POLLUTION CONTROL BOARD
ILLINOIS REGISTER
1
06
4)
Statutory authority
: 415 ILCS 5/7.2, 17, 17 .5, and 27 .
5)
A Complete description of the subjects and issues involved:
The following briefly
describes the subjects and issues involved in the docket R06-15 rulemaking . A
comprehensive description is contained in the Board's opinion and order of July 20,
2006, proposing amendments in docket R06-15, which opinion and order is available
from the address below .
This proceeding updates the Illinois Safe Drinking Water Act (SDWA) rules to
correspond with amendments adopted by the United States Environmental Protection
Agency (USEPA) that appeared in the Federal Register during a single update period
.
The docket and time period that is involved in this proceeding is the following
:
R06-15
Federal SDWA amendments that occurred during the period July 1,
2005 through December 31, 2005 .
The R06-15 docket only amends rules in Part 611
. The following table briefly
summarizes the sole federal action in the update period :
October 13, 2005
(70 Fed. Reg. 59848)
USEPA adopted new requirements for the filing and
receipt of required documents as electronic documents .
The filings included are all documents whose filing is
provided by the primary drinking water regulations
.
NOTICE OF PROPOSED AMENDMENTS
RECEIVE
CLERK'S OFFICE
1 }
Heading of the Part : Primary Drinking Water Standards
AUG 0
1 2006
2)
STATE OF ILLINIG
Code citation : 35 Ill
. Adm
. Code 611
Pollution
Control B C
3)
Section numbers:
Proposed action :
611 .102
Amend
611 .105
New Section
611 .111
Amend
611 .212
Amend
611 .359
Amend
611 .380
Amend
611
.609
Amend
611 .646
Amend
611 .APPENDIX D
;Amend
NOTICE OF PROPOSED AMENDMENTS
The USEPA action of October 13, 2005 (70 Fed. Reg . 59848) established the Cross-
Media Electronic Reporting Rule (CROMERR) . The CROMERR sets standards for the
filing of documents in various federal program areas in an electronic format . While the
CROMERR does not require the filing of documents in an electronic format, it does
impose minimum requirements on documents that are filed in such a format and on the
electronic document receiving systems used to receive them. The CROMERR imposes
requirements on electronic filings submitted to USEPA and on USEPA's Central Data
Exchange (CDX) that receives them, as well as on any electronic document filings
submitted to the states and any systems used by the states to receive those filings .
Tables appear in the Board's opinion and order of July 20, 2006 in docket R06-15 that list
numerous corrections and amendments that are not based on current federal amendments .
The tables contain deviations from the literal text of the federal amendments underlying
these amendments, as well as corrections and clarifications that the Board made in the
base text involved. Persons interested in the details of those corrections and amendments
should refer to the July 20, 2006 opinion and order in docket R06-15 .
Section 17 .5 of the Environmental Protection Act [415 ILCS 5/17 .5] provides that
Section 5-35 of the Administrative Procedure Act [5 ILCS 100/5-35] does not apply to
this rulemaking. Because this rulemaking is not subject to Section 5-35 of the APA, it is
not subject to First Notice or to Second Notice review by the Joint Committee on
Administrative Rules (JCAR).
6)
Published studies or reports, and sources of underlying data, used to compose this
rulemaking : None
7)
Will this rulemaking replace any emergency amendments currently in effect? No
8)
Does this rulemaking contain an automatic repeal date? No
9)
Does this rulemaking contain incorporation by reference? Yes. Section 611 .102 is the
centralized location of all incorporations of documents used for the purposes of
compliance with all of Part 611 . The amendments update all citations to the Code of
Federal Regulations to the latest edition available, although those updates do not
necessarily incorporate the cited federal regulations . Second, the amendments add
incorporation of segments of the Code of Federal Regulations that embody key elements
of the federal CROMERR requirements . Third, the amendments remove the
incorporation by reference of appendix C to 40 CFR 136, since this document is not
referenced in any substantive segment of the rules
. The amendments also update the
ILLINOIS REGISTER
2
POLLUTION CONTROL BOARD
06
NOTICE OF PROPOSED AMENDMENTS
version of appendix B to 40 CFR 136 incorporated by reference to the latest edition
available
. Finally, the amendments add to each incorporation by reference of a segment
of the
Code of Federal Regulations
a citation to the segments of the Illinois regulations
for which the incorporation is made
.
10)
Are there any other proposed rulemakings pending on this Part?
No
11) Statement of statewide policy obiectives, : These proposed amendments do not create or
enlarge a state mandate, as defined in Section 3(b) of the State Mandates Act [30 ILCS
805/3(b)(2002)] .
12) Time, Place and manner in which interested persons may comment on this proposed
rulemaking :
The Board will accept written public comment on this proposal for a period
of 45 days after the date of this publication
. Comments should reference docket R06-15
and be addressed to :
Ms. Dorothy M
. Gunn, Clerk
Illinois Pollution Control Board
State of Illinois Center, Suite 11-500
100 W. Randolph St
.
Chicago, IL 60601
Please direct inquiries to the following person and reference docket
g96-15
:
Michael J . McCambridge
Staff Attorney
Illinois Pollution Control Board
100W. Randolph 11-500
Chicago, IL 60601
312-814-6924
E-mail: mccambm@ipcb .state.il.us
Request
copies of the Board's opinion and order at 312-814-3620, or downld
from the Board's Wr
ite at
httv:llwww.ipcb .state.il .us.
13)
Initialregulatoryflexibility analysis
:
A)
yes of small businesses, smallmunicipalities,
andnot-for-profit
corporations
ILLINOIS REGISTER
3
POLLUTION CONTROL BOARD
06
NOTICE OF PROPOSED AMENDMENTS
affected: This rulemaking may affect those small businesses, small
municipalities, and not-for-profit corporations that own or operate a public water
supply.
B)
Reporting, bookkeeping or other procedures required for compliance : The
existing rules and proposed amendments require extensive reporting, bookkeeping
and other procedures, including the preparation of reports, water analyses, and
maintenance of operating records .
C)
Types of professional skills necessary for compliance
: Compliance with the
existing rules and proposed amendments may require the services of an attorney,
certified public accountant, chemist, and registered professional engineer
.
14) Regulatory agenda on which this rulemaking was summarized : December 2005
The full text of the Proposed Amendments begins on the next page :
ILLINOIS REGISTER
4
POLLUTION CONTROL BOARD
06
TITLE 35 :
ENVIRONMENTAL PROTECTION
SUBTITLE F : PUBLIC WATER SUPPLIES
CHAPTER I
: POLLUTION CONTROL BOARD
PART 611
PRIMARY DRINKING WATER STANDARDS
SUBPART A : GENERAL
Section
611 .100
Purpose, Scope, and Applicability
611 .101
Definitions
611 .102
Incorporations by Reference
611 .103
Severability
611 .105
Electronic Reporting
611 .107
Agency Inspection of PWS Facilities
611 .108
Delegation to Local Government
611 .109
Enforcement
611 .110
Special Exception Permits
611 .111
Relief Equivalent to SDWA Section 1415(a) Variances
611 .112
Relief Equivalent to SDWA Section 1416 Exemptions
611 .113
Alternative Treatment Techniques
611 .114
Siting Requirements
611 .115
Source Water Quantity
611 .120
Effective Dates
611 .121
Maximum Contaminant Levels and Finished Water Quality
611 .125
Fluoridation Requirement
611 .126
Prohibition on Use of Lead
611 .130
Special Requirements for Certain Variances and Adjusted Standards
611 .131
Relief Equivalent to SDWA Section 1415(e) Small System Variance
611 .160
Composite Correction Program
SUBPART B
: FILTRATION AND DISINFECTION
Section
611 .201
Requiring a Demonstration
611 .202
Procedures for Agency Determinations
611 .211
Filtration Required
611 .212
Groundwater under Direct Influence of Surface Water
611 .213
No Method of HPC Analysis
611 .220
General Requirements
611 .230
Filtration Effective Dates
611 .231
Source water Quality Conditions
611 .232
Site-Specific Conditions
611 .233
Treatment Technique Violations
611 .240
Disinfection
611 .241
Unfiltered PWSs
611 .242
Filtered PWSs
611 .250
Filtration
611 .261
Unfiltered PWSs : Reporting and Recordkeeping
611 .262
Filtered PWSs : Reporting and Recordkeeping
611 .271
Protection during Repair Work
611 .272
Disinfection Following Repair
611 .276
Recycle Provisions
SUBPART C : USE OF NON-CENTRALIZED TREATMENT DEVICES
"C
CLERKS
774
OFFICE
VED
AUG p
1203
STATE OF ILLiNOIs
Pollution Control Board
Section
611 .280
Point-of-Entry Devices
611 .290
Use of Point-of-Use Devices or Bottled Water
SUBPART D ; TREATMENT TECHNIQUES
Section
611 .295
General Requirements
611 .296
Acrylamide and Epichlorohydrin
611 .297
Corrosion Control
SUBPART F : MAXIMUM
CONTAMINANT LEVELS (MCLs) AND
MAXIMUM RESIDUAL DISINFECTANT LEVELS (MRDL5)
Section
611 .300
Old MCLs for Inorganic Chemical Contaminants
611 .301
Revised MCLs for Inorganic Chemical Contaminants
611 .310
old Maximum Contaminant Levels (MCLs) for organic Chemical
Contaminants 611 .311
Revised MCLS for Organic Chemical Contaminants
611 .312
Maximum Contaminant Levels (MCLs) for Disinfection Byproducts (DEPS)
611
.313
Maximum Residual Disinfectant Levels (MRDLS)
611 .320
Turbidity (Repealed)
611 .325
Microbiological Contaminants
611 .330
Maximum Contaminant Levels for Radionuclides
611 .331
Beta Particle and Photon Radioactivity (Repealed)
SUBPART G : LEAD AND COPPER
Section
611 .350
General Requirements
611 .351
Applicability of Corrosion Control
611 .352
Corrosion Control Treatment
611 .353
Source Water Treatment
611 .354
Lead Service Line Replacement
611 .355
Public Education and Supplemental Monitoring
611 .356
Tap Water Monitoring for Lead and Copper
611 .357
Monitoring for Water Quality Parameters
611 .358
Monitoring for Lead and Copper in Source Water
611 .359
Analytical Methods
611 .360
Reporting
611 .361
Recordkeeping
SUBPART I : DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS,
AND DISINFECTION BYPRODUCT PRECURSORS
Section
611 .380
General Requirements
611 .381
Analytical Requirements
611 .382
Monitoring Requirements
611 .383
Compliance Requirements
611 .384
Reporting and Recordkeeping Requirements
611 .385
Treatment Technique for Control of Disinfection Byproduct (DBP)
Precursors
SUBPART K : GENERAL MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .480
Alternative Analytical Techniques
611 .490
Certified Laboratories
611 .491
Laboratory Testing Equipment
611 .500
Consecutive PWSs
611 .510
special monitoring for Unregulated Contaminants (Repealed)
SUBPART L : MICROBIOLOGICAL MONITORING
AND ANALYTICAL REQUIREMENTS
Section
611 .521
Routine Coliform Monitoring
611 .522
Repeat Coliform Monitoring
611 .523
Invalidation of Total Coliform Samples
611 .524
Sanitary Surveys
611 .525
Fecal Coliform and E . Coli Testing
611 .526
Analytical Methodology
611 .527
Response to Violation
611 .531
Analytical Requirements
611 .532
Unfiltered PWSs
611 .533
Filtered PWSs
SUBPART M : TURBIDITY MONITORING AND ANALYTICAL REQUIREMENTS
Section
611
.560
Turbidity
SUBPART N
: INORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .591
Violation of a State MCL
611
.592
Frequency of State monitoring
611 .600
Applicability
611 .601
Monitoring Frequency
611 .602
Asbestos Monitoring Frequency
611 .603
Inorganic Monitoring Frequency
611 .604
Nitrate Monitoring
611 .605
Nitrite Monitoring
611 .606
Confirmation Samples
611 .607
More Frequent Monitoring and Confirmation Sampling
611 .608
Additional Optional Monitoring
611 .609
Determining Compliance
611 .610
Inorganic Monitoring Times
611 .611
Inorganic Analysis
611 .612
Monitoring Requirements for Old Inorganic MCLs
611 .630
Special Monitoring for Sodium
611 .631
Special Monitoring for Inorganic Chemicals (Repealed)
SUBPART 0 : ORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .640
Definitions
611 .641
Old MCLs
611 .645
Analytical methods for organic Chemical Contaminants
611 .646
Phase I, Phase II, and Phase V Volatile Organic Contaminants
611 .647
Sampling for Phase I Volatile Organic Contaminants (Repealed)
611 .648
Phase II, Phase IIB, and Phase V Synthetic Organic Contaminants
611
.650
Monitoring for 36 Contaminants (Repealed)
611 .657
Analytical Methods for 36 Contaminants
(Repealed)
611 .658
Special Monitoring for Organic Chemicals
(Repealed)
SUBPART P : THM MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .680
Sampling, Analytical, and other Requirements
611 .683
Reduced Monitoring Frequency (Repealed)
611 .684
Averaging (Repealed)
611 .685
Analytical Methods
611 .686
Modification to System (Repealed)
611 .687
Sampling for THM Potential (Repealed)
611 .688
Applicability Dates (Repealed)
SUBPART Q : RADIOLOGICAL MONITORING AND ANALYTICAL REQUIREMENTS
Section
611 .720
Analytical Methods
611 .731
Gross Alpha
611 .732
Beta Particle and Photon Radioactivity
611 .733
General Monitoring and Compliance Requirements
SUBPART R : ENHANCED FILTRATION AND DISINFECTION
:
SYSTEMS THAT SERVE 10,000 OR MORE PEOPLE
Section
611 .740
General Requirements
611 .741
Standards for Avoiding Filtration
611 .742
Disinfection Profiling and Benchmarking
611 .743
Filtration
611 .744
Filtration Sampling Requirements
611 .745
Reporting and Recordkeeping Requirements
SUBPART T : REPORTING AND RECORDKEEPING
Section
611 .830
Applicability
611 .831
Monthly Operating Report
611 .832
Notice by Agency (Repealed)
611 .833
Cross Connection Reporting
611 .840
Reporting
611 .851
Reporting MCL, MRDL, and other Violations (Repealed)
611 .852
Reporting other Violations (Repealed)
611 .853
Notice to New Billing Units (Repealed)
611 .854
General Content of Public Notice (Repealed)
611 .855
Mandatory Health Effects Language (Repealed)
611 .856
Fluoride Notice (Repealed)
611 .858
Fluoride Secondary Standard (Repealed)
611 .860
Record Maintenance
611 .870
List of 36 Contaminants (Repealed)
SUBPART U : CONSUMER CONFIDENCE REPORTS
Section
611 .881
Purpose and Applicability
611 .882
Compliance Dates
611 .883
Content of the Reports
611 .910
Notice by the Agency on Behalf of a PWS
SUBPART X : ENHANCED FILTRATION AND DISINFECTION
SYSTEMS SERVING FEWER THAN 10,000 PEOPLE
Section
611 .950
General Requirements
611 .951
Finished Water Reservoirs
611 .952
Additional Watershed Control Requirements for Unfiltered Systems
611 .953
Disinfection Profile
611 .954
Disinfection Benchmark
611 .955
Combined Filter Effluent Turbidity Limits
611 .956
Individual Filter Turbidity Requirements
611 .957
Reporting and Recordkeeping Requirements
611 .
A Regulated Contaminants
611 .
B Percent Inactivation of G . Lamblia Cysts
611 .
C Common Names of Organic Chemicals
611 .
D Defined Substrate Method for the Simultaneous Detection
of Total Coliforms and Eschericia Coli from Drinking Water
611 .
E Mandatory Lead Public Education Information for
Community Water Systems
611 .
F Mandatory Lead Public Education Information for Non-
Transient Non-Community Water Systems
611 .
G NPDWR Violations and Situations Requiring Public Notice
611 .
H Standard Health Effects Language for Public Notification
611 .
I Acronyms Used in Public Notification Regulation
611 .Ta~1'ART,F
A Total Coliform Monitoring Frequency
611 .Table7a F
B Fecal or Total Coliform Density Measurements
611 . Tabl cTARLE C Frequency of RDC Measurement
611 .Ta~TAR7,F D Number of Lead and Copper Monitoring Sites
611 .TablcTb;jLE E Lead and Copper Monitoring Start Dates
611 .TabloTABLE F Number of water Quality Parameter Sampling Sites
611 . TabloTALE G Summary of Section 611 .357 Monitoring Requirements for Water
Quality Parameters
611 . Tab1cTABLE Z Federal Effective Dates
I
AUTHORITY : Implementing Sections 7 .2, 17, and 17 .5 and authorized by section 27
of the Environmental Protection Act [415 ILCS 5/7 .2, 17, 17 .5, and 27) .
611 .884
611 .885
SUBPART V :
Section
Required Additional Health Information
Report Delivery and Recordkeeping
PUBLIC NOTIFICATION OF DRINKING WATER VIOLATIONS
611 .901
General Public Notification Requirements
611 .902
Tier 1 Public Notice : Form, Manner, and Frequency of Notice
611 .903
Tier 2 Public Notice : Form, Manner, and Frequency of Notice
611 .904
Tier 3 Public Notice : Form, Manner, and Frequency of Notice
611 .905
Content of the Public Notice
611 .906
Notice to New Billing Units or New Customers
611 .907
Special Notice of the Availability of Unregulated Contaminant
Monitoring
611 .908
Results
Special Notice for Exceedence of the Fluoride Secondary Standard
611 .909
Special Notice for Nitrate Exceedences above the MCL by a Non-
Community Water System
SOURCE : Adopted in R88-26 at 14 Ill . Reg . 16517, effective September 20, 1990
;
amended in R90-21 at 14 Ill . Reg . 20448, effective December 11, 1990
; amended in
R90-13 at 15 Ill . Reg . 1562, effective January 22, 1991
; amended in R91-3 at 16
111
. Reg
. 19010, effective December 1, 1992 ; amended in R92-3 at 17 Ill . Reg .
7796, effective May 18, 1993 ; amended in R93-1 at 17 111 . Reg
. 12650, effective
July 23, 1993 ; amended in R94-4 at 18 111 . Reg . 12291, effective July 28, 1994
;
amended in R94-23 at 19 111 . Reg . 8613, effective June 20, 1995
; amended in P95-
17 at 20 Ill . Reg . 14493, effective October 22, 1996
; amended in R98-2 at 22
Ill . Reg . 5020, effective March 5, 1998 ; amended in R99-6 at 23 111
. Reg . 2756,
effective February 17, 1999
; amended in R99-12 at 23 111 . Reg . 10348, effective
August 11, 1999
; amended in R00-8 at 23 111 . Reg . 14715, effective December 8,
1999 ; amended in R00-10 at 24 Ill . Reg . 14226, effective September 11, 2000 ;
amended in R01-7 at 25 111 . Reg . 1329, effective January 11, 2001 ; amended in
RO1-20 at 25 111 . Reg . 13611, effective October 9, 2001
; amended in R02-5 at 26
111 . Reg . 3522, effective February 22, 2002 ; amended in R03-4 at 27 111
. Reg .
1183, effective January 1D, 2003
; amended in R03-15 at 27 111 . Reg . 16447,
effective October 10, 2003
; amended in R04-3 at 28 111 . Reg . 5269, effective
March 10, 2004 ; amended in R04-13 at 28 Ill . Reg . 12666, effective August 26,
2004 ; amended in R05-6 at 29 Ill . Reg . 2287, effective January 28, 2005 ; amended
in
SUBPART
R06-15
A :
at
GENERAL30
Ill . Reg . -, effective
Section 611 .102
Incorporations by Reference
a)
Abbreviations and short-name listing of references
. The following names
and abbreviated names, presented in alphabetical order, are used in this Part to
refer to materials incorporated by reference :
"Amco-AEPA-1 Polymer" is available from Advanced Polymer Systems .
"ASTM Method" means a method published by and available from the American
Society for Testing and Materials (ASTM) .
"Colisure Test" means "Colisure Presence/Absence Test for Detection and
Identification of Coliform Bacteria and Escherichia Coli in Drinking Water,"
available from Millipore Corporation, Technical Services Department .
"Colitaga Test" means "Colitaga Product as a Test for Detection and
Identification of Coliforms and E . coli Bacteria in Drinking Water and Source
Water as Required in National Primary Drinking Water Regulations," available
from CPI International .
"Dioxin and Furan Method 1613" means "Tetra- through Octa- Chlorinated
Dioxins and Furans by Isotope-Dilution HRGC/HRMS," available from NTIS .
"GLI Method 2" means GLI Method 2, "Turbidity," Nov
. 2, 1992, available
from Great Lakes Instruments, Inc .
"Hach FilterTrak Method 10133" means "Determination of Turbidity by Laser
Nephelometry," available from Hach Co .
I
"HASL Procedure Manual" means HASL Procedure Manual, HASL 300, available
from ERDA Health and Safety Laboratory .
"Kelada 01" means "Kelada Automated Test Methods for Total Cyanide, Acid
Dissociable Cyanide, And Thiocyanate," Revision 1 .2, August 2001, EPA # 821-B-
01-009, available from the National Technical Information Service (NTIS) .
"Membrane Filter Technique using Chromocult Dolifarm Agar" means
"Chromocult Coliform Agar Presence/Absence Membrane Filter Test Method for
Detection and Identification of Coliform Bacteria and Escherichia coli in
Finished Waters," available from EMD Chemicals Inc .
"NCRP" means "National Council on Radiation Protection ."
"NTIS" means "National Technical Information Service ."
"New Jersey Radium Method" means "Determination of Radium 228 in Drinking
Water," available from the New Jersey Department of Environmental Protection .
"New York Radium Method" means "Determination of Ra-226 and Ra-228 (Ra-
02),"
available from the New York Department of Public Health .
"ONGP-MUG Test" (meaning "minimal medium ortho-nitrophenyl-beta-d-
galactopyranoside-4-methyl-umbelliferyl -beta-d-glucuronide test"), also called
the "Autoanalysis Colilert System," is Method 9223, available in "Standard
Methods for the Examination of Water and Wastewater," 18th ed
., from American
Public Health Association .
"Palintest Method 1001" means "Method Number 1001," available from
Palintest, Ltd, or the Hach Company .
"QuikChem Method 10-204-00-1-X" means "Digestion and distillation of total
cyanide in drinking and wastewaters using MICRO DIST and determination of
cyanide by flow injection analysis," available from Lachat Instruments
.
"Readycult Coliforms 100 Presence/Absence Test" means "Readycult Coliforms
100 Presence/Absence Test for Detection and Identification of Coliform Bacteria
and Escherichia coli in Finished Waters," available from EMD Chemicals Inc .
"SimPlate Method" means "IDEXX SimPlate TM HPC Test Method for
Heterotrophs in Water," available from IDEXX Laboratories, Inc
.
"Radiochemical Methods" means "Interim Radiochemical Methodology
for
Drinking Water," available from NTIS .
"Standard Methods" means "Standard Methods for the Examination of Water
and Wastewater," available from the American Public Health Association or the
American Waterworks Association .
"Syngenta AG-625" means "Atrazine in Drinking Water by Immunoassay,"
February 2001 is available from Syngenta Crop Protection, Inc .
"Technical Bulletin 601" means "Technical Bulletin 601, Standard Method of
Testing for Nitrate in Drinking Water," July 1994, available from Analytical
Technology, Inc .
"Technicon methods" means "Fluoride in Water and Wastewater," available
from Bran & Luebbe .
"USDOE Manual" means "EMI, Procedures Manual," available from the United
State Department of Energy
.
"USEPA Asbestos Methods-100
.1" means Method 100 .1, "Analytical Method for
Determination of Asbestos Fibers in Water," September 1983, available from NTIS .
"USEPA Asbestos Methods-100
.2" means Method 100 .2, "Determination of
Asbestos Structures over 10-mm in Length in Drinking Water," June 1994,
available from NTIS .
"USEPA Environmental Inorganics Methods" means "Methods for the
Determination of Inorganic Substances in Environmental Samples," August 1993,
available from NITS .
"USEPA Environmental Metals Methods" means "Methods for the Determination
of Metals in Environmental Samples," available from NTIS
.
"USEPA Inorganic Methods" means "Methods for Chemical Analysis of Water
and Wastes," March 1983, available from NTIS
.
"USEPA Interim Radiochemical Methods" means "Interim Radiochemical
Methodology for Drinking Water," EPA 600/4-75-DOS (revised), March 1976
.
Available from NTIS .
"USEPA Organic Methods" means "Methods for the Determination of organic
Compounds in Drinking Water," July 1991, for Methods 502
.2, 505, 507, 508, 508A,
515 .1, and 531 .1 ; "Methods for the Determination of organic compounds in
Drinking Water -- Supplement I," July 1990, for Methods 506, 547, 550, 550
.1,
and 551
; and "Methods for the Determination of organic Compounds in Drinking
Water --
Supplement II," August 1992, for Methods 515 .2, 524 .2, 548 .1, 549 .1,
552 .1, and 555, available from NTIS . Methods 504
.1, 508 .1, and 525 .2 are
available from EPA EMSL
; "Methods for the Determination of Organic Compounds" in
Drinking Water -- Supplement II, August 1992, for Method 552
.1 ; "Methods for the
Determination of organic compounds in Drinking Water
-- Supplement III," August
1995, for Methods 502
.2, 524 .2, 551 .1, and 552 .2 . Method 515
.4, "Determination
of Chlorinated Acids in Drinking Water by
Liquid-Liquid Microextraction,
Derivatization and Fast Gas Chromatography with Electron Capture Detection,"
Revision 1 .0, April 2000, EPA 815/B-00/001, and method 531
.2, "Measurement of N-
methylcarbamoyloximes and N-methylcarbamates in Water by Direct Aqueous
Injection HPLC with Postcolumn Derivatization," Revision 1
.0, September 2001,
EPA 815/B/01/002, are both available on-line from USEPA, Office of Ground Water
and Drinking Water .
"USEPA Radioactivity Methods" means "Prescribed Procedures for Measurement
of Radioactivity in Drinking Water," EPA 600/4-80-032, August 1980 . Available
from NTIS .
"USEPA Radiochemical Analyses" means "Radiochemical Analytical Procedures
for Analysis of Environmental Samples," March 1979 . Available from NTIS .
"USEPA Radiochemistry Methods" means "Radiochemistry Procedures Manual,"
EPA 520/5-84-006, December 1987 . Available from NTIS .
°USEPA Technical Notes" means "Technical Notes on Drinking Water methods,"
available from NTIS .
"USGS Methods" means
"Methods of
Analysis by the U.S . Geological Survey
National Water Quality Laboratory -- Determination of Inorganic and Organic
Constituents in Water and Fluvial Sediments," available from NTIS and USGS .
"Waters Method B-1011" means "Waters Test Method for the Determination of
Nitrite/Nitrate in Water Using Single Column Ion Chromatography," available from
Waters Corporation, Technical Services Division .
b)
The Board incorporates the following publications by reference ;
Advanced Polymer Systems, 3696 Haven Avenue, Redwood City, CA 94063 415-
366-2626 .
Amco-AEPA-l Polymer
. See 40 CFR 141 .22(a) (2003 ) ( 2005) . Also, as
referenced in ASTM D1889 .
American Public Health Association, 1015 Fifteenth Street NW, Washington,
DC 20005 800-645-5476 .
