ILLINOIS POLLUTION CONTROL BOARD
December 17, 1998
IN THE MATTER OF:
)
)
RCRA UPDATE, USEPA REGULATIONS
)
R98-21
(July 1, 1997, through December 31, 1997)
)
(Identical-in-Substance
)
Rulemaking - Land)
________________________________________
IN THE MATTER OF:
)
)
RCRA UPDATE, USEPA REGULATIONS
)
R99-2
(January 1, 1998, through June 30, 1998)
)
(Identical-in-Substance
)
Rulemaking - Land)
________________________________________
IN THE MATTER OF:
)
)
UIC UPDATE, USEPA REGULATIONS
)
R99-7
(January 1, 1998, through June 30, 1998)
)
(Identical-in-Substance
)
Rulemaking - Land)
Adopted Rule. Final Order.
ORDER OF THE BOARD (by K.M. Hennessey):
Pursuant to Sections 13(c) and 22.4(a) of the Environmental Protection Act (Act) (415
ILCS 5/13(c) & 22.4(a) (1996)), the Board adopts amendments to the Illinois regulations that
are “identical-in-substance” to hazardous waste regulations adopted by the United States
Environmental Protection Agency (USEPA) to implement Subtitle C of the federal Resource
Conservation and Recovery Act of 1976 (RCRA Subtitle C), 42 U.S.C. §§ 6921
et seq
.
(1996). The Board further adopts amendments to the Illinois regulations that are “identical-in-
substance” to underground injection control (UIC) regulations adopted by the USEPA to
implement provisions of the Safe Drinking Water Act (SDWA), 42 U.S.C. § 300h
et seq
.
(1996). The nominal timeframe of this consolidated docket includes federal RCRA Subtitle C
amendments adopted by USEPA in the periods July 1, 1997, through December 31, 1997, and
January 1, 1998, through June 30, 1998. The nominal timeframe also includes federal UIC
amendments adopted in the period January 1, 1998, through June 30, 1998.
Section 22.4(a) provides for quick adoption of regulations that are “identical-in-
substance” to federal regulations adopted by USEPA to implement Sections 3001 through 3005
of RCRA, 42 U.S.C. §§ 6921-6925 (1996)) and that Title VII of the Act and Section 5 of the
Administrative Procedure Act (APA) (5 ILCS 100/5-35 & 5-40 (1996)) shall not apply.
Section 13(c) similarly provides for quick adoption of regulations that are “identical-in-
2
substance” to federal regulations adopted by USEPA to implement Section 1421 of SDWA, 42
U.S.C. § 300h (1996)). Because this consolidated rulemaking is not subject to Section 5 of
the APA, it is not subject to first-notice or to second-notice review by the Joint Committee on
Administrative Rules (JCAR). The federal RCRA Subtitle C regulations are found at 40
C.F.R. 260 through 268, 270 through 271, 279, and, more recently, 273. The federal UIC
regulations are found at 40 C.F.R. 144 through 148.
This order is supported by an opinion adopted on the same day. The Board will wait
the 30 days for USEPA review that are provided in the state primacy agreement, then file the
Amendments with the Secretary of State and submit Notices of Adopted Amendments for
publication in the
Illinois Register
. The complete text of the adopted rules follows.
IT IS SO ORDERED.
I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control Board, do hereby certify
that the above order was adopted on the 17th day of December 1998 by a vote of 6-0.
Dorothy M. Gunn, Clerk
Illinois Pollution Control Board
3
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER b: PERMITS
PART 703
RCRA PERMIT PROGRAM
SUBPART A: GENERAL PROVISIONS
Section
703.100
Scope and Relation to Other Parts
703.101
Purpose
703.110
References
SUBPART B: PROHIBITIONS
Section
703.120
Prohibitions in General
703.121
RCRA Permits
703.122
Specific Inclusions in Permit Program
703.123
Specific Exclusions from Permit Program
703.124
Discharges of Hazardous Waste
703.125
Reapplications
703.126
Initial Applications
703.127
Federal Permits (Repealed)
SUBPART C: AUTHORIZATION BY RULE AND INTERIM STATUS
Section
703.140
Purpose and Scope
703.141
Permits by Rule
703.150
Application by Existing HWM Facilities and Interim Status Qualifications
703.151
Application by New HWM Facilities
703.152
Amended Part A Application
703.153
Qualifying for Interim Status
703.154
Prohibitions During Interim Status
703.155
Changes During Interim Status
703.156
Interim Status Standards
703.157
Grounds for Termination of Interim Status
703.158
Permits for Less Than an Entire Facility
703.159
Closure by Removal
703.160
Procedures for Closure Determination
SUBPART D: APPLICATIONS
Section
703.180
Applications in General
703.181
Contents of Part A
4
703.182
Contents of Part B
703.183
General Information
703.184
Facility Location Information
703.185
Groundwater Protection Information
703.186
Exposure Information
703.187
Solid Waste Management Units
703.188
Other Information
703.191
Public Participation: Pre-Application Public Notice and Meeting
703.192
Public Participation: Public Notice of Application
703.193
Public Participation: Information Repository
703.200
Specific Part B Application Information
703.201
Containers
703.202
Tank Systems
703.203
Surface Impoundments
703.204
Waste Piles
703.205
Incinerators that Burn Hazardous Waste
703.206
Land Treatment
703.207
Landfills
703.208
Boilers and Industrial Furnaces Burning Hazardous Waste
703.209
Miscellaneous Units
703.210
Process Vents
703.211
Equipment
703.212
Drip Pads
703.213
Air Emission Controls for Tanks, Surface Impoundments, and Containers
SUBPART E: SHORT TERM AND PHASED PERMITS
Section
703.221
Emergency Permits
703.222
Incinerator Conditions Prior to Trial Burn
703.223
Incinerator Conditions During Trial Burn
703.224
Incinerator Conditions After Trial Burn
703.225
Trial Burns for Existing Incinerators
703.230
Land Treatment Demonstration
703.231
Research, Development and Demonstration Permits
703.232
Permits for Boilers and Industrial Furnaces Burning Hazardous Waste
SUBPART F: PERMIT CONDITIONS OR DENIAL
Section
703.240
Permit Denial
703.241
Establishing Permit Conditions
703.242
Noncompliance Pursuant to Emergency Permit
703.243
Monitoring
703.244
Notice of Planned Changes (Repealed)
703.245
Twenty-four Hour Reporting
703.246
Reporting Requirements
5
703.247
Anticipated Noncompliance
703.248
Information Repository
SUBPART G: CHANGES TO PERMITS
Section
703.260
Transfer
703.270
Modification
703.271
Causes for Modification
703.272
Causes for Modification or Reissuance
703.273
Facility Siting
703.280
Permit Modification at the Request of the Permittee
703.281
Class 1 Modifications
703.282
Class 2 Modifications
703.283
Class 3 Modifications
703.Appendix A
Classification of Permit Modifications
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14289, effective October 12, 1983;
amended in R83-24 at 8 Ill. Reg. 206, effective December 27, 1983; amended in R84-9 at 9 Ill. Reg.
11899, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1110, effective January 2, 1986;
amended in R85-23 at 10 Ill. Reg. 13284, effective July 28, 1986; amended in R86-1 at 10 Ill. Reg.
14093, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20702, effective December 2,
1986; amended in R86-28 at 11 Ill. Reg. 6121, effective March 24, 1987; amended in R86-46 at 11
Ill. Reg. 13543, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19383, effective
November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2584, effective January 15, 1988; amended
in R87-39 at 12 Ill. Reg. 13069, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 447,
effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18477, effective November 13, 1989;
amended in R89-9 at 14 Ill. Reg. 6278, effective April 16, 1990; amended in R90-2 at 14 Ill. Reg.
14492, effective August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9616, effective June 17, 1991;
amended in R91-1 at 15 Ill. Reg. 14554, effective September 30, 1991; amended in R91-13 at 16 Ill.
Reg. 9767, effective June 9, 1992; amended in R92-10 at 17 Ill. Reg. 5774, effective March 26,
1993; amended in R93-4 at 17 Ill. Reg. 20794, effective November 22, 1993; amended in R93-16 at
18 Ill. Reg. 6898, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg. 12392, effective July 29,
1994; amended in R94-5 at 18 Ill. Reg. 18316, effective December 20, 1994; amended in R95-6 at
19 Ill. Reg. 9920, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11225, effective August
1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 553, effective December 16, 1997;
amended in R98-12 at 22 Ill. Reg. 7632, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at
22 Ill. Reg. 17930, effective September 28, 1998; amended in R98-21/R99-2/R99-7 at 22 Ill. Reg.
________, effective ______________________.
6
SUBPART C: AUTHORIZATION BY RULE AND INTERIM STATUS
Section 703.155
Changes During Interim Status
a)
Except as provided in subsection (b), below, the owner or operator of an
interim status facility may make the following changes at the facility:
1)
Treatment, storage or disposal of new hazardous wastes not previously
identified in Part A of the permit application (and, in the case of newly
listed or identified wastes, addition of the units being used to treat, store
or dispose of the hazardous wastes on the date of the listing or
identification) if the owner or operator submits a revised Part A permit
application prior to such treatment, storage or disposal;
2)
Increases in the design capacity of processes used at the facility if the
owner or operator submits a revised Part A permit application prior to
such a change (along with a justification explaining the need for the
change) and the Agency approves the change because:
A)
There is a lack of available treatment, storage or disposal
capacity at other hazardous waste management facilities; or
B)
The change is necessary to comply with a federal, State or local
requirement, including 35 Ill. Adm. Code 725, 728 or 729.;
3)
Changes in the processes for the treatment, storage or disposal of
hazardous waste may be made at a facility or addition of processes if the
owner or operator submits a revised Part A permit application prior to
such a change (along with a justification explaining the need for change)
and the Agency approves the change because:
A)
The change is necessary to prevent a threat to human health or
the environment because of an emergency situation; or
B)
The change is necessary to comply with a federal, State or local
requirement, including 35 Ill. Adm. Code 725, 728 or 729;
4)
Changes in the ownership or operational control of a facility if the new
owner or operator submits a revised Part A permit application no later
than 90 days prior to the scheduled change. When a transfer of
ownership or operational control of a facility occurs, the old owner or
operator shall comply with the requirements of 35 Ill. Adm. Code
725.Subpart H (financial requirements), until the new owner or operator
has demonstrated to the Agency that it is complying with the
requirements of that Subpart. The new owner or operator shall
7
demonstrate compliance with the financial assurance requirements within
six months after the date of the change in the ownership or operational
control of the facility. Upon demonstration to the Agency by the new
owner or operator of compliance with the financial assurance
requirements, the Agency shall notify the old owner or operator in
writing that the old owner or operator no longer needs to comply with 35
Ill. Adm. Code 725.Subpart H as of the date of demonstration. All
other interim status duties are transferred effective immediately upon the
date of the change of ownership or operational control of the facility;
5)
Changes made in accordance with an interim status corrective action
order issued by: USEPA under Section 3008(h) of the Resource
Conservation and Recovery Act or other federal authority; a court
pursuant to a judicial action brought USEPA; a court pursuant to the
Environmental Protection Act; or, the Board. Changes under this
subsection are limited to the treatment, storage or disposal of solid waste
from releases that originate within the boundary of the facility.;
6)
Addition of newly regulated units for the treatment, storage or disposal
of hazardous waste if the owner or operator submits a revised Part A
permit application on or before the date on which the unit becomes
subject to the new requirements.
b)
Except as specifically allowed under this subsection, changes listed under
subsection (a), above, must not be made if they amount to reconstruction of the
HWM facility. Reconstruction occurs when the capital investment in the
changes to the facility exceeds fifty percent of the capital cost of a comparable
entirely new HWM facility. If all other requirements are met, the following
changes may be made even if they amount to a reconstruction:
1)
Changes made solely for the purpose of complying with requirements of
35 Ill. Adm. Code 725.293 for tanks and ancillary equipment.
2)
If necessary to comply with federal, State or local requirements,
including 35 Ill. Adm. Code 725, 728 or 729, changes to an existing
unit, changes solely involving tanks or containers, or addition of
replacement surface impoundments that satisfy the statutory standards of
Section 35 Ill. Adm. Code 728.139.
3)
Changes that are necessary to allow owners or operators to continue
handling newly listed or identified hazardous wastes that have been
treated, stored or disposed of at the facility prior to the effective date of
the rule establishing the new listing or identification.
8
4)
Changes during closure of a facility or of a unit within a facility made in
accordance with an approved closure plan.
5)
Changes necessary to comply with an interim status corrective action
order issued by: USEPA under Section 3008(h) of the Resource
Conservation and Recovery Act or other federal authority; a court
pursuant to a judicial action brought by USEPA; a court pursuant to the
Environmental Protection Act; or, the Board. Changes under this
subsection are limited to the treatment, storage or disposal of solid waste
from releases that originate within the boundary of the facility.
6)
Changes to treat or store, in tanks, containers or containment buildings,
hazardous wastes subject to land disposal restrictions imposed in 35 Ill.
Adm. Code 728, provided that such changes are made solely for the
purpose of complying with 35 Ill. Adm. Code 728.
7)
Addition of newly regulated units under subsection (a)(6), above.
8)
Changes necessary to comply with the federal Clean Air Act (CAA)
Maximum Achievable Control Technology (MACT) emissions standards
of 40 CFR 63, Subpart EEE--National Emission Standards for
Hazardous Air Pollutants From Hazardous Waste Combustors.
Board Note: BOARD NOTE: Derived from 40 CFR 270.72 (19907), as amended 57 at 63
Fed. Reg. 37281 33829 August 18, 1992. (June 19, 1998). The federal CAA MACT
standards are directly implemented in Illinois pursuant to Section 39.5 of the Environmental
Protection Act [415 ILCS 5/39.5].
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART G: CHANGES TO PERMITS
Section 703.280
Permit Modification at the Request of the Permittee
a)
Class 1 modifications.See Section 703.281.
b)
Class 2 modifications.See Section 703.282.
c)
Class 3 modifications.See Section 703.283.
d)
Other modifications.
1)
In the case of modifications not explicitly listed in Appendix A, the
permittee may submit a Class 3 modification request to the Agency, or
the permittee may request a determination by the Agency that the
9
modification be reviewed and approved as a Class 1 or Class 2
modification.If the permittee requests that the modification be classified
as a Class 1 or 2 modification, the permittee shall provide the Agency
with the necessary information to support the requested classification.
2)
The Agency shall make the determination described in subsection (d)(1),
above, as promptly as practicable.In determining the appropriate class
for a specific modification, the Agency shall consider the similarity of
the modification to other modifications codified in Appendix A and the
following criteria:
A)
Class 1 modifications apply to minor changes that keep the
permit current with routine changes to the facility or its
operation.These changes do not substantially alter the permit
conditions or reduce the capacity of the facility to protect human
health or the environment.In the case of Class 1 modifications,
the Agency may require prior approval.
B)
Class 2 modifications apply to changes that are necessary to
enable a permittee to respond, in a timely manner, to any of the
following:
i)
Common variations in the types and quantities of the
wastes managed under the facility permit,;
ii)
Technological advances,; and
iii)
Changes necessary to comply with new regulations, where
these changes can be implemented without substantially
changing design specifications or management practices in
the permit.
C)
Class 3 modifications substantially alter the facility or its
operation.
e)
Temporary authorizations.
1)
Upon request of the permittee, the Agency shall, without prior public
notice and comment, grant the permittee a temporary authorization in
accordance with this subsection.Temporary authorizations have a term of
not more than 180 days.
2)
Procedures.
A)
The permittee may request a temporary authorization for:
10
i)
Any Class 2 modification meeting the criteria in
subsection (e)(3)(B) of this Section; and
ii)
Any Class 3 modification that meets the criteria in
subsection (e)(3)(B)(i), below; or that meets the criteria in
subsection subsections (e)(3)(B)(iii) through (v), below,
and provides improved management or treatment of a
hazardous waste already listed in the facility permit.
B)
The temporary authorization request must include:
i)
A description of the activities to be conducted under the
temporary authorization;
ii)
An explanation of why the temporary authorization is
necessary; and
iii)
Sufficient information to ensure compliance with 35 Ill.
Adm. Code 724 standards.
C)
The permittee shall send a notice about the temporary
authorization request to all persons on the facility mailing list
maintained by the Agency and to appropriate units of State and
local governments as specified in 35 Ill. Adm. Code
705.163(a)(5).This notification must be made within seven days
after submission of the authorization request.
3)
The Agency shall approve or deny the temporary authorization as
quickly as practical.To issue a temporary authorization, the Agency shall
find:
A)
The authorized activities are in compliance with the standards of
35 Ill. Adm. Code 724.
B)
The temporary authorization is necessary to achieve one of the
following objectives before action is likely to be taken on a
modification request:
i)
To facilitate timely implementation of closure or
corrective action activities;
ii)
To allow treatment or storage in tanks, containers or in
containment buildings in accordance with 35 Ill. Adm.
Code 728;
11
iii)
To prevent disruption of ongoing waste management
activities;
iv)
To enable the permittee to respond to sudden changes in
the types or quantities of the wastes managed under the
facility permit; or
v)
To facilitate other changes to protect human health and the
environment.
4)
A temporary authorization shall be reissued for one additional term of up
to 180 days provided that the permittee has requested a Class 2 or 3
permit modification for the activity covered in the temporary
authorization, and:
A)
The reissued temporary authorization constitutes the Agency’s
decision on a Class 2 permit modification in accordance with
Section 703.282(f)(1)(D) or (f)(2)(D),; or
B)
The Agency determines that the reissued temporary authorization
involving a Class 3 permit modification request is warranted to
allow the authorized activities to continue while the modification
procedures of 35 Ill. Adm. Code 703.283 are conducted.
f)
Public notice and appeals of permit modification decisions.
1)
The Agency shall notify persons on the facility mailing list and
appropriate units of State and local government within 10 days of after
any decision to grant or deny a Class 2 or 3 permit modification
request.The Agency shall also notify such persons within 10 days after
an automatic authorization for a Class 2 modification goes into effect
under Section 703.282(f)(3) or (f)(5).
2)
The Agency’s decision to grant or deny a Class 2 or 3 permit
modification request may be appealed under the permit appeal
procedures of 35 Ill. Adm. Code 705.212.
3)
An automatic authorization that goes into effect under Section
703.282(f)(3) or (f)(5) may be appealed under the permit appeal
procedures of 35 Ill. Adm. Code 705.212; however, the permittee may
continue to conduct the activities pursuant to the automatic authorization
until the Board enters a final order on the appeal notwithstanding the
provisions of 35 Ill. Adm. Code 705.204.
12
g)
Newly regulated wastes and units.
1)
The permittee is authorized to continue to manage wastes listed or
identified as hazardous under 35 Ill. Adm. Code 721, or to continue to
manage hazardous waste in units newly regulated as hazardous waste
management units, if:
A)
The unit was in existence as a hazardous waste facility with
respect to the newly listed or characterized waste or newly
regulated waste management unit on the effective date of the final
rule listing or identifying the waste, or regulating the unit;
B)
The permittee submits a Class 1 modification request on or
before the date on which the waste becomes subject to the new
requirements;
C)
The permittee is in compliance with the applicable standards of
35 Ill. Adm. Code 725 and 726;
D)
The permittee also submits a complete class 2 or 3 modification
request within 180 days after the effective date of the rule listing
or identifying the waste, or subjecting the unit to management
standards under 35 Ill. Adm. Code 724, 725 or 726; and
E)
In the case of land disposal units, the permittee certifies that such
unit is in compliance with all applicable requirements of 35 Ill.
Adm. Code 725 for groundwater monitoring and financial
responsibility requirements on the date 12 months after the
effective date of the rule identifying or listing the waste as
hazardous, or regulating the unit as a hazardous waste
management unit.If the owner or operator fails to certify
compliance with all these requirements, the owner or operator
loses authority to operate under this Section.
2)
New wastes or units added to a facility’s permit under this subsection do
not constitute expansions for the purpose of the 25 percent capacity
expansion limit for Class 2 modifications.
h)
Military hazardous waste munitions treatment and disposal.The permittee is
authorized to continue to accept waste military munitions notwithstanding any
permit conditions barring the permittee from accepting off-site wastes, if:
1)
The facility was in existence as a hazardous waste facility and the facility
was already permitted to handle the waste military munitions on the date
13
when the waste military munitions became subject to hazardous waste
regulatory requirements;
2)
On or before the date when the waste military munitions become subject
to hazardous waste regulatory requirements, the permittee submits a
Class 1 modification request to remove or amend the permit provision
restricting the receipt of off-site waste munitions; and
3)
The permittee submits a complete Class 2 modification request within
180 days of after the date when the waste military munitions became
subject to hazardous waste regulatory requirements.
i)
Permit modification list.The Agency shall maintain a list of all approved permit
modifications and shall publish a notice once a year in a State-wide newspaper
that an updated list is available for review.
j)
Combustion facility changes to meet federal 40 CFR 63 MACT standards. The
following procedures apply to hazardous waste combustion facility permit
modifications requested under Section 703.Appendix A, paragraph L(9).
1)
Facility owners or operators must comply with the federal notification of
intent to comply (NIC) requirements of 40 CFR 63.1211 before a permit
modification can be requested under this Section.
2)
If the Agency does not act to either approve or deny the request within 90
days of receiving it, the request shall be deemed approved. The Agency
may, at its discretion, extend this 90-day deadline one time for up to 30
days by notifying the facility owner or operator in writing before the 90
days has expired.
BOARD NOTE: Derived from 40 CFR 270.42(d) through (i) (j) (1997), as amended at 63
Fed. Reg. 33829 (June 19, 1998).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 703.Appendix A
Classification of Permit Modifications
Class Modifications
A.
General Permit Provisions
1
1.
Administrative and informational changes.
1
2.
Correction of typographical errors.
14
1
3.
Equipment replacement or upgrading with functionally equivalent components
(e.g., pipes, valves, pumps, conveyors, controls).
4.
Changes in the frequency of or procedures for monitoring, reporting, sampling
or maintenance activities by the permittee:
1
a.
To provide for more frequent monitoring, reporting or maintenance.
2
b.
Other changes.
5.
Schedule of compliance:
1*
a.
Changes in interim compliance dates, with prior approval of the Agency.
3
b.
Extension of final compliance date.
1*
6.
Changes in expiration date of permit to allow earlier permit termination, with
prior approval of the Agency.
1*
7.
Changes in ownership or operational control of a facility, provided the
procedures of Section 703.260(b) are followed.
B.
General Facility Standards
1.
Changes to waste sampling or analysis methods:
1
a.
To conform with Agency guidance or Board regulations.
1*
b.
To incorporate changes associated with F039 (multi-source leachate)
sampling or analysis methods.
1*
c.
To incorporate changes associated with underlying hazardous constituents
in ignitable or corrosive wastes.
2
d.
Other changes.
2.
Changes to analytical quality assurance/control plan:
1
a.
To conform with agency guidance or regulations.
2
b.
Other changes.
1
3.
Changes in procedures for maintaining the operating record.
2
4.
Changes in frequency or content of inspection schedules.
15
5.
Changes in the training plan:
2
a.
That affect the type or decrease the amount of training given to
employees.
1
b.
Other changes.
6.
Contingency plan:
2
a.
Changes in emergency procedures (i.e., spill or release response
procedures).
1
b.
Replacement with functionally equivalent equipment, upgrade or relocate
emergency equipment listed.
2
c.
Removal of equipment from emergency equipment list.
1
d.
Changes in name, address or phone number of coordinators or other
persons or agencies identified in the plan.
Note: When a permit modification (such as introduction of a new unit) requires
a change in facility plans or other general facility standards, that change must be
reviewed under the same procedures as the permit modification.
7.
CQA plan:
1
a.
Changes that the CQA officer certifies in the operating record will
provide equivalent or better certainty that the unit components meet the
design specifications.
2
b.
Other changes.
Note: When a permit modification (such as introduction of a new unit) requires
a change in facility plans or other general facility standards, that change shall be
reviewed under the same procedures as a permit modification.
C.
Groundwater Protection
1.
Changes to wells:
2
a.
Changes in the number, location, depth or design of upgradient or
downgradient wells of permitted groundwater monitoring system.
16
1
b.
Replacement of an existing well that has been damaged or rendered
inoperable, without change to location, design or depth of the well.
1*
2.
Changes in groundwater sampling or analysis procedures or monitoring schedule,
with prior approval of the Agency.
1*
3.
Changes in statistical procedure for determining whether a statistically significant
change in groundwater quality between upgradient and downgradient wells has
occurred, with prior approval of the Agency.
2*
4.
Changes in point of compliance.
5.
Changes in indicator parameters, hazardous constituents or concentration limits
(including ACLs (Alternate Concentration Limits)):
3
a.
As specified in the groundwater protection standard.
2
b.
As specified in the detection monitoring program.
2
6.
Changes to a detection monitoring program as required by 35 Ill. Adm. Code
724.198(j), unless otherwise specified in this Appendix.
7.
Compliance monitoring program:
3
a.
Addition of compliance monitoring program as required by 35 Ill. Adm.
Code 724.198(h)(4) and 724.199.
2
b.
Changes to a compliance monitoring program as required by 35 Ill. Adm.
Code 724.199(k), unless otherwise specified in this Appendix.
8.
Corrective action program:
3
a.
Addition of a corrective action program as required by 35 Ill. Adm. Code
724.199(i)(2) and 724.200.
2
b.
Changes to a corrective action program as required by 35 Ill. Adm. Code
724.200(h), unless otherwise specified in this Appendix.
D.
Closure
1.
Changes to the closure plan:
1*
a.
Changes in estimate of maximum extent of operations or maximum
inventory of waste on-site at any time during the active life of the facility,
with prior approval of the Agency.
17
1*
b.
Changes in the closure schedule for any unit, changes in the final closure
schedule for the facility or extension of the closure period, with prior
approval of the Agency.
1*
c.
Changes in the expected year of final closure, where other permit
conditions are not changed, with prior approval of the Agency.
1*
d.
Changes in procedures for decontamination of facility equipment or
structures, with prior approval of the Agency.
2
e.
Changes in approved closure plan resulting from unexpected events
occurring during partial or final closure, unless otherwise specified in this
Appendix.
2
f.
Extension of the closure period to allow a landfill, surface impoundment
or land treatment unit to receive non-hazardous wastes after final receipt
of hazardous wastes under 35 Ill. Adm. Code 724.213(d) or (e).
3
2.
Creation of a new landfill unit as part of closure.
3.
Addition of the following new units to be used temporarily for closure activities:
3
a.
Surface impoundments.
3
b.
Incinerators.
3
c.
Waste piles that do not comply with 35 Ill. Adm. Code 724.350(c).
2
d.
Waste piles that comply with 35 Ill. Adm. Code 724.350(c).
2
e.
Tanks or containers (other than specified below).
1*
f.
Tanks used for neutralization, dewatering, phase separation or component
separation, with prior approval of the Agency.
E.
Post-Closure
1
1.
Changes in name, address or phone number of contact in post-closure plan.
2
2.
Extension of post-closure care period.
3
3.
Reduction in the post-closure care period.
18
1
4.
Changes to the expected year of final closure, where other permit conditions are
not changed.
2
5.
Changes in post-closure plan necessitated by events occurring during the active
life of the facility, including partial and final closure.
F.
Containers
1.
Modification or addition of container units:
3
a.
Resulting in greater than 25% percent increase in the facility’s container
storage capacity, except as provided in F(1)(c) and F(4)(a).
2
b.
Resulting in up to 25% percent increase in the facility’s container storage
capacity, except as provided in F(1)(c) and F(4)(a).
1
c.
Or treatment processes necessary to treat wastes that are restricted from
land disposal to meet some or all of the applicable treatment standards or
to treat wastes to satisfy (in whole or in part) the standard of “use of
practically available technology that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a)(2)(ii), incorporated by reference in
35 Ill. Adm. Code 728.108, with prior approval of the Agency.This
modification may also involve the addition of new waste codes or
narrative description of wastes.It is not applicable to dioxin-containing
wastes (F020, F021, F022, F023, F026, F027 and F028).
2.
Modification of container units without an increased capacity or alteration of the
system:
2
a.
Modification of a container unit without increasing the capacity of the
unit.
1
b.
Addition of a roof to a container unit without alteration of the
containment system.
3.
Storage of different wastes in containers, except as provided in F(4):
3
a.
That require additional or different management practices from those
authorized in the permit.
2
b.
That do not require additional or different management practices from
those authorized in the permit.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
19
4.
Storage or treatment of different wastes in containers:
2
a.
That require addition of units or change in treatment process or
management standards, provided that the wastes are restricted from land
disposal and are to be treated to meet some or all of the applicable
treatment standards, or are to be treated to satisfy (in whole or in part) the
standard of “use of practically available technology that yields the greatest
environmental benefit” contained in 40 CFR 268.8(a)(2)(ii), incorporated
by reference in 35 Ill. Adm. Code 728.108.It is not applicable to dioxin-
containing wastes (F020, F021, F022, F023, F026, F027 and F028).
1*
b.
That do not require the addition of units or a change in the treatment
process or management standards, and provided that the units have
previously received wastes of the same type (e.g., incinerator scrubber
water).This modification is not applicable to dioxin-containing wastes
(F020, F021, F022, F023, F026, F027 and F028).
G.
Tanks
1.
3
a.
Modification or addition of tank units resulting in greater than 25%
percent increase in the facility’s tank capacity, except as provided in
paragraphs G(1)(c), G(1)(d) and G(1)(e).
2
b.
Modification or addition of tank units resulting in up to 25% percent
increase in the facility’s tank capacity, except as provided in paragraphs
G(1)(d) and G(1)(e).
2
c.
Addition of a new tank that will operate for more than 90 days using any
of the following physical or chemical treatment technologies:
neutralization, dewatering, phase separation or component separation.
1*
d.
After prior approval of the Agency, addition of a new tank that will
operate for up to 90 days using any of the following physical or chemical
treatment technologies: neutralization, dewatering, phase separation or
component separation.
20
1*
e.
Modification or addition of tank units or treatment processes that are
necessary to treat wastes that are restricted from land disposal to meet
some or all of the applicable treatment standards or to treat wastes to
satisfy (in whole or in part) the standard of “use of practically available
technology that yields the greatest environmental benefit” contained in 40
CFR 268.8(a)(2)(ii), incorporated by reference in 35 Ill. Adm. Code
728.108, with prior approval of the Agency.This modification may also
involve the addition of new waste codes.It is not applicable to dioxin-
containing wastes (F020, F021, F022, F023, F026, F027 and F028).
2
2.
Modification of a tank unit or secondary containment system without increasing
the capacity of the unit.
1
3.
Replacement of a tank with a tank that meets the same design standards and has a
capacity within ± 10% percent of the replaced tank provided:
a.
The capacity difference is no more than 1500 gallons,
b.
The facility’s permitted tank capacity is not increased, and
c.
The replacement tank meets the same conditions in the permit.
2
4.
Modification of a tank management practice.
5.
Management of different wastes in tanks:
3
a.
That require additional or different management practices, tank design,
different fire protection specifications or significantly different tank
treatment process from that authorized in the permit, except as provided
in paragraph G(5)(c).
2
b.
That do not require additional or different management practices, tank
design, different fire protection specification or significantly different
tank treatment process than authorized in the permit, except as provided
in paragraph G(5)(d).
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
21
1*
c.
That require addition of units or change in treatment processes or
management standards, provided that the wastes are restricted from land
disposal and are to be treated to meet some or all of the applicable
treatment standards, or that are to be treated to satisfy (in whole or in
part) the standard of “use of practically available technology that yields
the greatest environmental benefit” contained in 40 CFR 268.8(a)(2)(ii),
incorporated by reference in 35 Ill. Adm. Code 728.108.The modification
is not applicable to dioxin-containing wastes (F020, F021, F022, F023,
F026, F027 and F028).
1
d.
That do not require the addition of units or a change in the treatment
process or management standards, and provided that the units have
previously received wastes of the same type (e.g., incinerator scrubber
water).This modification is not applicable to dioxin-containing wastes
(F020, F021, F022, F023, F026, F027 and F028).
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
H.
Surface Impoundments
3
1.
Modification or addition of surface impoundment units that result in increasing
the facility’s surface impoundment storage or treatment capacity.
3
2.
Replacement of a surface impoundment unit.
2
3.
Modification of a surface impoundment unit without increasing the facility’s
surface impoundment storage or treatment capacity and without modifying the
unit’s liner, leak detection system or leachate collection system.
2
4.
Modification of a surface impoundment management practice.
5.
Treatment, storage or disposal of different wastes in surface impoundments:
3
a.
That require additional or different management practices or different
design of the liner or leak detection system than authorized in the permit.
2
b.
That do not require additional or different management practices or
different design of the liner or leak detection system than authorized in
the permit.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
22
1
c.
That are wastes restricted from land disposal that meet the applicable
treatment standards or that are treated to satisfy the standard of “use of
practically available technology that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a)(2)(ii), incorporated by reference in
35 Ill. Adm. Code 728.108, and provided that the unit meets the
minimum technological requirements stated in 40 CFR 268.5(h)(2),
incorporated by reference in 35 Ill. Adm. Code 728.105.This
modification is not applicable to dioxin-containing wastes (F020, F021,
F022, F023, F026, F027 and F028).
1
d.
That are residues from wastewater treatment or incineration, provided the
disposal occurs in a unit that meets the minimum technological
requirements stated in 40 CFR 268.5(h)(2), incorporated by reference in
35 Ill. Adm. Code 728.105, and provided further that the surface
impoundment has previously received wastes of the same type (for
example, incinerator scrubber water).This modification is not applicable
to dioxin-containing wastes (F020, F021, F022, F023, F026, F027 and
F028).
1*
6.
Modifications of unconstructed units to comply with 35 Ill. Adm. Code
724.321(c), 724.322, 724.323 and 724.326(d).
7.
Changes in response action plan:
3
a.
Increase in action leakage rate.
3
b.
Change in a specific response reducing its frequency or effectiveness.
2
c.
Other changes.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
I.
Enclosed Waste Piles.For all waste piles, except those complying with 35 Ill. Adm.
Code 724.350(c), modifications are treated the same as for a landfill.The following
modifications are applicable only to waste piles complying with 35 Ill. Adm. Code
724.350(c).
1.
Modification or addition of waste pile units:
3
a.
Resulting in greater than 25% percent increase in the facility’s waste pile
storage or treatment capacity.
2
b.
Resulting in up to 25% percent increase in the facility’s waste pile storage
or treatment capacity.
23
2
2.
Modification of waste pile unit without increasing the capacity of the unit.
1
3.
Replacement of a waste pile unit with another waste pile unit of the same design
and capacity and meeting all waste pile conditions in the permit.
2
4.
Modification of a waste pile management practice.
5.
Storage or treatment of different wastes in waste piles:
3
a.
That require additional or different management practices or different
design of the unit.
2
b.
That do not require additional or different management practices or
different design of the unit.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
2
6.
Conversion of an enclosed waste pile to a containment building unit.
Note: See Section 703.280(g) for modification procedures to be used for the
management of newly listed or identified wastes.
J.
Landfills and Unenclosed Waste Piles
3
1.
Modification or addition of landfill units that result in increasing the facility’s
disposal capacity.
3
2.
Replacement of a landfill.
3
3.
Addition or modification of a liner, leachate collection system, leachate detection
system, run-off control or final cover system.
2
4.
Modification of a landfill unit without changing a liner, leachate collection
system, leachate detection system, run-off control or final cover system.
2
5.
Modification of a landfill management practice.
6.
Landfill different wastes:
3
a.
That require additional or different management practices, different
design of the liner, leachate collection system or leachate detection
system.
24
2
b.
That do not require additional or different management practices,
different design of the liner, leachate collection system or leachate
detection system.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
1
c.
That are wastes restricted from land disposal that meet the applicable
treatment standards or that are treated to satisfy the standard of “use of
practically available technology that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a)(2)(ii), incorporated by reference in
35 Ill. Adm. Code 728.108, and provided that the landfill unit meets the
minimum technological requirements stated in 40 CFR 268.5(h)(2),
incorporated by reference in 35 Ill. Adm. Code 728.105.This
modification is not applicable to dioxin-containing wastes (F020, F021,
F022, F023, F026, F027 and F028).
1
d.
That are residues from wastewater treatment or incineration, provided the
disposal occurs in a landfill unit that meets the minimum technological
requirements stated in 40 CFR 268.5(h)(2), incorporated by reference in
35 Ill. Adm. Code 728.105, and provided further that the landfill has
previously received wastes of the same type (for example, incinerator
ash).This modification is not applicable to dioxin-containing wastes
(F020, F021, F022, F023, F026, F027 and F028).
1*
7.
Modification of unconstructed units to comply with 35 Ill. Adm. Code
724.351(c), 724.352, 724.353, 724.354(c), 724.401(c), 724.402, 724.403(c) and
724.404.
8.
Changes in response action plan:
3
a.
Increase in action leakage rate.
3
b.
Change in a specific response reducing its frequency or effectiveness.
2
c.
Other changes.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
K.
Land Treatment
3
1.
Lateral expansion of or other modification of a land treatment unit to increase
area extent.
25
2
2.
Modification of run-on control system.
3
3.
Modify run-off control system.
2
4.
Other modification of land treatment unit component specifications or standards
required in permit.
5.
Management of different wastes in land treatment units:
3
a.
That require a change in permit operating conditions or unit design
specifications.
2
b.
That do not require a change in permit operating conditions or unit design
specifications.
Note: See Section 703.280(g) for modification procedures to be used for
the management of newly listed or identified wastes.
6.
Modification of a land treatment unit management practice to:
3
a.
Increase rate or change method of waste application.
1
b.
Decrease rate of waste application.
2
7.
Modification of a land treatment unit management practice to change measures of
pH or moisture content or to enhance microbial or chemical reactions.
3
8.
Modification of a land treatment unit management practice to grow food chain
crops, to add to or replace existing permitted crops with different food chain
crops or to modify operating plans for distribution of animal feeds resulting from
such crops.
3
9.
Modification of operating practice due to detection of releases from the land
treatment unit pursuant to 35 Ill. Adm. Code 724.378(g)(2).
3
10.
Changes in the unsaturated zone monitoring system resulting in a change to the
location, depth, number of sampling points or replace unsaturated zone
monitoring devices or components of devices with devices or components that
have specifications different from permit requirements.
2
11.
Changes in the unsaturated zone monitoring system that do not result in a change
to the location, depth, number of sampling points, or that replace unsaturated
zone monitoring devices or components of devices with devices or components
having specifications different from permit requirements.
26
2
12.
Changes in background values for hazardous constituents in soil and soil-pore
liquid.
2
13.
Changes in sampling, analysis or statistical procedure.
2
14.
Changes in land treatment demonstration program prior to or during the
demonstration.
1*
15.
Changes in any condition specified in the permit for a land treatment unit to
reflect results of the land treatment demonstration, provided performance
standards are met, and the Agency’s prior approval has been received.
1*
16.
Changes to allow a second land treatment demonstration to be conducted when
the results of the first demonstration have not shown the conditions under which
the wastes can be treated completely, provided the conditions for the second
demonstration are substantially the same as the conditions for the first
demonstration and have received the prior approval of the Agency.
3
17.
Changes to allow a second land treatment demonstration to be conducted when
the results of the first demonstration have not shown the conditions under which
the wastes can be treated completely, where the conditions for the second
demonstration are not substantially the same as the conditions for the first
demonstration.
2
18.
Changes in vegetative cover requirements for closure.
L.
Incinerators, Boilers and Industrial Furnaces
3
1.
Changes to increase by more than 25% percent any of the following limits
authorized in the permit: A thermal feed rate limit, a feedstream feed rate limit, a
chlorine/chloride feed rate limit, a metal feed rate limit or an ash feed rate
limit.The Agency shall require a new trial burn to substantiate compliance with
the regulatory performance standards unless this demonstration can be made
through other means.
2
2.
Changes to increase by up to 25% percent any of the following limits authorized
in the permit: A thermal feed rate limit, a feedstream feed rate limit, a
chlorine/chloride feed rate limit, a metal feed rate limit or an ash feed rate
limit.The Agency shall require a new trial burn to substantiate compliance with
the regulatory performance standards unless this demonstration can be made
through other means.
27
3
3.
Modification of an incinerator, boiler or industrial furnace unit by changing the
internal size or geometry of the primary or secondary combustion units, by
adding a primary or secondary combustion unit, by substantially changing the
design of any component used to remove HCl/Cl2, metals or particulate from the
combustion gases or by changing other features of the incinerator, boiler or
industrial furnace that could affect its capability to meet the regulatory
performance standards.The Agency shall require a new trial burn to substantiate
compliance with the regulatory performance standards, unless this demonstration
can be made through other means.
2
4.
Modification of an incinerator, boiler or industrial furnace unit in a manner that
will not likely affect the capability of the unit to meet the regulatory performance
standards but which will change the operating conditions or monitoring
requirements specified in the permit.The Agency may require a new trial burn to
demonstrate compliance with the regulatory performance standards.
5.
Operating requirements:
3
a.
Modification of the limits specified in the permit for minimum or
maximum combustion gas temperature, minimum combustion gas
residence time,oxygen concentration in the secondary combustion
chamber, flue gas carbon monoxide or hydrocarbon concentration,
maximum temperature at the inlet to the PM emission control system or
operating parameters for the air pollution control system.The Agency
shall require a new trial burn to substantiate compliance with the
regulatory performance standards unless this demonstration can be made
through other means.
3
b.
Modification of any stack gas emission limits specified in the permit, or
modification of any conditions in the permit concerning emergency
shutdown or automatic waste feed cutoff procedures or controls.
2
c.
Modification of any other operating condition or any inspection or
recordkeeping requirement specified in the permit.
6.
Burning different wastes:
3
a.
If the waste contains a POHC that is more difficult to burn than
authorized by the permit or if burning of the waste requires compliance
with different regulatory performance standards than specified in the
permit, the Agency shall require a new trial burn to substantiate
compliance with the regulatory performance standards, unless this
demonstration can be made through other means.
28
2
b.
If the waste does not contain a POHC that is more difficult to burn than
authorized by the permit and if burning of the waste does not require
compliance with different regulatory performance standards than specified
in the permit.
BOARD NOTENote: See Section 703.280(g) for modification procedures
to be used for the management of newly listed or identified wastes.
7.
Shakedown and trial burn:
2
a.
Modification of the trial burn plan or any of the permit conditions
applicable during the shakedown period for determining operational
readiness after construction, the trial burn period or the period
immediately following the trial burn.
1*
b.
Authorization of up to an additional 720 hours of waste burning during
the shakedown period for determining operational readiness after
construction, with the prior approval of the Agency.
1*
c.
Changes in the operating requirements set in the permit for conducting a
trial burn, provided the change is minor and has received the prior
approval of the Agency.
1*
d.
Changes in the ranges of the operating requirements set in the permit to
reflect the results of the trial burn, provided the change is minor and has
received the prior approval of the Agency.
1
8.
Substitution of an alternate type of nonhazardous waste fuel that is not specified
in the permit.
1*
9.
Technology changes needed to meet standards under federal 40 CFR 63 (Subpart
EEE--National Emission Standards for Hazardous Air Pollutants From Hazardous
Waste Combustors), provided the procedures of 35 Ill. Adm. Code 703.280(j)
are followed.
M.
Containment Buildings.
1.
Modification or addition of containment building units:
3
a.
Resulting in greater than 25% percent increase in the facility’s
containment building storage or treatment capacity.
2
b.
Resulting in up to 25% percent increase in the facility’s containment
building storage or treatment capacity.
29
2
2.
Modification of a containment building unit or secondary containment system
without increasing the capacity of the unit.
3.
Replacement of a containment building with a containment building that meets
the same design standards provided:
1
a.
The unit capacity is not increased.
1
b.
The replacement containment building meets the same conditions in the
permit.
2
4.
Modification of a containment building management practice.
5.
Storage or treatment of different wastes in containment buildings:
3
a.
That require additional or different management practices.
2
b.
That do not require additional or different management practices
N.
Corrective Action.
3
1.
Approval of a corrective action management unit pursuant to 35 Ill. Adm. Code
724.652.
2
2.
Approval of a temporary unit or time extension pursuant to 35 Ill. Adm. Code
724.653.
Note:* indicates modifications requiring prior Agency approval.
BOARD NOTE: Derived from 40 CFR 270.42, Appendix I (19927), as amended at 58 63
Fed. Reg. 868533829 February 16, 1993 (June 19, 1998).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 720
HAZARDOUS WASTE MANAGEMENT SYSTEM: GENERAL
30
SUBPART A: GENERAL PROVISIONS
Section
720.101
Purpose, Scope, and Applicability
720.102
Availability of Information; Confidentiality of Information
720.103
Use of Number and Gender
SUBPART B: DEFINITIONS
Section
720.110
Definitions
720.111
References
SUBPART C: RULEMAKING PETITIONS AND OTHER PROCEDURES
Section
720.120
Rulemaking
720.121
Alternative Equivalent Testing Methods
720.122
Waste Delisting
720.123
Petitions for Regulation as Universal Waste
720.130
Procedures for Solid Waste Determinations
720.131
Solid Waste Determinations
720.132
Boiler Determinations
720.133
Procedures for Determinations
720.140
Additional regulation of certain hazardous waste Recycling Activities on a case-
by-case Basis
720.141
Procedures for case-by-case regulation of hazardous waste Recycling Activities
720.Appendix A
Overview of 40 CFR, Subtitle C Regulations
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982; amended
and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982; amended in R82-19
at 7 Ill. Reg. 14015, effective October 12, 1983; amended in R84-9, 53 PCB 131 at 9 Ill. Reg. 11819,
effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 968, effective January 2, 1986; amended
in R86-1 at 10 Ill. Reg. 13998, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20630,
effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6017, effective March 24, 1987;
amended in R86-46 at 11 Ill. Reg. 13435, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg.
19280, effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2450, effective January 15,
1988; amended in R87-39 at 12 Ill. Reg. 12999, effective July 29, 1988; amended in R88-16 at 13 Ill.
Reg. 362, effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18278, effective
November 13, 1989; amended in R89-2 at 14 Ill. Reg. 3075, effective February 20, 1990; amended
in R89-9 at 14 Ill. Reg. 6225, effective April 16, 1990; amended in R90-10 at 14 Ill. Reg. 16450,
effective September 25, 1990; amended in R90-17 at 15 Ill. Reg. 7934, effective May 9, 1991;
amended in R90-11 at 15 Ill. Reg. 9323, effective June 17, 1991; amended in R91-1 at 15 Ill. Reg.
14446, effective September 30, 1991; amended in R91-13 at 16 Ill. Reg. 9489, effective June 9,
1992; amended in R92-1 at 16 Ill. Reg. 17636, effective November 6, 1992; amended in R92-10 at
17 Ill. Reg. 5625, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20545, effective
November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6720, effective April 26, 1994; amended in
31
R94-7 at 18 Ill. Reg. 12160, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17480,
effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9508, effective June 27, 1995;
amended in R95-20 at 20 Ill. Reg. 10929, August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill.
Reg. 256, effective December 16, 1997; amended in R98-12 at 22 Ill. Reg. 7590, effective April 15,
1998; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg. 17496, effective September 28, 1998;
amended in R98-21/R99-2/R99-7 at 22 Ill. Reg. ________, effective ______________________.
