tI,
19
th
20
th
or
21st
ed.
9309
JCAR35O61
1-0815204r01
9310
BOARD
NOTE:
On March
12, 2007
(at
72 Fed.
Reg. 11200),
9311
USEPA
amended
the
entries
for iron
in the
table
at 40 CFR
9312
143.4(b)
to
allow
the use
of Standard
Methods
Online
(at
9313
www.standardmethods.org),
Method
3111 B, Method
3113
B,
and
9314
Method
3120
B (as approved
in 1999).
The Board
has instead
9315
cited
to the
21
st
edition
of Standard
Methods
for
the Examination
9316
of
Water
and
Wastewater
(the
printed
version
of Standard
9317
Methods),
since the versions
of
Method 3111,
Method
3113,
and
9318
Method
3120 that
appear
in that
printed
volume
are those
cited
by
9319
USEPA as
acceptable
for use.
USEPA
later
added Method
3111
9320
B,
Method
3113 B,
and
Method
3120 B
from
the
21
st
edition of
9321
Standard Methods
as
approved alternative
methods in
appendix
A
9322
to
subpart
C,
added on
June 3,2008
(at
73
Fed.
Reg.
31616).
9323
9324
B)
USEPA
Environmental
Metals Methods.
9325
9326
i)
Method
200.7; or
9327
9328
ii)
Method
200.9.
9329
9330
)
Axially
viewed
inductively-coupled
plasma
—
atomic
emission
9331
spectrometry
(AVICP-AES):
USEPA
Methods:
Method
200.5.
9332
9333
BOARD
NOTE:
USEPA added
this method
as an
approved
9334
alternative
method
in
appendix
A to
subpart C
of
40
CFR
141,
9335
added
on June 3,2008
(at 73
Fed.
Reg.
31616).
9336
9337
3)
Manganese.
9338
9339
A)
Standard
Methods.
9340
9341
i)
Method3lll
B,
18
t
of19
t
,or215ted.;
9342
9343
ii)
Method
3113
B,
18
th
19
th
or21
t
ed.; or
9344
9345
iii)
Method
3120
B,
l8tI,
19
th 020
th
or
21st
ed.
9346
9347
BOARD
NOTE:
On March
12, 2007
(at
72 Fed.
Reg. 11200),
9348
USEPA
amended
the
entries
for manganese
in the
table at
40 CFR
9349
143
.4(b) to
allow
the use
of Standard
Methods
Online
(at
9350
www.standardmethods.org),
Method
3111
B,
Method
3113
B,
and
9351
Method
3120
B
(as
approved
in 1999).
The
Board
has instead
9352
cited to the
21
5t
edition
of Standard
Methods
for the Examination
JCAR35O61 1-0815204r01
9353
of Water
and
Wastewater
(the
printed version
of Standard
9354
Methods),
since the versions
of Method
31 11, Method
3113, and
9355
Method
3120
that
appear in that
printed
volume
are those
cited
by
9356
USEPA
as acceptable
for use. USEPA
later
added
Method 3111
9357
B,
Method 3113 B,
and Method3l2OB
from the
21st
edition
of
9358
Standard
Methods
as approved
alternative methods
in appendix
A
9359
to subpart
C,
added
on June 3,
2008
(at
73
Fed.
Reg. 31616).
9360
9361
B)
USEPA
Environmental
Metals
Methods.
9362
9363
i)
Method
200.7;
9364
9365
ii)
Method
200.8; or
9366
9367
iii)
Method 200.9.
9368
9369
Axially viewed inductively-coupled
plasma — atomic
emission
9370
spectrometry
(AVICP-AES): USEPA
Methods:
Method 200.5.
9371
9372
BOARD NOTE:
USEPA
added this method as
an approved
9373
alternative
method in appendix
A to
subpart
C
of 40 CFR 141,
9374
added on
June 3,2008
(at
73 Fed. Reg.
31616).
9375
9376
4)
Zinc.
9377
9378
A)
Standard
Methods.
9379
9380
i)
Method
3111
B,
18tef19th,or215ted.;or
9381
9382
ii)
Method 3120
B,
th
18 19
th
e20th
or
21
st
ed.
9383
9384
BOARD
NOTE: On
March
12,
2007
(at
72 Fed. Reg. 11200),
9385
USEPA
amended the entries
for zinc in
the table at 40 CFR
9386
143.4(b)
to allow the use
of Standard Methods
Online
(at
9387
www.standardmethods.org),
Method 3111 B
and Method
3120 B
9388
(as
approved
in 1999). The
Board
has instead
cited to the
21
st
9389
edition
of Standard Methods
for the Examination
of Water
and
9390
Wastewater
(the
printed
version of Standard
Methods),
since the
9391
versions
of Method 3111
and Method
3120 that appear in
that
9392
printed
volume
are
those cited
by
USEPA as acceptable
for use.
9393
USEPA
later
added Method 3111 B,
Method
3113
B, and Method
9394
3120
B fromthe
21
st
edition of
Standard Methods
as
approved
JCAR35O61 1-0815204r01
9395
alternative
methods in
appendix A to subpart
C, added
on June
3,
9396
2008
(at
73 Fed. Reg.
31616).
9397
9398
B)
USEPA Environmental
Metals Methods.
9399
9400
i)
Method
200.7; or
9401
9402
ii)
Method
200.8.
9403
9404
)
Axially
viewed
inductively-coupled
plasma — atomic
emission
9405
spectrometry
(AVICP-AES):
USEPA
Methods:
Method 200.5.
9406
9407
BOARD NOTE:
USEPA added
this method
as an approved
9408
alternative
method
in appendix
A to subpart
C
of
40 CFR 141,
9409
added on June 3, 2008
(at
73 Fed.
Reg. 31616).
9410
9411
BOARD NOTE:
The provisions
of subsections
(a) through
(f)
of this Section derive
from 40
9412
CFR 141.23(1)
through
(p)
(2007)(2002).
Subsections (f)(2) through
(0(4)
of
this Section
relate
9413
exclusively to
additional State
requirements. The
Board
retained
subsection
(0
of this Section
to
9414
set forth
methods for the inorganic
contaminants
for which
there is a State-only
MCL.
The
9415
methods
specified are those
set forth in 40
CFR
143
.4(b) (2007)
and appendix
A to 40 CFR
141,
9416
as added at 73 Fed. Reg.
31616 (June 3, 2008)(2002),
for
secondary
MCLs.
9417
9418
(Source: Amended
at 33 Ill.
Reg.
effective
9419
9420
SUBPART 0:
ORGANIC MONITORING
AND
ANALYTICAL
REQUIREMENTS
9421
9422
Section
611.645
Analytical
Methods for Organic
Chemical
Contaminants
9423
9424
Analysis forthe Section
611.311(a)
VOCs under Section
611.646; the
Section
611.311(c)
SOCs
9425
under Section 611.648;
the Section 611.310
old
MCLs
under Section
611.641; and for THMs,
9426
TTHMs, and TTHM potential
must
be conducted using the
methods listed
in this Section
or
by
9427
alternativeequivalent
methods as approved
by the
Agency
pursuant to Section
611.480.
All
9428
methods are from USEPA
Organic Methods,
unless otherwise
indicated.
All methods are
9429
incorporated
by
reference
in Section 611.102.
Other required
analytical test
procedures
germane
9430
to
the conduct of these
analyses are contained
in the USEPA
document,
“Technical
Notes of
9431
Drinking
Water
Methods,”
incorporated
by reference
in Section 611.102.
9432
9433
Volatile Organic Chemical
Contaminants
(VOCs).
9434
Contaminant
Analytical
Methods
Benzene
502.2, 524.2
Carbon
tetrachloride
502.2, 524.2,
551.1
JCAR35O61
1-0815204r01
Chlorobenzene
502.2,
524.2
1,2-Dichlorobenzene
502.2, 524.2
1,4-Dichlorobenzene
502.2, 524.2
1 ,2-Dichloroethane
502.2, 524.2
cis-Dichloroethylene
502.2, 524.2
trans-Dichioroethylene
502.2,
524.2
Dichioromethane
502.2,
524.2
1,2-Dichioropropane
502.2,
524.2
Ethylbenzene
502.2, 524.2
Styrene
502.2,
524.2
Tetrachioroethylene
502.2, 524.2, 551.1
1,1,1-Trichioroethane
502.2,
524.2,
551.1
Trichioroethylene
502.2,
524.2, 551.1
Toluene
502.2,
524.2
1
,2,4-Trichlorobenzene
502.2, 524.2
1,1 -Dichioroethylene
502.2,
524.2
1,1,2-Trichioroethane
502.2, 524.2
Vinyl chloride
502.2,
524.2
Xylenes
(total)
502.2, 524.2
9435
9436
Synthetic Organic Chemical
Contaminants
(SOCs).
9437
Contaminant
Analytical
Methods
2,3,7,8-Tetrachlorodibenzodioxin
(2,3,7,8-TCDD
or
Dioxin and
Furan Method
dioxin)
1613
2,4-D
515.2,
555,
515.1, 515.3,
OGWDW Methods,
Method
515.4, ASTM
Method D5317-93or
D5317-98
2,4,5-TP
(Silvex)
515.2, 555, 515.1,
515.3,
OGWDW
Methods,
Method 515.4,
ASTM
Method D5317-93or
D5317-98
Alachior
505*1,
507,
508.1, 525.2,
551.1
Atrazine
505*!,
507,
508.1, 525.2,
551.1, Syngenta
AG-625
Benzo(a)pyrene
525.2, 550,
550.1
JCAR35O61 1-0815204r01
Carbofuran
531.1, OGWDW
Methods,
Method 531.2,
Standard
Methods,
18
th
ed.
Supplement,
19
th
ed.,
or
20
th
ed.: Method 6610
or
Standard
Methods
21st
ed.
or Standard Methods
Online:
Method
6610 B
Chiordane
505, 508, 508.1, 525.2
Dalapon
515.1, 552.1, 552.2,
515.3,
OGWDW Methods,
Method 515.4, OGWDW
Methods, Method 552.3
Di(2-ethylhexyl)adipate
506,
525.2
Di(2-ethylhexyl)phthalate
506, 525.2
Dibromochloropropane
(DBCP)
504.1,
551.1
Dinoseb
515.1,
515.2, 515.3,
OGWDW
Methods,
Method 515.4, 555
Diquat
549.1
Endothall
548.1
Endrin
505, 508, 508.1,
525.2,
551.1
Ethylene Dibromide
(EDB)
504.1,
551.1
Glyphosate
547, Standard
Methods,
l8” ed.,
l9 ed., or2O’
ed.: Method
6651
Heptachlor
505, 508,
508.1, 525.2,
551.1
Heptachlor
Epoxide
505, 508,
508.1, 525.2,
551.1
Hexachlorobenzene
505,
508,
508.1, 525.2,
551.1
Hexachiorocyclopentadiene
505, 508,
508.1,
525.2,
551.1
Lindane
505, 508,
508.1, 525.2,
551.1
Methoxychior
505, 508,
508.1, 525.2,
551.1
JCAR35O61
1-0815204r01
Oxamyl
531.1,
OGWDW
Methods, Method
531.2,
Standard
Methods,
18
th
ed.