"Standard Methods for the Examination of Water and Wastewater," 17th
Edition, 1989 (referred to as "Standard Methods, 17th ed .") .
"Standard Methods for the Examination of Water and Wastewater," 18th
Edition, 1992, including "Supplement to the 18th Edition of Standard Methods for
the Examination of Water and Wastewater," 1994 (collectively referred to as
"Standard Methods, 18 th ed .") .
See the methods listed separately for the same
references under American Waterworks Association .
"Standard Methods for the Examination of Water and Wastewater," 19 th
Edition, 1995 (referred to as "Standard Methods, 19 th ed .")
.
"Standard Methods for the Examination of Water and Wastewater," 20th
Edition, 1998 (referred to as "Standard Methods, 20th ed .") .
American Waterworks Association et al ., 6666 West Quincy Ave
., Denver, CO
80235 303-794-7711 .
"National Field Evaluation of a Defined Substrate Method for the Simultaneous
Enumeration of Total Coliforms and Escherichia coli for Drinking Water :
Comparison with the Standard Multiple Tube Fermentation Method," S .C . Edberg,
M
.J
. Allen & D .B . Smith, Applied Environmental Microbiology, vol . 54, iss . 6, pp
1595-1601 (1988) .
"Standard Methods for the Examination of Water and Wastewater," 13th
Edition, 1971 (referred to as "Standard Methods, 13th ed.") .
Method 302, Gross Alpha and Gross Beta Radioactivity in Water (Total,
Suspended, and Dissolved) .
I
I
Method 303, Total Radioactive Strontium and Strontium 90 in Water
.
Method 304, Radium in Water by Precipitation .
Method 305, Radium 226 by Radon in Water (Soluble, Suspended, and Total)
.
Method 306, Tritium in Water .
"Standard Methods for the Examination of Water and Wastewater," 17th Edition,
1989 (referred to as "Standard Methods, 17th
ed.") .
Method 7110 B, Gross Alpha and Gross Beta Radioactivity in Water (Total,
Suspended, and Dissolved) .
Method 7500-Cs B, Radioactive Cesium, Precipitation Method .
Method 7500-3H B, Tritium in Water
.
Method 7500-I B, Radioactive Iodine, Precipitation Method
.
Method 7500-I C, Radioactive Iodine, Ion-Exchange Method .
Method 7500-I D, Radioactive Iodine,
Distillation Method .
Method 7500-Ra B, Radium in Water by Precipitation .
Method 7500-Ra C, Radium 226 by Radon in Water (Soluble, Suspended, and Total) .
Method 7500-Ra D, Radium, Sequential Precipitation Method (Proposed)
.
Method 7500-Sr B, Total Radioactive Strontium and Strontium 90 in Water .
Method 7500-U B, Uranium, Radiochemical Method (Proposed)
.
Method 7500-U C, Uranium, Isotopic Method (Proposed) .
"Standard Methods for the Examination of Water and Wastewater," 18th
Edition, 1992 (referred to as "Standard Methods, 18 th
ed.") .
Method 2130 B, Turbidity, Nephelometric Method
.
Method 2320 B, Alkalinity, Titration Method
.
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory and Field Methods .
Method 3111 B, Metals by Flame Atomic Absorption Spectrometry, Direct Air-
Acetylene Flame Method .
Method 3111 D, Metals by Flame Atomic Absorption Spectrometry, Direct
Nitrous Oxide-Acetylene Flame Method .
Method 3112 B, Metals by Cold-vapor Atomic Absorption Spectrometry, Cold-
Vapor Atomic Absorption Spectrometric Method .
Method 3113 B, Metals by Electrothermal Atomic Absorption Spectrometry,
Electrothermal Atomic Absorption Spectrometric Method .
Method 3114 B, Metals by Hydride Generation/Atomic Absorption
Spectrometry,
Manual Hydride Generation/Atomic Absorption Spectrometric Method
.
Method 3120 B, Metals by Plasma Emission Spectroscopy, Inductively Coupled
Plasma (ICP) Method .
Method 3500-Ca D, Calcium, EDTA Titrimetric Method
.
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion Chromatography, Ion
Chromatography with Chemical Suppression of Eluent Conductivity .
Method 4500-CN- C, Cyanide, Total Cyanide after Distillation
.
Method 4500-CN- E, Cyanide, Colorimetric Method
.
Method 4500-CN- F, Cyanide, Cyanide-Selective Electrode Method .
Method 4500-CN- G, Cyanide, Cyanides Amenable to Chlorination after
Distillation .
Method 4500-Cl D, Chlorine, Amperometric Titration Method
.
Method 4500-Cl E, Chlorine, Low-Level Amperometric Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method
.
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS) Method .
Method 4500-Cl I, Chlorine, Iodometric Electrode Method
.
Method 4500-C102 C, Chlorine Dioxide, Amperometric Method I .
Method 4500-C102 D, Chlorine Dioxide, DPD Method
.
Method 4500-C102 E, Chlorine Dioxide, Amperometric Method II (Proposed) .
Method 4500-H+ B, pH Value, Electrometric Method .
Method 4500-NO2- B, Nitrogen (Nitrite), Colorimetric Method .
Method 4500-N03- D, Nitrogen (Nitrate), Nitrate Electrode Method .
Method 4500-N03- E, Nitrogen (Nitrate), Cadmium Reduction Method .
Method 4500-NO3- F, Nitrogen (Nitrate), Automated Cadmium Reduction
Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-F- B, Fluoride, Preliminary Distillation Step .
Method 4500-F- C, Fluoride, Ion-Selective Electrode Method .
Method 4500-F- D, Fluoride,
SPADNS Method .
Method 4500-F- E,
Fluoride, Complexone Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid Reduction Method .
Method 4500-Si D, Silica, Molybdosilicate Method .
Method 4500-Si E, Silica, Heteropoly Blue Method .
Method 4500-Si F, Silica, Automated Method for Molybdate-Reactive Silica .
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110 B, Gross Alpha and Beta Radioactivity (Total, Suspended, and
Dissolved), Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity (Total, Suspended, and
Dissolved), Coprecipitation Method for Gross Alpha Radioactivity in Drinking
Water (Proposed) .
Method 7500-Cs B, Radioactive Cesium, Precipitation Method .
Method 7500-3 H B, Tritium, Liquid Scintillation
Spectrometric Method
.
Method 7500-I B, Radioactive Iodine, Precipitation Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange Method .
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method
.
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Ra D, Radium, Sequential Precipitation Method (Proposed) .
Method 7500-Sr B, Total Radioactive Strontium and Strontium 90,
Precipitation Method .
Method 7500-U B, Uranium, Radiochemical Method (Proposed)
.
Method 7500-U C, Uranium, Isotopic Method (Proposed) .
Method 9215 B, Heterotrophic Plate Count, Pour Plate Method .
Method 9221 A, Multiple-Tube Fermentation Technique for Members of the
Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique for Members of the
Coliform Group, Standard Total Coliform Fermentation Technique .
Method 9221 C, Multiple-Tube Fermentation Technique for Members of the
Coliform Group, Estimation of Bacterial Density .
Method 9221 D, Multiple-Tube Fermentation Technique for Members of the
Coliform Group, Presence-Absence
(P-A)
Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique for Members of the
Coliform Group, Fecal Coliform Procedure .
Method 9222 A, Membrane Filter Technique for Members of the Coliform
Group, Introduction .
Method 9222 B, Membrane Filter Technique for Members of the Coliform
Group, Standard Total Coliform Membrane Filter Procedure .
Method 9222 C, Membrane Filter Technique for Members of the Coliform
Group, Delayed-Incubation Total Coliform Procedure .
Method 9222 D, Membrane Filter Technique for Members of the Coliform
Group, Fecal Coliform Membrane Filter Procedure
.
Method 9223, Chromogenic Substrate Coliform Test (Proposed) .
"Supplement to the 18th Edition of Standard Methods for the Examination of Water
and Wastewater," American Public Health Association, 1994 .
Method 6610, Carbamate Pesticide Method
.
"Standard Methods for the Examination of Water and Wastewater," 19th
Edition, 1995 (referred to as "Standard Methods, 19th ed.") .
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method .
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory, and Field Methods .
Method 3111 B, Metals by Flame Atomic Absorption Spectrometry, Direct Air-
Acetylene Flame Method .
Method 3111 D, Metals by Flame Atomic Absorption Spectrometry, Direct
Nitrous Oxide-Acetylene Flame Method .
Method 3112 B, Metals by Cold-Vapor Atomic Absorption Spectrometry, Cold-
Vapor Atomic Absorption Spectrometric Method .
Method 3113 B, Metals by Electrothermal Atomic Absorption Spectrometry,
Electrothermal Atomic Absorption Spectrometric Method .
Method 3114 B, Metals by Hydride Generation/Atomic Absorption
Spectrometry, Manual Hydride Generation/Atomic Absorption Spectrometric Method .
Method 3120 B, Metals by Plasma Emission Spectroscopy, Inductively Coupled
Plasma (ICP) Method .
Method 3500-Ca D, Calcium, EDTA Titrimetric Method .
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion Chromatography, Ion
Chromatography with Chemical Suppression of Eluent Conductivity .
Method 4500-Cl D, Chlorine, Amperometric Titration Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric Method
.
Method 4500-Cl G, Chlorine, DPD Colorimetric Method .
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS) Method .
Method 4500-Cl I, Chlorine, Iodometric Electrode Method
.
Method 4500-C102 C, Chlorine Dioxide, Amperometric Method I
.
Method 4500-Cl02 D, Chlorine Dioxide, DPD Method .
Method 4500-C1o2 E, Chlorine Dioxide, Amperometric Method II (Proposed)
.
Method 4500-CN- C, Cyanide, Total Cyanide after Distillation
.
Method 4500-CN- E, Cyanide, Colorimetric Method .
Method 4500-CN- F, Cyanide, Cyanide-Selective Electrode Method
.
Method 4500-CN- G, Cyanide, Cyanides Amenable to Chlorination after
Distillation .
Method 4500-F- B, Fluoride, Preliminary Distillation Step .
Method 4500-F- C, Fluoride, Ton-Selective Electrode Method .
Method 4500-F- D, Fluoride, SPADNS Method .
Method 4500-F- E, Fluoride, Complexone Method .
Method 4500-H+ B, pH Value, Electrometric Method .
Method 4500-NO2- B, Nitrogen (Nitrite), Colorimetric Method .
Method 4500-N03- D, Nitrogen (Nitrate), Nitrate Electrode Method .
Method 4500-N03- E, Nitrogen (Nitrate), Cadmium Reduction Method .
Method 4500-N03- F, Nitrogen (Nitrate), Automated Cadmium Reduction
Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid Reduction Method .
Method 4500-Si D, Silica, Molybdosilicate Method .
Method 4500-Si E, Silica, Heteropoly Blue Method
.
Method 4500-Si F, Silica, Automated Method for Molybdate-Reactive Silica .
Method 5910 B, UV Absorbing Organic Constituents, Ultraviolet Absorption
Method .
Method 6251 B, Disinfection Byproducts : Haloacetic Acids and
Trichlorophenol, Micro Liquid-Liquid Extraction Gas Chromatographic Method .
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110 B, Gross Alpha and Gross Beta
Radioactivity, Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method for Gross Alpha
Radioactivity in Drinking Water (Proposed) .
Method 7120 B, Gamma-Emitting Radionuclides, Gamma Spectrometric Method .
Method 7500-Cs B, Radioactive Cesium, Precipitation Method .
Method 7500-3H B, Tritium, Liquid Scintillation
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange Method
.
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Ra D, Radium, Sequential Precipitation Method
.
Method 7500-Sr B, Total Radiactive Strontium and Strontium 90, Precipitation
Method .
Method 7500-U B, Uranium, Radiochemical Method .
Method 7500-U C, Uranium, Isotopic Method
.
Method 9215 B, Heterotrophic Plate Count, Pour Plate Method .
Method 9221 A, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Introduction .
Method 9221 8, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Standard Total Coliform Fermentation Technique .
Method 9221 C, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Estimation of Bacterial Density .
Method 9221 D, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Presence-Absence (P-A) Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Fecal Coliform Procedure .
Method
9222 A, Membrane Filter Technique for Members of the Coliform Group,
Introduction .
Method 9222 B, Membrane Filter Technique for Members of the Coliform Group,
Standard Total Coliform Membrane Filter Procedure .
Method 9222 C, Membrane Filter Technique for Members of the Coliform Group,
Delayed-Incubation Total Coliform Procedure .
Method 9222 D, Membrane Filter Technique for Members of the Coliform Group,
Fecal Coliform Membrane Filter Procedure .
Method 9223, Chromogenic Substrate Coliform Test (Proposed)
.
"Supplement to the 19th Edition of Standard Methods for the Examination of
Water and Wastewater," American Public Health Association, 1996
.
Method 5310 B, TOC, Combustion-Infrared Method .
Method 5310 C, TOC, Persulfate-Ultraviolet Oxidation Method .
Method 5310 D, TOC, Wet-Oxidation Method .
"Standard Methods for the Examination of Water and Wastewater," 20th Edition,
1998 (referred to as "Standard Methods, 20th ed .") .
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method .
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory, and Field Methods .
Method 3120 B, Metals by Plasma Emission Spectroscopy, Inductively Coupled
Plasma (ICP) Method .
Method 3500-Ca B, Calcium, EDTA Titrimetric Method
.
Method 3500-Mg B, Magnesium, EDTA Titrimetric Method .
Method 4110 B, Determination of Anions by Ion Chromatography, Ion Chromatography
with Chemical Suppression of Eluent Conductivity .
Method 4500-CN- C, Cyanide, Total Cyanide after Distillation
.
Method 4500-CN- E, Cyanide, Colorimetric Method .
Method 4500-CN- F, Cyanide, Cyanide-Selective Electrode Method .
Method 4500-CN- G, Cyanide, Cyanides Amenable to Chlorination after
Distillation .
Method 4500-Cl D, Chlorine, Amperometric Titration Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric Titration Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo Colorimetric Method .
Method
4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid Reduction Method .
Method 4500-Si C, Silica, Molybdosilicate Method .
Method 4500-Si D, Silica, Heteropoly Blue Method .
Method 4500-Si
Method 4500-Cl
Method 4500-Cl
Method 4500-Cl
Method 4500-Cl
Method 4500-Cl
E, Silica, Automated Method for Molybdate-Reactive Silica .
E, Chlorine (Residual), Low-Level Amperometric Titration Method .
F, Chlorine (Residual), DPD Ferrous Titrimetric Method .
G, Chlorine (Residual), DPD Colorimetric Method .
H, Chlorine (Residual), Syringaldazine (FACTS) Method .
I, Chlorine (Residual), lodometric Electrode Technique .
Method 4500-C102 D, Chlorine Dioxide, DPD Method
.
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method
.
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS) Method .
Method 4500-Cl I, Chlorine, Iodometric Electrode Method .
Method 4500-C102 C, Chlorine Dioxide, Amperometric Method I .
Method 4500-C102 D, Chlorine Dioxide, DPD Method .
Method 4500-C102 E, Chlorine Dioxide, Amperometric Method II (Proposed) .
Method 4500-F- B, Fluoride, Preliminary Distillation Step .
Method 4500-F- C, Fluoride, Ion-Selective Electrode Method .
Method 4500-F- D, Fluoride, SPADNS Method .
Method 4500-F- E, Fluoride, Complexone Method .
Method 4500-H+ B, pH Value, Electrometric Method
.
Method 4500-N02- B, Nitrogen (Nitrite), Colorimetric Method .
Method 4500-N03- D, Nitrogen (Nitrate), Nitrate Electrode Method .
Method 4500-N03- E, Nitrogen
(Nitrate), Cadmium Reduction Method .
Method 4500-N03- F, Nitrogen (Nitrate), Automated Cadmium Reduction Method
.
Method 4500-C102 E, Chlorine Dioxide, Amperometric Method II .
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110-B, Gross Alpha and Gross Beta Radioactivity, Evaporation Method for
Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity (Total, Suspended, and
Dissolved), Coprecipitation Method for Gross Alpha Radioactivity in Drinking
Water (Proposed) .
Method 7120-B, Gamma-Emitting Radionuclides, Gamma Spectrometric Method
.
Method 7500-Cs B, Radioactive Cesium, Precipitation Method .
Method 7500-3H B, Tritium, Liquid Scintillation Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange Method .
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Sr B, Total Radiactive Strontium and Strontium 90, Precipitation
Method .
Method 7500-U B, Uranium, Radiochemical Method .
Method 7500-U C, Uranium, Isotopic Method
.
Method 9215 B, Heterotrophic Plate Count, Pour Plate Method
.
Method 9221 A, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Standard Total Coliform Fermentation Technique
.
Method 9221 C, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Estimation of Bacterial Density .
Method 9221 D, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Presence-Absence (P-A) Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique for Members of the Coliform
Group, Fecal Coliform Procedure .
Method 9222 A, Membrane Filter Technique for Members of the Coliform Group,
Introduction .
Method 9222 B, Membrane Filter Technique for Members of the Coliform Group,
Standard Total Coliform Membrane Filter Procedure .
Method 9222 C,
Membrane Filter Technique for Members of the Coliform Group,
Delayed-Incubation Total Coliform Procedure
.
Method 9222 D, Membrane Filter Technique for Members of the Coliform Group,
Fecal Coliform Membrane Filter Procedure .
Method 9223, Chromogenic Substrate Coliform Test (Proposed) .
Analytical Technology, Inc
. ATI Orion, 529 Main Street, Boston, MA 02129 .
Technical Bulletin 601, "Standard Method of Testing for Nitrate in
Drinking Water," July, 1994, PN 221890-001 (referred to as "Technical Bulletin
601") .
ASTM
. American Society for Testing and Materials, 100 Barr Harbor Drive,
West Conshohocken, PA 19428-2959 610-832-9585
.
ASTM Method D511-93 A and B, "Standard Test Methods for Calcium and
Magnesium in Water," "Test Method A --
Complexometric Titration" & "Test Method
B -- Atomic Absorption Spectrophotometric," approved 1993
.
ASTM Method D515-88 A, "Standard Test Methods for Phosphorus in Water,"
"Test Method A
-- Colorimetric Ascorbic Acid Reduction," approved August 19,
1988 .
ASTM Method D859-88, "Standard Test Method for Silica in Water," approved
August 19, 1988 .
ASTM Method D1067-92 B, "Standard Test Methods for Acidity or Alkalinity
in Water," "Test Method B -- Electrometric or Color-Change Titration," approved
May 15, 1992 .
ASTM Method D1125-91 A, "Standard Test Methods for Electrical Conductivity
and Resistivity of Water," "Test Method A --
Field and Routine Laboratory
Measurement of Static (Non-Flowing) Samples," approved June 15, 1991
.
ASTM Method D1179-93 B, "Standard Test Methods for Fluoride in Water,"
"Test Method B
-- Ion Selective Electrode," approved 1993 .
ASTM Method D1253-86, "Standard Test Method for Residual Chlorine in Water,"
reapproved 1992 .
ASTM Method D1293-84, "Standard Test Methods for pH of Water," "Test
Method A
-- Precise Laboratory Measurement" & "Test Method B --
Routine or
Continuous Measurement," approved October 26, 1984
.
ASTM Method D1688-90 A or C, "Standard Test Methods for Copper in Water,"
"Test Method A -- Atomic Absorption, Direct" & "Test Method C- -Atomic
Absorption, Graphite Furnace," approved March 15, 1990
.
ASTM Method D2036-91 A or B, "Standard Test methods for cyanide in water,"
"Test Method A --
Total Cyanides after Distillation" & "Test Method B
--
Cyanides Amenable to Chlorination by Difference," approved September 15, 1991
.
I
I
I
ASTM Method D2459-72, "Standard Test Method for Gamma Spectrometry in
Water," approved
July 28, 1972, discontinued 1988
.
I
I
ASTM Method D2460-90, "Standard Test Method for Radionuclides of Radium in
Water," approved 1990 .
ASTM Method D2907-91, "Standard Test Methods for Microquantities of
Uranium in water by Fluorometry," "Test Method A -- Direct Fluorometric" & "Test
Method B - Extraction," approved June 15, 1991 .
ASTM Method D2972-93 B or C, "Standard Test Methods for Arsenic in Water,"
"Test Method B -- Atomic Absorption, Hydride Generation" & "Test Method C --
Atomic Absorption, Graphite Furnace," approved 1993 .
ASTM Method D3223-91, "Standard Test Method for Total Mercury in Water,"
approved September 23, 1991 .
ASTM Method D3454-91, "Standard Test Method for Radium-226 in Water,"
approved 1991 .
ASTM Method D3559-90 D, "Standard Test Methods for Lead in Water," "Test
Method D --
Atomic Absorption, Graphite Furnace," approved August 6, 1990 .
ASTM Method D3645-93 B, "Standard Test Methods for Beryllium in Water,"
"Method B -- Atomic Absorption, Graphite Furnace," approved 1993 .
ASTM Method D3649-91, "Standard Test Method for High-Resolution Gamma-Ray
Spectrometry of Water," approved 1991 .
ASTM Method D3697-92, "Standard Test Method for Antimony in Water,"
approved June 15, 1992 .
ASTM Method D3659-93 A, "Standard Test Methods for Selenium in Water,"
"Method A -- Atomic Absorption, Hydride Method," approved 1993
.
ASTM Method D3867-90 A and B, "Standard Test Methods for Nitrite-Nitrate
in Water," "Test Method A -- Automated Cadmium Reduction" & "Test Method B --
Manual Cadmium Reduction," approved January 10, 1990 .
ASTM Method D3972-90, "Standard Test Method for Isotopic Uranium in Water
by Radiochemistry," approved 1990 .
ASTM Method D4107-91, "Standard Test Method for Tritium in Drinking
Water," approved 1991 .
ASTM Method D4327-91, "Standard Test Method for Anions in Water by Ion
Chromatography," approved October 15, 1991 .
ASTM Method D4785-88, "Standard Test Method for Low-Level Iodine-131 in
Water," approved 1988 .
ASTM Method D5174-91, "Standard Test Method for Trace Uranium in Water by
Pulsed-Laser Phosphorimetry," approved 1991 .
ASTM Method D5673-03, "Standard Test Method for Elements in Water by Inductively
Coupled Plasma - Mass Spectrometry, " approved 2003 .
I
Bran & Luebbe, 1025 Busch Parkway, Buffalo Grove, IL 60089 .
"Fluoride in Water and Wastewater," Industrial Method #129-71W, December
1972 (referred to as "Technicon Methods : Method #129-71W") . See 40 CFR
141
.23(k)(1), footnote 11 (2003) ( 2005) .
"Fluoride in Water and Wastewater," #380-75WE, February 1976 (referred to
as "Technicon Methods : Method #380-75WE") . See 40 CFR 141 .23(k)(1), footnote
11
(2003)
( 2005) .
CPI International, Inc ., 5580 Skylane Blvd .
. Santa Rosa, CA 95403 . Telephone :
800-878-7654 . Fax : 707-545-7901
. Internet address : www .cpiinternational .com .
"Colitaga Product as a Test for Detection and Identification of Coliforms and E
.
coli Bacteria in Drinking Water and Source Water as Required in National Primary
Drinking Water Regulations," August 2001 .
EMD Chemicals Inc
. (an affiliate of Merck KGgA, Darmstadt, Germany), 480 S .
Democrat Road, Gibbstown, NJ 08027-1297 . Telephone
: 800-222-0342 . E -mail :
adellenbusc h®emscience .com .
"Chromocult Coliform Agar Presence/Absence Membrane Filter Test Method for
Detection and Identification of Coliform Bacteria and Escherichia coli in
Finished Waters," November 2000, Version 1 .0 .
"Readycult Coliforms 100 Presence/Absence Test for Detection and Identification
of Coliform Bacteria and Escherichia coli in Finished Waters," November 2000,
Version 1.0 .
ERDA Health and Safety Laboratory, New York, NY .
HASL Procedure Manual, HASL 300, 1973
. See 40 CFR 141 .25(b)(2) (2003)
42005) .
Great Lakes Instruments, Inc
., 8855 North 55th Street, Milwaukee, WI
53223 .
GLI Method 2, "Turbidity," Nov
. 2, 1992 .
The Hach Company, P .O . Box 389, Loveland, CO 80539-0389 . Phone : 800-227-
4224 .
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
"Determination of Turbidity by Laser Nephelometry," January 2000, Revision 2
.0
(referred to as "Hach FilterTrak Method 10133")
.
IDEXX Laboratories, Inc ., One IDEXX Drive, Westbrook, Maine 04092
. Telephone :
800-321-0207 .
"IDEXX SimPlate TM HPC Test Method for Heterotrophs in Water," November 2000
.
Lachat Instruments, 6645 W
. Mill Rd ., Milwaukee, WI 53218 . Phone
: 414-358-
4200 .
I
"Digestion and distillation of total cyanide in drinking and wastewaters using
MICRO DIST and determination of cyanide by flow injection analysis," Revision
2
.1, November 30, 2000 (referred to as "QuikChem Method 10-204-00-1-X")
.
Millipore Corporation, Technical Services Department, 80 Ashby Road,
Milford, MA 01730 800-654-5476 .
Colisure Presence/Absence Test for Detection and Identification of
Coliform Bacteria and Escherichia Coli in Drinking Water, February 28, 1994
(referred to as "Colisure Test") .
NCRP . National Council on Radiation Protection, 7910 Woodmont Ave .,
Bethesda, MD 301-657-2652
.
"Maximum Permissible Body Burdens and Maximum Permissible Concentrations
of Radionuclides in Air and in Water for Occupational Exposure," NCRP Report
Number 22, June 5, 1959 .
NSF
. National Sanitation Foundation International, 3475 Plymouth Road, PO
Box 130140, Ann Arbor, Michigan 48113-0140, 734-769-8010 .
NSF Standard 61, section 9, November 1998 .
NTIS . National Technical Information Service, U .S
. Department of
Commerce, 5285 Port Royal Road, Springfield, VA 22161, 703-487-4600 or 800-553-
6847 .
"Interim Radiochemical Methodology for Drinking Water," EPA 600/4-75-008
(revised), March 1976 (referred to as "USEPA Interim Radiochemical Methods") .
(Pages 1, 4, 6, 9, 13, 16, 24, 29, 34)
"Kelada Automated Test Methods for Total Cyanide, Acid Dissociable Cyanide, And
Thiocyanate," Revision 1 .2, August 2001, EPA # 821-B-01-009 (referred to as
"Kelada 01") .
"Maximum Permissible Body Burdens and Maximum Permissible Concentrations
of Radionuclides in Air and in Water for Occupational Exposure," NBS (National
Bureau of Standards) Handbook 69, as amended August 1963, U .S
. Department of
Commerce .
Method 100 .1, "Analytical Method for Determination of Asbestos Fibers in
Water," EPA-600/4-83-043, September 1983, Doc . No
. PB83-260471 (referred to as
"USEPA Asbestos Methods-100
.1") .
Method 100
.2, "Determination of Asbestos Structures over 10-mm in Length
in Drinking Water," EPA-600/4-83-043, June 1994, Doc
. No . PE94-201902 (referred
to as "USEPA Asbestos Methods-100 .2") .
"Methods for Chemical Analysis of Water and Wastes," March 1983, Doc
. No .
PB84-128677 (referred to as "USEPA Inorganic Methods") . (Methods 150
.1, 150 .2,
and 245
.2, which formerly appeared in this reference, are available from USEPA
EMSL .)
