OFFICE OF
THE SECRETARY OF STATE
JESSE WHITE • Secretary of State
RECEIVEDCLERK'S
OFFICE
POLLUTION CONTROL BOARD
!' I
1 2006
James R . Thompson Center 100 W . Randolph St ., Ste 11-500
Dorothy Gunn
STATE OF ILLINOIS
pollution
Control Board
CHICAGO, IL 60601
Dear Dorothy Gunn
Your rules Listed below met our codification standards and have been published in
Volume 30, Issue 31 of the Illinois Register, dated 08/04/2006 .
PROPOSED RULES
Primary Drinking Water Standards
35 III. Adm. Code 611
Page 13054
Point Of Contact
:Erin Conley
If you have any questions, you may contact the Administrative Code Division at
(217) 782 - 7017 .
07/28/2006
Index Department - Administrative Code Division - 111 East Monroe Springfield, IL 62756
4)
Statutory authority
:
415 ILCS 5/7.2, 17, 17.5, and 27 .
5)
A Complete description of the subjects and issues involved :
The following briefly describes the subjects and issues involved in the docket R06-15
rulemaking
. A comprehensive description is contained in the Board's opinion and order
of July 20, 2006, proposing amendments in docket R06-15, which opinion and order is
available from the address below
.
This proceeding updates the Illinois Safe Drinking Water Act (SDWA) rules to
correspond with amendments adopted by the United States Environmental Protection
Agency (USEPA) that appeared in the Federal Register during a single update period
.
The docket and time period that is involved in this proceeding is the following :
R06-15
Federal SDWA amendments that occurred during the period July 1,
2005 through December 31, 2005 .
The R06-15 docket only amends rules in Part 611 . The following table briefly
summarizes the sole federal action in the update period :
October 13, 2005
(70 Fed. Reg. 59848)
USEPA adopted new requirements for the filing and
receipt of required documents as electronic documents
.
The filings included are all documents whose filing is
provided by the primary drinking water regulations
.
RECEIVED
JUL 2 4 2006
SOS CODE DIV
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1)
Heading of the Part : Primary Drinking Water Standards
2)
Code citation : 35 Ill. Adm. Code 611
3)
Section numbers:
Proposed action :
611 .102
Amend
611 .105
New Section
611 .111
Amend
611 .212
Amend
611 .359
Amend
611 .380
Amend
611 .609
Amend
611 .646
Appendix D
Amend
New Section
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
The USEPA action of October 13, 2005 (70 Fed . Reg
. 59848) established the Cross-
Media Electronic Reporting Rule (CROMERR) . The CROMERR sets standards for the
filing of documents in various federal program areas in an electronic format
. While the
CROMERR does not require the filing of documents in an electronic format, it does
impose minimum requirements on documents that are filed in such a format and on the
electronic document receiving systems used to receive them . The CROMERR imposes
requirements on electronic filings submitted to USEPA and on USEPA's Central Data
Exchange (CDX) that receives them, as well as on any electronic document filings
submitted to the states and any systems used by the states to receive those filings .
Tables appear in the Board's opinion and order of July 20, 2006 in docket R06-15 that list
numerous corrections and amendments that are not based on current federal amendments .
The tables contain deviations from the literal text of the federal amendments underlying
these amendments, as well as corrections and clarifications that the Board made in the
base text involved . Persons interested in the details of those corrections and amendments
should refer to the July 20, 2006 opinion and order in docket R06-15 .
Section 17.5 of the Environmental Protection Act [415 ILCS 5/17 .5] provides that
Section 5-35 of the Administrative Procedure Act [5 ILCS 100/5-35] does not apply to
this rulemaking . Because this rulemaking is not subject to Section 5-35 of the APA, it is
not subject to First Notice or to Second Notice review by the Joint Committee on
Administrative Rules (JCAR).
6)
Published studies or reports, and sources of underlyinRdata, used to compose this
rulemaking : None
7)
Will these proposed amendments replace emergency amendments currently in effect?
No.
8)
Does this rulemaking contain an automatic repeal date? : No.
9)
Do these proposed amendments contain incorporations by reference?
Yes. Section 611
.102 is the centralized location of all incorporations of documents used
for the purposes of compliance with all of Part 611
. The amendments update all citations
to the Code of Federal Regulations
to the latest edition available, although those updates
do not necessarily incorporate the cited federal regulations
. Second, the amendments add
incorporations of segments of the Code of Federal Regulations
that embody key elements
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
of the federal CROMERR requirements . Third, the amendments remove the
incorporation by reference of appendix C to 40 C .F.R. 136, since this document is not
referenced in any substantive segment of the rules . The amendments also update the
version of appendix B to 40 C .F .R
. 136 incorporated by reference to the latest edition
available
. Finally, the amendments add to each incorporation by reference of a segment
of the Code of Federal Regulations
a citation to the segments of the Illinois regulations
for which the incorporation is made .
10)
Are there any other amendments pending on this Part? No.
11)
Statement of statewide policy objectives :
These proposed amendments do not create or enlarge a state mandate, as defined in
Section 3(b) of the State Mandates Act . [30 ILCS 805/3(b) (2002)]
.
12)
Time, Place and manner in which interested persons may comment on this proposed
rulemaking :
The Board will accept written public comment on this proposal for a period of 45 days
after the date of this publication. Comments should reference docket R06-15 and be
addressed to:
Ms. Dorothy M. Gunn, Clerk
Illinois Pollution Control Board
State of Illinois Center, Suite 11-500
100 W
. Randolph St .
Chicago, IL 60601
Please direct inquiries to the following person and reference docket R06-15 :
Michael J . McCambridge
Staff Attorney
Illinois Pollution Control Board
100 W
. Randolph 11-500
Chicago, IL 60601
Phone: 312-814-6924
E-mail: mccambm@ipcb.state.il.us
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Request copies of the Board's opinion and order at 312-814-3620, or download a copy
from the Board's Website at http :\\www.ipcb .state.il.us.
13)
Initial regulatory flexibility analysis :
A)
Types of small businesses, small municipalities, and not-for-profit corporations
affected:
This rulemaking may affect those small businesses, small municipalities, and not-
for-profit corporations that own or operate a public water supply . These proposed
amendments do not create or enlarge a state mandate, as defined in Section 3(b) of
the State Mandates Act . [30 ILCS 805/3(b) (2002)] .
B)
Reporting, bookkeeping or other procedures required for compliance :
The existing rules and proposed amendments require extensive reporting,
bookkeeping and other procedures, including the preparation of reports, water
analyses, and maintenance of operating records . These proposed amendments do
not create or enlarge a state mandate, as defined in Section 3(b) of the State
Mandates Act. [30 ILCS 805/3(b) (2002)] .
C)
Types of professional skills neceessary for compliance :
Compliance with the existing rules and proposed amendments may require the
services of an attorney, certified public accountant, chemist, and registered
professional engineer. These proposed amendments do not create or enlarge a
state mandate, as defined in Section 3(b) of the State Mandates Act . [30 ILCS
805/3(b) (2002)] .
14)
Regulatory agenda on which this rulemaking was summarized :
December 30, 2005, at 29111 . Reg. 21103, 21132
The full text of the proposed amendments begins on the next page :
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
TITLE 35 : ENVIRONMENTAL PROTECTION
SUBTITLE F : PUBLIC WATER SUPPLIES
CHAPTER I: POLLUTION CONTROL BOARD
PART 611
PRIMARY DRINKING WATER STANDARDS
SUBPART A : GENERAL
Section
611 .100
Purpose, Scope, and Applicability
611 .101
Definitions
611 .102
Incorporations by Reference
611 .103
Severability
611 .105 Electronic Reporting
611 .107
Agency Inspection of PWS Facilities
611 .108
Delegation to Local Government
611 .109
Enforcement
611 .110
Special Exception Permits
611 .111
Relief Equivalent to SDWA Section 1415(a) Variances
611.112
Relief Equivalent to SDWA Section 1416 Exemptions
611 .113
Alternative Treatment Techniques
611
.114
Siting Requirements
611 .115
Source Water Quantity
611 .120
Effective Dates
611 .121
Maximum Contaminant Levels and Finished Water Quality
611 .125
Fluoridation Requirement
611 .126
Prohibition on Use of Lead
611
.130
Special Requirements for Certain Variances and Adjusted Standards
611
.131
Relief Equivalent to SDWA Section 1415(e) Small System Variance
611 .160
Composite Correction Program
SUBPART B : FILTRATION AND DISINFECTION
Section
611 .201
Requiring a Demonstration
611 .202
Procedures for Agency Determinations
611 .211
Filtration Required
611 .212
Groundwater under Direct Influence of Surface Water
611 .213
No Method of HPC Analysis
611 .220
General Requirements
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
611 .230
Filtration Effective Dates
611 .231
Source Water Quality Conditions
611 .232
Site-Specific Conditions
611 .233
Treatment Technique Violations
611 .240
Disinfection
611 .241
Unfiltered PWSs
611 .242
Filtered PWSs
611 .250
Filtration
611 .261
Unfiltered PWSs: Reporting and Recordkeeping
611
.262
Filtered PWSs : Reporting and Recordkeeping
611 .271
Protection during Repair Work
611 .272
Disinfection Following Repair
611 .276
Recycle Provisions
SUBPART C
: USE OF NON-CENTRALIZED TREATMENT DEVICES
Section
611 .280
Point-of-Entry Devices
611 .290
Use of Point-of-Use Devices or Bottled Water
SUBPART D: TREATMENT TECHNIQUES
Section
611 .295
General Requirements
611 .296
Acrylamide and Epichlorohydrin
611 .297
Corrosion Control
SUBPART F: MAXIMUM CONTAMINANT LEVELS (MCLs) AND
MAXIMUM RESIDUAL DISINFECTANT LEVELS (MRDLs)
Section
611 .300
Old MCLs for Inorganic Chemical Contaminants
611 .301
Revised MCLs for Inorganic Chemical Contaminants
611 .310
Old Maximum Contaminant Levels (MCLs) for Organic Chemical Contaminants
611 .311
Revised MCLs for Organic Chemical Contaminants
611 .312
Maximum Contaminant Levels (MCLs) for Disinfection Byproducts (DBPs)
611 .313
Maximum Residual Disinfectant Levels (MRDLs)
611 .320
Turbidity (Repealed)
611 .325
Microbiological Contaminants
611 .330
Maximum Contaminant Levels for Radionuclides
611 .331
Beta Particle and Photon Radioactivity (Repealed)
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
SUBPART G : LEAD AND COPPER
Section
611 .350
General Requirements
611 .351
Applicability of Corrosion Control
611 .352
Corrosion Control Treatment
611 .353
Source Water Treatment
611 .354
Lead Service Line Replacement
611 .355
Public Education and Supplemental Monitoring
611 .356
Tap Water Monitoring for Lead and Copper
611 .357
Monitoring for Water Quality Parameters
611 .358
Monitoring for Lead and Copper in Source Water
611 .359
Analytical Methods
611 .360
Reporting
611 .361
Recordkeeping
SUBPART I: DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS,
AND DISINFECTION BYPRODUCT PRECURSORS
Section
611 .380
General Requirements
611 .381
Analytical Requirements
611 .382
Monitoring Requirements
611 .383
Compliance Requirements
611 .384
Reporting and Recordkeeping Requirements
611 .385
Treatment Technique for Control of Disinfection Byproduct (DBP) Precursors
SUBPART K : GENERAL MONITORING AND ANALYTICAL
REQUIREMENTS
Section
611 .480
Alternative Analytical Techniques
611 .490
Certified Laboratories
611 .491
Laboratory Testing Equipment
611 .500
Consecutive PWSs
611 .510
Special Monitoring for Unregulated Contaminants (Repealed)
SUBPART L
: MICROBIOLOGICAL MONITORING AND ANALYTICAL
REQUIREMENTS
Section
611 .521
Routine Coliform Monitoring
611 .522
Repeat Coliform Monitoring
611 .523
Invalidation of Total Coliform Samples
611 .524
Sanitary Surveys
611 .525
Fecal Coliform and E . Coli Testing
611 .526
Analytical Methodology
611 .527
Response to Violation
611 .531
Analytical Requirements
611 .532
Unfiltered PWSs
611 .533
Filtered PWSs
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
SUBPART M : TURBIDITY MONITORING AND ANALYTICAL