Supplement,
19
th
ed., or
20t1
ed.:
Method
6610
or
Standard
Methods
21st
ed.
or
Standard Methods
Online:
Method
6610 B
PCBs
(measured
for compliance purposes
as
508A
decchlorobiphenyl)
PCBs
(qualitatively
identified as Aroclors)
505, 508, 508.1, 525.2
Pentachlorophenol
515.1,
515.2, 525.2,
555,
515.3,
OGWDW
Methods,
Method 515.4,
ASTM
Method
D5317-93
or D53
17-98(2003)
Picloram
515.1, 515.2,
555,
515.3,
OGWDW
Methods,
Method
515.4,
ASTM
Method
D5317-93
or
D53
17-98(2003)
Simazine
505*1,
507, 508.1,
525.2,
551.2
Toxaphene
505, 508, 525.2,
508.1
9438
9439
Total Trihalomethanes
(TTHMs).
9440
Contaminant
Analytical
Methods
Total
Trihalomethanes (TTHMs),
Trihalomethanes
502.2, 524.2,
551.1
(THMs), and
Maximum
Total Trihalomethane
Potential
9441
9442
State-Only MCLs
(for which a method
is not listed above).
9443
Contaminant
Analytical Methods
Aldrin
505,
508, 508.1,
525.2
DDT
505, 508
Dieldrin
505,
508, 508.1,
525.2
9444
9445
that,
for the particular contaminant,
a
nitrogen-phosphorus
detector should
be
9446
substituted
for the electron capture
detector in
method 505 (or
another
approved
method
9447
should
be used)
to determine
alachlor, atrazine,
and
simazine
if lower detection
limits are
9448
required.
9449
JCAR35O61 1-0815204r01
9450
denotes that
Syngenta Method
AG-625 may not
be
used for
the analysis
of
atrazine
in any
9451
system
where chlorine dioxide
is
used for
drinking water treatment.
In samples
from all
other
9452
systems,
any result for
atrazine generated
by Syngenta Method
AG—625
that is greater than
9453
one-half
the maximum contaminant
level
(MCL)
(in
other
words, greater than
0.001
5mg/C
or
9454
1.5
tgfC)
must be confirmed
using
another
approved method
for this contaminant
and should
9455
use additional volume
of the original sample
collected
for compliance
monitoring. In
9456
instances
where
a result from Syngenta
Method
AG-625
triggers such confirmatory
testing,
9457
the confirmatory result
is to be
used
to determine compliance.
9458
9459
BOARD NOTE: Derived
from
40
CFR 141.24(e) (2007)
and appendix
A to 40 CFR 141,
as
9460
added at 73 Fed.
Reg.
31616 (June 3, 2008)(2005).
9461
9462
(Source:
Amended at 33 Ill. Reg.
effective
9463
9464
SUBPART
Q: RADIOLOGICAL
MONITORING
AND
ANALYTICAL
REQUIREMENTS
9465
9466
Section
611.720
Analytical Methods
9467
9468
a)
The
methods specified below,
or alternative
methods approved
by
the Agency
9469
pursuant
to Section 611.480,
incorporated
by
reference
in Section 611.102, are
to
9470
be
used to determine compliance
with
Section 611.330, except
in cases where
9471
alternative methods
have been approved
in accordance
with Section 611.480.
9472
9473
1)
Gross Alpha
and Beta.
9474
9475
A)
Standard Methods.
9476
9477
i)
Method 302,
13
th
ed.; or
9478
9479
ii)
Method 7110
B,
th,
17 18
th 19
th
820
th
or
21
st
ed.;
9480
9481
BOARD NOTE:
On March 12,
2007
(at
72 Fed.
Reg.
9482
11200),
USEPA
amended the
entry for gross alpha
and beta
9483
by evaporation
in the table at
corresponding 40
CFR
9484
141.25(a)
to allow
the use of
Standard Methods Online
(at
9485
www.standardmethods.org),
Method 7110 B
(as
approved
9486
in
2000).
The
Board has instead
cited to the
21
St
edition of
9487
Standard Methods
for
the
Examination of Water
and
9488
Wastewater
(the printed
version
of Standard
Methods),
9489
since the version
of Method
7110 that appears
in that
9490
printed
volume
is that
cited by USEPA as
acceptable
for
9491
use.
USEPA later added
Method 7110
B from the
21
st
9492
edition
of Standard
Methods as an approved
alternative
JCAR35O61
1-0815204r01
9493
method
in
appendix
A to
subpart
C,
added on
June 3, 2008
9494
(at
73
Fed. Reg.
31616).
9495
9496
B)
USEPA
Interim
Radiochemical
Methods:
page
1;
9497
9498
C)
USEPA
Radioactivity
Methods:
Method
900.0;
9499
9500
D)
USEPA
Radiochemical
Analyses:
page
1;
9501
9502
E)
USEPA
Radiochemistry
Methods:
Method
00-01;
or
9503
9504
F)
USGS
Methods:
Method
R-1 120-76.
9505
9506
2)
Gross
Alpha.
9507
9508
A)
Standard
Methods,
18t1I,
19
th
20
th
or
21st
ed.: Method
7110
C;
9509
or
9510
9511
BOARD
NOTE:
On March
12. 2007
(at
72 Fed.
Reg.
11200),
9512
USEPA
amended
the
entry
for gross
alpha by
coprecipitation
in the
9513
table
at corresponding
40 CFR
141.25(a)
to
allow
the use of
9514
Standard
Methods
Online
(at
www.standardmethods.org),
Method
9515
7110
C
(as
approved
in
2000).
The
Board has
instead cited
to
the
9516
21
St
edition
of Standard
Methods
for the
Examination
of Water and
9517
Wastewater
(the
printed
version
of Standard
Methods),
since
the
9518
version
of
Method 7110
that appears
in that
printed
volume
is
that
9519
cited
by
USEPA
as
acceptable
for use. USEPA
later
added
9520
Method 7110
C
from
the
21st
edition
of Standard
Methods
as
an
9521
approved
alternative
method
in
appendix
A
to
subpart
C, added
on
9522
June 3, 2008
(at 73 Fed.
Reg.
31616).
9523
9524
B)
USEPA Radiochemistry
Methods:
Method
00-02.
9525
9526
3)
Radium-226.
9527
9528
A)
ASTM Methods.
9529
9530
i)
Method
D2460-97D2460
90; or
9531
9532
ii)
Method D3454-97;
9533
9534
B)
New
York
Radium
Method;
9535
JCAR35O61
1-0815204r01
9536
C)
Standard
Methods.
9537
9538
i)
Method3o4,l3thed.;
9539
9540
ii)
Method
305,
13
th
ed.;
9541
9542
iii)
Method
7500-Ra
B,
17
th
18
th
19
th
020
th
or
21st
ed.;
or
9543
9544
iv)
Method
7500-Ra
C,
l7t,
18
th
19
th
20
th
or
21st
ed.;
9545
9546
BOARD
NOTE:
On
March
12,
2007
(at
72 Fed.
Reg.
11200),
9547
USEPA
amended
the
entries
for radium-226
in the
table
at
9548
corresponding
40 CFR
141.25(a)
to
allow
the
use of
Standard
9549
Methods
Online
(at
www.standardmethods.org),
Method
7500-Ra
9550
B and
C
(as
approved
in
2000).
The
Board
has
instead
cited
to the
9551
21
5t
edition
of
Standard
Methods
for
the
Examination
of
Water
and
9552
Wastewater
(the
printed
version
of
Standard
Methods), since
the
9553
version
of Method
7500-Ra
that
appears
in that
printed
volume
is
9554
that
cited
by
USEPA
as
acceptable
for
use. USEPA
later
added
9555
Method
7500-Ra
B and
C
from
the
21st
edition
of Standard
9556
Methods
as an
approved
alternative
method
in
appendix
A to
9557
subpart
C, added
on
June
3,2008
(at
73
Fed.
Reg. 31616).
9558
9559
D)
USDOE
Manual:
Method
Ra-04;
9560
9561
E)
USEPA
Interim
Radiochemical
Methods:
pages
13 and
16;
9562
9563
F)
USEPA
Radioactivity Methods:
Methods
903.0,
903.1;
9564
9565
G)
USEPA
Radiochemical
Analyses:
page
19;
9566
9567
H)
USEPA
Radiochemistry
Methods:
Methods
Ra-03,
Ra-04;
or
9568
9569
I)
USGS
Methods.
9570
9571
i)
MethodR-1140-76;or
9572
9573
ii)
MethodR-1141-76.
9574
9575
Georgia
Radium
Method.
9576
9577
4)
Radium-228.
9578
JCAR35061
1-0815204r01
9579
A)
Standard
Methods,
17t1,
18
th
19
th
20
th
or
21st
ed.:
Method
9580
7500-RaD;
9581
9582
BOARD
NOTE:
On
March
12, 2007
(at
72 Fed.
Reg.
11200),
9583
USEPA
amended
the
entry
for
radium-228
by
radiochemical
in the
9584
table
at
corresponding
40 CFR
141.25(a)
to
allow the
use
of
9585
Standard
Methods
Online
(at
www.standardmethods.org),
Method
9586
7500-Ra
D
(as
approved
in 2000).
The
Board
has
instead
cited to
9587
the
2151
edition
of Standard
Methods
for the
Examination
of
Water
9588
and
Wastewater
(the
printed
version
of
Standard
Methods),
since
9589
the version
of
Method
7500-Ra
that
appears
in that
printed
volume
9590
is
that cited
by USEPA
as
acceptable
for use.
USEPA
later
added
9591
Method
7500-Ra
D
from the
21st
edition
of
Standard
Methods
as
9592
an
approved
alternative
method
in appendix
A to subpart
C,
added
9593
on June
3,2008
(at
73
Fed.
Reg.
31616).
9594
9595
B)
New York
Radium
Method;
9596
9597
C)
USEPA
Interim
Radiochemical Methods:
page
24;
9598
9599
D)
USEPA
Radioactivity
Methods:
Method
904.0;
9600
9601
E)
USEPA
Radiochemical
Analyses:
page
19;
9602
9603
F)
USEPA
Radiochemistry
Methods:
Method
Ra-05;
9604
9605
G)
USGS Methods: Method
R-1142-76;er
9606
9607
H)
New
Jersey
Radium
Methodp
9608
9609
Georgia
Radium
Method.