SUBPART B: DEFINITIONS
Section 720.111
References
a)
The following publications are incorporated by reference for the purposes of this
Part and 35 Ill. Adm. Code 703 through 705, 721 through 726, 728, 730, 731,
733, 738, and 739:
ACI. Available from the American Concrete Institute, Box 19150,
Redford Station, Detroit, Michigan 48219:
ACI 318-83: “Building Code Requirements for Reinforced
Concrete”, adopted September, 1983.
ANSI. Available from the American National Standards Institute, 1430
Broadway, New York, New York 10018, 212-354-3300:
ANSI B31.3 and B31.4. See ASME/ANSI B31.3 and B31.4.
API. Available from the American Petroleum Institute, 1220 L Street,
N.W., Washington, D.C. 20005, 202-682-8000:
“Cathodic Protection of Underground Petroleum Storage Tanks
and Piping Systems”, API Recommended Practice 1632, Second
Edition, December, 1987.
“Evaporative Loss from External Floating-Roof Tanks”, API
Publication 2517, Third Edition, February, 1989.
“Guide for Inspection of Refinery Equipment, Chapter XIII,
Atmospheric and Low Pressure Storage Tanks”, 4th Edition,
1981, reaffirmed December, 1987.
“Installation of Underground Petroleum Storage Systems”, API
Recommended Practice 1615, Fourth Edition, November, 1987.
APTI. Available from the Air and Waste Management Association, Box
2861, Pittsburgh, PA 15230, 412-232-3444:
32
APTI Course 415: Control of Gaseous Emissions, USEPA
Publication EPA-450/2-81-005, December, 1981.
ASME. Available from the American Society of Mechanical Engineers,
345 East 47th Street, New York, NY 10017, 212-705-7722:
“Chemical Plant and Petroleum Refinery Piping”, ASME/ANSI
B31.3-1987, as supplemented by B31.3a-1988 and B31.3b-1988.
Also available from ANSI.
“Liquid Transportation Systems for Hydrocarbons, Liquid
Petroleum Gas, Anhydrous Ammonia, and Alcohols”,
ASME/ANSI B31.4-1986, as supplemented by B31.4a-1987.
Also available from ANSI.
ASTM. Available from American Society for Testing and Materials,
1916 Race Street, Philadelphia, PA 19103, 215-299-5400:
ASTM C 94-90, Standard Specification for Ready-Mixed
Concrete, approved March 30, 1990.
ASTM D 88-87, Standard Test Method for Saybolt Viscosity,
April 24, 1981, reapproved January, 1987.
ASTM D 93-85, Standard Test Methods for Flash Point by
Pensky-Martens Closed Tester, approved October 25, 1985.
ASTM D 1946-90, Standard Practice for Analysis of Reformed
Gas by Gas Chromatography, approved March 30, 1990.
ASTM D 2161-87, Standard Practice for Conversion of
Kinematic Viscosity to Saybolt Universal or to Saybolt Furol
Viscosity, March 27, 1987.
ASTM D 2267-88, Standard Test Method for Aromatics in Light
Naphthas and Aviation Gasolines by Gas Chromatography,
approved November 17, 1988.
ASTM D 2382-88, Standard Test Method for Heat of
Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High
Precision Method), approved October 31, 1988.
33
ASTM D 2879-92, Standard Test Method for Vapor Pressure-
Temperature Relationship and Initial Decomposition Temperature
of Liquids by Isoteniscope, approved 1992.
ASTM D 3828-87, Standard Test Methods for Flash Point of
Liquids by Setaflash Closed Tester, approved December 14,
1988.
ASTM E 168-88, Standard Practices for General Techniques of
Infrared Quantitative Analysis, approved May 27, 1988.
ASTM E 169-87, Standard Practices for General Techniques of
Ultraviolet-Visible Quantitative Analysis, approved February 1,
1987.
ASTM E 260-85, Standard Practice for Packed Column Gas
Chromatography, approved June 28, 1985.
ASTM Method G 21-70 (1984a) -- Standard Practice for
Determining Resistance of Synthetic Polymer Materials to Fungi.
ASTM Method G 22-76 (1984b) -- Standard Practice for
Determining Resistance of Plastics to Bacteria.
GPO. Available from the Superintendent of Documents, U.S.
Government Printing Office, Washington, D.C. 20402, 202-783-3238:
Standard Industrial Classification Manual (1972), and 1977
Supplement, republished in 1983.
“Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, USEPA Publication number SW-846 (Third Edition,
November, 1986), as amended by Updates I (July, 1992), II
(September, 1994), IIA (August, 1993), IIB (January, 1995), and
III (December, 1996) (Document Number 955-001-00000-1).
NACE. Available from the National Association of Corrosion
Engineers, 1400 South Creek Dr., Houston, TX 77084, 713-492-0535:
“Control of External Corrosion on Metallic Buried, Partially
Buried, or Submerged Liquid Storage Systems”, NACE
Recommended Practice RP-02-85, approved March, 1985.
34
NFPA. Available from the National Fire Protection Association,
Batterymarch Park, Boston, MA 02269, 617-770-3000 or 800-344-
3555:
“Flammable and Combustible Liquids Code” NFPA 30, issued
July 17, 1987. Also available from ANSI.
NTIS. Available from the U.S. Department of Commerce, National
Technical Information Service, 5285 Port Royal Road, Springfield, VA
22161, 703-487-4600:
APTI Course 415: Control of Gaseous Emissions, USEPA
Publication EPA-450/2-81-005, December, 1981.
“Generic Quality Assurance Project Plan for Land Disposal
Restrictions Program”, EPA/530-SW-87-011, March 15, 1987.
(Document number PB 88-170766.)
“Guideline on Air Quality Models”, Revised 1986. (Document
number PB86-245-248 (Guideline) and PB88-150-958
(Supplement), also set forth at 40 CFR 51, Appendix W).
“Methods for Chemical Analysis of Water and Wastes”, Third
Edition, March, 1983. (Document number PB 84-128677).
“Methods Manual for Compliance with BIF Regulations”,
December, 1990. (Document number PB91-120-006).
“Petitions to Delist Hazardous Wastes -- A Guidance Manual,
Second Edition”, EPA/530-R-93-007, March, 1993. (Document
Number PB 93-169 365).
“Screening Procedures for Estimating the Air Quality Impact of
Stationary Sources”, October, 1992, Publication Number EPA-
450/R-92-019.
“Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, USEPA Publication number SW-846 (Third Edition,
November, 1986), as amended by Updates I (July, 1992), II
(September, 1994), IIA (August, 1993), IIB (January, 1995), and
III (December, 1996) (Document Number 955-001-00000-1).
OECD. Organisation for Economic Co-operation and Development,
Environment Directorate, 2 rue Andre Pascal, 75775 Paris Cedex 16,
France):
35
OECD Guideline for Testing of Chemicals, Method 301B: “CO2
Evolution (Modified Sturm Test)”, adopted 17 July 1992.
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) of 27 May 1988.
STI. Available from the Steel Tank Institute, 728 Anthony Trail,
Northbrook, IL 60062, 708-498-1980:
“Standard for Dual Wall Underground Steel Storage Tanks”
(1986).
U.S. DOD. Available from the United States Department of Defense:
“DOD Ammunition and Explosive Safety Standards” (DOD
6055.9-STD), as in effect on November 8, 1995.
The Motor Vehicle Inspection Report (DD Form 626), as in
effect on November 8, 1995.
Requisition Tracking Form (DD Form 1348), as in effect on
November 8, 1995.
The Signature and Talley Record (DD Form 1907), as in effect
on November 8, 1995.
Special Instructions for Motor Vehicle Drivers (DD Form 836),
as in effect on November 8, 1995.
USEPA. Available from United States Environmental Protection
Agency, Office of Drinking Water, State Programs Division, WH 550
E, Washington, D.C. 20460:
“Technical Assistance Document: Corrosion, Its Detection and
Control in Injection Wells”, EPA 570/9-87-002, August, 1987.
USEPA. Available from Receptor Analysis Branch, USEPA (MD-14),
Research Triangle Park, NC 27711:
“Screening Procedures for Estimating the Air Quality Impact of
Stationary Sources, Revised”, October, 1992, Publication
Number EPA-450/R-92-019.
36
USEPA. Available from RCRA Information Center (RIC), 1235
Jefferson-Davis Highway, first floor, Arlington, VA 22203 (Docket # F-
94-IEHF-FFFFF):
OECD Amber List of Wastes, Appendix 4 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1993).
OECD Green List of Wastes, Appendix 3 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1994).
OECD Red List of Wastes, Appendix 5 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1993).
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) (May 27, 1988).
U.S. GSA. Available from the United States Government Services
Administration:
Government Bill of Lading (GBL) (GSA Standard Form 1109),
as in effect on November 8, 1995.
b)
Code of Federal Regulations. Available from the Superintendent of Documents,
U.S. Government Printing Office, Washington, D.C. 20401, 202-783-3238:
10 CFR 20, Appendix B (1997)
40 CFR 51.100(ii) (1997)
40 CFR 51, Appendix W (1997)
40 CFR 52.741, Appendix B (1997)
40 CFR 60 (1997)
40 CFR 61, Subpart V (1997)
40 CFR 63 (1997), as amended at 63 Fed. Reg. 18504 (Apr. 15, 1998)
37
40 CFR 136 (1997), as corrected at 63 Fed. Reg. 38756 (July 20, 1998)
and 63 Fed. Reg. 44146 (Aug. 18, 1998) and amended at 62 Fed. Reg.
48394 (Sep. 15, 1997)
40 CFR 142 (1997)
40 CFR 220 (1997)
40 CFR 260.20 (1997)
40 CFR 264 (1997)
40 CFR 268.41 (1990)
40 CFR 268.Appendix IX (1997)
40 CFR 302.4, 302.5 and 302.6 (1997)
40 CFR 761 (1997)
49 CFR 171 (1997)
49 CFR 173 (1997)
49 CFR 178 (1997)
c)
Federal Statutes
Section 3004 of the Resource Conservation and Recovery Act (42
U.S.C. USC 6901 et seq.), as amended through December 31, 1987.
Sections 201(v), 201(w), and 360b(j) of the Federal Food, Drug, and
Cosmetic Act (FFDCA; 21 U.S.C. USC §§ 321(v), 321(w) & 512(j)),
as amended through October 25, 1994.
Section 1412 of the Department of Defense Authorization Act of 1986,
Pub. L. 99-145, 50 U.S.C. USC 1521(j)(1) (1997).
d)
This Section incorporates no later editions or amendments.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
38
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 721
IDENTIFICATION AND LISTING OF HAZARDOUS WASTE
SUBPART A: GENERAL PROVISIONS
Section
721.101
Purpose and Scope
721.102
Definition of Solid Waste
721.103
Definition of Hazardous Waste
721.104
Exclusions
721.105
Special Requirements for Hazardous Waste Generated by Small Quantity
Generators
721.106
Requirements for Recyclable Materials
721.107
Residues of Hazardous Waste in Empty Containers
721.108
PCB Wastes Regulated under TSCA
721.109
Requirements for Universal Waste
SUBPART B: CRITERIA FOR IDENTIFYING THE CHARACTERISTICS
OF HAZARDOUS WASTE AND FOR LISTING HAZARDOUS WASTES
Section
721.110
Criteria for Identifying the Characteristics of Hazardous Waste
721.111
Criteria for Listing Hazardous Waste
SUBPART C: CHARACTERISTICS OF HAZARDOUS WASTE
Section
721.120
General
721.121
Characteristic of Ignitability
721.122
Characteristic of Corrosivity
721.123
Characteristic of Reactivity
721.124
Toxicity Characteristic
SUBPART D: LISTS OF HAZARDOUS WASTE
Section
721.130
General
721.131
Hazardous Wastes From Nonspecific Sources
721.132
Hazardous Waste from Specific Sources
721.133
Discarded Commercial Chemical Products, Off-Specification Species, Container
Residues, and Spill Residues Thereof
721.135
Wood Preserving Wastes
721.138
Comparable or Syngas Fuel Exclusion
39
721.Appendix A
Representative Sampling Methods
721.Appendix B
Method 1311 Toxicity Characteristic Leaching Procedure (TCLP)
721.Appendix C
Chemical Analysis Test Methods
Table A
Analytical Characteristics of Organic Chemicals (Repealed)
Table B
Analytical Characteristics of Inorganic Species (Repealed)
Table C
Sample Preparation/Sample Introduction Techniques (Repealed)
721.Appendix G
Basis for Listing Hazardous Wastes
721.Appendix H
Hazardous Constituents
721.Appendix I
Wastes Excluded by Administrative Action
Table A
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22 from
Non-Specific Sources
Table B
Wastes Excluded by USEPA under 40 CFR 260.20 and 260.22 from
Specific Sources
Table C
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22 from
Commercial Chemical Products, Off-Specification Species, Container
Residues, and Soil Residues Thereof
Table D
Wastes Excluded by the Board by Adjusted Standard
721.Appendix J
Method of Analysis for Chlorinated Dibenzo-p-Dioxins and
Dibenzofurans (Repealed)
721.Appendix Z
Table to Section 721.102
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982;
amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982;
amended in R82-18, 51 PCB 31, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in
R82-19, 53 PCB 131, at 7 Ill. Reg. 13999, effective October 12, 1983; amended in R84-34,
61 PCB 247, at 8 Ill. Reg. 24562, effective December 11, 1984; amended in R84-9, at 9 Ill.
Reg. 11834, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 998, effective January
2, 1986; amended in R85-2 at 10 Ill. Reg. 8112, effective May 2, 1986; amended in R86-1 at
10 Ill. Reg. 14002, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20647,
effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6035, effective March 24,
1987; amended in R86-46 at 11 Ill. Reg. 13466, effective August 4, 1987; amended in R87-32
at 11 Ill. Reg. 16698, effective September 30, 1987; amended in R87-5 at 11 Ill. Reg. 19303,
effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2456, effective January 15,
1988; amended in R87-30 at 12 Ill. Reg. 12070, effective July 12, 1988; amended in R87-39
at 12 Ill. Reg. 13006, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 382,
effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18300, effective November
13, 1989; amended in R90-2 at 14 Ill. Reg. 14401, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16472, effective September 25, 1990; amended in R90-17 at 15 Ill.
Reg. 7950, effective May 9, 1991; amended in R90-11 at 15 Ill. Reg. 9332, effective June 17,
1991; amended in R91-1 at 15 Ill. Reg. 14473, effective September 30, 1991; amended in
R91-12 at 16 Ill. Reg. 2155, effective January 27, 1992; amended in R91-26 at 16 Ill. Reg.
2600, effective February 3, 1992; amended in R91-13 at 16 Ill. Reg. 9519, effective June 9,
40
1992; amended in R92-1 at 16 Ill. Reg. 17666, effective November 6, 1992; amended in R92-
10 at 17 Ill. Reg. 5650, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20568,
effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6741, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12175, effective July 29, 1994; amended in R94-17 at
18 Ill. Reg. 17490, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9522,
effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10963, effective August 1, 1996;
amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 275, effective December 16, 1997; amended
in R98-12 at 22 Ill. Reg. 7615, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at
22 Ill. Reg. 17531, effective September 28, 1998; amended in R98-21/R99-2/R99-7 at 22 Ill.
Reg. ________, effective ______________________.
SUBPART A: GENERAL PROVISIONS
Section 721.102
Definition of Solid Waste
a)
Solid waste.
1)
A solid waste is any discarded material that is not excluded by Section
721.104(a) or that is not excluded pursuant to 35 Ill. Adm. Code
720.130 and 720.131.
2)
A discarded material is any material that is:
A)
Abandoned, as explained in subsection (b) of this Section;
B)
Recycled, as explained in subsection (c) of this Section;
C)
Considered inherently waste-like, as explained in subsection (d)
of this Section; or
D)
A military munition identified as a solid waste in 35 Ill. Adm.
Code 726.302.
b)
Materials are solid waste if they are abandoned by being:
1)
Disposed of; or
2)
Burned or incinerated; or
3)
Accumulated, stored or treated (but not recycled) before or in lieu of
being abandoned by being disposed of, burned or incinerated.
c)
Materials are solid wastes if they are recycled--or accumulated, stored or treated
before recycling--as specified in subsections (c)(1) through (c)(4) of this Section
if they are:
41
1)
Used in a manner constituting disposal.
A)
Materials noted with a “yes” in column 1 of the table in Section
721.Appendix Z of this Part are solid wastes when they are:
i)
Applied to or placed on the land in a manner that
constitutes disposal; or
ii)
Used to produce products that are applied to or placed on
the land or are otherwise contained in products that are
applied to or placed on the land (in which cases the
product itself remains a solid waste).
B)
However, commercial chemical products listed in Section
721.133 are not solid wastes if they are applied to the land and
that is their ordinary manner of use.
2)
Burned for energy recovery.
A)
Materials noted with a “yes” in column 2 of the table in Section
721.Appendix Z of this Part are solid wastes when they are:
i)
Burned to recover energy;
ii)
Used to produce a fuel or are otherwise contained in fuels
(in which case the fuel itself remains a solid waste);
iii)
Contained in fuels (in which case the fuel itself remains a
solid waste).
B)
However, commercial chemical products listed in Section
721.133 are not solid wastes if they are themselves fuels.
3)
Reclaimed. Materials noted with a “yes” in column 3 of the table in
Section 721.Appendix Z of this Part are solid wastes when reclaimed
(except as provided under Section 721.104(a)(15)). Materials noted with
a “--” in column 3 of Appendix Z of this Part are not solid wastes when
reclaimed (except as provided under Section 721.104(a)(15)).
4)
Accumulated speculatively. Materials noted with “yes” in column 4 of
the table in Section 721.Appendix Z of this Part are solid wastes when
accumulated speculatively.
42
d)
Inherently waste-like materials. The following materials are solid wastes when
they are recycled in any manner:
1)
Hazardous waste numbers F020, F021 (unless used as an ingredient to
make a product at the site of generation), F022, F023, F026, and F028.
2)
Secondary materials fed to a halogen acid furnace that exhibit a
characteristic of a hazardous waste or are listed as a hazardous waste as
defined in Subpart C or D of this Part, except for brominated material
that meets the following criteria:
A)
The material must contain a bromine concentration of at least 45
percent;
B)
The material must contain less than a total of one percent of toxic
organic compounds listed in Section 721.Appendix H of this
Part; and
C)
The material is processed continually on-site in the halogen acid
furnace via direct conveyance (hard piping).
3)
The following criteria are used to add wastes to the list:
A)
Disposal method or toxicity.
i)
The materials are ordinarily disposed of, burned, or
incinerated; or
ii)
The materials contain toxic constituents listed in Section
721.Appendix H of this Part and these constituents are not
ordinarily found in raw materials or products for which
the materials substitute (or are found in raw materials or
products in smaller concentrations) and are not used or
reused during the recycling process; and
B)
The material may pose a substantial hazard to human health and
the environment when recycled.
e)
Materials that are not solid waste when recycled.
1)
Materials are not solid wastes when they can be shown to be recycled by
being:
A)
Used or reused as ingredients in an industrial process to make a
product, provided the materials are not being reclaimed; or
43
B)
Used or reused as effective substitutes for commercial products;
or
C)
Returned to the original process from which they are generated
without first being reclaimed. The materials must be returned as
a substitute for feedstock materials. In cases where the original
process to which the material is returned is a secondary process,
the materials must be managed so there is no placement on the
land.
C)
In cases where the materials are generated and reclaimed within
the primary mineral processing industry, the conditions of the
exclusion found at Section 721.104(a)(15) apply rather than this
provision.
2)
The following materials are solid wastes, even if the recycling involves
use, reuse, or return to the original process (described in subsections
(e)(1)(A) through (e)(1)(C) of this Section):
A)
Materials used in a manner constituting disposal or used to
produce products that are applied to the land; or
B)
Materials burned for energy recovery, used to produce a fuel, or
contained in fuels; or
C)
Materials accumulated speculatively; or
D)
Materials listed in subsections (d)(1) and (d)(2) of this Section.
f)
Documentation of claims that materials are not solid wastes or are conditionally
exempt from regulation. Respondents in actions to enforce regulations
implementing Subtitle C of RCRA or Section 21 of the Environmental
Protection Act that raise a claim that a certain material is not a solid waste or
that the material is conditionally exempt from regulation must demonstrate that
there is a known market or disposition for the material and that they meet the
terms of the exclusion or exemption. In doing so, the person must provide
appropriate documentation (such as contracts showing that a second person uses
the material as an ingredient in a production process) to demonstrate that the
material is not a waste or that the material is exempt from regulation. In
addition, owners or operators of facilities claiming that they actually are
recycling materials must show that they have the necessary equipment to do so.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
44
Section 721.103
Definition of Hazardous Waste
a)
A solid waste, as defined in Section 721.102, is a hazardous waste if:
1)
It is not excluded from regulation as a hazardous waste under Section
721.104(b); and
2)
It meets any of the following criteria:
A)
It exhibits any of the characteristics of hazardous waste identified
in 721.Subpart C of this Part. However, any mixture of a waste
from the extraction, beneficiation, and processing of ores and
minerals excluded under Section 721.104(b)(7) and any other
solid waste exhibiting a characteristic of hazardous waste under
Subpart C of this Part is a hazardous waste only if it exhibits a
characteristic that would not have been exhibited by the excluded
waste alone if such mixture had not occurred, or if the mixture
continues to exhibit any of the characteristics exhibited by the
non-excluded wastes prior to mixture. Further, for the purposes
of applying the toxicity characteristic to such mixtures, the
mixture is also a hazardous waste if it exceeds the maximum
concentration for any contaminant listed in Section 721.124 that
would not have been exceeded by the excluded waste alone if the
mixture had not occurred or if it continues to exceed the
maximum concentration for any contaminant exceeded by the
nonexempt waste prior to mixture.
i)
Except that any mixture of a waste from the extraction,
beneficiation, or processing of ores or minerals excluded
under Section 721.104(b)(7) and any other solid waste
exhibiting a characteristic of hazardous waste under
721.Subpart C is a hazardous waste only: if it exhibits a
characteristic that would not have been exhibited by the
excluded waste alone if such mixture had not occurred, or
if it continues to exhibit any of the characteristics
exhibited by the non-excluded wastes prior to mixture.
ii)
Further, for the purposes of applying the toxicity
characteristic to such mixtures under subsection
(a)(2)(A)(i) above, the mixture is also a hazardous waste:
if it exceeds the maximum concentration for any
contaminant listed in Section 721.124 that would not have
been exceeded by the excluded waste alone if the mixture
had not occurred, or if it continues to exceed the
45
maximum concentration for any contaminant exceeded by
the nonexempt waste prior to mixture.
B)
It is listed in 721.Subpart D of this Part and has not been
excluded from the lists in 721.Subpart D of this Part under 35 Ill.
Adm. Code 720.120 and 720.122.
C)
It is a mixture of a solid waste and a hazardous waste that is
listed in 721.Subpart D of this Part solely because it exhibits one
or more of the characteristics of hazardous waste identified in
721.Subpart C of this Part, unless: the resultant mixture no
longer exhibits any characteristic of hazardous waste identified in
Subpart C of this Part, or unless the solid waste is excluded from
regulation under Section 721.104(b)(7) and the resultant mixture
no longer exhibits any characteristic of hazardous waste identified
in Subpart C of this Part for which the hazardous waste listed in
Subpart D of this Part was listed. (However, nonwastewater
mixtures are still subject to the requirements of 35 Ill. Adm.
Code 728, even if they no longer exhibit a characteristic at the
point of land disposal.)
i)
the resultant mixture no longer exhibits any characteristic
of hazardous waste identified in 721.Subpart C, or
ii)
the solid waste is excluded from regulation under Section
721.104(b)(7) and the resultant mixture no longer exhibits
any characteristic of hazardous waste identified in
721.Subpart C for which the hazardous waste listed in
721.Subpart D was listed.
iii)
Nonwastewater mixtures are still subject to the
requirements of 35 Ill. Adm. Code 728, even if they no
longer exhibit a characteristic at the point of land
disposal.
D)
It is a mixture of solid waste and one or more hazardous wastes
listed in 721.Subpart D of this Part and has not been excluded
from this subsection (a)(2) under 35 Ill. Adm. Code 720.120 and
720.122; however, the following mixtures of solid wastes and
hazardous wastes listed in 721.Subpart D of this Part are not
hazardous wastes (except by application of subsection (a)(2)(A)
or (a)(2)(B) above of this Section) if the generator demonstrates
that the mixture consists of wastewater the discharge of which is
subject to regulation under either 35 Ill. Adm. Code 309 or 310
46
(including wastewater at facilities that have eliminated the
discharge of wastewater) and:
i)
One or more of the following solvents listed in Section
721.131: carbon tetrachloride, tetrachloroethylene,
trichloroethylene, provided that the maximum total
weekly usage of these solvents (other than the amounts
that can be demonstrated not to be discharged to
wastewater) divided by the average weekly flow of
wastewater into the headworks of the facility’s wastewater
treatment or pretreatment system does not exceed 1 part
per million;
ii)
One or more of the following spent solvents listed in
Section 721.131: methylene chloride, 1,1,1-trichloro-
ethane, chlorobenzene, o-dichlorobenzene, cresols,
cresylic acid, nitrobenzene, toluene, methyl ethyl ketone,
carbon disulfide, isobutanol, pyridine, spent chlorofluoro-
carbon solvents, provided that the maximum total weekly
usage of these solvents (other than the amounts that can be
demonstrated not to be discharged to wastewater) divided
by the average weekly flow of wastewater into the
headworks of the facility’s wastewater treatment or
pretreatment system does not exceed 25 parts per million;
iii)
One of the following wastes listed in Section 721.132,
provided that the wastes are discharged to the refinery oil
recovery sewer before primary oil/water/solids
separation: heat exchanger bundle cleaning sludge from
the petroleum refining industry (USEPA hazardous waste
no. K050), crude oil storage tank sediment from
petroleum refining operations (USEPA hazardous waste
number K169), clarified slurry oil tank sediment and/or
in-line filter/separation solids from petroleum refining
operations (USEPA hazardous waste number K170), spent
hydrotreating catalyst (USEPA hazardous waste number
K171), and spent hydrorefining catalyst (USEPA
hazardous waste number K172);
iv)
A discarded commercial chemical product or chemical
intermediate listed in Section 721.133 arising from de
minimis losses of these materials from manufacturing
operations in which these materials are used as raw
materials or are produced in the manufacturing process.
For purposes of this subsection, “de minimis” losses
47
include those from normal material handling operations
(e.g., spills from the unloading or transfer of materials
from bins or other containers, leaks from pipes, valves, or
other devices used to transfer materials); minor leaks of
process equipment, storage tanks, or containers; leaks
from well-maintained pump packings and seals; sample
purgings; relief device discharges; discharges from safety
showers and rinsing and cleaning of personal safety
equipment; and rinsate from empty containers or from
containers that are rendered empty by that rinsing;
v)
Wastewater resulting from laboratory operations
containing toxic (T) wastes listed in 721.Subpart D of this
Part, provided that the annualized average flow of
laboratory wastewater does not exceed one percent of total
wastewater flow into the headworks of the facility’s
wastewater treatment or pretreatment system or provided
that the wastes’ combined annualized average
concentration does not exceed one part per million in the
headworks of the facility’s wastewater treatment or
pretreatment facility. Toxic (T) wastes used in
laboratories that are demonstrated not to be discharged to
wastewater are not to be included in this calculation;
vi)
One or more of the following wastes listed in Section
721.132: wastewaters from the production of carbamates
and carbamoyl oximes (USEPA Hazardous Waste No.
K157), provided that the maximum weekly usage of
formaldehyde, methyl chloride, methylene chloride, and
triethylamine (including all amounts that cannot be
demonstrated to be reacted in the process, destroyed
through treatment, or recovered, i.e., what is discharged
or volatilized) divided by the average weekly flow of
process wastewater prior to any dilutions into the
headworks of the facility’s wastewater treatment system
does not exceed a total of 5 parts per million by weight;
or
vii)
Wastewaters derived from the treatment of one or more of
the following wastes listed in Section 721.132: organic
waste (including heavy ends, still bottoms, light ends,
spent solvents, filtrates, and decantates) from the
production of carbamates and carbamoyl oximes (USEPA
Hazardous Waste No. K156), provided, that the
maximum concentration of formaldehyde, methyl
48
chloride, methylene chloride, and triethylamine prior to
any dilutions into the headworks of the facility’s
wastewater treatment system does not exceed a total of 5
milligrams per liter.
E)
Rebuttable presumption for used oil. Used oil containing more
than 1,000 ppm total halogens is presumed to be a hazardous
waste because it has been mixed with halogenated hazardous
waste listed in 721.Subpart D of this Part. Persons may rebut
this presumption by demonstrating that the used oil does not
contain hazardous waste (for example, by using an analytical
method from SW-846, incorporated by reference at 35 Ill. Adm.
Code 720.111, to show that the used oil does not contain
significant concentrations of halogenated hazardous constituents
listed in 721.Appendix H of this Part).
i)
The rebuttable presumption does not apply to
metalworking oils or fluids containing chlorinated
paraffins if they are processed through a tolling
arrangement as described in 35 Ill. Adm. Code
739.124(c) to reclaim metalworking oils or fluids. The
presumption does apply to metalworking oils or fluids if
such oils or fluids are recycled in any other manner, or
disposed.
ii)
The rebuttable presumption does not apply to used oils
contaminated with chlorofluorocarbons (CFCs) removed
from refrigeration units where the CFCs are destined for
reclamation. The rebuttable presumption does apply to
used oils contaminated with CFCs that have been mixed
with used oil from sources other than refrigeration units.
b)
A solid waste that is not excluded from regulation under subsection (a)(1) above
of this Section becomes a hazardous waste when any of the following events
occur:
1)
In the case of a waste listed in 721.Subpart D of this Part, when the
waste first meets the listing description set forth in 721.Subpart D of this
Part.
2)
In the case of a mixture of solid waste and one or more listed hazardous
wastes, when a hazardous waste listed in 721.Subpart D of this Part is
first added to the solid waste.
49
3)
In the case of any other waste (including a waste mixture), when the
waste exhibits any of the characteristics identified in 721.Subpart C of
this Part.
c)
Unless and until it meets the criteria of subsection (d) below of this Section, a
hazardous waste will remain a hazardous waste.
BOARD NOTE: This subsection corresponds with 40 CFR 261.3(c)(1). The
Board has codified 40 CFR 261.3(c)(2) at subsection (e) below of this Section.
d)
Any solid waste described in subsection (c) above of this Section is not a
hazardous waste if it meets the following criteria:
1)
In the case of any solid waste, it does not exhibit any of the
characteristics of hazardous waste identified in 721.Subpart C of this
Part. (However, wastes that exhibit a characteristic at the point of
generation may still be subject to the requirements of 35 Ill. Adm. Code
728, even if they no longer exhibit a characteristic at the point of land
disposal.)
2)
In the case of a waste that is a listed waste under 721.Subpart D of this
Part, a waste that contains a waste listed under 721.Subpart D of this
Part, or a waste that is derived from a waste listed in 721.Subpart D of
this Part, it also has been excluded from subsection (c) above of this
Section under 35 Ill. Adm. Code 720.120 and 720.122.
e)
Specific inclusions and exclusions.
1)
Except as otherwise provided in subsection (e)(2) below of this Section,
any solid waste generated from the treatment, storage, or disposal of a
hazardous waste, including any sludge, spill residue, ash, emission
control dust, or leachate (but not including precipitation run-off), is a
hazardous waste. (However, materials that are reclaimed from solid
wastes and that are used beneficially are not solid wastes and hence are
not hazardous wastes under this provision unless the reclaimed material
is burned for energy recovery or used in a manner constituting disposal.)
2)
The following solid wastes are not hazardous even though they are
generated from the treatment, storage, or disposal of a hazardous waste
unless they exhibit one or more of the characteristics of hazardous waste:
A)
Waste pickle liquor sludge generated by lime stabilization of
spent pickle liquor from the iron and steel industry (SIC Codes
331 and 332).
50
B)
Wastes from burning any of the materials exempted from
regulation by any of Section Section 721.106(a)(3)(DC) through
and (a)(3)(FD).
C)
Nonwastewater residues, such as slag, resulting from high
temperature metal recovery (HTMR) processing of K061, K062,
or F006 waste in the units identified in this subsection that are
disposed of in non-hazardous waste units, provided that these
residues meet the generic exclusion levels identified in the tables
in this subsection for all constituents and the residues exhibit no
characteristics of hazardous waste. The types of units identified
are rotary kilns, flame reactors, electric furnaces, plasma arc
furnaces, slag reactors, rotary hearth furnace/electric furnace
combinations, or the following types of industrial furnaces (as
defined in 35 Ill. Adm. Code 720.110): blast furnaces, smelting,
melting and refining furnaces (including pyrometallurgical
devices such as cupolas, reverberator furnaces, sintering
machines, roasters, and foundry furnaces), and other furnaces
designated by the Agency pursuant to that definition.
i)
Testing requirements must be incorporated in a facility’s
waste analysis plan or a generator’s self-implementing
waste analysis plan; at a minimum, composite samples of
residues must be collected and analyzed quarterly and
when the process or operation generating the waste
changes.
ii)
Persons claiming this exclusion in an enforcement action
will have the burden of proving by clear and convincing
evidence that the material meets all of the exclusion
requirements. The generic exclusion levels are:
Constituent
Maximum for any single
composite sample (mg/L)
Generic exclusion levels for K061 and K062
nonwastewater HTMR residues.
Antimony
0.10
Arsenic
0.50
Barium
7.6
Beryllium
0.010
Cadmium
0.050
Chromium (total)
0.33
Lead
0.15
51
Mercury
0.009
Nickel
1.0
Selenium
0.16
Silver
0.30
Thallium
0.020
Vanadium
1.26
Zinc
70
Generic exclusion levels for F006 nonwastewater HTMR
residues
Antimony
0.10
Arsenic
0.50
Barium
7.6
Beryllium
0.010
Cadmium
0.050
Chromium (total)
0.33
Cyanide (total) (mg/kg)
1.8
Lead
0.15
Mercury
0.009
Nickel
1.0
Selenium
0.16
Silver
0.30
Thallium
0.020
Zinc
70
iii)
A one-time notification and certification must be placed in
the facility’s files and sent to the Agency (or, for out-of-
State shipments, to the appropriate Regional
Administrator of USEPA or the state agency authorized to
implement 40 CFR 268 requirements) for K061, K062, or
F006 HTMR residues that meet the generic exclusion
levels for all constituents and do not exhibit any
characteristics and which are sent to RCRA Subtitle D
(municipal solid waste landfill) units. The notification
and certification that is placed in the generator’s or
treater’s files must be updated if the process or operation
generating the waste changes or if the RCRA Subtitle D
unit receiving the waste changes. However, the generator
or treater need only notify the Agency on an annual basis
if such changes occur. Such notification and certification
should be sent to the Agency by the end of the calendar
year, but no later than December 31. The notification
must include the following information: the name and
address of the nonhazardous waste management unit
52
receiving the waste shipment; the USEPA hazardous
waste number and treatability group at the initial point of
generation; and the treatment standards applicable to the
waste at the initial point of generation. The certification
must be signed by an authorized representative and must
state as follows:
“I certify under penalty of law that the generic
exclusion levels for all constituents have been met
without impermissible dilution and that no
characteristic of hazardous waste is exhibited. I
am aware that there are significant penalties for
submitting a false certification, including the
possibility of fine and imprisonment.”
BOARD NOTE: This subsection would normally correspond with 40 CFR
261.3(e), a subsection which has been deleted and marked “reserved” by
USEPA. Rather, this subsection corresponds with 40 CFR 261.3(c)(2), which
the Board codified here to comport with codification requirements and enhance
clarity.
D)
Biological treatment sludge from the treatment of one of the
following wastes listed in Section 721.132: organic waste
(including heavy ends, still bottoms, light ends, spent solvents,
filtrates, and decantates) from the production of carbamates and
carbamoyl oximes (USEPA Hazardous Waste No. K156) and
wastewaters from the production of carbamates and carbamoyl
oximes (USEPA Hazardous Waste No. K157).
E)
Catalyst inert support media separated from one of the following
wastes listed in Section 721.132: spent hydrotreating catalyst
(USEPA hazardous waste number K171) and spent hydrorefining
catalyst (USEPA hazardous waste number K172).
BOARD NOTE: This subsection would normally correspond with 40 CFR
261.3(e), a subsection which has been deleted and marked “reserved” by
USEPA. Rather, this subsection (e) corresponds with 40 CFR 261.3(c)(2),
which the Board codified here to comport with codification requirements and to
enhance clarity.
f)
Notwithstanding subsections (a) through (e) above of this Section and provided
the debris, as defined in 35 Ill. Adm. Code 728.102, does not exhibit a
characteristic identified at 721.Subpart C of this Part, the following materials
are not subject to regulation under 35 Ill. Adm. Code 720, 721 to 726, 728, or
730:
53
1)
Hazardous debris as defined in 35 Ill. Adm. Code 728.102 that has been
treated using one of the required extraction or destruction technologies
specified in 35 Ill. Adm. Code 728.Table F; persons claiming this
exclusion in an enforcement action will have the burden of proving by
clear and convincing evidence that the material meets all of the exclusion
requirements; or
2)
Debris as defined in 35 Ill. Adm. Code 728.102 that the Agency,
considering the extent of contamination, has determined is no longer
contaminated with hazardous waste.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.104
Exclusions
a)
Materials that are not solid wastes. The following materials are not solid wastes
for the purpose of this Part:
1)
Sewage:
A)
Domestic sewage (untreated sanitary wastes that pass through a
sewer system); and
B)
Any mixture of domestic sewage and other waste that passes
through a sewer system to publicly-owned treatment works for
treatment.
2)
Industrial wastewater discharges that are point source discharges with
National Pollutant Discharge Elimination System (NPDES) permits
issued by the Agency pursuant to Section 12(f) of the Environmental
Protection Act and 35 Ill. Adm. Code 309.
BOARD NOTE: This exclusion applies only to the actual point source
discharge. It does not exclude industrial wastewaters while they are
being collected, stored, or treated before discharge, nor does it exclude
sludges that are generated by industrial wastewater treatment.
3)
Irrigation return flows.
4)
Source, special nuclear, or by-product material as defined by the Atomic
Energy Act of 1954, as amended (42 U.S.C. 2011 et seq.).
5)
Materials subjected to in-situ mining techniques that are not removed
from the ground as part of the extraction process.
54
6)
Pulping liquors (i.e., black liquors) that are reclaimed in a pulping
liquor recovery furnace and then reused in the pulping process, unless
accumulated speculatively, as defined in Section 721.101(c).
7)
Spent sulfuric acid used to produce virgin sulfuric acid unless it is
accumulated speculatively, as defined in Section 721.101(c).
8)
Secondary materials that are reclaimed and returned to the original
process or processes in which they were generated where they are reused
in the production process, provided:
A)
Only tank storage is involved, and the entire process through
completion of reclamation is closed by being entirely connected
with pipes or other comparable enclosed means of conveyance;
B)
Reclamation does not involve controlled flame combustion (such
as occurs in boilers, industrial furnaces or incinerators);
C)
The secondary materials are never accumulated in such tanks for
over twelve months without being reclaimed; and
D)
The reclaimed material is not used to produce a fuel or used to
produce products that are used in a manner constituting disposal.
9)
Wood preserving wastes.
A)
Spent wood preserving solutions that have been used and which
are reclaimed and reused for their original intended purpose; and
B)
Wastewaters from the wood preserving process that have been
reclaimed and which are reused to treat wood.; and
C)
Prior to reuse, the wood preserving wastewaters and spent wood
preserving solutions described in subsections (a)(9)(A) and
(a)(9)(B) of this Section, so long as they meet all of the following
conditions:
i)
The wood preserving wastewaters and spent wood
preserving solutions are reused on-site at water borne
plants in the production process for their original intended
purpose;
55
ii)
Prior to reuse, the wastewaters and spent wood preserving
solutions are managed to prevent release to either land or
groundwater or both;
iii)
Any unit used to manage wastewaters or spent wood
preserving solutions prior to reuse can be visually or
otherwise determined to prevent such releases;
iv)
Any drip pad used to manage the wastewaters or spent
wood preserving solutions prior to reuse complies with the
standards in 35 Ill. Adm. Code 725.Subpart W, regardless
of whether the plant generates a total of less than 100
kg/month of hazardous waste; and
v)
Prior to operating pursuant to this exclusion, the plant
owner or operator submits a one-time notification to the
Agency stating that the plant intends to claim the
exclusion, giving the date on which the plant intends to
begin operating under the exclusion, and containing the
following language: “I have read the applicable
regulation establishing an exclusion for wood preserving
wastewaters and spent wood preserving solutions and
understand it requires me to comply at all times with the
conditions set out in the regulation.” The plant must
maintain a copy of that document in its on-site records for
a period of no less than three years from the date specified
in the notice. The exclusion applies only so long as the
plant meets all of the conditions. If the plant goes out of
compliance with any condition, it may apply to the Agency for
reinstatement. The Agency shall reinstate the exclusion in
writing if it finds that the plant has returned to compliance with
all conditions and that violations are not likely to recur. If the
Agency denies an application, it shall transmit to the
applicant specific, detailed statements in writing as to the
reasons it denied the application. The applicant under this
subsection (a)(9)(C)(v) may appeal the Ageny’s
determination to deny the reinstatement, to grant the
reinstatement with conditions, or to terminate a
reinstatement before the Board pursuant to Section 40 of
the Act [415 ILCS 5/40].
10)
Hazardous waste numbers K060, K087, K141, K142, K143, K144,
K145, K147, and K148, and any wastes from the coke by-products
processes that are hazardous only because they exhibit the toxicity
characteristic specified in Section 721.124, when subsequent to
generation these materials are recycled to coke ovens, to the tar recovery
56
process as a feedstock to produce coal tar, or are mixed with coal tar
prior to the tar’s sale or refining. This exclusion is conditioned on there
being no land disposal of the waste from the point it is generated to the
point it is recycled to coke ovens, to tar recovery, to the tar refining
processes, or prior to when it is mixed with coal.
11)
Nonwastewater splash condenser dross residue from the treatment of
hazardous waste number K061 in high temperature metals recovery
units, provided it is shipped in drums (if shipped) and not land disposed
before recovery.
12)
Recovered oil from petroleum refining, exploration, and production and
from transportation incident thereto that is to be inserted into the
petroleum refining process (SIC Code 2911) at or before a point (other
than direct insertion into a coker) where contaminants are removed.
This exclusion applies to recovered oil stored or transported prior to
insertion, except that the oil must not be stored in a manner involving
placement on the land and the oil must not be accumulated speculatively
before being recycled. Recovered oil is oil that has been reclaimed from
secondary materials (such as wastewater) generated from normal
petroleum refining, exploration, and production, and from transportation
practices. Recovered oil includes oil that is recovered from refinery
wastewater collection and treatment systems, oil recovered from oil and
gas drilling operations, and oil recovered from wastes removed from
crude oil storage tanks. Recovered oil does not include (among other
things) oil-bearing hazardous wastes listed in Subpart D of this Part
(e.g., K048 through K052, F037, and F038). However, oil recovered
from such wastes may be considered recovered oil. Recovered oil also
does not include used oil as defined in 35 Ill. Adm. Code
739.100.Certain oil-bearing hazardous secondary materials and
recovered oil, as follows:
A)
Oil-bearing hazardous secondary materials (i.e., sludges,
byproducts, or spent materials) that are generated at a petroleum
refinery (standard industrial classification (SIC code 2911) and
are inserted into the petroleum refining process (SIC code 2911:
including, but not limited to, distillation, catalytic cracking,
fractionation, or thermal cracking units (i.e., cokers)) unless the
material is placed on the land, or speculatively accumulated
before being so recycled. Materials inserted into thermal
cracking units are excluded under this subsection (a)(12),
provided that the coke product also does not exhibit a
characteristic of hazardous waste. Oil-bearing hazardous
secondary materials may be inserted into the same petroleum
refinery where they are generated or sent directly to another
57
petroleum refinery and still be excluded under this provision.
Except as provided in subsection (a)(12)(B) of this Section, oil-
bearing hazardous secondary materials generated elsewhere in the
petroleum industry (i.e., from sources other than petroleum
refineries) are not excluded under this section. Residuals
generated from processing or recycling materials excluded under
this subsection (a)(12)(A), where such materials as generated
would have otherwise met a listing under Subpart D of this Part,
are designated as USEPA hazardous waste number F037 listed
wastes when disposed of or intended for disposal.
B)
Recovered oil that is recycled in the same manner and with the
same conditions as described in subsection (a)(12)(A) of this
Section. Recovered oil is oil that has been reclaimed from
secondary materials (including wastewater) generated from
normal petroleum industry practices, including refining,
exploration and production, bulk storage, and transportation
incident thereto (SIC codes 1311, 1321, 1381, 1382, 1389, 2911,
4612, 4613, 4922, 4923, 4789, 5171, and 5172). Recovered oil
does not include oil-bearing hazardous wastes listed in Subpart D
of this Part; however, oil recovered from such wastes may be
considered recovered oil. Recovered oil does not include used
oil, as defined in 35 Ill. Adm. Code 739.100.
13)
Excluded scrap metal (processed scrap metal, unprocessed home scrap
metal, and unprocessed prompt scrap metal) being recycled.
14)
Shredded circuit boards being recycled, provided that they meet the
following conditions:
A)
The circuit boards are stored in containers sufficient to prevent a
release to the environment prior to recovery; and
B)
The circuit boards are free of mercury switches, mercury relays
and nickel-cadmium batteries and lithium batteries.
15)
Condensates derived from the overhead gases from kraft mill steam
strippers that are used to comply with federal Clean Air Act regulation 40
CFR 63.446(e). The exemption applies only to combustion at the mill
generating the condensates.
16)
Secondary materials (i.e., sludges, by-products, and spent materials as
defined in Section 721.101) (other than hazardous wastes listed in
Subpart D of this Part) generated within the primary mineral processing
industry from which minerals, acids, cyanide, water, or other values are
recovered by mineral processing, provided that:
58
A)
The secondary material is legitimately recycled to recover
minerals, acids, cyanide, water, or other values;
B)
The secondary material is not accumulated speculatively;
C)
Except as provided in subsection (a)(16)(D) of this Section, the
secondary material is stored in tanks, containers, or buildings that
meet the following minimum integrity standards: a building must
be an engineered structure with a floor, walls, and a roof all of
which are made of non-earthen materials providing structural
support (except that smelter buildings may have partially earthen
floors, provided that the secondary material is stored on the non-
earthen portion), and have a roof suitable for diverting rainwater
away from the foundation; a tank must be free standing, not be a
surface impoundment (as defined in 35 Ill. Adm. Code 720.110),
and be manufactured of a material suitable for containment of its
contents; a container must be free standing and be manufactured
of a material suitable for containment of its contents. If a tank or
container contains any particulate which may be subject to wind
dispersal, the owner or operator must operate the unit in a
manner that controls fugitive dust. A tank, container, or building
must be designed, constructed and operated to prevent significant
releases to the environment of these materials.