"Methods for the Determination of Inorganic Substances in Environmental
Samples," August 1993, PB94-120821 (referred to as "USEPA Environmental
Inorganic Methods") .
"Methods for the Determination of Metals in Environmental Samples," June
1991, Doc . No
. PB91-231498 and "Methods for the Determination of Metals in
Environmental
Samples -- Supplement I,"
May 1994, PB95-125472 (referred to as
"USEPA Environmental Metals Methods") .
"Methods for the Determination of Organic Compounds in Drinking Water,"
December 1988, revised July 1991, EPA-600/4-88/039 (referred to as "USEPA
Organic Methods") .
(For methods 502 .2, 505, 507, 508, 508A, 515 .1, and 531
.1 .)
"Methods for the Determination of Organic Compounds in Drinking Water
Supplement I," July 1990, EPA/600-4-90-020 (referred to as "USEPA Organic
Methods") .
(For methods 506, 547, 550, 550 .1, and 551 .)
"Methods for the Determination of Organic Compounds in Drinking Water
Supplement II," August 1992, EPA-600/R-92-129 (referred to as "USEPA Organic
Methods") .
(For methods 515 .2, 524 .2, 548 .1, 549 .1, 552 .1, and 555
.)
"Prescribed Procedures for Measurement of Radioactivity in Drinking
Water," EPA 600/4-80-032, August 1980 (document number PB 80-224744) (referred
to as "USEPA Radioactivity Methods") . (Methods 900, 901, 901 .1, 902, 903,
903
.1, 904, 905, 906, 908, 908 .1)
"Procedures for Radiochemical Analysis of Nuclear Reactor Aqueous
Solutions," H .L . Krieger and S . Gold, EPA-R4-73-014, May 1973, Doc
. No . PB222-
154/7BA .
"Radiochemical Analytical Procedures for Analysis of Environmental
Samples," March 1979, Doc . No . EMSL IV 053917 (referred to as "USEPA
Radiochemical Analyses") .
(Pages 1, 19, 33, 65, 87, 92)
"Radiochemistry Procedures Manual," EPA-520/5-84-006, December 1987, Doc
.
No . PB-84-215581 (referred to as "USEPA Radiochemistry Methods")
. (Methods 00-
01, 00-02, 00-07, H-02, Ra-03, Ra-04, Ra-05, Sr-04)
"Technical Notes on Drinking Water Methods," EPA-600/R-94-173, October
1994, Doc . No
. PB-104766 (referred to as "USEPA Technical Notes") .
BOARD NOTE : USEPA made the following assertion with regard to this
reference at 40 CFR 141
.23(k)(1) and 141
.24(e) and (n)(11) (2003) (2005) : "This
document contains other analytical test procedures and approved analytical
methods that remain available for compliance monitoring until July 1, 1996 ."
"Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope Dilution
HRGC/HRMS," October 1994, EPA-821-B-94-005 (referred to as "Dioxin and Furan
Method 1613") .
New Jersey Department of Environment, Division of Environmental Quality,
Bureau of Radiation and Inorganic Analytical Services, 9 Ewing Street, Trenton,
NJ 08625 .
"Determination of Radium 228 in Drinking Water," August 1990 .
New York Department of Health, Radiological Sciences Institute, Center for
Laboratories and Research, Empire State Plaza, Albany, NY 12201 .
"Determination of Ra-226 and Ra-228 (Ra-02),"
January 1980, Revised June
1982 .
I
I
I
Palintest, Ltd ., 21 Kenton Lands Road, P .O . Box 18395, Erlanger, KY 800-
835-9629 .
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
Syngenta Crop Protection, Inc
., 410 Swing Road, Post Office Box 18300,
Greensboro, NC 27419 . Telephone
: 336-632-6000 .
"Atrazine in Drinking Water by Immunoassay," February 2001 (referred to as
"Syngenta AG-625") .
United States Department of Energy, available at the Environmental
Measurements Laboratory, U .S
. Department of Energy, 376 Hudson Street, New York,
NY 10014-3621 .
"EML Procedures Manual," 27th Edition, Volume 1, 1990 .
United States Environmental Protection Agency, Office of Ground Water and
Drinking Water, accessible on-line and available by download from
http ://www .epa
.gov/safewater/methods/ .
Method 515
.4, "Determination of Chlorinated Acids in Drinking Water by Liquid-
Liquid Microextraction, Derivatization and Fast Gas Chromatography with Electron
Capture Detection," Revision 1 .0, April 2000, EPA 815/B-00/001 (document file
name "met515 4 .pdf") .
Method 531
.2, "Measurement of N-methylcarbamoyloximes and N-methylcarbamates in
Water by Direct Aqueous Injection HPLC with Postcolumn Derivatization," Revision
1
.0, September 2001, EPA 815/B/01/002 (document file name "met531 2 .pdf") .
United States Environmental Protection Agency, EMSL, Cincinnati, OH 45268
513-569-7586 .
"Interim Radiochemical Methodology for Drinking Water," EPA-600/4-75-008
(referred to as "Radiochemical Methods")
. (Revised) March 1976 .
"Methods for the Determination of Organic Compounds in Finished Drinking
Water and Raw Source Water" (referred to as "USEPA Organic Methods") . (For
methods 504 .1, 508 .1, and 525 .2 only.) See NTIS .
"Procedures for Radiochemical Analysis of Nuclear Reactor Aqueous
Solutions ." See NTIS .
USEPA, Science and Technology Branch, Criteria and Standards Division,
Office of Drinking Water, Washington, D .C . 20460 .
"Guidance Manual for Compliance with the Filtration and Disinfection
Requirements for Public Water Systems using Surface Water Sources," October
1989 .
USGS . Books and Open-File Reports Section, United States Geological
Survey, Federal Center, Box 25286, Denver, CO 80225-0425 .
Methods available upon request by method number from "Methods for Analysis
by the U .S
. Geological Survey National Water Quality Laboratory -- Determination
of Inorganic and Organic Constituents in Water and Fluvial Sediments," Open File
Report 93-125, 1993, or Book 5, Chapter A-1, "Methods for Determination of
85-495,
Inorganic1989,Substancesas
appropriatein
Water
(referredand
Fluvialto
asSediments,""USGS Methods")3rd
ed
.
., Open-File
Report
1-1030-85
1-1062-85
1-1601-85
1-1700-85
I-2598-85
1-2601-90
1-2700-85
1-3300-85
Methods available upon
request by method number from "Methods for
Determination of Radioactive Substances in Water and Fluvial Sediments," Chapter
A5 in Book 5 of "Techniques of Water-Resources Investigations of the United
States Geological Survey," 1997 .
R-1110-76
R-1111-76
R-1120-76
R-1140-76
R-1141-76
R-1142-76
R-1160-76
R-1171-76
R-1180-76
R-1181-76
R-1182-76
Waters Corporation, Technical Services Division, 34 Maple St
., Milford, MA
01757 800-252-4752 .
"Waters Test Method for Determination of Nitrite/Nitrate in Water Using
Single Column Ion Chromatography," Method B-1011, August 1987 (referred to as
"Waters Method B-1011") .
c)
The Board incorporates the following federal regulations by reference
:
40 CFR 3 .2, as added at 70 Fed . Reg . 59848 (Oct
. 13, 2005) (How Does This Part
Provide for Electronic Reporting?), referenced in Section 611
.105 .
40 CFR 3 .3, as added at 70 Fed . Reg . 59848 (Oct . 13, 2005) (what Definitions Are
Applicable to This
Part?),
referenced in Section 611 .105 .
40 CFR 3 .10, as added at 70 Fed . Reg . 59848 (Oct
. 13, 2005) (What Are the
Requirements for Electronic Reporting to EPA?), referenced in Section 611
.105 .
40 CFR 3 .2000, as added at 70 Fed . Reg . 59848 (Oct . 13, 2005) (What Are the
Requirements Authorized State, Tribe, and Local Programs' Reporting Systems Must
Meet?), referenced in Section 611 .105 .
Appendix B to 40 CFR 136, Appcndicco Band C (2003)J,Ajy
(2005),
in Sections 611 .359,
611 .646 .
d)
This Part incorporates no later amendments or editions .
(Source : Amended at 30 111 . Reg . -,
effective )
Section 611 .105
Electronic Reporting
The filing of any document pursuant to any provision of this Part as an
electronic document is subject to this Section
.
a)
Scope and Applicability .
1)
The USEPA, the Board, or the Agency may allow for the filing of electronic
documents . This Section does not require submission of electronic documents in
lieu of paper documents . This Section sets forth the requirements for the
optional electronic filing of any report or document that must be submitted to
the appropriate of the following :
A)
To USEPA directly under Title 40 of the Code of Federal Regulations ; or
B)
To the Board or the Agency pursuant to any provision of 35 111 . Adm . Code
702 through 705, 720 through 728, 730, 733, 738, or 739 .
2)
Electronic document filing under this Section can begin only after USEPA
has first done as follows :
A)
As to filing with USEPA, USEPA has published a notice in the Federal
Register announcing that USEPA is prepared to receive documents required or
permitted by the identified part or subpart of Title 40 of the Code of Federal
Regulations in an electronic format ; or
B) As to filing with the State, USEPA has granted approval of any electronic
document receiving system established by the Board or the Agency that meets the
requirements of 40 CFR 3 .2000, incorporated by reference in Section 611 .102(c) .
3)
This Section does not apply to any of the following documents, whether or
not the document is a document submitted to satisfy the requirements cited in
subsection (a) (1) of this Section :
A)
Any document submitted via fascimile
;
B)
Any document submitted via magnetic or optical media, such as diskette,
compact disc, digital video disc, or tape ; or
C) Any data transfer between USEPA, any state, or any local government and
either the Board or the Agency as part of administrative arrangements between
the parties to the transfer to share data .
4)
Upon USEPA conferring approval for the filing of any types of documents as
electronic documents, as described in subsection (a) (2) (B) of this Section, the
Agency or the Board, as appropriate, must publish a Notice of Public Information
in the Illinois Register that describes the documents approved for submission as
electronic documents, the electronic document receiving system approved to
receive them, the acceptable formats and procedures for their submission, and
the date on which the Board or the Agency will begin to receive those
submissions . In the event of cessation of USEPA approval or receiving any type
of document as an electronic document, the Board or the Agency must similarly
cause publication of a Notice of Public Information in the Illinois Register .
BOARD NOTE
: Subsection (a) of this Section is derived from 40 CFR 3 .1, as added
at 70 Fed . Reg . 59848 (Oct
. 13, 2005) .
b)
Definitions . For the purposes of this Section, terms will have the
meaning attributed them in 40 CFR 3
.3, incorporated by reference in 35 111
. Adm .
Code 611
.102(c) .
c)
Procedures for submission of electronic documents to USEPA
. Except as
provided in subsection (a) (3) of this Section, any person who is required under
Title 40 of the Code of Federal Regulations to create and submit or otherwise
provide a document to USEPA may satisfy this requirement with an electronic
document, in lieu of a paper document, provided the following conditions are
met :
1)
The person satisfies the requirements of 40 CFR 3
.10, incorporated by
reference in Section 611 .102(c) ; and
2)
USEPA has first published a notice in the Federal Register as described in
subsection (a) (2) of this Section .
BOARD NOTE
: Subsection (c) of this Section is derived from 40 CFR 3 .2(a) and
subpart B of 40 CFR 3, as added at 70 Fed
. Reg . 59848 (Oct . 13, 2005) .
d)
Procedures for submission of electronic documents to the Board or the
Agency .
1)
The Board or the Agency may, but is not required to, establish procedures
for the electronic submission of documents that meet the requirements of 40 CFR
3 .2 and 3
.2000, incorporated by reference in Section 611 .102(c) . The Board or
the Agency must establish any such procedures under the Administrative Procedure
Act (5 ILCS 100/Art" 5) .
2)
The Board or the Agency may not accept electronic documents under this
Section until after USEPA has approved the procedures in writing, and the Board
or the Agency has published a notice of eue*tha.t
approval in the Illinois
Register
. Nothing in this subsection (d) limits the authority of the Board or
the Agency under the Illinois Environmental Protection Act (415 ILCS 5] to
accept documents filed electronically .
BOARD NOTE
: Subsection (d) of this Section is derived from 40 CFR 3 .2(b) and
subpart D of 40
CFR 3, as added at 70 Fed . Reg . 59848 (Oct
. 13, 2005) .
e)
Effects of submission of an electronic document .
1)
If
a person who submits a document as an electronic document fails to
comply with the requirements pf,_this Section, that person is subject to the
penalties prescribed for failure to comply with the requirement that the
electronic document was intended to satisfy .
2)
Where a document submitted as an electronic document to satisfy a
reporting requirement bears an electronic signature, the electronic signature
legally binds, obligates, and makes the signer responsible to the same extent as
the signer's handwritten signature would on a paper document submitted to
satisfy the same reporting requirement .
3)
Proof that a particular signature device was used to create an electronic
signature will suffice to establish that the individual uniquely entitled to use
the device did so with the intent to sign the electronic document and give it
effect .
4)
Nothing in this Section limits the use of electronic documents or
information derived from electronic documents as evidence in enforcement or
other proceedings
.
BOARD NOTE : Subsection (e) of this Section is derived from 40 CPR 3
.4 and
3 .2000(c), as added at 70 Fed . Reg . 59848 (Oct . 13, 2005) .
f)
Public document subject to State laws
. Any electronic document filed with
the Board is a public document
. The document, its filing, its retention by the
Board, and its availability for public inspection and copying are subject to
various State laws, including, but not limited to, the following :
6)
Regulations relating to public access to Board records (2 111 . Adm . Code
2175) ; and
7)
Board procedural rules relating to protection of trade secrets and
confidential information (35 111
. Adm . Code 130),
g)
Nothing in this Section or in any provisions adopted pursuant to
subsection (c) (1) of this Section will create any right or privilege to submit
any document as an electronic document .
BOARD NOTE
: Subsection (g) of this Section is derived from 40 CFR 3
.2(c), as
added at 70 Fed . Reg
. 59848 (Oct . 13, 2005) .
BOARD NOTE
: Derived from 40 CFR 3, as added, and 40 CFR 142
.10(g) (2005), as
amended at 70 Fed . Reg . 59848 (Oct . 13, 2005) .
(Source : Added at 30 111
. Reg . -, effective )
1) The Administrative Procedure Act [5 ILCS 1003 ;
2)
The Freedom of Information Act [5 ILCS 140] ;
3) The State Records Act (5 ILLS 160] ;
4) The Electronic Commerce Security Act (5 ILCS 175] ;
5)
The Environmental Protection Act [415 ILCS 5] ;
Section 611 .111
Relief Equivalent to SDWA Section 1415(a) Variances
This Section is intended to describe how the Board grants State relief
equivalent to that available from USEPA under section 1415(a)(1)(A) and
(a) (1) (B) of the SDWA (42 USC 300g-4(a)(1)(A) and (a)
(1)(B)) . SDWA section
1415 variances do not require ultimate compliance within five years in every
situation . Variances under Sections 35-37 of the Act (415 ILCS 5/35-37] do
require compliance within five years in every case . Consequently, a PWS may
have the option of seeking State regulatory relief equivalent to a SDWA section
1415 variance through one of three procedural mechanisms : a variance under
Sections 35-37 of the Act [415 ILCS 5/35-37] and subpart B of 35 Ill
. Adm . Code
1D4 ; a site-specific rule under Sections 27-28 of the Act (415 ILCS 5/27-28] and
35 Ill . Adm . Code 102 ; or an adjusted standard under Section 28
.1 of the Act
[415 ILCS 5/28 .1] and Subpart D of 35 Ill . Adm . Code 104 .
a)
The Board will grant a PWS a variance, a site-specific rule, or an
adjusted standard from an MCL or a treatment technique pursuant to this Section .
1)
The PWS must file a petition pursuant to 35 Ill
. Adm . Code 102 or 104, as
applicable .
2)
If a State requirement does not have a federal counterpart, the Board may
grant relief from the State requirements without following this Section .
b)
Relief from an MCL .
1)
As part of the justification for relief from an MCL under this Section,
the PWS must demonstrate the following :
A)
Because of characteristics of the raw water sources and alternative
sources that are reasonably available to the system, the PWS cannot meet the
MCL ; and
B)
The PWS will install or has installed the best available technology (BAT)
(as identified in Subpart F of this Part), treatment technique, or other means
that the Agency finds available . BAT may vary depending on the following :
i)
The number of persons served by the system ;
ii)
Physical conditions related to engineering feasibility
; and
iii) Costs of compliance
; and
C)
The variance will not result in an unreasonable risk to health
.
2)
in any order granting relief under this subsection, the Board will
prescribe a schedule for the following :
A)
Compliance, including increments of progress, by the PWS, with each MCL
with respect to which the relief was granted
; and
B)
Implementation by the PWS of each additional control measure for each MCL
with respect to which the relief is granted, during the period ending on the
date compliance with such requirement is required .
3)
Schedule of compliance for relief from an MCL
.
A)
A schedule of compliance will require compliance with each MCL with
respect to which the relief was granted as expeditiously as practicable .
B)
If the Board prescribes a schedule requiring compliance with an MCL for
which the relief is granted later than five years from the date of issuance of
the relief, the Board will do the following :
i)
Document its rationale for the extended compliance schedule ;
ii) Discuss the rationale for the extended compliance schedule in the required
public notice and opportunity for public hearing ; and
iii) Provide the shortest practicable time schedule feasible under the
circumstances .
c)
Relief from a treatment technique requirement .
1)
As part of the justification for relief from a treatment technique
requirement under this Section, the PWS must demonstrate that the treatment
technique is not necessary to protect the health of persons served because of
the nature of the raw water source .
2)
The Board may prescribe monitoring and other requirements as a condition
for relief from a treatment technique requirement
.
d)
The Board will hold at least one public hearing . In addition the Board
will accept comments as appropriate pursuant to 35 111
. Adm
. Code 102 or 104 .
e)
The Board will not grant relief from any of the following :
1)
From the MCL for total coliforms . However, the Board may grant a variance
from the total coliform MCL of Section 611 .325 for PWSs that prove that the
violation of the total coliform MCL is due to persistent growth of total
coliform in the distribution system, rather than from fecal or pathogenic
contamination, from a treatment lapse or deficiency, or from a problem in the
operation or maintenance of the distribution system .
2)
From any of the treatment technique requirements of subpart B of this
Part .
3)
From the residual disinfectant concentration (RDC) requirements of
Sections 611 .241(c) and 611 .242(b) .
f)
The Agency must promptly send USEPA the opinion and order of the Board
granting
relief pursuant to this Section . The Board may reconsider and modify a
grant of relief, or relief conditions, if USEPA notifies the Board of a finding
pursuant to section 1415 of the SDWA (42 USC 300g-4) .
g)
in addition to the requirements of this Section, the provisions of Section
611 .130 or 611
.131 may apply to relief granted pursuant to this Section .
BOARD NOTE : Derived from 40 CFR 141 .4 (2002) (2005), from section
1415 (a) (1) (A) and (a) (1) (B) of the SDWA and from the "Guidance Manual for
Compliance with the Filtration and Disinfection Requirements for Public Water
Systems using Surface Water Sources,", incorporated by reference in section
611 .102 . USEPA has reserved the discretion to review and modify or nullify
Board determinations
made pursuant to this Section at 40 CFR 142 .23 (2002)
42005) .
(Source : Amended at 30 Ill . Reg . -, effective )
SUBPART B : FILTRATION AND DISINFECTION
Section 611 .212
Groundwater under Direct Influence of Surface Water
The Agency shall, pursuant to Section 611 .201, require all CWSs to demonstrate
whether they are using "groundwater under the direct influence of surface
water
."- The Agency must determine with information provided by the supplier
whether a PWS uses "groundwater under the direct influence of surface water" on
an individual basis . The Agency must determine that a groundwater source is
under the direct influence of surface water based upon the following :
a)
Physical characteristics of the source : whether the source is obviously a
surface water source, such as a lake or stream . Other sources that may be
subject to influence from surface waters include : springs, infiltration
galleries, wells, or other collectors in subsurface aquifers .
b)
Well construction characteristics and geology with field evaluation .
1)
The Agency may use the wellhead protection program's requirements, which
include delineation of wellhead protection areas, assessment of sources of
contamination and implementation of management control systems, to determine if
the wellhead is under the influence of surface water .
2)
Wells less than or equal to 50 feet in depth are likely to be under the
influence of surface water .
3)
Wells greater than 5o feet in depth are likely to be under the influence
of surface water, unless they include the following :
A)
A surface sanitary seal using bentonite clay, concrete, or similar
material;;_
B)
A well casing that penetrates consolidated (slowly permeable) material ;
and
C)
A well casing that is only perforated or screened below consolidated
(slowly permeable) material .
4)
A source that is less than 200 feet from any surface water is likely to be
under the influence of surface water .
c)
Any structural modifications to prevent the direct influence of surface
water and eliminate the potential for Giardia lamblia cyst contamination
.
d)
Source water quality records . The following are indicative that a source
is under the influence of surface water :
1)
A record of total coliform or fecal coliform contamination in untreated
samples collected over the past three years ;
I
I
2) A history of turbidity problems associated with the source
; or
3)
A history of known or suspected outbreaks of Giardia lamblia,
Cryptosporidium or other pathogenic organisms associated with surface water that
has been attributed to that source .
e)
Significant and relatively rapid shifts in water characteristics such as
turbidity, temperature, conductivity, or pH .
1)
A variation in turbidity of 0 .5 NTU or more over one year is indicative of
surface influence .
2)
A variation in temperature of 9-nine Fahrenheit degrees or more over one
year is indicative of surface influence .
f)
Significant and relatively rapid shifts in water characteristics such as
turbidity, temperature, conductivity, or pH that closely correlate to
climatological or surface water conditions are indicative of surface water
influence .
1)
Evidence of particulate matter associated with the surface water ; or.
2)
Turbidity or temperature data that correlates to that of a nearby surface
water source .
g)
Particulate analysis : Significant occurrence of insects or other
macroorganisms, algae, or large diameter pathogens such as Giardia lamblia is
indicative of surface influence .
1)
"Large diameter" particulates are those over 4--seven micrometers .
2)
Particulates must be measured as specified in the "Guidance Manual for
Compliance with the Filtration and Disinfection Requirements for Public Water
Systems using Surface Water Sources," ; incorporated by reference in Section
611 .102 .
h)
The potential for contamination by small-diameter pathogens, such as
bacteria or viruses, does not alone render the source "under the direct
influence of surface water ."-
BOARD NOTE : Derived from the definition of "groundwater under the - direct
influence of surface water" in 40 CFR 141 .2--(2002) (2005) ; from the Preamble at
54 Fed . Reg . 27489 (June 29, 1989) ; and from the USEPA "Guidance Manual for
Compliance with the Filtration and Disinfection Requirements for Public Water
Systems using Surface Water Sources,"
; incorporated by reference in Section
611 .102 .
(Source : Amended at 30 Ill . Reg . -, effective )
SUBPART G : LEAD AND COPPER
Section 611 .359
Analytical Methods
Analyses for lead, copper, pH, conductivity, calcium, alkalinity,
orthophosphate, silica, and temperature must be conducted using the methods set
forth in Section 611 .611(a) .
i
I
I
a)
Analyses for lead and copper performed for the purposes of compliance with
this Subpart G must only be conducted by laboratories that have been certified
by USEPA or the Agency . To obtain certification to conduct analyses for lead
and copper, laboratories must do the following :
1)
Analyze performance evaluation samples that include lead and copper
provided by USEPA Environmental Monitoring and Support Laboratory or equivalent
samples provided by the Agency ; and
2)
Achieve quantitative acceptance limits as follows :
A)
For lead
: ±30 percent of the actual amount in the performance evaluation
sample when the actual amount is greater than or equal to 0
.005 mg/l (the PQL
for lead is 0 .005 mg/1) ;
B)
For copper : ±10 percent of the actual amount in the performance
evaluation sample when the actual amount is greater than or equal to 0 .050 mg/l
(the PQL for copper is 0 .050
mg/1) ;
C)
Achieve the method detection limit (MDL) for lead (0
.001 mg/1, as defined
in Section 611 .350(a)) according to the procedures in 35 Ill . Adm
. Code 186 and
appendix B to 40 CFR
136,Appendix Dll : "Definition and Procedure for the
Determination of the Method Detection Limit -- Revision 1
.11" (2002) (2005),
incorporated by reference in Section 611 .102(c)
. This need only be accomplished
if the laboratory will be processing source water composite samples under
Section 611 .358(a)(1)(C) ; and
D)
Be currently certified by USEPA or the Agency to perform analyses to the
specifications described in subsection (a) (2) of this section .
BOARD NOTE : Subsection (a) is derived from 40 CFR 141
.89(a) and (a) (1) (2002)
(2005) .
b)
The Agency must, by a SEP issued pursuant to Section 611
.110, allow a
supplier to use previously collected monitoring data for the purposes of
monitoring under this Subpart G if the data were collected and analyzed in
accordance with the requirements of this Subpart G .
BOARD NOTE : Subsection (b) is derived from 40 CFR 141
.89(a)(2 ) (2002)
(2005) .
c)
Reporting
lead and copper levels .
1)
All lead and copper levels greater than or equal to the lead and copper
PQL (Pb ?= 0 .005 mg/l and Cu *_ 0 .050 mg/1) must be reported as measured
.
2)
All lead and copper levels measured less than the PQL and greater than
the
MDL (0 .005 mg/l > Pb > MDL and 0 .050 mg/1 > Cu > MDL) must be either reported
as measured or as one-half the PQL set forth in subsection (a) of this Section
(i .e., reported as 0
.0025 mg/1 for lead or 0 .025 mg/l for copper) .
3)
All lead and copper levels below the lead and copper MDL (MDL > Pb) must
be reported as zero .
BOARD NOTE : Subsection (c) is derived from 40
CFR
141
.89(a)(3) and (a) (4)
(2002)
( 2005) .
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(Source : Amended at 30 111 . Reg . -,
effective
}
SUBPART I : DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS,
AND DISINFECTION BYPRODUCT PRECURSORS
Section 611 .380
General Requirements
a)
The requirements of this Subpart I constitute NPDWRs .
1)
The regulations in this Subpart I establish standards under which a CWS
supplier or an NTNCWS supplier that adds a chemical disinfectant to the water in
any part of the drinking water treatment process or
which providca watcr that
containo a chcmi al disinfectant must modify its practices to meet MCLs and
MRDLs in Sections 611 .312 and 611 .313, respectively, and must meet the treatment
technique requirements for DBP precursors in Section 611
.385 .
2)
The regulations in this Subpart I establish standards under which a
transient non-CWS supplier that uses chlorine dioxide as a disinfectant or
oxidant must modify its practices to meet the MRDL for chlorine dioxide in
Section 611 .313 .
3)
The Board has established MCLS for TTHM and HAA5 and treatment technique
requirements for DBP precursors to limit the levels of known and unknown DBPs
that may have adverse health effects . These DBPs may include chloroform,
bromodichloromethane, dibromochloromethane, bromoform, dichloroacetic acid, and
trichloroacetic acid .
b)
compliance dates .
1)
CWSs and NTNCWSs
. Unless otherwise noted, a supplier must comply with the
requirements of this Subpart I as follows
: A Subpart B system supplier serving
10,000 or more persons must comply with this Subpart I beginning January 1,
2002 . A Subpart B system supplier serving fewer than 10,000 persons or a
supplier using only groundwater not under the direct influence of surface water
must comply with this Subpart I beginning January 1, 2004 .