REQUIREMENTS
Section
611.560
Turbidity
SUBPART N
: INORGANIC MONITORING AND ANALYTICAL
REQUIREMENTS
Section
611 .591
Violation of a State MCL
611 .592
Frequency of State Monitoring
611 .600
Applicability
611 .601
Monitoring Frequency
611 .602
Asbestos Monitoring Frequency
611 .603
Inorganic Monitoring Frequency
611 .604
Nitrate Monitoring
611 .605
Nitrite Monitoring
611 .606
Confirmation Samples
611 .607
More Frequent Monitoring and Confirmation Sampling
611 .608
Additional Optional Monitoring
611 .609
Determining Compliance
611 .610
Inorganic Monitoring Times
611
.611
Inorganic Analysis
611 .612
Monitoring Requirements for Old Inorganic MCLs
611 .630
Special Monitoring for Sodium
611 .631
Special Monitoring for Inorganic Chemicals (Repealed)
SUBPART 0 : ORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .640
Definitions
611 .641
Old MCLs
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
611 .645
Analytical Methods for Organic Chemical Contaminants
611 .646
Phase I, Phase II, and Phase V Volatile Organic Contaminants
611 .647
Sampling for Phase I Volatile Organic Contaminants (Repealed)
611 .648
Phase II, Phase IIB, and Phase V Synthetic Organic Contaminants
611 .650
Monitoring for 36 Contaminants (Repealed)
611 .657
Analytical Methods for 36 Contaminants (Repealed)
611 .658
Special Monitoring for Organic Chemicals (Repealed)
SUBPART P: THM MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .680
Sampling, Analytical, and other Requirements
611.683
Reduced Monitoring Frequency (Repealed)
611 .684
Averaging (Repealed)
611 .685
Analytical Methods
611 .686
Modification to System (Repealed)
611 .687
Sampling for THM Potential (Repealed)
611 .688
Applicability Dates (Repealed)
SUBPART Q: RADIOLOGICAL MONITORING AND ANALYTICAL
REQUIREMENTS
Section
611 .720
Analytical Methods
611 .731
Gross Alpha
611
.732
Beta Particle and Photon Radioactivity
611.733
General Monitoring and Compliance Requirements
SUBPART R: ENHANCED FILTRATION AND DISINFECTION
: SYSTEMS
THAT SERVE 10,000 OR MORE PEOPLE
Section
611
.740
General Requirements
611 .741
Standards for Avoiding Filtration
611
.742
Disinfection Profiling and Benchmarking
611 .743
Filtration
611 .744
Filtration Sampling Requirements
611 .745
Reporting and Recordkeeping Requirements
SUBPART T
: REPORTING AND RECORDKEEPING
Section
611
.830
Applicability
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
611 .831
Monthly Operating Report
611 .832
Notice by Agency (Repealed)
611 .833
Cross Connection Reporting
611 .840
Reporting
611 .851
Reporting MCL, MRDL, and other Violations (Repealed)
611 .852
Reporting other Violations (Repealed)
611.853
Notice to New Billing Units (Repealed)
611 .854
General Content of Public Notice (Repealed)
611 .855
Mandatory Health Effects Language (Repealed)
611 .856
Fluoride Notice (Repealed)
611 .858
Fluoride Secondary Standard (Repealed)
611 .860
Record Maintenance
611 .870
List of 36 Contaminants (Repealed)
SUBPART U: CONSUMER CONFIDENCE REPORTS
Section
611 .881
Purpose and Applicability
611 .882
Compliance Dates
611 .883
Content of the Reports
611 .884
Required Additional Health Information
611 .885
Report Delivery and Recordkeeping
SUBPART V
: PUBLIC NOTIFICATION OF DRINKING WATER
VIOLATIONS
Section
611 .901
General Public Notification Requirements
611 .902
Tier 1 Public Notice
: Form, Manner, and Frequency of Notice
611 .903
Tier 2 Public Notice
: Form, Manner, and Frequency of Notice
611 .904
Tier 3 Public Notice
: Form, Manner, and Frequency of Notice
611 .905
Content of the Public Notice
611 .906
Notice to New Billing Units or New Customers
611
.907
Special Notice of the Availability of Unregulated Contaminant Monitoring
Results
611
.908
Special Notice for Exceedence of the Fluoride Secondary Standard
611
.909
Special Notice for Nitrate Exceedences above the MCL by a Non-Community
Water System
611 .910
Notice by the Agency on Behalf of a PWS
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
SUBPART X : ENHANCED FILTRATION AND DISINFECTION--SYSTEMS
SERVING FEWER THAN 10,000 PEOPLE
Section
611 .950
General Requirements
611 .951
Finished Water Reservoirs
611 .952
Additional Watershed Control Requirements for Unfiltered Systems
611 .953
Disinfection Profile
611 .954
Disinfection Benchmark
611
.955
Combined Filter Effluent Turbidity Limits
611 .956
Individual Filter Turbidity Requirements
611 .957
Reporting and Recordkeeping Requirements
61 I . Appendix A
Regulated Contaminants
611 . Appendix B
Percent Inactivation of G . Lamblia Cysts
611 .Appendix C
Common Names of Organic Chemicals
611 .Appendix D
Defined Substrate Method for the Simultaneous Detection of Total
Coliforms and Eschericia Coli from Drinking Water
611 . Appendix E
Mandatory Lead Public Education Information for Community Water
Systems
611 .Appendix F
Mandatory Lead Public Education Information for Non-Transient Non-
Community Water Systems
611 . Appendix G
NPDWR Violations and Situations Requiring Public Notice
611 .Appendix H
Standard Health Effects Language for Public Notification
611 . Appendix I
Acronyms Used in Public Notification Regulation
611 .Table A
Total Coliform Monitoring Frequency
611 .Table B
Fecal or Total Coliform Density Measurements
611 .Table C
Frequency of RDC Measurement
611
. Table D
Number of Lead and Copper Monitoring Sites
61 1 .Table E
Lead and Copper Monitoring Start Dates
611 .Table F
Number of Water Quality Parameter Sampling Sites
611 .Table G
Summary of Section 611 .357 Monitoring Requirements for Water Quality
Parameters
611 .Table Z
Federal Effective Dates
AUTHORITY : Implementing Sections 7 .2, 17, and 17
.5 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/7
.2, 17, 17.5, and 27] .
SOURCE
: Adopted in R88-26 at 14111 . Reg
. 16517, effective September 20, 1990 ; amended in
R90-21 at 14111 . Reg
. 20448, effective December 11, 1990 ; amended in R90-13 at 15111
. Reg .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1562, effective January 22, 1991 ; amended in R91-3 at 16 Ill . Reg. 19010, effective December 1,
1992
; amended in R92-3 at 17111 . Reg. 7796, effective May 18, 1993 ; amended in R93-1 at 17111 .
Reg. 12650, effective July 23, 1993
; amended in R94-4 at 18111 . Reg . 12291, effective July 28,
1994
; amended in R94-23 at 19111
. Reg
. 8613, effective June 20, 1995 ; amended in R95-17 at 20
Ill. Reg. 14493, effective October 22, 1996; amended in R98-2 at 22 Ill
. Reg. 5020, effective
March 5, 1998 ; amended in R99-6 at 23 Ill . Reg. 2756, effective February 17, 1999
; amended in
R99-12 at 23 Ill. Reg
. 10348, effective August 11, 1999 ; amended in R00-8 at 23 111 . Reg. 14715,
effective December 8, 1999
; amended in R00-10 at 24111 . Reg. 14226, effective September 11,
2000; amended in R01-7 at 25111
. Reg . 1329, effective January 11, 2001 ; amended in R01-20 at 25
Ill . Reg. 13611, effective October 9, 2001 ; amended in R02-5 at 26111
. Reg. 3522, effective
February 22, 2002; amended in R03-4 at 27 Ill . Reg. 1183, effective January 10, 2003
; amended
in R03-15 at 27 Ill . Reg. 16447, effective October 10, 2003
; amended in R04-3 at 28 Ill . Reg.
5269, effective March 10, 2004
; amended in R04-13 at 28111 . Reg. 12666, effective August 26,
2004; amended in R05-6 at 29 Ill . Reg. 2287, effective January 28, 2005
; amended in R06-15 at
30 Ill. Reg. , effective SUBPART
A: GENERAL
Section 611 .102
Incorporations by Reference
a)
Abbreviations and short-name listing of references
. The following names and
abbreviated names, presented in alphabetical order, are used in this Part to refer to
materials incorporated by reference :
"Amco-AEPA-1 Polymer" is available from Advanced Polymer Systems .
"ASTM Method" means a method published by and available from the
American Society for Testing and Materials (ASTM) .
"Colisure Test" means "Colisure Presence/Absence Test for Detection and
Identification of Coliform Bacteria and Escherichia Coli in Drinking
Water," available from Millipore Corporation, Technical Services
Department .
"Colitag® Test" means "Colitag® Product as a Test for Detection and
Identification of Coliforms and E
. coli Bacteria in Drinking Water and
Source Water as Required in National Primary Drinking Water
Regulations," available from CPI International
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Dioxin and Furan Method 1613" means "Tetra- through Octa-
Chlorinated Dioxins and Furans by Isotope-Dilution HRGC/FIRMS,"
available from NTIS
.
"GLI Method 2" means GLI Method 2, "Turbidity," Nov
. 2, 1992,
available from Great Lakes Instruments, Inc
.
"Hach FilterTrak Method 10133" means "Determination of Turbidity by
Laser Nephelometry," available from Hach Co .
"HASL Procedure Manual" means HASL Procedure Manual, HASL 300,
available from ERDA Health and Safety Laboratory .
"Kelada 01" means "Kelada Automated Test Methods for Total Cyanide,
Acid Dissociable Cyanide, And Thiocyanate," Revision 1
.2, August 2001,
EPA # 821-B-01-009, available from the National Technical Information
Service (NTIS) .
"Membrane Filter Technique using Chromocult Doliform Agar" means
"Chromocult Coliform Agar Presence/Absence Membrane Filter Test
Method for Detection and Identification of Coliform Bacteria and
Escherichia coli in Finished Waters," available from EMD Chemicals Inc .
"NCRP" means "National Council on Radiation Protection
."
"NTIS" means "National Technical Information Service
."
"New Jersey Radium Method" means "Determination of Radium 228 in
Drinking Water," available from the New Jersey Department of
Environmental Protection .
"New York Radium Method" means "Determination of Ra-226 and Ra-
228 (Ra-02)," available from the New York Department of Public Health
.
"ONGP-MUG Test" (meaning "minimal medium ortho-nitrophenyl-beta-
d-galactopyranoside-4-methyl-umbelliferyl-beta-d-glucuronide test"), also
called the "Autoanalysis Colilert System," is Method 9223, available in
"Standard Methods for the Examination of Water and Wastewater," 18th
ed.,
from American Public Health Association.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Palintest Method 1001" means "Method Number 1001," available from
Palintest, Ltd . or the Hach Company.
"QuikChem Method 10-204-00-1-X" means "Digestion
and distillation
of total cyanide in drinking and wastewaters using MICRO DIST and
determination of cyanide by flow injection analysis," available from
Lachat Instruments .
"Readycult Coliforms 100 Presence/Absence Test" means
"Readycult
Coliforms 100 Presence/Absence Test for Detection and
Identification of
Coliform Bacteria and Escherichia coli in Finished Waters,"
available
from EMD Chemicals Inc .
"SimPlate Method" means "IDEXX SimPlate TM HPC Test Method
for
Heterotrophs in Water," available from IDEXX Laboratories,
Inc
.
"Radiochemical Methods" means "Interim Radiochemical
Methodology
for Drinking Water," available from NTIS .
"Standard Methods" means "Standard Methods for the Examination of
Water and Wastewater," available from the American Public Health
Association or the American Waterworks Association
.
"Syngenta AG-625" means "Atrazine in Drinking Water by
Immunoassay," February 2001 is available from Syngenta
Crop Protection,
Inc.
"Technical Bulletin 601" means "Technical Bulletin 601,
Standard
Method of Testing for Nitrate in Drinking Water," July
1994, available
from Analytical Technology, Inc
.
"Technicon Methods" means "Fluoride in Water and Wastewater,"
available from Bran & Luebbe
.
"USDOE Manual" means "EML Procedures Manual," available from the
United State Department of Energy
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"USEPA Asbestos Methods-100 .1" means Method 100 .1, "Analytical
Method for Determination of Asbestos Fibers in Water," September 1983,
available from NTIS.
"USEPA Asbestos Methods-100 .2" means Method 100 .2, "Determination
of Asbestos Structures over 10-mm in Length in Drinking Water," June
1994, available from NTIS .
"USEPA Environmental Inorganics Methods" means "Methods for the
Determination of Inorganic Substances in Environmental Samples,"
August 1993, available from NTIS .
"USEPA Environmental Metals Methods" means "Methods for the
Determination of Metals in Environmental Samples," available from
NTIS .
"USEPA Inorganic Methods" means "Methods for Chemical Analysis of
Water and Wastes," March 1983, available from NTIS
.
"USEPA Interim Radiochemical Methods" means "Interim Radiochemical
Methodology for Drinking Water," EPA 600/4-75-008 (revised), March
1976 . Available from NTIS.