9610
9611
5)
Uranium.
9612
9613
A)
Standard
Methods,
17
th,
l8tT,
19
th,
20
th
or
21St
ed.:
Method
9614
7500-U
C;
9615
9616
BOARD
NOTE:
On
March
12,
2007
(at
72 Fed.
Reg.
11200),
9617
USEPA
amended
the
entries
for
uranium
by radiochemical
and
9618
alpha
spectrometry
in
the
table
at corresponding
40 CFR
141.25(a)
9619
to
allow
the use
of
Standard
Methods
Online
(at
9620
www.standardmethods.org),
Method
7500-U
C
(as approved
in
9621
2000).
The
Board
has
instead
cited
to
the
21St
edition
of
Standard
JCAR35O61
1-0815204r01
9622
Methods
for
the Examination
of
Water
and Wastewater
(the
9623
printed
version of Standard
Methods),
since
the
version
of Method
9624
7500-U that
appears in
that printed
volume is that cited
by USEPA
9625
as acceptable
for
use. USEPA later
added Method 7500-U
B
from
9626
the
21
st
edition of Standard
Methods
as an
approved
alternative
9627
method
in appendix
A to subpart
C,
added on June
3,
2008
(at
73
9628
Fed. Reg. 31616).
9629
9630
B)
Standard
Methods,
20th ed.:
Method 3125;
9631
9632
C)
ASTM
Methods.
9633
9634
i)
Method
D2907-97;
9635
9636
ii)
Method D3972-97
or D3972-02;
9637
9638
iii)
Method D5174-97
or D5174-02;
or
9639
9640
iv)
Method
D5673-03 or Method
5673-05;
9641
9642
BOARD
NOTE:
USEPA added
this method as
an approved
9643
alternative method
in appendix
A
to subpart
C
of 40 CFR 141,
9644
added on June
3, 2008
(at
73 Fed. Reg. 31616).
9645
9646
D)
USEPA
Radioactivity Methods:
Methods
908.0, 908.1;
9647
9648
E)
USEPA
Environmental Metals
Methods:
Method 200.8;
9649
9650
F)
USEPA
Radiochemical Analyses:
page
33;
9651
9652
G)
USEPA
Radiochemistry Methods:
Method
00-07;
9653
9654
H)
USDOE Manual:
Method
U-02 or
U-04;
or
9655
9656
I)
USGS
Methods.
9657
9658
i)
MethodR-1180-76;
9659
9660
ii)
MethodR-1181-76;or
9661
9662
iii)
Method
R-1182-76.
9663
JCAR35O61
1-0815204r01
9664
BOARD
NOTE:
If
uranium
(U) is determined
by
mass, a conversion
9665
factor
of 0.67 pCi/jig
of
uranium
must
be used.
This
conversion
factor
is
9666
based on
the 1:1
activity
ratio
of
234
U
and
238
U
that
is characteristic
of
9667
naturally
occurring
uranium.
9668
9669
6)
Radioactive
Cesium.
9670
9671
A)
ASTM
Methods.
9672
9673
i)
Method
D2459-72;
or
9674
9675
ii)
Method
D3649-91
or D3649-98a;
9676
9677
B)
Standard
Methods.
9678
9679
i)
Method 7120,
l9t1
20
th
or
21st
ed.;
or
9680
9681
ii)
Method
7500-Cs
B,
17th,
18
th
19
th
20
th
or
21st
ed.;
9682
9683
BOARD
NOTE:
On March
12, 2007
(at 72 Fed.
Reg. 11200),
9684
USEPA
amended
the entries
for
radioactive
cesium
in
the table
at
9685
corresponding
40 CFR
141.25(a)
to allow
the
use
of
Standard
9686
Methods Online
(at www.standardmethods.org),
Method
7120
(as
9687
approved
in
1997)
and Method
7500-Cs
B (as approved
in 2000).
9688
The Board
has
instead
cited
to the
21
st
edition of
Standard Methods
9689
for the Examination
of Water
and
Wastewater
(the
printed
version
9690
of
Standard
Methods),
since
the versions
of Method
7120 and
9691
Method
7500-Cs
that
appear in
that printed
volume
are
those
cited
9692
by USEPA
as
acceptable
for
use. USEPA
later added
Method
9693
7120 and
Method
7500-Cs
B
from
the
21st
edition of
Standard
9694
Methods
as an
approved
alternative
method
in
appendix
A to
9695
subpart
C,
added on
June 3, 2008
(at
73
Fed.
Reg. 31616).
9696
9697
C)
USDOE
Manual:
Method
4.5.2.3;
9698
9699
D)
USEPA
Interim
Radiochemical
Methods:
page
4;
9700
9701
E)
USEPA
Radioactivity
Methods:
Methods
901.0, 901.1;
9702
9703
F)
USEPA
Radiochemical
Analyses:
page
92; or
9704
9705
G)
USGS
Methods.
9706
9707
i)
Method
R-1110-76;
or
JCAR35O61
1-0815204r01
9708
9709
ii)
MethodR-1111-76.
9710
9711
7)
Radioactive
Iodine.
9712
9713
A)
ASTM
Methods.
9714
9715
i)
D3649-91
orD3649-98a;
or
9716
9717
ii)
D4785-93orD4785-98;
9718
9719
B)
Standard
Methods.
9720
9721
i)
Method
7120,
19
th
20
th
or
21st
ed.;
9722
9723
ii)
Method
7500-I
B,
l7t,
18
th
19
th
820
th
or
21
st
ed.;
9724
9725
iii)
Method
7500-I
C,
17t,
18
th
19
th
e20th
or
21st
ed.;
or
9726
9727
iv)
Method
7500-I
D,
17
th,
18
th
19
th
20
th
or
21st
ed.;
9728
9729
BOARD
NOTE:
On
March
12,
2007 (at
72 Fed.
Reg.
11200),
9730
USEPA
amended
the
entries
for
radioactive
iodine
in
the
table
at
9731
corresponding 40
CFR
141.25(a)
to
allow
the
use of
Standard
9732
Methods
Online
(at
www.standardmethods.org),
Method
7120
(as
9733
approved
in
1997)
and
Method
7500-I
B,
C,
and D
(as
approved
in
9734
2000).
The Board
has
instead
cited
to
the
21
st
edition
of Standard
9735
Methods
for
the
Examination
of Water
and
Wastewater
(the
9736
printed
version
of
Standard
Methods),
since the
versions
of
9737
Method
7120
and
Method
7500-I
that
appear
in that
printed
9738
volume
are those
cited
by USEPA
as
acceptable
for use.
USEPA
9739
later
added
Method
7500-I
B,
C,
and
D
from the
21
st
edition
of
9740
Standard
Methods
as
an
approved
alternative
method
in
appendix
9741
A to
subpart
C,
added
on June
3, 2008
(at
73 Fed.
Reg.
31616).
9742
9743
C)
USDOE
Manual:
Method
4.5.2.3;
9744
9745
D)
USEPA
Interim
Radiochemical
Methods:
pages
6,
9;
9746
9747
E)
USEPA
Radiochemical
Analyses:
page
92;
or
9748
9749
F)
USEPA
Radioactivity
Methods:
Methods
901.1,
902.0.
9750
JCAR35O61 1-0815204r01
9751
8)
Radioactive
Strontium-89
& 90.
9752
9753
A)
Standard Methods.
9754
9755
i)
Method
303,
13
th
ed.; or
9756
9757
ii)
Method 7500-Sr
B,
th
17 1
gth 19
th 20
th
or
21
st
ed.;
9758
9759
BOARD
NOTE: On March 12, 2007
(at
72
Fed. Reg.
9760
11200),
USEPA amended
the entry for radioactive
9761
strontium
in the table at corresponding 40
CFR 141.25(a)
to
9762
allow the use of Standard
Methods Online (at
9763
www.standardmethods.org).
Method
7500-Sr B (as
9764
approved
in 2001). The Board
has instead cited to the
21st
9765
edition of Standard
Methods for the Examination
of Water
9766
and Wastewater
(the
printed version
of Standard Methods),
9767
since the version
of Method 7500-Sr that appears
in that
9768
printed volume
is that cited
by USEPA as acceptable
for
9769
use. USEPA later
added Method 7500-Sr B from
the
21
st
9770
edition
of Standard Methods
as an approved alternative
9771
method in
appendix A to subpart
C, added on June 3, 2008
9772
(at 73 Fed. Reg.
31616).
9773
9774
B)
USDOE
Manual.
9775
9776
i)
Method Sr-01; or
9777
9778
ii)
Method Sr-02;
9779
9780
C)
USEPA Interim Radiochemical
Methods: page 29;
9781
9782
D)
USEPA Radioactivity
Methods:
Method 905.0;
9783
9784
E)
USEPA Radiochemical
Analyses:
page 65;
9785
9786
F)
USEPA Radiochemistry
Methods:
Method Sr-04; or
9787
9788
G)
USGS Methods: MethodR-1160-76.
9789
9790
9)
Tritium.
9791
9792
A)
ASTM
Methods: Method D4107-91
or D4107-98;
9793
JCAR35O61 1-0815204r01
9794
B)
Standard Methods.
9795
9796
i)
Method
306,
13
th
ed.; or
9797
9798
ii)
Method 7500-
3
H
B, l7,
18
th 19
th
20
th
or
21st
ed.;
9799
9800
BOARD
NOTE: On March 12, 2007
(at
72 Fed. Reg.
9801
11200).
USEPA amended the entry for
tritium in the table
9802
at corresponding 40 CFR 141.25(a)
to allow the use
of
9803
Standard
Methods Online
(at
www.standardmethods.org),
9804
Method 7500-
3
HB (as approved
in 2000). The Board
has
9805
instead cited
to the
21
st
edition of Standard
Methods for the
9806
Examination
of Water and Wastewater
(the
printed version
9807
of Standard Methods),
since the version of Method
7500-
9808
3
H that
appears in that printed volume
is that cited by
9809
USEPA as acceptable for
use. USEPA later added
Method
9810
7500-
3
H
B from the
21st
edition of
Standard Methods as an
9811
approved alternative method
in appendix A to subpart
C,
9812
added
on June 3,2008 (at 73 Fed.
Reg.
31616).
9813
9814
C)
USEPA Interim Radiochemical
Methods: page 34;
9815
9816
D)
USEPA Radioactivity
Methods: Method
906.0;
9817
9818
E)
USEPA Radiochemical Analyses:
page 87;
9819
9820
F)
USEPA Radiochemistry
Methods: Method H-02;
or
9821
9822
G)
USGS Methods: MethodR-1171-76.