2)
Transient non-CWSs
. A Subpart B system supplier serving 10,000 or more
persons and using chlorine dioxide as a disinfectant or oxidant must comply with
any requirements for chlorine dioxide in this Subpart I beginning January 1,
2002 . A Subpart B system supplier serving fewer than 10,000 persons and using
chlorine dioxide as a disinfectant or oxidant or a supplier using only
groundwater not under the direct influence of surface water and using
that uoco
chlorine dioxide as a disinfectant or oxidant must comply with any requirements
for chlorine dioxide in this Subpart I beginning January 1, 2004
.
c)
Each CWS or NTNCWS supplier regulated under subsection (a) of this Section
must be operated by qualified personnel who meet the requirements specified in
35 Ill . Adm . Code 680 .
d)
Control of disinfectant residuals
. Notwithstanding the MRDLs in Section
611 .313, a supplier may increase residual disinfectant levels in the
distribution system of chlorine or chloramines (but not chlorine dioxide) to a
level and for a time necessary to protect public health, to address specific
microbiological contamination problems caused by circumstances such as, but not
limited to, distribution line breaks, storm run-off events, source water
contamination events, or cross-connection events
.
BOARD NOTE
: Derived from 40 CFR 141 .130 (2002 ) (2005) .
(Source : Amended at 30 111 . Reg . -, effective )
SUBPART N : INORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
Section 611 .609
Determining Compliance
Compliance with the MCLs of Section 611 .300 or 611 .301 (as appropriate) must be
determined based on the analytical results obtained at each sampling point .
a)
For suppliers that monitor at a frequency greater than annual, compliance
with the MCLs for antimony, arsenic (effective January 22, 2004), asbestos,
barium, beryllium, cadmium, chromium, cyanide, fluoride, mercury, nickel,
selenium, or thallium is determined by a running annual average at each sampling
point
. Effective January 22, 2004, if a system fails to collect the required
number of samples, compliance (average concentration) will be based on the total
number of samples collected .
1)
If the average at any sampling point is greater than the MCL, then the
supplier is out of compliance
.
2)
if any one sample would cause the annual average to be exceeded, then the
supplier is out of compliance immediately
.
3)
Any sample below the method detection limit must be calculated at zero for
the purpose of determining the annual average .
BOARD NOTE : The "method detection limit" is different from the "detection
limit, " as set forth in Section 611 .600
. The "method detection limit" is the
level of contaminant that can be determined by a particular method with a 95
percent degree of confidence, as determined by the method outlined in appendix B
to 40 CFR 136, Appendix D, incorporated by reference at Section 611 .102 .
b)
For suppliers that monitor annually or less frequently, compliance with
the MCLs
for antimony, arsenic (effective January 22, 2004), asbestos, barium,
beryllium, cadmium, chromium, cyanide, fluoride, mercury, nickel, selenium, or
thallium is determined by the level of the contaminant at any sampling point
.
If confirmation samples are required by the Agency, the determination of
compliance will be based on the average of the annual average of the initial MCL
exceedence and any Agency-required confirmation samples . Effective January 22,
2004, if a supplier fails to collect the required number of samples, compliance
(average concentration) will be based on the total number of samples collected .
c)
Compliance with the MCLs for nitrate and nitrite is determined based on
one sample if the levels of these contaminants are below the MCLs
. If the
levels of nitrate or nitrite in the initial sample exceed the MCLs, Section
611
.606 requires confirmation sampling, and compliance is determined based on
the average of the initial and confirmation samples
.
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d)
Arsenic sampling results must be reported to the nearest 0
.001 mg/l .
BOARD NOTE
: Derived from 40 CFR 141 .23(i) (2002) (2005) .
(Source : Amended at 30 111 . Reg . -,
effective )
SUBPART 0 : ORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
Section 611
.646
Phase I, Phase II, and Phase V Volatile Organic Contaminants
Monitoring of the Phase I, Phase II, and Phase V VOCs for the purpose of
determining compliance with the MCL must be conducted as follows :
a)
Definitions . As used in this Section the following have the given
meanings :
"Detect" and "detection" mean that the contaminant of interest is present
at a level greater than or equal to the "detection limit ."
"Detection limit" means 0 .0005 mg/1 .
BOARD NOTE : Derived from 40 CPR 141,24(t)(?), (f)(11), (f)(14)(i), and
(f)(20
) (2003)
(2005) . This is a "trigger level" for Phase I, Phase II, and
Phase V VOCs inasmuch as it prompts further action . The use of the term
"detect" in this Section is not intended to include any analytical capability of
quantifying lower levels of any contaminant, or the "method detection limit ."
Note, however, that certain language at the end of federal paragraph (f)(20) is
capable of meaning that the "method detection limit" is used to derive the
"detection limit ." The Board has chosen to disregard that language at the end
of paragraph (f)(20) in favor of the more direct language of paragraphs (f) (7)
and (f)(11) .
"Method detection limit," as used in subsections (q) and (t) of this
Section means the minimum concentration of a substance that can be measured and
reported with 99 percent confidence that the analyte concentration is greater
than zero and is determined from analysis of a sample in a given matrix
containing the analyte .
BOARD NOTE : Derived from appendix B to 40 CFR 136, Appcndix D(2003) 136
(2005) . The method detection limit is determined by the procedure set forth in
appendix B to
40 CFR
136, Appcndix n
incorporated by reference in Section
611 .102(c) . See subsection (t) of this Section .
b)
Required sampling
. Each supplier must take a minimum of one sample at
each sampling point at the times required in subsection (u) of this Section .
c) Sampling points .
1)
Sampling points for a GWS
. Unless otherwise provided by a SEP granted by
the Agency pursuant to Section 611 .110, a GWS supplier must take at least one
sample from each of the following points : each entry point that is
representative of each well after treatment .
2)
Sampling points for an SWS or mixed system supplier . Unless otherwise
provided by a SEP granted by the Agency pursuant to Section 611
.110, an SWS or
mixed system supplier must sample from each of the following points
:
A)
Each entry point after treatment ; or
B)
Points in the distribution system that are representative of each source .
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3)
The supplier must take each sample at the same sampling point unless the
Agency has granted a SEP pursuant to Section 611
.110 that designates another
location as more representative of each source, treatment plant, or within the
distribution system .
4)
If
a
system draws water from more than one source, and the sources are
combined before
distribution, the supplier must sample at an entry point during
periods of normal operating conditions when water is
representative of all
sources being used .
BOARD NOTE : Subsections (b) and (c) of this Section derived from 40 CFR
141 .24(f)(1) through (f) (3) (2003)
{ 2005) .
d)
Each CWS and NTNCWS supplier must take four consecutive quarterly samples
for each of the Phase I VOCs, excluding vinyl chloride, and Phase II VOCs during
each compliance period, beginning in the compliance period starting in the
initial compliance period .
e)
Reduction to annual monitoring frequency
. If the initial monitoring for
the Phase I, Phase II, and Phase V VOCs, as allowed in subsection (r)(1) of this
Section, was completed by December 31, 1992, and the supplier did not detect any
of the Phase I VOCs, including vinyl chloride ; Phase II VOCs ; or Phase V VOCs,
then the supplier must take one sample annually beginning in the initial
compliance period
.
f) GWS reduction to triennial monitoring frequency . After a minimum of three
years of annual sampling, GWS suppliers that have not previously detected any of
the Phase I VOCs, including vinyl chloride ; Phase II VOCs ; or Phase V VOCs must
take one sample during each three-year compliance period .
g)
A CWS or NTNCWS supplier that has completed the initial round of
monitoring required by subsection (d) of this Section and which did not detect
any of the Phase I VOCs, including vinyl chloride ; Phase II VOCs ; and Phase V
VOCs may apply to the Agency for a SEP pursuant to Section 611 .110 that
releases it from the requirements of subsection (e) or (f) of this Section . A
supplier that serves fewer than 3300 service connections may apply to the Agency
for a SEP that releases it from the requirements of subsection (d) of this
Section as to 1,2,4-trichlorobenzene .
BOARD NOTE : Derived from 40 CFR 141 .24(f)(7) and (f)(10 ) (2003) (2005),
and the discussion at 57 Fed . Reg . 31825 (July 17, 1992) . Provisions concerning
the term of the waiver appear in subsections (i) and (j) of this Section . The
definition of "detect," parenthetically added to the federal counterpart
paragraph, is in subsection (a) of this section .
h)
Vulnerability assessment .
The Agency must consider the factors of Section
611 .110(e) in granting a SEP from the
requirements of subsection
(d), (e),
or
(f) of this Section sought pursuant to subsection (g) of this Section .
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i)
A SEP issued to a GWS pursuant to subsection (g) of this Section is for a
maximum of six years,
except
that a SEP as to the subsection (d) of this
Section monitoring for 1,2,4-trichlorobenzene must apply only to the initial
round of monitoring . As a condition of a SEP, except as to a SEP from the
initial round of subsection (d) of this Section monitoring for 1,2,4-
trichlorobenzene, the supplier shall, within 30 months after the beginning of
the period for which the waiver was issued, reconfirm its vulnerability
assessment required by subsection (h) of this Section and submitted pursuant to
subsection (g) of this section, by taking one sample at each sampling point and
reapplying for a SEP pursuant to subsection (g) of this Section
. Based on this
application, the Agency must do either of the following :
1)
If it determines that the PWS meets the standard of Section 611 .610(e),
issue a SEP that reconfirms the prior SEP for the remaining three-year
compliance period of the six-year maximum term
; or
2)
Issue a new SEP
requiring the supplier to sample annually .
BOARD NOTE
: Subsection (i) of this Section does not apply to an SWS or
mixed system supplier .
j)
Special considerations for a SEP for an SWS or mixed-system supplier .
1)
The Agency must determine that an SWS is not vulnerable before issuing a
SEP pursuant to Section 611 .110 to an SWS supplier
. A SEP issued to an SWS or
mixed system supplier pursuant to subsection (g) of this Section is for a
maximum of one compliance period ; and
2)
The Agency may require, as a condition to a SEP issued to an SWS or mixed
supplier, that the supplier take such samples for Phase I, Phase II, and Phase V
VOCs at such a frequency as the Agency determines are necessary, based on the
vulnerability assessment .
BOARD NOTE
: There is a great degree of similarity between 40 CFR
141 .24(f)(7) (2003 ) (2005),
the provision applicable to GWSs, and 40 CFR
141 .24(f)(10 ) (2003) (2005), the provision for SWSs
. The Board has consolidated
the common requirements of both paragraphs into
subsection (g) of this Section .
Subsection (j) of this Section represents the elements unique to an SWSs or
mixed system, and subsection (i) of this Section relates to a GWS supplier
.
Although 40 CFR 141
.24(f)(7) and (f)(10) are silent as to a mixed system
supplier, the Board has included a mixed system supplier with an SWS supplier
because this best follows the federal scheme for all other
contaminants .
k)
If one of the Phase I VOCs, excluding vinyl chloride
; a Phase II VOC ; or a
Phase V VOC is detected in any sample, then the following must occur
:
1)
The supplier must monitor quarterly for that contaminant at each sampling
point that resulted in a detection .
2)
Annual monitoring .
A)
The Agency must grant a SEP pursuant to Section 611
.110 that allows a
supplier to reduce the monitoring frequency to annual at a sampling point if it
determines that the sampling point is reliably and consistently below the
MCL .
B)
A request for a SEP must include the following minimal information :
i)
For a GWS, two quarterly samples .
ii) For an SWS or mixed system supplier, four quarterly samples .
C)
In issuing a SEP, the Agency must specify the level of the contaminant
upon which the "reliably and consistently" determination was based
. Any SEP
that allows less frequent monitoring based on an Agency "reliably and
consistently" determination must include a condition requiring the supplier to
resume quarterly monitoring pursuant to subsection (k) (1) of this Section if it
violates the MCL specified by Section 611
.311 .
3)
Suppliers
that monitor annually must monitor during the quarters that
previously yielded the highest analytical result .
4)
Suppliers that do not detect a contaminant at a sampling point in three
consecutive annual samples may apply to the Agency for a SEP pursuant to Section
611
.110 that allows it to discontinue monitoring for that contaminant at that
point, as specified in subsection (g) of this Section .
5)
A GWS supplier that has detected one or more of the two-carbon
contaminants listed in subsection (k) (5) (A) of this Section must monitor
quarterly for vinyl chloride as described in subsection (k) (5) (B) of this
Section, subject to the limitation of subsection (k) (5) (C) of this section
.
A)
"Two-carbon contaminants" (Phase I or II VOC) are the following :
1,2-Dichloroethane (Phase I)
1,1-Dichloroethylene (Phase I)
cis-1,2-Dichloroethylene (Phase II)
trans-l,2-Dichloroethylene (Phase II)
Tetrachloroethylene (Phase II)
1,1,1-Trichloroethylene (Phase I)
Trichloroethylene (Phase I)
B)
The supplier must sample quarterly for vinyl chloride at each sampling
point at which it detected one or more of the two-carbon contaminants listed in
subsection (k) (5) (A) of this Section .
C)
The Agency must grant a SEP pursuant to Section 611
.110 that allows the
supplier to reduce the monitoring frequency for vinyl chloride at any sampling
point to once in each three-year compliance period if it determines that the
supplier has not detected vinyl chloride in the first sample required by
subsection (k) (5) (B) of this Section
.
1)
Quarterly monitoring following MCL violations .
1)
Suppliers that violate an MCL for one of the Phase I VOCs, including vinyl
chloride ; Phase II VOCs
; or Phase V VOCs, as determined by subsection (o) of
this Section, must monitor quarterly for that contaminant, at the sampling point
where the violation occurred, beginning the next quarter after the violation .
2)
Annual monitoring .
A)
The Agency must grant a SEP pursuant to Section 611 .110 that allows a
supplier to reduce the monitoring frequency to annually if it determines that
the sampling point is reliably and consistently below the MCL .
B)
A request for a SEP must include the following minimal information
: four
quarterly samples .
C)
In issuing a SEP, the Agency must specify the level of the contaminant
upon which the "reliably and consistently" determination was based . Any SEP
that allows less frequent monitoring based on an Agency "reliably and
consistently" determination must include a condition requiring the supplier to
resume quarterly monitoring pursuant to subsection (1)(1) of this Section if it
violates the
MCL specified by Section 611 .311 .
D)
The supplier must monitor during the quarters that previously yielded the
highest analytical result .
m)
Confirmation samples . The Agency may issue a SEP pursuant to Section
610 .110 to require a supplier to use a confirmation sample for results that it
finds dubious for whatever reason . The Agency must state its reasons for
issuing the SEP if the SEP is Agency-initiated .
1)
If a supplier detects
any of the Phase I, Phase II, or Phase V VOCs in a
sample, the supplier must take a confirmation sample as soon as possible, but no
later than 14 days after the supplier receives notice of the detection .
2)
Averaging is as specified in subsection (o) of this Section .
3)
The Agency must delete the original or confirmation sample if it
determines that a sampling error occurred, in which case the confirmation sample
will replace the original or confirmation sample .
n)
This subsection (n) corresponds with 40 CFR 141 .24(f)(14), an optional
USEPA provision relating to compositing of samples that USEPA does not require
for state programs
. This statement maintains structural consistency with USEPA
rules .
o)
Compliance with the
MCLs for the Phase I, Phase II, and Phase V VOCs must
be determined based on the analytical results obtained at each sampling point .
Effective January 22, 2004, if one sampling point is in violation of an MCL, the
system is in violation of the
MCL .
1)
Effective January 22, 2004, for a supplier that monitors more than once
per year, compliance with the MCL is determined by a running annual average at
each sampling point .
2)
Effective January 22, 2004, a supplier that monitors annually or less
frequently whose sample result exceeds the MCL must begin quarterly sampling .
The system will not be considered in violation of the MCL until it has completed
one year of quarterly sampling .
3)
Effective January 22, 20
if any sample result will cause the running
annual average to exceed the MCL at any sampling point, the supplier is out of
compliance with the MCL immediately .
4)
Effective January 22, 2004, if a supplier fails to collect the
required
number of samples, compliance will be based on the total number of samples
collected .
5)
Effective January 22, 2004, if a sample result is less than the detection
limit, zero will be used to calculate the annual average .
6)
Until January 22, 2004, for a supplier that conducts monitoring at a
frequency
greater than annual, compliance is determined by a running annual
average of all samples taken at each sampling point .
A)
If the annual average of any sampling point is greater than the MCL, then
the supplier is out of compliance .
B)
If the initial sample or a subsequent sample would cause the annual
average to exceed the MCL, then the supplier is out of compliance immediately .
C)
Any samples below the detection limit must be deemed as zero for purposes
of determining the annual average .
7)
Until January 22, 2004, if monitoring is conducted annually, or less
frequently, the supplier is out of compliance if the level of a contaminant at
any sampling point is greater than the MCL
. Until January 22, 2004, if a
confirmation sample is taken, the determination of compliance is based on the
average of two samples .
p)
This subsection (p) corresponds with 40 CFR 141 .24(f)(16), which USEPA
removed and reserved . This statement maintains structural consistency with the
federal regulations .
q) Analysis under this Section must only be conducted by laboratories that
have received certification by USEPA or the Agency according to the following
conditions :
1)
To receive certification to conduct analyses for the Phase I VOCs,
excluding vinyl chloride
; Phase II VOCs ; and Phase V VOCs, the laboratory must
do the following :
A)
It must analyze performance evaluation (PE) samples that include these
substances provided by the Agency pursuant to 35 111 . Adm . Code 186 .170 ;
B)
It must achieve the quantitative acceptance limits under subsections
(q) (1) (C) and (q) (1) (D) of this Section for at least 80 percent of the regulated
organic contaminants in the PE sample ;
C)
It must achieve quantitative results on the analyses performed under
subsection (q) (1) (A) of this Section that are within ± 20 percent of the actual
amount of the substances in the PE sample when the actual amount is greater than
or equal to 0.010
mg/1 ;
D)
It must achieve quantitative results on the analyses performed under
subsection (q) (1) (A) of this Section that are within ± 40 percent of the actual
amount of the substances in the PE sample when the actual amount is less than
0 .010 mg/l
; and
E) It must achieve a method detection limit of
0 .0005 mg/l, according to the
procedures in appendix B to 40 CFR
136, Appcndix D, incorporated by reference in
Section 611
.102 .
2)
To receive certification to conduct analyses for vinyl chloride the
laboratory must do the following
:
A)
It must analyze PE samples provided by the Agency pursuant to
35 111 . Adm .
Code
186 .170 ;
I
B)
It must achieve quantitative results on the analyses performed under
subsection (q) (2) (A) of this Section that are within ± 40 percent of the actual
amount of vinyl chloride in the PE sample
;
C)
It must achieve a method detection limit of 0 .0005 mg/1, according to the
procedures in appendix B to 40 CFR 136, Appcndi3c B, incorporated by reference in
Section 611 .102 ; and
D)
It must obtain certification pursuant to subsection (q) (1) of this Section
for Phase I VOCs, excluding vinyl chloride ; Phase II VOCs ; and Phase V VOCs .
r)
This subsection (r) corresponds with 40 CFR 141 .24(f)(18), an obsolete
provision that relates to the initial compliance period from 1993 through 1995 .
This statement maintains consistency with the federal regulations .
s) The Agency shall, by a SEP issued pursuant to Section 611 .110, increase
the number of sampling points or the frequency of monitoring if it determines
that it is necessary to detect variations within the PWS .
t)
Each laboratory certified for the analysis of Phase I, Phase II, or Phase
V VOCs pursuant to subsection (q) (1) or (q) (2) of this Section shall do the
following :
1)
Determine the method detection limit (MDL), as defined in appendix B to 40
CFR 136,
Appendix B,
incorporated by reference in Section 611 .102, at which it
is capable of detecting the Phase I, Phase II, and Phase V VOCs
; and,
2)
Achieve an MDL for each Phase I, Phase II, and Phase V VOC that is less
than or equal to 0 .0005 mg/1 .
u)
Each supplier must monitor, within each compliance period, at the time
designated by the Agency by SEP pursuant to Section 611 .110 .
v)
A new system supplier or a supplier that uses a new source of water that
begins operation after January 22, 2004 must demonstrate compliance with the MCL
within a period of time specified by a permit issued by the Agency . The
supplier must also comply with the initial sampling frequencies specified by the
Agency to ensure the supplier can demonstrate compliance with the MCL . Routine
and increased monitoring frequencies must be conducted in accordance with the
requirements in this Section .
BOARD NOTE : Derived from 40 CFR 141 .24(f)
(2003) (2005) .
(Source : Amended at 30 Ill . Reg . -, effective )
Section 611 .
D
Defined Substrate Method for the
Simultaneous Detection of Total Coliforms and Escherichia Coli from Drinking
Water
Autoanalysis Colilert Presence-Absence (AC P-A) Method .
The AC P-A test format must be either a 100 ml 10-tube most probable number
test (one tube positive denoting the presence of total coliforms in that
sample) or a single vessel containing sufficient reagent to receive 100 ml of
sample
. The reagent is available from Access Medical Systems, Branford
Connecticut .
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The AC P-A method must be performed as follows ;
1 .
For
the
10-tube
method, add 10 ml
of water sample to each test tube . For
the single-vessel
method, add 100 ml of water sample
to the vessel .
2 .
Dissolve the reagent powder by agitation . (This should produce a
colorless solution .)
3 .
Incubate the test tubes or vessel at 35A~*_C for 24 hours .
4 .
Development of yellow during incubation denotes the presence of total
coliforms in either the test tube or the vessel .
5 .
Expose each positive (yellow) test tube or vessel to a fluorescent (366
nm) light source . Fluorescence specifically demonstrates the presence of
Escherichia coli .
BOARD NOTE : Derived from S . Edberg, M . Allen & D . Smith, "National Field
Evaluation of a Defined Substrate Method for the Simultaneous Detection of Total
Coliforms and Escherichia coli from Drinking Water : Comparison with Presence-
Absence Techniques,"- Applied and Environmental Microbiology, vol . 55, pp . 1003-
1008, as incorporated by reference at 40 CFR 141
.21(f)(6)(iii) (2002) (2005) .
This method is for use in conjunction with the requirements of Section 611
.526 .