"USEPA Organic Methods" means "Methods for the Determination of
Organic Compounds in Drinking Water," July 1991, for Methods 502
.2,
505, 507, 508, 508A, 515
.1, and 531 .1
; "Methods for the Determination of
Organic Compounds in Drinking Water--Supplement I," July 1990, for
Methods 506, 547, 550, 550 .1, and 551 ; and "Methods for the
Determination of Organic Compounds in Drinking Water--Supplement II,
August 1992, for Methods 515 .2, 524 .2, 548 .1, 549.1, 552 .1, and 555,
available from NTIS
. Methods 504.1, 508 .1, and 525.2 are available from
EPA EMSL
; "Methods for the Determination of Organic Compounds" in
Drinking Water--Supplement II, August 1992, for Method 552 .1 ; "Methods
for the Determination of Organic Compounds in Drinking Water--
Supplement III," August 1995, for Methods 502
.2, 524.2, 551 .1, and 552
.2.
Method 515
.4, "Determination of Chlorinated Acids in Drinking Water by
Liquid-Liquid Microextraction, Derivatization and Fast Gas
Chromatography with Electron Capture Detection," Revision 1
.0, April
2000, EPA 815/B-00/001, and Method 531
.2, "Measurement of N-
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
methylcarbamoyloximes and N-methylcarbamates in Water by Direct
Aqueous Injection HPLC with Postcolumn Derivatization, '
Revision 1 .0,
September 2001, EPA 815/B/01/002, are both available on-line from
USEPA, Office of Ground Water and Drinking Water .
"USEPA Radioactivity Methods" means "Prescribed Procedures for
Measurement of Radioactivity in Drinking Water," EPA 600/4-80-032,
August 1980 . Available from NTIS .
"USEPA Radiochemical Analyses" means "Radiochemical Analytical
Procedures for Analysis of Environmental Samples," March 1979
.
Available from NTIS .
"USEPA Radiochemistry Methods" means "Radiochemistry Procedures
Manual," EPA 520/5-84-006, December 1987 . Available from NTIS .
"USEPA Technical Notes" means "Technical Notes on Drinking Water
Methods," available from NTIS .
"USGS Methods" means "Methods of Analysis by the U .S
. Geological
Survey National Water Quality Laboratory--Determination of Inorganic
and Organic Constituents in Water and Fluvial Sediments," available from
NTIS and USGS.
"Waters Method B-1011" means "Waters Test Method for the
Determination of Nitrite/Nitrate in Water Using Single Column Ion
Chromatography," available from Waters Corporation, Technical Services
Division.
b)
The Board incorporates the following publications by reference
:
Advanced Polymer Systems, 3696 Haven Avenue, Redwood City, CA
94063 415-366-2626
.
Amco-AEPA-1 Polymer. See 40 CFR 141 .22(a)
(2003) (2005) .
Also, as referenced in ASTM D1889 .
American Public Health Association, 1015 Fifteenth Street NW,
Washington, DC 20005 800-645-5476 .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Standard Methods for the Examination of Water and
Wastewater," 17th Edition, 1989 (referred to as "Standard
Methods, 17th ed.").
"Standard Methods for the Examination of Water and
Wastewater," 18th Edition, 1992, including "Supplement to the
18th Edition of Standard Methods for the Examination of Water
and Wastewater," 1994 (collectively referred to
as "Standard
Methods, 18th ed.").
See the methods listed separately for the
same references under American Waterworks Association .
"Standard Methods for the Examination of Water and
Wastewater," 19th Edition, 1995 (referred to as "Standard
Methods, 19th ed.").
"Standard Methods for the Examination of Water and
Wastewater," 20th Edition, 1998 (referred to as "Standard
Methods, 20th ed.").
American Waterworks Association et al
., 6666 West Quincy Ave .,
Denver, CO 80235 303-794-7711
.
"National Field Evaluation of a Defined Substrate Method for the
Simultaneous Enumeration of Total Coliforms and Escherichia coli
for Drinking Water
: Comparison with the Standard Multiple Tube
Fermentation Method," S.C
. Edberg, M .J. Allen & D .B . Smith,
Applied Environmental Microbiology, vol . 54, iss. 6, pp 1595-
1601 (1988).
"Standard Methods for the Examination of Water and
Wastewater," 13th Edition, 1971 (referred to as "Standard
Methods, 13th ed.").
Method 302, Gross Alpha and Gross Beta Radioactivity in
Water (Total, Suspended, and Dissolved)
.
Method 303, Total Radioactive Strontium and Strontium 90
in Water.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 304, Radium in Water by Precipitation
.
Method 305, Radium 226 by Radon in Water (Soluble,
Suspended, and Total) .
Method 306, Tritium in Water.
"Standard Methods for the Examination of Water and
Wastewater," 17th Edition, 1989 (referred to as "Standard
Methods, 17th ed.").
Method 7110 B, Gross Alpha and Gross Beta Radioactivity
in Water (Total, Suspended, and Dissolved).
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method.
Method 7500- 3H B, Tritium in Water .
Method 7500-I B, Radioactive Iodine, Precipitation
Method.
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method.
Method 7500-I D, Radioactive Iodine, Distillation Method
.
Method 7500-Ra B, Radium in Water by Precipitation
.
Method 7500-Ra C, Radium 226 by Radon in Water
(Soluble, Suspended, and Total)
.
Method 7500-Ra D, Radium, Sequential Precipitation
Method (Proposed)
.
Method 7500-Sr B, Total Radioactive Strontium and
Strontium 90 in Water .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 7500-U B, Uranium, Radiochemical Method
(Proposed)
.
Method 7500-U C, Uranium, Isotopic Method (Proposed) .
"Standard Methods for the Examination of Water and
Wastewater," 18th Edition, 1992 (referred to as "Standard
Methods, 18th ed.").
Method 2130 B, Turbidity, Nephelometric Method
.
Method 2320 B, Alkalinity, Titration Method .
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory and Field Methods .
Method 3111 B, Metals by Flame Atomic Absorption
Spectrometry, Direct Air-Acetylene Flame Method
.
Method 3111 D, Metals by Flame Atomic Absorption
Spectrometry, Direct Nitrous Oxide-Acetylene Flame
Method.
Method 3112 B, Metals by Cold-Vapor Atomic Absorption
Spectrometry, Cold-Vapor Atomic Absorption
Spectrometric Method .
Method 3113 B, Metals by Electrother mal Atomic
Absorption Spectrometry, Electrothermal Atomic
Absorption Spectrometric Method
.
Method 3114 B, Metals by Hydride Generation/Atomic
Absorption Spectrometry, Manual Hydride
Generation/Atomic Absorption Spectrometric Method
.
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 3500-Ca D, Calcium, EDTA Titrimetric Method .
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
Suppression of Eluent Conductivity .
Method 4500-CN- C, Cyanide, Total Cyanide after
Distillation.
Method 4500-CN" E, Cyanide, Colorimetric Method .
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
Method .
Method 4500-CN" G, Cyanide, Cyanides Amenable to
Chlorination after Distillation.
Method 4500-Cl D, Chlorine, Amperometric Titration
Method.
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method .
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method.
Method 4500-Cl I, Chlorine, lodometric Electrode Method .
Method 4500-C1O2 C, Chlorine Dioxide, Amperometric
Method I .
Method 4500-CIO2 D, Chlorine Dioxide, DPD Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-C102 E, Chlorine Dioxide, Amperometric
Method II (Proposed) .
Method 4500-F" B, Fluoride, Preliminary Distillation Step .
Method 4500-F-
C, Fluoride, Ion-Selective Electrode
Method.
Method 4500-F" D, Fluoride, SPADNS Method .
Method 4500-F" E, Fluoride, Complexone Method .
Method 4500-H+ B, pH Value, Electrometric Method .
Method 4500-NOZ B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3 D, Nitrogen (Nitrate), Nitrate Electrode
Method .
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method .
Method 4500-NO3 F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo
Calorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method .
Method 4500-Si D, Silica, Molybdosilicate Method.
Method 4500-Si E, Silica, Heteropoly Blue Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-Si F, Silica, Automated Method for
Molybdate-Reactive Silica .
Method 6651, Glyphosate Herbicide (Proposed)
.
Method 7110 B, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Evaporation Method for
Gross Alpha-Beta-
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method .
Method
7500_3H
B, Tritium, Liquid Scintillation
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation
Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method .
Method 7500-I D, Radioactive Iodine, Distillation
Method.
Method 7500-Ra B, Radium, Precipitation Method
.
Method 7500-Ra C, Radium, Emanation Method
.
Method 7500-Ra D, Radium, Sequential Precipitation
Method (Proposed) .
Method 7500-Sr B, Total Radioactive Strontium and
Strontium 90, Precipitation Method.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 7500-U B, Uranium, Radiochemical Method
(Proposed) .
Method 7500-U C, Uranium, Isotopic Method (Proposed) .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method.
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique
.
Method 9221 C, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density .
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test
.
Method 9221 E, Multiple-Tube Fermentation Technique for
Members of the Coliform Group, Fecal Coliform
Procedure .
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction .
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure .
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure.
Method 9223, Chromogenic Substrate Coliform Test
(Proposed) .
"Supplement to the 18th Edition of Standard Methods for the
Examination of Water and Wastewater," American Public Health
Association, 1994 .
Method 6610, Carbamate Pesticide Method .
"Standard Methods for the Examination of Water and
Wastewater," 19th Edition, 1995 (referred to as "Standard
Methods, 19th
ed.")
.
Method 2130 B, Turbidity, Nephelometric Method
.
Method 2320 B, Alkalinity, Titration Method
.
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory, and Field
Methods.
Method 3111 B, Metals by Flame Atomic Absorption
Spectrometry, Direct Air-Acetylene Flame Method .
Method 3111 D, Metals by Flame Atomic Absorption
Spectrometry, Direct Nitrous Oxide-Acetylene Flame
Method .
Method 3112 B, Metals by Cold-Vapor Atomic Absorption
Spectrometry, Cold-Vapor Atomic Absorption
Spectrometric Method.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 3113 B, Metals by Electrothermal Atomic
Absorption Spectrometry, Electrothermal Atomic
Absorption Spectrometric Method .
Method 3114 B, Metals by Hydride Generation/Atomic
Absorption Spectrometry, Manual Hydride
Generation/Atomic Absorption Spectrometric Method .
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method .
Method 3500-Ca D, Calcium, EDTA Titrimetric Method.
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
Suppression of Eluent Conductivity .
Method 4500-Cl D, Chlorine, Amperometric Titration
Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method
.
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method
.
Method 4500-Cl G, Chlorine, DPD Colorimetric Method .
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method .
Method 4500-Cl I, Chlorine, Iodometric Electrode Method .
Method 4500-CIO2
C, Chlorine Dioxide, Amperometric
Method I .
Method 4500-CIO2 D, Chlorine Dioxide, DPD Method.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-ClO2 E, Chlorine Dioxide, Amperometric
Method II (Proposed) .
Method 4500-CN C, Cyanide, Total Cyanide after
Distillation.
Method 4500-CN- E, Cyanide, Colorimetric Method.
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
Method .
Method 4500-CN- G, Cyanide, Cyanides Amenable to
Chlorination after Distillation.
Method 4500-F - B, Fluoride, Preliminary Distillation Step
.
Method 4500-F" C, Fluoride, Ion-Selective Electrode
Method.
Method 4500-F" D, Fluoride, SPADNS Method .
Method 4500-F" E, Fluoride, Complexone Method
.
Method 4500-H' B, pH Value, Electrometric Method
.
Method 4500-NO3 B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3 D, Nitrogen (Nitrate), Nitrate Electrode
Method.
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method.
Method 4500-NO3 F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo
Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method.
Method 4500-Si D, Silica, Molybdosilicate Method .
Method 4500-Si E, Silica, Heteropoly Blue Method.
Method 4500-Si F, Silica, Automated Method for
Molybdate-Reactive Silica
.
Method 5910 B, UV Absorbing Organic Constituents,
Ultraviolet Absorption Method .
Method 6251 B, Disinfection Byproducts
: Haloacetic Acids
and Trichlorophenol, Micro Liquid-Liquid Extraction Gas
Chromatographic Method .
Method 6651, Glyphosate Herbicide (Proposed)
.
Method 7110 B, Gross Alpha and Gross Beta Radioactivity,
Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
Method 7120 B, Gamma-Emitting Radionuclides, Gamma
Spectrometric Method
.
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 7500-3H B, Tritium, Liquid Scintillation
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation
Method.
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method.
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method
.
Method 7500-Ra D, Radium, Sequential Precipitation
Method.
Method 7500-Sr B, Total Radiactive Strontium and
Strontium 90, Precipitation Method .
Method 7500-U B, Uranium, Radiochemical Method.
Method 7500-U C, Uranium, Isotopic Method .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method.
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique .
Method 9221 C, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test.
Method 9221 E, Multiple-Tube Fermentation Technique for
Members of the Coliform Group, Fecal Coliform
Procedure.