9823
9824
10)
Gamma Emitters.
9825
9826
A)
ASTM Methods.
9827
9828
i)
Method
D3649-91 or D3649-98a;
or
9829
9830
ii)
Method D4785-93 or D4785-OOa;
9831
9832
B)
Standard
Methods.
9833
9834
i)
Method
7120,
19
th 20
th
or
21
st
ed.;
9835
9836
ii)
Method 7500-Cs B,
th
17
18
th 19
th
20
th
or
21
st
ed.; or
JCAR35O61 1-0815204r01
9837
9838
iii)
Method 7500-I B,
th
17 18
th 19
th
20
th
or
21
st
ed.;
9839
9840
BOARD NOTE: On
March
12, 2007
(at
72 Fed. Reg.
11200).
9841
USEPA amended the entries for gamma emitters in the
table at
9842
corresponding
40 CFR
141.25(a)
to allow the use of Standard
9843
Methods Online
(at
www.standardmethods.org), Method 7120
(as
9844
approved in
1997),
Method 7500-Cs
B
(as
approved in 2000),
and
9845
Method 7500-I B
(as
approved in
2000).
The Board has instead
9846
cited to the
21
St
edition
of
Standard
Methods for the Examination
9847
of Water and Wastewater
(the
printed version of Standard
9848
Methods),
since the versions of Method 7120,
Method 7500-Cs,
9849
and Method
7500-I that appear in that printed volume are those
9850
cited by USEPA as acceptable for use. USEPA later added
9851
Method 7150, Method
7500-Cs B, and Method 7500-I B from the
9852
21
St
edition of Standard Methods as an approved alternative
9853
method in appendix A to subpart
C, added on June 3,
2008
(at
73
9854
Fed.
Reg.
31616).
9855
9856
C)
USDOE Manual: Method Ga-01-R;
9857
9858
D)
USEPA
Radioactivity Methods: Methods 901.0, 901.1, or 902.0;
9859
9860
E)
USEPA Radiochemical Analyses: page 92; or
9861
9862
F)
USGS
Methods:
Method R-1 110-76.
9863
9864
b)
When the identification and
measurement of radionuclides other than those listed
9865
in subsection (a) of this Section are required, the following methods, incorporated
9866
by
reference in Section 611.102, are
to be used, except in cases where alternative
9867
methods
have been
approved in accordance with Section 611.480:
9868
9869
1)
Procedures for Radiochemical
Analysis of Nuclear Reactor Aqueous
9870
Solutions,’ available from NTIS.
9871
9872
2)
HASL Procedure Manual, HASL
300,
available
from
ERDA
Health and
9873
Safety Laboratory.
9874
9875
c)
For the purpose of monitoring radioactivity concentrations in drinking water,
the
9876
required sensitivity
of the radioanalysis is defined in terms of a detection limit.
9877
The detection limit must be that
concentration which can be counted with a
9878
precision ofplus or minus 100 percent
at
the
95 percent confidence level (1.96u,
9879
where u is
the standard
deviation of the net counting rate of the sample).
JCAR35O61 1-0815204r01
9880
9881
1)
To determine
compliance with Section
611.330(b), (c), and (e),
the
9882
detection limit must
not exceed the concentrations
set forth in the
9883
following
table:
9884
Contaminant
Detection Limit
Gross alpha particle
3 pCi/i
activity
Radium-226
1 pCi/2
Radium-228
1 pCi/i?
Uranium
1 jigfe
9885
9886
BOARD NOTE: Derived
from 40 CFR 141.25(c)
Table B_(2007)(2005).
9887
9888
2)
To
determine compliance
with Section 611.330(d), the
detection limits
9889
must not exceed
the concentrations listed in
the following table:
9890
Radionuclide
Detection Limit
Tritium
1,000
pCi/C
Strontium-89
10 pCi/C
Strontium-90
2
pCi/i?
Iodine-131
1 pCi/C
Cesium-134
10
pCi/C
Gross beta
4 pCi/C
Other radionuclides
1/10 of applicable
limit
9891
9892
BOARD
NOTE: Derived from 40
CFR 141.25(c) Table
C
(2007)(2005).
9893
9894
d)
To judge compliance with
the MCLs listed in
Section 611.330, averages
of data
9895
must be used and must be rounded
to the same number of significant
figures as
9896
the MCL for the substance
in question.
9897
9898
BOARD NOTE: Derived from 40 CFR 141.25 (2007)
and appendix A
to
40
CFR 141, as added
9899
at 73
Fed. Reg. 31616 (June 3, 2008)(2005).
9900
9901
(Source: Amended at 33 Ill. Reg.
effective
9902
9903
SUBPART S: GROUNDWATER
RULE
9904
9905
Section 611.801 Sanitary Surveys for GWS
Suppliers
9906
9907
a)
A
GWS
supplier
must provide the Agency,
at the Agency’s request, any existing
9908
information that will enable
the Agency to conduct
a sanitary survey.
JCAR35O61
1-0815204r01
9909
9910
b)
For the
purposes
of
this Subpart
5, a “sanitary survey,”
as conducted
by the
9911
Agency,
includes but
is not limited to,
an onsite
review
of the delineated
WHPAs
9912
(identifying sources
of contamination
within the WHPAs
and evaluations
ofor
the
9913
hydrogeologic
sensitivity of the
delineated WHPAs
conducted under
source water
9914
assessments or utilizing
other relevant
information
where available),
facilities,
9915
equipment, operation,
maintenance,
and monitoring
compliance
of a public
water
9916
system to evaluate
the adequacy
of the system,
its sources and
operations and the
9917
distribution of
safe
drinking
water.
9918
9919
c)
The
sanitary survey
must include
an evaluation
of the applicable
components
9920
listed in subsections
(c)(1) through
(c)(8) of this
Section:
9921
9922
1)
Source,
9923
9924
2)
Treatment,
9925
9926
3)
Distribution
system,
9927
9928
4)
Finished
water storage,
9929
9930
5)
Pumps,
pump
facilities,
and controls,
9931
9932
6)
Monitoring, reporting,
and data
verification,
9933
9934
7)
System management
and operation,
and
9935
9936
8)
Operator compliance
with Agency
requirements.
9937
9938
d)
The
Agency must repeat
the sanitary
survey as follows:
9939
9940
1)
The Agency must
conduct
a sanitary
survey that addresses
the eight
9941
sanitary survey
components listed
in subsection
(c) of this Section no
less
9942
frequently than every
three
years
for a
CWS
supplier,
except
as provided
9943
in subsection (d)(3)
of this Section,
and every
five
years for a non-CWS
9944
supplier. The Agency
may
conduct
more frequent sanitary
surveys
for any
9945
supplier. The
initial sanitary survey
for
each community
water system
9946
must be conducted
before December
31, 2012,
unless the supplier
meets
9947
the
requirements
of subsection
(d)(3) of this Section.
The initial
sanitary
9948
survey
for each
CWS supplier
that
meets the
requirements of subsection
9949
(d)(3) of this
Section
and
for each non-CWS
supplier must be
conducted
9950
before December
31, 2014.
The sanitary survey
must include
an
JCAR35O61
l-0815204r01
9951
evaluation
of each
of the elements
set forth
in
subsection
(c)
of this
9952
Section,
as applicable.
9953
9954
2)
The Agency
may
use a
phased
review
process to
meet
the
requirements
of
9955
subsection
(d)(1)
of this
Section
if all the
applicable
elements
of
9956
subsection
(c) of
this Section
are evaluated
within
the required
interval.
9957
9958
3)
The
Agency
may
conduct
sanitary
surveys once
every five
years for
9959
community
water
systems
under any
of the following
circumstances:
9960
9961
A)
If the
system
either
provides
at least
4-log
treatment
of viruses
9962
(using
inactivation,
removal,
or an
Agency-approved
combination
9963
of 4-log
inactivation
and removal)
before
or
at
the
first customer
9964
for all
its
groundwater
sources;
or
9965
9966
B)
If the supplier
has
an outstanding
performance
record,
as
9967
determined
by the
Agency
and
documented
in previous
sanitary
9968
surveys,
and
the
supplier
has
no history of
total coliforrn
MCL
or
9969
monitoring
violations
under
Sections
611.521
through
611.527
9970
since
the last
sanitary
survey.
9971
9972
4)
This subsection
(d)(4)
corresponds
with 40
CFR
142.16(o)(2)(iv),
which
9973
imposes
requirements
for
describing
the elements
of the
State’s
regulatory
9974
system.
This statement
maintains
structural
consistency
with the
9975
corresponding
federal
provision.
9976
9977
5)
The Agency
must
provide
a
GWS supplier
with
written
notice
by
a
SEP
9978
issued
pursuant to
Section 611.110
that
describes any
significant
9979
deficiency
which
it has
found no
later
than 30 days
after
the Agency
has
9980
identified
the significant
deficiency.
The
notice may
specify
corrective
9981
actions and
deadlines
for
completion
of corrective
actions.
The
Agency
9982
may
provide
the written
notice
at the time
of the
sanitary
survey.
9983
9984
BOARD NOTE:
Subsections
(a)
through
(c) are
derived
from
40 CFR
141.401 (2007)
9985
as added
at 71
Fed. Reg.
65574
ov.
8,
2006).
Subsection
(d) is derived
from
40
CFR
9986
142.16(o)(2)
(2007),
as added
at
71 Fed.
Reg. 65574
Nov.
8,
2006).
9987
9988
(Source:
Amended
at
33 Ill. Reg.
effective
9989
9990
Section 611.802
Groundwater
Source
Microbial
Monitoring
and
Analytical
Methods
9991
9992
a)
Triggered
source
water
monitoring.
9993
JCAR35O61 1-0815204r01
9994
1)
General requirements.
A
GWS
supplier must
conduct triggered source
9995
water monitoring
if the following
conditions exist:
9996
9997
A)
The supplier
does not provide at least 4-log treatment
of viruses
9998
(using inactivation,
removal, or an Agency-approved combination
9999
of
4-log virus inactivation
and removal) before or at the first
10000
customer
for each groundwater source; and
10001
10002
B)
The
supplier is notified that
a sample collected pursuant to
Section
10003
611.521 is
total coliform-positive, and the sample
is not
10004
invalidated
by the Agency pursuant
to Section 611.523.
10005
10006
2)
Sampling requirements.
A
GWS
supplier
must collect, within 24 hours
10007
after
notification of the total coliform-positive
sample, at least
one
10008
groundwater source
sample from each groundwater
source in use at the
10009
time the total
coliform-positive sample
was collected pursuant to Section
10010
611.521, except as
provided in subsection (a)(2)(B)
of this Section.