(Source : Amended at 30 111 . Reg . -, effective )
ILLINOIS RDCICTDR
JCAR150611-0611064r03
POLLUTIONCONTROL BOARD
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JCAR350611-0613054r01
1
TITLE 35
: ENVIRONMENTAL PROTECTION
2
SUBTITLE F
: PUBLIC WATER SUPPLIES
RECEIVED
3
CHAPTER I
: POLLUTION CONTROL BOARD
CLERK'S
OFFICE
4
5
PART 611
AUG 0
1
2006
6
PRIMARY DRINKING WATER STANDARDS
STATE OF
ILLtt,tDns
7
Pollution Corenoy
c
8
SUBPART A
: GENERAL
9
10 Section
11 611 .100
Purpose, Scope, and Applicability
12 611.101
Definitions
13 611 .102
Incorporations by Reference
14 611 .103
Severability
15 611 .105
Electronic Reporting
16
611.107
Agency Inspection of PWS Facilities
17 611 .108
Delegation to Local Government
18 611 .109
Enforcement
19
611
.110
Special Exception Permits
20
611 .111
Relief Equivalent to SDWA Section 1415(a) Variances
21
611 .112
Relief Equivalent to SDWA
Section 1416 Exemptions
22 611 .113
Alternative Treatment Techniques
23 611 .114
Siting Requirements
24 611 .115
Source Water Quantity
25 611 .120
Effective Dates
26 611 .121
Maximum Contaminant Levels
and Finished Water Quality
27 611 .125
Fluoridation Requirement
28 611 .126
Prohibition on Use of Lead
29 611 .130
Special Requirements for Certain
Variances and Adjusted Standards
30 611 .131
Relief Equivalent to SDWA Section 1415(e) Small System Variance
31 611 .160
Composite Correction Program
32
33
SUBPART B
: FILTRATION
AND DISINFECTION
34
35 Section
36 611 .201
Requiring a Demonstration
37 611 .202
Procedures for Agency Determinations
38 611 .211
FiltrationPApired
39 611 .212
Groundwater wider
Direct Influence of Surface Water
40
611 .213
No Meted c>fFIPC Analysis
41 611 .220
Genearal Requiiei tl
42 611 .230
Fiat on Ewective Dates
43 611 .231
Source Water Quality Conditions
JCAR350611-0613054r01
44
611
.232
Site-Specific Conditions
45
611 .233
Treatment Technique Violations
46 611 .240
Disinfection
47 611 .241
Unfiltered PWSs
48
611 .242
Filtered PWSs
49 611 .250
Filtration
50 611 .261
Unfiltered PWSs : Reporting and Recordkeeping
51 611 .262
Filtered PWSs
: Reporting and Recordkeeping
52 611 .271
Protection during Repair Work
53 611 .272
Disinfection Following Repair
54 611 .276
Recycle Provisions
55
56
SUBPART C
: USE OF NON-CENTRALIZED TREATMENT DEVICES
57
58 Section
59 611 .280
Point-of-Entry Devices
60
611 .290
Use of Point-of-Use Devices or Bottled Water
61
62
SUBPART D : TREATMENT TECHNIQUES
63
64 Section
65 611 .295
General Requirements
66 611 .296
Acrylamide and Epichlorohydrin
67 611 .297
Corrosion Control
68
69
SUBPART F
: MAXIMUM CONTAMINANT LEVELS (MCLs) AND
70
MAXIMUM RESIDUAL DISINFECTANT LEVELS (MRDLs)
71
72 Section
73 611 .300
Old MCLs for Inorganic Chemical Contaminants
74 611 .301
Revised MCLs for Inorganic Chemical Contaminants
75 611 .310
Old Maximum Contaminant Levels (MCLs) for Organic Chemical Contaminants
76
611 .311
Revised MCLs for Organic Chemical Contaminants
77 611 .312
Maximum Contaminant Levels (MCLs) for Disinfection Byproducts (DBPs)
78 611
.313
Maximum Residual Disinfectant Levels (MRDLs)
79 611 .320
Turbidity (Repealed)
80 611 .325
Microbiological Contaminants
81 611 .330
Maximum Contaminant Levels for Radionuclides
82 611 .331
Beta Particle and Photon Radioactivity (Repealed)
83
84
SUBPART G: LEAD AND COPPER
85
86 Section
JCAR350611-0613054r01
87 611 .350
General Requirements
88
611
.351
Applicability of Corrosion Control
89 611 .352
Corrosion Control Treatment
90 611 .353
Source Water Treatment
91 611 .354
Lead Service Line Replacement
92
611
.355
Public Education and Supplemental Monitoring
93 611 .356
Tap Water Monitoring for Lead and Copper
94 611 .357
Monitoring for Water Quality Parameters
95
611 .358
Monitoring for Lead and Copper in Source Water
96 611 .359
Analytical Methods
97 611
.360
Reporting
98 611 .361
Recordkeeping
99
100
SUBPART I
: DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS,
101
AND DISINFECTION BYPRODUCT PRECURSORS
102
103 Section
104 611 .380
General Requirements
105 611 .381
Analytical Requirements
106 611 .382
Monitoring Requirements
107 611 .383
Compliance Requirements
108 611 .384
Reporting and Recordkeeping Requirements
109 611 .385
Treatment Technique for Control of Disinfection Byproduct (DBP) Precursors
110
111
SUBPART K : GENERAL MONITORING AND ANALYTICAL REQUIREMENTS
112
113 Section
114 611 .480
Alternative Analytical Techniques
115 611 .490
Certified Laboratories
116 611 .491
Laboratory Testing Equipment
117 611 .500
Consecutive PWSs
118 611 .510
Special Monitoring for Unregulated Contaminants (Repealed)
119
120
SUBPART L : MICROBIOLOGICAL MONITORING
121
AND ANALYTICAL REQUIREMENTS
122
123 Section
124 611 .521
Routine Coliform Monitoring
125 611 .522
Repeat Coliform Monitoring
126
611.523
Invalidation of Total Coliform Samples
127 611 .524
Sanitary Surveys
128 611 .525
Fecal Coliform and E . Coli Testing
129 611.526
Analytical Methodology
JCAR350611-0613054r01
130 611 .527
Response to Violation
131
611 .531
Analytical Requirements
132 611 .532
Unfiltered PWSs
133 611 .533
Filtered PWSs
134
135
SUBPART M
: TURBIDITY MONITORING AND ANALYTICAL REQUIREMENTS
136
137 Section
138
611 .560
Turbidity
139
140
SUBPART N
: INORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
141
142 Section
143 611 .591
Violation of a State MCL
144 611 .592
Frequency of State Monitoring
145 611 .600
Applicability
146
611 .601
Monitoring Frequency
147 611 .602
Asbestos Monitoring Frequency
148 611 .603
Inorganic Monitoring Frequency
149
611 .604
Nitrate Monitoring
150
611 .605
Nitrite Monitoring
151 611 .606
Confirmation Samples
152 611 .607
More Frequent Monitoring and Confirmation Sampling
153 611 .608
Additional Optional Monitoring
154
611 .609
Determining Compliance
155 611 .610
Inorganic Monitoring Times
156 611 .611
Inorganic Analysis
157
611 .612
Monitoring Requirements for Old Inorganic MCLs
158 611 .630
Special Monitoring for Sodium
159 611 .631
Special Monitoring for Inorganic Chemicals (Repealed)
160
161
SUBPART 0
: ORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
162
163 Section
164 611 .640
Definitions
165
611 .641
Old MCLs
166
611 .645
Analytical Methods for Organic Chemical Contaminants
167 611 .646
Phase I, Phase II, and Phase V Volatile Organic Contaminants
168 611 .647
Sampling for Phase I Volatile Organic Contaminants (Repealed)
169
611 .648
Phase II, Phase IIB, and Phase V Synthetic Organic Contaminants
170 611 .650
Monitoring for 36 Contaminants (Repealed)
171 611 .657
Analytical Methods for 36 Contaminants (Repealed)
172 611 .658
Special Monitoring for Organic Chemicals (Repealed)
JCAR350611-0613054r01
173
174
SUBPART P : THM MONITORING AND ANALYTICAL REQUIREMENTS
175
176 Section
177 611 .680
Sampling, Analytical, and other Requirements
178 611 .683
Reduced Monitoring Frequency (Repealed)
179 611.684
Averaging (Repealed)
180 611 .685
Analytical Methods
181 611 .686
Modification to System (Repealed)
182 611 .687
Sampling for THM Potential (Repealed)
183 611 .688
Applicability Dates (Repealed)
184
185 SUBPART Q: RADIOLOGICAL MONITORING AND ANALYTICAL REQUIREMENTS
186
187 Section
188 611 .720
Analytical Methods
189 611 .731
Gross Alpha
190 611 .732
Beta Particle and Photon Radioactivity
191 611 .733
General Monitoring and Compliance Requirements
192
193
SUBPART R: ENHANCED FILTRATION AND DISINFECTION :
194
SYSTEMS THAT SERVE 10,000 OR MORE PEOPLE
195
196 Section
197 611.740
General Requirements
198 611 .741
Standards for Avoiding Filtration
199 611
.742
Disinfection Profiling and Benchmarking
200 611 .743
Filtration
201 611.744
Filtration Sampling Requirements
202 611 .745
Reporting and Recordkeeping Requirements
203
204
SUBPART T: REPORTING AND RECORDKEEPING
205
206 Section
207 611 .830
Applicability
208
611
.831
Monthly Operating Report
209 611 .832
Notice by Agency (Repealed)
210 611 .833
Cross Connection Reporting
211
611 .840
Reporting
212 611 .851
Reporting MCL, MRDL, and other Violations (Repealed)
213 611 .852
Reporting other Violations (Repealed)
214 611 .853
Notice to New Billing Units (Repealed)
215 611 .854
General Content of Public Notice (Repealed)
JCAR350611-0613054r01
216 611 .855
Mandatory Health Effects Language (Repealed)
217
611 .856
Fluoride Notice (Repealed)
218 611 .858
Fluoride Secondary Standard (Repealed)
219 611 .860
Record Maintenance
220 611 .870
List of 36 Contaminants (Repealed)
221
222
SUBPART U : CONSUMER CONFIDENCE REPORTS
223
224 Section
225 611 .881
Purpose and Applicability
226 611 .882
Compliance Dates
227 611 .883
Content of the Reports
228 611 .884
Required Additional Health Information
229 611 .885
Report Delivery and Recordkeeping
230
231
SUBPART V
: PUBLIC NOTIFICATION OF DRINKING WATER VIOLATIONS
232
233 Section
234 611 .901
General Public Notification Requirements
235 611 .902
Tier 1 Public Notice : Form, Manner, and Frequency of Notice
236 611 .903
Tier 2 Public Notice : Form, Manner, and Frequency of Notice
237 611 .904
Tier 3 Public Notice : Form, Manner, and Frequency of Notice
238 611 .905
Content of the Public Notice
239
611 .906
Notice to New Billing Units or New Customers
240 611 .907
Special Notice of the Availability of Unregulated Contaminant Monitoring
241
Results
242 611 .908
Special Notice for Exceedence of the Fluoride Secondary Standard
243 611 .909
Special Notice for Nitrate Exceedences above the MCL by a Non-Community
244
Water System
245 611 .910
Notice by the Agency on Behalf of a PWS
246
247
SUBPART X
: ENHANCED FILTRATION AND DISINFECTION -
248
SYSTEMS SERVING FEWER THAN 10,000 PEOPLE
249 Section
250 611 .950
General Requirements
251 611 .951
Finished Water Reservoirs
252 611 .952
Additional Watershed Control Requirements for Unfiltered Systems
253 611 .953
Disinfection Profile
254 611 .954
Disinfection Benchmark
255 611 .955
Combined Filter Effluent Turbidity Limits
256 611 .956
Individual Filter Turbidity Requirements
257
611 .957
Reporting and Recordkeeping Requirements
258
259
260
261
262
263
264
265
266
267
268
269
270
271
272
273
274
275
276
277
278
279
280
281
282
283
284
285
286
287
288
289
290
291
292
293
294
295
296
297
298
299
300
301
611 .APPENDIX A
611 .APPENDIX B
611 .APPENDIX C
611 .APPENDIX D
611 .APPENDIX E
611 .APPENDDC F
611
.APPENDIX G
611 .APPENDIX H
61 LAPPENDIX I
611 .TABLE A
611 .TABLE B
611 .TABLE C
61 I.TABLE D
611 .TABLE E
611 .TABLE F
611 .TABLE G
611 .TABLE Z
JCAR350611-0613054r01
Regulated Contaminants
Percent Inactivation of G . Lamblia Cysts
Common Names of Organic Chemicals
Defined Substrate Method for the Simultaneous Detection of Total
Coliforms and Eschericia Coli from Drinking Water
Mandatory Lead Public Education Information for Community Water
Systems
Mandatory Lead Public Education Information for Non-Transient Non-
Community Water Systems
NPDWR Violations and Situations Requiring Public Notice
Standard Health Effects Language for Public Notification
Acronyms Used in Public Notification Regulation
Total Coliform Monitoring Frequency
Fecal or Total Coliform Density Measurements
Frequency of RDC Measurement
Number of Lead and Copper Monitoring Sites
Lead and Copper Monitoring Start Dates
Number of Water Quality Parameter Sampling Sites
Summary of Section 611 .357 Monitoring Requirements for Water Quality
Parameters
Federal Effective Dates
AUTHORITY : Implementing Sections 7 .2, 17, and 17 .5 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/7 .2, 17, 17 .5, and 27] .
SOURCE
: Adopted in R88-26 at 14111
. Reg
. 16517, effective September 20, 1990 ; amended in
R90-21 at 14111 . Reg. 20448, effective December 11, 1990 ; amended in R90-13 at 15 Ill
. Reg .
1562, effective January 22, 1991 ; amended in R91-3 at 16 Ill . Reg
. 19010, effective December 1,
1992; amended in R92-3 at 17 Ill . Reg . 7796, effective May 18, 1993 ; amended in R93-1 at 17
Ill. Reg . 12650, effective July 23, 1993 ; amended in R94-4 at 18 Ill . Reg
. 12291, effective July
28, 1994; amended in R94-23 at 19 Ill . Reg . 8613, effective June 20, 1995
; amended in R95-17
at 20 Ill. Reg. 14493, effective October 22, 1996 ; amended in R98-2 at 22 Ill . Reg. 5020,
effective March 5, 1998; amended in R99-6 at 23 Ill . Reg. 2756, effective February 17, 1999 ;
amended in R99-12 at 23 Ill
. Reg. 10348, effective August 11, 1999 ; amended in R00-8 at 23 Ill .
Reg. 14715, effective December 8, 1999 ; amended in R00-10 at 24111 . Reg . 14226, effective
September 11, 2000 ; amended in R01-7 at 25 Ill . Reg. 1329, effective January 11, 2001
;
amended in R01-20 at 25 Ill
. Reg. 13611, effective October 9, 2001 ; amended in R02-5 at 26111.
Reg
. 3522, effective February 22, 2002 ; amended in R03-4 at 27 Ill . Reg . 1183, effective January
10, 2003 ; amended in R03-15 at 27 Ill . Reg. 16447, effective October 10, 2003 ; amended in
R04-3 at 28 Ill. Reg. 5269, effective March 10, 2004 ; amended in R04-13 at 28 Ill. Reg
. 12666,
effective August 26, 2004 ; amended in R05-6 at 29 Ill . Reg
. 2287, effective January 28, 2005 ;
amended in R06-15 at 30111 . Reg. , effective
JCAR350611-0613054r01
302
SUBPART A: GENERAL
303
304 Section 611.102 Incorporations by Reference
305
306
a)
Abbreviations and short-name listing of references . The following names and
307
abbreviated names, presented in alphabetical order, are used in this Part to refer to
308
materials incorporated by reference :
309
310
"Amco-AEPA-1 Polymer" is available from Advanced Polymer Systems
.
311
312
"ASTM Method" means a method published by and available from the
313
American Society for Testing and Materials (ASTM) .
314
315
"Colisure Test" means "Colisure Presence/Absence Test for Detection and
316
Identification of Coliform Bacteria and Escherichia Coli in Drinking
317
Water," available from Millipore Corporation, Technical Services
318
Department
.
319
320
"Colitag® Test" means "Colitag® Product as a Test for Detection and
321
Identification of Coliforms and E . coli Bacteria in Drinking Water and
322
Source Water as Required in National Primary Drinking Water
323
Regulations," available from CPI International.
324
325
"Dioxin and Furan Method 1613" means "Tetra- through Octa-Chlorinated
326
Dioxins and Furans by Isotope-Dilution HRGC/HRMS," available from
327
NTIS .
328
329
"GLI Method 2" means GLI Method 2, "Turbidity," Nov . 2, 1992,
330
available from Great Lakes Instruments, Inc .
331
332
"Hach FilterTrak Method 10133" means "Determination of Turbidity by
333
Laser Nephelometry," available from Hach Co .
334
335
"HASL Procedure Manual" means HASL Procedure Manual, HASL 300,
336
available from ERDA Health and Safety Laboratory .
337
338
"Kelada 01" means "Kelada Automated Test Methods for Total Cyanide,
339
Acid Dissociable Cyanide, And Thiocyanate," Revision 1 .2, August 2001,
340
EPA #821-B-01-009, available from the National Technical Information
341
Service (NTIS) .
342
343
"Membrane Filter Technique using Chromocult Doliform Agar" means
344
"Chromocult Coliform Agar Presence/Absence Membrane Filter Test
345
346
347
348
349
350
351
352
353
354
355
356
357
358
359
360
361
362
363
364
365
366
367
368
369
370
371
372
373
374
375
376
377
378
379
380
381
382
383
384
385
386
387
JCAR350611-0613054r01
Method for Detection and Identification of Coliform Bacteria and
Escherichia coli in Finished Waters," available from EMD Chemicals Inc .
"NCRP" means "National Council on Radiation Protection ."
"NTIS" means "National Technical Information Service ."
"New Jersey Radium Method" means "Determination of Radium 228 in
Drinking Water," available from the New Jersey Department of
Environmental Protection .
"New York Radium Method" means "Determination of Ra-226 and Ra-
228 (Ra-02)," available from the New York Department of Public Health.
"ONGP-MUG Test" (meaning "minimal medium ortho-nitrophenyl-beta-
d-galactopyranoside-4-methyl-umbelliferyl -beta-d-glucuronide test"),
also called the "Autoanalysis Colilert System," is Method 9223, available
in "Standard Methods for the Examination of Water and Wastewater," 18 th
ed., from American Public Health Association.
"Palintest Method 1001" means "Method Number 1001," available from
Palintest, Ltd
. or the Hach Company .
"QuikChem Method 10-204-00-1-X" means "Digestion and distillation of
total cyanide in drinking and wastewaters using MICRO DIST and
determination of cyanide by flow injection analysis," available from
Lachat Instruments .
"Readycult Coliforms 100 Presence/Absence Test" means "Readycult
Coliforms 100 Presence/Absence Test for Detection and Identification of
Coliform Bacteria and Escherichia coli in Finished Waters," available
from EMD Chemicals Inc .
"SimPlate Method" means "IDEXX SimPlate TM HPC Test Method for
Heterotrophs in Water," available from IDEXX Laboratories, Inc
.
"Radiochemical Methods" means "Interim Radiochemical Methodology
for Drinking Water," available from NTIS .
"Standard Methods" means "Standard Methods for the Examination of
Water and Wastewater," available from the American Public Health
Association or the American Waterworks Association
.
388
389
390
391
392
393
394
395
396
397
398
399
400
401
402
403
404
405
406
407
408
409
410
411
412
413
414
415
416
417
418
419
420
421
422
423
424
425
426
427
428
429
430
JCAR350611-0613054r01
"Syngenta AG-625" means "Atrazine in Drinking Water by
Immunoassay," February 2001 is available from Syngenta Crop
Protection, Inc
.
"Technical Bulletin 601" means "Technical Bulletin 601, Standard
Method of Testing for Nitrate in Drinking Water," July 1994, available
from Analytical Technology, Inc .
"Technicon Methods" means "Fluoride in Water and Wastewater,"
available from Bran & Luebbe .
"USDOE Manual" means "EML Procedures Manual," available from the
United State Department of Energy.
"USEPA Asbestos Methods-100
.1" means Method 100 .1, "Analytical
Method for Determination of Asbestos Fibers in Water," September 1983,
available from NTIS
.
"USEPA Asbestos Methods-100.2" means Method 100
.2, "Determination
of Asbestos Structures over 10-mm in Length in Drinking Water," June
1994, available from NTIS
.
"USEPA Environmental Inorganics Methods" means "Methods for the
Determination of Inorganic Substances in Environmental Samples,"
August 1993, available from NTIS .
"USEPA Environmental Metals Methods" means "Methods for the
Determination of Metals in Environmental Samples," available from
NTIS
.
"USEPA Inorganic Methods" means "Methods for Chemical Analysis of
Water and Wastes," March 1983, available from NTIS .
"USEPA Interim Radiochemical Methods" means "Interim Radiochemical
Methodology for Drinking Water," EPA 600/4-75-008 (revised), March
1976. Available from NTIS
.
"USEPA Organic Methods" means "Methods for the Determination of
Organic Compounds in Drinking Water," July 1991, for Methods 502 .2,
505, 507, 508, 508A, 515 .1, and 531 .1
; "Methods for the Determination of
Organic Compounds in Drinking Water -
Supplement I," July 1990, for
Methods 506, 547, 550, 550 .1, and 551
; and "Methods for the
Determination of Organic Compounds in Drinking Water -
Supplement
JCAR350611-0613054r01
431
II," August 1992, for Methods 515 .2, 524 .2, 548
.1, 549 .1, 552.1, and 555,
432
available from NTIS . Methods 504 .1, 508 .1, and 525 .2 are available from
433
EPA EMSL
; "Methods for the Determination of Organic Compounds" in
434
Drinking Water - Supplement II, August 1992, for Method 552
.1 ;
435
"Methods for the Determination of Organic Compounds in Drinking
436
Water - Supplement III," August 1995, for Methods 502 .2, 524 .2, 551 .1,
437
and 552 .2. Method 515
.4, "Determination of Chlorinated Acids in
438
Drinking Water by Liquid-Liquid Microextraction, Derivatization and Fast
439
Gas Chromatography with Electron Capture Detection," Revision 1 .0,
440
April 2000, EPA 815B-00/001, and Method 531 .2, "Measurement of N-
441
methylcarbamoyloximes and N-methylcarbamates in Water by Direct
442
Aqueous Injection HPLC with Postcolumn Derivatization," Revision 1 .0,
443
September 2001, EPA 815B/01/002, are both available on-line from
444
USEPA, Office of Ground Water and Drinking Water
.
445
446
"USEPA Radioactivity Methods" means "Prescribed Procedures for
447
Measurement of Radioactivity in Drinking Water," EPA 600/4-80-032,
448
August 1980 . Available from NTIS .
449
450
"USEPA Radiochemical Analyses" means "Radiochemical Analytical
451
Procedures for Analysis of Environmental Samples," March 1979 .
452
Available from NTIS .
453
454
"USEPA Radiochemistry Methods" means "Radiochemistry Procedures
455
Manual," EPA 520/5-84-006, December 1987 . Available from NTIS .
456
457
"USEPA Technical Notes" means "Technical Notes on Drinking Water
458
Methods," available from NTIS .
459
460
"USGS Methods" means "Methods of Analysis by the U .S . Geological
461
Survey National Water Quality Laboratory - Determination of Inorganic
462
and Organic Constituents in Water and Fluvial Sediments," available from
463
NTIS and USGS
.
464
465
"Waters Method B-1011" means "Waters Test Method for the
466
Determination of Nitrite/Nitrate in Water Using Single Column Ion
467
Chromatography," available from Waters Corporation, Technical Services
468
Division.
469
470
b)
The Board incorporates the following publications by reference :
471
472
Advanced Polymer Systems, 3696 Haven Avenue, Redwood City, CA
473
94063 415-366-2626.
474
475
476
477
478
479
480
481
482
483
484
485
486
487
488
489
490
491
492
493
494
495
496
497
498
499
500
501
502
503
504
505
506
507
508
509
510
511
512
513
514
515
516
JCAR350611-0613054r01
Amco-AEPA-1 Polymer
. See 40 CFR 141 .22(a) (2005)(2003).
Also, as referenced in ASTM D 1889.
American Public Health Association, 1015 Fifteenth Street NW,
Washington, DC 20005 800-645-5476 .
"Standard Methods for the Examination of Water and
Wastewater," 17"' Edition, 1989 (referred to as "Standard Methods,
17th ed.").
"Standard Methods for the Examination of Water and
Wastewater," 18
th
Edition, 1992, including "Supplement to the 18 th
Edition of Standard Methods for the Examination of Water and
Wastewater," 1994 (collectively referred to as "Standard Methods,
18 th ed."). Seethe methods listed separately for the same
references under American Waterworks Association .
"Standard Methods for the Examination of Water and
Wastewater," 19
th
Edition, 1995 (referred to as "Standard
Methods, 19 th ed.").
"Standard Methods for the Examination of Water and
Wastewater," 20th Edition, 1998 (referred to as "Standard Methods,
20th ed .").
American Waterworks Association et al ., 6666 West Quincy Ave .,
Denver, CO 80235 303-794-7711 .
"National Field Evaluation of a Defined Substrate Method for the
Simultaneous Enumeration of Total Coliforms and Escherichia coli
for Drinking Water : Comparison with the Standard Multiple Tube
Fermentation Method," S .C. Edberg, M .J. Allen & D .B. Smith,
Applied Environmental Microbiology, vol
. 54, iss. 6, pp 1595-
1601 (1988).
"Standard Methods for the Examination of Water and
Wastewater," 13 th Edition, 1971 (referred to as "Standard Methods,
13th ed.").
Method 302, Gross Alpha and Gross Beta Radioactivity in
Water (Total, Suspended, and Dissolved).
517
518
519
520
521
522
523
524
525
526
527
528
529
530
531
532
533
534
535
536
537
538
539
540
541
542
543
544
545
546
547
548
549
550
551
552
553
554
555
556
557
558
559
JCAR350611-0613054r01
Method 303, Total Radioactive Strontium and Strontium 90
in Water.
Method 304, Radium in Water by Precipitation
.
Method 305, Radium 226 by Radon in Water (Soluble,
Suspended, and Total) .
Method 306, Tritium in Water
.
"Standard Methods for the Examination of Water and
Wastewater," 17`h Edition, 1989 (referred to as "Standard Methods,
17th ed.") .
Method 7110 B, Gross Alpha and Gross Beta Radioactivity
in Water (Total, Suspended, and Dissolved).
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method.
Method
7500_3
H B, Tritium in Water .
Method 7500-I B, Radioactive Iodine, Precipitation
Method.
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method.
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium in Water by Precipitation.
Method 7500-Ra C, Radium 226 by Radon in Water
(Soluble, Suspended, and Total) .
Method 7500-Ra D, Radium, Sequential Precipitation
Method (Proposed).
Method 7500-Sr B, Total Radioactive Strontium and
Strontium 90 in Water .
Method 7500-U B, Uranium, Radiochemical Method
(Proposed).
560
561
562
563
564
565
566
567
568
569
570
571
572
573
574
575
576
577
578
579
580
581
582
583
584
585
586
587
588
589
590
591
592
593
594
595
596
597
598
599
600
601
602
JCAR350611-0613054r01
Method 7500-U C, Uranium, Isotopic Method (Proposed)
.
"Standard Methods for the Examination of Water and
Wastewater," 18"Edition, 1992 (referred to as "Standard Methods,
18 " ed.").
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method .
Method 2510 B, Conductivity, Laboratory Method
.
Method 2550, Temperature, Laboratory and Field Methods .
Method 3111 B, Metals by Flame Atomic Absorption
Spectrometry, Direct Air-Acetylene Flame Method .
Method 3111 D, Metals by Flame Atomic Absorption
Spectrometry, Direct Nitrous Oxide-Acetylene Flame
Method.
Method 3112 B, Metals by Cold-Vapor Atomic Absorption
Spectrometry, Cold-Vapor Atomic Absorption
Spectrometric Method .
Method 3113 B, Metals by Electrothermal Atomic
Absorption Spectrometry, Electrothermal Atomic
Absorption Spectrometric Method.
Method 3114 B, Metals by Hydride Generation/Atomic
Absorption Spectrometry, Manual Hydride
Generation/Atomic Absorption Spectrometric Method .
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method.
Method 3500-Ca D, Calcium, EDTA Titrimetric Method .
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
603
604
605
606
607
608
609
610
611
612
613
614
615
616
617
618
619
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621
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623
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626
627
628
629
630
631
632
633
634
635
636
637
638
639
640
641
642
643
644
645
JCAR350611-0613054r01
Suppression of Eluent Conductivity .
Method 4500-CN - C, Cyanide, Total Cyanide after
Distillation .
Method 4500-CN - E, Cyanide, Colorimetric Method .
Method 4500-CN F, Cyanide, Cyanide-Selective Electrode
Method.
Method 4500-CN G, Cyanide, Cyanides Amenable to
Chlorination after Distillation .
Method 4500-Cl D, Chlorine, Amperometric Titration
Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method .
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method .
Method 4500-Cl I, Chlorine, Iodometric Electrode Method
.
Method 4500-C1O2 C, Chlorine Dioxide, Amperometric
Method I.
Method 4500-C1O2 D, Chlorine Dioxide, DPD Method
.
Method 4500-C1O 2
E, Chlorine Dioxide, Amperometric
Method II (Proposed) .
Method 4500-F" B, Fluoride, Preliminary Distillation Step .
Method 4500-F- C, Fluoride, Ion-Selective Electrode
Method .
Method 4500-F - D, Fluoride, SPADNS Method
.
646
647
648
649
650
651
652
653
654
655
656
657
658
659
660
661
662
663
664
665
666
667
668
669
670
671
672
673
674
675
676
677
678
679
680
681
682
683
684
685
686
687
688
JCAR350611-0613054r01
Method 4500-F - E, Fluoride, Complexone Method.
Method 4500-H' B, pH Value, Electrometric Method .
Method 4500-NO3 B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3 D, Nitrogen (Nitrate), Nitrate Electrode
Method .
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method .
Method 4500-NO3 - F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
Method 4500-0 3
B, Ozone (Residual) (Proposed), Indigo
Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method .
Method 4500-Si D, Silica, Molybdosilicate Method .
Method 4500-Si E, Silica, Heteropoly Blue Method
.
Method 4500-Si F, Silica, Automated Method for
Molybdate-Reactive Silica
.
Method 6651, Glyphosate Herbicide (Proposed)
.
Method 7110 B, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Evaporation Method for
Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
689
690
691
692
693
694
695
696
697
698
699
700
701
702
703
704
705
706
707
708
709
710
711
712
713
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717
718
719
720
721
722
723
724
725
726
727
728
729
730
731
JCAR350611-0513054r01
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method.
Method 7500-3 H B, Tritium, Liquid Scintillation
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation
Method.
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method.
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Ra D, Radium, Sequential Precipitation
Method (Proposed) .
Method 7500-Sr B, Total Radioactive Strontium and
Strontium 90, Precipitation Method
.
Method 7500-U B, Uranium, Radiochemical Method
(Proposed).
Method 7500-U C, Uranium, Isotopic Method (Proposed) .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method.
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique.
Method 9221 C, Multiple-Tube
Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density
.
732
733
734
735
736
737
738
739
740
741
742
743
744
745
746
747
748
749
750
751
752
753
754
755
756
757
758
759
760
761
762
763
764
765
766
767
768
769
770
771
772
773
774
JCAR350611-0613054r01
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Fecal Coliform
Procedure.
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction .
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure.
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure.
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure.
Method 9223, Chromogenic Substrate Coliform Test
(Proposed).
"Supplement to the 18`h Edition of Standard Methods for the
Examination of Water and Wastewater," American Public Health
Association, 1994 .
Method 6610, Carbamate Pesticide Method .
"Standard Methods for the Examination of Water and
Wastewater," 19 th Edition, 1995 (referred to as "Standard Methods,
19th ed.").
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method
.
Method 2510 B, Conductivity, Laboratory Method .
Method 2550, Temperature, Laboratory, and Field
775
776
777
778
779
780
781
782
783
784
785
786
787
788
789
790
791
792
793
794
795
796
797
798
799
800
801
802
803
804
805
806
807
808
809
810
811
812
813
814
815
816
817
JCAR350611-061305401
Methods .
Method 3111 B, Metals by Flame Atomic Absorption
Spectrometry, Direct Air-Acetylene Flame Method .