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction .
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure .
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure.
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure.
Method 9223, Chromogenic Substrate Coliform Test
(Proposed) .
"Supplement to the 19th Edition of Standard Methods for the
Examination of Water and Wastewater," American Public Health
Association, 1996 .
Method 5310 B, TOC, Combustion-Infrared Method .
Method 5310 C, TOC, Persulfate-Ultraviolet Oxidation
Method.
Method 5310 D, TOC, Wet-Oxidation Method
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Standard Methods for the Examination of Water and
Wastewater," 20th Edition, 1998 (referred to as "Standard
Methods, 20th ed.").
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method .
Method 2510 B, Conductivity, Laboratory Method
.
Method 2550, Temperature, Laboratory, and Field
Methods.
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method .
Method 3500-Ca B, Calcium, EDTA Titrimetric Method
.
Method 3500-Mg B, Magnesium, EDTA Titrimetric
Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
Suppression of Eluent Conductivity .
Method 4500-CW C, Cyanide, Total Cyanide after
Distillation.
Method 4500-CN E, Cyanide, Colorimetric Method .
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
Method .
Method 4500-CN" G, Cyanide, Cyanides Amenable to
Chlorination after Distillation
.
Method 4500-Cl D, Chlorine, Amperometric Titration
Method.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method .
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method.
Method 4500-Cl I, Chlorine, Iodometric Electrode Method .
Method 4500-CIO2 C, Chlorine Dioxide, Amperometric
Method I .
Method 4500-CIO2 D, Chlorine Dioxide, DPD Method.
Method 4500-C1O2 E, Chlorine Dioxide, Amperometric
Method II (Proposed)
.
Method 4500-F- B, Fluoride, Preliminary Distillation Step
.
Method 4500-F - C, Fluoride, Ion-Selective Electrode
Method
.
Method 4500-F- D, Fluoride, SPADNS Method .
Method 4500-F" E, Fluoride, Complexone Method .
Method 4500-H' B, pH Value, Electrometric Method .
Method 4500-NO2 B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3 D, Nitrogen (Nitrate), Nitrate Electrode
Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method .
Method 4500-NO3 F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo
Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method .
Method 4500-Si C, Silica, Molybdosilicate Method .
Method 4500-Si D, Silica, Heteropoly Blue Method .
Method 4500-Si E, Silica, Automated Method for
Molybdate-Reactive Silica
.
Method 4500-Cl E, Chlorine (Residual), Low-Level
Amperometric Titration Method .
Method 4500-Cl F, Chlorine (Residual), DPD Ferrous
Titrimetric Method
.
Method 4500-Cl G, Chlorine (Residual), DPD Colorimetric
Method.
Method 4500-Cl H, Chlorine (Residual), Syringaldazine
(FACTS) Method
.
Method 4500-Cl I, Chlorine (Residual), Iodometric
Electrode Technique
.
Method 4500-CIO2
D, Chlorine Dioxide, DPD Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 4500-C1O2 E, Chlorine Dioxide, Amperometric
Method II.
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110-B, Gross Alpha and Gross Beta
Radioactivity, Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
Method 7120-B, Gamma-Emitting Radionuclides, Gamma
Spectrometric Method.
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method
.
Method 7500-3H B, Tritium, Liquid Scintillation
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation
Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method .
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Sr B, Total Radiactive Strontium and
Strontium 90, Precipitation Method .
Method 7500-U B, Uranium, Radiochemical Method .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 7500-U C, Uranium, Isotopic Method .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method.
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique.
Method 9221 C, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density.
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique for
Members of the Coliform Group, Fecal Coliform
Procedure.
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction
.
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure.
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure.
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 9223, Chromogenic Substrate Coliform Test
(Proposed).
Analytical Technology, Inc. ATI Orion, 529 Main Street, Boston, MA
02129.
Technical Bulletin 601, "Standard Method of Testing for Nitrate in
Drinking Water," July, 1994, PN 221890-001 (referred to as
"Technical Bulletin 601")
.
ASTM
. American Society for Testing and Materials, 100 Barr Harbor
Drive, West Conshohocken, PA 19428-2959 610-832-9585 .
ASTM Method D511-93 A and B, "Standard Test Methods for
Calcium and Magnesium in Water," "Test Method A--
Complexometric Titration" & "Test Method B--Atomic
Absorption Spectrophotometric," approved 1993 .
ASTM Method D515-88 A, "Standard Test Methods for
Phosphorus in Water," "Test Method A--Colorimetric Ascorbic
Acid Reduction," approved August 19, 1988 .
ASTM Method D859-88, "Standard Test Method for Silica in
Water," approved August 19, 1988 .
ASTM Method D1067-92 B, "Standard Test Methods for Acidity
or Alkalinity in Water," "Test Method B--Electrometric or Color-
Change Titration," approved May 15, 1992
.
ASTM Method Dl 125-91 A, "Standard Test Methods for
Electrical Conductivity and Resistivity of Water," "Test Method
A--Field and Routine Laboratory Measurement of Static (Non-
Flowing) Samples," approved June 15, 1991
.
ASTM Method Dl 179-93 B, "Standard Test Methods for Fluoride
in Water," "Test Method B--Ion Selective Electrode," approved
1993.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
ASTM Method D1253-86, "Standard Test Method for Residual
Chlorine in Water," reapproved 1992 .
ASTM Method D1293-84, "Standard Test Methods for pH of
Water," "Test Method A--Precise Laboratory Measurement" &
"Test Method B--Routine or Continuous Measurement," approved
October 26, 1984 .
ASTM Method D1688-90 A or C, "Standard Test Methods for
Copper in Water," "Test Method A--Atomic Absorption, Direct" &
"Test Method C--Atomic Absorption, Graphite Furnace," approved
March 15, 1990 .
ASTM Method D2036-91 A or B, "Standard Test Methods for
Cyanide in Water," "Test Method A--Total Cyanides after
Distillation" & "Test Method B--Cyanides Amenable to
Chlorination by Difference," approved September 15, 1991 .
ASTM Method D2459-72, "Standard Test Method for Gamma
Spectrometry in Water," approved July 28, 1972, discontinued
1988.
ASTM Method D2460-90, "Standard Test Method for
Radionuclides of Radium in Water," approved 1990 .
ASTM Method D2907-91, "Standard Test Methods for
Microquantities of Uranium in Water by Fluorometry," "Test
Method A--Direct Fluorometric" & "Test Method B-Extraction,"
approved June 15, 1991 .
ASTM Method D2972-93 B or C, "Standard Test Methods for
Arsenic in Water," "Test Method B--Atomic Absorption, Hydride
Generation" & "Test Method C--Atomic Absorption, Graphite
Furnace," approved 1993 .
ASTM Method D3223-91, "Standard Test Method for Total
Mercury in Water," approved September 23, 1991
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
ASTM Method D3454-91, "Standard Test Method for Radium-226
in Water," approved 1991 .
ASTM Method D3559-90 D, "Standard Test Methods for Lead in
Water," "Test Method D--Atomic Absorption, Graphite Furnace,"
approved August 6, 1990 .
ASTM Method D3645-93 B, "Standard Test Methods for
Beryllium in Water," "Method B--Atomic Absorption, Graphite
Furnace," approved 1993 .
ASTM Method D3649-91, "Standard Test Method for High-
Resolution Gamma-Ray Spectrometry of Water," approved 1991
.
ASTM Method D3697-92, "Standard Test Method for Antimony in
Water," approved June 15, 1992 .
ASTM Method D3859-93 A, "Standard Test Methods for
Selenium in Water," "Method A--Atomic Absorption, Hydride
Method," approved 1993 .
ASTM Method D3867-90 A and B, "Standard Test Methods for
Nitrite-Nitrate in Water," "Test Method A--Automated Cadmium
Reduction" & "Test Method B--Manual Cadmium Reduction,"
approved January 10, 1990 .
ASTM Method D3972-90, "Standard Test Method for Isotopic
Uranium in Water by Radiochemistry," approved 1990
.
ASTM Method D4107-91, "Standard Test Method for Tritium in
Drinking Water," approved 1991 .
ASTM Method D4327-91, "Standard Test Method for Anions in
Water by Ion Chromatography," approved October 15, 1991 .
ASTM Method D4785-88, "Standard Test Method for Low-Level
Iodine-131 in Water," approved 1988 .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
ASTM Method D5174-91, "Standard Test Method for Trace
Uranium in Water by Pulsed-Laser Phosphorimetry," approved
1991 .
ASTM Method D5673-03, "Standard Test Method for Elements in
Water by Inductively Coupled Plasma-Mass Spectrometry,"
approved 2003 .
Bran & Luebbe, 1025 Busch Parkway, Buffalo Grove, IL 60089 .
"Fluoride in Water and Wastewater," Industrial Method #129-
71W, December 1972 (referred to as "Technicon Methods :
Method #129-71W") . See 40 CFR 141 .23(k)(1), footnote 11
(2003) (2005).
"Fluoride in Water and Wastewater," #380-75 WE, February 1976
(referred to as "Technicon Methods : Method #380-75WE") . See
40 CFR 141
.23(k)(1), footnote 11 (2003) (2005) .
CPI International, Inc ., 5580 Skylane Blvd . Santa Rosa,
CA 95403 .
Telephone : 800-878-7654 . Fax
: 707-545-7901 . Internet address :
www.cpiintemational.com
.
"Colitag® Product as a Test for Detection and Identification of
Coliforms and E . coli Bacteria in Drinking Water and Source
Water as Required in National Primary Drinking Water
Regulations," August 2001 .
EMD Chemicals Inc . (an affiliate of Merck KGgA, Darmstadt, Germany),
480 S . Democrat Road, Gibbstown, NJ 08027-1297 .
Telephone: 800-
222-0342 . E-mail: adellenbusch@emscience
.com.
"Chromocult Coliform Agar Presence/Absence Membrane
Filter
Test Method for Detection and Identification of Coliform Bacteria
and Escherichia coli in Finished Waters," November 2000, Version
1 .0.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Readycult Coliforms 100 Presence/Absence Test for Detection
and Identification of Coliform Bacteria and Escherichia coli in
Finished Waters," November 2000, Version 1 .0.
ERDA Health and Safety Laboratory, New York, NY.
HASL Procedure Manual, HASL 300, 1973 . See 40 CFR
141 .25(b)(2) "~ (2005) .
Great Lakes Instruments, Inc ., 8855 North 55th Street, Milwaukee, WI
53223 .
GLI Method 2, "Turbidity," Nov . 2, 1992.
The Hach Company, P .O. Box 389, Loveland, CO 80539-0389
. Phone:
800-227-4224 .
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
"Determination of Turbidity by Laser Nephelometry," January
2000, Revision 2 .0 (referred to as "Hach FilterTrak Method
10133").
IDEXX Laboratories, Inc ., One IDEXX Drive, Westbrook, Maine 04092
.
Telephone : 800-321-0207 .
"IDEXX SimPlate TM HPC Test Method for Heterotrophs in
Water," November 2000 .
Lachat Instruments, 6645 W . Mill Rd
., Milwaukee, WI 53218 . Phone :
414-358-4200.
"Digestion and distillation of total cyanide in drinking and
wastewaters using MICRO DIST and determination of cyanide by
flow injection analysis," Revision 2 .1, November 30, 2000
(referred to as "QuikChem Method 10-204-00-1-X") .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Millipore Corporation, Technical Services Department, 80 Ashby Road,
Milford, MA 01730 800-654-5476 .
Colisure Presence/Absence Test for Detection and Identification of
Coliform Bacteria and Escherichia Coli in Drinking Water,
February 28, 1994 (referred to as "Colisure Test") .
NCRP . National Council on Radiation Protection, 7910 Woodmont Ave .,
Bethesda, MD 301-657-2652 .
"Maximum Permissible Body Burdens and Maximum Permissible
Concentrations of Radionuclides in Air and in Water for
Occupational Exposure," NCRP Report Number 22, June 5, 1959 .
NSF . National Sanitation Foundation International, 3475 Plymouth Road,
PO Box 130140, Ann Arbor, Michigan 48113-0140, 734-769-8010 .
NSF Standard 61, section 9, November 1998 .
NTIS. National Technical Information Service, U .S
. Department of
Commerce, 5285 Port Royal Road, Springfield, VA 22161, 703-487-4600
or 800-553-6847 .
"Interim Radiochemical Methodology for Drinking Water," EPA
600/4-75-008 (revised), March 1976 (referred to as "USEPA
Interim Radiochemical Methods") . (Pages 1, 4, 6, 9, 13, 16, 24,
29,34)
"Kelada Automated Test Methods for Total Cyanide, Acid
Dissociable Cyanide, And Thiocyanate," Revision 1 .2, August
2001, EPA # 821-B-01-009 (referred to as "Kelada 01") .