D)
The Agency shall allow by permit that solid mineral processing
secondary materials only may be placed on pads, rather than in
tanks, containers, or buildings if the facility owner or operator
can demonstrate the following: the solid mineral processing
secondary materials do not contain any free liquid; the pads are
designed, constructed, and operated to prevent significant
releases of the secondary material into the environment; and the
pads provide the same degree of containment afforded by the
non-RCRA tanks, containers, and buildings eligible for
exclusion.
i)
The Agency shall also consider whether storage on pads
poses the potential for significant releases via
groundwater, surface water, and air exposure pathways.
Factors to be considered for assessing the groundwater,
surface water, and air exposure pathways must include the
following: the volume and physical and chemical
properties of the secondary material, including its
potential for migration off the pad; the potential for
human or environmental exposure to hazardous
59
constituents migrating from the pad via each exposure
pathway; and the possibility and extent of harm to human
and environmental receptors via each exposure pathway.
ii)
Pads must meet the following minimum standards: they
must be designed of non-earthen material that is
compatible with the chemical nature of the mineral
processing secondary material; they must be capable of
withstanding physical stresses associated with placement
and removal; they must have run on/runoff controls; they
must be operated in a manner which controls fugitive
dust; and they must have integrity assurance through
inspections and maintenance programs.
iii)
Before making a determination under this subsection
(a)(16)(D), the Agency shall provide notice and the
opportunity for comment to all persons potentially
interested in the determination. This can be accomplished
by placing notice of this action in major local newspapers,
or broadcasting notice over local radio stations.
BOARD NOTE: See 35 Ill. Adm. Code 703.Subpart D
for the RCRA Subtitle C permit public notice
requirements.
E)
The owner or operator provides a notice to the Agency,
identifying the following information: the types of materials to
be recycled, the type and location of the storage units and
recycling processes, and the annual quantities expected to be
placed in land-based units. This notification must be updated
when there is a change in the type of materials recycled or the
location of the recycling process.
F)
For purposes of subsection (b)(7) of this Section, mineral
processing secondary materials must be the result of mineral
processing and may not include any listed hazardous wastes.
Listed hazardous wastes and characteristic hazardous wastes
generated by non-mineral processing industries are not eligible
for the conditional exclusion from the definition of solid waste.
17)
Comparable fuels or comparable syngas fuels (i.e., comparable or
syngas fuels) that meet the requirements of Section 721.138.
18)
Petrochemical recovered oil from an associated organic chemical
manufacturing facility, where the oil is to be inserted into the petroleum
60
refining process (SIC code 2911) along with normal petroleum refinery
process streams, provided that both of the following conditions are true
of the oil:
A)
The oil is hazardous only because it exhibits the characteristic of
ignitability (as defined in Section 721.121) or toxicity for
benzene (Section 721.124, USEPA hazardous waste code D018);
B
The oil generated by the organic chemical manufacturing
facility is not placed on the land, or speculatively
accumulated before being recycled into the petroleum
refining process. An “associated organic chemical
manufacturing facility” is a facility for which all of the
following is true: its primary SIC code is 2869, but its
operations may also include SIC codes 2821, 2822, and
2865; it is physically co-located with a petroleum
refinery; and the petroleum refinery to which the oil being
recycled is returned also provides hydrocarbon feedstocks
to the organic chemical manufacturing facility.
“Petrochemical recovered oil” is oil that has been
reclaimed from secondary materials (i.e., sludges,
byproducts, or spent materials, including wastewater)
from normal organic chemical manufacturing operations,
as well as oil recovered from organic chemical
manufacturing processes.
19)
Spent caustic solutions from petroleum refining liquid treating processes
used as a feedstock to produce cresylic or naphthenic acid unless the
material is placed on the land, or accumulated speculatively as defined in
Section 721.101(c).
b)
Solid wastes that are not hazardous wastes. The following solid wastes are not
hazardous wastes:
1)
Household waste, including household waste that has been collected,
transported, stored, treated, disposed, recovered (e.g., refuse-derived
fuel), or reused. “Household waste” means any waste material
(including garbage, trash, and sanitary wastes in septic tanks) derived
from households (including single and multiple residences, hotels, and
motels, bunkhouses, ranger stations, crew quarters, campgrounds, picnic
grounds, and day-use recreation areas). A resource recovery facility
managing municipal solid waste shall not be deemed to be treating,
storing, disposing of, or otherwise managing hazardous wastes for the
purposes of regulation under this Part, if such facility:
61
A)
Receives and burns only:
i)
Household waste (from single and multiple dwellings,
hotels, motels, and other residential sources); and
ii)
Solid waste from commercial or industrial sources that
does not contain hazardous waste; and
B)
Such facility does not accept hazardous waste and the owner or
operator of such facility has established contractual requirements
or other appropriate notification or inspection procedures to
assure that hazardous wastes are not received at or burned in such
facility.
BOARD NOTE: The U.S. Supreme Court determined, in City of
Chicago v. Environmental Defense Fund, Inc., 511 U.S. 328, 114 S.
Ct. 1588, 128 L. Ed. 2d 302 (1994), that this exclusion and RCRA
section 3001(i) (42 U.S.C. § USC 6921(i)) do not exclude the ash from
facilities covered by this subsection from regulation as a hazardous
waste. At 59 Fed. Reg. 29372 (June 7, 1994), USEPA granted facilities
managing ash from such facilities that is determined a hazardous waste
under Subpart C of this Part until December 7, 1994 to file a Part A
permit application pursuant to 35 Ill. Adm. Code 703.181. At 60 Fed.
Reg. 6666 (Feb. 3, 1995), USEPA stated that it interpreted that the point
at which ash becomes subject to RCRA Subtitle C regulation is when
that material leaves the combustion building (including connected air
pollution control equipment).
2)
Solid wastes generated by any of the following that are returned to the
soil as fertilizers:
A)
The growing and harvesting of agricultural crops, or
B)
The raising of animals, including animal manures.
3)
Mining overburden returned to the mine site.
4)
Fly ash waste, bottom ash waste, slag waste, and flue gas emission
control waste generated primarily from the combustion of coal or other
fossil fuels, except as provided in 35 Ill. Adm. Code 726.212 for
facilities that burn or process hazardous waste.
5)
Drilling fluids, produced waters, and other wastes associated with the
exploration, development, or production of crude oil, natural gas, or
geothermal energy.
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6)
Chromium wastes:
A)
Wastes that fail the test for the toxicity characteristic (Sections
721.124 and 721.Appendix B) because chromium is present or
which are listed in Subpart D of this Part due to the presence of
chromium, that do not fail the test for the toxicity characteristic
for any other constituent or which are not listed due to the
presence of any other constituent, and that do not fail the test for
any other characteristic, if it is shown by a waste generator or by
waste generators that:
i)
The chromium in the waste is exclusively (or nearly
exclusively) trivalent chromium;
ii)
The waste is generated from an industrial process that uses
trivalent chromium exclusively (or nearly exclusively) and
the process does not generate hexavalent chromium; and
iii)
The waste is typically and frequently managed in non-
oxidizing environments.
B)
Specific wastes that meet the standard in subsection (b)(6)(A) of
this Section (so long as they do not fail the test for the toxicity
characteristic for any other constituent and do not exhibit any
other characteristic) are:
i)
Chrome (blue) trimmings generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
ii)
Chrome (blue) shavings generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
iii)
Buffing dust generated by the following subcategories of
the leather tanning and finishing industry: hair
pulp/chrome tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no beamhouse,
through-the-blue;
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iv)
Sewer screenings generated by the following subcategories
of the leather tanning and finishing industry: hair
pulp/chrome tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no beamhouse,
through-the-blue, and shearling;
v)
Wastewater treatment sludges generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
vi)
Wastewater treatment sludges generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, and through-the-blue;
vii)
Waste scrap leather from the leather tanning industry, the
shoe manufacturing industry, and other leather product
manufacturing industries; and
viii) Wastewater treatment sludges from the production of
titanium dioxide pigment using chromium-bearing ores by
the chloride process.
7)
Solid waste from the extraction, beneficiation, and processing of ores
and minerals (including coal, phosphate rock, and overburden from the
mining of uranium ore), except as provided by 35 Ill. Adm. Code
726.212 for facilities that burn or process hazardous waste.
A)
For purposes of this subsection (b)(7), beneficiation of ores and
minerals is restricted to the following activities: crushing,;
grinding,; washing,; dissolution,; crystallization,; filtration,;
sorting,; sizing,; drying,; sintering,; pelletizing,; briquetting,;
calcining to remove water or carbon dioxide,; roasting,;
autoclaving or chlorination in preparation for leaching (except
where the roasting (or autoclaving or chlorination) and leaching
sequence produces a final or intermediate product that does not
undergo further beneficiation or processing),; gravity
concentration,; magnetic separation,; electrostatic separation,;
floatation,; ion exchange,; solvent extraction,; electrowinning,;
precipitation,; amalgamation,; and heap, dump, vat tank, and in
situ leaching.
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B)
For the purposes of this subsection (b)(7), solid waste from the
processing of ores and minerals includes only the following
wastes as generated:
Ai)
Slag from primary copper processing,;
Bii)
Slag from primary lead processing,;
Ciii) Red and brown muds from bauxite refining,;
Div) Phosphogypsum from phosphoric acid production,;
Ev)
Slag from elemental phosphorus production,;
Fvi) Gasifier ash from coal gasification,;
Gvii) Process wastewater from coal gasification,;
Hviii) Calcium sulfate wastewater treatment plant sludge from
primary copper processing,;
Iix)
Slag tailings from primary copper processing,;
Jx)
Fluorogypsum from hydrofluoric acid production,;
Kxi) Process wastewater from hydrofluoric acid production,;
Lxii) Air pollution control dust or sludge from iron blast
furnaces,;
Mxiii) Iron blast furnace slag,;
Nxiv) Treated residue from roasting and leaching of chrome
ore,;
Oxv) Process wastewater from primary magnesium processing
by the anhydrous process,;
Pxvi) Process wastewater from phosphoric acid production,;
Qxvii) Basic oxygen furnace and open hearth furnace air
pollution control dust or sludge from carbon steel
production,;
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Rxviii) Basic oxygen furnace and open hearth furnace slag from
carbon steel production,;
Sxix) Chloride processing waste solids from titanium
tetrachloride production,; and
Txx) Slag from primary zinc smelting production.
C)
A residue derived from co-processing mineral processing
secondary materials with normal beneficiation raw materials
remains excluded under this subsection (b) if the following
conditions are fulfilled:
i)
The owner or operator processes at least 50 percent by
weight normal beneficiation raw materials; and
ii)
The owner or operator legitimately reclaims the secondary
mineral processing materials.
8)
Cement kiln dust waste, except as provided by 35 Ill. Adm. Code
726.212 for facilities that burn or process hazardous waste.
9)
Solid waste that consists of discarded arsenical-treated wood or wood
products that fails the test for the toxicity characteristic for hazardous
waste codes D004 through D017 and which is not a hazardous waste for
any other reason if the waste is generated by persons that utilize the
arsenical-treated wood and wood products for these materials’ intended
end use.
10)
Petroleum-contaminated media and debris that fail the test for the
toxicity characteristic of Section 721.124 (hazardous waste codes D018
through D043 only) and which are subject to corrective action
regulations under 35 Ill. Adm. Code 731.
11)
This subsection corresponds with 40 CFR 261.4(b)(11), which expired
by its own terms on January 25, 1993. This statement maintains
structural parity with USEPA regulations.
12)
Used chlorofluorocarbon refrigerants from totally enclosed heat transfer
equipment, including mobile air conditioning systems, mobile
refrigeration, and commercial and industrial air conditioning and
refrigeration systems, that use chlorofluorocarbons as the heat transfer
fluid in a refrigeration cycle, provided the refrigerant is reclaimed for
further use.
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13)
Non-terne plated used oil filters that are not mixed with wastes listed in
Subpart D of this Part, if these oil filters have been gravity hot-drained
using one of the following methods:
A)
Puncturing the filter anti-drain back valve or the filter dome end
and hot-draining;
B)
Hot-draining and crushing;
C)
Dismantling and hot-draining; or
D)
Any other equivalent hot-draining method that will remove used
oil.
14)
Used oil re-refining distillation bottoms that are used as feedstock to
manufacture asphalt products.
c)
Hazardous wastes that are exempted from certain regulations. A hazardous
waste that is generated in a product or raw material storage tank, a product or
raw material transport vehicle or vessel, a product or raw material pipeline, or
in a manufacturing process unit, or an associated non-waste-treatment
manufacturing unit, is not subject to regulation under 35 Ill. Adm. Code 702,
703, 705, and 722 through 725, and 728 or to the notification requirements of
section 3010 of RCRA until it exits the unit in which it was generated, unless
the unit is a surface impoundment, or unless the hazardous waste remains in the
unit more than 90 days after the unit ceases to be operated for manufacturing or
for storage or transportation of product or raw materials.
d)
Samples
1)
Except as provided in subsection (d)(2) of this Section, a sample of solid
waste or a sample of water, soil, or air that is collected for the sole
purpose of testing to determine its characteristics or composition is not
subject to any requirements of this Part or 35 Ill. Adm. Code 702, 703,
705, and 722 through 728. The sample qualifies when:
A)
The sample is being transported to a laboratory for the purpose of
testing;
B)
The sample is being transported back to the sample collector after
testing;
C)
The sample is being stored by the sample collector before
transport to a laboratory for testing;
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D)
The sample is being stored in a laboratory before testing;
E)
The sample is being stored in a laboratory for testing but before it
is returned to the sample collector; or
F)
The sample is being stored temporarily in the laboratory after
testing for a specific purpose (for example, until conclusion of a
court case or enforcement action where further testing of the
sample may be necessary).
2)
In order to qualify for the exemption in subsection (d)(1)(A) or (d)(1)(B)
of this Section, a sample collector shipping samples to a laboratory and a
laboratory returning samples to a sample collector shall:
A)
Comply with U.S. Department of Transportation (USDOT), U.S.
Postal Service (USPS), or any other applicable shipping
requirements; or
B)
Comply with the following requirements if the sample collector
determines that USDOT, USPS, or other shipping requirements
do not apply to the shipment of the sample:
i)
Assure that the following information accompanies the
sample: The sample collector’s name, mailing address,
and telephone number; the laboratory’s name, mailing
address, and telephone number; the quantity of the
sample; the date of the shipment; and a description of the
sample.
ii)
Package the sample so that it does not leak, spill, or
vaporize from its packaging.
3)
This exemption does not apply if the laboratory determines that the waste
is hazardous but the laboratory is no longer meeting any of the
conditions stated in subsection (d)(1) of this Section.
e)
Treatability study samples.
1)
Except as is provided in subsection (e)(2) of this Section, a person that
generates or collects samples for the purpose of conducting treatability
studies, as defined in 35 Ill. Adm. Code 720.110, are not subject to any
requirement of 35 Ill. Adm. Code 721 through 723 or to the notification
requirements of section 3010 of the Resource Conservation and
Recovery Act. Nor are such samples included in the quantity
68
determinations of Section 721.105 and 35 Ill. Adm. Code 722.134(d)
when:
A)
The sample is being collected and prepared for transportation by
the generator or sample collector;
B)
The sample is being accumulated or stored by the generator or
sample collector prior to transportation to a laboratory or testing
facility; or
C)
The sample is being transported to the laboratory or testing
facility for the purpose of conducting a treatability study.
2)
The exemption in subsection (e)(1) of this Section is applicable to
samples of hazardous waste being collected and shipped for the purpose
of conducting treatability studies provided that:
A)
The generator or sample collector uses (in “treatability studies”)
no more than 10,000 kg of media contaminated with non-acute
hazardous waste, 1000 kg of non-acute hazardous waste other
than contaminated media, 1 kg of acute hazardous waste, or 2500
kg of media contaminated with acute hazardous waste for each
process being evaluated for each generated wastestream;
B)
The mass of each shipment does not exceed 10,000 kg; the
10,000 kg quantity may be all media contaminated with non-
acute hazardous waste, or may include 2500 kg of media
contaminated with acute hazardous waste, 1000 kg of hazardous
waste, and 1 kg of acute hazardous waste;
C)
The sample must be packaged so that it does not leak, spill, or
vaporize from its packaging during shipment and the
requirements of subsections (e)(2)(C)(i) or (e)(2)(C)(ii) of this
Section are met.
i)
The transportation of each sample shipment complies with
U.S. Department of Transportation (USDOT), U.S.
Postal Service (USPS), or any other applicable shipping
requirements; or
ii)
If the USDOT, USPS, or other shipping requirements do
not apply to the shipment of the sample, the following
information must accompany the sample: The name,
mailing address, and telephone number of the originator
of the sample; the name, address, and telephone number
69
of the facility that will perform the treatability study; the
quantity of the sample; the date of the shipment; and, a
description of the sample, including its USEPA hazardous
waste number;
D)
The sample is shipped to a laboratory or testing facility that is
exempt under subsection (f) of this Section, or has an appropriate
RCRA permit or interim status;
E)
The generator or sample collector maintains the following records
for a period ending three years after completion of the treatability
study:
i)
Copies of the shipping documents;
ii)
A copy of the contract with the facility conducting the
treatability study;
iii)
Documentation showing: The amount of waste shipped
under this exemption; the name, address, and USEPA
identification number of the laboratory or testing facility
that received the waste; the date the shipment was made;
and whether or not unused samples and residues were
returned to the generator; and
F)
The generator reports the information required in subsection
(e)(2)(E)(iii) of this Section in its report under 35 Ill. Adm. Code
722.141.
3)
The Agency may grant requests on a case-by-case basis for up to an
additional two years for treatability studies involving bioremediation.
The Agency may grant requests, on a case-by-case basis, for quantity
limits in excess of those specified in subsections (e)(2)(A), (e)(2)(B), and
(f)(4) of this Section, for up to an additional 5000 kg of media
contaminated with non-acute hazardous waste, 500 kg of non-acute
hazardous waste, 2500 kg of media contaminated with acute hazardous
waste, and 1 kg of acute hazardous waste:
A)
In response to requests for authorization to ship, store, and
conduct further treatability studies on additional quantities in
advance of commencing treatability studies. Factors to be
considered in reviewing such requests include the nature of the
technology, the type of process (e.g., batch versus continuous),
the size of the unit undergoing testing (particularly in relation to
scale-up considerations), the time or quantity of material required
70
to reach steady-state operating conditions, or test design
considerations, such as mass balance calculations.
B)
In response to requests for authorization to ship, store, and
conduct treatability studies on additional quantities after initiation
or completion of initial treatability studies when: There has been
an equipment or mechanical failure during the conduct of the
treatability study, there is need to verify the results of a
previously-conducted treatability study, there is a need to study
and analyze alternative techniques within a previously-evaluated
treatment process, or there is a need to do further evaluation of
an ongoing treatability study to determine final specifications for
treatment.
C)
The additional quantities allowed and timeframes allowed in
subsections (e)(3)(A) and (e)(3)(B) of this Section are subject to
all the provisions in subsections (e)(1) and (e)(2)(B) through
(e)(2)(F) of this Section. The generator or sample collector shall
apply to the Agency and provide in writing the following
information:
i)
The reason why the generator or sample collector requires
additional time or quantity of sample for the treatability
study evaluation and the additional time or quantity
needed;
ii)
Documentation accounting for all samples of hazardous
waste from the wastestream that have been sent for or
undergone treatability studies, including the date each
previous sample from the waste stream was shipped, the
quantity of each previous shipment, the laboratory or
testing facility to which it was shipped, what treatability
study processes were conducted on each sample shipped,
and the available results of each treatability study;
iii)
A description of the technical modifications or change in
specifications that will be evaluated and the expected
results;
iv)
If such further study is being required due to equipment or
mechanical failure, the applicant shall include information
regarding the reason for the failure or breakdown and also
include what procedures or equipment improvements have
been made to protect against further breakdowns; and
71
v)
Such other information as the Agency determines is
necessary.
4)
Final Agency determinations pursuant to this subsection (e) may be
appealed to the Board.
f)
Samples undergoing treatability studies at laboratories or testing facilities.
Samples undergoing treatability studies and the laboratory or testing facility
conducting such treatability studies (to the extent such facilities are not
otherwise subject to RCRA requirements) are not subject to any requirement of
this Part, or of 35 Ill. Adm. Code 702, 703, 705, 722 through 726, and 728 or
to the notification requirements of Section 3010 of the Resource Conservation
and Recovery Act, provided that the requirements of subsections (f)(1) through
(f)(11) of this Section are met. A mobile treatment unit may qualify as a testing
facility subject to subsections (f)(1) through (f)(11) of this Section. Where a
group of mobile treatment units are located at the same site, the limitations
specified in subsections (f)(1) through (f)(11) of this Section apply to the entire
group of mobile treatment units collectively as if the group were one mobile
treatment unit.
1)
No less than 45 days before conducting treatability studies, the facility
notifies the Agency in writing that it intends to conduct treatability
studies under this subsection (f).
2)
The laboratory or testing facility conducting the treatability study has a
USEPA identification number.
3)
No more than a total of 10,000 kg of “as received” media contaminated
with non-acute hazardous waste, 2500 kg of media contaminated with
acute hazardous waste, or 250 kg of other “as received” hazardous waste
is subject to initiation of treatment in all treatability studies in any single
day. “As received” waste refers to the waste as received in the shipment
from the generator or sample collector.
4)
The quantity of “as received” hazardous waste stored at the facility for
the purpose of evaluation in treatability studies does not exceed 10,000
kg, the total of which can include 10,000 kg of media contaminated with
non-acute hazardous waste, 2500 kg of media contaminated with acute
hazardous waste, 1000 kg of non-acute hazardous wastes other than
contaminated media, and 1 kg of acute hazardous waste. This quantity
limitation does not include treatment materials (including nonhazardous
solid waste) added to “as received” hazardous waste.
5)
No more than 90 days have elapsed since the treatability study for the
sample was completed, or no more than one year (two years for
72
treatability studies involving bioremediation) has elapsed since the
generator or sample collector shipped the sample to the laboratory or
testing facility, whichever date first occurs. Up to 500 kg of treated
material from a particular waste stream from treatability studies may be
archived for future evaluation up to five years from the date of initial
receipt. Quantities of materials archived are counted against the total
storage limit for the facility.
6)
The treatability study does not involve the placement of hazardous waste
on the land or open burning of hazardous waste.
7)
The facility maintains records for three years following completion of
each study that show compliance with the treatment rate limits and the
storage time and quantity limits. The following specific information
must be included for each treatability study conducted:
A)
The name, address, and USEPA identification number of the
generator or sample collector of each waste sample;
B)
The date the shipment was received;
C)
The quantity of waste accepted;
D)
The quantity of “as received” waste in storage each day;
E)
The date the treatment study was initiated and the amount of “as
received” waste introduced to treatment each day;
F)
The date the treatability study was concluded;
G)
The date any unused sample or residues generated from the
treatability study were returned to the generator or sample
collector or, if sent to a designated facility, the name of the
facility and the USEPA identification number.
8)
The facility keeps, on-site, a copy of the treatability study contract and
all shipping papers associated with the transport of treatability study
samples to and from the facility for a period ending three years from the
completion date of each treatability study.
9)
The facility prepares and submits a report to the Agency by March 15 of
each year that estimates the number of studies and the amount of waste
expected to be used in treatability studies during the current year, and
includes the following information for the previous calendar year:
73
A)
The name, address, and USEPA identification number of the
facility conducting the treatability studies;
B)
The types (by process) of treatability studies conducted;
C)
The names and addresses of persons for whom studies have been
conducted (including their USEPA identification numbers);
D)
The total quantity of waste in storage each day;
E)
The quantity and types of waste subjected to treatability studies;
F)
When each treatability study was conducted; and
G)
The final disposition of residues and unused sample from each
treatability study.
10)
The facility determines whether any unused sample or residues generated
by the treatability study are hazardous waste under Section 721.103 and,
if so, are subject to 35 Ill. Adm. Code 702, 703, and 721 through 728,
unless the residues and unused samples are returned to the sample
originator under the exemption of subsection (e) of this Section.
11)
The facility notifies the Agency by letter when the facility is no longer
planning to conduct any treatability studies at the site.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.105
Special Requirements for Hazardous Waste Generated by Small Quantity
Generators
a)
A generator is a conditionally exempt small quantity generator in a calendar
month if it generates no more than 100 kilograms of hazardous waste in that
month. 35 Ill. Adm. Code 700 explains the relation of this to the 100 kg/mo
exception of 35 Ill. Adm. Code 809.
b)
Except for those wastes identified in subsections (e), (f), (g) and (j) of this
Section, a conditionally exempt small quantity generator’s hazardous wastes are
not subject to regulation under 35 Ill. Adm. Code 702, 703, 705 and 722
through 726 and 728, and the notification requirements of section 3010 of
Resource Conservation and Recovery Act, provided the generator complies with
the requirements of subsections (f), (g) and (j) of this Section.
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c)
When making the quantity determinations of this Part and 35 Ill. Adm. Code
722, the generator must include all hazardous waste that it generates, except the
following hazardous waste:
1)
Hazardous waste that is exempt from regulation under Section
721.104(c) through (f), 721.106(a)(3), 721.107(a)(1), or 721.108;
2)
Hazardous waste that is managed immediately upon generation only in
on-site elementary neutralization units, wastewater treatment units, or
totally enclosed treatment facilities, as defined in 35 Ill. Adm. Code
720.110;
3)
Hazardous waste that is recycled, without prior storage or accumulation,
only in an on-site process subject to regulation under Section
721.106(c)(2);
4)
Hazardous waste that is used oil managed under the requirements of
Section 721.106(a)(4) and 35 Ill. Adm. Code 739;
5)
Hazardous waste that is spent lead-acid batteries managed under the
requirements of 35 Ill. Adm. Code 726.Subpart G; and
6)
Hazardous waste that is universal waste managed under Section 721.109
and 35 Ill. Adm. Code 733.
d)
In determining the quantity of hazardous waste it generates, a generator need
not include:
1)
Hazardous waste when it is removed from on-site storage; or
2)
Hazardous waste produced by on-site treatment (including reclamation)
of its hazardous waste so long as the hazardous waste that is treated was
counted once; or
3)
Spent materials that are generated, reclaimed and subsequently reused
on-site, so long as such spent materials have been counted once.
e)
If a generator generates acute hazardous waste in a calendar month in quantities
greater than set forth below, all quantities of that acute hazardous waste are
subject to full regulation under 35 Ill. Adm. Code 702, 703, 705 and 722
through 726 and 728, and the notification requirements of section 3010 of the
Resource Conservation and Recovery Act:
1)
A total of one kilogram of one or more of the acute hazardous wastes
listed in Section 721.131, 721.132, or 721.133(e); or
75
2)
A total of 100 kilograms of any residue or contaminated soil, waste or
other debris resulting from the clean-up of a spill, into or on any land or
water, of any one or more of the acute hazardous wastes listed in Section
721.131, 721.132, or 721.133(e).
BOARD NOTE: “Full regulation” means those regulations applicable to
generators of greater than 1000 kg of non-acute hazardous waste in a calendar
month.
f)
In order for acute hazardous wastes generated by a generator of acute hazardous
wastes in quantities equal to or less than those set forth in subsection (e)(1) or
(e)(2) of this Section to be excluded from full regulation under this Section, the
generator must comply with the following requirements:
1)
35 Ill. Adm. Code 722.111.
2)
The generator may accumulate acute hazardous waste on-site. If the
generator accumulates at any time acute hazardous wastes in quantities
greater than set forth in subsection (e)(1) or (e)(2) of this Section, all of
those accumulated wastes are subject to regulation under 35 Ill. Adm.
Code 702, 703, 705 and 722 through 726 and 728, and the applicable
notification requirements of section 3010 of the Resource Conservation
and Recovery Act. The time period of 35 Ill. Adm. Code 722.134(a),
for accumulation of wastes on-site, begins when the accumulated wastes
exceed the applicable exclusion limit.
3)
A conditionally exempt small quantity generator may either treat or
dispose of its acute hazardous waste in an on-site facility or ensure
delivery to an off-site treatment, storage, or disposal facility, any of
which, if located in the United States, meets any of the following
conditions:
A)
The facility is permitted under 35 Ill. Adm. Code 702 and 703;
B)
The facility has interim status under 35 Ill. Adm. Code 702, 703
and 725;
C)
The facility is authorized to manage hazardous waste by a state
with a hazardous waste management program approved by
USEPA pursuant to 40 CFR 271;
D)
The facility is permitted, licensed, or registered by a state to
manage municipal solid waste and, if managed in a municipal
76
solid waste landfill facility, the landfill is subject to 35 Ill. Adm.
Code 810 through 814 or 40 CFR 258;
E)
The facility is permitted, licensed, or registered by a state to
manage non-municipal non-hazardous waste and, if managed in a
non-municipal non-hazardous waste disposal unit, the unit is
subject to the requirements of 40 CFR 257.5 through 257.30;
BOARD NOTE: The Illinois non-hazardous waste landfill
regulations, 35 Ill. Adm. Code 810 through 814, do not allow the
disposal of hazardous waste in a landfill regulated under those
rules. The Board intends that subsections (f)(3)(D) and (f)(3)(E)
of this Section impose a federal requirement on the hazardous
waste generator. The Board specifically does not intend that
these subsections authorize any disposal of conditionally-exempt
small quantity generator waste in a landfill not specifically
permitted to accept the particular hazardous waste.
F)
The facility is one that:
i)
Beneficially uses or reuses or legitimately recycles or
reclaims its waste; or
ii)
Treats its waste prior to beneficial use or reuse, or
legitimate recycling or reclamation; or
G)
For universal waste managed under 35 Ill. Adm. Code 733 or 40
CFR 273, the facility is a universal waste handler or destination
facility subject to the requirements of 35 Ill. Adm. Code 733 or
40 CFR 273.
g)
In order for hazardous waste generated by a conditionally exempt small quantity
generator in quantities of less than 100 kilograms of hazardous waste during a
calendar month to be excluded from full regulation under this Section, the
generator must comply with the following requirements:
1)
35 Ill. Adm. Code 722.111;
2)
The conditionally exempt small quantity generator may accumulate
hazardous waste on-site. If it accumulates at any time more than a total
of 1000 kilograms of the generator’s hazardous waste, all of those
accumulated wastes are subject to regulation under the special provisions
of 35 Ill. Adm. Code 722 applicable to generators of between 100 kg
and 1000 kg of hazardous waste in a calendar month as well as the
requirements of 35 Ill. Adm. Code 702, 703, 705 and 723 through 726
77
and 728, and the applicable notification requirements of Section 3010 of
the Resource Conservation and Recovery Act. The time period of 35 Ill.
Adm. Code 722.134(d) for accumulation of wastes on-site begins for a
small quantity generator when the accumulated wastes exceed 1000
kilograms;
3)
A conditionally exempt small quantity generator may either treat or
dispose of its hazardous waste in an on-site facility or ensure delivery to
an off-site treatment, storage, or disposal facility, any of which, if
located in the United States, meets any of the following conditions:
A)
The facility is permitted under 35 Ill. Adm. Code 702 and 703;
B)
The facility has interim status under 35 Ill. Adm. Code 702, 703
and 725;
C)
The facility is authorized to manage hazardous waste by a state
with a hazardous waste management program approved by
USEPA under 40 CFR 271 (1986);
D)
The facility is permitted, licensed, or registered by a state to
manage municipal solid waste and, if managed in a municipal
solid waste landfill facility, the landfill is subject to 35 Ill. Adm.
Code 810 through 814 or 40 CFR 258;
E)
The facility is permitted, licensed, or registered by a state to
manage non-municipal non-hazardous waste and, if managed in a
non-municipal non-hazardous waste disposal unit, the unit is
subject to the requirements of 40 CFR 257.5 through 257.30;
BOARD NOTE: The Illinois non-hazardous waste landfill
regulations, 35 Ill. Adm. Code 810 through 814, do not allow the
disposal of hazardous waste in a landfill regulated under those
rules. The Board intends that subsections (g)(3)(D) and (g)(3)(E)
of this Section impose a federal requirement on the hazardous
waste generator. The Board specifically does not intend that
these subsections authorize any disposal of conditionally-exempt
small quantity generator waste in a landfill not specifically
permitted to accept the particular hazardous waste.
F)
The facility is one that:
i)
Beneficially uses or re-uses, or legitimately recycles or
reclaims the small quantity generator’s waste; or
78
ii)
Treats its waste prior to beneficial use or re-use, or
legitimate recycling or reclamation; or
G)
For universal waste managed under 35 Ill. Adm. Code 733 or 40
CFR 273, the facility is a universal waste handler or destination
facility subject to the requirements of 35 Ill. Adm. Code 733 or
40 CFR 273.
h)
Hazardous waste subject to the reduced requirements of this Section may be
mixed with non-hazardous waste and remain subject to these reduced
requirements even though the resultant mixture exceeds the quantity limitations
identified in this Section, unless the mixture meets any of the characteristics of
hazardous wastes identified in Subpart C.
i)
If a small quantity generator mixes a solid waste with a hazardous waste that
exceeds a quantity exclusion level of this Section, the mixture is subject to full
regulation.
j)
If a conditionally exempt small quantity generator’s hazardous wastes are mixed
with used oil, the mixture is subject to 35 Ill. Adm. Code 739, if it is destined
to be burned for energy recovery. Any material produced from such a mixture
by processing, blending, or other treatment is also so regulated if it is destined
to be burned for energy recovery.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.106
Requirements for Recyclable Materials
a)
Recyclable materials:
1)
Hazardous wastes that are recycled are subject to the requirements for
generators, transporters, and storage facilities of subsections (b) and (c)
of this Section, except for the materials listed in subsections (a)(2) and
(a)(3) of this Section. Hazardous wastes that are recycled will be known
as “recyclable materials”.
2)
The following recyclable materials are not subject to the requirements of
this Section but are regulated under 35 Ill. Adm. Code 726.Subparts C
through H and all applicable provisions in 35 Ill. Adm. Code 702, 703,
and 705.
A)
Recyclable materials used in a manner constituting disposal (35
Ill. Adm. Code 726.Subpart C);
79
B)
Hazardous wastes burned for energy recovery in boilers and
industrial furnaces that are not regulated under 35 Ill. Adm. Code
724.Subpart O or 725.Subpart O (35 Ill. Adm. Code 726.Subpart
H);
C)
Recyclable materials from which precious metals are reclaimed
(35 Ill. Adm. Code 726.Subpart F);
D)
Spent lead-acid batteries that are being reclaimed (35 Ill. Adm.
Code 726.Subpart G).
3)
The following recyclable materials are not subject to regulation under 35
Ill. Adm. Code 722 through 726, 728, or 702, 703, or 705 and are not
subject to the notification requirements of section 3010 of the Resource
Conservation and Recovery Act:
A)
Industrial ethyl alcohol that is reclaimed except that, unless
provided otherwise in an international agreement as specified in
35 Ill. Adm. Code 722.158:
i)
A person initiating a shipment for reclamation in a foreign
country and any intermediary arranging for the shipment
shall comply with the requirements applicable to a
primary exporter in 35 Ill. Adm. Code 722.153;
722.156(a)(1) through (a)(4), (a)(6), and (b); and
722.157; shall export such materials only upon consent of
the receiving country and in conformance with the
USEPA Acknowledgment of Consent, as defined in 35 Ill.
Adm. Code 722.Subpart E; and shall provide a copy of
the USEPA Acknowledgment of Consent to the shipment
to the transporter transporting the shipment for export;
ii)
Transporters transporting a shipment for export shall not
accept a shipment if the transporter knows that the
shipment does not conform to the USEPA
Acknowledgement of Consent, shall ensure that a copy of
the USEPA Acknowledgement of Consent accompanies
the shipment, and shall ensure that it is delivered to the
facility designated by the person initiating the shipment;
B)
Scrap metal that is not excluded under Section 721.104(a)(13);
C)
Fuels produced from the refining of oil-bearing hazardous wastes
along with normal process streams at a petroleum refining facility
if such wastes result from normal petroleum refining, production,
80
and transportation practices (this exemption does not apply to
fuels produced from oil recovered from oil-bearing hazardous
waste where such recovered oil is already excluded under Section
721.104(a)(12));
D)
Petroleum refining wastes.
i)
Hazardous waste fuel produced from oil-bearing
hazardous wastes from petroleum refining, production, or
transportation practices or produced from oil reclaimed
from such hazardous wastes, where such hazardous wastes
are reintroduced into a process that does not use
distillation or does not produce products from crude oil,
so long as the resulting fuel meets the used oil
specification under 35 Ill. Adm. Code 726.140(e) 739.111
and so long as no other hazardous wastes are used to
produce the hazardous waste fuel;
ii)
Hazardous waste fuel produced from oil-bearing
hazardous waste from petroleum refining production, and
transportation practices, where such hazardous wastes are
reintroduced into a refining process after a point at which
contaminants are removed, so long as the fuel meets the
used oil fuel specification under 35 Ill. Adm. Code
726.140(e) 739.111; and
iii)
Oil reclaimed from oil-bearing hazardous wastes from
petroleum refining, production, and transportation
practices, which reclaimed oil is burned as a fuel without
reintroduction to a refining process, so long as the
reclaimed oil meets the used oil fuel specification under
35 Ill. Adm. Code 726.140(e) 739.111; and.
E)
Petroleum coke produced from petroleum refinery hazardous
wastes containing oil by the same person that generated the
wastes unless the resulting coke product exceeds one or more of
the characteristics of hazardous waste in 721.Subpart C.
4)
Used oil that is recycled and is also a hazardous waste solely because it
exhibits a hazardous characteristic is not subject to the requirements of
35 Ill. Adm. Code 720 through 728, but it is regulated under 35 Ill.
Adm. Code 739. Used oil that is recycled includes any used oil that is
reused for any purpose following its original use (including the purpose
for which the oil was originally used). Such term includes, but is not
81
limited to, oil that is re-refined, reclaimed, burned for energy recovery,
or reprocessed.
5)
Hazardous waste that is exported to or imported from designated
member countries of the Organization for Economic Cooperation and
Development (OECD), as defined in Section 722.158(a)(1), for the
purpose of recovery is subject to the requirements of 35 Ill. Adm. Code
722.Subpart H if it is subject to either the hazardous waste manifesting
requirements of 35 Ill. Adm. Code 722 or the universal waste
management standards of 35 Ill. Adm. Code 733.
b)
Generators and transporters of recyclable materials are subject to the applicable
requirements of 35 Ill. Adm. Code 722 and 723 and the notification
requirements under section 3010 of the Resource Conservation and Recovery
Act, except as provided in subsection (a) of this Section.
c)
Storage and recycling:
1)
Owners or operators of facilities that store recyclable materials before
they are recycled are regulated under all applicable provisions of 35 Ill.
Adm. Code 702, 703, and 705; 724.Subparts A through L, AA, BB, and
CC; and 725.Subparts A through L, AA, BB, and CC; 726; 728; and
the notification requirement under section 3010 of the Resource
Conservation and Recovery Act, except as provided in subsection (a) of
this Section. (The recycling process itself is exempt from regulation,
except as provided in subsection (d) of this Section.)
2)
Owners or operators of facilities that recycle recyclable materials without
storing them before they are recycled are subject to the following
requirements, except as provided in subsection (a) of this Section:
A)
Notification requirements under section 3010 of the Resource
Conservation and Recovery Act,
B)
35 Ill. Adm. Code 725.171 and 725.172 (dealing with the use of
the manifest and manifest discrepancies), and
C)
subsection (d) of this Section.
d)
Owners or operators of facilities required to have a RCRA permit pursuant to 35
Ill. Adm. Code 703 with hazardous waste management units that recycle
hazardous wastes are subject to 35 Ill. Adm. Code 724.Subparts AA and BB
and 725.Subparts AA and BB.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
82
SUBPART D: LISTS OF HAZARDOUS WASTE
Section 721.131
Hazardous Wastes From Nonspecific Sources
a)
The following solid wastes are listed hazardous wastes from non-specific
sources unless they are excluded under 35 Ill. Adm. Code 720.120 and 720.122
and listed in Section 721.Appendix I of this Part.
USEPA
Hazardous
Waste No.
Industry and Hazardous Waste
Hazard
Code
F001
The following spent halogenated solvents used in
degreasing: tetrachloroethylene, trichloroethylene,
methylene chloride, 1,1,1-trichloroethane, carbon
tetrachloride and chlorinated fluorocarbons; all spent
solvent mixtures and blends used in degreasing
containing, before use, a total of ten percent or more
(by volume) of one or more of the above halogenated
solvents or those solvents listed in F002, F004 or
F005; and still bottoms from the recovery of these
spent solvents and spent solvent mixtures.
(T)
F002
The following spent halogenated solvents: tetrachloro-
ethylene, methylene chloride, trichloroethylene, 1,1,1-
trichloroethane, chlorobenzene, 1,1,2-trichloro-1,2,2-
trifluoroethane, orthodichlorobenzene, trichloro-
fluoromethane and 1,1,2-trichloroethane; all spent
solvent mixtures and blends containing, before use, a
total of ten percent or more (by volume) of one or
more of the above halogenated solvents or those
solvents listed in F001, F004 or F005; and still
bottoms from the recovery of these spent solvents and
spent solvent mixtures.
(T)
83
F003
The following spent non-halogenated solvents: xylene,
acetone, ethyl acetate, ethyl benzene, ethyl ether,
methyl isobutyl ketone, n-butyl alcohol, cyclohexanone
and methanol; all spent solvent mixtures and blends
containing, before use, only the above spent non-
halogenated solvents; and all spent solvent mixtures
and blends containing, before use, one or more of the
above non-halogenated solvents and a total of ten
percent or more (by volume) of one or more of those
solvents listed in F001, F002, F004 or F005; and still
bottoms from the recovery of these spent solvents and
spent solvent mixtures.
(I)
F004
The following spent non-halogenated solvents: cresols
and cresylic acid and nitrobenzene; all spent solvent
mixtures and blends containing, before use, a total of
ten percent or more (by volume) of one or more of the
above non-halogenated solvents or those solvents listed
in F001, F002 or F005; and still bottoms from the
recovery of these spent solvents and spent solvent
mixtures.
(T)
F005
The following spent non-halogenated solvents:
toluene, methyl ethyl ketone, carbon disulfide,
isobutanol, pyridine, benzene, 2-ethoxyethanol and 2-
nitropropane; all spent solvent mixtures and blends,
containing, before use, a total of ten percent or more
(by volume) of one or more of the above non-
halogenated solvents or those solvents listed in F001,
F002 or F004; and still bottoms from the recovery of
these spent solvents and spent solvent mixtures.
(I, T)
F006
Wastewater treatment sludges from electroplating
operations except from the following processes: (1)
sulfuric acid anodizing of aluminum; (2) tin plating on
carbon steel; (3) zinc plating (segregated basis) on
carbon steel; (4) aluminum or zinc-aluminum plating
on carbon steel; (5) cleaning/stripping associated with
tin, zinc and aluminum plating on carbon steel; and (6)
chemical etching and milling of aluminum.
(T)
F019
See Below
84
F007
Spent cyanide plating bath solutions from electroplating
operations.
(R, T)
F008
Plating bath residues from the bottom of plating baths
from electroplating operations where cyanides are used
in the process.
(R, T)
F009
Spent stripping and cleaning bath solutions from
electroplating operations where cyanides are used in the
process.
(R, T)
F010
Quenching bath residues from oil baths from metal heat
treating operations where cyanides are used in the
process.
(R, T)
F011
Spent cyanide solutions from salt bath pot cleaning
from metal heat treating operations.
(R, T)
F012
Quenching wastewater treatment sludges from metal
heat treating operations where cyanides are used in the
process.
(T)
F019
Wastewater treatment sludges from the chemical
conversion coating of aluminum except from zirconium
phosphating in aluminum can washing when such
phosphating is an exclusive conversion coating process.
(T)
F020
Wastes (except wastewater and spent carbon from
hydrogen chloride purification) from the production or
manufacturing use (as a reactant, chemical intermediate
or component in a formulating process) of tri- or tetra-
chlorophenol, or of intermediates used to produce their
pesticide derivatives. (This listing does not include
wastes from the production of hexachlorophene from
highly purified 2,4,5-trichlorophenol.)
(H)
F021
Wastes (except wastewater and spent carbon from
hydrogen chloride purification) from the production or
manufacturing use (as a reactant, chemical intermediate
or component in a formulating process) of pentachloro-
phenol, or of intermediates used to produce its
derivatives.
(H)
85
F022
Wastes (except wastewater and spent carbon from
hydrogen chloride purification) from the manufacturing
use (as a reactant, chemical intermediate or component
in a formulating process) of tetra-, penta- or hexa-
chlorobenzenes under alkaline conditions.
(H)
F023
Wastes (except wastewater and spent carbon from
hydrogen chloride purification) from the production of
materials on equipment previously used for the
production or manufacturing use (as a reactant,
chemical intermediate or component in a formulating
process) of tri- and tetrachlorophenols. (This listing
does not include wastes from equipment used only for
the production or use of hexachlorophene from highly
purified 2,4,5-trichlorophenol.)
(H)
F024
Process wastes including but not limited to, distillation
residues, heavy ends, tars, and reactor cleanout wastes,
from the production of certain chlorinated aliphatic
hydrocarbons by free radical catalyzed processes.
These chlorinated aliphatic hydrocarbons are those
having carbon chain lengths ranging from one to and
including five, with varying amounts and positions of
chlorine substitution. (This listing does not include
wastewaters, wastewater treatment sludges, spent
catalysts and wastes listed in this Section or Section
721.132.)
(T)
F025
Condensed light ends, spent filters and filter aids, and
spent desiccant wastes from the production of certain
chlorinated aliphatic hydrocarbons by free radical
catalyzed processes. These chlorinated aliphatic
hydrocarbons are those having carbon chain lengths
ranging from one to and including five, with varying
amounts and positions of chlorine substitution.
(T)
F026
Wastes (except wastewater and spent carbon from
hydrogen chloride purification) from the production of
materials on equipment previously used for the
manufacturing use (as a reactant, chemical intermediate
or component in a formulating process) of tetra-,
penta- or hexachlorobenzene under alkaline conditions.
(H)
86
F027
Discarded unused formulations containing tri-, tetra- or
pentachlorophenol or discarded unused formulations
containing compounds derived from these chloro-
phenols. (This listing does not include formulations
containing hexachlorophene synthesized from
prepurified 2,4,5-trichlorophenol as the sole
component).
(H)
F028
Residues resulting from the incineration or thermal
treatment of soil contaminated with hazardous waste
numbers F020, F021, F022, F023, F026 and F027.
(T)
F032
Wastewaters, (except those that have not come into
contact with process contaminants), process residuals,
preservative drippage and spent formulations from
wood preserving processes generated at plants that
currently use or have previously used chlorophenolic
formulations (except potentially cross-contaminated
wastes that have had the F032 waste code deleted in
accordance with Section 721.135 and where the
generator does not resume or initiate use of chloro-
phenolic formulations). This listing does not include
K001 bottom sediment sludge from the treatment of
wastewater from wood preserving processes that use
creosote or pentachlorophenol.
(T)
F034
Wastewaters, (except those that have not come into
contact with process contaminants), process residuals,
preservative drippage and spent formulations from
wood preserving processes generated at plants that use
creosote formulations. This listing does not include
K001 bottom sediment sludge from the treatment of
wastewater from wood preserving processes that use
creosote or pentachlorophenol.