Method 3111 D, Metals by Flame Atomic Absorption
Spectrometry, Direct Nitrous Oxide-Acetylene Flame
Method .
Method 3112 B, Metals by Cold-Vapor Atomic Absorption
Spectrometry, Cold-Vapor Atomic Absorption
Spectrometric Method .
Method 3113 B, Metals by Electrothermal Atomic
Absorption Spectrometry, Electrothermal Atomic
Absorption Spectrometric Method .
Method 3114 B, Metals by Hydride Generation/Atomic
Absorption Spectrometry, Manual Hydride
Generation/Atomic Absorption Spectrometric Method .
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method .
Method 3500-Ca D, Calcium, EDTA Titrimetric Method .
Method 3500-Mg E, Magnesium, Calculation Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
Suppression of Eluent Conductivity
.
Method 4500-Cl D, Chlorine, Amperometric Titration
Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method
.
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method
.
818
819
820
821
822
823
824
825
826
827
828
829
830
831
832
833
834
835
836
837
838
839
840
841
842
843
844
845
846
847
848
849
850
851
852
853
854
855
856
857
858
859
860
JCAR350611-0613054r01
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method .
Method 4500-Cl I, Chlorine, lodometric Electrode Method.
Method 4500-C1O2 C, Chlorine Dioxide, Amperometric
Method I .
Method 4500-C1O2 D, Chlorine Dioxide, DPD Method .
Method 4500-C1O2 E, Chlorine Dioxide, Amperometric
Method II (Proposed) .
Method 4500-CN C, Cyanide, Total Cyanide after
Distillation .
Method 4500-CN E, Cyanide, Colorimetric Method .
Method 4500-CN-
F, Cyanide, Cyanide-Selective Electrode
Method .
Method 4500-CN - G, Cyanide, Cyanides Amenable to
Chlorination after Distillation .
Method 4500-F- B, Fluoride, Preliminary Distillation Step
.
Method 4500-F" C, Fluoride, Ion-Selective Electrode
Method .
Method 4500-F
- D, Fluoride, SPADNS Method .
Method 4500-F - E, Fluoride, Complexone Method
.
Method 4500-H` B, pH Value, Electrometric Method
.
Method 4500-NOi B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3 D, Nitrogen (Nitrate), Nitrate Electrode
Method
.
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method .
861
862
863
864
865
866
867
868
869
870
871
872
873
874
875
876
877
878
879
880
881
882
883
884
885
886
887
888
889
890
891
892
893
894
895
896
897
898
899
900
901
902
903
JCAR350611-0613054r01
Method 4500-NO3 F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo
Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method .
Method 4500-Si D, Silica, Molybdosilicate Method
.
Method 4500-Si E, Silica, Heteropoly Blue Method
.
Method 4500-Si F, Silica, Automated Method for
Molybdate-Reactive Silica .
Method 5910 B, UV Absorbing Organic Constituents,
Ultraviolet Absorption Method .
Method 6251 B, Disinfection Byproducts : Haloacetic
Acids and Trichlorophenol, Micro Liquid-Liquid
Extraction Gas Chromatographic Method .
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110 B, Gross Alpha and Gross Beta
Radioactivity, Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
Method 7120 B, Gamma-Emitting Radionuclides, Gamma
Spectrometric Method .
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method .
Method 7500-3H B, Tritium, Liquid Scintillation
7CAR350611-0613054r01
Spectrometric Method .
Method 7500-I B, Radioactive Iodine, Precipitation
Method .
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method .
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Ra D, Radium, Sequential Precipitation
Method.
Method 7500-Sr B, Total Radiactive Strontium and
Strontium 90, Precipitation Method .
Method 7500-U B, Uranium, Radiochemical Method .
Method 7500-U C, Uranium, Isotopic Method .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method.
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction.
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique.
Method 9221 C, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density.
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test .
946
947
948
949
950
951
952
953
954
955
956
957
958
959
960
961
962
963
964
965
966
967
968
969
970
971
972
973
974
975
976
977
978
979
980
981
982
983
984
985
986
987
988
JCAR350611-061305401
Method 9221 E, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Fecal Coliform
Procedure.
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction .
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure.
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure.
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure .
Method 9223, Chromogenic Substrate Coliform Test
(Proposed) .
"Supplement to the 19 th Edition of Standard Methods for the
Examination of Water and Wastewater," American Public Health
Association, 1996 .
Method 5310 B, TOC, Combustion-Infrared Method
.
Method 5310 C, TOC, Persulfate-Ultraviolet Oxidation
Method.
Method 5310 D, TOC, Wet-Oxidation Method .
"Standard Methods for the Examination of Water and
Wastewater," 20`h Edition, 1998 (referred to as "Standard Methods,
20`h ed.").
Method 2130 B, Turbidity, Nephelometric Method .
Method 2320 B, Alkalinity, Titration Method
.
Method 2510 B, Conductivity, Laboratory Method .
989
990
991
992
993
994
995
996
997
998
999
1000
1001
1002
1003
1004
1005
1006
1007
1008
1009
1010
1011
1012
1013
1014
1015
1016
1017
1018
1019
1020
1021
1022
1023
1024
1025
1026
1027
1028
1029
1030
JCAR350611-0613054r01
Method 2550, Temperature, Laboratory, and Field
Methods .
Method 3120 B, Metals by Plasma Emission Spectroscopy,
Inductively Coupled Plasma (ICP) Method .
Method 3500-Ca B, Calcium, EDTA Titrimetric Method.
Method 3500-Mg B, Magnesium, EDTA Titrimetric
Method .
Method 4110 B, Determination of Anions by Ion
Chromatography, Ion Chromatography with Chemical
Suppression of Eluent Conductivity .
Method 4500-CN C, Cyanide, Total Cyanide after
Distillation
.
Method 4500-CN E, Cyanide, Colorimetric Method .
Method 4500-CN - F, Cyanide, Cyanide-Selective Electrode
Method .
Method 4500-CN G, Cyanide, Cyanides Amenable to
Chlorination after Distillation .
Method 4500-Cl D, Chlorine, Amperometric Titration
Method .
Method 4500-Cl E, Chlorine, Low-Level Amperometric
Titration Method .
Method 4500-Cl F, Chlorine, DPD Ferrous Titrimetric
Method .
Method 4500-Cl G, Chlorine, DPD Colorimetric Method
.
Method 4500-Cl H, Chlorine, Syringaldazine (FACTS)
Method .
Method 4500-Cl I, Chlorine, lodometric Electrode Method
.
1031
1032
1033
1034
1035
1036
1037
1038
1039
1040
1041
1042
1043
1044
1045
1046
1047
1048
1049
1050
1051
1052
1053
1054
1055
1056
1057
1058
1059
1060
1061
1062
1063
1064
1065
1066
1067
1068
1069
1070
1071
1072
1073
JCAR350611-0613054r01
Method 4500-C102 C, Chlorine Dioxide, Amperometric
Method I.
Method 4500-002 D, Chlorine Dioxide, DPD Method .
Method 4500-CIO2 E, Chlorine Dioxide, Amperometric
Method II (Proposed) .
Method 4500-F B, Fluoride, Preliminary Distillation Step .
Method 4500-F" C, Fluoride, Ion-Selective Electrode
Method
.
Method 4500-F D, Fluoride, SPADNS Method .
Method 4500-F- E, Fluoride, Complexone Method .
Method 4500-H + B, pH Value, Electrometric Method .
Method 4500-N02 B, Nitrogen (Nitrite), Colorimetric
Method .
Method 4500-NO3" D, Nitrogen (Nitrate), Nitrate Electrode
Method .
Method 4500-NO3 E, Nitrogen (Nitrate), Cadmium
Reduction Method .
Method 4500-NO3 F, Nitrogen (Nitrate), Automated
Cadmium Reduction Method .
Method 4500-03 B, Ozone (Residual) (Proposed), Indigo
Colorimetric Method .
Method 4500-P E, Phosphorus, Ascorbic Acid Method .
Method 4500-P F, Phosphorus, Automated Ascorbic Acid
Reduction Method .
Method 4500-Si C, Silica, Molybdosilicate Method .
Method 4500-Si D, Silica, Heteropoly Blue Method
.
1074
1075
1076
1077
1078
1079
1080
1081
1082
1083
1084
1085
1086
1087
1088
1089
1090
1091
1092
1093
1094
1095
1096
1097
1098
1099
1100
1101
1102
1103
1104
1105
1106
1107
1108
1109
1110
1111
1112
1113
1114
1115
JCAR350611-0613054r01
Method 4500-Si E, Silica, Automated Method for
Molybdate-Reactive Silica .
Method 4500-Cl E, Chlorine (Residual), Low-Level
Amperometric Titration Method .
Method 4500-Cl F, Chlorine (Residual), DPD Ferrous
Titrimetric Method .
Method 4500-Cl G, Chlorine (Residual), DPD Colorimetric
Method .
Method 4500-Cl H, Chlorine (Residual), Syringaldazine
(FACTS) Method .
Method 4500-Cl I, Chlorine (Residual), Iodometric
Electrode Technique .
Method 4500-C102 D, Chlorine Dioxide, DPD Method .
Method 4500-C102 E, Chlorine Dioxide, Amperometric
Method II .
Method 6651, Glyphosate Herbicide (Proposed) .
Method 7110-B, Gross Alpha and Gross Beta
Radioactivity, Evaporation Method for Gross Alpha-Beta .
Method 7110 C, Gross Alpha and Beta Radioactivity
(Total, Suspended, and Dissolved), Coprecipitation Method
for Gross Alpha Radioactivity in Drinking Water
(Proposed) .
Method 7120-B, Gamma-Emitting Radionuclides, Gamma
Spectrometric Method .
Method 7500-Cs B, Radioactive Cesium, Precipitation
Method
.
Method 7500-3H B, Tritium, Liquid Scintillation
Spectrometric Method .
1116
1117
1118
1119
1120
1121
1122
1123
1124
1125
1126
1127
1128
1129
1130
1131
1132
1133
1134
1135
1136
1137
1138
1139
1140
1141
1142
1143
1144
1145
1146
1147
1148
1149
1150
1151
1152
1153
1154
1155
1156
1157
1158
JCAR350611-0613054r01
Method 7500-I B, Radioactive Iodine, Precipitation
Method.
Method 7500-I C, Radioactive Iodine, Ion-Exchange
Method.
Method 7500-I D, Radioactive Iodine, Distillation Method .
Method 7500-Ra B, Radium, Precipitation Method .
Method 7500-Ra C, Radium, Emanation Method .
Method 7500-Sr B, Total Radiactive Strontium and
Strontium 90, Precipitation Method .
Method 7500-U B, Uranium, Radiochemical Method .
Method 7500-U C, Uranium, Isotopic Method .
Method 9215 B, Heterotrophic Plate Count, Pour Plate
Method .
Method 9221 A, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Introduction .
Method 9221 B, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Standard Total
Coliform Fermentation Technique.
Method 9221 C, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Estimation of
Bacterial Density.
Method 9221 D, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Presence-Absence (P-
A) Coliform Test .
Method 9221 E, Multiple-Tube Fermentation Technique
for Members of the Coliform Group, Fecal Coliform
Procedure.
Method 9222 A, Membrane Filter Technique for Members
of the Coliform Group, Introduction .
1159
1160
1161
1162
1163
1164
1165
1166
1167
1168
1169
1170
1171
1172
1173
1174
1175
1176
1177
1178
1179
1180
1181
1182
1183
1184
1185
1186
1187
1188
1189
1190
1191
1192
1193
1194
1195
1196
1197
1198
1199
1200
1201
JCAR350611-0613054r01
Method 9222 B, Membrane Filter Technique for Members
of the Coliform Group, Standard Total Coliform Membrane
Filter Procedure.
Method 9222 C, Membrane Filter Technique for Members
of the Coliform Group, Delayed-Incubation Total Coliform
Procedure.
Method 9222 D, Membrane Filter Technique for Members
of the Coliform Group, Fecal Coliform Membrane Filter
Procedure .
Method 9223, Chromogenic Substrate Coliform Test
(Proposed).
Analytical Technology, Inc
. ATI Orion, 529 Main Street, Boston, MA
02129 .
Technical Bulletin 601, "Standard Method of Testing for Nitrate in
Drinking Water," July, 1994, PN 221890-001 (referred to as
"Technical Bulletin 601
") .
ASTM. American Society for Testing and Materials, 100 Barr Harbor
Drive, West Conshohocken, PA 19428-2959 610-832-9585
.
ASTM Method D511-93 A and B, "Standard Test Methods for
Calcium and Magnesium in Water," "Test Method A
-
Complexometric Titration" & "Test Method B -
Atomic
Absorption Spectrophotometric," approved 1993
.
ASTM Method D515-88 A, "Standard Test Methods for
Phosphorus in Water," "Test Method A
-
Colorimetric Ascorbic
Acid Reduction," approved August 19, 1988
.
ASTM Method D859-88, "Standard Test Method for Silica in
Water," approved August 19, 1988 .
ASTM Method D1067-92 B, "Standard Test Methods for Acidity
or Alkalinity in Water," "Test Method B
-
Electrometric or Color-
Change Titration," approved May 15, 1992
.
ASTM Method D1125-91 A, "Standard Test Methods for
1202
1203
1204
1205
1206
1207
1208
1209
1210
1211
1212
1213
1214
1215
1216
1217
1218
1219
1220
1221
1222
1223
1224
1225
1226
1227
1228
1229
1230
1231
1232
1233
1234
1235
1236
1237
1238
1239
1240
1241
1242
1243
1244
JCAR350611-0613054r01
Electrical Conductivity and Resistivity of Water," "Test Method A
- Field and Routine Laboratory Measurement of Static (Non-
Flowing) Samples," approved June 15, 1991 .
ASTM Method DI 179-93 B, "Standard Test Methods for Fluoride
in Water," "Test Method B -
Ion Selective Electrode," approved
1993 .
ASTM Method D1253-86, "Standard Test Method for Residual
Chlorine in Water," reapproved 1992 .
ASTM Method D1293-84, "Standard Test Methods for pH of
Water," "Test Method A -
Precise Laboratory Measurement" &
"Test Method B - Routine or Continuous Measurement," approved
October 26, 1984
.
ASTM Method D1688-90 A or C, "Standard Test Methods for
Copper in Water," "Test Method A - Atomic Absorption, Direct"
& "Test Method C -Atomic Absorption, Graphite Furnace,"
approved March 15, 1990 .
ASTM Method D2036-91 A or B, "Standard Test Methods for
Cyanide in Water," "Test Method A
- Total Cyanides after
Distillation" & "Test Method B - Cyanides Amenable to
Chlorination by Difference," approved September 15, 1991 .
ASTM Method D2459-72, "Standard Test Method for Gamma
Spectrometry in Water," approved July 28, 1972, discontinued
1988 .
ASTM Method D2460-90, "Standard Test Method for
Radionuclides of Radium in Water," approved 1990,
ASTM Method D2907-91, "Standard Test Methods for
Microquantities of Uranium in Water by Fluorometry," "Test
Method A - Direct Fluorometric" & "Test Method B -
Extraction," approved June 15, 1991 .
ASTM Method D2972-93 B or C, "Standard Test Methods for
Arsenic in Water," "Test Method B - Atomic Absorption, Hydride
Generation" & "Test Method C
-
Atomic Absorption, Graphite
Furnace," approved 1993 .
1245
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1247
1248
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1250
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1278
1279
1280
1281
1282
1283
1284
1285
1286
1287
JCAR350611-0613054r01
ASTM Method D3223-91, "Standard Test Method for Total
Mercury in Water," approved September 23, 1991 .
ASTM Method D3454-91, "Standard Test Method for Radium-226
in Water," approved 1991 .
ASTM Method D3559-90 D, "Standard Test Methods for Lead in
Water," "Test Method D - Atomic Absorption, Graphite Furnace,"
approved August 6, 1990 .
ASTM Method D3645-93 B, "Standard Test Methods for
Beryllium in Water," "Method B - Atomic Absorption, Graphite
Furnace," approved 1993 .
ASTM Method D3649-91, "Standard Test Method for High-
Resolution Gamma-Ray Spectrometry of Water," approved 1991
.
ASTM Method D3697-92, "Standard Test Method for Antimony in
Water," approved June 15, 1992 .
ASTM Method D3859-93 A, "Standard Test Methods for
Selenium in Water," "Method A - Atomic Absorption, Hydride
Method," approved 1993
.
ASTM Method D3867-90 A and B, "Standard Test Methods for
Nitrite-Nitrate in Water," "Test Method A - Automated Cadmium
Reduction" & "Test Method B - Manual Cadmium Reduction,"
approved January 10, 1990 .
ASTM Method D3972-90, "Standard Test Method for Isotopic
Uranium in Water by Radiochemistry," approved 1990
.
ASTM Method D4107-91, "Standard Test Method for Tritium in
Drinking Water," approved 1991
.
ASTM Method D4327-91, "Standard Test Method for Anions in
Water by Ion Chromatography," approved October 15, 1991
.
ASTM Method D4785-88, "Standard Test Method for Low-Level
Iodine-131 in Water," approved 1988 .
ASTM Method D5174-91, "Standard Test Method for Trace
Uranium in Water by Pulsed-Laser Phosphorimetry," approved
1288
1289
1290
1291
1292
1293
1294
1295
1296
1297
1298
1299
1300
1301
1302
1303
1304
1305
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1307
1308
1309
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1311
1312
1313
1314
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1317
1318
1319
1320
1321
1322
1323
1324
1325
1326
1327
1328
1329
1330
JCAR350611-0613054r01
1991
.
ASTM Method D5673-03, "Standard Test Method for Elements in
Water by Inductively Coupled Plasma - Mass Spectrometry, "
approved 2003 .
Bran & Luebbe, 1025 Busch Parkway, Buffalo Grove, IL 60089 .
"Fluoride in Water and Wastewater," Industrial Method 4129-
71W, December 1972 (referred to as "Technicon Methods : Method
#129-71W"). See 40 CFR 141 .23(k)(1), footnote 11 (2005)(2003).
"Fluoride in Water and Wastewater," #380-75WE, February 1976
(referred to as "Technicon Methods
: Method #380-75WE") . See
40 CFR 141 .23(k)(1), footnote 11 (2005){0033 .
CPI International, Inc., 5580 Skylane Blvd ., Santa Rosa, CA 95403 .
Telephone
: 800-878-7654
. Fax : 707-545-7901 . Internet address :
www.cpiintemational .com.
"Colitag® Product as a Test for Detection and Identification of
Coliforms and E. coli Bacteria in Drinking Water and Source
Water as Required in National Primary Drinking Water
Regulations," August 2001 .
EMD Chemicals Inc. (an affiliate of Merck KGgA, Darmstadt, Germany),
480 S . Democrat Road, Gibbstown, NJ 08027-1297
. Telephone : 800-
222-0342. E-mail: adellenbusch@emscience .com.
"Chromocult Coliform Agar Presence/Absence Membrane Filter
Test Method for Detection and Identification of Coliform Bacteria
and Escherichia coli in Finished Waters," November 2000, Version
1 .0.
"Readycult Coliforms 100 Presence/Absence Test for Detection
and Identification of Coliform Bacteria and Escherichia coli in
Finished Waters," November 2000, Version 1 .0
.
ERDA Health and Safety Laboratory, New York, NY
.
HASL Procedure Manual, HASL 300, 1973
. See 40 CFR
141
.25(b)(2) 2(005)(20034
.
1331
1332
1333
1334
1335
1336
1337
1338
1339
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1366
1367
1368
1369
1370
1371
1372
1373
JCAR350611-0613054r01
Great Lakes Instruments, Inc ., 8855 North 55`h Street, Milwaukee, WI
53223
.
GLI Method 2, "Turbidity," Nov . 2, 1992.
The Hach Company, P .O. Box 389, Loveland, CO 80539-0389 . Phone:
800-227-4224.
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
"Determination of Turbidity by Laser Nephelometry," January
2000, Revision 2 .0 (referred to as "Hach FilterTrak Method
10133") .
IDEXX Laboratories, Inc., One IDEXX Drive, Westbrook, Maine 04092 .
Telephone : 800-321-0207 .
"IDEXX SimPlate TM HPC Test Method for Heterotrophs in
Water," November 2000 .
Lachat Instruments, 6645 W . Mill Rd., Milwaukee, WI 53218 . Phone :
414-358-4200 .
"Digestion and distillation of total cyanide in drinking and
wastewaters using MICRO DIST and determination of cyanide by
flow injection analysis," Revision 2 .1, November 30, 2000
(referred to as "QuikChem Method 10-204-00-1-X") .
Millipore Corporation, Technical Services Department, 80 Ashby Road,
Milford, MA 01730 800-654-5476.
Colisure Presence/Absence Test for Detection and Identification of
Coliform Bacteria and Escherichia Coli in Drinking Water,
February 28, 1994 (referred to as "Colisure Test") .
NCRP . National Council on Radiation Protection, 7910 Woodmont Ave.,
Bethesda, MD 301-657-2652
.
"Maximum Permissible Body Burdens and Maximum Permissible
Concentrations of Radionuclides in Air and in Water for
Occupational Exposure," NCRP Report Number 22, June 5, 1959 .
1374
1375
1376
1377
1378
1379
1380
1381
1382
1383
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1385
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1387
1388
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1401
1402
1403
1404
1405
1406
1407
1408
1409
1410
1411
1412
1413
1414
1415
1416
JCAR350611-0613054r01
NSF. National Sanitation Foundation International, 3475 Plymouth Road,
PO Box 130140, Ann Arbor, Michigan 48113-0140, 734-769-8010 .
NSF Standard 61, section 9, November 1998 .
NTIS . National Technical Information Service, U.S. Department of
Commerce, 5285 Port Royal Road, Springfield, VA 22161, 703-487-4600
or 800-553-6847.
"Interim Radiochemical Methodology for Drinking Water," EPA
600/4-75-008 (revised), March 1976 (referred to as "USEPA
Interim Radiochemical Methods"). (Pages 1, 4, 6, 9, 13, 16, 24, 29,
34)
"Kelada Automated Test Methods for Total Cyanide, Acid
Dissociable Cyanide, And Thiocyanate," Revision 1 .2, August
2001, EPA # 821-B-01-009 (referred to as "Kelada 01 ").
"Maximum Permissible Body Burdens and Maximum Permissible
Concentrations of Radionuclides in Air and in Water for
Occupational Exposure," NBS (National Bureau of Standards)
Handbook 69, as amended August 1963, U .S. Department of
Commerce .
Method 100.1, "Analytical Method for Determination of Asbestos
Fibers in Water," EPA-600/4-83-043, September 1983, Doc . No.
PB83-260471 (referred to as "USEPA Asbestos Methods-100 .1").
Method 100.2, "Determination of Asbestos Structures over 10-mm
in Length in Drinking Water," EPA-600/4-83-043, June 1994,
Doc. No. PB94-201902 (referred to as "USEPA Asbestos
Methods-100 .2") .
"Methods for Chemical Analysis of Water and Wastes," March
1983, Doc. No. PB84-128677 (referred to as "USEPA Inorganic
Methods"). (Methods 150 .1, 150 .2, and 245 .2, which formerly
appeared in this reference, are available from USEPA EMSL.)
"Methods for the Determination of Inorganic Substances in
Environmental Samples," August 1993, PB94-120821 (referred to
as "USEPA Environmental Inorganic Methods") .
1417
1418
1419
1420
1421
1422
1423
1424
1425
1426
1427
1428
1429
1430
1431
1432
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1435
1436
1437
1438
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1443
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1447
1448
1449
1450
1451
1452
1453
1454
1455
1456
1457
1458
1459
JCAR350611-0613054r01
"Methods for the Determination of Metals in Environmental
Samples," June 1991, Doc . No. PB91-231498 and "Methods for
the Determination of Metals in Environmental Samples -
Supplement I," May 1994, PB95-125472 (referred to as "USEPA
Environmental Metals Methods").
"Methods for the Determination of Organic Compounds in
Drinking Water," December 1988, revised July 1991, EPA-600/4-
88/039 (referred to as "USEPA Organic Methods") . (For methods
502.2, 505, 507, 508, 508A, 515 .1, and 531 .1 .)
"Methods for the Determination of Organic Compounds in
Drinking Water - Supplement I," July 1990, EPA/600-4-90-020
(referred to as "USEPA Organic Methods")
. (For methods 506,
547, 550, 550 .1, and 551 .)
"Methods for the Determination of Organic Compounds in
Drinking Water - Supplement II," August 1992, EPA-600/R-92-
129 (referred to as "USEPA Organic Methods") . (For methods
515 .2, 524 .2, 548 .1, 549 .1, 552 .1, and 555 .)
"Prescribed Procedures for Measurement of Radioactivity in
Drinking Water," EPA 600/4-80-032, August 1980 (document
number PB 80-224744) (referred to as "USEPA Radioactivity
Methods"). (Methods 900, 901, 901 .1, 902, 903, 903 .1, 904, 905,
906, 908, 908
.1)
"Procedures for Radiochemical Analysis of Nuclear Reactor
Aqueous Solutions," H .L. Krieger and S. Gold, EPA-R4-73-014,
May 1973, Doc
. No. PB222-154/7BA .
"Radiochemical Analytical Procedures for Analysis of
Environmental Samples," March 1979, Doc. No. EMSL LV
053917 (referred to as "USEPA Radiochemical Analyses") .
(Pages 1, 19, 33, 65, 87, 92)
"Radiochemistry Procedures Manual," EPA-520/5-84-006,
December 1987, Doc . No. PB-84-215581 (referred to as "USEPA
Radiochemistry Methods") . (Methods 00-01, 00-02, 00-07, H-02,
Ra-03, Ra-04, Ra-05, Sr-04)
"Technical Notes on Drinking Water Methods," EPA-600/R-94-
173, October 1994, Doc . No. PB-104766 (referred to as "USEPA
1460
1461
1462
1463
1464
1465
1466
1467
1468
1469
1470
1471
1472
1473
1474
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1478
1479
1480
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1483
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1493
1494
1495
1496
1497
1498
1499
1500
1501
1502
JCAR350611-0613054r01
Technical Notes") .
BOARD NOTE : USEPA made the following assertion with
regard to this reference at 40 CFR 141
.23(k)(1) and 141 .24(e) and
(n)(11) 2(005X2003) :
"This document contains other analytical
test procedures and approved analytical methods that remain
available for compliance monitoring until July 1, 1996
."
"Tetra- through Octa-Chlorinated Dioxins and Furans by Isotope
Dilution HRGC/HRMS," October 1994, EPA-821-B-94-005
(referred to as "Dioxin and Furan Method 1613")
.
New Jersey Department of Environment, Division of Environmental
Quality, Bureau of Radiation and Inorganic Analytical Services, 9 Ewing
Street, Trenton, NJ 08625.
"Determination of Radium 228 in Drinking Water," August 1990
.
New York Department of Health, Radiological Sciences Institute, Center
for Laboratories and Research, Empire State Plaza, Albany, NY 12201 .
"Determination of Ra-226 and Ra-228
(Ra-02)," January 1980,
Revised June 1982 .
Palintest, Ltd
., 21 Kenton Lands Road, P.O
. Box 18395, Erlanger, KY
800-835-9629 .
"Lead in Drinking Water by Differential Pulse Anodic Stripping
Voltammetry," Method 1001, August 1999 .
Syngenta Crop Protection, Inc
., 410 Swing Road, Post Office Box 18300,
Greensboro, NC 27419 . Telephone
: 336-632-6000 .