"Maximum Permissible Body Burdens and Maximum Permissible
Concentrations of Radionuclides in Air and in Water for
Occupational Exposure," NBS (National Bureau of Standards)
Handbook 69, as amended August 1963, U .S
. Department of
Commerce .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Method 100.1, "Analytical Method for Determination of Asbestos
Fibers in Water," EPA-600/4-83-043, September 1983, Doc . No.
PB83-260471 (referred to as "USEPA Asbestos Methods-100
.1").
Method 100.2, "Determination of Asbestos Structures over 10-mm
in Length in Drinking Water," EPA-600/4-83-043, June 1994, Doc .
No. PB94-201902 (referred to as "USEPA Asbestos Methods-
100.2").
"Methods for Chemical Analysis of Water and Wastes," March
1983, Doc. No . PB84-128677 (referred to as "USEPA Inorganic
Methods"). (Methods 150.1, 150 .2, and 245.2, which formerly
appeared in this reference, are available from USEPA EMSL .)
"Methods for the Determination of Inorganic Substances in
Environmental Samples," August 1993, PB94-120821 (referred to
as "USEPA Environmental Inorganic Methods").
"Methods for the Determination of Metals in Environmental
Samples," June 1991, Doc . No. PB91-231498 and "Methods for
the Determination of Metals in Environmental Samples--
Supplement I," May 1994, PB95-125472 (referred to as "USEPA
Environmental Metals Methods").
"Methods for the Determination of Organic Compounds in
Drinking Water," December 1988, revised July 1991, EPA-600/4-
88/039 (referred to as "USEPA Organic Methods")
. (For methods
502.2, 505, 507, 508, 508A, 515 .1, and 531 .1
.)
"Methods for the Determination of Organic Compounds in
Drinking Water--Supplement I," July 1990, EPA/600-4-90-020
(referred to as "USEPA Organic Methods")
. (For methods 506,
547, 550, 550 .1, and 551 .)
"Methods for the Determination of Organic Compounds in
Drinking Water--Supplement II," August 1992, EPA-600/R-92-129
(referred to as "USEPA Organic Methods")
. (For methods 515 .2,
524.2, 548 .1, 549.1, 552 .1, and 555.)
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
"Prescribed Procedures for Measurement of Radioactivity in
Drinking Water," EPA 600/4-80-032, August 1980 (document
number PB 80-224744) (referred to as "USEPA Radioactivity
Methods") . (Methods 900, 901, 901 .1, 902, 903, 903 .1, 904, 905,
906, 908, 908 .1)
"Procedures for Radiochemical Analysis of Nuclear Reactor
Aqueous Solutions," H .L. Krieger and S . Gold, EPA-R4-73-014,
May 1973, Doc. No. PB222-154/7BA .
"Radiochemical Analytical Procedures for Analysis of
Environmental Samples," March 1979, Doc . No. EMSL LV
053917 (referred to as "USEPA Radiochemical Analyses")
. (Pages
1, 19, 33, 65, 87, 92)
"Radiochemistry Procedures Manual," EPA-520/5-84-006,
December 1987, Doc . No
. PB-84-215581 (referred to as "USEPA
Radiochemistry Methods") . (Methods 00-0 1, 00-02, 00-07, H-02,
Ra-03, Ra-04, Ra-05, Sr-04)
"Technical Notes on Drinking Water Methods," EPA-600/R-94-
173, October 1994, Doc . No. PB-104766 (referred to as "USEPA
Technical Notes") .
BOARD NOTE
: USEPA made the following assertion with regard
to this reference at 40 CFR 141 .23(k)(1) and 141 .24(e) and (n)(11)
(2003) (2005) : "This document contains other analytical test
procedures and approved analytical methods that remain available
for compliance monitoring until July 1, 1996 ."
"Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope
Dilution HRGC/HRMS," October 1994, EPA-821-B-94-005
(referred to as
"Dioxin and Furan Method 1613") .
New Jersey Department of Environment, Division of Environmental
Quality, Bureau of Radiation and Inorganic Analytical Services, 9 Ewing
Street, Trenton, NJ 08625 .
"Determination of Radium 228 in Drinking Water," August 1990
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
New York Department of Health, Radiological Sciences Institute, Center
for Laboratories and Research, Empire State Plaza, Albany, NY 12201 .
"Determination of Ra-226 and Ra-228 (Ra-02)," January 1980,
Revised June 1982 .
Palintest, Ltd ., 21 Kenton Lands Road, P .O. Box 18395, Erlanger, KY
800-835-9629.
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
Syngenta Crop Protection, Inc ., 410 Swing Road, Post Office Box 18300,
Greensboro, NC 27419 . Telephone : 336-632-6000.
"Atrazine in Drinking Water by Immunoassay," February 2001
(referred to as "Syngenta AG-625") .
United States Department of Energy, available at the Environmental
Measurements Laboratory, U
.S
. Department of Energy, 376 Hudson
Street, New York, NY 10014-3621 .
"EML Procedures Manual," 27th Edition, Volume 1, 1990 .
United States Environmental Protection Agency, Office of Ground Water
and Drinking Water, accessible on-line and available by download from
http://www.epa.gov/safewater/methods/.
Method 515 .4, "Determination of Chlorinated Acids in Drinking
Water by Liquid-Liquid Microextraction, Derivatization and Fast
Gas Chromatography with Electron Capture Detection," Revision
1 .0, April 2000, EPA 815/B-00/001 (document file name
"met515 4 .pdf') .
Method 531
.2, "Measurement of N-methylcarbamoyloximes and
N-methylcarbamates in Water by Direct Aqueous Injection HPLC
with Postcolumn Derivatization," Revision 1
.0, September 2001,
EPA 815/B/01/002 (document file name "met531 2 .pdf')
.
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
United States Environmental Protection Agency, EMSL, Cincinnati, OH
45268 513-569-7586.
"Interim Radiochemical Methodology for Drinking Water," EPA-
600/4-75-008 (referred to as "Radiochemical Methods") .
(Revised) March 1976 .
"Methods for the Determination of Organic Compounds in
Finished Drinking Water and Raw Source Water" (referred to as
"USEPA Organic Methods") . (For methods 504.1, 508 .1, and
525 .2 only .) See NTIS .
"Procedures for Radiochemical Analysis of Nuclear Reactor
Aqueous Solutions ." See NTIS .
USEPA, Science and Technology Branch, Criteria and Standards Division,
Office of Drinking Water, Washington, D .C. 20460.
"Guidance Manual for Compliance with the Filtration and
Disinfection Requirements for Public Water Systems using Surface
Water Sources," October 1989.
USGS. Books and Open-File Reports Section, United States Geological
Survey, Federal Center, Box 25286, Denver, CO 80225-0425 .
Methods available upon request by method number from "Methods
for Analysis by the U.S . Geological Survey National Water Quality
Laboratory--Determination of Inorganic and Organic Constituents
in Water and Fluvial Sediments," Open File Report 93-125, 1993,
or Book 5, Chapter A-1, "Methods for Determination of Inorganic
Substances in Water and Fluvial Sediments," 3rd ed
., Open-File
Report 85-495, 1989, as appropriate (referred to as "USGS
Methods").
1-1030-85
1-1062-85
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1-1601-85
1-1700-85
1-2598-85
1-2601-90
1-2700-85
1-3300-85
Methods available upon request by method number from "Methods
for Determination of Radioactive Substances in Water and Fluvial
Sediments," Chapter A5 in Book 5 of "Techniques of Water-
Resources Investigations of the United States Geological Survey,"
1997 .
R-1 110-76
R-1111-76
R-1120-76
R-1140-76
R-1141-76
R-1 142-76
R-1160-76
R-1171-76
R-1180-76
R-1181-76
R-1182-76
ILLINOIS
REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Waters Corporation, Technical Services Division, 34 Maple St
., Milford,
MA 01757 800-252-4752 .
"Waters Test Method for Determination of Nitrite/Nitrate in Water
Using Single Column Ion Chromatography," Method B-101 1,
August 1987 (referred to as "Waters Method B-101
1") .
c)
The Board incorporates the following federal regulations by reference
:
40 CFR 3 .2, as added at 70 Fed
. Reg. 59848 (Oct
. 13, 2005) (How Does
This Part Provide for Electronic Reporting?), referenced in Section
611 .105.
40 CFR 3
.3, as added at 70 Fed. Reg
. 59848 (Oct. 13, 2005) (What
Definitions Are Applicable to This Part?), referenced in Section 611
.105 .
40 CFR 3
.10, as added at 70 Fed . Reg
. 59848 (Oct. 13, 2005) (What Are
the Requirements for Electronic Reporting to EPA?), referenced in Section
611 .105.
40 CFR 3 .2000, as added at 70 Fed
. Reg
. 59848 (Oct. 13, 2005) (What Are
the Requirements Authorized State, Tribe, and Local Programs' Reporting
Systems Must Meet?), referenced in Section 611
.105.
Appendix B to 40 CFR 136,Appendices
B and C (2003) (2005),
reverenced in Sections 611 .359, 611
.609 & 611 .646.
d)
This Part incorporates no later amendments or editions
.
(Source
: Amended at 30 Ill . Reg.
, effective )
Section 611
.105
Electronic Reporting
The filing of any document pursuant to any provision of this Part as an electronic document is
subject to this Section .
a) Scope
and Applicability
.
ILLINOIS
REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1) The
USEPA, the Board, or the Agency may allow for the filing of
electronic documents
. This Section does not require submission of
electronic documents in lieu of paper documents
. This Section sets forth
the requirements for the optional electronic filing of any report or
document that must be submitted to the appropriate of the following_
A) To
USEPA directly under Title 40 of the Code of Federal
Regulations ; or
B) To the Board or the Agency pursuant to any provision of 35 Ill
.
Adm
. Code 702 through 705, 720 through 728, 730, 733, 738, or
739.
2) Electronic
document filing under this Section can begin only after USEPA
has first done as follows :
A) As
to filing with USEPA, USEPA has published a notice in the
Federal Register announcing that USEPA is prepared to receive
documents required or permitted by the identified part or subpart of
Title 40 of the Code of Federal Regulations in an electronic format
;
or
B) As
to filing with the State, USEPA has granted approval of any
electronic document receiving system established by the Board or
the Agency that meets the requirements of 40 CFR 3
.2000,
incorporated by reference in Section 611 .102(c).
3) This
Section does not apply to any of the following documents, whether or
not the document is a document submitted to satisfy the requirements cited
in subsection(a)(1)of this Section :
A) Any document submitted via fascimile
;
B) Any
document submitted via magnetic or optical media, such as
diskette, compact disc, digital video disc, or tape
; or
C) Any
data transfer between USEPA, any state, or any local
government and either the Board or the Agency as part of
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
administrative arrangements between the parties to the transfer to
share data.
4) Upon USEPA conferring approval for the filing of any types of documents
as electronic documents, as described in subsection (a)(2)(B)of this
Section, the Agency or the Board, as appropriate, must publish a Notice of
Public Information in the Illinois Register that describes the documents
approved for submission as electronic documents, the electronic document
receiving system approved to receive them, the acceptable formats and
procedures for their submission, and the date on which the Board or the
Agency will begin to receive those submissions . In the event of cessation
of USEPA approval or receiving any type of document as an electronic
document, the Board or the Agency must similarly cause publication of a
Notice of Public Information in the Illinois Register .
BOARD NOTE
: Subsection (a) of this Section is derived from 40 CFR 3
.1, as
added at 70 Fed
. Reg . 59848 (Oct . 13, 2005) .
b) Definitions
. For the purposes of this Section, terms will have the meaning
attributed them in 40 CFR 3
.3, incorporated by reference in 35 111 . Adm. Code
611 .102(c) .
c) Procedures for submission of electronic documents to USEPA
. Except as
provided in subsection (a)(3)of
this Section, any person who is required under
Title 40 of the Code of Federal Regulations to create and submit or otherwise
provide a document to USEPA may satisfy this requirement with an electronic
document, in lieu of a paper document, provided the following conditions are met :
1) The
person satisfies the requirements of 40 CFR 3.10, incorporated by
reference in Section 611
.102(c) ; and
2)
USEPA has first published a notice in the Federal Register as described in
subsection(a)(2)of this Section.
BOARD NOTE : Subsection (c) of this Section is derived from 40 CFR 3
.2(a) and
subpart B of 40 CFR 3,asadded at 70 Fed. Reg. 59848 (Oct
. 13, 2005) .
d) Procedures
for submission of electronic documents to the Board or the Agency .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1)
The Board or the Agency may, but is not required to, establish procedures
for the electronic submission of documents that meet the requirements of
40 CFR 3.2 and 3 .2000, incorporated by reference in Section 611
.102(c).
The Board or the Agency must establish any such procedures under the
Administrative Procedure Act f 5 ILCS 100/51
.