(T)
F035
Wastewaters, (except those that have not come into
contact with process contaminants), process residuals,
preservative drippage and spent formulations from
wood preserving processes generated at plants that use
inorganic preservatives containing arsenic or
chromium. This listing does not include K001 bottom
sediment sludge from the treatment of wastewater from
wood preserving processes that use creosote or penta-
chlorophenol.
(T)
87
F037
Petroleum refinery primary oil/water/solids separation
sludge -- Any sludge generated from the gravitational
separation of oil/water/solids during the storage or
treatment of process wastewaters and oily cooling
wastewaters from petroleum refineries. Such sludges
include, but are not limited to, those generated in:
oil/water/solids separators; tanks and impoundments;
ditches and other conveyances; sumps; and stormwater
units receiving dry weather flow. Sludges generated in
stormwater units that do not receive dry weather flow,
sludges generated from non-contact once-through
cooling waters segregated for treatment from other
process or oily cooling waters, sludges generated in
aggressive biological treatment units as defined in
subsection (b)(2), below, (including sludges generated
in one or more additional units after wastewaters have
been treated in aggressive biological treatment units)
and K051 wastes are not included in this listing. This
listing does include residuals generated from processing
or recycling oil-bearing hazardous secondary materials
excluded under Section 721.104(a)(12)(A) if those
residuals are to be disposed of.
(T)
F038
Petroleum refinery secondary (emulsified)
oil/water/solids separation sludge -- Any sludge or
float generated from the physical or chemical
separation of oil/water/solids in process wastewaters
and oily cooling wastewaters from petroleum
refineries. Such wastes include, but are not limited to,
all sludges and floats generated in: induced air
floatation (IAF) units, tanks and impoundments, and all
sludges generated in DAF units. Sludges generated in
stormwater units that do not receive dry weather flow,
sludges generated from non-contact once-through
cooling waters segregated for treatment from other
process or oily cooling waters, sludges and floats
generated in aggressive biological treatment units as
defined in subsection (b)(2), below, (including sludges
and floats generated in one or more additional units
after wastewaters have been treated in aggressive
biological treatment units), F037, K048 and K051
wastes are not included in this listing.
(T)
88
F039
Leachate (liquids which have percolated through land
disposed wastes) resulting from the disposal of more
than one restricted waste classified as hazardous under
Subpart D. (Leachate resulting from the disposal of
one or more of the following USEPA hazardous wastes
and no other hazardous wastes retains its USEPA
hazardous waste number(s): F020, F021, F022, F026,
F027 or F028.)
(T)
BOARD NOTE: The primary hazardous properties of these materials have been
indicated by the letters T (Toxicity), R (Reactivity), I (Ignitability), and C
(Corrosivity). The letter H indicates Acute Hazardous Waste.
b)
Listing specific definitions.
1)
For the purpose of the F037 and F038 listings, oil/water/solids is defined
as oil or water or solids.
2)
For the purposes of the F037 and F038 listings:
A)
Aggressive biological treatment units are defined as units which
employ one of the following four treatment methods: activated
sludge; trickling filter; rotating biological contactor for the
continuous accelerated biological oxidation of wastewaters; or,
high-rate aeration. High-rate aeration is a system of surface
impoundments or tanks, in which intense mechanical aeration is
used to completely mix the wastes, enhance biological activity,
and:
i)
The units employ a minimum of 6 six horsepower per
million gallons of treatment volume; and either
ii)
The hydraulic retention time of the unit is no longer than
5 five days; or
iii)
The hydraulic retention time is no longer than 30 days and
the unit does not generate a sludge that is a hazardous
waste by the toxicity characteristic.
B)
Generators and treatment, storage or disposal (TSD) facilities
have the burden of proving that their sludges are exempt from
listing as F037 or F038 wastes under this definition. Generators
and TSD facilities shall maintain, in their operating or other on
site records, documents and data sufficient to prove that:
89
i)
The unit is an aggressive biological treatment unit as
defined in this subsection; and
ii)
The sludges sought to be exempted from F037 or F038
were actually generated in the aggressive biological
treatment unit.
3)
Time of generation. For the purposes of the designated waste, the time
of generation is as follows:
A)
The For the F037 listing, sludges are considered to be generated
at the moment of deposition in the unit, where deposition is
defined as at least a temporary cessation of lateral particle
movement.
B)
The For the F038 listing:
i)
Sludges are considered to be generated at the moment of
deposition in the unit, where deposition is defined as at
least a temporary cessation of lateral particle movement;
and
ii)
Floats are considered to be generated at the moment they
are formed in the top of the unit.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.132
Hazardous Waste from Specific Sources
The following solid wastes are listed hazardous wastes from specific sources unless they are
excluded under 35 Ill. Adm. Code 720.120 and 720.122 and listed in Section 721.Appendix I
of this Part.
USEPA
Hazardous
Waste No.
Industry and Hazardous Waste
Hazard
Code
Wood Preservation:
K001
Bottom sediment sludge from the treatment of wastewaters from
wood preserving processes that use creosote or pentachloro-
phenol.
(T)
90
Inorganic Pigments:
K002
Wastewater treatment sludge from the production of chrome
yellow and orange pigments.
(T)
K003
Wastewater treatment sludge from the production of molybdate
orange pigments.
(T)
K004
Wastewater treatment sludge from the production of zinc yellow
pigments.
(T)
K005
Wastewater treatment sludge from the production of chrome
green pigments.
(T)
K006
Wastewater treatment sludge from the production of chrome
oxide green pigments (anhydrous and hydrated).
(T)
K007
Wastewater treatment sludge from the production of iron blue
pigments.
(T)
K008
Oven residue from the production of chrome oxide green
pigments.
(T)
Organic Chemicals:
K009
Distillation bottoms from the production of acetaldehyde from
ethylene.
(T)
K010
Distillation side cuts from the production of acetaldehyde from
ethylene.
(T)
K011
Bottom stream from the wastewater stripper in the production of
acrylonitrile.
(R,T)
K013
Bottom stream from the acetonitrile column in the production of
acrylonitrile.
(T)
K014
Bottoms from the acetonitrile purification column in the
production of acrylonitrile.
(T)
K015
Still bottoms from the distillation of benzyl chloride.
(T)
K016
Heavy ends or distillation residues from the production of
carbon tetrachloride.
(T)
91
K017
Heavy ends (still bottoms) from the purification column in the
production of epichlorohydrin.
(T)
K018
Heavy ends from the fractionation column in ethyl chloride
production.
(T)
K019
Heavy ends from the distillation of ethylene dichloride in
ethylene dichloride production.
(T)
K020
Heavy ends from the distillation of vinyl chloride in vinyl
chloride monomer production.
(T)
K021
Aqueous spent antimony catalyst waste from fluoromethanes
production.
(T)
K022
Distillation bottom tars from the production of phenol/acetone
from cumene.
(T)
K023
Distillation light ends from the production of phthalic anhydride
from naphthalene.
(T)
K024
Distillation bottoms from the production of phthalic anhydride
from naphthalene.
(T)
K093
Distillation light ends from the production of phthalic anhydride
from ortho-xylene.
(T)
K094
Distillation bottoms from the production of phthalic anhydride
from ortho-xylene.
(T)
K025
Distillation bottoms from the production of nitrobenzene by the
nitration of benzene.
(T)
K026
Stripping still tails from the production of methyl ethyl
pyridines.
(T)
K027
Centrifuge and distillation residues from toluene diisocyanate
production.
(R,T)
K028
Spent catalyst from the hydrochlorinator reactor in the
production of 1,1,1-trichloroethane.
(T)
K029
Waste from the product stream stripper in the production of
1,1,1-trichloroethane.
(T)
92
K095
Distillation bottoms from the production of 1,1,1-trichloro-
ethane.
(T)
K096
Heavy ends from the heavy ends column from the production of
1,1,1-trichloroethane.
(T)
K030
Column bottoms or heavy ends from the combined production
of trichloroethylene and perchloroethylene.
(T)
K083
Distillation bottoms from aniline production.
(T)
K103
Process residues from aniline extraction from the production of
aniline.
(T)
K104
Combined wastewater streams generated from
nitrobenzene/aniline production.
(T)
K085
Distillation or fractionation column bottoms
from the production of chlorobenzenes.
(T)
K105
Separated aqueous stream from the reactor product washing step
in the production of chlorobenzenes.
(T)
K107
Column bottoms from product separation from the production
of 1,1-dimethylhydrazine (UDMH) from carboxylic acid
hydrazides.
(C,T)
K108
Condensed column overheads from product separation and
condensed reactor vent gases from the production of 1,1-di-
methylhydrazine (UDMH) from carboxylic acid hydrazides.
(I,T)
K109
Spent filter cartridges from the product purification from the
production of 1,1-dimethylhydrazine (UDMH) from carboxylic
acid hydrazides.
(T)
K110
Condensed column overheads from intermediate separation from
the production of 1,1-dimethylhydrazine (UDMH) from
carboxylic acid hydrazides.
(T)
K111
Product wastewaters from the production of dinitrotoluene via
nitration of toluene.
(C,T)
K112
Reaction by-product water from the drying column in the
production of toluenediamine via hydrogenation of di-
nitrotoluene.
(T)
93
K113
Condensed liquid light ends from the purification of toluenedi-
amine in the production of toluenediamine via hydrogenation of
dinitrotoluene.
(T)
K114
Vicinals from the purification of toluenediamine in the
production of toluenediamine via hydrogenation of
dinitrotoluene.
(T)
K115
Heavy ends from the purification of toluenediamine in the
production of toluenediamine via hydrogenation of di-
nitrotoluene.
(T)
K116
Organic condensate from the solvent recovery column in the
production of toluene diisocyanate via phosgenation of
toluenediamine.
(T)
K117
Wastewater from the reactor vent gas scrubber in the production
of ethylene dibromide via bromination of ethene.
(T)
K118
Spent adsorbent solids from purification of ethylene dibromide
in the production of ethylene dibromide via bromination of
ethene.
(T)
K136
Still bottoms from the purification of ethylene dibromide in the
production of ethylene dibromide via bromination of ethene.
(T)
K140
Floor sweepings, off-specification product and spent filter
media from the production of 2,4,6-tribromophenol.
(T)
K156
Organic waste (including heavy ends, still bottoms, light ends,
spent solvents, filtrates, and decantates) from the production of
carbamates and carbamoyl oximes. (This listing does not apply
to wastes generated from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
K157
Wastewaters (including scrubber waters, condenser waters,
washwaters, and separation waters) from the production of
carbamates and carbamoyl oximes. (This listing does not apply
to wastes generated from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
94
K158
Bag house dusts and filter/separation solids from the production
of carbamates and carbamoyl oximes. (This listing does not
apply to wastes generated from the manufacture of 3-iodo-2-
propynyl n-butylcarbamate.)
(T)
K159
Organics from the treatment of thiocarbamate wastes.
(T)
K161
Purification solids (including filtration, evaporation, and
centrifugation solids), bag house dust and floor sweepings from
the production of dithiocarbamate acids and their salts. (This
listing does not include K125 or K126.)
(R,T)
Inorganic Chemicals:
K071
Brine purification muds from the mercury cell process in
chlorine production, where separately prepurified brine is not
used.
(T)
K073
Chlorinated hydrocarbon waste from the purification step of the
diaphragm cell process using graphite anodes in chlorine
production.
(T)
K106
Wastewater treatment sludge from the mercury cell process in
chlorine production.
(T)
Pesticides:
K031
By-product salts generated in the production of MSMA and
cacodylic acid.
(T)
K032
Wastewater treatment sludge from the production of chlordane.
(T)
K033
Wastewater and scrub water from the chlorination of
cyclopentadiene in the production of chlordane.
(T)
K034
Filter solids from the filtration of hexachlorocyclopentadiene in
the production of chlordane.
(T)
K097
Vacuum stripper discharge from the chlordane chlorinator in the
production of chlordane.
(T)
K035
Wastewater treatment sludges generated in the production of
creosote.
(T)
95
K036
Still bottoms from toluene reclamation distillation in the
production of disulfoton.
(T)
K037
Wastewater treatment sludges from the production of disulfoton. (T)
K038
Wastewater from the washing and stripping of phorate
production.
(T)
K039
Filter cake from the filtration of diethylphosphorodithioic acid
in the production of phorate.
(T)
K040
Wastewater treatment sludge from the production of phorate.
(T)
K041
Wastewater treatment sludge from the production of toxaphene.
(T)
K098
Untreated process wastewater from the production of
toxaphene.
(T)
K042
Heavy ends or distillation residues from the distillation of tetra-
chlorobenzene in the production of 2,4,5-T.
(T)
K043
2,6-Dichlorophenol waste from the production of 2,4-D.
(T)
K099
Untreated wastewater from the production of 2,4-D.
(T)
K123
Process wastewater (including supernates, filtrates and
washwaters) from the production of ethylenebisdithiocarbamic
acid and its salts.
(T)
K124
Reactor vent scrubber water from the production of ethylenebis-
dithiocarbamic acid and its salts.
(C,T)
K125
Filtration, evaporation and centrifugation solids from the
production of ethylenebisdithiocarbamic acid and its salts.
(T)
K126
Baghouse dust and floor sweepings in milling and packaging
operations from the production or formulation of ethylenebisdi-
thiocarbamic acid and its salts.
(T)
K131
Wastewater from the reactor and spent sulfuric acid from the
acid dryer from the production of methyl bromide.
(C,T)
K132
Spent absorbent and wastewater separator solids from the
production of methyl bromide.
(T)
96
Explosives:
K044
Wastewater treatment sludges from the manufacturing and
processing of explosives.
(R)
K045
Spent carbon from the treatment of wastewater containing
explosives.
(R)
K046
Wastewater treatment sludges from the manufacturing,
formulation and loading of lead-based initiating compounds.
(T)
K047
Pink/red water from TNT operations.
(R)
Petroleum Refining:
K048
Dissolved air flotation (DAF) float from the petroleum refining
industry.
(T)
K049
Slop oil emulsion solids from the petroleum refining industry.
(T)
K050
Heat exchanger bundle cleaning sludge from the petroleum
refining industry.
(T)
K051
API separator sludge from the petroleum refining industry.
(T)
K052
Tank bottoms (leaded) from the petroleum refining industry.
(T)
K169
Crude oil storage tank sediment from petroleum refining
operations.
(T)
K170
Clarified slurry oil tank sediment or in-line filter/separation
solids from petroleum refining operations.
(T)
K171
Spent hydrotreating catalyst from petroleum refining operations,
including guard beds used to desulfurize feeds to other catalytic
reactors (this listing does not include inert support media).
(I,T)
K172
Spent hydrorefining catalyst from petroleum refining operations,
including guard beds used to desulfurize feeds to other catalytic
reactors (this listing does not include inert support media).
(I,T)
Iron and Steel:
K061
Emission control dust/sludge from the primary production of
steel in electric furnaces.
(T)
97
K062
Spent pickle liquor generated by steel finishing operations of
facilities within the iron and steel industry (SIC Codes 331 and
332) (as defined in 35 Ill. Adm. Code 720.110).
(C,T)
Primary Copper:
K064
Acid plant blowdown slurry or sludge resulting from the
thickening of blowdown slurry from primary copper production.
(T)
Primary Lead:
K065
Surface impoundment solids contained in and dredged from
surface impoundments at primary lead smelting facilities.
(T)
Primary Zinc:
K066
Sludge from treatment of process wastewater or acid plant
blowdown from primary zinc production.
(T)
BOARD NOTE: This waste listing is the subject of a judicial remand in American Mining
Congress v. EPA, 907 F.2d 1179 (D.D.C. 1990). The Board intends that this listing not
become enforceable in Illinois until the first date upon which the Board RCRA program
becomes “not equivalent to the Federal program”, within the meaning of section 3006(b) of
the RCRA Act, 42 U.S.C. USC 6926(b), the Board RCRA rules become “less stringent” than
the USEPA rules, as this phrase is used in section 3009, 42 U.S.C. USC 6929, or the Board
RCRA rules are not “identical in substance” with the federal rules as that term is intended by
415 ILCS 5/7.2 and 22.4 as a result of some action by USEPA with regard to this listing in
response to the American Mining Congress remand.
Primary Aluminum:
K088
Spent potliners from primary aluminum reduction.
(T)
Ferroalloys:
K090
Emission control dust or sludge from ferrochromiumsilicon
production.
(T)
K091
Emission control dust or sludge from ferrochromium
production.
(T)
Secondary Lead:
K069
Emission control dust/sludge from secondary lead smelting.
(T)
98
BOARD NOTE: This listing is administratively stayed for sludge generated from secondary
acid scrubber systems. The stay will remain in effect until this note is removed.
K100
Waste leaching solution from acid leaching of emission control
dust/sludge from secondary lead smelting.
(T)
Veterinary Pharmaceuticals:
K084
Wastewater treatment sludges generated during the production
of veterinary pharmaceuticals from arsenic or organo-arsenic
compounds.
(T)
K101
Distillation tar residues from the distillation of aniline-based
compounds in the production of veterinary pharmaceuticals
from arsenic or organo-arsenic compounds.
(T)
K102
Residue from use of activated carbon for decolorization in the
production of veterinary pharmaceuticals from arsenic or
organo-arsenic compounds.
(T)
Ink Formulation:
K086
Solvent washes and sludges, caustic washes and sludges, or
water washes and sludges from cleaning tubs and equipment
used in the formulation of ink from pigments, dryers, soaps and
stabilizers containing chromium and lead.
(T)
Coking:
K060
Ammonia still lime sludge from coking operations.
(T)
K087
Decanter tank tar sludge from coking operations.
(T)
K141
Process residues from the recovery of coal tar, including, but
not limited to, collecting sump residues from the production of
coke from coal or the recovery of coke by-products produced
from coal. This listing does not include K087 (decanter tank tar
sludges from coking operations).
(T)
K142
Tar storage tank residues from the production of coke from coal
or from the recovery of coke by-products produced from coal.
(T)
99
K143
Process residues from the recovery of light oil, including, but
not limited to, those generated in stills, decanters, and wash oil
recovery units from the recovery of coke by-products produced
from coal.
(T)
K144
Wastewater sump residues from light oil refining, including, but
not limited to, intercepting or contamination sump sludges from
the recovery of coke by-products produced from coal.
(T)
K145
Residues from naphthalene collection and recovery operations
from the recovery of coke by-products produced from coal.
(T)
K147
Tar storage tank residues from coal tar refining.
(T)
K148
Residues from coal tar distillation, including but not limited to,
still bottoms.
(T)
K149
Distillation bottoms from the production of
α-
(or methyl-)
chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional
groups. (This waste does not include still bottoms from the
distillation of benzyl chloride.)
(T)
K150
Organic residuals, excluding spent carbon adsorbent, from the
spent chlorine gas and hydrochloric acid recovery processes
associated with the production of
α-
(or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and
compounds with mixtures of these functional groups.
(T)
K151
Wastewater treatment sludges, excluding neutralization and
biological sludges, generated during the treatment of
wastewaters from the production of
α-
(or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and
compounds with mixtures of these functional groups.
(T)
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.133
Discarded Commercial Chemical Products, Off-Specification Species,
Container Residues, and Spill Residues Thereof
The following materials or items are hazardous wastes if and when they are discarded or
intended to be discarded as described in Section 721.102(a)(2)(A), when they are mixed with
waste oil or used oil or other material and applied to the land for dust suppression or road
treatment, when they are otherwise applied to the land in lieu of their original intended use or
when they are contained in products that are applied to land in lieu of their original intended
100
use, or when, in lieu of their original intended use, they are produced for use as (or as a
component of) a fuel, distributed for use as a fuel, or burned as a fuel.
a)
Any commercial chemical product, or manufacturing chemical intermediate
having the generic name listed in subsection (e) or (f) of this Section.
b)
Any off-specification commercial chemical product or manufacturing chemical
intermediate which, if it met specifications, would have the generic name listed
in subsection (e) or (f) of this Section.
c)
Any residue remaining in a container or inner liner removed from a container
that has held any commercial chemical product or manufacturing chemical
intermediate having the generic name listed in subsection (e) or (f) of this
Section, unless the container is empty as defined in Section 721.107(b)(3).
BOARD NOTE: Unless the residue is being beneficially used or reused, or
legitimately recycled or reclaimed, or being accumulated, stored, transported,
or treated prior to such use, reuse, recycling, or reclamation, the Board
considers the residue to be intended for discard, and thus a hazardous waste.
An example of a legitimate reuse of the residue would be where the residue
remains in the container and the container is used to hold the same commercial
chemical product or manufacturing chemical intermediate it previously held.
An example of the discard of the residue would be where the drum is sent to a
drum reconditioner that reconditions the drum but discards the residue.
d)
Any residue or contaminated soil, water, or other debris resulting from the
cleanup of a spill into or on any land or water of any commercial chemical
product or manufacturing chemical intermediate having the generic name listed
in subsection (e) or (f) of this Section, or any residue or contaminated soil,
water, or other debris resulting from the cleanup of a spill into or on any land
or water, of any off-specification chemical product or manufacturing chemical
intermediate which, if it met specifications, would have the generic name listed
in subsection (e) or (f) of this Section.
BOARD NOTE: The phrase “commercial chemical product or manufacturing
chemical intermediate having the generic name listed in ...” refers to a chemical
substance that is manufactured or formulated for commercial or manufacturing
use which consists of the commercially pure grade of the chemical, any
technical grades of the chemical that are produced or marketed, and all
formulations in which the chemical is the sole active ingredient. It does not
refer to a material, such as a manufacturing process waste, that contains any of
the substances listed in subsection (e) or (f) of this Section. Where a
manufacturing process waste is deemed to be a hazardous waste because it
contains a substance listed in subsection (e) or (f) of this Section, such waste
101
will be listed in either Sections 721.131 or 721.132 or will be identified as a
hazardous waste by the characteristics set forth in Subpart C.
e)
The commercial chemical products, manufacturing chemical intermediates, or
off-specification commercial chemical products or manufacturing chemical
intermediates referred to in subsections (a) through (d) of this Section, are
identified as acute hazardous waste (H) and are subject to the small quantity
exclusion defined in Section 721.105(e). These wastes and their corresponding
USEPA Hazardous Waste Numbers are:
BOARD NOTE: For the convenience of the regulated community the primary
hazardous properties of these materials have been indicated by the letters T
(Toxicity), and R (Reactivity). The absence of a letter indicates that the
compound only is listed for acute toxicity.
USEPA
Hazardous
Waste No.
Chemical
Abstracts No.
(CAS No.)
Substance
P023
107-20-0
Acetaldehyde, chloro-
P002
591-08-2
Acetamide, N-(aminothioxomethyl)
P057
640-19-7
Acetamide, 2-fluoro-
P058
62-74-8
Acetic acid, fluoro-, sodium salt
P002
591-08-2
1-Acetyl-2-thiourea
P003
107-02-8
Acrolein
P070
116-06-3
Aldicarb
P203
1646-88-4
Aldicarb sulfone
P004
309-00-2
Aldrin
P005
107-18-6
Allyl alcohol
P006
20859-73-8
Aluminum phosphide (R,T)
P007
2763-96-4
5-(Aminomethyl)-3-isoxazolol
P008
504-24-5
4-Aminopyridine
P009
131-74-8
Ammonium picrate (R)
P119
7803-55-6
Ammonium vanadate
P099
506-61-6
Argentate(1-), bis(cyano-C)-, potassium
P010
7778-39-4
Arsenic acid H3AsO4
P012
1327-53-3
Arsenic oxide As2O3
P011
1303-28-2
Arsenic oxide As2O5
P011
1303-28-2
Arsenic pentoxide
P012
1327-53-3
Arsenic trioxide
P038
692-42-2
Arsine, diethyl-
P036
696-28-6
Arsonous dichloride, phenyl-
P054
151-56-4
Aziridine
P067
75-55-8
Aziridine, 2-methyl
P013
542-62-1
Barium cyanide
102
P024
106-47-8
Benzenamine, 4-chloro-
P077
100-01-6
Benzenamine, 4-nitro-
P028
100-44-7
Benzene, (chloromethyl)-
P042
51-43-4
1,2-Benzenediol, 4-[1-hydroxy-2-(methyl-
amino)ethyl]-, (R)-
P046
122-09-8
Benzeneethanamine,
α
,
α-dimethyl-
P014
108-98-5
Benzenethiol
P127
1563-66-2
7-Benzofuranol, 2,3-dihydro-2,2-dimethyl-,
methylcarbamate
P188
57-64-7
Benzoic acid, 2-hydroxy-, compound with (3aS-
cis)-1,2,3,3a,8,8a-hexahydro-1,3a,8-trimethyl-
pyrrolo[2,3-b]indol-5-yl methylcarbamate ester
(1:1)
P001
81-81-2
*
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-
phenylbutyl)-, and salts, when present at
concentrations greater than 0.3 percent
P028
100-44-7
Benzyl chloride
P015
7440-41-7
Beryllium powder
P017
598-31-2
Bromoacetone
P018
357-57-3
Brucine
P045
39196-18-6
2-Butanone,3,3-dimethyl-1-(methylthio)-, O-
[methylamino)carbonyl] oxime
P021
592-01-8
Calcium cyanide
P021
592-01-8
Calcium cyanide Ca(CN)2
P189
55285-14-8
Carbamic acid, [(dibutylamino)- thio]methyl-,
2,3-dihydro-2,2-dimethyl-7-benzofuranyl ester
P191
644-64-4
Carbamic acid, dimethyl-, 1-[(dimethyl-amino)-
carbonyl]-5-methyl-1H-pyrazol-3-yl ester
P192
119-38-0
Carbamic acid, dimethyl-, 3-methyl-1-(1-
methylethyl)-1H-pyrazol-5-yl ester
P190
1129-41-5
Carbamic acid, methyl-, 3-methylphenyl ester
P127
1563-66-2
Carbofuran
P022
75-15-0
Carbon disulfide
P095
75-44-5
Carbonic dichloride
P189
55285-14-8
Carbosulfan
P023
107-20-0
Chloroacetaldehyde
P024
106-47-8
p-Chloroaniline
P026
5344-82-1
1-(o-Chlorophenyl)thiourea
P027
542-76-7
3-Chloropropionitrile
P029
544-92-3
Copper cyanide
P029
544-92-3
Copper cyanide CuCN
P202
64-00-6
m-Cumenyl methylcarbamate
P030
Cyanides (soluble cyanide salts), not otherwise
specified
P031
460-19-5
Cyanogen
103
P033
506-77-4
Cyanogen chloride
P033
506-77-4
Cyanogen chloride CNCl
P034
131-89-5
2-Cyclohexyl-4,6-dinitrophenol
P016
542-88-1
Dichloromethyl ether
P036
696-28-6
Dichlorophenylarsine
P037
60-57-1
Dieldrin
P038
692-42-2
Diethylarsine
P041
311-45-5
Diethyl-p-nitrophenyl phosphate
P040
297-97-2
O,O-Diethyl O-pyrazinyl phosphorothioate
P043
55-91-4
Diisopropylfluorophosphate (DFP)
P191
644-64-4
Dimetilan
P004
309-00-2
1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-hexahydro-,
(1α,4α,4aβ,5α,8α,8aβ)-
P060
465-73-6
1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-hexahydro-,
(1α,4α,4aβ,5β,8β,8aβ)-
P037
60-57-1
2,7:3,6-Dimethanonaphth[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-1a,2,2a,3,6,6a,7,7a-
octahydro-, (1aα,2β,2aα,3β,6β,6aα,7β,7aα)-
P051
72-20-8
*
2,7:3,6-Dimethanonaphth[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-1a,2,2a,3,6,6a,7,7a-
octahydro-, (1aα,2β,2aβ,3α,6α,6aβ,7β,7aα)-,
and metabolites
P044
60-51-5
Dimethoate
P046
122-09-8
α
,
α-Dimethylphenethylamine
P047
534-52-1
*
4,6-Dinitro-o-cresol and salts
P048
51-28-5
2,4-Dinitrophenol
P020
88-85-7
Dinoseb
P085
152-16-9
Diphosphoramide, octamethyl-
P111
107-49-3
Diphosphoric acid, tetraethyl ester
P039
298-04-4
Disulfoton
P049
541-53-7
Dithiobiuret
P185
26419-73-8
1,3-Dithiolane-2-carboxaldehyde, 2,4-dimethyl-
, O-[(methylamino)- carbonyl]oxime
P050
115-29-7
Endosulfan
P088
145-73-3
Endothall
P051
72-20-8
Endrin
P051
72-20-8
Endrin, and metabolites
P042
51-43-4
Epinephrine
P031
460-19-5
Ethanedinitrile
P194
23135-22-0
Ethanimidothioc acid, 2-(dimethylamino)-N-
[[(methylamino)carbonyl]oxy]-2-oxo-, methyl
ester
104
P066
16752-77-5
Ethanimidothioic acid, N-[[(methylamino)-
carbonyl]oxy]-, methyl ester
P101
107-12-0
Ethyl cyanide
P054
151-56-4
Ethylenimine
P097
52-85-7
Famphur
P056
7782-41-4
Fluorine
P057
640-19-7
Fluoroacetamide
P058
62-74-8
Fluoroacetic acid, sodium salt
P198
23422-53-9
Formetanate hydrochloride
P197
17702-57-7
Formparanate
P065
628-86-4
Fulminic acid, mercury (2+) salt (R,T)
P059
76-44-8
Heptachlor
P062
757-58-4
Hexaethyl tetraphosphate
P116
79-19-6
Hydrazinecarbothioamide
P068
60-34-4
Hydrazine, methyl-
P063
74-90-8
Hydrocyanic acid
P063
74-90-8
Hydrogen cyanide
P096
7803-51-2
Hydrogen phosphide
P060
465-73-6
Isodrin
P192
119-38-0
Isolan
P202
64-00-6
3-Isopropylphenyl-N-methylcarbamate
P007
2763-96-4
3(2H)-Isoxazolone, 5-(aminomethyl)-
P196
15339-36-3
Manganese, bis(dimethylcarbamodithioato-
S,S’)-
P196
15339-36-3
Manganese dimethyldithiocarbamate
P092
62-38-4
Mercury, (acetato-O)phenyl-
P065
628-86-4
Mercury fulminate (R,T)
P082
62-75-9
Methanamine, N-methyl-N-nitroso-
P064
624-83-9
Methane, isocyanato-
P016
542-88-1
Methane, oxybis[chloro-
P112
509-14-8
Methane, tetranitro- (R)
P118
75-70-7
Methanethiol, trichloro-
P198
23422-53-9
Methanimidamide, N,N-dimethyl-N’-[3-
[[(methylamino)-carbonyl]oxy]phenyl]-,
monohydrochloride
P197
17702-57-7
Methanimidamide, N,N-dimethyl-N’-[2-methyl-
4-[[(methylamino)carbonyl]oxy]phenyl]-
P199
2032-65-7
Methiocarb
P050
115-29-7
6,9-Methano-2,4,3-benzodioxathiepen,
6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexa-
hydro-, 3-oxide
P059
76-44-8
4,7-Methano-1H-indene, 1,4,5,6,7,8,8-hepta-
chloro-3a,4,7,7a-tetrahydro-
P066
16752-77-5
Methomyl
P068
60-34-4
Methyl hydrazine
105
P064
624-83-9
Methyl isocyanate
P069
75-86-5
2-Methyllactonitrile
P071
298-00-0
Methyl parathion
P190
1129-41-5
Metolcarb
P129
315-8-4
Mexacarbate
P072
86-88-4
α-Naphthylthiourea
P073
13463-39-3
Nickel carbonyl
P073
13463-39-3
Nickel carbonyl Ni(CO)4, (T-4)-
P074
557-19-7
Nickel cyanide
P074
557-19-7
Nickel cyanide Ni(CN)2
P075
54-11-5
*
Nicotine, and salts
P076
10102-43-9
Nitric oxide
P077
100-01-6
p-Nitroaniline
P078
10102-44-0
Nitrogen dioxide
P076
10102-43-9
Nitrogen oxide NO
P078
10102-44-0
Nitrogen oxide NO2
P081
55-63-0
Nitroglycerine (R)
P082
62-75-9
N-Nitrosodimethylamine
P084
4549-40-0
N-Nitrosomethylvinylamine
P085
152-16-9
Octamethylpyrophosphoramide
P087
20816-12-0
Osmium oxide OsO4, (T-4)-
P087
20816-12-0
Osmium tetroxide
P088
145-73-3
7-Oxabicyclo[2.2.1]heptane-2,3-dicarboxylic
acid
P194
23135-22-0
Oxamyl
P089
56-38-2
Parathion
P034
131-89-5
Phenol, 2-cyclohexyl-4,6-dinitro-
P128
315-18-4
Phenol, 4-(dimethylamino)-3,5-dimethyl-,
methylcarbamate (ester)
P199
2032-65-7
Phenol, (3,5-dimethyl-4-(methylthio)-, methyl-
carbamate
P048
51-28-5
Phenol, 2,4-dinitro-
P047
534-52-1
*
Phenol, 2-methyl-4,6-dinitro-, and salts
P202
64-00-6
Phenol, 3-(1-methylethyl)-, methyl carbamate
P201
2631-37-0
Phenol, 3-methyl-5-(1-methylethyl)-, methyl
carbamate
P020
88-85-7
Phenol, 2-(1-methylpropyl)-4,6-dinitro-
P009
131-74-8
Phenol, 2,4,6-trinitro-, ammonium salt (R)
P092
62-38-4
Phenylmercury acetate
P093
103-85-5
Phenylthiourea
P094
298-02-2
Phorate
P095
75-44-5
Phosgene
P096
7803-51-2
Phosphine
P041
311-45-5
Phosphoric acid, diethyl 4-nitrophenyl ester
106
P039
298-04-4
Phosphorodithioic acid, O,O-diethyl S-[2-
(ethylthio)ethyl] ester
P094
298-02-2
Phosphorodithioic acid, O,O-diethyl S-[(ethyl-
thio)methyl] ester
P044
60-51-5
Phosphorodithioic acid, O,O-dimethyl S-[2-
(methylamino)-2-oxoethyl]ester
P043
55-91-4
Phosphorofluoridic acid, bis(1-methylethyl)ester
P089
56-38-2
Phosphorothioic acid, O,O-diethyl O-(4-
nitrophenyl) ester
P040
297-97-2
Phosphorothioic acid, O,O-diethyl O-pyrazinyl
ester
P097
52-85-7
Phosphorothioic acid, O-[4-[(dimethylamino)-
sulfonyl)]phenyl] O,O-dimethyl ester
P071
298-00-0
Phosphorothioic acid, O,O-dimethyl O-(4-
nitrophenyl) ester
P204
57-47-6
Physostigmine
P188
57-64-7
Physostigmine salicylate
P110
78-00-2
Plumbane, tetraethyl-
P098
151-50-8
Potassium cyanide
P098
151-50-8
Potassium cyanide KCN
P099
506-61-6
Potassium silver cyanide
P201
2631-37-0
Promecarb
P203
1646-88-4
Propanal, 2-methyl-2-(methyl-sulfonyl)-, O-
[(methylamino)carbonyl] oxime
P070
116-06-3
Propanal, 2-methyl-2-(methylthio)-, O-
[(methylamino)carbonyl]oxime
P101
107-12-0
Propanenitrile
P027
542-76-7
Propanenitrile, 3-chloro-
P069
75-86-5
Propanenitrile, 2-hydroxy-2-methyl-
P081
55-63-0
1,2,3-Propanetriol, trinitrate- (R)
P017
598-31-2
2-Propanone, 1-bromo-
P102
107-19-7
Propargyl alcohol
P003
107-02-8
2-Propenal
P005
107-18-6
2-Propen-1-ol
P067
75-55-8
1,2-Propylenimine
P102
107-19-7
2-Propyn-1-ol
P008
504-24-5
4-Pyridinamine
P075
54-11-5
*
Pyridine, 3-(1-methyl-2-pyrrolidinyl)-, (S)- and
salts
P204
57-47-6
Pyrrolo[2,3-b]indol-5-ol, 1,2,3,3a,8,8a-hexa-
hydro-1,3a,8-trimethyl-, methylcarbamate
(ester), (3aS-cis)-
P114
12039-52-0
Selenious acid, dithallium (1+) salt
P103
630-10-4
Selenourea
P104
506-64-9
Silver cyanide
107
P104
506-64-9
Silver cyanide AgCN
P105
26628-22-8
Sodium azide
P106
143-33-9
Sodium cyanide
P106
143-33-9
Sodium cyanide NaCN
P108
57-24-9
*
Strychnidin-10-one, and salts
P018
357-57-3
Strychnidin-10-one, 2,3-dimethoxy-
P108
57-24-9
*
Strychnine and salts
P115
7446-18-6
Sulfuric acid, dithallium (1+) salt
P109
3689-24-5
Tetraethyldithiopyrophosphate
P110
78-00-2
Tetraethyl lead
P111
107-49-3
Tetraethylpyrophosphate
P112
509-14-8
Tetranitromethane (R)
P062
757-58-4
Tetraphosphoric acid, hexaethyl ester
P113
1314-32-5
Thallic oxide
P113
1314-32-5
Thallium oxide Tl2O3
P114
12039-52-0
Thallium (I) selenite
P115
7446-18-6
Thallium (I) sulfate
P109
3689-24-5
Thiodiphosphoric acid, tetraethyl ester
P045
39196-18-4
Thiofanox
P049
541-53-7
Thioimidodicarbonic diamide [(H2N)C(S)]2NH
P014
108-98-5
Thiophenol
P116
79-19-6
Thiosemicarbazide
P026
5344-82-1
Thiourea, (2-chlorophenyl)-
P072
86-88-4
Thiourea, 1-naphthalenyl-
P093
103-85-5
Thiourea, phenyl-
P123
8001-35-2
Toxaphene
P185
26419-73-8
Tirpate
P118
75-70-7
Trichloromethanethiol
P119
7803-55-6
Vanadic acid, ammonium salt
P120
1314-62-1
Vanadium oxide V2O5
P120
1314-62-1
Vanadium pentoxide
P084
4549-40-0
Vinylamine, N-methyl-N-nitroso-
P001
81-81-2
*
Warfarin, and salts, when present at
concentrations greater than 0.3 percent
P121
557-21-1
Zinc cyanide
P121
557-21-1
Zinc cyanide Zn(CN)2
P205
137-30-4
Zinc, bis(dimethylcarbamodithioato-S,S’)-
P122
1314-84-7
Zinc phosphide Zn3P2, when present at
concentrations greater than 10% percent (R,T)
P205
137-30-4
Ziram
BOARD NOTE: An asterisk (*) following the CAS number indicates that the
CAS number is given for the parent compound only.
108
f)
The commercial chemical products, manufacturing chemical intermediates, or
off-specification commercial chemical products referred to in subsections (a)
through (d) of this Section, are identified as toxic wastes (T) unless otherwise
designated and are subject to the small quantity exclusion defined in Section
721.105(a) and (g). These wastes and their corresponding USEPA Hazardous
Waste Numbers are:
BOARD NOTE: For the convenience of the regulated community, the primary
hazardous properties of these materials have been indicated by the letters T
(Toxicity), R (Reactivity), I (Ignitability), and C (Corrosivity). The absence of
a letter indicates that the compound is only listed for toxicity.
USEPA
Hazardous
Waste No.
Chemical
Abstracts No.
(CAS No.)