10011
10012
A)
The Agency
may, by a SEP issued pursuant
to Section 611.110,
10013
extend the 24-hour time
limit on a case-by-case basis if it
10014
determines
that the supplier cannot
collect the groundwater
source
10015
water sample
within 24 hours due
to circumstances beyond the
10016
supplier’s
control. In the case of an extension,
the Agency must
10017
specify how much time
the supplier has to collect the
sample.
10018
10019
B)
If approved
by the Agency, a supplier with
more than one
10020
groundwater source may
meet the requirements of this
subsection
10021
(a)(2)
by sampling a representative
groundwater source or sources.
10022
If directed by the Agency
by a SEP issued pursuant to Section
10023
611.110, the
supplier must submit for Agency
approval a triggered
10024
source
water monitoring plan
that identifies one or more
10025
groundwater sources
that are representative of each monitoring
site
10026
in the
system’s sample siting plan
pursuant to Section 611.521 and
10027
that the system intends
to use for representative sampling
pursuant
10028
to this subsection
(a).
10029
10030
C)
A
GWS supplier that serves 1,000
or fewer people may use a
10031
repeat sample
collected from a groundwater
source to meet both
10032
the requirements of Section
611.522 and to satisfy the monitoring
10033
requirements
of subsection (a)(2)
of this Section for that
10034
groundwater
source only if the Agency
approves the use of E. coli
10035
as a fecal indicator
for source water monitoring
pursuant to this
10036
subsection
(a) by a SEP issued
pursuant to Section 611.110. If
the
JCAR35O61
1-0815204r01
10037
repeat sample
collected
from the
groundwater
source
is E.coli
10038
positive,
the
system must
comply
with subsection
(a)(3)
of this
10039
Section.
10040
10041
3)
Additional
requirements.
If
the Agency
does
not
require
corrective
action
10042
pursuant
to Section
611
.803(a)(2)
for a fecal
indicator-positive
source
10043
water
sample
collected pursuant
to
subsection
(a)(2) of this
Section
that is
10044
not
invalidated
pursuant
to
subsection
(d) of
this Section,
the system
must
10045
collect
five additional
source
water
samples
from
the same
source
within
10046
24
hours after
being notified
of the
fecal indicator-positive
sample.
10047
10048
4)
Consecutive
and
wholesale
systems.
10049
10050
A)
In addition
to the
other
requirements
of this
subsection
(a),
a
10051
consecutive
GWS
supplier
that has a total
coliform-positive
sample
10052
collected
pursuant
to Section
611.521
must
notify the
wholesale
10053
systems
within
24
hours after
being notified
of the
total coliform
10054
positive
sample.
10055
10056
B)
In addition
to the
other
requirements
of this
subsection
(a),
a
10057
wholesale
GWS
supplier must
comply
with the following
10058
requirements:
10059
10060
i)
A
wholesale
GWS
supplier
that
receives
notice
from a
10061
consecutive
system
it
serves that
a
sample
collected
10062
pursuant
to Section
611.521
is
total
coliform-positive
must,
10063
within
24
hours
after being
notified,
collect
a sample from
10064
its
groundwater
sources
pursuant
to
subsection
(a)(2)
of this
10065
Section
and analyze
it
for a fecal
indicator
pursuant
to
10066
subsection
(c)
of this Section.
10067
10068
ii)
If the
sample
collected pursuant
to
subsection
(a)(4)(B)(i)
10069
of
this
section is
fecal indicator-positive,
the wholesale
10070
GWS
supplier
must notify
all
consecutive
systems
served
10071
by
that
groundwater
source
of the fecal
indicator
source
10072
water positive
within 24
hours of
being
notified
of the
10073
groundwater
source
sample
monitoring
result and
must
10074
meet
the requirements
of
subsection
(a)(3) of this
Section.
10075
10076
5)
Exceptions
to
the
triggered source
water
monitoring
requirements.
A
10077
GWS
supplier is
not required
to comply
with the
source water
monitoring
10078
requirements
of subsection
(a) of this
Section
if
either
of
the following
10079
conditions
exists:
JCAR35O61 1-0815204r01
10080
10081
A)
The Agency determines,
and
documents in writing,
by a SEP
10082
issued pursuant
to Section 611.110,
that the total coliform-positive
10083
sample collected
pursuant
to Section 6 11.521 is
caused by a
10084
distribution
system deficiency;
or
10085
10086
B)
The total
coliform-positive
sample collected
pursuant to
Section
10087
6 11.521
is collected at
a location that meets
Agency criteria for
10088
distribution
system conditions
that will cause
total coliform
10089
positive
samples.
10090
10091
b)
Assessment source
water monitoring.
If directed by the
Agency by a SEP issued
10092
pursuant
to Section 611.110,
a GWS
supplier must conduct
assessment
source
10093
water monitoring
that
meets Agency-determined
requirements
for such
10094
monitoring.
A
GWS
supplier
conducting
assessment source
water monitoring
10095
may use
a triggered
source water sample
collected pursuant
to subsection (a)(2)
of
10096
this
Section to meet the
requirements
of subsection (b) of this
Section. Agency-
10097
determined
assessment
source water monitoring
requirements
may include the
10098
following:
10099
10100
1)
Collection
of a total of 12 groundwater
source
samples that represent
each
10101
month the system
provides
groundwater to the
public;
10102
10103
2)
Collection
of samples from
each well,
unless the system obtains
written
10104
Agency
approval to conduct
monitoring at
one
or more
wells within the
10105
GWS
that are representative
of multiple
wells used
by
that system
and
10106
which
draw water from
the same hydrogeologic
setting;
10107
10108
3)
Collection of a standard
sample volume
of at least 100 me
for fecal
10109
indicator
analysis, regardless
of the fecal
indicator or analytical
method
10110
used;
10111
10112
4)
Analysis
of all
groundwater
source samples
using one
of
the
analytical
10113
methods
listed in subsection
(c)(2) of this
Section for the presence
of E.
10114
coli, enterococci,
or coliphage;
10115
10116
5)
Collection
of groundwater
source samples
at a location
prior
to any
10117
treatment
of the groundwater
source unless
the Agency approves
a
10118
sampling location after
treatment; and
10119
10120
6)
Collection of
groundwater source
samples at the well itself,
unless the
10121
system’s configuration
does not
allow for sampling
at the well itself
and
10122
the
Agency
approves an alternate
sampling
location
by a SEP issued
JCAR35O61 1-0815204r01
10123
pursuant to Section
611.110
that is
representative
of the water
quality
of
10124
that well.
10125
10126
c)
Analytical
methods.
10127
10128
1)
A
GWS
supplier
subject
to the
source
water monitoring
requirements
of
10129
subsection
(a)
of
this
Section must
collect a standard
sample volume
of at
10130
least
100 m for fecal
indicator
analysis,
regardless
of the fecal indicator
10131
or analytical
method
used.
10132
10133
2)
A
GWS
supplier
must analyze
all groundwater source
samples
collected
10134
pursuant
to subsection
(a) of this Section
using
one of the analytical
10135
methods
listed in
subsections (c)(2)(A)
through (c)(2)(C)
of this
Section
10 136
or alternative
methods
approved
by
the Agency pursuant
to Section
10137
611.480,
subject to
the limitations
of
subsection
(c)(2)(D)
of this Section,
10138
for the presence
of E.
coli, enterococci,
or coliphage:
10139
10140
A)
E.coli:
10141
10142
i)
Autoanalysis
Colilert
System, Standard
Methods,
20
th
10143
21ed.,
Method 9223
B.
10144
10145
ii)
Colisure
Test,
Standard Methods,
or
21st
ed.,
Method
10146
9223 B.
10147
10148
iii)
Membrane
Filter Method with
MI Agar, USEPA
Method
10149
1604.
10150
10151
iv)
m-ColiBlue24
Test.
10152
10153
v)
E*Colite
Test.
10154
10155
vi)
EC-MUG, Standard
Methods,
20
th
ed., Method 9221
F.
10156
10157
vii)
NA—MUG, Standard
Methods,
20t
ed., Method 9222
G.
10158
10159
jIi
Colilert-18,
Standard
Methods,
20
th
or
21st
ed.,
Method
10160
9222G.
10161
10162
BOARD
NOTE:
EC-MUG
(Standard
Methods, Method
9221F) or
10163
NA-MUG
(Standard
Methods, Method
9222G) can
be used for
E.
10164
coli testing step,
as described in
Section
611.526(a)
or (b) after
use
10165
of
Standard Methods,
Method
9221 B, 9221 D, 9222
B, or 9222
C.
JCAR35O61
1-0815204r01
10166
On June
3, 2008
(at
73 Fed.
Reg. 31616),
USEPA
added appendix
10167
A to subpart
C
of
40
CFR 141,
which authorized
alternative
10168
methods
to those
listed for
E. coli
by
Colilert
and
Colisure and
10169
added
Colilert-18
in the table
at corresponding
40
CFR
10170
141.402(c)(2)
to
allow the
use of the
21st
edition
of
Standard
10171
Methods
for
the
Examination
of
Water and
Wastewater
and
10172
Standard
Methods
Online
(at
www.standardmethods.org),
Method
10173
9223
B
(as
approved
in 1997).
The Board
has
instead
cited only
to
10174
the
2lS
edition of
Standard
Methods
for
the
Examination
of Water
10175
and Wastewater
(the
printed version
of
Standard
Methods),
since
10176
the
version
of
Method
9223
B
that appears
in
that printed
volume
10177
is
that cited
by
USEPA
as acceptable
for use.
USEPA
also added
10178
the
version
of
Method
9223 B that
appears
in
the
20
th
edition
of
10179
Standard
Methods
as to
Colilert-18.
10180
10181
B)
Enterococci:
10182
10183
i)
Multiple-Tube
Technique,
Standard
Methods,
20
th
ed.,
10184
Method
9230 B
or Standard
Methods
Online, Method
9230
10185
B.
10186
10187
BOARD
NOTE:
On June
3, 2008
(at 73 Fed.
Reg. 31616),
10188
USEPA
added
appendix
A to subpart
C of
40
CFR 141,
10189
which
authorized
alternative
methods
to
those
listed
for
10190
enterococci
by multiple-tube
techniciue
at corresponding
40
10191
CFR
141.402(c)(2)
to allow the
use of the
Standard
10192
Methods
Online
(at
www.standardmethods.org),
Method
10193
9230
B
(as
approved
in
2004).
10194
10195
ii)
Membrane
Filter Technique,
Standard
Methods,
20
th
ed.,
10196
Method
9230
C,
and
USEPA
Method
1600.