2)
The Board or the Agency may not accept electronic documents under this
Section until after USEPA has approved the procedures in writing, and the
Board or the Agency has published a notice of such approval in the Illinois
Register . Nothing in this subsection (d) limits the authority of the Board
or the Agency under the Illinois Environmental Protection Act r415 ILCS
51 to accept documents filed electronically.
BOARD NOTE : Subsection (d) of this Section is derived from 40 CFR 3
.2(b)
and subpart D of 40 CFR 3, as added at 70 Fed
. Reg. 59848 (Oct. 13, 2005) .
e) Effects of submission of an electronic document .
1) If a person who submits a document as an electronic document fails to
comply with the requirements this Section, that person is subiect to the
penalties prescribed for failure to comply with the requirement that the
electronic document was intended to satisfy.
2) Where a document submitted asan electronic document to satisfy a
reporting requirement bears an electronic signature, the electronic
signature legally binds, obligates, and makes the signer responsible to the
same extent as the signer's handwritten signature would on a paper
document submitted to satisfy the same reporting requirement
.
3) Proof
that a particular signature device was used to create an electronic
signature will suffice to establish that the individual uniquely entitled to
use the device did so with the intent to sign the electronic document and
give it effect .
4) Nothing
in this Section limits the use of electronic documents or
information derived from electronic documents as evidence in
enforcement or other proceedings .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
BOARD NOTE : Subsection (e) of this Section is derived from 40 CFR 3 .4 and
3 .2000(c) . as added at 70 Fed . Reg. 59848 (Oct . 13, 2005).
f) Public document subject to State laws . Any electronic document filed with the
Board is a public document . The document, its filing, its retention by the Board,
and its availability for public inspection and copying are subject to various State
laws, including, but not limited to, the following :
1) The Administrative Procedure Act [5 ILCS 100] ;
2) The Freedom of Information Act f 5 ILCS 1401
;
3) The
State Records Act [5 ILCS 160] ;
4) The
Electronic Commerce Security Act [5 ILCS 175] ;
5) The Environmental Protection Act [415 ILCS 5] ;
6) Regulations relating to public access to Board records (2 Ill
. Adm. Code
2175) ; and
7) Board procedural rules relating to protection of trade secrets and
confidential information (35 Ill . Adm. Code 130) .
g) Nothing in this Section or in any provisions adopted pursuant to subsection (c)(1)
of this Section will create any right or privilege to submit any document as an
electronic document
.
BOARD NOTE : Subsection (g) of this Section is derived from 40 CFR
3.2(c),as
added at 70 Fed . Reg. 59848 (Oct. 13, 2005).
BOARD NOTE : Derived from 40 CFR 3,asadded,
and 40 CFR 142 .10(g) (2005),as amended
at 70 Fed. Reg
. 59848 (Oct
. 13, 2005) .
(Source: Added at 30 Ill . Reg. , effective )
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
Section 611 .111
Relief Equivalent to SDWA Section 1415(a) Variances
This Section is intended to describe how the Board grants State relief equivalent to that available
from USEPA under section 1415(a)(1)(A) and (a)(1)(B) of the SDWA (42 USC 300g-4(a)(l)(A)
and (a)(1)(B))
. SDWA section 1415 variances do not require ultimate compliance within five
years in every situation . Variances under Sections 35-37 of the Act [415 ILCS 5/35-37] do
require compliance within five years in every case . Consequently, a PWS may have the option of
seeking State regulatory relief equivalent to a SDWA section 1415 variance through one of three
procedural mechanisms: a variance under Sections 35-37 of the Act [415 ILCS 5/35-37] and
Subpart B of 35 Ill. Adm. Code 104 ; a site-specific rule under Sections 27-28 of the Act [415
ILCS 5/27-28] and 35 111 . Adm. Code 102
; or an adjusted standard under Section 28 .1 of the Act
[415 ILCS 5/28
.1] and Subpart D of 35 Ill . Adm. Code 104.
a)
The Board will grant a PWS a variance, a site-specific rule, or an adjusted
standard from an MCL or a treatment technique pursuant to this Section .
1)
The PWS must file a petition pursuant to 35 Ill . Adm
. Code 102 or 104, as
applicable.
2)
If a State requirement does not have a federal counterpart, the Board may
grant relief from the State requirements without following this Section
.
b)
Relief from an MCL.
1)
As part of the justification for relief from an MCL under this Section, the
PWS must demonstrate the following:
A)
Because of characteristics of the raw water sources and alternative
sources that are reasonably available to the system, the PWS
cannot meet the MCL ; and
B)
The PWS will install or has installed the best available technology
(BAT) (as identified in Subpart F of this Part), treatment technique,
or other means that the Agency finds available
. BAT may vary
depending on the following :
i)
The number of persons served by the system
;
ii)
Physical conditions related to engineering feasibility
; and
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
iii)
Costs of compliance ; and
C)
The variance will not result in an unreasonable risk to health .
2)
In any order granting relief under this subsection, the Board will prescribe
a schedule for the following :
A)
Compliance, including increments of progress, by the PWS, with
each MCL with respect to which the relief was granted ; and
B)
Implementation by the PWS of each additional control measure for
each MCL with respect to which the relief is granted, during the
period ending on the date compliance with such requirement is
required .
3)
Schedule of compliance for relief from an MCL.
A)
A schedule of compliance will require compliance with each MCL
with respect to which the relief was granted as expeditiously as
practicable .
B)
If the Board prescribes a schedule requiring compliance with an
MCL for which the relief is granted later than five years from the
date of issuance of the relief, the Board will do the following :
i)
Document its rationale for the extended compliance
schedule;
ii)
Discuss the rationale for the extended compliance schedule
in the required public notice and opportunity for public
hearing; and
iii)
Provide the shortest practicable time schedule feasible under
the circumstances .
c)
Relief from a treatment technique requirement
.
0
g)
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
1)
As part of the justification for relief from a treatment technique
requirement under this Section, the PWS must demonstrate that the
treatment technique is not necessary to protect the health of persons served
because of the nature of the raw water source .
2)
The Board may prescribe monitoring and other requirements as a
condition for relief from a treatment technique requirement .
d)
The Board will hold at least one public hearing . In addition the Board will accept
comments as appropriate pursuant to 35 Ill . Adm. Code 102 or 104
.
e)
The Board will not grant relief from any of the following:
1)
From the MCL for total coliforms . However, the Board may grant a
variance from the total coliform MCL of Section 611 .325 for PWSs that
prove that the violation of the total coliform MCL is due to persistent
growth of total coliform in the distribution system, rather than from fecal
or pathogenic contamination, from a treatment lapse or deficiency, or from
a problem in the operation or maintenance of the distribution system .
2)
From any of the treatment technique requirements of Subpart B of this
Part.
3)
From the residual disinfectant concentration (RDC) requirements of
Sections 611 .241(c) and 611 .242(b).
The Agency must promptly send USEPA the opinion and order of the Board
granting relief pursuant to this Section . The Board may reconsider and modify a
grant of relief, or relief conditions, if USEPA notifies the Board of a finding
pursuant to section 1415 of the SDWA (42 USC 300g-4) .
In addition to the requirements of this Section, the provisions of Section 611
.130
or 611 .131 may apply to relief granted pursuant to this Section
.
BOARD NOTE
: Derived from 40 CFR 1414 (2002)12005),
from section 1415(a)(I)(A) and
(a)(1)(B)
of the SDWA and from the "Guidance Manual for Compliance with the Filtration and
Disinfection Requirements for Public Water Systems using Surface Water Sources,"-,
incorporated by reference in Section 611 .102
. USEPA has reserved the discretion to review and
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
modify or nullify Board determinations made pursuant to this Section at 40 CFR 142 .23 (2002)
(2005) .
(Source: Amended at 30 Ill . Reg. , effective )
SUBPART B : FILTRATION AND DISINFECTION
Section 611 .212
Groundwater under Direct Influence of Surface Water
The Agency shall, pursuant to Section 611
.201, require all CWSs to demonstrate whether they
are using "groundwater under the direct influence of surface water_"
. The Agency must
determine with information provided by the supplier whether a PWS uses "groundwater under
the direct influence of surface water" on an individual basis . The Agency must determine that a
groundwater source is under the direct influence of surface water based upon the following
:
a)
Physical characteristics of the source : whether the source is obviously a surface
water source, such as a lake or stream
. Other sources that may be subject to
influence from surface waters include
: springs, infiltration galleries, wells, or
other collectors in subsurface aquifers.
b)
Well construction characteristics and geology with field evaluation .
1)
The Agency may use the wellhead protection program's requirements,
which include delineation of wellhead protection areas, assessment of
sources of contamination and implementation of management control
systems, to determine if the wellhead is under the influence of surface
water.
2)
Wells less than or equal to 50 feet in depth are likely to be under the
influence of surface water .
3)
Wells greater than 50 feet in depth are likely to be under the influence of
surface water, unless they include the following :
A)
A surface sanitary seal using bentonite clay, concrete, or similar
material,
B)
A well casing that penetrates consolidated (slowly permeable)
material ; and
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C)
A well casing that is only perforated or screened below
consolidated (slowly permeable) material.
4)
A source that is less than 200 feet from any surface water is likely to be
under the influence of surface water .
c)
Any structural modifications to prevent the direct influence of surface water and
eliminate the potential for Giardia lamblia cyst contamination .
d)
Source water quality records . The following are indicative that a source is under
the influence of surface water :
1)
A record of total coliform or fecal coliform contamination in untreated
samples collected over the past three years ;
2)
A history ofturbidity problems associated with the source
; or
3)
A history of known or suspected outbreaks of Giardia lamblia,
Cryptosporidium or other pathogenic organisms associated with surface
water that has been attributed to that source .
e)
Significant and relatively rapid shifts in water characteristics such as turbidity,
temperature, conductivity, or pH
.
I)
A variation in turbidity of 0 .5 NTU or more over one year is indicative of
surface influence.
2)
A variation in temperature of 9-nine Fahrenheit degrees or more over one
year is indicative of surface influence.
f)
Significant and relatively rapid shifts in water characteristics such as turbidity,
temperature, conductivity, or pH that closely correlate to climatological or surface
water conditions are indicative of surface water influence
.
1)
Evidence of particulate matter associated with the surface water
; or
2)
Turbidity or temperature data that correlates to that of a nearby surface
water source .
g)
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Particulate analysis: Significant occurrence of insects or other macroorganisms,
algae, or large diameter pathogens such as Giardia lamblia is indicative of surface
influence .
1)
"Large diameter" particulates are those over 7-seven micrometers .
2)
Particulates must be measured as specified in the "Guidance Manual for
Compliance with the Filtration and Disinfection Requirements for Public
Water Systems using Surface Water Sources,"; incorporated by reference
in Section 611 .102.
h)
The potential for contamination by small-diameter pathogens, such as bacteria or
viruses, does not alone render the source "under the direct influence of surface
water.".
BOARD NOTE : Derived from the definition of "groundwater under the direct influence of
surface water" in 40 CFR 141 .2 (2002) (2005) ; from the Preamble at 54 Fed . Reg. 27489 (June
29, 1989)
; and from the USEPA "Guidance Manual for Compliance with the Filtration and
Disinfection Requirements for Public Water Systems using Surface Water Sources,",
incorporated by reference in Section 611 .102
.
(Source: Amended at 30 Ill . Reg
.
, effective )
SUBPART G: LEAD AND COPPER
Section 611 .359
Analytical Methods
Analyses for lead, copper, pH, conductivity, calcium, alkalinity, orthophosphate, silica, and
temperature must be conducted using the methods set forth in Section 611 .611(a).
a)
Analyses for lead and copper performed for the purposes of compliance with this
Subpart G must only be conducted by laboratories that have been certified by
USEPA or the Agency
. To obtain certification to conduct analyses for lead and
copper, laboratories must do the following :
1)
Analyze performance evaluation samples that include lead and copper
provided by USEPA Environmental Monitoring and Support Laboratory or
equivalent samples provided by the Agency ; and
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2)
Achieve quantitative acceptance limits as follows :
A)
For lead : ±30 percent of the actual amount in the performance
evaluation sample when the actual amount is greater than or equal
to 0.005 mg/f (the PQL for lead is 0.005 mg/f)
;
B)
For copper : ±10 percent of the actual amount in the performance
evaluation sample when the actual amount is greater than or equal
to 0.050
mg/f (the PQL for copper is 0 .050 mg/f) ;
C)
Achieve the method detection limit (MDL) for lead (0 .001 mg/Q, as
defined in Section 611 .350(a)) according to the procedures in 35
Ill. Adm. Code 186 and appendix B to 40 CFR 136, Appendix B:
"Definition and Procedure for the Determination of the Method
Detection Limit--Revision 1 .11" (2002) (2005), incorporated by
reference in Section 611 .102(c) .