"Atrazine in Drinking Water by Immunoassay," February 2001
(referred to as "Syngenta AG-625")
.
United States Department of Energy, available at the Environmental
Measurements Laboratory, U .S
. Department of Energy, 376 Hudson
Street, New York, NY 10014-3621
.
"EML Procedures Manual," 27`h
Edition, Volume 1, 1990 .
United States Environmental Protection Agency, Office of Ground Water
and Drinking Water, accessible on-line and available by download from
JCAR350611-0613054r01
1503
http://wivw.epa.gov/safewater/methods/ .
1504
1505
Method 515 .4, "Determination of Chlorinated Acids in Drinking
1506
Water by Liquid-Liquid Microextraction, Derivatization and Fast
1507
Gas Chromatography with Electron Capture Detection," Revision
1508
1 .0, April 2000, EPA 815B-00/001 (document file name
1509
"met515 4.pdf') .
1510
1511
Method 531 .2, "Measurement of N-methylcarbamoyloximes and
1512
N-methylcarbamates in Water by Direct Aqueous Injection HPLC
1513
with Postcolumn Derivatization," Revision 1 .0, September 2001,
1514
EPA 815B/01/002 (document file name "met531 2 .pdf').
1515
1516
United States Environmental Protection Agency, EMSL, Cincinnati, OH
1517
45268 513-569-7586 .
1518
1519
"Interim Radiochemical Methodology for Drinking Water," EPA-
1520
600/4-75-008 (referred to as "Radiochemical Methods") .
1521
(Revised) March 1976 .
1522
1523
"Methods for the Determination of Organic Compounds in
1524
Finished Drinking Water and Raw Source Water" (referred to as
1525
"USEPA Organic Methods"). (For methods 504 .1, 508 .1, and
1526
525 .2 only.) See NTIS .
1527
1528
"Procedures for Radiochemical Analysis of Nuclear Reactor
1529
Aqueous Solutions ." See NTIS .
1530
1531
USEPA, Science and Technology Branch, Criteria and Standards
1532
Division, Office of Drinking Water, Washington, D .C
. 20460.
1533
1534
"Guidance Manual for Compliance with the Filtration and
1535
Disinfection Requirements for Public Water Systems using Surface
1536
Water Sources," October 1989 .
1537
1538
USGS . Books and Open-File Reports Section, United States Geological
1539
Survey, Federal Center, Box 25286, Denver, CO 80225-0425
.
1540
1541
Methods available upon request by method number from "Methods
1542
for Analysis by the U .S . Geological Survey National Water
1543
Quality Laboratory
- Determination of Inorganic and Organic
1544
Constituents in Water and Fluvial Sediments," Open File Report
1545
93-125, 1993, or Book 5, Chapter A-1, "Methods for
JCAR350611-0613054r01
1546
Determination of Inorganic Substances in Water and Fluvial
1547
Sediments," 3rd ed ., Open-File Report 85-495, 1989, as
1548
appropriate (referred to as "USGS Methods")
.
1549
1550
1-1030-85
1551
1552
1-1062-85
1553
1554
1-1601-85
1555
1556
1-1700-85
1557
1558
1-2598-85
1559
1560
1-2601-90
1561
1562
1-2700-85
1563
1564
1-3300-85
1565
1566
Methods available upon request by method number from "Methods
1567
for Determination of Radioactive Substances in Water and Fluvial
1568
Sediments," Chapter A5 in Book 5 of "Techniques of Water-
1569
Resources Investigations of the United States Geological Survey,"
1570
1997 .
1571
1572
R-1110-76
1573
1574
R-1111-76
1575
1576
R-1120-76
1577
1578
R-1140-76
1579
1580
R-1141-76
1581
1582
R-1142-76
1583
1584
R-1160-76
1585
1586
R-1171-76
1587
1588
R-1180-76
1589
1590
1591
1592
1593
1594
1595
1596
1597
1598
1599
1600
1601
1602
1603
1604
1605
1606
1607
1608
1609
1610
1611
1612
1613
1614
1615
1616
1617
1618
1619
1620
1621
1622
1623
1624
1625
1626
1627
1628
1629
1630
1631
JCAR350611-0613054r01
R-1181-76
R-1182-76
Waters Corporation, Technical Services Division, 34 Maple St ., Milford,
MA 01757 800-252-4752.
"Waters Test Method for Determination of Nitrite/Nitrate in Water
Using Single Column Ion Chromatography," Method B-101 1,
August 1987 (referred to as "Waters Method B-1011") .
c)
The Board incorporates the following federal regulations by reference
:
40 CFR 3 .2, as added at 70 Fed . Reg . 59848 (Oct . 13, 2005) (How Does
This Part Provide for Electronic Reporting?), referenced in Section
611 .105 .
40 CFR 3
.3, as added at 70 Fed
. Reg . 59848 (Oct. 13, 2005) (What
Definitions Are Applicable to This Part?), referenced in Section 611 .105.
40 CFR 3 .10, as added at 70 Fed. Reg. 59848 (Oct. 13, 2005) (What Are
the Requirements for Electronic Reporting to EPA?), referenced in Section
611 .105.
40 CFR 3 .2000, as added at 70 Fed . Reg
. 59848 (Oct . 13, 2005) (What
Are the Requirements Authorized State, Tribe, and Local Programs'
Reporting Systems Must Meet?), referenced in Section 611 .105.
Appendix B to 40 CFR 136 (2005), referenced in Sections 611 .359,
611 .609, and 611 .646.,
d)
This Part incorporates no later amendments or editions .
(Source : Amended at 30 Ill . Reg
. ,
effective )
Section 611 .105 Electronic Reporting
The filing of any document pursuant to any provision of this Part as an electronic document is
subject to this Section .
1
Scope and Applicability .
JCAR350611-0613054r01
1632
1)
The USEPA, the Board, or the Agency may allow for the filing of
1633
electronic documents . This Section does not require submission of
1634
electronic documents in lieu of paper documents . This Section sets forth
1635
the requirements for the optional electronic filing of any report or
1636
document that must be submitted to the appropriate of the following ;
1637
1638
Al
To USEPA directly under Title 40 of the Code of Federal
1639
Regulations; or
1640
1641
B)
To the Board or the Agency pursuant to any provision of 35 Ill .
1642
Adm. Code 702 through 705, 720 through 728, 730, 733, 738, or
1643
739 .
1644
1645
2j
Electronic document filing under this Section can begin only after USEPA
1646
has first done as follows :
1647
1648
A)
As to filing with USEPA, USEPA has published a notice in the
1649
Federal Register announcing that USEPA is prepared to receive
1650
documents required or permitted by the identified part or subpart
1651
of Title 40 of the Code of Federal Regulations in an electronic
1652
format; or
1653
1654
B~
As to filing with the State, USEPA has granted approval of any
1655
electronic document receiving system established by the Board or
1656
the Agency that meets the requirements of 40 CFR 3 .2000,
1657
incorporated by reference in Section 611
.102(c) .
1658
1659
3)
This Section does not apply to any of the following documents, whether or
1660
not the document is a document submitted to satisfy the requirements cited
1661
in subsection(a)(1)of this Section :
1662
1663
Al
Any document submitted via fascimile ;
1664
1665
B)
Any document submitted via magnetic or optical media, such as
1666
diskette, compact disc, digital video disc, or tape ; or
1667
1668
Q
Any data transfer between USEPA, any state, or any local
1669
government and either the Board or the Agency as part of
1670
administrative arrangements between the parties to the transfer to
1671
share data.
1672
1673
41
Upon USEPA conferring approval for the filing of any types of documents
1674
as electronic documents, as described in subsection
(a)(2)(B)of this
JCAR350611-0613054r01
1675
Section, the Agency or the Board, as appropriate, must publish a Notice of
1676
Public Information in the Illinois Register that describes the documents
1677
approved for submission as electronic documents, the electronic document
1678
receiving system approved to receive them, the acceptable formats and
1679
procedures for their submission, and the date on which the Board or the
1680
Agency will begin to receive those submissions . In the event of cessation
1681
of USEPA approval or receiving any type of document as an electronic
1682
document, the Board or the Agency must similarly cause publication of a
1683
Notice of Public Information in the Illinois Register .
1684
1685
BOARD NOTE : Subsection (a) of this Section is derived from 40 CFR 3 .1, as
1686
added at 70 Fed . Reg . 59848 (Oct . 13, 2005) .
1687
1688
b)
Definitions. For the purposes of this Section, terms will have the meaning
1689
attributed them in 40 CFR 3 .3, incorporated by reference in 35 Ill . Adm . Code
1690
611 .102(c) .
1691
1692
cj
Procedures for submission of electronic documents to USEPA . Except as
1693
provided in subsection
(a)(3)of this Section, any person who is required under
1694
Title 40 of the Code of Federal Regulations to create and submit or otherwise
1695
provide a document to USEPA may satisfy this requirement with an electronic
1696
document, in lieu of a paper document, provided the following conditions are met:
1697
1698
1)
The_person satisfies the requirements of 40 CFR 3.10, incorporated by
1699
reference in Section 611 .102(c) ; and
1700
1701
USEPA has first published a notice in the Federal Register as described in
1702
subsection(a)(2)of this Section .
1703
1704
BOARD NOTE : Subsection (c) of this Section is derived from 40 CFR 3 .2(a)
1705
and subpart B of 40 CFR 3, asadded at 70 Fed. Reg. 59848 (Oct
. 13, 2005).
1706
1707
J
Procedures for submission of electronic documents to the Board or the Agency
.
1708
1709
1)
The Board or the Agency may, but is not required to, establish procedures
1710
for the electronic submission of documents that meet the requirements of
1711
40 CFR 3 .2 and 3 .2000, incorporated by reference in Section 611
.102(c) .
1712
The Board or the Agency must establish any such procedures under the
1713
Administrative Procedure Act [5 ILCS 100/Art . 5L
1714
1715
22
The Board or the Agency may not accept electronic documents under this
1716
Section until after USEPA has approved the procedures in writing, and the
1717
Board or the Agency has published a notice of that approval in the Illinois
JCAR350611-061305401
1718
Register. Nothing in this subsection (d) limits the authority of the Board
1719
or the Agency under the Illinois Environmental Protection Act [415 ILCS
1720
51 to accept documents filed electronically .
1721
1722
BOARD NOTE : Subsection (d) of this Section is derived from 40 CFR 3 .2(b)
1723
and subpart D of 40 CFR 3, as added at 70 Fed . Reg . 59848 (Oct . 13, 2005) .
1724
1725
e_l
Effects of submission of an electronic document .
1726
1727
1l
If a person who submits a documentasan electronic document fails to
1728
comply with the requirements of this Section, that person is subject to the
1729
penalties prescribed for failure to comply with the requirement that the
1730
electronic document was intended to satisfy .
1731
1732
2)
Where a document submitted as an electronic document to satisfy a
1733
reporting requirement bears an electronic signature, the electronic
1734
signature legally binds, obligates, and makes the signer responsible to the
1735
same extentasthe signer's handwritten signature would on a paper
1736
document submitted to satisfy the same reporting requirement .
1737
1738
Proof that a particular signature device was used to create an electronic
1739
signature will suffice to establish that the individual uniquely entitled to
1740
use the device did so with the intent to sign the electronic document and
1741
give it effect.
1742
1743
4)
Nothing in this Section limits the use of electronic documents or
1744
information derived from electronic documents as evidence in
1745
enforcement or other proceedings.
1746
1747
BOARD NOTE : Subsection (e) of this Section is derived from 40 CFR 3
.4 and
1748
3.2000(c), as added at 70 Fed . Reg. 59848 (Oct . 13, 2005) .
1749
1750
f)
Public document subject to State laws
. Any electronic document filed with the
1751
Board is a public document. The document, its filing, its retention by the Board,
1752
and its availability for public inspection and copying are subject to various State
1753
laws, including, but not limited to, the following :
1754
1755
11
The Administrative Procedure Act [5 ILCS 1001
;
1756
1757
2)
The Freedom of Information Act [5 ILCS 140] ;
1758
1759
The State Records Act [5 ILCS 1601
;
1760
JCAR350611-061305401
1761
4)
The Electronic Commerce Security Act [5 ILCS 1751
;
1762
1763
5)
The Environmental Protection Act [415 ILCS 5]
;
1764
1765
)
Regulations relating to public access to Board records (2 Ill. Adm . Code
1766
2175), and
1767
1768
7)
Board procedural rules relating to protection of trade secrets and
1769
confidential information (35 III . Adm. Code 130) .
1770
1771
g)
Nothing in this Section or in any provisions adopted pursuant to subsection (c)(1)
1772
of this Section will create any right or privilege to submit any document as an
1773
electronic document .
1774
1775
BOARD NOTE : Subsection (g) of this Section is derived from 40 CFR 3 .2(c),as
1776
added at 70 Fed . Reg . 59848 (Oct . 13, 2005) .
1777
1778 BOARD NOTE
: Derived from 40 CFR 3, as added, and 40 CFR 142 .10(g) (2005), asamended
1779
at 70 Fed. Reg . 59848 (Oct . 13, 2005) .
1780
1781
(Source : Added at 30111 . Reg. , effective )
1782
1783
Section 611.111
Relief Equivalent to SDWA Section 1415(a) Variances
1784
1785
This Section is intended to describe how the Board grants State relief equivalent to that available
1786
from USEPA under section 1415(a)(1)(A) and (a)(1)(B) of the SDWA (42 USC 300g-4(a)(1)(A)
1787 and (a)(1)(B)). SDWA section 1415 variances do not require ultimate compliance within five
1788
years in every situation . Variances under Sections 35-37 of the Act [415 ILCS 5/35-37] do
1789
require compliance within five years in every case . Consequently, a PWS may have the option
1790
of seeking State regulatory relief equivalent to a SDWA section 1415 variance through one of
1791
three procedural mechanisms: a variance under Sections 35-37 of the Act [415 ILCS 5/35-37]
1792
and Subpart B of 35 Ill. Adm
. Code 104; a site-specific rule under Sections 27-28 of the Act [415
1793
ILCS 5/27-28] and 35 Ill . Adm. Code 102; or an adjusted standard under Section 28
.1 of the Act
1794
[415 ILCS 5/28
.1] and Subpart D of 35 III . Adm. Code 104 .
1795
1796
a)
The Board will grant a PWS a variance, a site-specific rule, or an adjusted
1797
standard from an MCL or a treatment technique pursuant to this Section .
1798
1799
1)
The PWS must file a petition pursuant to 35 Ill . Adm. Code 102 or 104,
1800
as applicable .
1801
1802
2)
If a State requirement does not have a federal counterpart, the Board may
1803
grant relief from the State requirements without following this Section
.
JCAR350611-0613054r01
1804
1805
b)
Relief from an MCL .
1806
1807
1)
As part of the justification for relief from an MCL under this Section, the
1808
PWS must demonstrate the following:
1809
1810
A)
Because of characteristics of the raw water sources and alternative
1811
sources that are reasonably available to the system, the PWS
1812
cannot meet the MCL
; and
1813
1814
B)
The PWS will install or has installed the best available technology
1815 (BAT) (as identified in Subpart F of this Part), treatment technique,
1816
or other means that the Agency finds available
. BAT may vary
1817
depending on the following :
1818
1819
i)
The number of persons served by the system
;
1820
1821
ii)
Physical conditions related to engineering feasibility
; and
1822
1823
iii)
Costs of compliance ; and
1824
1825
C)
The variance will not result in an unreasonable risk to health
.
1826
1827
2)
In any order granting relief under this subsection, the Board will prescribe
1828
a schedule for the following
:
1829
1830
A)
Compliance, including increments of progress, by the PWS, with
1831
each MCL with respect to which the relief was granted
; and
1832
1833
B)
Implementation by the PWS of each additional control measure for
1834
each MCL with respect to which the relief is granted, during the
1835
period ending on the date compliance with such requirement is
1836
required.
1837
1838
3)
Schedule of compliance for relief from an MCL
.
1839
1840
A)
A schedule of compliance will require compliance with each MCL
1841
with respect to which the relief was granted as expeditiously as
1842
practicable .
1843
1844
B)
If the Board prescribes a schedule requiring compliance with an
1845
MCL for which the relief is granted later than five years from the
1846
date of issuance of the relief, the Board will do the following
:
1847
1848
1849
1850
1851
1852
1853
1854
1855
1856
1857
1858
c)
Relief from a treatment technique requirement .
1859
1860
1861
1862
1863
1864
1865
1866
1867
1868
d)
1869
1870
1871
e)
1872
1873
1874
1875
1876
1877
1878
1879
1880
1881
1882
1883
1884
1885
1886
f)
1887
1888
1889
JCAR350611-0613054r01
i)
Document its rationale for the extended compliance
schedule ;
ii)
Discuss the rationale for the extended compliance schedule
in the required public notice and opportunity for public
hearing; and
iii)
Provide the shortest practicable time schedule feasible
under the circumstances .
1)
As part of the justification for relief from a treatment technique
requirement under this Section, the PWS must demonstrate that the
treatment technique is not necessary to protect the health of persons served
because of the nature of the raw water source .
2)
The Board may prescribe monitoring and other requirements as a
condition for relief from a treatment technique requirement .
The Board will hold at least one public hearing
. In addition the Board will accept
comments as appropriate pursuant to 35 III . Adm. Code 102 orl04 .
The Board will not grant relief from any of the following :
1)
From the MCL for total coliforms . However, the Board may grant a
variance from the total coliform MCL of Section 611 .325 for PWSs that
prove that the violation of the total coliform MCL is due to persistent
growth of total coliform in the distribution system, rather than from fecal
or pathogenic contamination, from a treatment lapse or deficiency, or from
a problem in the operation or maintenance of the distribution system
.
2)
From any of the treatment technique requirements of Subpart B of this
Part
.
3)
From the residual disinfectant concentration (RDC) requirements of
Sections 611 .241(c) and 611
.242(b)
.
The Agency must promptly send USEPA the opinion and order of the Board
granting relief pursuant to this Section
. The Board may reconsider and modify a
grant of relief, or relief conditions, if USEPA notifies the Board of a finding
pursuant to section 1415 of the SDWA (42 USC 300g-4)
.
JCAR350611-0613054r01
1890
1891
g)
In addition to the requirements of this Section, the provisions of Section 611 .130
1892
or 611 .131 may apply to relief granted pursuant to this Section .
1893
1894
BOARD NOTE: Derived from 40 CFR 141 .4 (2005)(2002), from section
1895
1415(a)(1)(A) and (a)(1)(B) of the SDWA and from the "Guidance Manual for
1896
Compliance with the Filtration and Disinfection Requirements for Public Water
1897
Systems using Surface Water Sources", incorporated by reference in Section
1898
611 .102. USEPA has reserved the discretion to review and modify or nullify
1899
Board determinations made pursuant to this Section at 40 CFR 142 .23
1900
(200,(2002).
1901
1902
(Source: Amended at 30 111 . Reg. , effective )
1903
1904
SUBPART B : FILTRATION AND DISINFECTION
1905
1906 Section 611 .212 Groundwater under Direct Influence of Surface Water
1907
1908 The Agency shall, pursuant to Section 611 .201, require all CWSs to demonstrate whether they
1909 are using "groundwater under the direct influence of surface water."
: The Agency must
1910 determine with information provided by the supplier whether a PWS uses "groundwater under
1911
the direct influence of surface water" on an individual basis
. The Agency must determine that a
1912
groundwater source is under the direct influence of surface water based upon the following :
1913
1914
a)
Physical characteristics of the source : whether the source is obviously a surface
1915
water source, such as a lake or stream . Other sources that may be subject to
1916
influence from surface waters include : springs, infiltration galleries, wells, or
1917
other collectors in subsurface aquifers .
1918
1919
b)
Well construction characteristics and geology with field evaluation
.
1920
1921
1)
The Agency may use the wellhead protection program's requirements,
1922
which include delineation of wellhead protection areas, assessment of
1923
sources of contamination and implementation of management control
1924
systems, to determine if the wellhead is under the influence of surface
1925
water
.
1926
1927
2)
Wells less than or equal to 50 feet in depth are likely to be under the
1928
influence of surface water .
1929
1930
3)
Wells greater than 50 feet in depth are likely to be under the influence of
1931
surface water, unless they include the following :
1932
JCAR350611-0613054r01
1933
A)
A surface sanitary seal using bentonite clay, concrete, or similar
1934
material
;;
1935
1936
B)
A well casing that penetrates consolidated (slowly permeable)
1937
material ; and
1938
1939
C)
A well casing that is only perforated or screened below
1940
consolidated (slowly permeable) material .
1941
1942
4)
A source that is less than 200 feet from any surface water is likely to be
1943
under the influence of surface water.
1944
1945
c)
Any structural modifications to prevent the direct influence of surface water and
1946
eliminate the potential for Giardia lamblia cyst contamination .
1947
1948
d)
Source water quality records. The following are indicative that a source is under
1949
the influence of surface water
:
1950
1951
1)
A record of total coliform or fecal coliform contamination in untreated
1952
samples collected over the past three years ;
1953
1954
2)
A history of turbidity problems associated with the source ; or
1955
1956
3)
A history of known or suspected outbreaks of Giardia lamblia,
1957
Cryptosporidium or other pathogenic organisms associated with surface
1958
water that has been attributed to that source .
1959
1960
e)
Significant and relatively rapid shifts in water characteristics such as turbidity,
1961
temperature, conductivity, or pH.
1962
1963
1)
A variation in turbidity of 0 .5 NTU or more over one year is indicative of
1964
surface influence.
1965
1966
2)
A variation in temperature of nine9 Fahrenheit degrees or more over one
1967
year is indicative of surface influence .
1968
1969
f)
Significant and relatively rapid shifts in water characteristics such as turbidity,
1970
temperature, conductivity, or pH that closely correlate to climatological or surface
1971
water conditions are indicative of surface water influence .
1972
1973
1)
Evidence of particulate matter associated with the surface water
; or,
1974
1975
2)
Turbidity or temperature data that correlates to that of a nearby surface
JCAR350611-061305401
1976
water source .
1977
1978
g)
Particulate analysis
: Significant occurrence of insects or other macroorganisms,
1979
algae, or large diameter pathogens such as Giardia lamblia is indicative of surface
1980
influence.
1981
1982
1)
"Large diameter" particulates are those over seven; micrometers
.
1983
1984
2)
Particulates must be measured as specified in the "Guidance Manual for
1985
Compliance with the Filtration and Disinfection Requirements for Public
1986
Water Systems using Surface Water Sources,"3
incorporated by reference
1987
in Section 611 .102 .
1988
1989
h)
The potential for contamination by small-diameter pathogens, such as bacteria or
1990
viruses, does not alone render the source "under the direct influence of surface
1991
water."-.
1992
1993
BOARD NOTE
: Derived from the definition of "groundwater under the direct influence of
1994
surface water" in 40 CFR 141
.2 2(005x2002) ; from the Preamble at 54 Fed
. Reg . 27489 (June
1995 29, 1989)
; and from the USEPA "Guidance Manual for Compliance with the Filtration and
1996
Disinfection Requirements for Public Water Systems using Surface Water Sources,"
;
1997
incorporated by reference in Section 611 .102
.
1998
1999
(Source: Amended at 30 Ill
. Reg. , effective )
2000
2001
SUBPART G
: LEAD AND COPPER
2002
2003 Section 611 .359 Analytical Methods
2004
2005
Analyses for lead, copper, pH, conductivity, calcium, alkalinity, orthophosphate, silica, and
2006
temperature must be conducted using the methods set forth in Section 611
.611(a) .
2007
2008
a)
Analyses for lead and copper performed for the purposes of compliance with this
2009
Subpart G must only be conducted by laboratories that have been certified by
2010
USEPA Or the Agency
. To obtain certification to conduct analyses for lead and
2011
copper, laboratories must do the following
:
2012
2013
1)
Analyze performance evaluation samples that include lead and copper
2014
provided by USEPA Environmental Monitoring and Support Laboratory
2015
or equivalent samples provided by the Agency
; and
2016
2017
2)
Achieve quantitative acceptance limits as follows
:
2018
JCAR350611-0613054r01
2019
A)
For lead: ±30 percent of the actual amount in the performance
2020
evaluation sample when the actual amount is greater than or equal
2021
to 0.005
mg/f (the PQL for lead is 0
.005 mg/f)
;
2022
2023
B)
For copper: ±10 percent of the actual amount in the performance
2024
evaluation sample when the actual amount is greater than or equal
2025
to 0.050 mg/f (the PQL for copper is 0 .050 mg/f) ;
2026
2027
C)
Achieve the method detection limit (MDL) for lead (0 .001 mg/f,
2028
as defined in Section 611
.350(a)) according to the procedures in 35
2029
Ill. Adm. Code 186 and appendix B to 40 CFR 136, Appendix B :
2030
"Definition and Procedure for the Determination of the Method
2031
Detection Limit -Revision 1 .11" (2005), incorporated by
2032
reference in Section 611 .102(c)(2002) . This need only be
2033
accomplished if the laboratory will be processing source water
2034
composite samples under Section 611 .358(a)(1)(C); and
2035
2036
D)
Be currently certified by USEPA or the Agency to perform
2037
analyses to the specifications described in subsection (a)(2) of this
2038
Section.
2039
2040
BOARD NOTE : Subsection (a) is derived from 40 CFR 141 .89(a) and (a)(1)
2041
2(005x2002) .
2042
2043
b)
The Agency must, by a SEP issued pursuant to Section 61 l .110, allow a supplier
2044
to use previously collected monitoring data for the purposes of monitoring under
2045
this Subpart G if the data were collected and analyzed in accordance with the
2046
requirements of this Subpart G.
2047
2048
BOARD NOTE : Subsection (b) is derived from 40 CFR 141
.89(a)(2)
2049
(2005)(2002).
2050
2051
c)
Reporting lead and copper levels .
2052
2053
1)
All lead and copper levels greater than or equal to the lead and copper
2054
PQL (Pb ?0 .005 mg/f and Cu ?0
.050 mg/f) must be reported as
2055
measured .
2056
2057
2)
All lead and copper levels measured less than the PQL and greater than
2058
the MDL (0.005 mg/f> Pb> MDL and 0.050 mg/f > Cu > MDL) must be
2059
either reported as measured or as one-half the PQL set forth in subsection
2060
(a) of this Section (i.e., reported as 0.0025
mg/f for lead or 0 .025 mg/f for
2061
copper).
JCAR350611-0613054r01
2062
2063
3)
All lead and copper levels below the lead and copper MDL (MDL > Pb)
2064
must be reported as zero .
2065
2066 BOARD NOTE: Subsection (c) is derived from 40 CFR 141
.89(a)(3) and (a)(4) (2005)(2002).
2067
2068
(Source : Amended at 30 Ill
. Reg . , effective )
2069
2070
SUBPART I
: DISINFECTANT RESIDUALS, DISINFECTION BYPRODUCTS,
2071
AND DISINFECTION BYPRODUCT PRECURSORS
2072
2073 Section 611 .380 General Requirements
2074
2075
a)
The requirements of this Subpart I constitute NPDWRs
.
2076
2077
1)
The regulations in this Subpart I establish standards under which a CWS
2078
supplier or an NTNCWS supplier that adds a chemical disinfectant to the
2079
water in any part of the drinking water treatment process orivhieh
2080
must modify its
2081
practices to meet MCLs and MRDLs in Sections 611 .312 and 611 .313,
2082
respectively, and must meet the treatment technique requirements for DBP
2083
precursors in Section 611 .385 .