10197
10198
BOARD
NOTE:
The
holding
time
and temperature
for
10199
groundwater
samples
are specified
in
subsection
(c)(2)(D)
10200
of
this Section,
rather
than as specified
in Section
8 of
10201
USEPA
Method
1600.
10202
10203
iii)
Enterolert.
10204
10205
BOARD
NOTE: Medium
is
available
through
1I)EXX
10206
Laboratories,
Inc.,
at the address
set forth
in Section
10207
611.102(b).
Preparation
and
use of the
medium
must be as
JCAR35O61
1-0815204r01
10208
set
forth in the article that
embodies
the
method
as
10209
incorporated
by
reference
in Section
6
11.102(b).
10210
10211
C)
Coliphage:
10212
10213
i)
Two-Step Enrichment
Presence-Absence
Procedure,
10214
USEPA Method
1601.
10215
10216
ii)
Single Agar Layer
Procedure,
USEPA Method 1602.
10217
10218
D)
Limitation on methods
use.
The time
from sample collection
to
10219
initiation
of
analysis
may not exceed 30
hours. The
GWS supplier
10220
is encouraged
but is not
required
to
hold samples below
10°C
10221
during
transit.
10222
10223
d)
Invalidation
of a fecal
indicator-positive groundwater
source sample.
10224
10225
1)
A GWS supplier
may obtain Agency
invalidation
of a fecal indicator-
10226
positive groundwater
source sample
collected pursuant
to subsection
(a)
of
10227
this Section
only under either
of the following
conditions:
10228
10229
A)
The
supplier provides
the Agency with
written notice
from the
10230
laboratory
that
improper sample analysis
occurred;
or
10231
10232
B)
The Agency determines
and
documents in writing
by a SEP issued
10233
pursuant
to Section 611.110 that
there is
substantial
evidence that
a
10234
fecal indicator-positive
groundwater
source sample
is not related
to
10235
source
water
quality.
10236
10237
2)
If the
Agency invalidates
a fecal indicator-positive
groundwater source
10238
sample, the GWS supplier
must collect
another source water
sample
10239
pursuant
to subsection (a)
of this Section
within 24 hours after
being
10240
notified
by
the
Agency
of its invalidation decision,
and
the supplier must
10241
have
it analyzed for the same
fecal
indicator
using the analytical
methods
10242
in subsection
(c) of this
Section. The Agency
may
extend
the 24-hour
10243
time
limit on a case-by-case
basis
if the
supplier cannot collect
the
source
10244
water sample
within
24 hours due to circumstances
beyond
its control.
In
10245
the
case of an extension,
the Agency must
specify how
much time the
10246
system has to collect
the sample.
10247
10248
e)
Sampling
location.
10249
JCAR35O61 1-0815204r01
10250
1)
Any groundwater
source
sample required
pursuant to subsection
(a)
of this
10251
Section must
be collected
at a location prior
to any treatment of
the
10252
groundwater
source
unless
the Agency approves
a sampling
location
after
10253
treatment.
10254
10255
2)
If the supplier’s
system
configuration
does not allow for
sampling at
the
10256
well
itself, it may collect
a sample at an
Agency-approved
location to
meet
10257
the
requirements of subsection
(a)
of this Section if the
sample is
10258
representative
of
the water quality
of that well.
10259
10260
f)
New sources.
If directed
by the Agency
by a SEP issued pursuant
to Section
10261
611.110,
a GWS supplier that
places a new
groundwater source
into service
after
10262
November
30, 2009 must
conduct assessment
source
water
monitoring pursuant
10263
to
subsection
(b) of this Section.
If directed
by the SEP, the system
must
begin
10264
monitoring
before the groundwater
source is used
to provide
water to the public.
10265
10266
g)
Public Notification.
A
GWS
supplier with a groundwater
source
sample collected
10267
pursuant to subsection
(a) or
(b) of this Section
that is fecal indicator-positive
and
10268
which is not
invalidated pursuant
to subsection
(d) of this
Section,
including a
10269
consecutive
system supplier
served
by the
groundwater source,
must conduct
10270
public notification
pursuant
to Section 611.902.
10271
10272
h)
Monitoring
Violations.
A failure
to meet
the requirements
of subsections
(a)
10273
through (f) of this Section
is a monitoring
violation that
requires the
GWS
10274
supplier
to provide
public notification
pursuant
to
Section 611.904.
10275
10276
BOARD
NOTE:
Derived
from 40 CFR 141.402
(2007)
and
appendix A to 40
CFR 141.
10277
as
added
at 73 Fed. Reg. 31616
(June
3,
2008), as added at 71
Fed. Reg. 65574
(Nov.
8,
10278
2006).
10279
10280
(Source:
Amended
at
33
Ill.
Reg.
effective
10281
10282
SUBPART U:
CONSUMER CONFIDENCE
REPORTS
10283
10284
Section 611.884
Required Additional
Health
Information
10285
10286
a)
All
reports must prominently
display
the following
language: “Some people
may
10287
be more vulnerable
to contaminants
in drinking water than
the general
population.
10288
Immuno-compromised
persons such
as persons with
cancer undergoing
10289
chemotherapy, persons
who have
undergone organ
transplants, people
with
10290
HIV/AIDS or other
immune
system disorders, some
elderly, and
infants can
be
10291
particularly
at risk from infections.
These people
should
seek
advice about
10292
drinking water from
their health
care providers.
USEPA or Centers
for Disease
JCAR35O61 1-0815204r01
10293
Control and Prevention guidelines
on appropriate means to lessen
the risk of
10294
infection
by Cryptosporidium and other microbial
contaminants are available
10295
from the USEPA Safe Drinking
Water Hotline (800-426-4791).
10296
10297
b)
A
supplier
that detects arsenic above 0.005
mg/i and up to and including
0.010
10298
mgf€ must do the following:
10299
10300
1)
The supplier must include in its report
a short informational statement
10301
about arsenic,
using the following language:
“While your drinking water
10302
meets USEPA’s standard for arsenic,
it does contain low levels of
arsenic.
10303
USEPA’s
standard balances the current understanding
of arsenic’s possible
10304
health effects against the costs
of removing arsenic from drinking water.
10305
USEPA continues to research
the health effects
of
low levels
of arsenic,
10306
which
is a naturally-occurring mineral known
to cause cancer in humans
10307
at high concentrations and is linked
to other health effects such as
skin
10308
damage and
circulatory problems.”; or
10309
10310
2)
The
supplier may write its own educational
statement, but only in
10311
consultation with the Agency.
10312
10313
c)
A supplier that detects
nitrate at levels above 5 mg/2,
but below the MCL, must
10314
do the following:
10315
10316
1)
The supplier must include a short
informational statement about the
10317
impacts
of nitrate on children, using the following
language: “Nitrate in
10318
drinking water at levels above
10 ppm is a health risk for infants
of less
10319
than six months of age. High nitrate levels
in drinking water can cause
10320
blue baby syndrome.
Nitrate levels may rise quickly for short
periods of
10321
time because of rainfall or agricultural
activity. If you are caring for an
10322
infant you should ask advice
from your health care provider”; or
10323
10324
2)
The CWS supplier may write its
own educational statement, but only
in
10325
consultation with the Agency.d)A
CWS supplier that detects lead
above
10326
the
action level in more than five percent,
and up to and including ten
10327
percent, of homes sampled
must do the following:
10328
10329
cU
Every
report
must include
the following lead-specific information:
10330
10331
j
A short informational statement
about lead in drinking water and its
10332
effects on children.
The statement must include
the following
10333
information:
10334
JCAR35O61
1-0815204r01
If present,
elevated levels
of lead
can
cause
serious health
problems,
especially
for pregnant
women
and young
children.
Lead in drinking
water
is primarily
from materials
and
components
associated
with service
lines and
home plumbing.
[NE
OF
SUPPLIER]
is responsible
for
providing
high quality
drinking
water,
but cannot
control
the variety
of
materials
used
in
plumbing
components.
When
your water
has been
sitting for
several hours,
you
can minimize
the potential
for lead
exposure
by flushing
your
tap for
30
seconds
to two minutes
before
using water
for
drinking
or cooking.
If
you are concerned
about
lead in
your water,
you
may wish
to
have
your water
tested.
Information
on lead in
drinking
water,
testing methods,
and
steps you
can take to
minimize
exposure
is available
from
the
Safe Drinking
Water
Hotline
or at http
://www.epa.
gov/safewater/lead.
A supplier
may
write
its
own
educational
statement,
but only
in
consultation
with
the Agency.
The
CWS
supplier
must
include a short
informational
statement
about
the
special impact
of lead
on
children,
using the
following
language:
“Infants
and
young children
are
typically
more
vulnerable
to
lead
in drinking
water
than
the general
population.
It is
possible that
lead
levels
at your
home
may be hier
than
at other homes
in the
community
as a result
of
materials
used in
your home’s
plumbing.
If you are
concerned
about
elevated
lead
levels
in
your home’s
water,
you may
wish
to have
your
water tested
and flush
your tap
for 30 seconds
to
two
minutes
before
using
tap water.
Additional
information
is
available from
the
USEPA
Safe
Drinking
Water
Hotline
(800
426 4791)”;
or
2)
The
CWS
supplier
may
write
its own educational
statement,
but
only
in
consultation
with
the
Agency.
e)
A
CWS
supplier
that
detects
TTHM above
0.080
mg/e,
but below
the MCL
in
Section
611.312,
as an annual
average,
monitored
and
calculated
under
the
provisions
of former
Section
611.680,
must include
the health
effects language
prescribed
by
Appendix A
of this Part.
f)
Until
January 22,
2006, a
CWS
supplier
that detects
arsenic
above 0.0
10 mg/i
and
up to
and including
0.05
mg/e must
include the
arsenic
health
effects
language
prescribed
by
Appendix
A to this
Part.
BOARD
NOTE:
Derived from
40 CFR
141.154
(2007),
as amended
at
72
Fed. Reg.
7782
(October
12, 2007)(2003).
10335
10336
10337
10338
10339
10340
10341
10342
10343
10344
10345
10346
10347
10348
10349
10350
10351
10352
10353
4-)
10354
10355
10356
10357
10358
10359
10360
10361
10362
10363
10364
10365
10366
10367
10368
10369
10370
10371
10372
10373
10374
10375
10376
10377
JCAR35O61 1-0815204r01
10378
10379
(Source: Amended
at 33 Ill. Reg.
effective
10380
10381
SUBPART W:
INITIAL
DISTRIBUTION
SYSTEM EVALUATIONS
10382
10383
Section
611.920 General Requirements
10384
10385
a)
USEPA
has designated
that the requirements
of
this
Subpart W constitute
10386
National Primary Drinking
Water
Regulations. The regulations
in this
Subpart
W
10387
establish
monitoring
and other requirements
for identifying
Subpart Y compliance
10388
monitoring locations
for determining
compliance with
maximum
contaminant
10389
levels
for TTHMs and
HAA5. The supplier
must
use an initial distribution
10390
system evaluation (IDSE)
to determine the
locations in
its distribution
system that
10391
are
representative of high
TTHM
and
HAA5 concentrations
throughout
the
10392
supplier’s
distribution
system. An LDSE is
used
in conjunction
with, but separate
10393
from,
Subpart I compliance
monitoring,
to identify and select
Subpart Y
10394
compliance
monitoring
locations.