This need only be accomplished
if the laboratory will be processing source water composite
samples under Section 611 .358(a)(1)(C)
; and
D)
Be currently certified by USEPA or the Agency to perform
analyses to the specifications described in subsection (a)(2) of this
Section
.
BOARD NOTE
: Subsection (a) is derived from 40 CFR 141 .89(a) and (a)(1)
(2002)(2005) .
b)
The Agency must, by a SEP issued pursuant to Section 611 .110, allow a supplier
to use previously collected monitoring data for the purposes of monitoring under
this Subpart G if the data were collected and analyzed in accordance with the
requirements of this Subpart G.
BOARD NOTE : Subsection (b) is derived from 40 CFR 141
.89(a)(2) (2002)
(2005) .
c)
Reporting lead and copper levels .
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1)
All lead and copper levels greater than or equal to the lead and copper
PQL (Pb 2:0.005 mg/f and Cu ? 0.050 mg/f) must be reported as
measured.
2)
All lead and copper levels measured less than the PQL and greater than the
MDL (0.005
mg/f > Pb > MDL and 0.050 mg/f > Cu > MDL) must be
either reported as measured or as one-half the PQL set forth in subsection
(a) of this Section
(i.e.,
reported
as
0.0025 mg/f for lead or 0
.025 mg/f for
copper).
3)
All lead and copper levels below the lead and copper MDL (MDL > Pb)
must be reported as zero.
BOARD NOTE : Subsection (c) is derived from 40 CFR 141 .89(a)(3) and
(a)(4)
(2002)(2005) .
(Source: Amended at 30 Ill . Reg
. ,
effective )
SUBPART I
: DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS, AND
DISINFECTION BYPRODUCT PRECURSORS
Section 611 .380
General Requirements
a)
The requirements of this Subpart I constitute NPDWRs .
1)
The regulations in this Subpart I establish standards under which a CWS
supplier or an NTNCWS supplier that adds a chemical disinfectant to the
water in any part of the drinking water treatment process or whichprevides
must modify its practices to
meet MCLs and MRDLs in Sections 611 .312 and 611
.313, respectively, and
must meet the treatment technique requirements for DBP precursors in
Section 611 .385.
2)
The regulations in this Subpart I establish standards under which a transient
non-CWS supplier that uses chlorine dioxide as a disinfectant or oxidant
must modify its practices to meet the MRDL for chlorine dioxide in Section
611 .313.
b)
Compliance dates.
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3)
The Board has established MCLs for TTHM and HAAS and treatment
technique requirements for DBP precursors to limit the levels of known
and unknown DBPs that may have adverse health effects . These DBPs
may include chloroform, bromodichloromethane, dibromochloromethane,
bromoform, dichloroacetic acid, and trichloroacetic acid .
1)
CWSs and NTNCWSs . Unless otherwise noted, a supplier must comply
with the requirements of this Subpart I as follows : A Subpart B system
supplier serving 10,000 or more persons must comply with this Subpart I
beginning January 1, 2002 . A Subpart B system supplier serving fewer
than 10,000 persons or a supplier using only groundwater not under the
direct influence of surface water must comply with this Subpart I
beginning January 1, 2004 .
2)
Transient non-CWSs. A Subpart B system supplier serving 10,000 or
more persons and using chlorine dioxide as a disinfectant or oxidant must
comply with any requirements for chlorine dioxide in this Subpart I
beginning January 1, 2002
. A Subpart B system supplier serving fewer
than 10,000 persons and using chlorine dioxide as a disinfectant or oxidant
or a supplier using only groundwater not under the direct influence of
surface water and using that uses chlorine dioxide
as a disinfectant or
oxidant must comply with any requirements for chlorine dioxide in this
Subpart I beginning January 1, 2004 .
c)
Each CWS or NTNCWS supplier regulated under subsection (a) of this Section
must be operated by qualified personnel who meet the requirements specified in 35
Ill. Adm
. Code 680.
d)
Control of disinfectant residuals . Notwithstanding the MRDLs in Section 611
.313,
a supplier may increase residual disinfectant levels in the distribution system of
chlorine or chloramines (but not chlorine dioxide) to a level and for a time necessary
to protect public health, to address specific microbiological contamination problems
caused by circumstances such as, but not limited to, distribution line breaks, storm
run-off events, source water contamination events, or cross-connection events
.
BOARD NOTE
: Derived from 40 CFR 141 .130 (2002) (2005) .
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(Source: Amended at 30 111 . Reg. , effective )
SUBPART N : INORGANIC MONITORING AND ANALYTICAL
REQUIREMENTS
Section 611 .609
Determining Compliance
Compliance with the MCLs of Section 611 .300 or 611 .301 (as appropriate) must be determined
based on the analytical results obtained at each sampling point .
a)
For suppliers that monitor at a frequency greater than annual, compliance with the
MCLs for antimony, arsenic (effective January 22, 2004), asbestos, barium,
beryllium, cadmium, chromium, cyanide, fluoride, mercury, nickel, selenium, or
thallium is determined by a running annual average at each sampling point .
Effective January 22, 2004, if a system fails to collect the required number of
samples, compliance (average concentration) will be based on the total number of
samples collected .
1)
If the average at any sampling point is greater than the MCL, then the
supplier is out of compliance .
2)
If any one sample would cause the annual average to be exceeded, then the
supplier is out of compliance immediately .
3)
Any sample below the method detection limit must be calculated at zero
for the purpose of determining the annual average
.
BOARD NOTE : The "method detection limit" is different from the
"detection limit, " as set forth in Section 611 .600. The "method detection
limit" is the level of contaminant that can be determined by a particular
method with a 95 percent degree of confidence, as determined by the
method outlined in
appendix B to 40 CFR 136, Appendix B, incorporated
by reference at Section 611 .102
.
b)
For suppliers that monitor annually or less frequently, compliance with the MCLs
for antimony, arsenic (effective January 22, 2004), asbestos, barium, beryllium,
cadmium, chromium, cyanide, fluoride, mercury, nickel, selenium, or thallium is
determined by the level of the contaminant at any sampling point. If confirmation
samples are required by the Agency, the determination of compliance will be
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based on the average of the annual average of the initial MCL exceedence and any
Agency-required confirmation samples . Effective January 22, 2004, if a supplier
fails to collect the required number of samples, compliance (average
concentration) will be based on the total number of samples collected .
c)
Compliance with the MCLs for nitrate and nitrite is determined based on one
sample if the levels of these contaminants are below the MCLs . If the levels of
nitrate or nitrite in the initial sample exceed the MCLs, Section 611 .606 requires
confirmation sampling, and compliance is determined based on the average of the
initial and confirmation samples .
d)
Arsenic sampling results must be reported to the nearest 0 .001 mg/f .
BOARD NOTE: Derived from 40 CFR 141
.23(i)
(2002) (2005) .
(Source: Amended at 30 Ill
. Reg. ,
effective )
SUBPART 0: ORGANIC MONITORING AND ANALYTICAL
REQUIREMENTS
Section 611 .646
Phase I, Phase II, and Phase V Volatile Organic Contaminants
Monitoring of the Phase I, Phase II, and Phase V VOCs for the purpose of determining
compliance with the MCL must be conducted as follows :
a)
Definitions . As used in this Section the following have the given meanings
:
"Detect" and "detection" mean that the contaminant of interest is present
at a level greater than or equal to the "detection limit."
"Detection limit" means 0 .0005 mg/f.
BOARD NOTE : Derived from 40 CFR 141 .24(f)(7),
(f)(11), (f)(14)(i),
and (f)(20)-(200-3) (20051 . This is a "trigger level" for Phase I, Phase II,
and Phase V VOCs inasmuch as it prompts further action . The use of the
term "detect" in this Section is not intended to include any analytical
capability of quantifying lower levels of any contaminant, or the "method
detection limit ." Note, however, that certain language at the end of federal
paragraph (f)(20) is capable of meaning that the "method detection limit"
is used to derive the "detection limit ." The Board has chosen to disregard
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that language at the end of paragraph (f)(20) in favor of the more direct
language of paragraphs (f)(7) and
(f)(11).
"Method detection limit," as used in subsections (q) and (t) of this Section
means the minimum concentration of a substance that can be measured
and reported with 99 percent confidence that the analyte concentration is
greater than zero and is determined from analysis of a sample in a given
matrix containing the analyte .
BOARD NOTE
: Derived from appendix B to 40 CFR 136, ppendix B
(20" (2005)
. The method detection limit is determined by the procedure
set forth in appendix B to 40 CFR 136, Appendix B incorporated by
reference in Section 611 .102(c) . See subsection (t) of this Section .
b)
Required sampling . Each supplier must take a minimum of one sample at each
sampling point at the times required in subsection (u) of this Section .
c)
Sampling points .
1)
Sampling points for a GWS . Unless otherwise provided by a SEP granted
by the Agency pursuant to Section 611 .110, a GWS supplier must take at
least one sample from each of the following points : each entry point that
is representative of each well after treatment .
2)
Sampling points for an SWS or mixed system supplier . Unless otherwise
provided by a SEP granted by the Agency pursuant to Section 611 .110, an
SWS or mixed system supplier must sample from each of the following
points:
A)
Each entry point after treatment; or
B)
Points in the distribution system that are representative of each
source.
3)
The supplier must take each sample at the same sampling point unless the
Agency has granted a SEP pursuant to Section 611
.110 that designates
another location as more representative of each source, treatment plant, or
within the distribution system .
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4)
If a system draws water from more than one source, and the sources are
combined before distribution, the supplier must sample at an entry point
during periods of normal operating conditions when water is
representative of all sources being used .
BOARD NOTE : Subsections (b) and (c) of this Section derived from 40 CFR
141 .24(f)(1) through (f)(3)(2003) (2005) .
d)
Each CWS and NTNCWS supplier must take four consecutive quarterly samples
for each of the Phase I VOCs, excluding vinyl chloride, and Phase II VOCs during
each compliance period, beginning in the compliance period starting in the initial
compliance period .
e)
Reduction to annual monitoring frequency . If the initial monitoring for the Phase
I, Phase II, and Phase V VOCs, as allowed in subsection (r)(1) of this Section, was
completed by December 31, 1992, and the supplier did not detect any of the Phase
I VOCs, including vinyl chloride ; Phase 11 VOCs
; or Phase V VOCs, then the
supplier must take one sample annually beginning in the initial compliance period
.
GWS reduction to triennial monitoring frequency . After a minimum of three
years of annual sampling, GWS suppliers that have not previously detected any of
the Phase I VOCs, including vinyl chloride ; Phase II VOCs
; or Phase V VOCs
must take one sample during each three-year compliance period
.
A CWS or NTNCW S supplier that has completed the initial round of monitoring
required by subsection (d) of this Section and which did not detect any of the
Phase I VOCs, including vinyl chloride
; Phase II VOCs ; and Phase V VOCs may
apply to the Agency for a SEP pursuant to Section 611 .110 that releases it from
the requirements of subsection (e) or
(0
of this Section
. A supplier that serves
fewer than 3300 service connections may apply to the Agency for a SEP that
releases it from the requirements of subsection (d) of this Section as to 1,2,4-tri-
chlorobenzene .
0
g)
BOARD NOTE : Derived from 40 CFR 141
.24(0(7) and (f)(10)(2003) (2005),
and the discussion at 57 Fed . Reg
. 31825 (July 17, 1992) . Provisions concerning
the term of the waiver appear in subsections (i) and (j) of this Section
. The
definition of "detect," parenthetically added to the federal counterpart paragraph,
is in subsection (a) of this Section.
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h)
Vulnerability assessment . The Agency must consider the factors of Section
611 .110(e) in granting a SEP from the requirements of subsection (d), (e), or (f) of
this Section sought pursuant to subsection (g) of this Section .
i)
A SEP issued to a GWS pursuant to subsection (g) of this Section is for a
maximum of six years, except that a SEP as to the subsection (d) of this Section
monitoring for 1,2,4-trichlorobenzene must apply only to the initial round of
monitoring. As a condition of a SEP, except as to a SEP from the initial round of
subsection (d) of this Section monitoring for 1,2,4-trichlorobenzene, the supplier
shall, within 30 months after the beginning of the period for which the waiver was
issued, reconfirm its vulnerability assessment required by subsection (h) of this
Section and submitted pursuant to subsection (g) of this Section, by taking one
sample at each sampling point and reapplying for a SEP pursuant to subsection (g)
of this Section. Based on this application, the Agency must do either of the
following :
1)
If it determines that the PWS meets the standard of Section 611 .610(e),
issue a SEP that reconfirms the prior SEP for the remaining three-year
compliance period of the six-year maximum term ; or
2)
Issue a new SEP requiring the supplier to sample annually .
BOARD NOTE
: Subsection (i) of this Section does not apply to an SWS or
mixed system supplier.
Special considerations for a SEP for an SWS or mixed-system supplier
.