Substance
U394
30558-43-1
A2213
U001
75-07-0
Acetaldehyde (I)
U034
75-87-6
Acetaldehyde, trichloro-
U187
62-44-2
Acetamide, N-(4-ethoxyphenyl)-
U005
53-96-3
Acetamide, N-9H-fluoren-2-yl-
U240
P 94-75-7
Acetic acid, (2,4-dichlorophenoxy)-, salts and
esters
U112
141-78-6
Acetic acid, ethyl ester (I)
U144
301-04-2
Acetic acid, lead (2+) salt
U214
563-68-8
Acetic acid, thallium (1+) salt
See F027
93-76-5
Acetic acid, (2,4,5-trichlorophenoxy)-
U002
67-64-1
Acetone (I)
U003
75-05-8
Acetonitrile (I,T)
U004
98-86-2
Acetophenone
U005
53-96-3
2-Acetylaminofluorene
U006
75-36-5
Acetyl chloride (C,R,T)
U007
79-06-1
Acrylamide
U008
79-10-7
Acrylic acid (I)
U009
107-13-1
Acrylonitrile
U011
61-82-5
Amitrole
U012
62-53-3
Aniline (I,T)
U136
75-60-5
Arsinic acid, dimethyl-
U014
492-80-8
Auramine
U015
115-02-6
Azaserine
U010
50-07-7
Azirino[2',3':3,4]pyrrolo[1,2-a]indole-4,7-di-
one, 6-amino-8-[[(aminocarbonyl)oxy]methyl]-
1,1a,2,8,8a,8b-hexahydro-8a-methoxy-5-
methyl-, [1a-S-(1aα,8β,8aα,8bα)]-
U280
101-27-9
Barban
109
U278
22781-23-3
Bendiocarb
U364
22961-82-6
Bendiocarb phenol
U271
17804-35-2
Benomyl
U157
56-49-5
Benz[j]aceanthrylene, 1,2-dihydro-3-methyl-
U016
225-51-4
Benz(c)acridine
U017
98-87-3
Benzal chloride
U192
23950-58-5
Benzamide, 3,5-dichloro-N-(1,1-dimethyl-2-
propynyl)-
U018
56-55-3
Benz[a]anthracene
U094
57-97-6
Benz[a]anthracene, 7,12-dimethyl-
U012
62-53-3
Benzenamine (I,T)
U014
492-80-8
Benzenamine, 4,4'-carbonimidoylbis[N,N-di-
methyl-
U049
3165-93-3
Benzenamine, 4-chloro-2-methyl-,
hydrochloride
U093
60-11-7
Benzenamine, N,N-dimethyl-4-(phenylazo)-
U328
95-53-4
Benzenamine, 2-methyl-
U353
106-49-0
Benzenamine, 4-methyl-
U158
101-14-4
Benzenamine, 4,4'-methylenebis[2-chloro-
U222
636-21-5
Benzenamine, 2-methyl-, hydrochloride
U181
99-55-8
Benzenamine, 2-methyl-5-nitro-
U019
71-43-2
Benzene (I,T)
U038
510-15-6
Benzeneacetic acid, 4-chloro-α-(4-chloro-
phenyl)-α-hydroxy-, ethyl ester
U030
101-55-3
Benzene, 1-bromo-4-phenoxy-
U035
305-03-3
Benzenebutanoic acid, 4-[bis(2-chloroethyl)-
amino]-
U037
108-90-7
Benzene, chloro-
U221
25376-45-8
Benzenediamine, ar-methyl-
U028
117-81-7
1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl)
ester
U069
84-74-2
1,2-Benzenedicarboxylic acid, dibutyl ester
U088
84-66-2
1,2-Benzenedicarboxylic acid, diethyl ester
U102
131-11-3
1,2-Benzenedicarboxylic acid, dimethyl ester
U107
117-84-0
1,2-Benzenedicarboxylic acid, dioctyl ester
U070
95-50-1
Benzene, 1,2-dichloro-
U071
541-73-1
Benzene, 1,3-dichloro-
U072
106-46-7
Benzene, 1,4-dichloro-
U060
72-54-8
Benzene, 1,1'-(2,2-dichloroethylidene)bis[4-
chloro-
U017
98-87-3
Benzene, (dichloromethyl)-
U223
26471-62-5
Benzene, 1,3-diisocyanatomethyl- (R,T)
U239
1330-20-7
Benzene, dimethyl- (I,T)
U201
108-46-3
1,3-Benzenediol
U127
118-74-1
Benzene, hexachloro-
110
U056
110-82-7
Benzene, hexahydro- (I)
U220
108-88-3
Benzene, methyl-
U105
121-14-2
Benzene, 1-methyl-2,4-dinitro-
U106
606-20-2
Benzene, 2-methyl-1,3-dinitro-
U055
98-82-8
Benzene, (1-methylethyl)- (I)
U169
98-95-3
Benzene, nitro-
U183
608-93-5
Benzene, pentachloro-
U185
82-68-8
Benzene, pentachloronitro-
U020
98-09-9
Benzenesulfonic acid chloride (C,R)
U020
98-09-9
Benzenesulfonyl chloride (C,R)
U207
95-94-3
Benzene, 1,2,4,5-tetrachloro-
U061
50-29-3
Benzene, 1,1'-(2,2,2-trichloroethylidene)bis[4-
chloro-
U247
72-43-5
Benzene, 1,1'-(2,2,2-trichloroethylidene)bis[4-
methoxy-
U023
98-07-7
Benzene, (trichloromethyl)-
U234
99-35-4
Benzene, 1,3,5-trinitro-
U021
92-87-5
Benzidene
U202
P 81-07-2
1,2-Benzisothiazol-3(2H)-one, 1,1-dioxide, and
salts
U203
94-59-7
1,3-Benzodioxole, 5-(2-propenyl)-
U141
120-58-1
1,3-Benzodioxole, 5-(1-propenyl)-
U090
94-58-6
1,3-Benzodioxole, 5-propyl-
U278
22781-23-3
1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl
carbamate
U364
22961-82-6
1,3-Benzodioxol-4-ol, 2,2-dimethyl-
U367
1563-38-8
7-Benzofuranol, 2,3-dihydro-2,2-dimethyl-
U064
189-55-9
Benzo[rst]pentaphene
U248
P 81-81-2
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-
phenylbutyl)-, and salts, when present at
concentrations of 0.3 percent or less
U022
50-32-8
Benzo[a]pyrene
U197
106-51-4
p-Benzoquinone
U023
98-07-7
Benzotrichloride (C,R,T)
U085
1464-53-5
2,2'-Bioxirane
U021
92-87-5
[1,1'-Biphenyl]-4,4'-diamine
U073
91-94-1
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dichloro-
U091
119-90-4
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy-
U095
119-93-7
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethyl-
U225
75-25-2
Bromoform
U030
101-55-3
4-Bromophenyl phenyl ether
U128
87-68-3
1,3-Butadiene, 1,1,2,3,4,4-hexachloro-
U172
924-16-3
1-Butanamine, N-butyl-N-nitroso-
U031
71-36-3
1-Butanol (I)
U159
78-93-3
2-Butanone (I,T)
111
U160
1338-23-4
2-Butanone, peroxide (R,T)
U053
4170-30-3
2-Butenal
U074
764-41-0
2-Butene, 1,4-dichloro- (I,T)
U143
303-34-4
2-Butenoic acid, 2-methyl-, 7-[[2,3-dihydroxy-
2-(1-methoxyethyl)-3-methyl-1-oxobutoxy]-
methyl]-2,3,5,7a-tetrahydro-1H-pyrrolizin-1-yl
ester, [1S-[1α(Z), 7(2S*,3R*), 7aα]]-
U031
71-36-3
n-Butyl alcohol (I)
U136
75-60-5
Cacodylic acid
U032
13765-19-0
Calcium chromate
U372
10605-21-7
Carbamic acid, 1H-benzimidazol-2-yl, methyl
ester
U271
17804-35-2
Carbamic acid, [1-[(butylamino)carbonyl]-1H-
benzimidazol-2-yl]-, methyl ester
U280
101-27-9
Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-
butynyl ester
U238
51-79-6
Carbamic acid, ethyl ester
U178
615-53-2
Carbamic acid, methylnitroso-, ethyl ester
U373
122-42-9
Carbamic acid, phenyl-, 1-methylethyl ester
U409
23564-05-8
Carbamic acid, [1,2-phenylenebis(imino-
carbonothioyl)]bis-, dimethyl ester
U097
79-44-7
Carbamic chloride, dimethyl-
U114
P 111-54-6
Carbamodithioic acid, 1,2-ethanediylbis-, salts
and esters
U062
2303-16-4
Carbamothioic acid, bis(1-methylethyl)-, S-
(2,3-dichloro-2-propenyl) ester
U389
2303-17-5
Carbamothioic acid, bis(1-methylethyl)-, S-
(2,3,3-trichloro-2-propenyl) ester
U387
52888-80-9
Carbamothioic acid, dipropyl-, S-(phenyl-
methyl) ester
U279
63-25-2
Carbaryl
U372
10605-21-7
Carbendazim
U367
1563-38-8
Carbofuran phenol
U215
6533-73-9
Carbonic acid, dithallium (1+) salt
U033
353-50-4
Carbonic difluoride
U156
79-22-1
Carbonochloridic acid, methyl ester (I,T)
U033
353-50-4
Carbon oxyfluoride (R,T)
U211
56-23-5
Carbon tetrachloride
U034
75-87-6
Chloral
U035
305-03-3
Chlorambucil
U036
57-74-9
Chlordane,
α
and
γ
isomers
U026
494-03-1
Chlornaphazin
U037
108-90-7
Chlorobenzene
U038
510-15-6
Chlorobenzilate
U039
59-50-7
p-Chloro-m-cresol
112
U042
110-75-8
2-Chloroethyl vinyl ether
U044
67-66-3
Chloroform
U046
107-30-2
Chloromethyl methyl ether
U047
91-58-7
β-Chloronaphthalene
U048
95-57-8
o-Chlorophenol
U049
3165-93-3
4-Chloro-o-toluidine, hydrochloride
U032
13765-19-0
Chromic acid H2CrO4, calcium salt
U050
218-01-9
Chrysene
U051
Creosote
U052
1319-77-3
Cresol (Cresylic acid)
U053
4170-30-3
Crotonaldehyde
U055
98-82-8
Cumeme (I)
U246
506-68-3
Cyanogen bromide CNBr
U197
106-51-4
2,5-Cyclohexadiene-1,4-dione
U056
110-82-7
Cyclohexane (I)
U129
58-89-9
Cyclohexane, 1,2,3,4,5,6-hexachloro-,
(1α,2α,3β,4α,5α,6β)-
U057
108-94-1
Cyclohexanone (I)
U130
77-47-4
1,3-Cyclopentadiene, 1,2,3,4,5,5-hexachloro-
U058
50-18-0
Cyclophosphamide
U240
P 94-75-7
2,4-D, salts and esters
U059
20830-81-3
Daunomycin
U060
72-54-8
DDD
U061
50-29-3
DDT
U062
2303-16-4
Diallate
U063
53-70-3
Dibenz[a,h]anthracene
U064
189-55-9
Dibenzo[a,i]pyrene
U066
96-12-8
1,2-Dibromo-3-chloropropane
U069
84-74-2
Dibutyl phthalate
U070
95-50-1
o-Dichlorobenzene
U071
541-73-1
m-Dichlorobenzene
U072
106-46-7
p-Dichlorobenzene
U073
91-94-1
3,3'-Dichlorobenzidine
U074
764-41-0
1,4-Dichloro-2-butene (I,T)
U075
75-71-8
Dichlorodifluoromethane
U078
75-35-4
1,1-Dichloroethylene
U079
156-60-5
1,2-Dichloroethylene
U025
111-44-4
Dichloroethyl ether
U027
108-60-1
Dichloroisopropyl ether
U024
111-91-1
Dichloromethoxy ethane
U081
120-83-2
2,4-Dichlorophenol
U082
87-65-0
2,6-Dichlorophenol
U084
542-75-6
1,3-Dichloropropene
U085
1464-53-5
1,2:3,4-Diepoxybutane (I,T)
U395
5952-26-1
Diethylene glycol, dicarbamate
113
U108
123-91-1
1,4-Diethyleneoxide
U028
117-81-7
Diethylhexyl phthalate
U086
1615-80-1
N,N’-Diethylhydrazine
U087
3288-58-2
O,O-Diethyl S-methyl dithiophosphate
U088
84-66-2
Diethyl phthalate
U089
56-53-1
Diethylstilbestrol
U090
94-58-6
Dihydrosafrole
U091
119-90-4
3,3'-Dimethoxybenzidine
U092
124-40-3
Dimethylamine (I)
U093
60-11-7
p-Dimethylaminoazobenzene
U094
57-97-6
7,12-Dimethylbenz[a]anthracene
U095
119-93-7
3,3'-Dimethylbenzidine
U096
80-15-9
α
,
α-Dimethylbenzylhydroperoxide
(R)
U097
79-44-7
Dimethylcarbamoyl chloride
U098
57-14-7
1,1-Dimethylhydrazine
U099
540-73-8
1,2-Dimethylhydrazine
U101
105-67-9
2,4-Dimethylphenol
U102
131-11-3
Dimethyl phthalate
U103
77-78-1
Dimethyl sulfate
U105
121-14-2
2,4-Dinitrotoluene
U106
606-20-2
2,6-Dinitrotoluene
U107
117-84-0
Di-n-octyl phthalate
U108
123-91-1
1,4-Dioxane
U109
122-66-7
1,2-Diphenylhydrazine
U110
142-84-7
Dipropylamine (I)
U111
621-64-7
Di-n-propylnitrosamine
U041
106-89-8
Epichlorohydrin
U001
75-07-0
Ethanal (I)
U404
121-44-8
Ethanamine, N,N-diethyl-
U174
55-18-5
Ethanamine, N-ethyl-N-nitroso-
U155
91-80-5
1,2-Ethanediamine, N,N-dimethyl-N’-2-
pyridinyl-N’-(2-thienylmethyl)-
U067
106-93-4
Ethane, 1,2-dibromo-
U076
75-34-3
Ethane, 1,1-dichloro-
U077
107-06-2
Ethane, 1,2-dichloro-
U131
67-72-1
Ethane, hexachloro-
U024
111-91-1
Ethane, 1,1'-[methylenebis(oxy)]bis[2-chloro-
U117
60-29-7
Ethane, 1,1'-oxybis- (I)
U025
111-44-4
Ethane, 1,1'-oxybis[2-chloro-
U184
76-01-7
Ethane, pentachloro-
U208
630-20-6
Ethane, 1,1,1,2-tetrachloro-
U209
79-34-5
Ethane, 1,1,2,2-tetrachloro-
U218
62-55-5
Ethanethioamide
U226
71-55-6
Ethane, 1,1,1-trichloro-
U227
79-00-5
Ethane, 1,1,2-trichloro-
114
U410
59669-26-0
Ethanimidothioic acid, N,N’- [thiobis[(methyl-
imino)carbonyloxy]]bis-, dimethyl ester
U394
30558-43-1
Ethanimidothioic acid, 2-(dimethylamino)-N-
hydroxy-2-oxo-, methyl ester
U359
110-80-5
Ethanol, 2-ethoxy-
U173
1116-54-7
Ethanol, 2,2'-(nitrosoimino)bis-
U395
5952-26-1
Ethanol, 2,2'-oxybis-, dicarbamate
U004
98-86-2
Ethanone, 1-phenyl-
U043
75-01-4
Ethene, chloro-
U042
110-75-8
Ethene, (2-chloroethoxy)-
U078
75-35-4
Ethene, 1,1-dichloro-
U079
156-60-5
Ethene, 1,2-dichloro-, (E)-
U210
127-18-4
Ethene, tetrachloro-
U228
79-01-6
Ethene, trichloro-
U112
141-78-6
Ethyl acetate (I)
U113
140-88-5
Ethyl acrylate (I)
U238
51-79-6
Ethyl carbamate (urethane)
U117
60-29-7
Ethyl ether
U114
P 111-54-6
Ethylenebisdithiocarbamic acid, salts and esters
U067
106-93-4
Ethylene dibromide
U077
107-06-2
Ethylene dichloride
U359
110-80-5
Ethylene glycol monoethyl ether
U115
75-21-8
Ethylene oxide (I,T)
U116
96-45-7
Ethylenethiourea
U076
75-34-3
Ethylidene dichloride
U118
97-63-2
Ethyl methacrylate
U119
62-50-0
Ethyl methanesulfonate
U120
206-44-0
Fluoranthene
U122
50-00-0
Formaldehyde
U123
64-18-6
Formic acid (C,T)
U124
110-00-9
Furan (I)
U125
98-01-1
2-Furancarboxaldehyde (I)
U147
108-31-6
2,5-Furandione
U213
109-99-9
Furan, tetrahydro- (I)
U125
98-01-1
Furfural (I)
U124
110-00-9
Furfuran (I)
U206
18883-66-4
Glucopyranose, 2-deoxy-2-(3-methyl-3-nitroso-
ureido)-, D-
U206
18883-66-4
D-Glucose, 2-deoxy-2-[[(methylnitrosoamino)-
carbonyl]amino]-
U126
765-34-4
Glycidylaldehyde
U163
70-25-7
Guanidine, N-methyl-N’-nitro-N-nitroso-
U127
118-74-1
Hexachlorobenzene
U128
87-68-3
Hexachlorobutadiene
U130
77-47-4
Hexachlorocyclopentadiene
115
U131
67-72-1
Hexachloroethane
U132
70-30-4
Hexachlorophene
U243
1888-71-7
Hexachloropropene
U133
302-01-2
Hydrazine (R,T)
U086
1615-80-1
Hydrazine, 1,2-diethyl-
U098
57-14-7
Hydrazine, 1,1-dimethyl-
U099
540-73-8
Hydrazine, 1,2-dimethyl-
U109
122-66-7
Hydrazine, 1,2-diphenyl-
U134
7664-39-3
Hydrofluoric acid (C,T)
U134
7664-39-3
Hydrogen fluoride (C,T)
U135
7783-06-4
Hydrogen sulfide
U135
7783-06-4
Hydrogen sulfide H2S
U096
80-15-9
Hydroperoxide, 1-methyl-1-phenylethyl- (R)
U116
96-45-7
2-Imidazolidinethione
U137
193-39-5
Indeno[1,2,3-cd]pyrene
U190
85-44-9
1,3-Isobenzofurandione
U140
78-83-1
Isobutyl alcohol (I,T)
U141
120-58-1
Isosafrole
U142
143-50-0
Kepone
U143
303-34-4
Lasiocarpene
U144
301-04-2
Lead acetate
U146
1335-32-6
Lead, bis(acetato-O)tetrahydroxytri-
U145
7446-27-7
Lead phosphate
U146
1335-32-6
Lead subacetate
U129
58-89-9
Lindane
U163
70-25-7
MNNG
U147
108-31-6
Maleic anhydride
U148
123-33-1
Maleic hydrazide
U149
109-77-3
Malononitrile
U150
148-82-3
Melphalan
U151
7439-97-6
Mercury
U152
126-98-7
Methacrylonitrile (I,T)
U092
124-40-3
Methanamine, N-methyl- (I)
U029
74-83-9
Methane, bromo-
U045
74-87-3
Methane, chloro- (I,T)
U046
107-30-2
Methane, chloromethoxy-
U068
74-95-3
Methane, dibromo-
U080
75-09-2
Methane, dichloro-
U075
75-71-8
Methane, dichlorodifluoro-
U138
74-88-4
Methane, iodo-
U119
62-50-0
Methanesulfonic acid, ethyl ester
U211
56-23-5
Methane, tetrachloro-
U153
74-93-1
Methanethiol (I,T)
U225
75-25-2
Methane, tribromo-
U044
67-66-3
Methane, trichloro-
116
U121
75-69-4
Methane, trichlorofluoro-
U036
57-74-9
4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8-
octachloro-2,3,3a,4,7,7a-hexahydro-
U154
67-56-1
Methanol (I)
U155
91-80-5
Methapyrilene
U142
143-50-0
1,3,4-Metheno-2H-cyclobuta[cd]pentalen-2-
one, 1,1a,3,3a,4,5,5,5a,5b,6-decachloro-
octahydro-
U247
72-43-5
Methoxychlor
U154
67-56-1
Methyl alcohol (I)
U029
74-83-9
Methyl bromide
U186
504-60-9
1-Methylbutadiene (I)
U045
74-87-3
Methyl chloride (I,T)
U156
79-22-1
Methyl chlorocarbonate (I,T)
U226
71-55-6
Methylchloroform
U157
56-49-5
3-Methylcholanthrene
U158
101-14-4
4,4'-Methylenebis(2-chloroaniline)
U068
74-95-3
Methylene bromide
U080
75-09-2
Methylene chloride
U159
78-93-3
Methyl ethyl ketone (MEK) (I,T)
U160
1338-23-4
Methyl ethyl ketone peroxide (R,T)
U138
74-88-4
Methyl iodide
U161
108-10-1
Methyl isobutyl ketone (I)
U162
80-62-6
Methyl methacrylate (I,T)
U161
108-10-1
4-Methyl-2-pentanone (I)
U164
56-04-2
Methylthiouracil
U010
50-07-7
Mitomycin C
U059
20830-81-3
5,12-Naphthacenedione, 8-acetyl-10-[(3-amino-
2,3,6-trideoxy)-α-L-lyxo-hexapyranosyl)oxyl]-
7,8,9,10-tetrahydro-6,8,11-trihydroxy-1-
methoxy-, (8S-cis)-
U167
134-32-7
1-Naphthalenamine
U168
91-59-8
2-Naphthalenamine
U026
494-03-1
Naphthaleneamine, N,N’-bis(2-chloroethyl)-
U165
91-20-3
Naphthalene
U047
91-58-7
Naphthalene, 2-chloro-
U166
130-15-4
1,4-Naphthalenedione
U236
72-57-1
2,7-Naphthalenedisulfonic acid, 3,3'-[(3,3'-di-
methyl-[1,1'-biphenyl]-4,4'-diyl)bis(azo)bis[5-
amino-4-hydroxy]-, tetrasodium salt
U279
63-25-2
1-Naphthalenol, methylcarbamate
U166
130-15-4
1,4-Naphthoquinone
U167
134-32-7
α-Naphthylamine
U168
91-59-8
β-Naphthylamine
U217
10102-45-1
Nitric acid, thallium (1+) salt
117
U169
98-95-3
Nitrobenzene (I,T)
U170
100-02-7
p-Nitrophenol
U171
79-46-9
2-Nitropropane (I,T)
U172
924-16-3
N-Nitrosodi-n-butylamine
U173
1116-54-7
N-Nitrosodiethanolamine
U174
55-18-5
N-Nitrosodiethylamine
U176
759-73-9
N-Nitroso-N-ethylurea
U177
684-93-5
N-Nitroso-N-methylurea
U178
615-53-2
N-Nitroso-N-methylurethane
U179
100-75-4
N-Nitrosopiperidine
U180
930-55-2
N-Nitrosopyrrolidine
U181
99-55-8
5-Nitro-o-toluidine
U193
1120-71-4
1,2-Oxathiolane, 2,2-dioxide
U058
50-18-0
2H-1,3,2-Oxazaphosphorin-2-amine, N,N-bis-
(2-chloroethyl)tetrahydro-, 2-oxide
U115
75-21-8
Oxirane (I,T)
U126
765-34-4
Oxiranecarboxyaldehyde
U041
106-89-8
Oxirane, (chloromethyl)-
U182
123-63-7
Paraldehyde
U183
608-93-5
Pentachlorobenzene
U184
76-01-7
Pentachloroethane
U185
82-68-8
Pentachloronitrobenzene (PCNB)
See F027
87-86-5
Pentachlorophenol
U161
108-10-1
Pentanol, 4-methyl-
U186
504-60-9
1,3-Pentadiene (I)
U187
62-44-2
Phenacetin
U188
108-95-2
Phenol
U048
95-57-8
Phenol, 2-chloro-
U039
59-50-7
Phenol, 4-chloro-3-methyl-
U081
120-83-2
Phenol, 2,4-dichloro-
U082
87-65-0
Phenol, 2,6-dichloro-
U089
56-53-1
Phenol, 4,4'-(1,2-diethyl-1,2-ethenediyl)bis-,
(E)-
U101
105-67-9
Phenol, 2,4-dimethyl-
U052
1319-77-3
Phenol, methyl-
U132
70-30-4
Phenol, 2,2'-methylenebis[3,4,6-trichloro-
U411
114-26-1
Phenol, 2-(1-methylethoxy)-, methylcarbamate
U170
100-02-7
Phenol, 4-nitro-
See F027
87-86-5
Phenol, pentachloro-
See F027
58-90-2
Phenol, 2,3,4,6-tetrachloro-
See F027
95-95-4
Phenol, 2,4,5-trichloro-
See F027
88-06-2
Phenol, 2,4,6-trichloro-
U150
148-82-3
L-Phenylalanine, 4-[bis(2-chloroethyl)amino]-
U145
7446-27-7
Phosphoric acid, lead (2+) salt (2:3)
118
U087
3288-58-2
Phosphorodithioic acid, O,O-diethyl S-methyl
ester
U189
1314-80-3
Phosphorus sulfide (R)
U190
85-44-9
Phthalic anhydride
U191
109-06-8
2-Picoline
U179
100-75-4
Piperidine, 1-nitroso-
U192
23950-58-5
Pronamide
U194
107-10-8
1-Propanamine (I,T)
U111
621-64-7
1-Propanamine, N-nitroso-N-propyl-
U110
142-84-7
1-Propanamine, N-propyl- (I)
U066
96-12-8
Propane, 1,2-dibromo-3-chloro-
U083
78-87-5
Propane, 1,2-dichloro-
U149
109-77-3
Propanedinitrile
U171
79-46-9
Propane, 2-nitro- (I,T)
U027
108-60-1
Propane, 2,2'-oxybis[2-chloro-
See F027
93-72-1
Propanoic acid, 2-(2,4,5-trichlorophenoxy)-
U193
1120-71-4
1,3-Propane sultone
U235
126-72-7
1-Propanol, 2,3-dibromo-, phosphate (3:1)
U140
78-83-1
1-Propanol, 2-methyl- (I,T)
U002
67-64-1
2-Propanone (I)
U007
79-06-1
2-Propenamide
U084
542-75-6
1-Propene, 1,3-dichloro-
U243
1888-71-7
1-Propene, 1,1,2,3,3,3-hexachloro-
U009
107-13-1
2-Propenenitrile
U152
126-98-7
2-Propenenitrile, 2-methyl- (I,T)
U008
79-10-7
2-Propenoic acid (I)
U113
140-88-5
2-Propenoic acid, ethyl ester (I)
U118
97-63-2
2-Propenoic acid, 2-methyl-, ethyl ester
U162
80-62-6
2-Propenoic acid, 2-methyl-, methyl ester (I,T)
U373
122-42-9
Propham
U411
114-26-1
Propoxur
See F027
93-72-1
Propionic acid, 2-(2,4,5-trichlorophenoxy)-
U194
107-10-8
n-Propylamine (I,T)
U083
78-87-5
Propylene dichloride
U387
52888-80-9
Prosulfocarb
U148
123-33-1
3,6-Pyridazinedione, 1,2-dihydro-
U196
110-86-1
Pyridine
U191
109-06-8
Pyridine, 2-methyl-
U237
66-75-1
2,4-(1H,3H)-Pyrimidinedione, 5-[bis(2-chloro-
ethyl)amino]-
U164
58-04-2
4(1H)-Pyrimidinone, 2,3-dihydro-6-methyl-2-
thioxo-
U180
930-55-2
Pyrrolidine, 1-nitroso-
U200
50-55-5
Reserpine
U201
108-46-3
Resorcinol
119
U202
P 81-07-2
Saccharin and salts
U203
94-59-7
Safrole
U204
7783-00-8
Selenious acid
U204
7783-00-8
Selenium dioxide
U205
7488-56-4
Selenium sulfide
U205
7488-56-4
Selenium sulfide SeS2 (R,T)
U015
115-02-6
L-Serine, diazoacetate (ester)
See F027
93-72-1
Silvex (2,4,5-TP)
U206
18883-66-4
Streptozotocin
U103
77-78-1
Sulfuric acid, dimethyl ester
U189
1314-80-3
Sulfur phosphide (R)
See F027
93-76-5
2,4,5-T
U207
95-94-3
1,2,4,5-Tetrachlorobenzene
U208
630-20-6
1,1,1,2-Tetrachloroethane
U209
79-34-5
1,1,2,2-Tetrachloroethane
U210
127-18-4
Tetrachloroethylene
See F027
58-90-2
2,3,4,6-Tetrachlorophenol
U213
109-99-9
Tetrahydrofuran (I)
U214
563-68-8
Thallium (I) acetate
U215
6533-73-9
Thallium (I) carbonate
U216
7791-12-0
Thallium (I) chloride
U216
7791-12-0
Thallium chloride TlCl
U217
10102-45-1
Thallium (I) nitrate
U218
62-55-5
Thioacetamide
U410
59669-26-0
Thiodicarb
U153
74-93-1
Thiomethanol (I,T)
U244
137-26-8
Thioperoxydicarbonic diamide [(H2N)C(S)]2S2,
tetramethyl-
U409
23564-05-8
Thiophanate-methyl
U219
62-56-6
Thiourea
U244
137-26-8
Thiram
U220
108-88-3
Toluene
U221
25376-45-8
Toluenediamine
U223
26471-62-5
Toluene diisocyanate (R,T)
U328
95-53-4
o-Toluidine
U353
106-49-0
p-Toluidine
U222
636-21-5
o-Toluidine hydrochloride
U389
2303-17-5
Triallate
U011
61-82-5
1H-1,2,4-Triazol-3-amine
U408
118-79-6
2,4,6-Tribromophenol
U227
79-00-5
1,1,2-Trichloroethane
U228
79-01-6
Trichloroethylene
U121
75-69-4
Trichloromonofluoromethane
See F027
95-95-4
2,4,5-Trichlorophenol
See F027
88-06-2
2,4,6-Trichlorophenol
120
U404
121-44-8
Triethylamine
U234
99-35-4
1,3,5-Trinitrobenzene (R,T)
U182
123-63-7
1,3,5-Trioxane, 2,4,6-trimethyl-
U235
126-72-7
Tris(2,3-dibromopropyl) phosphate
U236
72-57-1
Trypan blue
U237
66-75-1
Uracil mustard
U176
759-73-9
Urea, N-ethyl-N-nitroso-
U177
684-93-5
Urea, N-methyl-N-nitroso-
U043
75-01-4
Vinyl chloride
U248
P 81-81-2
Warfarin, and salts, when present at
concentrations of 0.3 percent or less
U239
1330-20-7
Xylene (I)
U200
50-55-5
Yohimban-16-carboxylic acid, 11,17-dimeth-
oxy-18-[(3,4,5-trimethoxybenzoyl)oxy]-,
methyl ester, (3β,16β,17α,18β,20α)-
U249
1314-84-7
Zinc phosphide Zn3P2, when present at
concentrations of 10 percent or less
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.138
Comparable or Syngas Fuel Exclusion
Wastes that meet the following comparable or syngas fuel requirements are not solid wastes:
a)
Comparable fuel specifications.
1)
Physical specifications.
A)
Heating value. The heating value must exceed 5,000 Btu/lb
(11,500 J/g).
B)
Viscosity. The viscosity must not exceed: 50 cs, as-fired.
2)
Constituent specifications. For the compounds listed, the constituent
specification levels and minimum required detection limits (where non-
detect is the constituent specification) are set forth in the table at
subsection (d) of this Section.
b)
Synthesis gas fuel specification. Synthesis gas fuel (i.e., syngas fuel) that is
generated from hazardous waste must fulfill the following requirements:
1)
It must have a minimum Btu value of 100 Btu/Scf;
2)
It must contain less than 1 ppmv of total halogen;
121
3)
It must contain less than 300 ppmv of total nitrogen other than diatomic
nitrogen (N2);
4)
It must contain less than 200 ppmv of hydrogen sulfide; and
5)
It must contain less than 1 ppmv of each hazardous constituent in the
target list of Appendix H constituents.
c)
Implementation. Waste that meets the comparable or syngas fuel specifications
provided by subsection (a) or (b) of this Section (these constituent levels must
be achieved by the comparable fuel when generated, or as a result of treatment
or blending, as provided in subsection (c)(3) or (c)(4) of this Section) is
excluded from the definition of solid waste provided that the following
requirements are met:
1)
Notices. For purposes of this Section, the person claiming and
qualifying for the exclusion is called the comparable or syngas fuel
generator and the person burning the comparable or syngas fuel is called
the comparable or syngas burner. The person that generates the
comparable fuel or syngas fuel must claim and certify to the exclusion.
A)
Notice to the Agency.
i)
The generator must submit a one-time notice to the
Agency, certifying compliance with the conditions of the
exclusion and providing documentation as required by
subsection (c)(1)(A)(iii) of this Section;
ii)
If the generator is a company that generates comparable or
syngas fuel at more than one facility, the generator shall
specify at which sites the comparable or syngas fuel will
be generated;
iii)
A comparable or syngas fuel generator’s notification to
the Agency must contain the items listed in subsection
(c)(1)(C) of this Section.
B)
Public notice. Prior to burning an excluded comparable or
syngas fuel, the burner must publish in a major newspaper of
general circulation local to the site where the fuel will be burned,
a notice entitled “Notification of Burning a Comparable or
Syngas Fuel Excluded Under the Resource Conservation and
Recovery Act” containing the following information:
122
i)
The name, address, and USEPA identification number of
the generating facility;
ii)
The name and address of the unit(s) that will burn the
comparable or syngas fuel;
iii)
A brief, general description of the manufacturing,
treatment, or other process generating the comparable or
syngas fuel;
iv)
An estimate of the average and maximum monthly and
annual quantity of the waste claimed to be excluded; and
v)
The name and mailing address of the Agency office, to
which the claim was submitted.
C)
Required content of comparable or syngas notification to the
Agency.
i)
The name, address, and USEPA identification number of
the person or facility claiming the exclusion;
ii)
The applicable USEPA hazardous waste code(s) for the
hazardous waste;
iii)
The name and address of the units that meet the
requirements of subsection (c)(2) of this Section which
will burn the comparable or syngas fuel; and
iv)
The following statement, signed and submitted by the
person claiming the exclusion or its authorized
representative:
Under penalty of criminal and civil prosecution for
making or submitting false statements,
representations, or omissions, I certify that the
requirements of 35 Ill. Adm. Code 721.138 have
been met for all waste identified in this
notification. Copies of the records and
information required by 35 Ill. Adm. Code
721.138(c)(10) are available at the comparable or
syngas fuel generator’s facility. Based on my
inquiry of the individuals immediately responsible
for obtaining the information, the information is,
to the best of my knowledge and belief, true,
123
accurate, and complete. I am aware that there are
significant penalties for submitting false
information, including the possibility of fine and
imprisonment for knowing violations.
BOARD NOTE: Subsections (c)(1)(C)(i) through (c)(1)(C)(iv)
are derived from 40 CFR 261.138(c)(1)(i)(C)(
1
) and
(c)(1)(i)(C)(
4
), which the Board has codified here to comport
with Illinois Administrative Code format requirements.
2)
Burning. The comparable or syngas fuel exclusion for fuels that meet
the requirements of subsection (a) or (b) and (c)(1) of this Section
applies only if the fuel is burned in the following units that also shall be
subject to federal, State, and local air emission requirements, including
all applicable federal Clean Air Act (CAA) maximum achievable control
technology (MACT) requirements:
A)
Industrial furnaces, as defined in 35 Ill. Adm. Code 720.110;
B)
Boilers, as defined in 35 Ill. Adm. Code 720.110, that are further
defined as follows:
i)
Industrial boilers located on the site of a facility engaged
in a manufacturing process where substances are
transformed into new products, including the component
parts of products, by mechanical or chemical processes;
or
ii)
Utility boilers used to produce electric power, steam,
heated or cooled air, or other gases or fluids for sale;
C)
Hazardous waste incinerators subject to regulation under 35 Ill.
Adm. Code 724.Subpart O or 725.Subpart O or applicable CAA
MACT standards.
3)
Blending to meet the viscosity specification. A hazardous waste blended
to meet the viscosity specification must fulfill the following
requirements:
A)
As generated and prior to any blending, manipulation, or
processing, the waste must meet the constituent and heating value
specifications of subsections (a)(1)(A) and (a)(2) of this Section;
124
B)
The waste must be blended at a facility that is subject to the
applicable requirements of 35 Ill. Adm. Code 724 and 725 or 35
Ill. Adm. Code 722.134; and
C)
The waste must not violate the dilution prohibition of subsection
(c)(6) of this Section.
4)
Treatment to meet the comparable fuel exclusion specifications.
A)
A hazardous waste may be treated to meet the exclusion
specifications of subsections (a)(1) and (a)(2) of this Section
provided the treatment fulfills the following requirements:
i)
The treatment destroys or removes the constituent listed in
the specification or raises the heating value by removing
or destroying hazardous constituents or materials;
ii)
The treatment is performed at a facility that is subject to
the applicable requirements of 35 Ill. Adm. Code 724 and
725 or 35 Ill. Adm. Code 722.134; and
iii)
The treatment does not violate the dilution prohibition of
subsection (c)(6) of this Section.
B)
Residuals resulting from the treatment of a hazardous waste listed
in Subpart D of this Part to generate a comparable fuel remain a
hazardous waste.
5)
Generation of a syngas fuel.
A)
A syngas fuel can be generated from the processing of hazardous
wastes to meet the exclusion specifications of subsection (b) of
this Section provided the processing fulfills the following
requirements:
i)
The processing destroys or removes the constituent listed
in the specification or raises the heating value by
removing or destroying constituents or materials;
ii)
The processing is performed at a facility that is subject to
the applicable requirements of 35 Ill. Adm. Code 724 and
725 or 35 Ill. Adm. Code 722.134 or is an exempt
recycling unit pursuant to Section 721.106(c); and
125
iii)
The processing does not violate the dilution prohibition of
subsection (c)(6) of this Section.
B)
Residuals resulting from the treatment of a hazardous waste listed
in Subpart D of this Part to generate a syngas fuel remain a
hazardous waste.
6)
Dilution prohibition for comparable and syngas fuels. No generator,
transporter, handler, or owner or operator of a treatment, storage, or
disposal facility shall in any way dilute a hazardous waste to meet the
exclusion specifications of subsection (a)(1)(A), (a)(2) or (b) of this
Section.
7)
Waste analysis plans. The generator of a comparable or syngas fuel
shall develop and follow a written waste analysis plan which describes
the procedures for sampling and analysis of the hazardous waste to be
excluded. The waste analysis plan shall be developed in accordance with
the applicable sections of the “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods” (SW-846). The plan shall be followed and
retained at the facility excluding the waste.
A)
At a minimum, the plan must specify the following:
i)
The parameters for which each hazardous waste will be
analyzed and the rationale for the selection of those
parameters;
ii)
The test methods which will be used to test for these
parameters;
iii)
The sampling method which will be used to obtain a
representative sample of the waste to be analyzed;
iv)
The frequency with which the initial analysis of the waste
will be reviewed or repeated to ensure that the analysis is
accurate and up to date; and
v)
If process knowledge is used in the waste determination,
any information prepared by the generator in making such
determination.
B)
The waste analysis plan must also contain records of the
following:
126
i)
The dates and times waste samples were obtained, and the
dates the samples were analyzed;
ii)
The names and qualifications of the person(s) who
obtained the samples;
iii)
A description of the temporal and spatial locations of the
samples;
iv)
The name and address of the laboratory facility at which
analyses of the samples were performed;
v)
A description of the analytical methods used, including
any clean-up and sample preparation methods;
vi)
All quantitation limits achieved and all other quality
control results for the analysis (including method blanks,
duplicate analyses, matrix spikes, etc.), laboratory quality
assurance data, and description of any deviations from
analytical methods written in the plan or from any other
activity written in the plan which occurred;
vii)
All laboratory results demonstrating that the exclusion
specifications have been met for the waste; and
viii) All laboratory documentation that supports the analytical
results, unless a contract between the claimant and the
laboratory provides for the documentation to be
maintained by the laboratory for the period specified in
subsection (c)(11) of this Section and also provides for the
availability of the documentation to the claimant upon
request.
C)
Syngas fuel generators shall submit for approval, prior to
performing sampling, analysis, or any management of a syngas
fuel as an excluded waste, a waste analysis plan containing the
elements of subsection (c)(7)(A) of this Section to the Agency.
The approval of waste analysis plans must be stated in writing
and received by the facility prior to sampling and analysis to
demonstrate the exclusion of a syngas. The approval of the waste
analysis plan may contain such provisions and conditions as the
regulatory authority deems appropriate.
8)
Comparable fuel sampling and analysis.
127
A)
General. For each waste for which an exclusion is claimed, the
generator of the hazardous waste must test for all the constituents
on Appendix H of this Part, except those that the generator
determines, based on testing or knowledge, should not be present
in the waste. The generator is required to document the basis of
each determination that a constituent should not be present. The
generator may not determine that any of the following categories
of constituents should not be present:
i)
A constituent that triggered the toxicity characteristic for
the waste constituents that were the basis of the listing of
the waste stream, or constituents for which there is a
treatment standard for the waste code in 35 Ill. Adm.
Code 728.140;
ii)
A constituent detected in previous analysis of the waste;
iii)
Constituents introduced into the process that generates the
waste; or
iv)
Constituents that are byproducts or side reactions to the
process that generates the waste.
Note to subsection (c)(8): Any claim under this Section must be valid
and accurate for all hazardous constituents; a determination not to test
for a hazardous constituent will not shield a generator from liability
should that constituent later be found in the waste above the exclusion
specifications.
B)
For each waste for which the exclusion is claimed where the
generator of the comparable or syngas fuel is not the original
generator of the hazardous waste, the generator of the
comparable or syngas fuel may not use process knowledge
pursuant to subsection (c)(8)(A) of this Section and must test to
determine that all of the constituent specifications of subsections
(a)(2) and (b) of this Section have been met.
C)
The comparable or syngas fuel generator may use any reliable
analytical method to demonstrate that no constituent of concern is
present at concentrations above the specification levels. It is the
responsibility of the generator to ensure that the sampling and
analysis are unbiased, precise, and representative of the waste.
For the waste to be eligible for exclusion, a generator must
demonstrate the following:
128
i)
That each constituent of concern is not present in the
waste above the specification level at the 95 percent upper
confidence limit around the mean; and
ii)
That the analysis could have detected the presence of the
constituent at or below the specification level at the 95
percent upper confidence limit around the mean.
D)
Nothing in this subsection (c)(8) preempts, overrides or otherwise
negates the provision in 35 Ill. Adm. Code 722.111 that requires
any person which generates a solid waste to determine if that
waste is a hazardous waste.
E)
In an enforcement action, the burden of proof to establish
conformance with the exclusion specification shall be on the
generator claiming the exclusion.
F)
The generator must conduct sampling and analysis in accordance
with its waste analysis plan developed under subsection (c)(7) of
this Section.
G)
Syngas fuel and comparable fuel that has not been blended in
order to meet the kinematic viscosity specifications must be
analyzed as generated.
H)
If a comparable fuel is blended in order to meet the kinematic
viscosity specifications, the generator shall undertake the
following actions:
i)
Analyze the fuel as generated to ensure that it meets the
constituent and heating value specifications; and
ii)
After blending, analyze the fuel again to ensure that the
blended fuel continues to meet all comparable or syngas
fuel specifications.
I)
Excluded comparable or syngas fuel must be re-tested, at a
minimum, annually and must be retested after a process change
that could change the chemical or physical properties of the
waste.
9)
Speculative accumulation. Any persons handling a comparable or
syngas fuel are subject to the speculative accumulation test under Section
721.102(c)(4).
129
10)
Records. The generator must maintain records of the following
information on-site:
A)
All information required to be submitted to the implementing
authority as part of the notification of the claim:
i)
The owner or operator name, address, and RCRA facility
USEPA identification number of the person claiming the
exclusion;
ii)
The applicable USEPA hazardous waste codes for each
hazardous waste excluded as a fuel; and
iii)
The certification signed by the person claiming the
exclusion or his authorized representative.
B)
A brief description of the process that generated the hazardous
waste and process that generated the excluded fuel, if not the
same;
C)
An estimate of the average and maximum monthly and annual
quantities of each waste claimed to be excluded;
D)
Documentation for any claim that a constituent is not present in
the hazardous waste as required under subsection (c)(8)(A) of this
Section;
E)
The results of all analyses and all detection limits achieved as
required under subsection (c)(8) of this Section;
F)
If the excluded waste was generated through treatment or
blending, documentation as required under subsection (c)(3) or
(c)(4) of this Section;
G)
If the waste is to be shipped off-site, a certification from the
burner as required under subsection (c)(12) of this Section;
H)
A waste analysis plan and the results of the sampling and analysis
that includes the following:
i)
The dates and times waste samples were obtained, and the
dates the samples were analyzed;
ii)
The names and qualifications of the person(s) that
obtained the samples;
130
iii)
A description of the temporal and spatial locations of the
samples;
iv)
The name and address of the laboratory facility at which
analyses of the samples were performed;
v)
A description of the analytical methods used, including
any clean-up and sample preparation methods;
vi)
All quantitation limits achieved and all other quality
control results for the analysis (including method blanks,
duplicate analyses, matrix spikes, etc.), laboratory quality
assurance data, and description of any deviations from
analytical methods written in the plan or from any other
activity written in the plan which occurred;
vii)
All laboratory analytical results demonstrating that the
exclusion specifications have been met for the waste; and
viii) All laboratory documentation that supports the analytical
results, unless a contract between the claimant and the
laboratory provides for the documentation to be
maintained by the laboratory for the period specified in
subsection (c)(11) of this Section and also provides for the
availability of the documentation to the claimant upon
request; and
I)
If the generator ships comparable or syngas fuel off-site for
burning, the generator shall retain for each shipment the
following information on-site:
i)
The name and address of the facility receiving the
comparable or syngas fuel for burning;
ii)
The quantity of comparable or syngas fuel shipped and
delivered;
iii)
The date of shipment or delivery;
iv)
A cross-reference to the record of comparable or syngas
fuel analysis or other information used to make the
determination that the comparable or syngas fuel meets
the specifications as required under subsection (c)(8) of
this Section; and
131
v)
A one-time certification by the burner as required under
subsection (c)(12) of this Section.
11)
Records retention. Records must be maintained for the period of three
years. A generator shall maintain a current waste analysis plan during
that three year period.
12)
Burner certification. Prior to submitting a notification to the Agency, a
comparable or syngas fuel generator that intends to ship their fuel off-
site for burning must obtain a one-time written, signed statement from
the burner that includes the following:
A)
A certification that the comparable or syngas fuel will only be
burned in an industrial furnace or boiler, utility boiler, or
hazardous waste incinerator, as required under subsection (c)(2)
of this Section;
B)
Identification of the name and address of the units that will burn
the comparable or syngas fuel; and
C)
A certification that the state in which the burner is located is
authorized to exclude wastes as comparable or syngas fuel under
the provisions of this Section.
13)
Ineligible waste codes. Wastes that are listed because of presence of
dioxins or furans, as set out in Appendix G of this Part, are not eligible
for this exclusion, and any fuel produced from or otherwise containing
these wastes remains a hazardous waste subject to full RCRA hazardous
waste management requirements.
d)
Table of detection and detection limit values for comparable fuel specification:
Chemical name
CAS No
Concentration
limit (mg/kg at
10,000 Btu/lb)
Minimum re-
quired detection
limit (mg/kg)
Total Nitrogen as N
na
4900
Total Halogens as Cl
na
540
Total Organic Halogens as
Cl
na
25 or individual
halogenated
organics listed
below.
Polychlorinated biphenyls,
total [Arocolors, total]
a
1336-36-3
Non-detect
1.4
Cyanide, total
57-12-5
Non-detect
1.0
132
Metals:
Antimony, total
7440-36-0
7.9
Arsenic, total
7440-38-2
0.23
Barium, total
7440-39-3
23
Beryllium, total
7440-41-7
1.2
Cadmium, total
7440-43-9
1.2
Chromium, total
7440-47-3
2.3
Cobalt
7440-48-4
4.6
Lead, total
7439-92-1
31
Manganese
7439-96-5
1.2
Mercury, total
7439-97-6
0.24
Nickel, total
7440-02-0
58
Selenium, total
7782-49-2
0.15
Silver, total
7440-22-4
2.3
Thallium, total
7440-28-0
23
Hydrocarbons:
Benzo[a]anthracene
56-55-3
1100
Benzene
71-43-2
4100
Benzo[b]fluoranthene
205-99-2
960
Benzo[k]fluoranthene
207-08-9
1900
Benzo[a]pyrene
50-32-8
960
Chrysene
218-01-9
1400
Dibenzo[a,h]anthracene
53-70-3
960
7,12-Dimethylbenz[a]-
anthracene
57-97-6
1900
Fluoranthene
206-44-0
1900
Indeno(1,2,3-cd)pyrene
193-39-5
960
3-Methylcholanthrene
56-49-5
1900
Naphthalene
91-20-3
3200
Toluene
108-88-3
36000
Oxygetes:
Acetophenone
98-86-2
1900
Acrolein
107-02-8
37
Allyl alcohol
107-18-6
30
Bis(2-ethylhexyl)-
phthalate [Di-2-ethyl-
hexyl phthalate]
117-81-7
1900
Butyl benzyl phthalate
85-68-7
1900
o-Cresol [2-Methyl
phenol]
95-48-7
220
m-Cresol [3-Methyl
phenol]
108-39-4
220
133
p-Cresol [4-Methyl
phenol]
106-44-5
220
Di-n-butyl phthalate
84-74-2
1900
Diethyl phthalate
84-66-2
1900
2,4-Dimethylphenol
105-67-9
1900
Dimethyl phthalate
131-11-3
1900
Di-n-octyl phthalate
117-84-0
960
Endothall
145-73-3
100
Ethyl methacrylate
97-63-2
37
2-Ethoxyethanol
[Ethylene glycol
monoethyl ether].
110-80-5
100
Isobutyl alcohol
78-83-1
37
Isosafrole
120-58-1
1900
Methyl ethyl ketone [2-
Butanone]
78-93-3
37.
Methyl methacrylate
80-62-6
37.
1,4-Naphthoquinone
130-15-4
1900.
Phenol
108-95-2
1900.
Propargyl alcohol [2-
Propyn-l-ol]
107-19-7
30.
Safrole
94-59-7
1900.
Sulfonated Organics:
Carbon disulfide
75-15-0
Non-detect
37
Disulfoton
298-04-4
Non-detect
1900
Ethyl methanesulfonate
62-50-0
Non-detect
1900
Methyl methane-
sulfonate
66-27-3
Non-detect
1900
Phorate
298-02-2
Non-detect
1900
1,3-Propane sultone
1120-71-4
Non-detect
100
Tetraethyldithiopyro-
phosphate [Sulfotepp]
3689-24-5
Non-detect
1900
Thiophenol [Benzene-
thiol]
108-98-5
Non-detect
30
O,O,O-Triethyl
phosphorothioate
126-68-1
Non-detect
1900
Nitrogenated Organics:
Acetonitrile [Methyl
cyanide]
75-05-8
Non-detect
37
2-Acetylaminofluorene
[2-AAF]
53-96-3
Non-detect
1900
Acrylonitrile
107-13-1
Non-detect
37
4-Aminobiphenyl
92-67-1
Non-detect
1900
4-Aminopyridine
504-24-5
Non-detect
100
134
Aniline
62-53-3
Non-detect
1900
Benzidine
92-87-5
Non-detect
1900
Dibenz[a,j]acridine
224-42-0
Non-detect
1900
O,O-Diethyl O-
pyrazinyl phophoro-
thioate [Thionazin].
297-97-2
Non-detect
1900
Dimethoate
60-51-5
Non-detect
1900
p-(Dimethylamino)azo-
benzene [4-Dimethyl-
aminoazobenzene].
60-11-7
Non-detect
1900
3,3'-Dimethylbenzidine
119-93-7
Non-detect
1900
a,a-Dimethylphenethyl-
amine.
122-09-8
Non-detect
1900
3,3'-Dimethoxy-
benzidine
119-90-4
Non-detect
100
1,3-Dinitrobenzene [m-
Dinitrobenzene]
99-65-0
Non-detect
1900
4,6-Dinitro-o-cresol
534-52-1
Non-detect
1900
2,4-Dinitrophenol
51-28-5
Non-detect
1900
2,4-Dinitrotoluene
121-14-2
Non-detect
1900
2,6-Dinitrotoluene
606-20-2
Non-detect
1900
Dinoseb [2-sec-Butyl-
4,6-dinitrophenol]
88-85-7
Non-detect
1900
Diphenylamine
122-39-4
Non-detect
1900
Ethyl carbamate
[Urethane]
51-79-6
Non-detect
100
Ethylenethiourea (2-
Imidazolidinethione)
96-45-7
Non-detect
110
Famphur
52-85-7
Non-detect
1900
Methacrylonitrile
126-98-7
Non-detect
37
Methapyrilene
91-80-5
Non-detect
1900
Methomyl
16752-77-5
Non-detect
57
2-Methyllactonitrile
[Acetone cyanohydrin].