2084
2085
2086
2087
2088
2089
2090
3)
The Board has established MCLs for TTHM and HAAS and treatment
2091
technique requirements for DBP precursors to limit the levels of known
2092
and unknown DBPs that may have adverse health effects . These DBPs
2093
may include chloroform, bromodichloromethane, dibromochloromethane,
2094
bromoform, dichloroacetic acid, and trichloroacetic acid.
2095
2096
b)
Compliance dates
.
2097
2098
1)
CWSs and NTNCWSs . Unless otherwise noted, a supplier must comply
2099
with the requirements of this Subpart I as follows : A Subpart B system
2100
supplier serving 10,000 or more persons must comply with this Subpart I
2101
beginning January 1, 2002 . A Subpart B system supplier serving fewer
2102
than 10,000 persons or a supplier using only groundwater not under the
2103
direct influence of surface water must comply with this Subpart I
2104
beginning January 1, 2004 .
The regulations in this Subpart I establish standards under which a
transient non-CWS supplier that uses chlorine dioxide as a disinfectant or
oxidant must modify its practices to meet the MRDL for chlorine dioxide
in Section 611 .313.
JCAR350611-0613054r01
2105
2106
2)
Transient non-CWSs . A Subpart B system supplier serving 10,000 or
2107
more persons and using chlorine dioxide as a disinfectant or oxidant must
2108
comply with any requirements for chlorine dioxide in this Subpart I
2109
beginning January 1, 2002 . A Subpart B system supplier serving fewer
2110
than 10,000 persons and using chlorine dioxide as a disinfectant or oxidant
2111
or a supplier using only groundwater not under the direct influence of
2112
surface water and using chlorine dioxide as a disinfectant or oxidant must
2113
comply with any requirements for chlorine dioxide in this Subpart I
2114
beginning January 1, 2004
.
2115
2116
c)
Each CWS or NTNCWS supplier regulated under subsection (a) of this Section
2117
must be operated by qualified personnel who meet the requirements specified in
2118
35 111. Adm. Code 680 .
2119
2120
d)
Control of disinfectant residuals . Notwithstanding the MRDLs in Section
2121
611 .313, a supplier may increase residual disinfectant levels in the distribution
2122
system of chlorine or chloramines (but not chlorine dioxide) to a level and for a
2123
time necessary to protect public health, to address specific microbiological
2124
contamination problems caused by circumstances such as, but not limited to,
2125
distribution line breaks, storm run-off events, source water contamination events,
2126
or cross-connection events .
2127
2128
BOARD NOTE : Derived from 40 CFR 141 .130 2(002002).
2129
2130
(Source
: Amended at 30 Ill
. Reg. , effective )
2131
2132
SUBPART N : INORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
2133
2134 Section 611 .609 Determining Compliance
2135
2136
Compliance with the MCLs of Section 611 .300 or 611 .301 (as appropriate) must be determined
2137
based on the analytical results obtained at each sampling point .
2138
2139
a)
For suppliers that monitor at a frequency greater than annual, compliance with the
2140
MCLs for antimony, arsenic (effective January 22, 2004), asbestos, barium,
2141
beryllium, cadmium, chromium, cyanide, fluoride, mercury, nickel, selenium, or
2142
thallium is determined by a running annual average at each sampling point
.
2143
Effective January 22, 2004, if a system fails to collect the required number of
2144
samples, compliance (average concentration) will be based on the total number of
2145
samples collected .
2146
2147
1)
If the average at any sampling point is greater than the MCL, then the
JCAR35061 l-0613054r01
2148
supplier is out of compliance .
2149
2150
2)
If any one sample would cause the annual average to be exceeded, then the
2151
supplier is out of compliance immediately
.
2152
2153
3)
Any sample below the method detection limit must be calculated at zero
2154
for the purpose of determining the annual average .
2155
2156
BOARD NOTE: The "method detection limit" is different from the
2157
"detection limit," as set forth in Section 611
.600
. The "method detection
2158
limit" is the level of contaminant that can be determined by a particular
2159
method with a 95 percent degree of confidence, as determined by the
2160
method outlined in appendix B to 40 CFR 136, Appendix B, incorporated
2161
by reference at Section 611 .102.
2162
2163
b)
For suppliers that monitor annually or less frequently, compliance with the MCLs
2164
for antimony, arsenic (effective January 22, 2004), asbestos, barium, beryllium,
2165
cadmium, chromium, cyanide, fluoride, mercury, nickel, selenium, or thallium is
2166
determined by the level of the contaminant at any sampling point . If confirmation
2167
samples are required by the Agency, the determination of compliance will be
2168
based on the average of the annual average of the initial MCL exceedence and any
2169
Agency-required confirmation samples . Effective January 22, 2004, if a supplier
2170
fails to collect the required number of samples, compliance (average
2171
concentration) will be based on the total number of samples collected
.
2172
2173
c)
Compliance with the MCLs for nitrate and nitrite is determined based on one
2174
sample if the levels of these contaminants are below the MCLs . If the levels of
2175
nitrate or nitrite in the initial sample exceed the MCLs, Section 611 .606 requires
2176
confirmation sampling, and compliance is determined based on the average of the
2177
initial and confirmation samples .
2178
2179
d)
Arsenic sampling results must be reported to the nearest 0 .001 mg/P.
2180
2181 BOARD NOTE: Derived from 40 CFR 141 .23(1) (2005)(2002).
2182
2183
(Source: Amended at 30111 . Reg. , effective )
2184
2185
SUBPART 0
: ORGANIC MONITORING AND ANALYTICAL REQUIREMENTS
2186
2187
Section 611 .646 Phase 1, Phase II, and Phase V Volatile Organic Contaminants
2188
2189 Monitoring of the Phase I, Phase II, and Phase V VOCs for the purpose of determining
2190 compliance with the MCL must be conducted as follows:
JCAR350611-061305401
2191
2192
a)
Definitions . As used in this Section the following have the given meanings :
2193
2194
"Detect" and "detection" mean that the contaminant of interest is present at
2195
a level greater than or equal to the "detection limit ."
2196
2197
"Detection limit" means 0.0005 mg/2 .
2198
2199
BOARD NOTE: Derived from 40 CFR 141 .24(f)(7), (f)(11), (f)(14)(i),
2200
and (f)(20) 2(005)(2003) . This is a "trigger level" for Phase I, Phase II,
2201
and Phase V VOCs inasmuch as it prompts further action . The use of the
2202
term "detect" in this Section is not intended to include any analytical
2203
capability of quantifying lower levels of any contaminant, or the "method
2204
detection limit ." Note, however, that certain language at the end of federal
2205
paragraph (f)(20)
is capable of meaning that the "method detection limit"
2206
is used to derive the "detection limit ." The Board has chosen to disregard
2207
that language at the end of paragraph (f)(20)
in favor of the more direct
2208
language of paragraphs (f)(7) and
(f)(11)
.
2209
2210
"Method detection limit," as used in subsections (q) and (t) of this Section
2211
means the minimum concentration of a substance that can be measured
2212
and reported with 99 percent confidence that the analyte concentration is
2213
greater than zero and is determined from analysis of a sample in a given
2214
matrix containing the analyte.
2215
2216
BOARD NOTE : Derived from appendix B to 40 CFR 136, Appendix B
2217
(2005)(2003). The method detection limit is determined by the procedure
2218
set forth in appendix B to 40 CFR 136,
incorporated by reference in
2219
Section 611 .102(c) Appendix B. See subsection (t) of this Section .
2220
2221
b)
Required sampling
. Each supplier must take a minimum of one sample at each
2222
sampling point at the times required in subsection (u) of this Section .
2223
2224
c)
Sampling points .
2225
2226
1)
Sampling points for a GWS
. Unless otherwise provided by a SEP granted
2227
by the Agency pursuant to Section 611
.110, a GWS supplier must take at
2228
least one sample from each of the following points : each entry point that
2229
is representative of each well after treatment .
2230
2231
2)
Sampling points for an SWS or mixed system supplier
. Unless otherwise
2232
provided by a SEP granted by the Agency pursuant to Section 611
.110, an
2233
SWS or mixed system supplier must sample from each of the following
JCAR350611-0613054r0l
2234
points:
2235
2236
A)
2237
Each entry point after treatment
; or
2238
B)
2239
Points in the distribution system that are representative of each
source.
2240
2241
3)
2242
The supplier must take each sample at the same sampling point unless the
2243
Agency has granted a SEP pursuant to Section 611
.110 that designates
2244
another location as more representative of each source, treatment plant, or
2245
within the distribution system
.
2246
4)
2247
If a system draws water from more than one source, and the sources are
2248
combined before distribution, the supplier must sample at an entry point
2249
during periods of normal operating conditions when water is
2250
representative of all sources being used .
2251
2252
BOARD NOTE
: Subsections (b) and (c) of this Section derived from 40 CFR
141 .24(f)(1) through
(f)(3) zoos
2253
2254
d)
2255
Each CWS and NTNCWS supplier must take four consecutive quarterly samples
for each of the Phase I VOCs, excluding vinyl chloride, and Phase II VOCs
2256
during each compliance period, beginning in the compliance period starting in the
2257
initial compliance period .
2258
2259
e)
2260
Reduction to annual monitoring frequency
. If the initial monitoring for the Phase
2261
I, Phase II, and Phase V VOCs, as allowed in subsection
(r)(1) of this Section,
2262
was completed by December 31, 1992, and the supplier did not detect any of the
2263
Phase I VOCs, including vinyl chloride
; Phase II VOCs ; or Phase V VOCs, then
2264
the supplier must take one sample annually beginning in the initial compliance
period .
2265
2266
f)
2267
GWS reduction to triennial monitoring frequency
. After a minimum of three
years of annual sampling, GWS suppliers that have not previously detected any of
2268
2269
the Phase I VOCs, including vinyl chloride ; Phase II VOCs
; or Phase V VOCs
2270
must take one sample during each three-year compliance period
.
2271
g)
A CWS or NTNCWS supplier that has completed the initial round of monitoring
2272
required by subsection (d) of this Section and which did not detect any of the
2273
2274
Phase I VOCs, including vinyl chloride
; Phase II VOCs ; and Phase V VOCs may
2275
apply to the Agency for a SEP pursuant to Section 611
.110 that releases it from
2276
the requirements of subsection (e) or (1) of this Section
. A supplier that serves
fewer than 3300 service connections may apply to the Agency for a SEP that
JCAR350611-061305401
2277
releases it from the requirements of subsection (d) of this Section as to 1,2,4-
2278
trichlorobenzene .
2279
2280
BOARD NOTE : Derived from 40 CFR 141
.24(f)(7) and (f)(10) (2005)(2003),
2281
and the discussion at 57 Fed . Reg. 31825 (July 17, 1992). Provisions concerning
2282
the term of the waiver appear in subsections (i) and (j) of this Section . The
2283
definition of "detect," parenthetically added to the federal counterpart paragraph,
2284
is in subsection (a) of this Section
.
2285
2286
h)
Vulnerability assessment . The Agency must consider the factors of Section
2287
611 .110(e) in granting a SEP from the requirements of subsection (d), (e), or (f)
2288
of this Section sought pursuant to subsection (g) of this Section .
2289
2290
i)
A SEP issued to a GWS pursuant to subsection (g) of this Section is for a
2291
maximum of six years, except that a SEP as to the subsection (d) of this Section
2292
monitoring for 1,2,4-trichlorobenzene must apply only to the initial round of
2293
monitoring. As a condition of a SEP, except as to a SEP from the initial round
2294
of subsection (d) of this Section monitoring for 1,2,4-trichlorobenzene, the
2295
supplier shall, within 30 months after the beginning of the period for which the
2296
waiver was issued, reconfirm its vulnerability assessment required by subsection
2297
(h) of this Section and submitted pursuant to subsection (g) of this Section, by
2298
taking one sample at each sampling point and reapplying for a SEP pursuant to
2299
subsection (g) of this Section . Based on this application, the Agency must do
2300
either of the following :
2301
2302
1)
If it determines that the PWS meets the standard of Section 611
.610(e),
2303
issue a SEP that reconfirms the prior SEP for the remaining three-year
2304
compliance period of the six-year maximum term ; or
2305
2306
2)
Issue a new SEP requiring the supplier to sample annually .
2307
2308
BOARD NOTE : Subsection (i) of this Section does not apply to an SWS or
2309
mixed system supplier.
2310
2311
j)
Special considerations for a SEP for an SWS or mixed-system supplier .
2312
2313
1)
The Agency must determine that an SWS is not vulnerable before issuing
2314
a SEP pursuant to Section 611 .110 to an SWS supplier
. A SEP issued to
2315
an SWS or mixed system supplier pursuant to subsection (g) of this
2316
Section is for a maximum of one compliance period ; and
2317
2318
2)
The Agency may require, as a condition to a SEP issued to an SWS or
2319
mixed supplier, that the supplier take such samples for Phase I, Phase II,
JCAR350611-0613054r01
2320
and Phase V VOCs at such a frequency as the Agency determines are
2321
necessary, based on the vulnerability assessment .
2322
2323
BOARD NOTE
: There is a great degree of similarity between 40 CFR
2324
141 .24(f)(7)
200()5
(2003, the provision applicable to GWSs, and 40 CFR
2325
141 .24(f)(10) (2005)(2003), the provision for SWSs. The Board has consolidated
2326
the common requirements of both paragraphs into subsection (g) of this Section .
2327
Subsection (j) of this Section represents the elements unique to an SWSs or mixed
2328
system, and subsection (i) of this Section relates to a GWS supplier
. Although 40
2329
CFR 141.24(f)(7) and (f)(10) are silent as to a mixed system supplier, the Board
2330
has included a mixed system supplier with an SWS supplier because this best
2331
follows the federal scheme for all other contaminants .
2332
2333
k)
If one of the Phase I VOCs, excluding vinyl chloride
; a Phase II VOC; or a Phase
2334
V VOC is detected in any sample, then the following must occur :
2335
2336
1)
The supplier must monitor quarterly for that contaminant at each sampling
2337
point that resulted in a detection .
2338
2339
2)
Annual monitoring
.
2340
2341
A)
The Agency must grant a SEP pursuant to Section 611
.110 that
2342
allows a supplier to reduce the monitoring frequency to annual at a
2343
sampling point if it determines that the sampling point is reliably
2344
and consistently below the MCL.
2345
2346
B)
A request for a SEP must include the following minimal
2347
information
:
2348
2349
i)
For a GWS, two quarterly samples .
2350
2351
ii)
For an SWS or mixed system supplier, four quarterly
2352
samples.
2353
2354
C)
In issuing a SEP, the Agency must specify the level of the
2355
contaminant upon which the "reliably and consistently"
2356
determination was based . Any SEP that allows less frequent
2357
monitoring based on an Agency "reliably and consistently"
2358
determination must include a condition requiring the supplier to
2359
resume quarterly monitoring pursuant to subsection (k)(1) of this
2360
Section if it violates the MCL specified by Section 611 .311 .
2361
2362
3)
Suppliers that monitor annually must monitor during the quarters that
JCAR350611-0613054r01
2363
previously yielded the highest analytical result .
2364
2365
4)
Suppliers that do not detect a contaminant at a sampling point in three
2366
consecutive annual samples may apply to the Agency for a SEP pursuant
2367
to Section 611 .110 that allows it to discontinue monitoring for that
2368
contaminant at that point, as specified in subsection (g) of this Section .
2369
2370
5)
A GWS supplier that has detected one or more of the two-carbon
2371
contaminants listed in subsection (k)(5)(A) of this Section must monitor
2372
quarterly for vinyl chloride as described in subsection (k)(5)(B) of this
2373
Section, subject to the limitation of subsection (k)(5)(C) of this Section .
2374
2375
A)
"Two-carbon contaminants" (Phase I or II VOC) are the following :
2376
2377
1,2-Dichloroethane (Phase I)
2378
2379
1,1-Dichloroethylene (Phase I)
2380
2381
cis-1,2-Dichloroethylene (Phase II)
2382
2383
trans-1,2-Dichloroethylene (Phase II)
2384
2385
Tetrachloroethylene (Phase II)
2386
2387
1,1,1-Trichloroethylene (Phase I)
2388
2389
Trichloroethylene (Phase I)
2390
2391
B)
The supplier must sample quarterly for vinyl chloride at each
2392
sampling point at which it detected one or more of the two-carbon
2393
contaminants listed in subsection (k)(5)(A) of this Section .
2394
2395
C)
The Agency must grant a SEP pursuant to Section 611
.110 that
2396
allows the supplier to reduce the monitoring frequency for vinyl
2397
chloride at any sampling point to once in each three-year
2398
compliance period if it determines that the supplier has not
2399
detected vinyl chloride in the first sample required by subsection
2400
(k)(5)(B) of this Section .
2401
2402
1)
Quarterly monitoring following MCL violations
.
2403
2404
1)
Suppliers that violate an MCL for one of the Phase I VOCs, including
2405
vinyl chloride; Phase II VOCs ; or Phase V VOCs, as determined by
JCAR350611-0613054r01
2406
subsection (o) of this Section, must monitor quarterly for that contaminant,
2407
at the sampling point where the violation occurred, beginning the next
2408
quarter after the violation
.
2409
2410
2)
Annual monitoring
.
2411
2412
A)
The Agency must grant a SEP pursuant to Section 611 .110 that
2413
allows a supplier to reduce the monitoring frequency to annually if
2414
it determines that the sampling point is reliably and consistently
2415
below the MCL .
2416
2417
B)
A request for a SEP must include the following minimal
2418
information : four quarterly samples .
2419
2420
C)
In issuing a SEP, the Agency must specify the level of the
2421
contaminant upon which the "reliably and consistently"
2422
determination was based . Any SEP that allows less frequent
2423
monitoring based on an Agency "reliably and consistently"
2424
determination must include a condition requiring the supplier to
2425
resume quarterly monitoring pursuant to subsection (1)(1) of this
2426
Section if it violates the MCL specified by Section 611
.311 .
2427
2428
D)
The supplier must monitor during the quarters that previously
2429
yielded the highest analytical result .
2430
2431
m)
Confirmation samples . The Agency may issue a SEP pursuant to Section 610 .110
2432
to require a supplier to use a confirmation sample for results that it finds dubious
2433
for whatever reason . The Agency must state its reasons for issuing the SEP if the
2434
SEP is Agency-initiated.
2435
2436
1)
If a supplier detects any of the Phase I, Phase II, or Phase V VOCs in a
2437
sample, the supplier must take a confirmation sample as soon as possible,
2438
but no later than 14 days after the supplier receives notice of the detection
.
2439
2440
2)
Averaging is as specified in subsection (o) of this Section .
2441
2442
3)
The Agency must delete the original or confirmation sample if it
2443
determines that a sampling error occurred, in which case the confirmation
2444
sample will replace the original or confirmation sample .
2445
2446
n)
This subsection (n) corresponds with 40 CFR 141 .24(£)(14), an optional USEPA
2447
provision relating to compositing of samples that USEPA does not require for
2448
state programs
. This statement maintains structural consistency with USEPA
JCAR350611-0613054r01
2449
rules .
2450
2451
o)
2452
Compliance with the MCLs for the Phase I, Phase II, and Phase V VOCs must be
2453
determined based on the analytical results obtained at each sampling point
.
Effective January 22, 2004, if one sampling point is in violation of an MCL, the
2454
system is in violation of the MCL.
2455
2456
1)
Effective January 22, 2004, for a supplier that monitors more than once
2457
per year, compliance with the MCL is determined by a running annual
2458
average at each sampling point .
2459
2460
2)
Effective January 22, 2004, a supplier that monitors annually or less
2461
frequently whose sample result exceeds the MCL must begin quarterly
2462
sampling
. The system will not be considered in violation of the MCL until
2463
it has completed one year of quarterly sampling
.
2464
2465
3)
Effective January 22, 2004, if any sample result will cause the running
2466
annual average to exceed the MCL at any sampling point, the supplier is
2467
out of compliance with the MCL immediately .
2468
2469
4)
Effective January 22, 2004, if a supplier fails to collect the required
2470
number of samples, compliance will be based on the total number of
2471
samples collected .
2472
2473
5)
Effective January 22, 2004, if a sample result is less than the detection
2474
2475
limit, zero will be used to calculate the annual average .
2476
6)
2477
Until January 22, 2004, for a supplier that conducts monitoring at a
frequency greater than annual, compliance is determined by a running
2478
annual average of all samples taken at each sampling point .
2479
2480
A)
2481
If the annual average of any sampling point is greater than the
MCL, then the supplier is out of compliance .
2482
2483
B)
If the initial sample or a subsequent sample would cause the annual
2484
average to exceed the MCL, then the supplier is out of compliance
2485
immediately .
2486
2487
C)
Any samples below the detection limit must be deemed as zero for
2488
purposes of determining the annual average.
2489
2490
7)
Until January 22, 2004, if monitoring is conducted annually, or less
2491
frequently, the supplier is out of compliance if the level of a contaminant
JCAR350611-0613054r01
2492
at any sampling point is greater than the MCL
. Until January 22, 2004, if
2493
a confirmation sample is taken, the determination of compliance is based
2494
on the average of two samples .
2495
2496
p)
This subsection (p) corresponds with 40 CFR 141 .24(f)(16), which USEPA
2497
removed and reserved . This statement maintains structural consistency with the
2498
federal regulations .
2499
2500
q)
Analysis under this Section must only be conducted by laboratories that have
2501
received certification by USEPA or the Agency according to the following
2502
conditions:
2503
2504
1)
To receive certification to conduct analyses for the Phase I VOCs,
2505
excluding vinyl chloride
; Phase II VOCs ; and Phase V VOCs, the
2506
laboratory must do the following :
2507
2508
A)
It must analyze performance evaluation (PE) samples that include
2509
these substances provided by the Agency pursuant to 35 Ill . Adm.
2510
Code 186 .170;
2511
2512
B)
It must achieve the quantitative acceptance limits under
2513
subsections (q)(1)(C) and (q)(1)(D) of this Section for at least 80
2514
percent of the regulated organic contaminants in the PE sample ;
2515
2516
C)
It must achieve quantitative results on the analyses performed
2517
under subsection (q)(1)(A) of this Section that are within t 20
2518
percent of the actual amount of the substances in the PE sample
2519
when the actual amount is greater than or equal to 0
.010 mg/f ;
2520
2521
D)
It must achieve quantitative results on the analyses performed
2522
under subsection (q)(1)(A) of this Section that are within ± 40
2523
percent of the actual amount of the substances in the PE sample
2524
when the actual amount is less than 0 .010 mg/f ; and
2525
2526
E)
It must achieve a method detection limit of 0 .0005 mg/f, according
2527
to the procedures in appendix B to 40 CFR 136, appendix B,
2528
incorporated by reference in Section 611 .102.
2529
2530
2)
To receive certification to conduct analyses for vinyl chloride the
2531
laboratory must do the following :
2532
2533
A)
It must analyze PE samples provided by the Agency pursuant to 35
2534
Ill . Adm. Code 186 .170;
JCAR350611-0613054r01
2535
2536
B)
It must achieve quantitative results on the analyses performed
2537
2538
under subsection
(q)(2)(A)
of this Section that are within ± 40
2539
percent of the actual amount of vinyl chloride in the PE sample
;
2540
C)
2541
It must achieve a method detection limit of 0
.0005 mg/f, according
2542
to the procedures in
appendix B to 40 CFR 136,
appendix B,
2543
incorporated by reference in Section 611 .102; and
2544
D)
2545
It must obtain certification pursuant to subsection
(q)(1) of this
2546
Section for Phase I VOCs, excluding vinyl chloride ; Phase II
VOCs
; and Phase V VOCs .
2547
2548
r)
2549
This subsection (r) corresponds with 40 CFR 141
.24(1)(1 8), an obsolete provision
2550
that relates to the initial compliance period from 1993 through 1995
. This
statement maintains consistency with the federal regulations .
2551
2552
2553
s)
2554
The Agency shall, by a SEP issued pursuant to Section 611
.110, increase the
number of sampling points or the frequency of monitoring if it determines that it
2555
is necessary to detect variations within the PWS .
2556
2557
t)
Each laboratory certified for the analysis of Phase I, Phase II, or Phase V VOCs
2558
pursuant to subsection (q)(1) or (q)(2)
of this Section shall do the following :
2559
2560
1)
2561
Determine the method detection limit (MDL), as defined in
appendix B to
2562
40 CFR
136, Appendix B, incorporated by reference in Section 611
.102,
at which it is capable of detecting the Phase I, Phase II, and Phase V
2563
VOCs; and,
2564
2565
2)
Achieve an MDL for each Phase I, Phase II, and Phase V VOC that is less
2566
than or equal to 0 .0005 mg/f
.
2567
2568
u)
Each supplier must monitor, within each compliance period, at the time
2569
2570
designated by the Agency by SEP pursuant to Section 611
.110.
2571
v)
A new system supplier or a supplier that uses a new source of water that begins
2572
operation after January 22, 2004 must demonstrate compliance with the MCL
2573
within a period of time specified by a permit issued by the Agency . The supplier
2574
must also comply with the initial sampling frequencies specified by the Agency to
2575
ensure the supplier can demonstrate compliance with the MCL
. Routine and
2576
increased monitoring frequencies must be conducted in accordance with the
2577
requirements in this Section
.
2578
2579 BOARD NOTE : Derived from 40 CFR 141 .24(0 (2005)(2003) .
2580
2581
(Source: Amended at 30 Ill . Reg. , effective )
JCAR350611-0613054r01
JCAR350611-0613054r01
2582 Section 611 .APPENDIX D Defined Substrate Method for the Simultaneous Detection of
2583 Total Coliforms and Escherichia Coli from Drinking Water
2584
2585 Autoanalysis Colilert Presence-Absence (AC P-A) Method .
2586
2587 The AC P-A test format must be either a 100-mt 10-tube most probable number test (one tube
2588 positive denoting the presence of total coliforms in that sample) or a single vessel containing
2589 sufficient reagent to receive 100 mQ of sample . The reagent is available from Access Medical
2590 Systems, Branford Connecticut
.
2591
2592 The AC P-A method must be performed as follows :
2593
2594
1 .
For the 10-tube method, add 10 mf of water sample to each test tube
. For the
2595
single-vessel method, add 100 mf of water sample to the vessel.
2596
2597
2.
Dissolve the reagent powder by agitation . (This should produce a colorless
2598
solution .)
2599
2600
3 .
Incubate the test tubes or vessel at 35° C for 24 hours .
2601
2602
4 .
Development of yellow during incubation denotes the presence of total coliforms
2603
in either the test tube or the vessel .
2604
2605
5 .
Expose each positive (yellow) test tube or vessel to a fluorescent (366 nm) light
2606
source . Fluorescence specifically demonstrates the presence of Escherichia coli .
2607
2608
BOARD NOTE : Derived from S. Edberg, M . Allen & D . Smith, "National Field
2609
Evaluation of a Defined Substrate Method for the Simultaneous Detection of
2610
Total Coliforms and Escherichia coli from Drinking Water
: Comparison with
2611
Presence-Absence Techniques: % Applied and Environmental Microbiology, vol .
2612
55, pp. 1003-1008, as incorporated by reference at 40 CFR 141 .21(f)(6)(iii)
2613
2005 2002). This method is for use in conjunction with the requirements of
2614
Section 611 .526.
2615
2616
(Source
: Amended at 30 Ill
. Reg,
,
effective
)