1)
The Agency must determine that an SWS is not vulnerable before issuing
a SEP pursuant to Section 611 .110 to an SWS supplier. A SEP issued to
an SWS or mixed system supplier pursuant to subsection (g) of this
Section is for a maximum of one compliance period ; and
2)
The Agency may require, as a condition to a SEP issued to an SWS or
mixed supplier, that the supplier take such samples for Phase I, Phase II,
and Phase V VOCs at such a frequency as the Agency determines are
necessary, based on the vulnerability assessment .
BOARD NOTE : There is a great degree of similarity between 40 CFR
141 .24(f)(7) (20033) (2005), the provision applicable to GWSs, and 40 CFR
J)
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141 .24(f)(10) (2003) (2005), the provision for SWSs . The Board has consolidated
the common requirements of both paragraphs into subsection (g) of this Section
.
Subsection (j) of this Section represents the elements unique to an SWSs or mixed
system, and subsection (i) of this Section relates to a GWS supplier
. Although 40
CFR 141 .24(f)(7) and (f)(10) are silent as to a mixed system supplier, the Board
has included a mixed system supplier with an SWS supplier because this best
follows the federal scheme for all other contaminants.
k)
If one of the Phase I VOCs, excluding vinyl chloride ; a Phase II VOC ; or a Phase
V VOC is detected in any sample, then the following must occur :
1)
The supplier must monitor quarterly for that contaminant at each sampling
point that resulted in a detection .
2)
Annual monitoring.
A)
The Agency must grant a SEP pursuant to Section 611 .110 that
allows a supplier to reduce the monitoring frequency to annual at a
sampling point if it determines that the sampling point is reliably
and consistently below the MCL .
B)
A request for a SEP must include the following minimal
information
:
i)
For a GWS, two quarterly samples .
ii)
For an SWS or mixed system supplier, four quarterly
samples.
C)
In issuing a SEP, the Agency must specify the level of the
contaminant upon which the "reliably and consistently"
determination was based . Any SEP that allows less frequent
monitoring based on an Agency "reliably and consistently"
determination must include a condition requiring the supplier to
resume quarterly monitoring pursuant to subsection
(k)(1) of this
Section if it violates the MCL specified by Section 611
.311 .
3)
Suppliers that monitor annually must monitor during the quarters that
previously yielded the highest analytical result .
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4)
Suppliers that do not detect a contaminant at a sampling point in three
consecutive annual samples may apply to the Agency for a SEP pursuant
to Section 611
.110 that allows it to discontinue monitoring for that
contaminant at that point, as specified in subsection (g) of this Section
.
5)
A GWS supplier that has detected one or more of the two-carbon
contaminants listed in subsection (k)(5)(A) of this Section must monitor
quarterly for vinyl chloride as described in subsection (k)(5)(B) of this
Section, subject to the limitation of subsection (k)(5)(C)
of this Section .
A)
"Two-carbon contaminants" (Phase I or II VOC) are the following :
1,2-Dichloroethane (Phase I)
1, 1 -Dichloroethylene (Phase I)
cis-1,2-Dichloroethylene (Phase II)
trans- l,2-Dichloroethylene (Phase II)
Tetrachloroethylene (Phase II)
1,1,1-Trichloroethylene (Phase I)
Trichloroethylene (Phase 1)
B)
The supplier must sample quarterly for vinyl chloride at each
sampling point at which it detected one or more of the two-carbon
contaminants listed in subsection
(k)(5)(A) of this Section
.
C)
The Agency must grant a SEP pursuant to Section 611
.110 that
allows the supplier to reduce the monitoring frequency for vinyl
chloride at any sampling point to once in each three-year
compliance period if it determines that the supplier has not
detected vinyl chloride in the first sample required by subsection
(k)(5)(B) of this Section .
1)
Quarterly monitoring following MCL violations .
1)
Suppliers that violate an MCL for one of the Phase I VOCs, including
vinyl chloride
; Phase II VOCs ; or Phase V VOCs, as determined by
subsection (o) of this Section, must monitor quarterly for that contaminant,
at the sampling point where the violation occurred, beginning the next
quarter after the violation .
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2)
Annual monitoring .
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A)
The Agency must grant a SEP pursuant to Section 611 .110 that
allows a supplier to reduce the monitoring frequency to annually if
it determines that the sampling point is reliably and consistently
below the MCL.
B)
A request for a SEP must include the following minimal
information : four quarterly samples .
C)
In issuing a SEP, the Agency must specify the level of the
contaminant upon which the "reliably and consistently"
determination was based . Any SEP that allows less frequent
monitoring based on an Agency "reliably and consistently"
determination must include a condition requiring the supplier to
resume quarterly monitoring pursuant to subsection (1)(1) of this
Section if it violates the MCL specified by Section 611 .311 .
D)
The supplier must monitor during the quarters that previously
yielded the highest analytical result .
m) Confirmation samples
. The Agency may issue a SEP pursuant to Section 610 .110
to require a supplier to use a confirmation sample for results that it finds dubious
for whatever reason . The Agency must state its reasons for issuing the SEP if the
SEP is Agency-initiated.
I)
If a supplier detects any of the Phase I, Phase II, or Phase V VOCs in a
sample, the supplier must take a confirmation sample as soon as possible,
but no later than 14 days after the supplier receives notice of the detection .
2)
Averaging is as specified in subsection (o) of this Section .
3)
The Agency must delete the original or confirmation sample if it
determines that a sampling error occurred, in which case the confirmation
sample will replace the original or confirmation sample .
n)
This subsection (n) corresponds with 40 CFR 141 .24(f)(14), an optional USEPA
provision relating to compositing of samples that USEPA does not require for
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state programs
. This statement maintains structural consistency with USEPA
rules .
o)
Compliance with the MCLs for the Phase I, Phase II, and Phase V VOCs must be
determined based on the analytical results obtained at each sampling point .
Effective January 22, 2004, if one sampling point is in violation of an MCL, the
system is in violation of the MCL
.
1)
Effective January 22, 2004, for a supplier that monitors more than once
per year, compliance with the MCL is determined by a running annual
average at each sampling point.
2)
Effective January 22, 2004, a supplier that monitors annually or less
frequently whose sample result exceeds the MCL must begin quarterly
sampling
. The system will not be considered in violation of the MCL until
it has completed one year of quarterly sampling .
3)
Effective January 22, 2004, if any sample result will cause the running
annual average to exceed the MCL at any sampling point, the supplier is
out of compliance with the MCL immediately.
4)
Effective January 22, 2004, if a supplier fails to collect the required
number of samples, compliance will be based on the total number of
samples collected .
5)
Effective January 22, 2004, if a sample result is less than the detection
limit, zero will be used to calculate the annual average .
6)
Until January 22, 2004, for a supplier that conducts monitoring at a
frequency greater than annual, compliance is determined by a running
annual average of all samples taken at each sampling point
.
A)
If the annual average of any sampling point is greater than the
MCL, then the supplier is out of compliance .
B) If the initial sample or a subsequent sample would cause the annual
average to exceed the MCL, then the supplier is out of compliance
immediately.
p)
q)
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C)
Any samples below the detection limit must be deemed as zero for
purposes of determining the annual average .
7)
Until January 22, 2004, if monitoring is conducted annually, or less
frequently, the supplier is out of compliance if the level of a contaminant
at any sampling point is greater than the MCL . Until January 22, 2004, if
a confirmation sample is taken, the determination of compliance is based
on the average of two samples .
This subsection (p) corresponds with 40 CFR 141 .24(£)(16), which USEPA
removed and reserved . This statement maintains structural consistency with the
federal regulations.
Analysis under this Section must only be conducted by laboratories that have
received certification by USEPA or the Agency according to the following
conditions:
1)
To receive certification to conduct analyses for the Phase I VOCs,
excluding vinyl chloride; Phase II VOCs ; and Phase V VOCs, the
laboratory must do the following:
A) It must analyze performance evaluation (PE) samples that include
these substances provided by the Agency pursuant to 35 III . Adm.
Code 186 .170;
B)
It must achieve the quantitative acceptance limits under
subsections (q)(1)(C) and (q)(1)(D)
of this Section for at least 80
percent of the regulated organic contaminants in the PE sample ;
C)
It must achieve quantitative results on the analyses performed
under subsection (q)(1)(A) of this Section that are within
f 20
percent of the actual amount of the substances in the PE sample
when the actual amount is greater than or equal to 0 .010 mg/f ;
D)
It must achieve quantitative results on the analyses performed
under subsection (q)(1)(A) of this Section that are within ± 40
percent of the actual amount of the substances in the PE sample
when the actual amount is less than 0 .010 mg/Q
; and
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
E)
It must achieve a method detection limit of 0 .0005 mg/f, according
to the procedures in appendix B to 40 CFR 136, Appendix B,
incorporated by reference in Section 611 .102 .
2)
To receive certification to conduct analyses for vinyl chloride the
laboratory must do the following :
A)
It must analyze PE samples provided by the Agency pursuant to 35
Ill. Adm. Code 186 .170;
B)
It must achieve quantitative results on the analyses performed
under subsection (q)(2)(A) of this Section that are within ± 40
percent of the actual amount of vinyl chloride in the PE sample ;
C)
It must achieve a method detection limit of 0 .0005 mg/f, according
to the procedures in appendix B to 40 CFR 136 Appendix B,
incorporated by reference in Section 611 .102 ; and
D)
It must obtain certification pursuant to subsection
(q)(1) of this
Section for Phase I VOCs, excluding vinyl chloride
; Phase 11
VOCs; and Phase V VOCs
.
r)
This subsection (r) corresponds with 40 CFR 141 .24(f)(18), an obsolete
provision that relates to the initial compliance period from 1993 through 1995 .
This statement maintains consistency with the federal regulations .
s)
The Agency shall, by a SEP issued pursuant to Section 611 .110, increase the
number of sampling points or the frequency of monitoring if it determines that it
is necessary to detect variations within the PWS .
t)
Each laboratory certified for the analysis of Phase I, Phase II, or Phase V V OCs
pursuant to subsection
(q)(1) or (q)(2) of this Section shall do the following :
1)
Determine the method detection limit (MDL), as defined in
appendix B to
40 CFR 136, Appendix-B, incorporated by reference in Section 611
.102, at
which it is capable of detecting the Phase I, Phase II, and Phase V VOCs
;
and,
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
2)
Achieve an MDL for each Phase I, Phase II, and Phase V VOC that is less
than or equal to 0 .0005 mg/f .
u)
Each supplier must monitor, within each compliance period, at the time
designated by the Agency by SEP pursuant to Section 611
.110
.
v)
A new system supplier or a supplier that uses a new source of water that begins
operation after January 22, 2004 must demonstrate compliance with the MCL
within a period of time specified by a permit issued by the Agency . The supplier
must also comply with the initial sampling frequencies specified by the Agency to
ensure the supplier can demonstrate compliance with the MCL . Routine and
increased monitoring frequencies must be conducted in accordance with the
requirements in this Section .
BOARD NOTE : Derived from 40 CFR 141 .24(f)(2003) (2005) .
(Source: Amended at 30 Ill . Reg . , effective )
Section 611
.Appendix D
Defined Substrate Method for the Simultaneous Detection of Total
Coliforms and Escherichia Coli from Drinking Water
Autoanalysis Colilert Presence-Absence (AC P-A) Method .
The AC P-A test format must be either a 100 mf 10-tube most probable number test (one tube
positive denoting the presence of total coliforms in that sample) or a single vessel containing
sufficient reagent to receive 100 mE of sample . The reagent is available from Access Medical
Systems, Branford Connecticut.
The AC P-A method must be performed as follows :
1 .
For the 10-tube method, add 10 mf of water sample to each test tube
. For the single-
vessel method, add 100 me of water sample to the vessel
.
2.
Dissolve the reagent powder by agitation . (This should produce a colorless solution
.)
3.
Incubate the test tubes or vessel at 35°C for 24 hours
.
4 .
Development of yellow during incubation denotes the presence of total coliforms in either
the test tube or the vessel .
ILLINOIS REGISTER
POLLUTION CONTROL BOARD
NOTICE OF PROPOSED AMENDMENTS
5 .
Expose each positive (yellow) test tube or vessel to a fluorescent (366 nm) light source.
Fluorescence specifically demonstrates the presence of Escherichia coli .
BOARD NOTE : Derived from S . Edberg, M
. Allen & D . Smith, "National Field
Evaluation of a Defined Substrate Method for the Simultaneous Detection of Total
Coliforms and Escherichia coli from Drinking Water : Comparison with Presence-
Absence Techniques,"3 Applied and Environmental Microbiology, vol . 55, pp . 1003-
1008, as incorporated by reference at 40 CFR 141 .21(f)(6)(iii) (2002) (2005) . This
method is for use in conjunction with the requirements of Section 611 .526
.
(Source: Amended at 30 Ill
. Reg. , effective )