75-86-5
Non-detect
100
Methyl parathion
298-00-0
Non-detect
1900
MNNG (N-Metyl-N-
nitroso-N’-nitro-
guanidine)
70-25-7
Non-detect
110
1-Naphthylamine, [α-
Naphthylamine]
134-32-7
Non-detect
1900
2-Naphthylamine, [β-
Naphthylamine]
91-59-8
Non-detect
1900
Nicotine
54-11-5
Non-detect
100
135
4-Nitroaniline, [p-
Nitroaniline]
100-01-6
Non-detect
1900
Nitrobenzene
98-95-3
Non-detect
1900
p-Nitrophenol, [p-
Nitrophenol]
100-02-7
Non-detect
1900
5-Nitro-o-toluidine
99-55-8
Non-detect
1900
N-Nitrosodi-n-butyl-
amine
924-16-3
Non-detect
1900
N-Nitrosodiethylamine
55-18-5
Non-detect
1900
N-Nitrosodiphenyl-
amine, [Diphenyl-
nitrosamine]
86-30-6
Non-detect
1900
N-Nitroso-N-methyl-
ethylamine
10595-95-6
Non-detect
1900
N-Nitrosomorpholine
59-89-2
Non-detect
1900
N-Nitrosopiperidine
100-75-4
Non-detect
1900
N-Nitrosopyrrolidine
930-55-2
Non-detect
1900
2-Nitropropane
79-46-9
Non-detect
30
Parathion
56-38-2
Non-detect
1900
Phenacetin
62-44-2
Non-detect
1900
1,4-Phenylene diamine,
[p-Phenylenediamine]
106-50-3
Non-detect
1900
N-Phenylthiourea
103-85-5
Non-detect
57
2-Picoline [alpha-
Picoline]
109-06-8
Non-detect
1900
Propythioracil [6-
Propyl-2-thiouracil]
51-52-5
Non-detect
100
Pyridine
110-86-1
Non-detect
1900
Strychnine
57-24-9
Non-detect
100
Thioacetamide
62-55-5
Non-detect
57
Thiofanox
39196-18-4
Non-detect
100
Thiourea
62-56-6
Non-detect
57
Toluene-2,4-diamine
[2,4-Diaminotoluene]
95-80-7
Non-detect
57
Toluene-2,6-diamine
[2,6-Diaminotoluene]
823-40-5
Non-detect
57
o-Toluidine
95-53-4
Non-detect
2200
p-Toluidine
106-49-0
Non-detect
100
1,3,5-Trinitrobenzne,
[sym-Trinitobenzene]
99-35-4
Non-detect
2000
Halogenated Organics
b
:
Allyl chloride
107-05-1
Non-detect
37
Aramite
104-57-8
Non-detect
1900
136
Benzal chloride [Di-
chloromethyl benzene]
98-87-3
Non-detect
100
Benzyl chloride
100-44-77
Non-detect
100
Bis(2-chloroethyl)ether
[Dichloroethyl ether]
111-44-4
Non-detect
1900
Bromoform [Tribromo-
methane]
75-25-2
Non-detect
37
Bromomethane [Methyl
bromide]
74-83-9
Non-detect
37
4-Bromophenyl phenyl
ether [p-Bromodiphenyl
ether]
101-55-3
Non-detect
1900
Carbon tetrachloride
56-23-5
Non-detect
37
Chlordane
57-74-9
Non-detect
14
p-Chloroaniline
106-47-8
Non-detect
1900
Chlorobenzene
108-90-7
Non-detect
37
Chlorobenzilate
510-15-6
Non-detect
1900
p-Chloro-m-cresol
59-50-7
Non-detect
1900
2-Chloroethyl vinyl
ether
110-75-8
Non-detect
37
Chloroform
67-66-3
Non-detect
37
Chloromethane [Methyl
chloride]
74-87-3
Non-detect
37
2-Chlorophthalene
[beta-Chlorophthalene]
91-58-7
Non-detect
1900
2-Chlorophenol [o-
Chlorophenol]
95-57-8
Non-detect
1900
Chloroprene [2-Chloro-
1,3-butadiene]
1126-99-8
Non-detect
37
2,4-D [2,4-Dichloro-
phenoxyacetic acid]
94-75-7
Non-detect
7.0
Diallate
2303-16-4
Non-detect
1900
1,2-Dibromo-3-chloro-
propane
96-12-8
Non-detect
37
1,2-Dichlorobenzene
[o-Dichlorobenzene]
95-50-1
Non-detect
1900
1,3-Dichlorobenzene
[m-Dichlorobenzene]
541-73-1
Non-detect
1900
1,4-Dichlorobenzene
[p-Dichlorobenzene]
106-46-7
Non-detect
1900
3,3'-Dichlorobenzidine
91-94-1
Non-detect
1900
Dichlorodifluoro-
methane [CFC-12]
75-71-8
Non-detect
37
137
1,2-Dichloroethane
[Ethylene dichloride]
107-06-2
Non-detect
37
1,1-Dichloroethylene
[Vinylidene chloride]
75-35-4
Non-detect
37
Dichloromethoxy
ethane [Bis(2-chloro-
ethoxy)methane
111-91-1
Non-detect
1900
2,4-Dichlorophenol
120-83-2
Non-detect
1900
2,6-Dichlorophenol
87-65-0
Non-detect
1900
1,2-Dichloropropane
[Propylene dichloride]
78-87-5
Non-detect
37
cis-1,3-Dichloro-
propylene
10061-01-5
Non-detect
37
trans-1,3-Dichloro-
propylene
10061-02-6
Non-detect
37
1,3-Dichloro-2-
propanol
96-23-1
Non-detect
30
Endosulfan I
959-98-8
Non-detect
1.4
Endosulfan II
33213-65-9
Non-detect
1.4
Endrin
72-20-8
Non-detect
1.4
Endrin aldehyde
7421-93-4
Non-detect
1.4
Endrin Ketone
53494-70-5
Non-detect
1.4
Epichlorohydrin [1-
Chloro-2,3-epoxy
propane]
106-89-8
Non-detect
30
Ethylidene dichloride
[1,1-Dichloroethane]
75-34-3
Non-detect
37
2-Fluoroacetamide
640-19-7
Non-detect
100
Heptachlor
76-44-8
Non-detect
1.4
Heptachlor epoxide
1024-57-3
Non-detect
2.8
Hexachlorobenzene
118-74-1
Non-detect
1900
Hexachloro-1,3-buta-
diene [Hexachlorobuta-
diene]
87-68-3
Non-detect
1900
Hexachlorocyclopenta-
diene
77-47-4
Non-detect
1900
Hexachloroethane
67-72-1
Non-detect
1900
Hexachlorophene
70-30-4
Non-detect
1000
Hexachloropropene
[Hexachloropropylene]
1888-71-7
Non-detect
1900
Isodrin
465-73-6
Non-detect
1900
Kepone [Chlordecone]
143-50-0
Non-detect
3600
138
Lindane [gamma-Hexa-
chlorocyclohexane]
[gamma-BHC]
58-89-9
non-detect
1.4
Methylene chloride
[Dichloromethane]
75-09-2
non-detect
37
4,4'-methylene-bis(2-
chloroaniline)
101-14-4
non-detect
100
Methyl iodide [Iodo-
methane]
74-88-4
non-detect
37
Pentachlorobenzene
608-93-5
non-detect
1900
Pentachloroethane
76-01-7
non-detect
37
Pentachloronitro-
benzene [PCNB]
[Quintobenzene]
[Quintozene]
82-68-8
non-detect
1900
Pentachlorophenol
87-86-5
non-detect
1900
Pronamide
23950-58-5
non-detect
1900
Silvex [2,4,5-Tri-
chlorophenoxy-
propionic acid]
93-72-1
non-detect
7.0
2,3,7,8-Tetrachloro-
dibenzo-p-dioxin
[2,3,7,8-TCDD]
1746-01-6
non-detect
30
1,2,4,5-Tetrachloro-
benzene
95-94-3
non-detect
1900
1,1,2,2-Tetrachloro-
ethane
79-34-5
non-detect
37
Tetrachloroethylene
[Perchloroethylene]
127-18-4
non-detect
37
2,3,4,6-Tetrachloro-
phenol
58-90-2
non-detect
1900
1,2,4-Trichlorobenzene
120-82-1
non-detect
1900
1,1,1-Trichloroethane
[Methyl chloroform]
71-55-6
non-detect
37
1,1,2-Trichloroethane
[Vinyl trichloride]
79-00-5
non-detect
37
Trichloroethylene
79-01-6
non-detect
37
Trichlorofluoromethane
[Trichloromonofluoro-
methane]
75-69-4
non-detect
37
2,4,5-Trichlorophenol
95-95-4
non-detect
1900
2,4,6-Trichlorophenol
88-06-2
non-detect
1900
1,2,3-Trichloropropane
96-18-4
non-detect
37
Vinyl Chloride
75-01-4
non-detect
37
139
a
Absence of PCBs can also be demonstrated by using appropriate screening
methods, e.g., immunoassay kit for PCB in oils (Method 4020) or colorimetric
analysis for PCBs in oil (Method 9079).
b
Some minimum required detection limits are above the total halogen limit of
540 ppm. The detection limits reflect what was achieved during USEPA testing
and analysis and also analytical complexity associated with measuring all
halogen compounds on Appendix H of this Part at low levels. USEPA stated
that it recognizes that in practice the presence of these compounds will be
functionally limited by the molecular weight and the total halogen limit of 540
ppm.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 721.Appendix G
Basis for Listing Hazardous Wastes
USEPA hazard-
ous waste No.
Hazardous constituents for which listed
F001
Tetrachloroethylene, methylene chloride, trichloroethylene, 1,1,1-
trichloroethane, carbon tetrachloride, chlorinated fluorocarbons.
F002
Tetrachloroethylene, methylene chloride, trichloroethylene, 1,1,1-
trichloroethane, 1,1,2-trichlorethane, chlorobenzene, 1,1,2-trichloro-1,2,2-
trifluoroethane, ortho-dichlorobenzene, trichlorofluoromethane.
F003
N.A.
F004
Cresols and cresylic acid, nitrobenzene.
F005
Toluene, methyl ethyl ketone, carbon disulfide, isobutanol, pyridine, 2-
ethoxyethanol, benzene, 2-nitropropane.
F006
Cadmium, hexavalent chromium, nickel, cyanide (complexed).
F007
Cyanide (salts).
F008
Cyanide (salts).
F009
Cyanide (salts).
F010
Cyanide (salts).
F011
Cyanide (salts).
F012
Cyanide (complexed).
F019
Hexavalent chromium, cyanide (complexed).
F020
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans; tri- and tetrachlorophenols and their
clorophenoxy derivative acids, esters, ethers, amines and other salts.
F021
Penta- and hexachlorodibenzo-p-dioxins; penta- and
hexachlorodibenzofurans; pentachlorophenol and its derivatives.
F022
Tetra-, penta- and hexachlorodibenzo-p-dioxins; tetra-, penta- and
hexachlorodibenzofurans.
140
F023
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans; tri- and tetra- chlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amines and other salts.
F024
Chloromethane, dichloromethane, trichloromethane, carbon tetrachloride,
chloroethylene, 1,1-dichloroethane, 1,2-dichloroethane, trans-1,2-
dichloroethylene, 1,1-dichloroethylene, 1,1,1-trichloroethane, 1,1,2-
trichloroethane, trichloroethylene, 1,1,1,2-tetrachloroethane, 1,1,2,2-
tetrachloroethane, tetrachloroethylene, pentachloroethane,
hexachloroethane, allyl chloride (3-chloropropene), dichloropropane,
dichloropropene, 2-chloro-1,3-butadiene, hexachloro-1,3-butadiene,
hexachlorochylopentadiene, hexachlorocylohexane, benzene,
chlorobenzene, dichlorobenzenes, 1,2,4-trichlorobenzene,
tetrachlorobenzenes, pentachlorobenzene, hexachlorobenzene, toluene,
naphthalene.
F025
Chloromethane, dicloromethane, trichloromethane; carbon tetrachloride;
chloroethylene; 1,1-dichloroethane; 1,2-dichloroethane; trans-1,2-
dichloroethylene; 1,1-dichloroethylene; 1,1,1-trichloroethane; 1,1,2-
trichloroethane; trichloroethylene; 1,1,1,2-tetrachloroethane; 1,1,2,2-
tetrachloroethane; tetrachloroethylene; pentachloroethane;
hexachloroethane; allyl chloride (3-chloropropene); dichloropropane;
dichloropropene; 2-chloro-1,3-butadiene; hexachloro-1,3-butadiene;
hexachlorocyclopentadiene; benzene; chlorobenzene; dichlorobenzene;
1,2,4-trichlorobenzene; tetrachlorobenzene; pentachlorobenzene;
hexachlorobenzene; toluene; naphthalene.
F026
Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and
hexachlorodibenzofurans.
F027
Tetra-, penta, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and
hexachlorodibenzofurans; tri-, tetra-, and pentachlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amine and other salts.
F028
Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and
hexachlorodibenzofurans; tri-, tetra-, and pentachlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amine and other salts.
F032
Benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)anthracene, indeno(1,2,3-
cd)pyrene, pentachlorophenol, arsenic, chromium, tetra-, penta-, hexa-,
heptachlorordibenzo-p-dioxins, tetra-, penta-, hexa-,
heptachlorodibenzofurans.
F034
Benz(a)anthracene, benzo(k)fluoranthene, benzo(a)pyrene,
dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene, naphthalene, arsenic
chromium.
F035
Arsenic, chromium and lead.
F037
Benzene, benzo(a)pyrene, chrysene, lead, chromium.
F038
Benzene, benzo(a)pyrene, chrysene, lead, chromium.
F039
All constituents for which treatment standards are specified for multi-
source leachate (wastewaters and non-wastewaters) under 35 Ill. Adm.
Code 728.Table B (Constituent Concentrations in Waste).
141
K001
Pentachlorophenol, phenol, 2-chlorophenol, p-chloro-m-cresol, 2,4-
dimethylphenol, 2,4- dinitrophenol, trichlorophenols, tetrachlorophenols,
2,4- dinitrophenol, cresosote, chrysene, naphthalene, fluoranthene,
benzo(b)fluoranthene, benzo(a)pyrene, indeno(1,2,3-cd)pyrene, benz(a)
anthracene, dibenz(a)anthracene, acenaphthalene.
K002
Hexavalent chromium, lead.
K003
Hexavalent chromium, lead.
K004
Hexavalent chromium.
K005
Hexavalent chromium, lead.
K006
Hexavalent chromium.
K007
Cyanide (complexed), hexavalent chromium.
K008
Hexavalent chromium.
K009
Chloroform, formaldehyde, methylene chloride, methyl chloride,
paraldehyde, formic acid.
K010
Chloroform, formaldehyde, methylene chloride, methyl chloride,
paraldehyde, formic acid, chloroacetaldehyde.
K011
Acrylonitrile, acetonitrile, hydrocyanic acid.
K013
Hydrocyanic acid, acrylonitrile, acetonitrile.
K014
Acetonitrile, acrylamide.
K015
Benzyl chloride, chlorobenzene, toluene, benzotrichloride.
K016
Hexachlorobenzene, hexachlorobutadiene, carbon tetrachloride,
hexachloroethane, perchloroethylene.
K017
Epichlorohydrin, chloroethers [bis(chloromethyl) ether and bis- (2-
chloroethyl) ethers], trichloropropane, dichloropropanols.
K018
1,2-dichloroethane, trichloroethylene, hexachlorobutadiene,
hexachlorobenzene.
K019
Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon
tetrachloride, chloroform, vinyl chloride, vinylidene chloride.
K020
Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
tetrachloro-ethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon
tetrachloride, chloroform, vinyl chloride, vinylidene chloride.
K021
Antimony, carbon tetrachloride, chloroform.
K022
Phenol, tars (polycyclic aromatic hydrocarbons).
K023
Phthalic anhydride, maleic anhydride.
K024
Phthalic anhydride, 1,4-naphthoguinone.
K025
Meta-dinitrobenzene, 2,4-dinitrotoluene.
K026
Paraldehyde, pyridines, 2-picoline.
K027
Toluene diisocyanate, toluene-2,4-diamine.
K028
1,1,1-trichloroethane, vinyl chloride.
K029
1,2-dichloroethane, 1,1,1-trichloroethane, vinyl chloride, vinylidene
chloride, chloroform.
142
K030
Hexachlorobenzene, hexachlorobutadiene, hexachloroethane, 1,1,1,2-
tetrachloroethane, 1,1,2,2-tetrachloroethane, ethylene dichloride.
K031
Arsenic.
K032
Hexachlorocyclopentadiene.
K033
Hexachlorocyclopentadiene.
K034
Hexachlorocyclopentadiene.
K035
Creosote, chrysene, naphthalene, fluoranthene, benzo(b) fluoranthene,
benzo(a)-pyrene, indeno(1,2,3-cd) pyrene, benzo(a)anthracene,
dibenzo(a)anthracene, acenaphthalene.
K036
Toluene, phosphorodithioic and phosphorothioic acid esters.
K037
Toluene, phosphorodithioic and phosphorothioic acid esters.
K038
Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters.
K039
Phosphorodithioic and phosphorothioic acid esters.
K040
Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters.
K041
Toxaphene.
K042
Hexachlorobenzene, ortho-dichlorobenzene.
K043
2,4-dichlorophenol, 2,6-dichlorophenol, 2,4,6-trichlorophenol.
K044
N.A.
K045
N.A.
K046
Lead.
K047
N.A.
K048
Hexavalent chromium, lead.
K049
Hexavalent chromium, lead.
K050
Hexavalent chromium.
K051
Hexavalent chromium, lead.
K052
Lead.
K060
Cyanide, naphthalene, phenolic compounds, arsenic.
K061
Hexavalent chromium, lead, cadmium.
K062
Hexavalent chromium, lead.
K064
Lead, cadmium.
K065
Lead, cadmium.
K066
Lead, cadmium.
K069
Hexavalent chromium, lead, cadmium.
K071
Mercury.
K073
Chloroform, carbon tetrachloride, hexachloroethane, trichloroethane,
tetrachloroethylene, dichloroethylene, 1,1,2,2-tetrachloroethane.
K083
Aniline, diphenylamine, nitrobenzene, phenylenediamine.
K084
Arsenic.
K085
Benzene, dichlorobenzenes, trichlorobenzenes, tetrachlorobenzenes,
pentachlorobenzene, hexachlorobenzene, benzyl chloride.
K086
Lead, hexavalent chromium.
K087
Phenol, naphthalene.
K088
Cyanide (complexes).
K090
Chromium.
K091
Chromium.
143
K093
Phthalic anhydride, maleic anhydride.
K094
Phthalic anhydride.
K095
1,1,2-trichloroethane, 1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane.
K096
1,2-dichloroethane, 1,1,1-trichloroethane, 1,1,2-trichloroethane.
K097
Chlordane, heptachlor.
K098
Toxaphene.
K099
2,4-dichlorophenol, 2,4,6-trichlorophenol.
K100
Hexavalent chromium, lead, cadmium.
K101
Arsenic.
K102
Arsenic.
K103
Aniline, nitrobenzene, phenylenediamine.
K104
Aniline, benzene, diphenylamine, nitrobenzene, phynylenediamine.
K105
Benzene, monochlorobenzene, dichlorobenzenes, 2,4,6-trichlorophenol.
K106
Mercury.
K111
2,4-Dinitrotoluene.
K112
2,4-Toluenediamine, o-toluidine, p-toluidine, aniline.
K113
2,4-Toluenediamine, o-toluidine, p-toluidine, aniline.
K114
2,4-Toluenediamine, o-toluidine, p-toluidine.
K115
2,4-Toluenediamine.
K116
Carbon tetrachloride, tetrachloroethylene, chloroform, phosgene.
K117
Ethylene dibromide.
K118
Ethylene dibromide.
K123
Ethylene thiourea.
K124
Ethylene thiourea.
K125
Ethylene thiourea.
K126
Ethylene thiourea.
K131
Dimethyl sulfate, methyl bromide.
K132
Methyl bromide.
K136
Ethylene dibromide.
K140
2,4,6-Tribromophenol.
K141
Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene.
K142
Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene.
K143
Benzene, benz(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene.
K144
Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene.
K145
Benzene, benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)anthracene,
naphthalene.
K147
Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene.
K148
Benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene.
144
K149
Benzotrichloride, benzyl chloride, chloroform, chloromethane,
chlorobenzene, 1,4-dichlorobenzene, hexachlorobenzene,
pentachlorobenzene, 1,2,4,5-tetrachlorobenzene, toluene.
K150
Carbon tetrachloride, chloroform, chloromethane, 1,4-dichlorobenzene,
hexachlorobenzene, pentachlorobenzene, 1,2,4,5-tetrachlorobenzene,
1,1,2,2-tetrachloroethane, tetrachloroethylene, 1,2,4-trichlorobenzene.
K151
Benzene, carbon tetrachloride, chloroform, hexachlorobenzene,
pentachlorobenzene, toluene, 1,2,4,5-tetrachlorobenzene,
tetrachloroethylene.
K156
Benomyl, carbaryl, carbendazim, carbofuran, carbosulfan, formaldehyde,
methylene chloride, triethylamine.
K157
Carbon tetrachloride, formaldehyde, methyl chloride, methylene chloride,
pyridine, triethylamine.
K158
Benomyl, carbendazim, carbofuran, carbosulfan, chloroform, methylene
chloride.
K159
Benzene, butylate, EPTC, molinate, pebulate, vernolate.
K161
Antimony, arsenic, metam-sodium, ziram.
K169
Benzene.
K170
Benzo(a)pyrene, dibenz(a,h)anthracene, benzo (a) anthracene,
benzo(b)fluoranthene, benzo(k)fluoranthene, 3-methylcholanthrene, 7,12-
dimethylbenz(a)anthracene.
K171
Benzene, arsenic.
K172
Benzene, arsenic.
N.A.--Waste is hazardous because it fails the test for the characteristic of ignitability,
corrosivity or reactivity.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.Appendix H
Hazardous Constituents
Common Name
Chemical Abstracts Name
Chemical
Abstracts
Number
(CAS No.)
USEPA
Hazard-
ous
Waste
Number
A2213
Ethanimidothioic acid, 2-
(dimethylamino)-N-hydroxy-2-
oxo-, methyl ester
30558-43-1
U394
Acetonitrile
Same
75-05-8
U003
Acetophenone
Ethanone, 1-phenyl-
98-86-2
U004
2-Acetylaminofluorene
Acetamide, N-9H-fluoren-2-yl- 53-96-3
U005
Acetyl chloride
Same
75-36-5
U006
1-Acetyl-2-thiourea
Acetamide, N-
(aminothioxomethyl)-
591-08-2
P002
145
Acrolein
2-Propenal
107-02-8
P003
Acrylamide
2-Propenamide
79-06-1
U007
Acrylonitrile
2-Propenenitrile
107-13-1
U009
Aflatoxins
Same
1402-68-2
Aldicarb
Propanal, 2-methyl-2-
(methylthio)-, O-
[(methylamino)carbonyl]oxime
116-06-3
P070
Aldicarb sulfone
Propanal, 2-methyl-2- (methyl-
sulfonyl)-, O-[(methylamino)-
carbonyl]oxime
1646-88-4
P203
Aldrin
1,4,5,8-Dimethanonaphthalene,
1,2,3,4,10,10-hexachloro-
1,4,4a,5,8,8a-hexahydro-, (1-
α
,4-α,4a-β,5-α,8-α,8a-β)-
309-00-2
P004
Allyl alcohol
2-Propen-1-ol
107-18-6
P005
Allyl chloride
1-Propene, 3-chloro-
107-18-6
Aluminum phosphide
Same
20859-73-8
P006
4-Aminobiphenyl
[1,1'-Biphenyl]-4-amine
92-67-1
5-(Aminomethyl)-3-isoxazolol
3(2H)-Isoxazolone, 5-(amino-
methyl)-
2763-96-4
P007
4-Aminopyridine
4-Pyridinamine
504-24-5
P008
Amitrole
1H-1,2,4-Triazol-3-amine
61-82-5
U011
Ammonium vanadate
Vanadic acid, ammonium salt
7803-55-6
U119
Aniline
Benzenamine
62-53-3
U012
Antimony
Same
7440-36-0
Antimony compounds, N.O.S.
(not otherwise specified)
Aramite
Sulfurous acid, 2-chloroethyl-,
2-[4-(1,1-dimethylethyl)-
phenoxy]-1-methylethyl ester
140-57-8
Arsenic
Arsenic
7440-38-2
Arsenic compounds, N.O.S.
Arsenic acid
Arsenic acid H3AsO4
7778-39-4
P010
Arsenic pentoxide
Arsenic oxide As2O5
1303-28-2
P011
Arsenic trioxide
Arsenic oxide As2O3
1327-53-3
P012
Auramine
Benzenamine, 4,4'-carbon-
imidoylbis[N, N-dimethyl-
492-80-8
U014
Azaserine
L-Serine, diazoacetate (ester)
115-02-6
U015
Barban
Carbamic acid, (3-chloro-
phenyl)-, 4-chloro-2-butynyl
ester
101-27-9
U280
Barium
Same
7440-39-3
Barium compounds, N.O.S.
Barium cyanide
Same
542-62-1
P013
146
Bendiocarb
1,3-Benzodioxol-4-ol-2,2-
dimethyl-, methyl carbamate
22781-23-3
U278
Bendiocarb phenol
1,3-Benzodioxol-4-ol-2,2-
dimethyl-,
22961-82-6
U364
Benomyl
Carbamic acid, [1- [(butyl-
amino)carbonyl]-1H-benz-
imidazol-2-yl]-, methyl ester
17804-35-2
U271
Benz[c]acridine
Same
225-51-4
U016
Benz[a]anthracene
Same
56-55-3
U018
Benzal chloride
Benzene, (dichloromethyl)-
98-87-3
U017
Benzene
Same
71-43-2
U018
Benzenearsonic acid
Arsonic acid, phenyl-
98-05-5
Benzidine
[1,1'-Biphenyl]-4,4'-diamine
92-87-5
U021
Benzo[b]fluoranthene
Benz[e]acephenanthrylene
205-99-2
Benzo[j]fluoranthene
Same
205-82-3
Benzo(k)fluoranthene
Same
207-08-9
Benzo[a]pyrene
Same
50-32-8
U022
p-Benzoquinone
2,5-Cyclohexadiene-1,4-dione
106-51-4
U197
Benzotrichloride
Benzene, (trichloromethyl)-
98-07-7
U023
Benzyl chloride
Benzene, (chloromethyl)-
100-44-7
P028
Beryllium powder
Same
7440-41-7
P015
Beryllium compounds, N.O.S.
Bis(pentamethylene)thiuram
tetrasulfide
Piperidine, 1,1'-(tetrathio-
dicarbonothioyl)-bis-
120-54-7
Bromoacetone
2-Propanone, 1-bromo-
598-31-2
P017
Bromoform
Methane, tribromo-
75-25-2
U225
4-Bromophenyl phenyl ether
Benzene, 1-bromo-4-phenoxy-
101-55-3
U030
Brucine
Strychnidin-10-one, 2,3-
dimethoxy-
357-57-3
P018
Butylate
Carbamothioic acid, bis(2-
methylpropyl)-, S-ethyl ester
2008-41-5
Butyl benzyl phthalate
1,2-Benzenedicarboxylic acid,
butyl phenylmethyl ester
85-68-7
Cacodylic acid
Arsenic acid, dimethyl-
75-60-5
U136
Cadmium
Same
7440-43-9
Cadmium compounds, N.O.S.
Calcium chromate
Chromic acid H2CrO4, calcium
salt
13765-19-0
U032
Calcium cyanide
Calcium cyanide Ca(CN)2
592-01-8
P021
Carbaryl
1-Naphthalenol, methyl-
carbamate
63-25-2
U279
Carbendazim
Carbamic acid, 1H-benz-
imidazol-2-yl, methyl ester
10605-21-7
U372
147
Carbofuran
7-Benzofuranol, 2,3-dihydro-
2,2-dimethyl-, methyl-
carbamate
1563-66-2
P127
Carbofuran phenol
7-Benzofuranol, 2,3-dihydro-
2,2-dimethyl-
1563-38-8
U367
Carbosulfan
Carbamic acid, [(dibutyl-
amino)thio] methyl-, 2,3-
dihydro-2,2-dimethyl-7-benzo-
furanyl ester
55285-14-8
P189
Carbon disulfide
Same
75-15-0
P022
Carbon oxyfluoride
Carbonic difuoride
353-50-4
U033
Carbon tetrachloride
Methane, tetrachloro-
56-23-5
U211
Chloral
Acetaldehyde, trichloro-
75-87-6
U034
Chlorambucil
Benzenebutanoic acid, 4[bis-(2-
chloroethyl)amino]-
305-03-3
U035
Chlordane
4,7-Methano-1H-indene,
1,2,4,5,6,7,8,8-octachloro-
2,3,3a,4,7,7a-hexahydro-
57-74-9
U036
Chlordane,
α
and
γ
isomers
U036
Chlorinated benzenes, N.O.S.
Chlorinated ethane, N.O.S.
Chlorinated fluorocarbons,
N.O.S.
Chlorinated naphthalene, N.O.S.
Chlorinated phenol, N.O.S.
Chlornaphazine
Naphthalenamine, N,N’-bis(2-
chloroethyl)-
494-03-1
U026
Chloroacetaldehyde
Acetaldehyde, chloro-
107-20-0
P023
Chloroalkyl ethers, N.O.S.
p-Chloroaniline
Benzenamine, 4-chloro-
106-47-8
P024
Chlorobenzene
Benzene, chloro-
108-90-7
U037
Chlorobenzilate
Benzeneacetic acid, 4-chloro-α-
(4-chlorophenyl)-α-hydroxy-,
ethyl ester
510-15-6
U038
p-Chloro-m-cresol
Phenol, 4-chloro-3-methyl-
59-50-7
U039
2-Chloroethyl vinyl ether
Ethene, (2-chloroethoxy)-
110-75-8
U042
Chloroform
Methane, trichloro-
67-66-3
U044
Chloromethyl methyl ether
Methane, chloromethoxy-
107-30-2
U046
β-Chloronaphthalene
Naphthalene, 2-chloro-
91-58-7
U047
o-Chlorophenol
Phenol, 2-chloro-
95-57-8
U048
1-(o-Chlorophenyl)thiourea
Thiourea, (2-chlorophenyl)-
5344-82-1
P026
Chloroprene
1,3-Butadiene, 2-chloro-
126-99-8
3-Chloropropionitrile
Propanenitrile, 3-chloro-
542-76-7
P027
Chromium
Same
7440-47-3
Chromium compounds, N.O.S.
148
Chrysene
Same
218-01-9
U050
Citrus red No. 2
2-Naphthalenol, 1-[(2,5-
dimethoxyphenyl)azo]-
6358-53-8
Coal tar creosote
Same
8007-45-2
Copper cyanide
Copper cyanide CuCN
544-92-3
P029
Copper dimethyldithiocarbamate
Copper, bis(dimethylcarbamo-
dithioato-S,S’)-,
137-29-1
Creosote
Same
U051
Cresols (Cresylic acid)
Phenol, methyl-
1319-77-3
U052
Crotonaldehyde
2-Butenal
4170-30-3
U053
m-Cumenyl methylcarbamate
Phenol, 3-(methylethyl)-,
methyl carbamate
64-00-6
P202
Cyanides (soluble salts and
complexes), N.O.S.
P030
Cyanogen
Ethanedinitrile
460-19-5
P031
Cyanogen bromide
Cyanogen bromide (CN)Br
506-68-3
U246
Cyanogen chloride
Cyanogen chloride (CN)Cl
506-77-4
P033
Cycasin
β-D-glucopyranoside,
(methyl-
ONN-azoxy)methyl-
14901-08-7
Cycloate
Carbamothioic acid, cyclo-
hexylethyl-, S-ethyl ester
1134-23-2
2-Cyclohexyl-4,6-dinitrophenol
Phenol, 2-cyclohexyl-4,6-
dinitro-
131-89-5
P034
Cyclophosphamide
2H-1,3,2-Oxazaphosphorin-2-
amine, N,N-bis(2-chloro-
ethyl)tetrahydro-, 2-oxide
50-18-0
U058
2,4-D
Acetic acid, (2,4-dichloro-
phenoxy)-
94-75-7
U240
2,4-D, salts and esters
Acetic acid, (2,4-
dichlorophenoxy)-, salts and
esters
U240
Daunomycin
5, 12-Naphthacenedione, 8-
acetyl-10-[(3-amino-2,3,6-
trideoxy-α-L-lyxo-hexo-
pyranosyl)oxy]-7,8,9,10-
tetrahydro-6,8,11-trihydroxy-l-
methoxy-, 8S-cis)-
20830-81-3
U059
Dazomet
2H-1,3,5-thiadiazine-2-thione,
tetrahydro-3,5-dimethyl
533-74-4
DDD
Benzene, 1,1'-(2,2-dichloro-
ethylidene)bis[4-chloro-
72-54-8
U060
DDE
Benzene, 1,1'-(dichloroethenyl-
idene)bis[4-chloro-
72-55-9
DDT
Benzene, 1,1'-(2,2,2-trichloro-
ethylidene)bis[4-chloro-
50-29-3
U061
149
Diallate
Carbamothioic acid, bis(1-
methylethyl)-, S-(2,3-dichloro-
2-propenyl) ester
2303-16-4
U062
Dibenz[a,h]acridine
Same
226-36-8
Dibenz[a,j]acridine
Same
224-42-0
Dibenz[a,h]anthracene
Same
53-70-3
U063
7H-Dibenzo[c,g]carbazole
Same
194-59-2
Dibenzo[a,e]pyrene
Naphtho[1,2,3,4-def]chrysene
192-65-4
Dibenzo[a,h]pyrene
Dibenzo[b,def]chrysene
189-64-0
Dibenzo[a,i]pyrene
Benzo[rst]pentaphene
189-55-9
U064
1,2-Dibromo-3-chloropropane
Propane, 1,2-dibromo-3-
chloro-
96-12-8
U066
Dibutyl phthalate
1,2-Benzenedicarboxylic acid,
dibutyl ester
84-74-2
U069
o-Dichlorobenzene
Benzene, 1,2-dichloro-
95-50-1
U070
m-Dichlorobenzene
Benzene, 1,3-dichloro-
541-73-1
U071
p-Dichlorobenzene
Benzene, 1,4-dichloro-
106-46-7
U072
Dichlorobenzene, N.O.S.
Benzene, dichloro-
25321-22-6
3,3'-Dichlorobenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dichloro-
91-94-1
U073
1,4-Dichloro-2-butene
2-Butene, 1,4-dichloro-
764-41-0
U074
Dichlorodifluoromethane
Methane, dichlorodifluoro-
75-71-8
U075
Dichloroethylene, N.O.S.
Dichloroethylene
25323-30-2
1,1-Dichloroethylene
Ethene, 1,1-dichloro-
75-35-4
U078
1,2-Dichloroethylene
Ethene, 1,2-dichloro-, (E)-
156-60-5
U079
Dichloroethyl ether
Ethane, 1,1'-oxybis[2-chloro-
111-44-4
U025
Dichloroisopropyl ether
Propane, 2,2'-oxybis[2-chloro-
108-60-1
U027
Dichloromethoxyethane
Ethane, 1,1'-[methylenebis-
(oxy)bis[2-chloro-
111-91-1
U024
Dichloromethyl ether
Methane, oxybis[chloro-
542-88-1
P016
2,4-Dichlorophenol
Phenol, 2,4-dichloro-
120-83-2
U081
2,6-Dichlorophenol
Phenol, 2,6-dichloro-
87-65-0
U082
Dichlorophenylarsine
Arsonous dichloride, phenyl-
696-28-6
P036
Dichloropropane, N.O.S.
Propane, dichloro-
26638-19-7
Dichloropropanol, N.O.S.
Propanol, dichloro-
26545-73-3
Dichloropropene, N.O.S.
1-Propene, dichloro-
26952-23-8
1,3-Dichloropropene
1-Propene, 1,3-dichloro-
542-75-6
U084
Dieldrin
2,7:3,6-Dimethanonaphth[2, 3-
b]oxirene,3,4,5,6,9,9-hexa-
chloro-1a,2,2a,3,6, 6a,7,7a-
octahydro-,
(1aα,2β,2aα,3β,6β,6aα,7β,7a
α)-
60-57-1
P037
1,2:3,4-Diepoxybutane
2,2'-Bioxirane
1464-53-5
U085
Diethylarsine
Arsine, diethyl-
692-42-2
P038
150
Diethylene glycol, dicarbamate
Ethanol, 2,2'-oxybis-,
dicarbamate
5952-26-1
U395
1,4-Diethyleneoxide
1,4-Dioxane
123-91-1
U108
Diethylhexyl phthalate
1,2-Benzenedicarboxylic acid,
bis(2-ethylhexyl) ester
117-81-7
U028
N,N’-Diethylhydrazine
Hydrazine, 1,2-diethyl-
1615-80-1
U086
O,O-Diethyl-S-methyl dithio-
phosphate
Phosphorodithioic acid, O,O-
diethyl S-methyl ester
3288-58-2
U087
Diethyl-p-nitrophenyl phosphate
Phosphoric acid, diethyl 4-
nitrophenyl ester
311-45-5
P041
Diethyl phthalate
1,2-Benzenedicarboxylic acid,
diethyl ester
84-66-2
U088
O,O-Diethyl O-pyrazinyl
phosphorothioate
Phosphorothioic acid, O,O-
diethyl O-pyrazinyl ester
297-97-2
P040
Diethylstilbestrol
Phenol, 4,4'-(1,2-diethyl-1,2-
ethenediyl)bis-, (E)-
56-53-1
U089
Dihydrosafrole
1,3-Benzodioxole, 5-propyl-
94-58-6
U090
Diisopropylfluorophosphate
(DFP)
Phosphorofluoridic acid, bis(1-
methylethyl) ester
55-91-4
P043
Dimethoate
Phosphorodithioic acid, O,O-
dimethyl S-[2-(methylamino)-2-
oxoethyl] ester
60-51-5
P044
Dimetilan
Carbamic acid, dimethyl-, 1-
[(dimethylamino) carbonyl]-5-
methyl-1H-pyrazol-3-yl ester
644-64-4
P191
3,3'-Dimethoxybenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dimethoxy-
119-90-4
U091
p-Dimethylaminoazobenzene
Benzenamine, N,N-dimethyl-4-
(phenylazo)-
60-11-7
U093
7,12-Dimethylbenz[a]anthracene
Benz[a]anthracene, 7,12-
dimethyl-
57-97-6
U094
3,3'-Dimethylbenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dimethyl-
119-93-7
U095
Dimethylcarbamoyl chloride
Carbamic chloride, dimethyl-
79-44-7
U097
1,1-Dimethylhydrazine
Hydrazine, 1,1-dimethyl-
57-14-7
U098
1,2-Dimethylhydrazine
Hydrazine, 1,2-dimethyl-
540-73-8
U099
α
,
α-Dimethylphenethylamine
Benzeneethanamine,
α
,
α-
dimethyl-
122-09-8
P046
2,4-Dimethylphenol
Phenol, 2,4-dimethyl-
105-67-9
U101
Dimethylphthalate
1,2-Benzenedicarboxylic acid,
dimethyl ester
131-11-3
U102
Dimethyl sulfate
Sulfuric acid, dimethyl ester
77-78-1
U103
Dinitrobenzene, N.O.S.
Benzene, dinitro-
25154-54-5
4,6-Dinitro-o-cresol
Phenol, 2-methyl-4,6-dinitro-
534-52-1
P047
4,6-Dinitro-o-cresol salts
P047
151
2,4-Dinitrophenol
Phenol, 2,4-dinitro-
51-28-5
P048
2,4-Dinitrotoluene
Benzene, 1-methyl-2,4-dinitro-
121-14-2
U105
2,6-Dinitrotoluene
Benzene, 2-methyl-1,3-dinitro-
606-20-2
U106
Dinoseb
Phenol, 2-(1-methylpropyl)-
4,6-dinitro-
88-85-7
P020
Di-n-octyl phthalate
1,2-Benzenedicarboxylic acid,
dioctyl ester
117-84-0
U107
Diphenylamine
Benzenamine, N-phenyl-
122-39-4
1,2-Diphenylhydrazine
Hydrazine, 1,2-diphenyl-
122-66-7
U109
Di-n-propylnitrosamine
1-Propanamine, N-nitroso-N-
propyl-
621-64-7
U111
Disulfiram
Thioperoxydicarbonic diamide,
tetraethyl
97-77-8
Disulfoton
Phosphorodithioic acid, O,O-
diethyl S-[2-(ethylthio)ethyl]
ester
298-04-4
P039
Dithiobiuret
Thioimidodicarbonic diamide
[(H2N)C(S)]2NH
541-53-7
P049
Endosulfan
6, 9-Methano-2,4,3-benzo-
dioxathiepen,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-oxide,
115-29-7
P050
Endothal
7-Oxabicyclo[2.2.1]heptane-
2,3-dicarboxylic acid
145-73-3
P088
Endrin
2,7:3,6-Dimethanonaphth[2,3-
b]oxirene, 3,4,5,6,9,9-hexa-
chloro-1a,2,2a,3,6,6a,7,7a-
octahydro-, (1a
α
,2β,2aβ,3α,6α,6aβ,7β,7aα)-,
72-20-8
P051
Endrin metabolites
P051
Epichlorohydrin
Oxirane, (chloromethyl)-
106-89-8
U041
Epinephrine
1,2-Benzenediol, 4-[1-hydroxy-
2-(methylamino)ethyl]-, (R)-
51-43-4
P042
EPTC
Carbamothioic acid, dipropyl-,
S-ethyl ester
759-94-4
Ethyl carbamate (urethane)
Carbamic acid, ethyl ester
51-79-6
U238
Ethyl cyanide
Propanenitrile
107-12-0
P101
Ethylenebisdithiocarbamic acid
Carbamodithioic acid, 1,2-
ethanediylbis-
111-54-6
U114
Ethylenebisdithiocarbamic acid,
salts and esters
U114
Ethylene dibromide
Ethane, 1,2-dibromo-
106-93-4
U067
Ethylene dichloride
Ethane, 1,2-dichloro-
107-06-2
Ethylene glycol monoethyl ether
Ethanol, 2-ethoxy-
110-80-5
U359
Ethyleneimine
Aziridine
151-56-4
P054
152
Ethylene oxide
Oxirane
75-21-8
U115
Ethylenethiourea
2-Imidazolidinethione
96-45-7
U116
Ethylidine dichloride
Ethane, 1,1-dichloro-
75-34-3
U076
Ethyl methacrylate
2-Propenoic acid, 2-methyl-,
ethyl ester
97-63-2
U118
Ethyl methanesulfonate
Methanesulfonic acid, ethyl
ester
62-50-0
U119
Ethyl Ziram
Zinc, bis(diethylcarbamo-
dithioato-S,S’)-
14324-55-1
U407
Famphur
Phosphorothioc acid, O-[4-
[(dimethylamino)sulfonyl]-
phenyl] O,O-dimethyl ester
52-85-7
P097
Ferbam
Iron, tris(dimethylcarbamo-
dithioato-S,S’)-,
14484-64-1
Fluoranthene
Same
206-44-0
U120
Fluorine
Same
7782-41-4
P056
Fluoroacetamide
Acetamide, 2-fluoro-
640-19-7
P057
Fluoroacetic acid, sodium salt
Acetic acid, fluoro-, sodium
salt
62-74-8
P058
Formaldehyde
Same
50-00-0
U122
Formetanate hydrochloride
Methanimidamide, N,N-
dimethyl-N’-[3-[[(methyl-
amino)carbonyl]oxy]phenyl]-,
monohydrochloride
23422-53-9
P198
Formic acid
Same
64-18-16
U123
Formparanate
Methanimidamide, N,N-
dimethyl-N’-[2-methyl-4-
[[(methylamino)carbonyl]oxy]-
phenyl]-
17702-57-7
P197
Glycidylaldehyde
Oxiranecarboxaldehyde
765-34-4
U126
Halomethanes, N.O.S.
Heptachlor
4,7-Methano-1H-
indene,1,4,5,6,7,8,8-
heptachloro-3a,4,7,7a-tetra-
hydro-
76-44-8
P059
Heptachlor epoxide
2,5-Methano-2H-indeno[1,
2b]oxirene, 2,3,4,5,6,7,7-
heptachloro-1a,1b,5,5a,6,6a-
hexahydro-,
(1aα,1bβ,2α,5α,5aβ,6β,6aα)-
1024-57-3
Heptachlor epoxide (α,
β
, and
γ
isomers)
Heptachlorodibenzofurans
Heptachlorodibenzo-p-dioxins
Hexachlorobenzene
Benzene, hexachloro-
118-74-1
U127
153
Hexachlorobutadiene
1,3-Butadiene, 1,1,2,3,4,4-
hexachloro-
87-68-3
U128
Hexachlorocyclo-pentadiene
1,3-Cyclopentadiene,
1,2,3,4,5,5-hexachloro-
77-47-4
U130
Hexachlorodibenzo-p-dioxins
Hexachlorodibenzofurans
Hexachloroethane
Ethane, hexachloro-
67-72-1
U131
Hexachlorophene
Phenol, 2,2'-methylene-
bis[3,4,6-trichloro-
70-30-4
U132
Hexachloropropene
1-Propene, 1,1,2,3,3,3-
hexachloro-
1888-71-7
U243
Hexaethyltetraphosphate
Tetraphosphoric acid,
hexaethyl ester
757-58-4
P062
Hydrazine
Same
302-01-2
U133
Hydrogen cyanide
Hydrocyanic acid
74-90-8
P063
Hydrogen fluoride
Hydrofluoric acid
7664-39-3
U134
Hydrogen sulfide
Hydrogen sulfide H2S
7783-06-4
U135
Indeno[1,2,3-cd]pyrene
Same
193-39-5
U137
3-Iodo-2-propynyl-n-butyl-
carbamate
Carbamic acid, butyl-, 3-iodo-
2-propynyl ester
55406-53-6
Isobutyl alcohol
1-Propanol, 2-methyl-
78-83-1
U140
Isodrin
1,4:5,8-Dimethanonaph-
thalene,1,2,3,4,10,10-hexa-
chloro-1,4,4a,5,8,8a-
hexahydro-,
(1α,4α,4aβ,5β,8β,8aβ)-,
465-73-6
P060
Isolan
Carbamic acid, dimethyl-, 3-
methyl-1-(1-methylethyl)-1H-
pyrazol-5-yl ester
119-38-0
P192
Isosafrole
1,3-Benzodioxole, 5-(1-
propenyl)-
120-58-1
U141
Kepone
1,3,4-Metheno-2H-cyclobuta-
[cd]pentalen-2-one,
1,1a,3,3a,4,5,5,5a,5b,6-
decachlorooctahydro-,
143-50-0
U142
Lasiocarpine
2-Butenoic acid, 2-methyl-, 7-
[[2,3-dihydroxy-2-(1-
methoxyethyl)-3-methyl-1-
oxobutoxy]methyl]-2,3,5,7a-
tetrahydro-1H-pyrrolizin-l-yl
ester, [1S-[1-
α(Z),7(2S*,3R*),7aα]]-
303-34-1
U143
Lead
Same
7439-92-1
Lead and compounds, N.O.S.
Lead acetate
Acetic acid, lead (2+) salt
301-04-2
U144
154
Lead phosphate
Phosphoric acid, lead (2+) salt
(2:3)
7446-27-7
U145
Lead subacetate
Lead, bis(acetato-O)tetra-
hydroxytri-
1335-32-6
U146
Lindane
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
1α,2α,3β,4α,5α,6β)-
58-89-9
U129
Maleic anhydride
2,5-Furandione
108-31-6
U147
Maleic hydrazide
3,6-Pyridazinedione, 1,2-
dihydro-
123-33-1
U148
Malononitrile
Propanedinitrile
109-77-3
U149
Manganese dimethyldithio-
carbamate
Manganese, bis(dimethyl-
carbamodithioato-S,S’)-,
15339-36-3
P196
Melphalan
L-Phenylalanine, 4-[bis(2-
chloroethyl)amino]-
148-82-3
U150
Mercury
Same
7439-97-6
U151
Mercury compounds, N.O.S.