10395
10396
b)
Applicability.
A supplier
is subject to the
requirements
of this Subpart
W
if
it
10397
fulfills
any of the following
conditions:
10398
10399
1)
The supplier
owns or operates
a
community
water system that uses
a
10400
primary or
residual disinfectant
other
than
ultraviolet light;
10401
10402
2)
The
supplier delivers water
that has been
treated with
a primary or residual
10403
disinfectant
other than
ultraviolet light;
or
10404
10405
3)
The supplier owns or
operates a
non-transient
non-community
water
10406
system
that serves at least
10,000 people,
and it either
uses a primary
or
10407
residual
disinfectant other
than ultraviolet
light, or it delivers
water that
10408
has
been treated with a primary
or residual
disinfectant other
than
10409
ultraviolet
light.
10410
10411
c)
Schedule. A supplier
must
comply
with the requirements
of this
Subpart W on
10412
the
schedule
provided in subsection
(c)(1)
of this
Section based on its
system
10413
type, as set forth
in the
applicable
of subsections
(c)(1)(A) through
10414
(c)(1)(E)(c)(1)(D)
of this Section,
subject
to the
conditions of subsections
10415
(c)(1 )(F)(c)(1 )(E)
through
(c)(1
)(H)(c)( 1
)(G)
of this Section:
10416
10417
1)
Compliance dates.
10418
10419
A)
A supplier
that is not part of
a combined
distribution system, or
a
10420
supplier that
serves
the
largest population in
a combined
JCAR35O61 1-0815204r01
10421
distribution system,
and which serves a
population of 100,000
or
10422
more
persons must either
have submitted its standard monitoring
10423
plan, its system-specific
study plan,
or its 40/30 certification
or
10424
must have obtained
or have been subject to a very
small system
10425
waiver
before October 1, 2006.
The supplier must further
10426
complete
its standard monitoring
or system-specific study
before
10427
September
30,
2008
and submit its IDSE
report to the Agency
10428
before January 1, 2009.
10429
10430
B)
A supplier that is
not part of a combined distribution
system, or
a
10431
supplier
that serves the largest
population in a combined
10432
distribution
system,
and which serves a population
of 50,000 to
10433
99,999 persons
must either have
submitted its standard monitoring
10434
plan,
its system-specific study
plan, or its 40/30 certification
or
10435
must have obtained
or have been subject to
a
very
small system
10436
waiver
before April 1, 2007. The
supplier must further complete
10437
its standard monitoring
or system-specific study
before March
31,
10438
2009
and submit its IDSE report
to the Agency before July 1,
10439
2009.
10440
10441
C)
A supplier
that is not part of a
combined distribution
system,
or a
10442
supplier that serves
the largest population
in a combined
10443
distribution
system, and which serves a population
of 10,000 to
10444
49,999
persons must
submit its standard monitoring plan,
its
10445
system-specific study plan, or its 40/30
certification or must
obtain
10446
or be subject
to a very small system waiver
before October 1,
10447
2007.
The supplier must
further complete its standard monitoring
10448
or system-specific
study before September
30,
2009
and submit
its
10449
IDSE report to the Agency
before January 1, 2010.
10450
10451
D)
A supplier
that is not part of a combined
distribution system,
or a
10452
supplier that serves
the largest population in a combined
10453
distribution
system, and which serves
a population of fewer than
10454
10,000
persons (and which
is a CWS) must submit its standard
10455
monitoring
plan, its system-specific
study plan, or its
40/30
10456
certification or must
obtain or be subject to a very small
system
10457
waiver
before April 1, 2008. The
supplier must further complete
10458
its standard
monitoring or system-specific
study before March
31,
10459
2010
and submit its IDSE
report to the Agency before July
1,
10460
2010.
10461
10462
A supplier that
is part of a combined distribution
system which
10463
does
not serve the largest
population in the combined
system,
JCAR35O61
1-0815204r01
10464
which
is a wholesale system
supplier or
a consecutive
system
10465
supplier,
must submit
its standard
monitoring
plan, its system—
10466
specific
study
plan, or its 40/30
certification
or must
obtain or be
10467
subject
to a very small
system waiver;
must further complete
its
10468
standard
monitoring
or system-specific
study; and submit
its IDSE
10469
report
to the Agency
at the same time
as the supplier
in the
10470
combined
system
that has
the earliest
compliance
date.
10471
10472
FE)
If, within 12 months
after the date
when
submission
of the standard
10473
monitoring
plan,
the system-specific
study plan,
or the 40/30
10474
certification or
becoming subject
to a very
small
system waiver is
10475
due,
as identified
in the applicable
of subsections
(a)(1) through
10476
(a)(4) of this Section,
the
Agency
does not approve
a supplie?s
10477
plan
or notify
the supplier that it has
not yet completed
its review,
10478
the
supplier may consider
the
plan
that it submitted as
approved.
10479
The
supplier must
implement that plan,
and
it must
complete
10480
standard
monitoring
or a system-specific
study no later
than
the
10481
date
when completion
of the standard
monitoring
or system-
10482
specific
study is due,
as identified
in the applicable of
subsections
10483
(a)(1)
through
(a)(4) of this Section.
10484
10485
F)
The supplier must
submit
its
40/3
0 certification pursuant
to Section
10486
611.923
before
the date indicated
in the applicable
of subsections
10487
(a)(1) through
(a)(4) of this
Section.
10488
10489
HG)
If, within
three months after
the due date
for submission
of the
10490
IDSE report
identified
in this subsection
(c)(1) (nine months
after
10491
this
date
if the supplier must
comply on
the schedule in
subsection
10492
(c)(1)(C)
of this Section),
the Agency
does not approve the
10493
supplier’s
IDSE report or notify
the supplier
that it has not
yet
10494
completed
its review,
the
supplier may consider
the report
that it
10495
submitted
to the Agency, and
the
supplier
must implement the
10496
recommended
Subpart
Y monitoring as required.
10497
10498
2)
For
the purpose
of
determining the
applicable compliance
schedule
in
10499
subsection (c)(1)
of this Section, the
Agency
may,
by a SEP issued
10500
pursuant
to Section
611.110,
determine
that a combined
distribution
10501
system does not
include certain consecutive
systems
based on such
factors
10502
as the receipt of water
from a
wholesale
system
only on an emergency
10503
basis
or the receipt
of only
a small percentage and
small volume
of water
10504
from a wholesale
system. The
Agency may
also determine,
by a SEP
10505
issued pursuant
to Section
611.110, that
a combined distribution
system
10506
does not
include certain
wholesale systems
based
on such
factors as the
JCAR35O61 1-0815204r01
10507
delivery
of water to a consecutive
system only on an emergency
basis or
10508
the delivery of only a small
percentage and small
volume of water to
a
10509
consecutive system.
10510
10511
d)
A supplier must do one of the
following: it must conduct
standard monitoring
10512
that meets the requirements in Section
611.921; it must conduct
a system-specific
10513
study that meets the requirements in Section
611.922; it must certify to
the
10514
Agency that it meets the 40/30
certification criteria
under Section 611.923;
or
it
10515
must qualify for a very small system
waiver under Section 611.924.
10516
10517
1)
The supplier must have taken
the full complement of routine
TTHM and
10518
HAA5 compliance
samples required
of
a
system that serves the
10519
appropriate population and which
uses the appropriate source
water under
10520
Subpart I of this Part
(or the supplier must have
taken the full complement
10521
of reduced TTHM and HAA5 compliance
samples required of a system
10522
with the supplier’s population
and source water under Subpart
I of this Part
10523
if the supplier
meets reduced monitoring
criteria under Subpart I of this
10524
Part) during the period
specified in Section 611.923(a) to
meet the 40/30
10525
certification criteria in Section 611.923.
The supplier must have taken
10526
TTHM and
HAA5 samples under Sections 611.381
and 611.382 to be
10527
eligible for the very
small system waiver in Section 611.924.
10528
10529
2)
If the supplier has not taken the required
samples, the supplier must
10530
conduct standard
monitoring that meets the
requirements in Section
10531
611.921, or a
system-specific study that meets the requirements
in Section
10532
611.922.
10533
10534
e)
The
supplier must use
only the analytical methods
specified in Section 611.381,
10535
or otherwise approved by the Agency
for monitoring under this Subpart
W, to
10536
demonstrate compliance
with the requirements of this
Subpart W.
10537
10538
f)
IDSE results will not be used
for the purpose of determining compliance
with
10539
MCLs in
Section 611.3 12.
10540
10541
BOARD NOTE: Derived from 40
CFR
141.600
(2007’)(2006).
10542
10543
(Source: Amended at 33 Ill. Reg.
effective
10544
10545
SUBPART
Z: ENHANCED
TREATMENT FOR
CRYPTOSPORIDIUM
10546
10547
Section 611.1004 Source Water Monitoring Requirements:
Analytical Methods
10548
10549
a)
Cryptosporidium. A
supplier must analyze for Cryptosporidium
using USEPA
10550
OGWDW Methods, Method 1623
(05) or USEPA OGWDW Methods, Method
JCAR35O61 1-0815204r01
10551
1622
(05), or alternative methods approved
by
the
Agency pursuant to Section
10552
611.480, each incorporated
by reference in Section 611.102.
10553
10554
1)
The supplier
must analyze at least a 10 £ sample
or a packed pellet volume
10555
of at least 2
m as generated by the methods listed in subsection (a)
of this
10556
Section. A supplier unable
to
process
a 10 £ sample must analyze as
much
10557
sample
volume as can be filtered
by
two filters
approved by USEPA for
10558
the methods
listed in subsection (a) of this Section, up
to
a packed
pellet
10559
volume of at least 2 m2.
10560
10561
2)
Matrix spike (MS) samples.
10562
10563
A)
MS samples, as required
by
the methods
in subsection (a) of this
10564
Section,
must be spiked and filtered by a laboratory approved
for
10565
Cryptosporidium analysis pursuant to
Section 611.1005.