Mercury fulminate
Fulminic acid, mercury (2+)
salt
628-86-4
P065
Metam Sodium
Carbamodithioic acid, methyl-,
monosodium salt
137-42-8
Methacrylonitrile
2-Propenenitrile, 2-methyl-
126-98-7
U152
Methapyrilene
1,2-Ethanediamine, N,N-
dimethyl-N’-2-pyridinyl-N’-(2-
thienylmethyl)-
91-80-5
U155
Methiocarb
Phenol, (3,5-dimethyl-4-
(methylthio)-, methylcarbamate
2032-65-7
P199
Metholmyl
Ethanimidothioic acid, N-
[[(methylamino)carbonyl]oxy]-,
methyl ester
16752-77-5
P066
Methoxychlor
Benzene, 1,1'-(2,2,2-trichloro-
ethylidene)bis[4-methoxy-
72-43-5
U247
Methyl bromide
Methane, bromo-
74-83-9
U029
Methyl chloride
Methane, chloro-
74-87-3
U045
Methylchlorocarbonate
Carbonochloridic acid, methyl
ester
79-22-1
U156
Methyl chloroform
Ethane, 1,1,1-trichloro-
71-55-6
U226
3-Methylcholanthrene
Benz[j]aceanthrylene, 1,2-
dihydro-3-methyl-
56-49-5
U157
4,4'-Methylenebis(2-chloro-
aniline)
Benzenamine, 4,4'-methylene-
bis[2-chloro-
101-14-4
U158
Methylene bromide
Methane, dibromo-
74-95-3
U068
Methylene chloride
Methane, dichloro-
75-09-2
U080
Methyl ethyl ketone (MEK)
2-Butanone
78-93-3
U159
Methyl ethyl ketone peroxide
2-Butanone, peroxide
1338-23-4
U160
155
Methyl hydrazine
Hydrazine, methyl-
60-34-4
P068
Methyl iodide
Methane, iodo-
74-88-4
U138
Methyl isocyanate
Methane, isocyanato-
624-83-9
P064
2-Methyllactonitrile
Propanenitrile, 2-hydroxy-2-
methyl-
75-86-5
P069
Methyl methacrylate
2-Propenoic acid, 2-methyl-,
methyl ester
80-62-6
U162
Methyl methanesulfonate
Methanesulfonic acid, methyl
ester
66-27-3
Methyl parathion
Phosphorothioic acid, O,O-
dimethyl O-(4-nitrophenyl)
ester
298-00-0
P071
Methylthiouracil
4-(1H)-Pyrimidinone, 2,3-
dihydro-6-methyl-2-thioxo-
56-04-2
U164
Metolcarb
Carbamic acid, methyl-, 3-
methylphenyl ester
1129-41-5
P190
Mexacarbate
Phenol, 4-(dimethylamino)-3,5-
dimethyl-, methylcarbamate
(ester)
315-18-4
P128
Mitomycin C
Azirino[2', 3':3, 4]pyrrolo[1,
2-a]indole-4, 7-dione, 6-amino-
8-[[(aminocarbonyl)oxy]-
methyl]-1,1a,2,8,8a,8b-
hexahydro-8a-methoxy-5-
methyl-, [1a-S-
(1aα,8β,8aα,8bα)]-,
50-07-7
U010
Molinate
1H-Azepine-1-carbothioic acid,
hexahydro-, S-ethyl ester
2212-67-1
MNNG
Guanidine, N-methyl-N’-nitro-
N-nitroso-
70-25-7
U163
Mustard gas
Ethane, 1,1'-thiobis[2-chloro-
505-60-2
U165
Naphthalene
Same
91-20-3
U165
1,4-Naphthoquinone
1,4-Naphthalenedione
130-15-4
U166
α-Naphthylamine
1-Naphthalenamine
134-32-7
U167
β-Naphthylamine
2-Naphthalenamine
91-59-8
U168
α-Naphthylthiourea
Thiourea, 1-naphthalenyl-
86-88-4
P072
Nickel
Same
7440-02-0
Nickel compounds, N.O.S.
Nickel carbonyl
Nickel carbonyl Ni(CO)4, (T-
4)-
13463-39-3
P073
Nickel cyanide
Nickel cyanide Ni(CN)2
557-19-7
P074
Nicotine
Pyridine, 3-(1-methyl-2-
pyrrolidinyl)-, (S)-
54-11-5
P075
Nicotine salts
P075
Nitric oxide
Nitrogen oxide NO
10102-43-9
P076
156
p-Nitroaniline
Benzenamine, 4-nitro-
100-01-6
P077
Nitrobenzene
Benzene, nitro-
98-95-3
P078
Nitrogen dioxide
Nitrogen oxide NO2
10102-44-0
P078
Nitrogen mustard
Ethanamine, 2-chloro-N-(2-
chloroethyl)-N-methyl-
51-75-2
Nitrogen mustard, hydrochloride
salt
Nitrogen mustard N-oxide
Ethanamine, 2-chloro-N-(2-
chloroethyl)-N-methyl-, N-
oxide
126-85-2
Nitrogen mustard, N-oxide,
hydrochloride salt
Nitroglycerin
1,2,3-Propanetriol, trinitrate
55-63-0
P081
p-Nitrophenol
Phenol, 4-nitro-
100-02-7
U170
2-Nitropropane
Propane, 2-nitro-
79-46-9
U171
Nitrosamines, N.O.S.
35576-91-1
N-Nitrosodi-n-butylamine
1-Butanamine, N-butyl-N-
nitroso-
924-16-3
U172
N-Nitrosodiethanolamine
Ethanol, 2,2'-(nitroso-
imino)bis-
1116-54-7
U173
N-Nitrosodiethylamine
Ethanamine, N-ethyl-N-nitroso- 55-18-5
U174
N-Nitrosodimethylamine
Methanamine, N-methyl-N-
nitroso-
62-75-9
P082
N-Nitroso-N-ethylurea
Urea, N-ethyl-N-nitroso-
759-73-9
U176
N-Nitrosomethylethylamine
Ethanamine, N-methyl-N-
nitroso-
10595-95-6
N-Nitroso-N-methylurea
Urea, N-methyl-N-nitroso-
684-93-5
U177
N-Nitroso-N-methylurethane
Carbamic acid, methylnitroso-,
ethyl ester
615-53-2
U178
N-Nitrosomethylvinylamine
Vinylamine, N-methyl-N-
nitroso-
4549-40-0
P084
N-Nitrosomorpholine
Morpholine, 4-nitroso-
59-89-2
N-Nitrosonornicotine
Pyridine, 3-(1-nitroso-2-
pyrrolidinyl)-, (S)-
16543-55-8
N-Nitrosopiperidine
Piperidine, 1-nitroso-
100-75-4
U179
N-Nitrosopyrrolidine
Pyrrolidine, 1-nitroso-
930-55-2
U180
N-Nitrososarcosine
Glycine, N-methyl-N-nitroso-
13256-22-9
5-Nitro-o-toluidine
Benzenamine, 2-methyl-5-
nitro-
99-55-8
U181
Octamethylpyrophosphoramide
Diphosphoramide, octamethyl-
152-16-9
P085
Osmium tetroxide
Osmium oxide OsO4, (T-4)
20816-12-0
P087
Oxamyl
Ethanimidothioc acid, 2-
(dimethylamino)-N-[[(methyl-
amino)carbonyl]oxy]-2-oxo-,
methyl ester
23135-22-0
P194
157
Paraldehyde
1,3,5-Trioxane, 2,4,6-tri-
methyl-
123-63-7
U182
Parathion
Phosphorothioic acid, O,O-
diethyl O-(4-nitrophenyl) ester
56-38-2
P089
Pebulate
Carbamothioic acid, butylethyl-
, S-propyl ester
1114-71-2
Pentachlorobenzene
Benzene, pentachloro-
608-93-5
U183
Pentachlorodibenzo-p-dioxins
Pentachlorodibenzofurans
Pentachloroethane
Ethane, pentachloro-
76-01-7
U184
Pentachloronitrobenzene (PCNB) Benzene, pentachloronitro-
82-68-8
U185
Pentachlorophenol
Phenol, pentachloro-
87-86-5
See F027
Phenacetin
Acetamide, N-(4-
ethoxyphenyl)-
62-44-2
U187
Phenol
Same
108-95-2
U188
Phenylenediamine
Benzenediamine
25265-76-3
Phenylmercury acetate
Mercury, (acetato-O)phenyl-
62-38-4
P092
Phenylthiourea
Thiourea, phenyl-
103-85-5
P093
Phosgene
Carbonic dichloride
75-44-5
P095
Phosphine
Same
7803-51-2
P096
Phorate
Phosphorodithioic acid, O,O-
diethyl S-[(ethylthio)methyl]
ester
298-02-2
P094
Phthalic acid esters, N.O.S.
Phthalic anhydride
1,3-Isobenzofurandione
85-44-9
U190
Physostigmine
Pyrrolo[2,3-b]indol-5-ol,
1,2,3,3a,8,8a-hexahydro-
1,3a,8-trimethyl-, methyl-
carbamate (ester), (3aS-cis)-
57-47-6
P204
Physostigmine salicylate
Benzoic acid, 2-hydroxy-,
compound with (3aS-cis)-
1,2,3,3a,8,8a-hexahydro-
1,3a,8-trimethylpyrrolo[2,3-b]-
indol-5-yl methylcarbamate
ester (1:1)
57-64-7
P188
2-Picoline
Pyridine, 2-methyl-
109-06-8
U191
Polychlorinated biphenyls,
N.O.S.
Potassium cyanide
Same
151-50-8
P098
Potassium dimethyldithio-
carbamate
Carbamodithioc acid, dimethyl,
potassium salt
128-03-0
Potassium n-hydroxymethyl-n-
methyl-dithiocarbamate
Carbamodithioc acid,
(hydroxymethyl)methyl-,
monopotassium salt
51026-28-9
158
Potassium n-methyldithio-
carbamate
Carbamodithioc acid, methyl-
monopotassium salt
137-41-7
Potassium silver cyanide
Argentate(1-), bis(cyano-C)-,
potassium)
506-61-6
P099
Potassium pentachlorophenate
Pentachlorophenol, potassium
salt
7778736
None
Promecarb
Phenol, 3-methyl-5-(1-methyl-
ethyl)-, methyl carbamate
2631-37-0
P201
Pronamide
Benzamide, 3,5-dichloro-N-
(1,1-dimethyl-2-propynyl)-
23950-58-5
U192
1,3-Propane sultone
1,2-Oxathiolane, 2,2-dioxide
1120-71-4
U193
Propham
Carbamic acid, phenyl-, 1-
methylethyl ester
122-42-9
U373
Propoxur
Phenol, 2-(1-methylethoxy)-,
methylcarbamate
114-26-1
U411
n-Propylamine
1-Propanamine
107-10-8
U194
Propargyl alcohol
2-Propyn-1-ol
107-19-7
P102
Propylene dichloride
Propane, 1,2-dichloro-
78-87-5
U083
1,2-Propylenimine
Aziridine, 2-methyl-
75-55-8
P067
Propylthiouracil
4(1H)-Pyrimidinone, 2,3-
dihydro-6-propyl-2-thioxo-
51-52-5
Prosulfocarb
Carbamothioic acid, dipropyl-,
S-(phenylmethyl) ester
52888-80-9
U387
Pyridine
Same
110-86-1
U196
Reserpine
Yohimban-16-carboxylic acid,
11,17-dimethoxy-18-[(3,4,5-
trimethoxybenzoyl)oxy]-,
methyl ester,
(3β,16β,17α,18β,20α)-,
50-55-5
U200
Resorcinol
1,3-Benzenediol
108-46-3
U201
Saccharin
1,2-Benzisothiazol-3(2H)-one,
1,1-dioxide
81-07-2
U202
Saccharin salts
U202
Safrole
1,3-Benzodioxole, 5-(2-
propenyl)-
94-59-7
U203
Selenium
Same
7782-49-2
Selenium compounds, N.O.S.
Selenium dioxide
Selenious acid
7783-00-8
U204
Selenium sulfide
Selenium sulfide SeS2
7488-56-4
U205
Selenium, tetrakis(dimethyl-
dithiocarbamate
Carbamodithioic acid,
dimethyl-, tetraanhydrosulfide
with orthothioselenious acid
144-34-3
Selenourea
Same
630-10-4
P103
Silver
Same
7440-22-4
Silver compounds, N.O.S.
159
Silver cyanide
Silver cyanide AgCN
506-64-9
P104
Silvex (2,4,5-TP)
Propanoic acid, 2-(2,4,5-
trichlorophenoxy)-
93-72-1
See F027
Sodium cyanide
Sodium cyanide NaCN
143-33-9
P106
Sodium dibutyldithiocarbamate
Carbamodithioic acid, dibutyl-,
sodium salt
136-30-1
Sodium diethyldithiocarbamate
Carbamodithioic acid, diethyl-,
sodium salt
148-18-5
Sodium dimethyldithiocarbamate Carbamodithioic acid,
dimethyl-, sodium salt
128-04-1
Sodium pentachlorophenate
Pentachlorophenol, sodium salt 131522
None
Streptozotocin
D-Glucose, 2-deoxy-2-
[[(methylnitrosoamino)ca-
rbonyl]amino]-
18883-66-4
U206
Strychnine
Strychnidin-10-one
57-24-9
P108
Strychnine salts
P108
Sulfallate
Carbamodithioic acid, diethyl-,
2-chloro-2-propenyl ester
95-06-7
TCDD
Dibenzo[b,e][1,4]dioxin,
2,3,7,8-tetrachloro-
1746-01-6
Tetrabutylthiuram disulfide
Thioperoxydicarbonic diamide,
tetrabutyl
1634-02-2
Tetramethylthiuram monosulfide
Bis(dimethylthiocarbamoyl)
sulfide
97-74-5
1,2,4,5-Tetrachlorobenzene
Benzene, 1,2,4,5-tetrachloro-
95-94-3
U207
Tetrachlorodibenzo-p-dioxins
Tetrachlorodibenzofurans
Tetrachloroethane, N.O.S.
Ethane, tetrachloro-, N.O.S.
25322-20-7
1,1,1,2-Tetrachloroethane
Ethane, 1,1,1,2-tetrachloro-
630-20-6
U208
1,1,2,2-Tetrachloroethane
Ethane, 1,1,2,2-tetrachloro-
79-34-5
U209
Tetrachloroethylene
Ethene, tetrachloro-
127-18-4
U210
2,3,4,6-Tetrachlorophenol
Phenol, 2,3,4,6-tetrachloro-
58-90-2
See F027
2,3,4,6-Tetrachlorophenol,
potassium salt
Same
53535276
None
2,3,4,6-Tetrachlorophenol,
sodium salt
Same
25567559
None
Tetraethyldithiopyrophosphate
Thiodiphosphoric acid,
tetraethyl ester
3689-24-5
P109
Tetraethyl lead
Plumbane, tetraethyl-
78-00-2
P110
Tetraethylpyrophosphate
Diphosphoric acid, tetraethyl
ester
107-49-3
P111
Tetranitromethane
Methane, tetranitro-
509-14-8
P112
Thallium
Same
7440-28-0
Thallium compounds
Thallic oxide
Thallium oxide Tl2O3
1314-32-5
P113
160
Thallium (I) acetate
Acetic acid, thallium (1+) salt
563-68-8
U214
Thallium (I) carbonate
Carbonic acid, dithallium (1+)
salt
6533-73-9
U215
Thallium (I) chloride
Thallium chloride TlCl
7791-12-0
U216
Thallium (I) nitrate
Nitric acid, thallium (1+) salt
10102-45-1
U217
Thallium selenite
Selenious acid, dithallium (1+)
salt
12039-52-0
P114
Thallium (I) sulfate
Sulfuric acid, dithallium (1+)
salt
7446-18-6
P115
Thioacetamide
Ethanethioamide
62-55-5
U218
Thiodicarb
Ethanimidothioic acid, N,N’-
[thiobis[(methylimino)-
carbonyloxy]]-bis-, dimethyl
ester
59669-26-0
U410
Thiofanox
2-Butanone, 3,3-dimethyl-1-
(methylthio)-, O-
[(methylamino)carbonyl]oxime
39196-18-4
P045
Thiophanate-methyl
Carbamic acid, [1,2-
phyenylenebis(iminocarbono-
thioyl)]-bis-, dimethyl ester
23564-05-8
U409
Thiomethanol
Methanethiol
74-93-1
U153
Thiophenol
Benzenethiol
108-98-5
P014
Thiosemicarbazide
Hydrazinecarbothioamide
79-19-6
P116
Thiourea
Same
62-56-6
P219
Thiram
Thioperoxydicarbonic diamide
[(H2N)C(S)]2S2, tetramethyl-
137-26-8
U244
Tirpate
1,3-Dithiolane-2-carbox-
aldehyde, 2,4-dimethyl-, O-
[(methylamino)carbonyl] oxime
26419-73-8
P185
Toluene
Benzene, methyl-
108-88-3
U220
Toluenediamine
Benzenediamine, ar-methyl-
25376-45-8
U221
Toluene-2,4-diamine
1,3-Benzenediamine, 4-methyl- 95-80-7
Toluene-2,6-diamine
1,3-Benzenediamine, 2-methyl- 823-40-5
Toluene-3,4-diamine
1,2-Benzenediamine, 4-methyl- 496-72-0
Toluene diisocyanate
Benzene, 1,3-diisocyanato-
methyl-
26471-62-5
U223
o-Toluidine
Benzenamine, 2-methyl-
95-53-4
U328
o-Toluidine hydrochloride
Benzeneamine, 2-methyl-,
hydrochloride
636-21-5
U222
p-Toluidine
Benzenamine, 4-methyl-
106-49-0
U353
Toxaphene
Same
8001-35-2
P123
Triallate
Carbamothioic acid, bis(1-
methylethyl)-, S-(2,3,3-tri-
chloro-2-propenyl) ester
2303-17-5
U389
2,4,6-Tribromophenol
Tribromophenol, 2,4,6-
118-79-6
U408
161
1,2,4-Trichlorobenzene
Benzene, 1,2,4-trichloro-
120-82-1
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
79-00-5
U227
Trichloroethylene
Ethene, trichloro-
79-01-6
U228
Trichloromethanethiol
Methanethiol, trichloro-
75-70-7
P118
Trichloromonofluoromethane
Methane, trichlorofluoro-
75-69-4
U121
2,4,5-Trichlorophenol
Phenol, 2,4,5-trichloro-
95-95-4
See F027
2,4,6-Trichlorophenol
Phenol, 2,4,6-trichloro-
88-06-2
See F027
2,4,5-T
Acetic acid, (2,4,5-trichloro-
phenoxy)-
93-76-5
See F027
Trichloropropane, N.O.S.
25735-29-9
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
96-18-4
Triethylamine
Ethanamine, N,N-diethyl-
121-44-8
U404
O,O,O-Triethylphosphorothioate Phosphorothioic acid, O,O,O-
triethyl ester
126-68-1
1,3,5-Trinitrobenzene
Benzene, 1,3,5-trinitro-
99-35-4
U234
Tris(l-aziridinyl)phosphine
sulfide
Aziridine, 1,1',1"-phosphino-
thioylidynetris-
52-24-4
Tris(2,3-dibromopropyl)
phosphate
1-Propanol, 2,3-dibromo-,
phosphate (3:1)
126-72-7
U235
Trypan blue
2,7-Naphthalenedisulfonic acid,
3,3'-[(3,3'-dimethyl[1,1'-
biphenyl]-4,4'-diyl)-
bis(azo)]bis[5-amino-4-
hydroxy]-, tetrasodium salt
72-57-1
U236
Uracil mustard
2,4-(1H,3H)-Pyrimidinedione,
5-[bis(2-chloroethyl)amino]-
66-75-1
U237
Vanadium pentoxide
Vanadium oxide V2O5
1314-62-1
P120
Vernolate
Carbamothioc acid, dipropyl-,
S-propyl ester
1929-77-7
Vinyl chloride
Ethene, chloro-
75-01-4
U043
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl-
butyl)-, when present at
concentrations less than 0.3
percent
81-81-2
U248
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl-
butyl)-, when present at
concentrations greater than 0.3
percent
81-81-2
P001
Warfarin salts, when present at
concentrations less than 0.3
percent
U248
162
Warfarin salts, when present at
concentrations greater than 0.3
percent
P001
Zinc cyanide
Zinc cyanide Zn(CN)2
557-21-1
P121
Zinc phosphide
Zinc phosphide P2Zn3, when
present at concentrations
greater than 10 percent
1314-84-7
P122
Zinc phosphide
Zinc phosphide P2Zn3, when
present at concentrations of 10
percent or less
1314-84-7
U249
Ziram
Zinc, bis(dimethylcarbamo-
dithioato-S,S’)- (T-4)-
137-30-4
P205
Note: The abbreviation N.O.S. (not otherwise specified) signifies those members of the
general class not specifically listed by name in this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.Appendix Z
Table to Section 721.102
Table
*1
*2
*3
*4
Use
constituting
disposal
Burning for
energy
recovery or
use to produce
a fuel
Reclamation
(except as
provided in
Section
721.104-
(a)(15) for
mineral
processing
secondary
materials)
Speculative
accumulation
Applicable Subsection of
Section 721.102:
(c)(1)
(c)(2)
(c)(3)
(c)(4)
Spent materials
Yes
Yes
Yes
Yes
Sludges (listed in
Section 721.131 or
721.132)
Yes
Yes
Yes
Yes
Sludges exhibiting a
characteristic of
hazardous waste
Yes
Yes
No
--
Yes
163
By-products (listed in
Section 721.131 or
721.132)
Yes
Yes
Yes
Yes
By-products exhibiting a
characteristic of
hazardous waste
Yes
Yes
No
--
Yes
Commercial chemical
products listed in
Section 721.133
Yes
Yes
No
--
No
--
Scrap metal other than
excluded scrap metal
(see Section 721.101-
(c)(9))
Yes
Yes
Yes
Yes
Yes - Defined as a solid waste
No - Not defined as a solid waste
*1 - Use constituting disposal (Section 721.102(c)(1))
*2 - Burning for energy recovery or use to produce a fuel (Section 721.102(c)(2))
*3 - Reclamation (Section 721.102(c)(3))
*4 - Speculative accumulation (Section 721.102(c)(4))
BOARD NOTE: Derived from Table 1 to 40 CFR 261.2(c)(4) (1997), as amended at 63 Fed.
Reg. 28636 (May 26, 1998). The terms “spent materials”, “sludges”, “by-products”, “scrap
metal”, and “processed scrap metal” are defined in Section 721.101.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 724
STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS
WASTE TREATMENT, STORAGE, AND DISPOSAL FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
724.101
Purpose, Scope and Applicability
724.103
Relationship to Interim Status Standards
164
SUBPART B: GENERAL FACILITY STANDARDS
Section
724.110
Applicability
724.111
Identification Number
724.112
Required Notices
724.113
General Waste Analysis
724.114
Security
724.115
General Inspection Requirements
724.116
Personnel Training
724.117
General Requirements for Ignitable, Reactive or Incompatible Wastes
724.118
Location Standards
724.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
724.130
Applicability
724.131
Design and Operation of Facility
724.132
Required Equipment
724.133
Testing and Maintenance of Equipment
724.134
Access to Communications or Alarm System
724.135
Required Aisle Space
724.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
724.150
Applicability
724.151
Purpose and Implementation of Contingency Plan
724.152
Content of Contingency Plan
724.153
Copies of Contingency Plan
724.154
Amendment of Contingency Plan
724.155
Emergency Coordinator
724.156
Emergency Procedures
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND
REPORTING
Section
724.170
Applicability
724.171
Use of Manifest System
724.172
Manifest Discrepancies
724.173
Operating Record
724.174
Availability, Retention and Disposition of Records
724.175
Annual Report
724.176
Unmanifested Waste Report
724.177
Additional Reports
165
SUBPART F: RELEASES FROM SOLID WASTE MANAGEMENT UNITS
Section
724.190
Applicability
724.191
Required Programs
724.192
Groundwater Protection Standard
724.193
Hazardous Constituents
724.194
Concentration Limits
724.195
Point of Compliance
724.196
Compliance Period
724.197
General Groundwater Monitoring Requirements
724.198
Detection Monitoring Program
724.199
Compliance Monitoring Program
724.200
Corrective Action Program
724.201
Corrective Action for Solid Waste Management Units
SUBPART G: CLOSURE AND POST-CLOSURE
Section
724.210
Applicability
724.211
Closure Performance Standard
724.212
Closure Plan; Amendment of Plan
724.213
Closure; Time Allowed For Closure
724.214
Disposal or Decontamination of Equipment, Structures and Soils
724.215
Certification of Closure
724.216
Survey Plat
724.217
Post-closure Care and Use of Property
724.218
Post-closure Plan; Amendment of Plan
724.219
Post-closure Notices
724.220
Certification of Completion of Post-closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
724.240
Applicability
724.241
Definitions of Terms As Used In This Subpart
724.242
Cost Estimate for Closure
724.243
Financial Assurance for Closure
724.244
Cost Estimate for Post-closure Care
724.245
Financial Assurance for Post-closure Care
724.246
Use of a Mechanism for Financial Assurance of Both Closure and Post-closure
Care
724.247
Liability Requirements
724.248
Incapacity of Owners or Operators, Guarantors or Financial Institutions
724.251
Wording of the Instruments
166
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
724.270
Applicability
724.271
Condition of Containers
724.272
Compatibility of Waste With Container
724.273
Management of Containers
724.274
Inspections
724.275
Containment
724.276
Special Requirements for Ignitable or Reactive Waste
724.277
Special Requirements for Incompatible Wastes
724.278
Closure
724.279
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
724.290
Applicability
724.291
Assessment of Existing Tank System’s Integrity
724.292
Design and Installation of New Tank Systems or Components
724.293
Containment and Detection of Releases
724.294
General Operating Requirements
724.295
Inspections
724.296
Response to Leaks or Spills and Disposition of Leaking or unfit-for-use Tank
Systems
724.297
Closure and Post-Closure Care
724.298
Special Requirements for Ignitable or Reactive Waste
724.299
Special Requirements for Incompatible Wastes
724.300
Air Emission Standards
SUBPART K: SURFACE IMPOUNDMENTS
Section
724.320
Applicability
724.321
Design and Operating Requirements
724.322
Action Leakage Rate
724.323
Response Actions
724.326
Monitoring and Inspection
724.327
Emergency Repairs; Contingency Plans
724.328
Closure and Post-closure Care
724.329
Special Requirements for Ignitable or Reactive Waste
724.330
Special Requirements for Incompatible Wastes
724.331
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
724.332
Air Emission Standards
167
SUBPART L: WASTE PILES
Section
724.350
Applicability
724.351
Design and Operating Requirements
724.352
Action Leakage Rate
724.353
Response Action Plan
724.354
Monitoring and Inspection
724.356
Special Requirements for Ignitable or Reactive Waste
724.357
Special Requirements for Incompatible Wastes
724.358
Closure and Post-closure Care
724.359
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
SUBPART M: LAND TREATMENT
Section
724.370
Applicability
724.371
Treatment Program
724.372
Treatment Demonstration
724.373
Design and Operating Requirements
724.376
Food-chain Crops
724.378
Unsaturated Zone Monitoring
724.379
Recordkeeping
724.380
Closure and Post-closure Care
724.381
Special Requirements for Ignitable or Reactive Waste
724.382
Special Requirements for Incompatible Wastes
724.383
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
SUBPART N: LANDFILLS
Section
724.400
Applicability
724.401
Design and Operating Requirements
724.402
Action Leakage Rate
724.403
Monitoring and Inspection
724.404
Response Actions
724.409
Surveying and Recordkeeping
724.410
Closure and Post-closure Care
724.412
Special Requirements for Ignitable or Reactive Waste
724.413
Special Requirements for Incompatible Wastes
724.414
Special Requirements for Bulk and Containerized Liquids
724.415
Special Requirements for Containers
724.416
Disposal of Small Containers of Hazardous Waste in Overpacked Drums (Lab
Packs)
724.417
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
168
SUBPART O: INCINERATORS
Section
724.440
Applicability
724.441
Waste Analysis
724.442
Principal Organic Hazardous Constituents (POHCs)
724.443
Performance Standards
724.444
Hazardous Waste Incinerator Permits
724.445
Operating Requirements
724.447
Monitoring and Inspections
724.451
Closure
SUBPART S: CORRECTIVE ACTION FOR SOLID WASTE
MANAGEMENT UNITS
Section
724.652
Corrective Action Management Units
724.653
Temporary Units
SUBPART W: DRIP PADS
Section
724.670
Applicability
724.671
Assessment of existing drip pad integrity
724.672
Design and installation of new drip pads
724.673
Design and operating requirements
724.674
Inspections
724.675
Closure
SUBPART X: MISCELLANEOUS UNITS
Section
724.700
Applicability
724.701
Environmental Performance Standards
724.702
Monitoring, Analysis, Inspection, Response, Reporting and Corrective Action
724.703
Post-closure Care
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
724.930
Applicability
724.931
Definitions
724.932
Standards: Process Vents
724.933
Standards: Closed-Vent Systems and Control Devices
724.934
Test Methods and Procedures
724.935
Recordkeeping requirements
724.936
Reporting Requirements
169
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
724.950
Applicability
724.951
Definitions
724.952
Standards: Pumps in Light Liquid Service
724.953
Standards: Compressors
724.954
Standards: Pressure Relief Devices in Gas/Vapor Service
724.955
Standards: Sampling Connecting Systems
724.956
Standards: Open-ended Valves or Lines
724.957
Standards: Valves in Gas/Vapor or Light Liquid Service
724.958
Standards: Pumps, Valves, Pressure Relief Devices and Other Connectors
724.959
Standards: Delay of Repair
724.960
Standards: Closed-vent Systems and Control Devices
724.961
Alternative Percentage Standard for Valves
724.962
Skip Period Alternative for Valves
724.963
Test Methods and Procedures
724.964
Recordkeeping Requirements
724.965
Reporting Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section
724.980
Applicability
724.981
Definitions
724.982
Standards: General
724.983
Waste Determination Procedures
724.984
Standards: Tanks
724.985
Standards: Surface Impoundments
724.986
Standards: Containers
724.987
Standards: Closed-vent Systems and Control Devices
724.988
Inspection and Monitoring Requirements
724.989
Recordkeeping Requirements
724.990
Reporting Requirements
724.991
Alternative Control Requirements for Tanks
SUBPART DD: CONTAINMENT BUILDINGS
Section
724.1100
Applicability
724.1101
Design and operating standards
724.1102
Closure and Post-closure Care
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section
724.1200
Applicability
170
724.1201
Design and Operating Standards
724.1202
Closure and Post-Closure Care
724.Appendix A
Recordkeeping Instructions
724.Appendix B
EPA Report Form and Instructions (Repealed)
724.Appendix D
Cochran’s Approximation to the Behrens-Fisher Student’s T-Test
724.Appendix E
Examples of Potentially Incompatible Waste
724.Appendix I
Groundwater Monitoring List
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14059, effective October 12, 1983;
amended in R84-9 at 9 Ill. Reg. 11964, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg.
1136, effective January 2, 1986; amended in R86-1 at 10 Ill. Reg. 14119, effective August 12, 1986;
amended in R86-28 at 11 Ill. Reg. 6138, effective March 24, 1987; amended in R86-28 at 11 Ill. Reg.
8684, effective April 21, 1987; amended in R86-46 at 11 Ill. Reg. 13577, effective August 4, 1987;
amended in R87-5 at 11 Ill. Reg. 19397, effective November 12, 1987; amended in R87-39 at 12 Ill.
Reg. 13135, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 458, effective December 28,
1988; amended in R89-1 at 13 Ill. Reg. 18527, effective November 13, 1989; amended in R90-2 at
14 Ill. Reg. 14511, effective August 22, 1990; amended in R90-10 at 14 Ill. Reg. 16658, effective
September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9654, effective June 17, 1991; amended in
R91-1 at 15 Ill. Reg. 14572, effective October 1, 1991; amended in R91-13 at 16 Ill. Reg. 9833,
effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17702, effective November 6, 1992;
amended in R92-10 at 17 Ill. Reg. 5806, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg.
20830, effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6973, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12487, effective July 29, 1994; amended in R94-17 at 18 Ill.
Reg. 17601, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9951, effective June 27,
1995; amended in R95-20 at 20 Ill. Reg. 11244, August 1, 1996; amended in R96-10/R97-3/R97-5 at
22 Ill. Reg. 636, effective December 16, 1997; amended in R98-12 at 22 Ill. Reg. 7638, effective
April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg. 17972, effective September 28, 1998;
amended in R98-21/R99-2/R99-7 at 22 Ill. Reg. ________, effective ______________________.
SUBPART B: GENERAL FACILITY STANDARDS
Section 724.115
General Inspection Requirements
a)
The owner or operator shall conduct inspections often enough to identify
problems in time to correct them before they harm human health or the
environment. The owner or operator shall inspect the facility for malfunctions
and deterioration, operator errors, and discharges that may be causing or may
lead to:
1)
Release of hazardous waste constituents to the environment; or
2)
A threat to human health.
171
b)
Inspection schedule.
1)
The owner or operator shall develop and follow a written schedule for
inspecting monitoring equipment, safety and emergency equipment,
security devices, and operating and structural equipment (such as dikes
and sump pumps) that are important to preventing, detecting, or
responding to environmental or human health hazards.
2)
The owner or operator shall keep this schedule at the facility.
3)
The schedule must identify the types of problems (e.g., malfunctions or
deterioration) that are to be looked for during the inspection (e.g.,
inoperative sump pump, leaking fitting, eroding dike, etc.).
4)
The frequency of inspection may vary for the items on the schedule.
However, it the frequency should be based on the rate of deterioration of
the equipment and the probability of an environmental or human health
incident if the deterioration, malfunction, or any operator error goes
undetected between inspections. Areas subject to spills, such as loading
and unloading areas, must be inspected daily when in use. At a
minimum, the inspection schedule must include the items and
frequencies called for in Sections 724.274, 724.293, 724.295, 724.326,
724.354, 724.378, 724.403, 724.447, 724.702, 724.933, 724.952,
724.953, 724.958, 724.988, and 724.991(b) 724.983 through 724.990,
where applicable.
BOARD NOTE: 35 Ill. Adm. Code 703 requires the inspection schedule
to be submitted with Part B of the permit application. The Agency must
evaluate the schedule along with the rest of the application to ensure that
it adequately protects human health and the environment. As part of this
review, the Agency may modify or amend the schedule as may be
necessary.
c)
The owner or operator shall remedy any deterioration or malfunction of
equipment or structures that the inspection reveals on a schedule which ensures
that the problem does not lead to an environmental or human health hazard.
Where a hazard is imminent or has already occurred, remedial action must be
taken immediately.
d)
The owner or operator shall record inspections in an inspection log or
summary. The owner or operator shall keep these records for at least three
years from the date of inspection. At a minimum, these records must include
the date and time of the inspection, the name of the inspector, a notation of the
observations made and the date, and nature of any repairs or other remedial
actions.
172
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 724.173
Operating Record
a)
The owner or operator shall keep a written operating record at the facility.
b)
The following information must be recorded as it becomes available and
maintained in the operating record until closure of the facility:
1)
A description and the quantity of each hazardous waste received and the
method or methods and date or dates of its treatment, storage, or
disposal at the facility, as required by Section 724.Appendix A of this
Part;
2)
The location of each hazardous waste within the facility and the quantity
at each location. For disposal facilities, the location and quantity of each
hazardous waste must be recorded on a map or diagram of each cell or
disposal area. For all facilities, this information must include cross-
references to specific manifest document numbers, if the waste was
accompanied by a manifest;
BOARD NOTE: See Section 724.219 for related requirements.
3)
Records and results of waste analyses and waste determinations
performed as specified in Sections 724.113, 724.117, 724.414, 724.441,
724.934, 724.963, and 724.983 and in 35 Ill. Adm. Code 728.104(a)
and 728.107;
4)
Summary reports and details of all incidents that require implementing
the contingency plan, as specified in Section 724.156(j);
5)
Records and results of inspections, as required by Section 724.115(d)
(except these data need to be kept only three years);
6)
Monitoring, testing, or analytical data and corrective action data where
required by 724.Subpart F of this Part or Sections 724.119, 724.291,
724.293, 724.295, 724.322, 724.323, 724.326, 724.352 through
724.354, 724.376, 724.378, 724.380, 724.402 through 724.404,
724.409, 724.447, 724.702, 724.934(c) through (f), 724.935,
724.963(d) through (i), 724.964, 724.988, 724.989, and 724.991
724.982 through 724.990;
173
7)
For off-site facilities, notices to generators as specified in Section
724.112(b);
8)
All closure cost estimates under Section 724.242 and, for disposal
facilities, all post-closure cost estimates under Section 724.244;
9)
A certification by the permittee, no less often than annually: that the
permittee has a program in place to reduce the volume and toxicity of
hazardous waste that the permittee generates, to the degree the permittee
determines to be economically practicable, and that the proposed method
of treatment, storage, or disposal is that practicable method currently
available to the permittee that minimizes the present and future threat to
human health and the environment;
10)
Records of the quantities (and date of placement) for each shipment of
hazardous waste placed in land disposal units under an extension of the
effective date of any land disposal restriction granted pursuant to 35 Ill.
Adm. Code 728.105, a petition pursuant to 35 Ill. Adm. Code 728.106
or a certification under 35 Ill. Adm. Code 728.108, and the applicable
notice required of a generator under 35 Ill. Adm. Code 728.107(a);
11)
For an off-site treatment facility, a copy of the notice, and the
certification and demonstration, if applicable, required of the generator
or the owner or operator under 35 Ill. Adm. Code 728.107 or 728.108;
12)
For an on-site treatment facility, the information contained in the notice
(except the manifest number), and the certification and demonstration, if
applicable, required of the generator or the owner or operator under 35
Ill. Adm. Code 728.107 or 728.108;
13)
For an off-site land disposal facility, a copy of the notice, and the
certification and demonstration, if applicable, required of the generator
or the owner or operator of a treatment facility under 35 Ill. Adm. Code
728.107 or 728.108, whichever is applicable; and
14)
For an on-site land disposal facility, the information contained in the
notice required of the generator or owner or operator of a treatment
facility under 35 Ill. Adm. Code 728.107, except for the manifest
number, and the certification and demonstration, required under 35 Ill.
Adm. Code 728.108, whichever is applicable.;
15)
For an off-site storage facility, a copy of the notice, and the certification
and demonstration if applicable, required of the generator or the owner
or operator under 35 Ill. Adm. Code 728.107 or 728.108; and
174
16)
For an on-site storage facility, the information contained in the notice
(except the manifest number), and the certification and demonstration if
applicable, required of the generator or the owner or operator under 35
Ill. Adm. Code 728.107 or 728.108.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 724.930
Applicability
a)
This Subpart applies to owners and operators of facilities that treat, store or
dispose of hazardous wastes (except as provided in Section 724.101).
b)
Except for Sections 724.934(d) and (e), this Subpart applies to process vents
associated with distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operations that manage hazardous wastes
with organic concentrations of at least 10 ppmw (parts per million by weight), if
these operations are conducted in:
1)
Units that are subject to the permitting requirements of 35 Ill. Adm.
Code 703;
2)
A unit (including a hazardous waste recycling unit) that is not exempt
from permitting under the provisions of 35 Ill. Adm. Code 722.134(a)
(i.e., a hazardous waste recycling unit that is not a 90-day tank or
container) and that is located at a hazardous waste management facility
otherwise subject to the permitting requirements of 35 Ill. Adm. Code
703; or
3)
A unit that is exempt from permitting under the provisions of 35 Ill.
Adm. Code 722.134(a) (i.e., a 90-day tank or container) and which is not
a recycling unit under the provisions of 35 Ill. Adm. Code 721.106.
c)
If the owner or operator of process vents subject to the requirements of Sections
724.932 through 724.936 has received a RCRA permit prior to December 21,
1990, the requirements of Sections 724.932 through 724.936 must be
incorporated when the permit is reissued under 35 Ill. Adm. Code 705.201 or
reviewed under 35 Ill. Adm. Code 702.161.
c)
For the owner and operator of a facility subject to this Subpart that received a final
permit under 35 Ill. Adm. Code 702, 703, and 705 prior to December 6, 1996, the
requirements of this Subpart shall be incorporated into the permit when the permit is
reissued, renewed, or modified in accordance with the requirements of 35 Ill.
175
Adm. Code 703 and 705. Until such date when the owner and operator receives a
final permit incorporating the requirements of this subpart, the owner and operator is
subject to the requirements of 35 Ill. Adm. Code 725.Subpart AA.
BOARD NOTE: The requirements of Sections 724.932 through 724.936 apply
to process vents on hazardous waste recycling units previously exempt under 35
Ill. Adm. Code 721.106(c)(1). Other exemptions under 35 Ill. Adm. Code
721.104, 722.134 and 724.101(g) are not affected by these requirements.
d)
This subsection (d) corresponds with 40 CFR 264.1030(d), which is marked
“reserved” by USEPA. This statement maintains structural consistency with
USEPA rules.
e)
The requirements of this Subpart do not apply to the process vents at a facility where
the facility owner or operator certifies that all of the process vents which would
otherwise be subject to this Subpart are equipped with and operating air emission
controls in accordance with the process vent requirements of an applicable federal
Clean Air Act regulation codified under 40 CFR 60, 61, or 63. The documentation of
compliance under regulations at 40 CFR 60, 61, or 63 must be kept with, or made
readily available with, the facility operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.931
Definitions
As used in this Subpart, all terms not defined in the Subpart have the meaning given them in
the Resource Conservation and Recovery Act and 35 Ill. Adm. Code 720 through 726.
“Air stripping operation” is a desorption operation employed to transfer one or
more volatile components from a liquid mixture into a gas (air) either with or
without the application of heat to the liquid. Packed towers, spray towers and
bubble-cap, sieve, or valve-type plate towers are among the process
configurations used for contacting the air and a liquid.
“Bottoms receiver” means a container or tank used to receive and collect the
heavier bottoms fractions of the distillation feed stream that remain in the liquid
phase.
BTU “Btu” means British thermal unit.
“Closed-vent system” means a system that is not open to the atmosphere and
that is composed of piping, connections, and, if necessary, flow-inducing
devices that transport gas or vapor from a piece or pieces of equipment to a
control device.
“Condenser” means a heat-transfer device that reduces a thermodynamic fluid
from its vapor phase to its liquid phase.
176
“Connector” means flanged, screwed, welded or other joined fittings used to
connect two pipelines or a pipeline and a piece of equipment. For the purposes
of reporting and recordkeeping, “connector” means flanged fittings that are not
covered by insulation or other materials that prevent location of the fittings.
“Continuous recorder” means a data-recording device recording an
instantaneous data value at least once every 15 minutes.
“Control device” means an enclosed combustion device, vapor recovery system,
or flare. Any device the primary function of which is the recovery or capture
of solvents or other organics for use, reuse, or sale (e.g., a primary condenser
on a solvent recovery unit) is not a control device.
“Control device shutdown” means the cessation of operation of a control device
for any purpose.
“Distillate receiver” means a container or tank used to receive and collect liquid
material (condensed) from the overhead condenser of a distillation unit and from
which the condensed liquid is pumped to larger storage tanks or other process
units.
“Distillation operation” means an operation, either batch or continuous,
separating one or more feed stream(s) into two or more exit streams, each exit
stream having component concentrations different from those in the feed
stream(s). The separation is achieved by the redistribution of the components
between the liquid and vapor phase as they approach equilibrium within the
distillation unit.
“Double block and bleed system” means two block valves connected in series
with a bleed valve or line that can vent the line between the two block valves.
“Equipment” means each valve, pump, compressor, pressure relief device,
sampling connection system, open-ended valve or line, or flange, and any
control devices or systems required by this Subpart.
“First attempt at repair” means to take rapid action for the purpose of stopping
or reducing leakage of organic material to the atmosphere using best practices.
“Flame zone” means the portion of the combustion chamber in a boiler
occupied by the flame envelope.
“Flow indicator” means a device that indicates whether gas flow is present in a
vent stream.
177
First attempt at repair means to take rapid action for the purpose of stopping or
reducing leakage of organic material to the atmosphere using best practices.
“Fractionation operation” means a distillation operation or method used to
separate a mixture of several volatile components of different boiling points in
successive stages, each stage removing from the mixture some proportion of one
of the components.
“ft” means foot.
“h” means hour.
“Hazardous waste management unit shutdown” means a work practice or
operational procedure that stops operation of a hazardous waste management
unit or part of a hazardous waste management unit. An unscheduled work
practice or operational procedure that stops operation of a hazardous waste
management unit or part of a hazardous waste management unit for less than 24
hours is not a hazardous waste management unit shutdown. The use of spare
equipment and technically feasible bypassing of equipment without stopping
operation are not hazardous waste management unit shutdowns.
“Hot well” means a container for collecting condensate as in a steam condenser
serving a vacuum-jet or steam-jet ejector.
“In gas-vapor service” means that the piece of equipment contains or contacts a
hazardous waste stream that is in the gaseous state at operating conditions.
“In heavy liquid service” means that the piece of equipment is not in gas-vapor
service or in light liquid service.
“In light liquid service” means that the piece of equipment contains or contacts
a waste stream where the vapor pressure of one or more of the organic
components in the stream is greater than 0.3 kilopascals (kPa) at 20° C, the
total concentration of the pure organic components having a vapor pressure
greater than 0.3 kPa at 20° C is equal to or greater than 20 percent by weight,
and the fluid is a liquid at operating conditions.
“In situ sampling systems” means nonextractive samplers or in-line samplers.
“In vacuum service” means that equipment is operating at an internal pressure
that is at least 5 kPa below ambient pressure.
“Kg” means kilogram.
“kPa” means kilopascals.
178
“lb” means pound.
“m” means meter.
“Mg” means Megagrams, or metric tonnes.
“MJ” means Megajoules, or ten to the sixth Joules.
“MW” means Megawatts.
“Malfunction” means any sudden failure of a control device or a hazardous
waste management unit or failure of a hazardous waste management unit to
operate in a normal or usual manner, so that organic emissions are increased.
“Open-ended valve or line” means any valve, except pressure relief valves,
having one side of the valve seat in contact with process fluid and one side open
to the atmosphere, either directly or through open piping.
“ppmv” means parts per million by volume.
“ppmw” meant means parts per million by weight.
“Pressure release” means the emission of materials resulting from the system
pressure being greater than the set pressure of the pressure relief device.
“Process heater” means a device that transfers heat liberated by burning fuel to
fluids contained in tubes, including all fluids except water that are heated to
produce steam.
“Process vent” means any open-ended pipe or stack that is vented to the
atmosphere either directly, through a vacuum-producing system, or through a
tank (e.g., distillate receiver, condenser, bottoms receiver, surge control tank,
separator tank, or hot well) associated with hazardous waste distillation,
fractionation, thin-film evaporation, solvent extraction, or air or steam stripping
operations.
“Repaired” means that equipment is adjusted, or otherwise altered, to eliminate
a leak.
“s” means second.
“scm” means standard cubic meter.
“scft” meant means standard cubic foot.
179
“Sensor” means a device that measures a physical quantity or the change in a
physical quantity, such as temperature, pressure, flow rate, pH, or liquid level.
“Separator tank” means a device used for separation of two immiscible liquids.
“Solvent extraction operation” means an operation or method of separation in
which a solid or solution is contracted with a liquid solvent (the two being
mutually insoluble) to preferentially dissolve and transfer one or more
components into the solvent.
“Startup” means the setting in operation of a hazardous waste management unit
or control device for any purpose.
“Steam stripping operation” means a distillation operation in which vaporization
of the volatile constituents of a liquid mixture takes place by the introduction of
steam directly in to the charge.
“Surge control tank” means a large-sized pipe or storage reservoir sufficient to
contain the surging liquid discharge of the process tank to which it is connected.