10566
10567
B)
If
the volume of the MS sample is greater than
10 £,
the
supplier
10568
may filter all but
10 £ of
the
MS sample in the field, and ship the
10569
filtered sample and the remaining 10 £
of source water to the
10570
laboratory.
In this case, the laboratory must spike the remaining
10571
10 £ of water and filter it
through the filter used to collect the
10572
balance of the sample in the field.
10573
10574
3)
Flow cytometer-counted
spiking suspensions must
be
used for
MS
10575
samples and ongoing precision
and recovery samples.
10576
10577
b)
E. coli. A supplier must
use methods for enumeration of E. coli in source water
10578
approved in 40 CFR 136.3(a), or alternative methods
approved by the Agency
10579
pursuant to Section 611.480,
incorporated by reference in Section 611.102.
10580
10581
1)
The time from sample collection
to initiation of analysis may not exceed
10582
30
hours, unless
the supplier meets the condition of subsection (b)(2)
of
10583
this Section.
10584
10585
2)
The Agency may, by a SEP issued pursuant
to Section 611.110, approve
10586
on a case-by-case
basis the holding of an E. coli sample for up to 48
hours
10587
between sample collection and initiation
of analysis if it determines that
10588
analyzing
an E. coli sample within 30 hours
is not feasible. B. coli
10589
samples held
between 30 to 48 hours must be analyzed
by
the
10590
Autoanalysis Colilert System
reagent version of Standard Methods,
18
th
10591
19
th,
or
20
th
ed., Method 9223 B, as listed
in 40 CFR 136.3(a),
10592
incorporated
by reference in Section 611.102.
10593
JCAR35O61 1-0815204r01
10594
3)
A supplier must maintain
the temperature of its samples between 0°C
and
10595
10°C during storage and transit to the laboratory.
10596
10597
4
The supplier may use the membrane filtration, two-step
procedure
10598
described in Standard Methods,
20t11
ed., Method 9222 D and
G,
10599
incorporated
by reference in Section 611.102.
10600
10601
BOARD NOTE: On June 3,2008 (at
73
Fed. Reg. 31616),
USEPA added
10602
appendix
A to subpart
C
of 40 CFR 141, which authorized alternative
10603
methods to those listed for
E.
coli
by
multiple-tube
technique at
10604
corresponding
40 CFR
141.402(c)(2)
to allow the use of Standard
10605
Methods for the Examination of Water
and
Wastewater,
Method
9222
D
10606
andG.
10607
10608
c)
Turbidity. A supplier must use methods
for
turbidity
measurement approved in
10609
Section 611.53 1(a).
10610
10611
BOARD NOTE: Derived from
40
CFR 141.704 (2007) and appendix A to 40 CFR 141, as
10612
added at 73
Fed. Reg. 31616
(June
3, 2008)(2006).
10613
10614
(Source: Amended at 33 Ill. Reg.
effective
10615
10616
Section 611.1007
Source Water Monitoring Requirements:
Grandfathering Previously
10617
Collected Data
10618
10619
a)
Initial source monitoring
and Cryptosporidium samples.
10620
10621
1)
A supplier
may comply with the initial source water monitoring
10622
requirements of Section 611.1001(a)
by
grandfathering sample results
10623
collected before the supplier
is required to begin monitoring (i.e.,
10624
previously collected data). To be grandfathered, the sample results and
10625
analysis must meet the criteria in this
Section and
the
Agency must
10626
approve the
use of the data by a SEP issued pursuant to Section 611.110.
10627
10628
2)
A filtered system
supplier may grandfather Cryptosporidium samples to
10629
meet the requirements of Section 611.1001(a) when the supplier does
not
10630
have corresponding B. coli and turbidity samples. A supplier that
10631
grandfathers Cryptosporidium
samples without E. coli and turbidity
10632
samples is not required to collect E. coli and turbidity
samples
when
it
10633
completes the requirements for Cryptosporidium monitoring pursuant
to
10634
Section6ll.1001(a).
10635
JCAR35O61
1-0815204r01
10636
b)
E. coli sample
analysis.
The
analysis of E. coli samples
must
meet
the analytical
10637
method and approved
laboratory
requirements
of Sections 611.1004
and
10638
611.1005.
10639
10640
c)
Cryptosporidium
sample analysis.
The analysis
of Cryptosporidium
samples
must
10641
meet the criteria
in
this
subsection (c).
10642
10643
1)
Laboratories
must
analyzeanalyzed
Cryptosporidium
samples using
one of
10644
the following
analytical methods,
or alternative
methods approved by
the
10645
Agency pursuant
to Section 611.480:
10646
10647
A)
USEPA
OGWDW
Methods,
Method 1623 (05),
incorporated
by
10648
reference
in Section 611.102;
10649
10650
B)
USEPA
OGWDW Methods,
Method 1622 (05),
incorporated
by
10651
reference
in Section 611.102;
10652
10653
C)
USEPA OGWDW
Methods, Method
1623
(01),
incorporated
by
10654
reference in
Section 611.102;
10655
10656
D)
USEPA
OGWDW Methods,
Method 1622
(01), incorporated
by
10657
reference
in
Section 611.102;
10658
10659
E)
USEPA OGWDW Methods,
Method
1623 (99), incorporated
by
10660
reference
in Section
611.102; or
10661
10662
F)
USEPA OGWDW
Methods,
Method
1622 (99), incorporated
by
10663
reference
in
Section
611.102.
10664
10665
2)
For each
Cryptosporidium
sample, the laboratory
analyzed at least
10
e of
10666
sample or
at least 2 m of
packed pellet
or
as much
volume
as could be
10667
filtered
by two filters that USEPA
approved
for the methods listed
in
10668
subsection (c)(1)
of this Section.
10669
10670
d)
Sampling location.
The sampling
location must meet the
conditions in
Section
10671
611.1003.
10672
10673
e)
Sampling frequency.
Cryptosporidium
samples were
collected no less frequently
10674
than each
calendar
month on a regular
schedule,
beginning no earlier
than January
10675
1999. Sample collection
intervals
may vary for the
conditions
specified in
10676
Section 611
.1002(b)(1) and (b)(2)
if the supplier
provides documentation
of
the
10677
condition
when reporting monitoring
results.
10678
JCAR35061 1-0815204r01
10679
1)
The Agency may,
by
a SEP
issued pursuant to Section 611.110, approve
10680
grandfathering
of previously collected data where there are time
gaps in
10681
the sampling frequency if
the supplier conducts additional monitoring
that
10682
the Agency has specified
by
a
SEP
issued
pursuant to Section 611.110 to
10683
ensure that
the data used to comply with the initial source water
10684
monitoring requirements
of Section 611.1001(a) are seasonally
10685
representative and unbiased.
10686
10687
2)
A supplier may
grandfather previously collected data where the sampling
10688
frequency within each month varied. If the
Cryptosporidium sampling
10689
frequency varied,
the supplier must follow the monthly averaging
10690
procedure in Section 611.1010(b)(5) or Section
611.1012(a)(3), as
10691
applicable, when calculating
the bin classification for a filtered system
10692
supplier or
the mean Cryptosporidium concentration for an unfiltered
10693
system supplier.
10694
10695
f)
Reporting monitoring results for grandfathering. A
supplier that requests to
10696
grandfather previously
collected monitoring results must report the following
10697
infonnation by the applicable dates listed
in this subsection. A supplier must
10698
report this information to the Agency.
10699
10700
1)
A supplier must report that
it intends to submit previously collected
10701
monitoring results for grandfathering.
This report must specify the
10702
number of previously collected results the supplier will submit,
the dates
10703
of the first and last
sample, and whether a supplier will conduct additional
10704
source water monitoring to
meet the requirements of Section 611.1001(a).
10705
The supplier must report this information no later than the applicable
date
10706
set forth in Section 611.1002.
10707
10708
2)
A supplier must report previously collected
monitoring results for
10709
grandfathering, along
with the associated documentation listed in
10710
subsections (f)(2)(A) through (f)(2)(D) of this Section,
no later than two
10711
months after the applicable
date listed in Section 611.1001(c).
10712
10713
A)
For each sample result,
a supplier must report the applicable data
10714
elements in Section 611.1006.
10715
10716
B)
A supplier must certify that the
reported monitoring results include
10717
all results that it generated during the time
period
beginning
with
10718
the first reported
result and ending with the final reported result.
10719
This applies to samples
that were collected from the sampling
10720
location specified for source water
monitoring pursuant to this
10721
Subpart Z,
which were not spiked, and which were analyzed
using
JCAR35O61 1-0815204r01
10722
the laboratory’s
routine process for the analytical methods listed
in
10723
this Section.
10724
10725
C)
The supplier must
certify that the samples were representative
of a
10726
plant’s source waters and the source waters have
not changed. It
10727
must
report a description of the sampling locations, which
must
10728
address the
position of the sampling location in relation to its water
10729
sources and treatment processes,
including points of chemical
10730
addition
and filter backwash recycle.
10731
10732
D)
For
Cryptosporidium samples, the laboratory or laboratories
that
10733
analyzed the samples
must provide a letter certifying that the
10734
quality
control criteria specified in the methods listed in subsection
10735
(c)(1) of this Section were met for each sample batch
associated
10736
with the reported
results. Alternatively, the laboratory may
10737
provide bench sheets and sample examination report forms
for
10738
each field, matrix
spike, initial precision and recovery, ongoing
10739
precision and recovery, and method blank sample associated
with
10740
the reported results.
10741
10742
g)
If the Agency determines that a previously collected data set submitted for
10743
grandfathering was
generated during source water conditions that were not normal
10744
for the supplier, such as a drought,
the Agency may, by a SEP issued pursuant to
10745
Section 611.110, disapprove the data.
Alternatively, the Agency may, by a SEP
10746
issued pursuant to Section 611.110, approve the previously collected data if
the
10747
supplier reports additional
source water monitoring data, as determined by the
10748
Agency, to ensure that the data set used pursuant
to
Section
611.1010 or Section
10749
611.1012 represents
average source water conditions for the supplier.
10750
10751
h)
If a
supplier submits previously
collected data that fully meet the number of
10752
samples required for initial source water monitoring pursuant to Section
10753
611.1001(a), and some of the data are rejected
due to not meeting the
10754
requirements
of this
Section, the supplier must conduct additional monitoring to
10755
replace rejected data on a schedule that the Agency has
approved by a SEP issued
10756
pursuant to Section
611.110. A supplier is not required to begin this additional
10757
monitoring until two months afier notification that data
have been rejected and
10758
additional
monitoring
is necessary.
10759
10760
BOARD NOTE: Derived from 40 CFR 141.707 (2007)(2006).
10761
10762
(Source:
Amended at 33 Ill.
Reg.
effective