“Thin-film evaporation operation” means a distillation operation that employs a
heating surface consisting of a large diameter tube that may be either straight or
tapered, horizontal or vertical. Liquid is spread on the tube wall by a rotating
assembly of blades that maintain a close clearance from the wall or actually ride
on the film of liquid on the wall.
“Vapor incinerator” means any enclosed combustion device that is used for
destroying organic compounds and does not extract energy in the form of steam
or process heat.
“Vented” means discharged through an opening, typically an open-ended pipe
or stack, allowing the passage of a stream of liquids, gases, or fumes into the
atmosphere. The passage of liquids, gases, or fumes is caused by mechanical
means such as compressors or vacuum-producing systems or by process-related
means such as evaporation produced by heating and not caused by tank loading
and unloading (working losses) or by natural means such as diurnal temperature
changes.
“yr” means year.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
180
Section 724.933
Standards: Closed-Vent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control devices used to
comply with provisions of this Part shall comply with the provisions of
this Section.
2)
Implementation Schedule.
A)
The owner or operator of an existing facility that cannot install a
closed-vent system and control device to comply with the
provisions of this Subpart on the effective date that the facility
becomes subject to the provisions of this Subpart shall prepare an
implementation schedule that includes dates by which the closed-
vent system and control device will be installed and in operation.
The controls must be installed as soon as possible, but the
implementation schedule may allow up to 30 months after the
effective date that the facility becomes subject to this Subpart for
installation and startup.
B)
All units Any unit that begin begins operation after December 21,
1990, and which is subject to the provisions of this Subpart when
operation begins, must comply with the rules immediately (i.e.,
must have control devices installed and operating on startup of
the affected unit); the 2-year 30-month implementation schedule
does not apply to these units.
C)
The owner or operator of any facility in existence on the effective date
of a statutory or regulatory amendment that renders the facility
subject to this Subpart shall comply with all requirements of this
subpart as soon as practicable but no later than 30 months after the
effective date of the amendment. When control equipment required
by this Subpart can not be installed and begin operation by the
effective date of the amendment, the facility owner or operator shall
prepare an implementation schedule that includes the following
information: Specific calendar dates for award of contracts or
issuance of purchase orders for the control equipment, initiation of
on-site installation of the control equipment, completion of the control
equipment installation, and performance of any testing to
demonstrate that the installed equipment meets the applicable
standards of this Subpart. The owner or operator shall enter the
implementation schedule in the operating record or in a permanent,
readily available file located at the facility.
D)
An owner or operator of a facility or unit that becomes newly subject
to the requirements of this Subpart after December 8, 1997 due to an
action other than those described in subsection (a)(2)(C) of this
181
Section must comply with all applicable requirements immediately
(i.e., the facility or unit must have control devices installed and
operating on the date the facility or unit becomes subject to this
Subpart; the 30-month implementation schedule does not apply).
b)
A control device involving vapor recovery (e.g., a condenser or adsorber) must
be designed and operated to recover the organic vapors vented to it with an
efficiency of 95 weight percent or greater unless the total organic emission
limits of Section 724.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler, or process
heater) must be designed and operated to reduce the organic emissions vented to
it by 95 weight percent or greater; to achieve a total organic compound
concentration of 20 ppmv, expressed as the sum of the actual compounds and
not in carbon equivalents, on a dry basis, corrected to three percent oxygen; or
to provide a minimum residence time of 0.50 seconds at a minimum
temperature of 760 degrees Celsius (° C). If a boiler or process heater is used
as the control device, then the vent stream must be introduced into the flame
zone of the boiler or process heater.
d)
Flares:
1)
A flare must be designed for and operated with no visible emissions, as
determined by the methods specified in subsection (e)(1), except for
periods not to exceed a total of 5 minutes during any 2 consecutive
hours.
2)
A flare must be operated with a flame present at all times, as determined
by the methods specified in subsection (f)(2)(C) of this Section.
3)
A flare must be used only if the net heating value of the gas being
combusted is 11.2 MJ/scm (300 Btu/scf) or greater and the flare is
steam-assisted or air-assisted or if the net heating value of the gas being
combusted is 7.45 MJ/scm (200 Btu/scf) or greater and the flare is
nonassisted. The net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2) of this Section.
4)
Exit Velocity.
A)
A steam-assisted or nonassisted flare must be designed for and
operated with an exit velocity, as determined by the methods
specified in subsection (e)(3) of this Section, less than 18.3 m/s
(60 ft/s), except as provided in subsections (d)(4)(B) and
(d)(4)(C) of this Section.
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B)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, equal to or greater than 18.3
m/s (60 ft/s) but less than 122 m/s (400 ft/s) is allowed if the net
heating value of the gas being combusted is greater than 37.3
MJ/scm (1000 Btu/scf).
C)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, less than the velocity, V, as
determined by the method specified in subsection (e)(4) of this
Section and less than 122 m/s (400 ft/s) is allowed.
5)
An air-assisted flare must be designed and operated with an exit velocity
less than the velocity, V, as determined by the method specified in
subsection (e)(5) of this Section.
6)
A flare used to comply with this Section must be steam-assisted, air-
assisted, or nonassisted.
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be used to determine the compliance of a
flare with the visible emission provisions of this Subpart. The
observation period is 2 hours and must be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare must be
calculated using the following equation:
H
T
=K
i
i
i1
n
×
CH
=
∑×
Where:
HT is the net heating value of the sample in MJ/scm; where the
net enthalpy per mole of offgas is based on combustion at 25° C
and 760 mm Hg, but the standard temperature for determining
the volume corresponding to 1 mole is 20° C.
K = 1.74
×
10
7
(1/ppm)(g mol/scm)(MJ/kcal) where standard
temperature for (g mol/scm) 20° C.
183
Σ(Xi)
means the sum of the values of X for each component i,
from i=1 to n.
Ci is the concentration of sample component i in ppm on a wet
basis, as measured for organics by Reference Method 18 in 40
CFR 60, and for carbon monoxide, by ASTM D 1946-90,
incorporated by reference in 35 Ill. Adm. Code 720.111.
Hi is the net heat of combustion of sample component i,
kcal/gmol at 25° C and 760 mm Hg. The heats of combustion
must be determined using ASTM D 2382, incorporated by
reference in 35 Ill. Adm. Code 720.111, if published values are
not available or cannot be calculated.
3)
The actual exit velocity of a flare must be determined by dividing the
volumetric flow rate (in units of standard temperature and pressure), as
determined by Reference Methods 2, 2A, 2C, or 2D in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111, as appropriate,
by the unobstructed (free) cross-sectional area of the flare tip.
4)
The maximum allowed velocity in m/s, Vmax, for a flare complying with
subsection (d)(4)(C) must be determined by the following equation:
log
(
V
)
H
28.8
10
max
31.7
T
=
+
Where:
log10 means logarithm to the base 10
HT is the net heating value as determined in subsection (e)(2).
5)
The maximum allowed velocity in m/s, Vmax, for an air-assisted flare
must be determined by the following equation:
V
max
=
8.706
+
0.7084H
T
Where:
HT is the net heating value as determined in subsection (e)(2) of
this Section.
f)
The owner or operator shall monitor and inspect each control device required to
comply with this Section to ensure proper operation and maintenance of the
control device by implementing the following requirements:
184
1)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a flow indicator that provides a record of stream flow from
each affected process vent to the control device at least once every hour.
The flow indicator sensor must be installed in the vent stream at the
nearest feasible point to the control device inlet but before the point at
which the vent streams are combined.
2)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a device to continuously monitor control device operation
as specified below:
A)
For a thermal vapor incinerator, a temperature monitoring device
equipped with a continuous recorder. The device must have
accuracy of ±1 percent of the temperature being monitored in °
C or ±0.5° C, whichever is greater. The temperature sensor
must be installed at a location in the combustion chamber
downstream of the combustion zone.
B)
For a catalytic vapor incinerator, a temperature monitoring
device equipped with a continuous recorder. The device must be
capable of monitoring temperature at two locations and have an
accuracy of ±1 percent of the temperature being monitored in °
C or ±0.5° C, whichever is greater. One temperature sensor
must be installed in the vent stream at the nearest feasible point to
the catalyst bed inlet and a second temperature sensor must be
installed in the vent stream at the nearest feasible point to the
catalyst bed outlet.
C)
For a flare, a heat sensing monitoring device equipped with a
continuous recorder that indicates the continuous ignition of the
pilot flame.
D)
For a boiler or process heater having a design heat input capacity
less than 44 MW, a temperature monitoring device equipped with
a continuous recorder. The device must have an accuracy of ±1
percent of the temperature being monitored in ° C or ±0.5° C,
whichever is greater. The temperature sensor must be installed at
a location in the furnace downstream of the combustion zone.
E)
For a boiler or process heater having a design heat input capacity
greater than or equal to 44 MW, a monitoring device equipped
with a continuous recorder to measure parameters that indicate
good combustion operating practices are being used.
185
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the
condenser; or
ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable of
monitoring temperature with an accuracy of ±1 percent of
the temperature being monitored in ° C or ±0.5° C,
whichever is greater. The temperature sensor must be
installed at a location in the exhaust vent stream from the
condenser exit (i.e., product side).
G)
For a carbon adsorption system that regenerates the carbon bed
directly in the control device such as a fixed-bed carbon
adsorber, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the carbon
bed, or
ii)
A monitoring device equipped with a continuous recorder
to measure a parameter that indicates the carbon bed is
regenerated on a regular, predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsections (f)(1) and (f)(2) at least once each operating day to check
control device operation and, if necessary, immediately implement the
corrective measures necessary to ensure the control device operates in
compliance with the requirements of this Section.
g)
An owner or operator using a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
at a regular, predetermined time interval that is no longer than the carbon
service life established as a requirement of Section 724.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system such as a carbon
canister that does not regenerate the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
on a regular basis by using one of the following procedures:
186
1)
Monitor the concentration level of the organic compounds in the exhaust
vent stream from the carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon immediately when
carbon breakthrough is indicated. The monitoring frequency must be
daily or at an interval no greater than 20 percent of the time required to
consume the total carbon working capacity established as a requirement
of Section 724.935(b)(4)(C)(vii), whichever is longer.
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design carbon
replacement interval established as a requirement of Section
724.935(b)(4)(C)(vii).
i)
An alternative operational or process parameter may be monitored if the
operator demonstrates that the parameter will ensure that the control device is
operated in conformance with these standards and the control device’s design
specifications.
j)
An owner or operator of an affected facility seeking to comply with the
provisions of this Part by using a control device other than a thermal vapor
incinerator, catalytic vapor incinerator, flare, boiler, process heater, condenser,
or carbon adsorption system is required to develop documentation including
sufficient information to describe the control device operation and identify the
process parameter or parameters that indicate proper operation and maintenance
of the control device.
k)
A closed-vent system must meet either of the following design requirements:
1)
A closed-vent system must be designed to operate with no detectable
emissions, as indicated by an instrument reading of less than 500 ppmv
above background, as determined by the methods specified at Section
724.934(b), and by visual inspections; or
2)
A closed-vent system must be designed to operate at a pressure below
atmospheric pressure. The system must be equipped with at least one
pressure gauge or other pressure measurement device that can be read
from a readily accessible location to verify that negative pressure is
being maintained in the closed-vent system when the control device is
operating.
l)
The owner or operator shall monitor and inspect each closed-vent system
required to comply with this Section to ensure proper operation and maintenance
of the closed-vent system by implementing the following requirements:
187
1)
Each closed-vent system that is used to comply with subsection (k)(1) of
this Section shall be inspected and monitored in accordance with the
following requirements:
A)
An initial leak detection monitoring of the closed-vent system
shall be conducted by the owner or operator on or before the date
that the system becomes subject to this Section. The owner or
operator shall monitor the closed-vent system components and
connections using the procedures specified in Section 724.934(b)
to demonstrate that the closed-vent system operates with no
detectable emissions, as indicated by an instrument reading of
less than 500 ppmv above background.
B)
After initial leak detection monitoring required in subsection
(l)(1)(A) of this Section, the owner or operator shall inspect and
monitor the closed-vent system as follows:
i)
Closed-vent system joints, seams, or other connections
that are permanently or semi-permanently sealed (e.g., a
welded joint between two sections of hard piping or a
bolted and gasketed ducting flange) must be visually
inspected at least once per year to check for defects that
could result in air pollutant emissions. The owner or
operator shall monitor a component or connection using
the procedures specified in Section 724.934(b) to
demonstrate that it operates with no detectable emissions
following any time the component is repaired or replaced
(e.g., a section of damaged hard piping is replaced with
new hard piping) or the connection is unsealed (e.g., a
flange is unbolted).
ii)
Closed-vent system components or connections other than
those specified in subsection (l)(1)(B)(i) of this Section
must be monitored annually and at other times as
requested by the Regional Administrator, except as
provided for in subsection (o) of this Section, using the
procedures specified in Section 724.934(b) to demonstrate
that the components or connections operate with no
detectable emissions.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect or leak in accordance with the
requirements of subsection (l)(3) of this Section.
188
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 724.935.
2)
Each closed-vent system that is used to comply with subsection (k)(2) of
this Section must be inspected and monitored in accordance with the
following requirements:
A)
The closed-vent system must be visually inspected by the owner
or operator to check for defects that could result in air pollutant
emissions. Defects include, but are not limited to, visible cracks,
holes, or gaps in ductwork or piping or loose connections.
B)
The owner or operator shall perform an initial inspection of the
closed-vent system on or before the date that the system becomes
subject to this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (l)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 724.935.
3)
The owner or operator shall repair all detected defects as follows:
A)
Detectable emissions, as indicated by visual inspection or by an
instrument reading greater than 500 ppmv above background,
must be controlled as soon as practicable, but not later than 15
calendar days after the emission is detected, except as provided
for in subsection (l)(3)(C) of this Section.
B)
A first attempt at repair must be made no later than five calendar
days after the emission is detected.
C)
Delay of repair of a closed-vent system for which leaks have been
detected is allowed if the repair is technically infeasible without a
process unit shutdown, or if the owner or operator determines
that emissions resulting from immediate repair would be greater
than the fugitive emissions likely to result from delay of repair.
Repair of such equipment must be completed by the end of the
next process unit shutdown.
189
D)
The owner or operator shall maintain a record of the defect repair
in accordance with the requirements specified in Section 724.935.
m)
A closed-vent system or control device used to comply with provisions of this
Subpart must be operated at all times when emissions may be vented to it.
n)
The owner or operator using a carbon adsorption system to control air pollutant
emissions shall document that all carbon removed that is a hazardous waste and
that is removed from the control device is managed in one of the following
manners, regardless of the volatile organic concentration of the carbon:
1)
It is regenerated or reactivated in a thermal treatment unit that meets one
of the following:
A)
The owner or operator of the unit has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 724.Subpart X of this Part; or
B)
The unit is equipped with and operating air emission controls in
accordance with the applicable requirements of 724.Subparts AA
and CC of this Part or 35 Ill. Adm. Code 725.Subparts AA and
CC; or
C)
The unit is equipped with and operating air emission controls in
accordance with a national emission standard for hazardous air
pollutants under 40 CFR 61 or 40 CFR 63.
2)
It is incinerated in a hazardous waste incinerator for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 724.Subpart O of this Part; or
B)
The owner or operator has certified compliance in accordance
with the interim status requirements of 35 Ill. Adm. Code
725.Subpart O.
3)
It is burned in a boiler or industrial furnace for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 726.Subpart H; or
190
B)
The owner or operator has designed and operates the boiler or
industrial furnace in accordance with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
o)
Any components of a closed-vent system that are designated, as described in
Section 724.935(c)(9), as unsafe to monitor are exempt from the requirements
of subsection (l)(1)(B)(ii) of this Section if both of the following conditions are
fulfilled:
1)
The owner or operator of the closed-vent system has determined that the
components of the closed-vent system are unsafe to monitor because
monitoring personnel would be exposed to an immediate danger as a
consequence of complying with subsection (l)(1)(B)(ii) of this Section;
and
2)
The owner or operator of the closed-vent system adheres to a written
plan that requires monitoring the closed-vent system components using
the procedure specified in subsection (l)(1)(B)(ii) as frequently as
practicable during safe-to-monitor times.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 724.950
Applicability
a)
The regulations in this Subpart apply to owners and operators of facilities that
treat, store, or dispose of hazardous wastes (except as provided in Section
724.101).
b)
Except as provided in Section 724.964(k), this Subpart applies to equipment that
contains or contacts hazardous wastes with organic concentrations of at least 10
percent by weight that are managed in one of the following:
1)
A unit that is subject to the RCRA permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705,
2)
A unit (including a hazardous waste recycling unit) that is not exempt
from permitting under the provisions of 35 Ill. Adm. Code 722.134(a)
(i.e., a hazardous waste recycling unit that is not a “90-day” tank or
container) and that is located at a hazardous waste management facility
otherwise subject to the permitting requirements of 35 Ill. Adm. Code
702, 703, and 705, or
191
3)
A unit that is exempt from permitting under the provisions of 35 Ill.
Adm. Code 722.134(a) (i.e., a “90-day” tank or container) and which is
not a recycling unit under the provisions of 35 Ill. Adm. Code 721.106.
c)
If the owner or operator of equipment subject to the requirements of Sections
724.952 through 724.965 has received a RCRA permit prior to December 21,
1990, the requirements of Sections 724.952 through 724.965 must be
incorporated when the permit is reissued under 35 Ill. Adm. Code 705.201 or
reviewed under 35 Ill. Adm. Code 702.161.
c)
For the owner or operator of a facility subject to this Subpart that received a final
permit under 35 Ill. Adm. Code 702, 703, and 705 prior to December 6, 1996, the
requirements of this Subpart shall be incorporated into the permit when the permit is
reissued, renewed, or modified in accordance with the requirements of 35 Ill.
Adm. Code 703 and 705. Until such date when the owner or operator receives a
final permit incorporating the requirements of this Subpart, the owner or operator is
subject to the requirements of 35 Ill. Adm. Code 725.Subpart BB.
d)
Each piece of equipment to which this Subpart applies must be marked in such a
manner that it can be distinguished readily from other pieces of equipment.
e)
Equipment that is in vacuum service is excluded from the requirements of
Sections 724.952 to 724.960, if it is identified as required in Section
724.964(g)(5).
f)
Equipment that contains or contacts hazardous waste with an organic
concentration of at least 10 percent by weight for a period of less than 300
hours per calendar year is excluded from the requirements of Sections 724.952
through 724.960 if it is identified as required in Section 724.964(g)(6).
BOARD NOTE: The requirements of Sections 724.952 through 724.965 apply
to equipment associated with hazardous waste recycling units previously exempt
under 35 Ill. Adm. Code 721.106(c)(1). Other exemptions under 35 Ill. Adm.
Code 721.104 and 724.101(g) are not affected by these requirements.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.960
Standards: Closed-vent Systems and Control Devices
a)
Owners An owner or operators operator of a closed-vent systems and system or
control devices device subject to this Subpart shall comply with the provisions
of Section 724.933.
b)
Implementation Schedule.
1)
The owner or operator of an existing facility that cannot install a closed-vent
system and control device to comply with the provisions of this Subpart on
192
the effective date that the facility becomes subject to the provisions of this
Subpart shall prepare an implementation schedule that includes dates by
which the closed-vent system and control device will be installed and in
operation. The controls must be installed as soon as possible, but the
implementation schedule may allow up to 30 months after the effective date
that the facility becomes subject to this Subpart for installation and startup.
2)
Any unit that begins operation after December 21, 1990, and which is subject
to the provisions of this Subpart when operation begins, must comply with
the rules immediately (i.e., the unit must have control devices installed and
operating on startup of the affected unit); the 30-month implementation
schedule does not apply.
3)
The owner or operator of any facility in existence on the effective date of a
statutory or regulatory amendment that renders the facility subject to this
Subpart shall comply with all requirements of this Subpart as soon as
practicable but no later than 30 months after the effective date of the
amendment. When control equipment required by this Subpart can not be
installed and begin operation by the effective date of the amendment, the
facility owner or operator shall prepare an implementation schedule that
includes the following information: Specific calendar dates for award of
contracts or issuance of purchase orders for the control equipment, initiation
of on-site installation of the control equipment, completion of the control
equipment installation, and performance of any testing to demonstrate that
the installed equipment meets the applicable standards of this Subpart. The
owner or operator shall enter the implementation schedule in the operating
record or in a permanent, readily available file located at the facility.
4)
An owner or operator of a facility or unit that becomes newly subject to the
requirements of this Subpart due to an action other than those described in
subsection (b)(3) of this Section shall comply with all applicable requirements
immediately (i.e., the facility or unit must have control devices installed and
operating on the date the facility or unit becomes subject to this Subpart; the
30-month implementation schedule does not apply).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.962
Skip Period Alternative for Valves
a)
Election
1)
An owner or operator subject to the requirements of Section 724.957
may elect for all valves within a hazardous waste management unit to
comply with one of the alternative work practices specified in
subsections (b)(2) and (3).
2)
An owner or operator shall notify the Agency before implementing one
of the alternative work practices.
b)
Reduced Monitoring
193
1)
An owner or operator shall comply with the requirements for valves, as
described in Section 724.957, except as described in subsection
subsections (b)(2) and (3).
2)
After two consecutive quarterly leak detection periods with the
percentage of valves leaking equal to or less than 2 two percent, an
owner or operator may begin to skip one of the quarterly leak detection
periods (i.e., the owner or operator may monitor for leaks once every six
months) for the valves subject to the requirements in Section 724.957.
3)
After five consecutive quarterly leak detection periods with the
percentage of valves leaking equal to or less than 2 two percent, an
owner or operator may begin to skip three of the quarterly leak detection
periods (i.e., the owner or operator may monitor for leaks once every year)
for the valves subject to the requirements in Section 724.957.
4)
If the percentage of valves leaking is greater than 2 percent, the owner
or operator shall monitor monthly in compliance with the requirements
in Section 724.957, but may again elect to use this Section after meeting
the requirements of Section 724.957(c)(1).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.964
Recordkeeping Requirements
a)
Lumping Units
1)
Each owner or operator subject to the provisions of this Subpart shall
comply with the recordkeeping requirements of this Section.
2)
An owner or operator of more than one hazardous waste management
unit subject to the provisions of this Subpart may comply with the
recordkeeping requirements for these hazardous waste management units
in one recordkeeping system if the system identifies each record by each
hazardous waste management unit.
b)
Owners and operators shall record the following information in the facility
operating record:
1)
For each piece of equipment to which this Subpart applies:
A)
Equipment identification number and hazardous waste
management unit identification.
194
B)
Approximate locations within the facility (e.g., identify the
hazardous waste management unit on a facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total organics in the hazardous wastestream at
the equipment.
E)
Hazardous waste state at the equipment (e.g., gas-vapor or
liquid).
F)
Method of compliance with the standard (e.g., “monthly leak
detection and repair” or “equipped with dual mechanical seals”).
2)
For facilities that comply with the provisions of Section 724.933(a)(2),
an implementation schedule as specified in that Section.
3)
Where an owner or operator chooses to use test data to demonstrate the
organic removal efficiency or total organic compound concentration
achieved by the control device, a performance test plan as specified in
Section 724.935(b)(3).
4)
Documentation of compliance with Section 724.960, including the
detailed design documentation or performance test results specified in
Section 724.935(b)(4).
c)
When each leak is detected as specified in Sections 724.952, 724.953, 724.957
or 724.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked with the
equipment identification number, the date evidence of a potential leak
was found in accordance with Section 724.958(a), and the date the leak
was detected, must be attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be removed after
it has been repaired.
3)
The identification on a valve may be removed after it has been
monitored for 2 successive months as specified in Section 724.957(c)
and no leak has been detected during those 2 months.
d)
When each leak is detected as specified in Sections Section 724.952, 724.953,
724.957 or 724.958, the following information must be recorded in an
inspection log and must be kept in the facility operating record:
195
1)
The instrument and operator identification numbers and the equipment
identification number.
2)
The date evidence of a potential leak was found in accordance with
Section 724.958(a).
3)
The date the leak was detected and the dates of each attempt to repair the
leak.
4)
Repair methods applied in each attempt to repair the leak.
5)
“Above 10,000”, if the maximum instrument reading measured by the
methods specified in Section 724.963(b) after each repair attempt is
equal to or greater than 10,000 ppm.
6)
“Repair delayed” and the reason for the delay if a leak is not repaired
within 15 calendar days after discovery of the leak.
7)
Documentation supporting the delay of repair of a valve in compliance
with Section 724.959(c).
8)
The signature of the owner or operator (or designate) whose decision it
was that repair could not be effected without a hazardous waste
management unit shutdown.
9)
The expected date of successful repair of the leak if a leak is not repaired
within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection information for
each closed-vent system and control device required to comply with the
provisions of Section 724.960 must be recorded and kept up-to-date in the
facility operating record as specified in Section 724.935(c)(1) and (c)(2), and
monitoring, operating and inspection information in Section 724.935(c)(3)
through (c)(8).
f)
For a control device other than a thermal vapor incinerator, catalytic vapor
incinerator, flare, boiler, process heater, condenser, or carbon adsorption
system, the Agency shall specify the appropriate recordkeeping requirements,
indicating proper operation and maintenance of the control device, in the RCRA
permit.
196
g)
The following information pertaining to all equipment subject to the
requirements in Sections 724.952 through 724.960 must be recorded in a log
that is kept in the facility operating record:
1)
A list of identification numbers for equipment (except welded fittings)
subject to the requirements of this Subpart.
2)
List of Equipment
A)
A list of identification numbers for equipment that the owner or
operator elects to designate for no detectable emissions, as
indicated by an instrument reading of less than 500 ppm above
background, under the provisions of Sections 724.952(e),
724.953(i) and 724.957(f).
B)
The designation of this equipment as subject to the requirements
of Section 724.952(e), 724.953(i) or 724.957(f) must be signed
by the owner or operator.
3)
A list of equipment identification numbers for pressure relief devices
required to comply with Section 724.954(a).
4)
Compliance tests.
A)
The dates of each compliance test required in Sections
724.952(e), 724.953(i), 724.954 and 724.957(f).
B)
The background level measured during each compliance test.
C)
The maximum instrument reading measured at the equipment
during each compliance test.
5)
A list of identification numbers for equipment in vacuum service.
6)
Identification, either by list or location (area or group), of equipment
that contains or contacts hazardous waste with an organic concentration
of at least 10 percent by weight for a period of less than 300 hours per
year.
h)
The following information pertaining to all valves subject to the requirements of
Section 724.957(g) and (h) must be recorded in a log that is kept in the facility
operating record:
197
1)
A list of identification numbers for valves that are designated as unsafe
to monitor, an explanation for each valve stating why the valve is unsafe
to monitor, and the plan for monitoring each valve.
2)
A list of identification numbers for valves that are designated as difficult
to monitor, an explanation for each valve stating why the valve is
difficult to monitor, and the planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility operating record for
valves complying with Section 724.962:
1)
A schedule of monitoring.
2)
The percent of valves found leaking during each monitoring period.
j)
The following information must be recorded in a log that is kept in the facility
operating record:
1)
Criteria required in Sections 724.952(d)(5)(B) and 724.953(e)(2) and an
explanation of the design criteria.
2)
Any changes to these criteria and the reasons for the changes.
k)
The following information must be recorded in a log that is kept in the facility
operating record for use in determining exemptions as provided in Section
724.950 and other specific Subparts:
1)
An analysis determining the design capacity of the hazardous waste
management unit.
2)
A statement listing the hazardous waste influent to and effluent from
each hazardous waste management unit subject to the requirements in
Section 724.960 and an analysis determining whether these hazardous
wastes are heavy liquids.
3)
An up-to-date analysis and the supporting information and data used to
determine whether or not equipment is subject to the requirements in
Sections 724.952 through 724.960. The record must include supporting
documentation as required by Section 724.963(d)(3) when application of
the knowledge of the nature of the hazardous wastestream or the process
by which it was produced is used. If the owner or operator takes any
action (e.g., changing the process that produced the waste) that could
result in an increase in the total organic content of the waste contained in
or contacted by equipment determined not to be subject to the
198
requirements in Sections 724.952 through 724.960, then a new
determination is required.
l)
Records of the equipment leak information required by subsection (d) of this
Section and the operating information required by subsection (e) of this Section
need be kept only 3 years.
m)
The owner or operator of any facility with equipment that is subject to this
Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart
V or 63, incorporated by reference in 35 Ill. Adm. Code 720.111, may elect to
determine compliance with this Subpart by documentation of compliance either
pursuant to Section 724.964, or by documentation of compliance with the
regulations at 40 CFR 60, 61, or 63, pursuant to those the relevant provisions of
40 CFR 60, or 61, or 63.to the extent that the documentation under the
regulation at 40 CFR 60 or 61 duplicates the documentation required under this
Subpart. The documentation of compliance under the regulation at 40 CFR 60,
or 61, or 63 must be kept with or made readily available with the facility
operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section 724.980
Applicability
a)
The requirements of this Subpart apply, effective October 6, 1996, to owners
and operators of all facilities that treat, store, or dispose of hazardous waste in
tanks, surface impoundments, or containers subject to 724.Subpart I, J, or K of
this Part, except as Section 724.101 and subsection (b) of this Section provide
otherwise.
BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
(Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828 (May 19,
1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed. Reg. 28508 (June 5,
1996), USEPA delayed the effective date until October 6, 1996. If action by
USEPA or a decision of a federal court changes the effectiveness of these
regulations, the Board does not intend that the 724.Subpart CC rules be
enforceable to the extent that they become more stringent than the federal
regulations upon which they are based.
b)
The requirements of this Subpart do not apply to the following waste
management units at the facility:
199
1)
A waste management unit that holds hazardous waste placed in the unit
before October December 6, 1996, and in which no hazardous waste is
added to the unit on or after this date December 6, 1996.
2)
A container that has a design capacity less than or equal to 0.1 m
3
(3.5
ft
3
or 26.4 gal).
3)
A tank in which an owner or operator has stopped adding hazardous
waste and the owner or operator has begun implementing or completed
closure pursuant to an approved closure plan.
4)
A surface impoundment in which an owner or operator has stopped
adding hazardous waste (except to implement an approved closure plan)
and the owner or operator has begun implementing or completed closure
pursuant to an approved closure plan.
5)
A waste management unit that is used solely for on-site treatment or
storage of hazardous waste that is generated as the result of
implementing remedial activities required pursuant to the Act or Board
regulations or under the corrective action authorities of RCRA section
3004(u), 3004(v) or 3008(h); CERCLA authorities; or similar federal or
State authorities.
6)
A waste management unit that is used solely for the management of
radioactive mixed waste in accordance with all applicable regulations
under the authority of the Atomic Energy Act (42 U.S.C. USC 2011 et
seq.) and the Nuclear Waste Policy Act.
7)
A hazardous waste management unit that the owner or operator certifies
is equipped with and operating air emission controls in accordance with
the requirements of an applicable federal Clean Air Act regulation
codified under 40 CFR 60, 61, or 63. For the purpose of complying
with this subsection (b)(7), a tank for which the air emission control
includes an enclosure, as opposed to a cover, must be in compliance
with the enclosure and control device requirements of Section
724.984(i), except as provided in Section 724.982(c)(5).
8)
A tank that has a process vent, as defined in 35 Ill. Adm. Code 724.931.
c)
For the owner and operator of a facility subject to this Subpart and that received
a final RCRA permit prior to October December 6, 1996, the requirements of
this Subpart shall be incorporated into the permit when the permit is reissued,
renewed, or modified in accordance with the requirements of 35 Ill. Adm. Code
703 and 705. Until such date when the owner and operator receives a final
200
permit incorporating the requirements of this Subpart, the owner and operator is
subject to the requirements of 35 Ill. Adm. Code 725.Subpart CC.
d)
The requirements of this Subpart, except for the recordkeeping requirements
specified in Section 724.989(i), are stayed for a tank or container used for the
management of hazardous waste generated by organic peroxide manufacturing
and its associated laboratory operations, when the owner or operator of the unit
meets all of the following conditions:
1)
The owner or operator identifies that the tank or container receives
hazardous waste generated by an organic peroxide manufacturing process
producing more than one functional family of organic peroxides or
multiple organic peroxides within one functional family, that one or
more of these organic peroxides could potentially undergo self-
accelerating thermal decomposition at or below ambient temperatures,
and that organic peroxides are the predominant products manufactured
by the process. For the purposes of this subsection, “organic peroxide”
means an organic compound that contains the bivalent -O-O- structure
and which may be considered to be a structural derivative of hydrogen
peroxide where one or both of the hydrogen atoms has been replaced by
an organic radical.
2)
The owner or operator prepares documentation, in accordance with
Section 724.989(i), explaining why an undue safety hazard would be
created if air emission controls specified in Sections 724.984 through
724.987 are installed and operated on the tanks and containers used at
the facility to manage the hazardous waste generated by the organic
peroxide manufacturing process or processes meeting the conditions of
subsection (d)(1) of this Section.
3)
The owner or operator notifies the Agency in writing that hazardous
waste generated by an organic peroxide manufacturing process or
processes meeting the conditions of subsection (d)(1) of this Section are
managed at the facility in tanks or containers meeting the conditions of
subsection (d)(2) of this Section. The notification must state the name
and address of the facility and be signed and dated by an authorized
representative of the facility owner or operator.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.982
Standards: General
a)
This Section applies to the management of hazardous waste in tanks, surface
impoundments, and containers subject to this Subpart.
201
b)
The owner or operator shall control air pollutant emissions from each waste
management unit in accordance with the standards specified in Section Sections
724.984 through 724.987, as applicable to the waste management unit, except
as provided for in subsection (c) of this Section.
c)
A tank, surface impoundment, or container is exempt from standards specified
in Sections 724.984 through 724.987, as applicable, provided that all hazardous
waste placed in the waste management unit is one of the following:
1)
A tank, surface impoundment, or container for which all hazardous
waste entering the unit has an average VO concentration at the point of
waste origination of less than 500 parts per million by weight (ppmw).
The average VO concentration shall be determined by the procedures
specified in Section 724.983(a). The owner or operator shall review and
update, as necessary, this determination at least once every 12 months
following the date of the initial determination for the hazardous waste
streams entering the unit.
2)
A tank, surface impoundment, or container for which the organic content
of all the hazardous waste entering the waste management unit has been
reduced by an organic destruction or removal process that achieves any
one of the following conditions:
A)
The process removes or destroys the organics contained in the
hazardous waste to a level such that the average VO
concentration of the hazardous waste at the point of waste
treatment is less than the exit concentration limit (Ct) established
for the process. The average VO concentration of the hazardous
waste at the point of waste treatment and the exit concentration
limit for the process shall be determined using the procedures
specified in Section 724.983(b).
B)
The process removes or destroys the organics contained in the
hazardous waste to a level such that the organic reduction
efficiency (R) for the process is equal to or greater than 95%
percent, and the average VO concentration of the hazardous
waste at the point of waste treatment is less than 100 ppmw. The
organic reduction efficiency for the process and the average VO
concentration of the hazardous waste at the point of waste
treatment shall be determined using the procedures specified in
Section 724.983(b).
C)
The process removes or destroys the organics contained in the
hazardous waste to such a level that the actual organic mass
removal rate (MR) for the process is equal to or greater than the
202
required organic mass removal rate (RMR) established for the
process. The required organic mass removal rate and the actual
organic mass removal rate for the process must be determined
using the procedures specified in Section 724.983(b).
D)
The process is a biological process that destroys or degrades the
organics contained in the hazardous waste so that either of the
following conditions is met:
i)
The organic reduction efficiency (R) for the process is
equal to or greater than 95% percent, and the organic
biodegradation efficiency (Rbio) for the process is equal to
or greater than 95% percent. The organic reduction
efficiency and the organic biodegradation efficiency for
the process shall be determined using the procedures
specified in Section 724.983(b).
ii)
The total actual organic mass biodegradation rate (MRbio)
for all hazardous waste treated by the process is equal to
or greater than the required organic mass removal rate
(RMR). The required organic mass removal rate and the
actual organic mass biodegradation rate for the process
shall be determined using the procedures specified in
Section 724.983(b).
E)
The process removes or destroys the organics contained in the
hazardous waste and meets all of the following conditions:
i)
From the point of waste origination through the point
where the hazardous waste enters the treatment process,
the hazardous waste is continuously managed in waste
management units that use air emission controls in
accordance with the standards specified in Sections
724.984 through 724.987, as applicable to the waste
management unit.
ii)
From the point of waste origination through the point
where the hazardous waste enters the treatment process,
any transfer of the hazardous waste is accomplished
through continuous hard-piping or other closed system
transfer that does not allow exposure of the waste to the
atmosphere.
BOARD NOTE: The USEPA considers a drain system
that meets the requirements of 40 CFR 63, subpart RR,
203
“National Emission Standards for Individual Drain
Systems”, to be a closed system.
iii)
The average VO concentration of the hazardous waste at
the point of waste treatment is less than the lowest average
VO concentration at the point of waste origination,
determined for each of the individual hazardous waste
streams entering the process or 500 ppmw, whichever
value is lower. The average VO concentration of each
individual hazardous waste stream at the point of waste
origination shall be determined using the procedures
specified in Section 724.983(a). The average VO
concentration of the hazardous waste at the point of waste
treatment shall be determined using the procedures
specified in Section 724.983(b).
F)
A process that removes or destroys the organics contained in the
hazardous waste to a level such that the organic reduction
efficiency (R) for the process is equal to or greater than 95%
percent and the owner or operator certifies that the average VO
concentration at the point of waste origination for each of the
individual waste streams entering the process is less than 10,000
ppmw. The organic reduction efficiency for the process and the
average VO concentration of the hazardous waste at the point of
waste origination shall be determined using the procedures
specified in Section 724.983(b) and Section 724.983(a),
respectively.
G)
A hazardous waste incinerator for which either of the following
conditions is true:
i)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
726.Subpart H; or
ii)
The owner or operator has designed and operates the
incinerator in accordance with the interim status
requirements of 35 Ill. Adm. Code 725.Subpart O.
H)
A boiler or industrial furnace for which either of the following
conditions is true:
i)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
204
implements the requirements of 35 Ill. Adm. Code
726.Subpart H; or
ii)
The owner or operator has designed and operates the
boiler or industrial furnace in accordance with the interim
status requirements of 35 Ill. Adm. Code 726.Subpart H.
I)
For the purpose of determining the performance of an organic
destruction or removal process in accordance with the conditions
in each of subsections (c)(2)(A) through (c)(2)(F) of this Section,
the owner or operator shall account for VO concentrations
determined to be below the limit of detection of the analytical
method by using the following VO concentration:
i)
If Method 25D in 40 CFR 60, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111, is used for
the analysis, one-half the blank value determined in
Section 4.4 of the method or a value of 25 ppmw, whichever
is less.
ii)
If any other analytical method is used, one-half the sum of
the limit limits of detection established for the method
each organic constituent in the waste that has a Henry’s law
constant value at least 0.1 mole-fraction-in-the-gas-
phase/mole-fraction-in-the-liquid-phase (0.1 Y/X) (which can
also be expressed as 1.8 x 10
-6
atmospheres/gram-mole/m
3
)
at 25° C .
3)
A tank or surface impoundment used for biological treatment of hazardous
waste in accordance with the requirements of subsection (c)(2)(D) of this
Section.
4)
A tank, surface impoundment, or container for which all hazardous
waste placed in the unit fulfills either of the following conditions:
A)
It meets the numerical concentration limits for organic hazardous
constituents, applicable to the hazardous waste, as specified in 35
Ill. Adm. Code 728.Table T; or
B)
It has The organic hazardous constituents in the waste have been
treated by the treatment technology established by USEPA for the
waste, as set forth in 35 Ill. Adm. Code 728.142(a), or treated
have been removed or destroyed by an equivalent method of
treatment approved by the Agency pursuant to 35 Ill. Adm. Code
728.142(b).
205
5)
A tank used for bulk feed of hazardous waste to a waste incinerator and
all of the following conditions are met:
A)
The tank is located inside an enclosure vented to a control device
that is designed and operated in accordance with all applicable
requirements specified under 40 CFR 61, subpart FF, “National
Emission Standards for Benzene Waste Operations”, incorporated
by reference in 35 Ill. Adm. Code 720.111, for a facility at
which the total annual benzene quantity from the facility waste is
equal to or greater than 10 megagrams (11 tons) per year;
B)
The enclosure and control device serving the tank were installed
and began operation prior to November 25, 1996; and
C)
The enclosure is designed and operated in accordance with the
criteria for a permanent total enclosure as specified in “Procedure
T--Criteria for and Verification of a Permanent or Temporary
Total Enclosure” under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code 720.111. The
enclosure may have permanent or temporary openings to allow
worker access; passage of material into or out of the enclosure by
conveyor, vehicles, or other mechanical or electrical equipment;
or to direct air flow into the enclosure. The owner or operator
shall perform the verification procedure for the enclosure as
specified in Section 5.0 to “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure”
annually.
d)
The Agency may at any time perform or request that the owner or operator
perform a waste determination for a hazardous waste managed in a tank, surface
impoundment, or container that is exempted from using air emission controls
under the provisions of this Section as follows:
1)
The waste determination for average VO concentration of a hazardous
waste at the point of waste origination shall be performed using direct
measurement in accordance with the applicable requirements of Section
724.983(a). The waste determination for a hazardous waste at the point
of waste treatment shall be performed in accordance with the applicable
requirements of Section 724.983(b).
2)
In performing a waste determination pursuant to subsection (d)(1) of this
Section, the sample preparation and analysis shall be conducted as
follows:
206
A)
In accordance with the method used by the owner or operator to
perform the waste analysis, except in the case specified in
subsection (d)(2)(B) of this Section.
B)
If the Agency determines that the method used by the owner or
operator was not appropriate for the hazardous waste managed in
the tank, surface impoundment, or container, then the Agency
may choose an appropriate method.
3)
Where the owner or operator is requested to perform the waste
determination, the Agency may elect to have an authorized
representative observe the collection of the hazardous waste samples
used for the analysis.
4)
Where the results of the waste determination performed or requested by
the Agency do not agree with the results of a waste determination
performed by the owner or operator using knowledge of the waste, then
the results of the waste determination performed in accordance with the
requirements of subsection (d)(1) of this Section shall be used to
establish compliance with the requirements of this Subpart.
5)
Where the owner or operator has used an averaging period greater than
one hour for determining the average VO concentration of a hazardous
waste at the point of waste origination, the Agency may elect to establish
compliance with this Subpart by performing or requesting that the owner
or operator perform a waste determination using direct measurement
based on waste samples collected within a one-hour period as follows:
A)
The average VO concentration of the hazardous waste at the point
of waste origination shall be determined by direct measurement in
accordance with the requirements of Section 724.983(a).
B)
Results of the waste determination performed or requested by the
Agency showing that the average VO concentration of the
hazardous waste at the point of waste origination is equal to or
greater than 500 ppmw shall constitute noncompliance with this
Subpart, except in a case as provided for in subsection (d)(5)(C)
of this Section.
C)
Where the average VO concentration of the hazardous waste at
the point of waste origination previously has been determined by
the owner or operator using an averaging period greater than one
hour to be less than 500 ppmw but because of normal operating
process variations the VO concentration of the hazardous waste
determined by direct measurement for any given one-hour period
207
may be equal to or greater than 500 ppmw, information that was
used by the owner or operator to determine the average VO
concentration of the hazardous waste (e.g., test results,
measurements, calculations, and other documentation) and
recorded in the facility records in accordance with the
requirements of Section 724.983(a) and Section 724.989 shall be
considered by the Agency together with the results of the waste
determination performed or requested by the Agency in
establishing compliance with this Subpart.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.983
Waste Determination Procedures
a)
Waste determination procedure for average volatile organic (VO) concentration
of a hazardous waste at the point of waste origination.
1)
An owner or operator shall determine the average VO concentration at
the point of waste origination for each hazardous waste placed in a waste
management unit exempted under the provisions of Section
724.982(c)(1) from using air emission controls in accordance with
standards specified in Section 724.984 through Section 724.987, as
applicable to the waste management unit.
2)
The For a waste determination that is required by subsection (a)(1) of this
Section, the average VO concentration of a hazardous waste at the point
of waste origination may shall be determined in accordance with the
procedures specified in 35 Ill. Adm. Code 725.984(a)(2) through (a)(4).
b)
Waste determination procedures for treated hazardous waste.
1)
An owner or operator shall perform the applicable waste determination
for each treated hazardous waste placed in a waste management unit
exempted under the provisions of Section 724.982(c)(2)(A) through
(c)(2)(F from using air emission controls in accordance with standards
specified in Sections 724.984 through 724.987, as applicable to the
waste management unit.
2)
The waste determination for a treated hazardous waste shall be
performed in accordance with the procedures specified in 35 Ill. Adm.
Code 725.984(b)(2) through (b)(9), as applicable to the treated
hazardous waste.
c)
Procedure to determine the maximum organic vapor pressure of a hazardous
waste in a tank.
208
1)
An owner or operator shall determine the maximum organic vapor
pressure for each hazardous waste placed in a tank using Tank Level 1
controls in accordance with standards specified in Section 724.984(c).
2)
The maximum organic vapor pressure of the hazardous waste may be
determined in accordance with the procedures specified in 35 Ill. Adm.
Code 725.984(c)(2) through (c)(4).
d)
The procedure for determining no detectable organic emissions for the purpose
of complying with this Subpart must be conducted in accordance with the
procedures specified in 40 CFR 265.984(d) 35 Ill. Adm. Code 725.984(d).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.984
Standards: Tanks
a)
The provisions of this Section apply to the control of air pollutant emissions
from tanks for which Section 724.982(b) references the use of this Section for
such air emission control.
b)
The owner or operator shall control air pollutant emissions from each tank
subject to this Section in accordance with the following requirements, as
applicable:
1)
For a tank that manages hazardous waste that meets all of the conditions
specified in subsections (b)(1)(A) through (b)(1)(C) of this Section, the
owner or operator shall control air pollutant emissions from the tank in
accordance with the Tank Level 1 controls specified in subsection (c) of
this Section or the Tank Level 2 controls specified in subsection (d) of
this Section.
A)
The hazardous waste in the tank has a maximum organic vapor
pressure that is less than the maximum organic vapor pressure
limit for the tank’s design capacity category as follows:
i)
For a tank design capacity equal to or greater than 151 m
3
(39,900 gal), the maximum organic vapor pressure limit
for the tank is 5.2 kPa (0.75 psig).
ii)
For a tank design capacity equal to or greater than 75 m
3
(19,800 gal) but less than 151 m
3
(39,900 gal), the
maximum organic vapor pressure limit for the tank is 27.6
kPa (4.00 psig).
209
iii)
For a tank design capacity less than 75 m
3
(19,800 gal),
the maximum organic vapor pressure limit for the tank is
76.6 kPa (11.1 psig).
B)
The hazardous waste in the tank is not heated by the owner or
operator to a temperature that is greater than the temperature at
which the maximum organic vapor pressure of the hazardous
waste is determined for the purpose of complying with subsection
(b)(1)(A) of this Section.
C)
The hazardous waste in the tank is not treated by the owner or
operator using a waste stabilization process, as defined in 35 Ill.
Adm. Code 725.981.
2)
For a tank that manages hazardous waste that does not meet all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank by using Tank Level 2 controls in accordance with the
requirements of subsection (d) of this Section. Examples of tanks
required to use Tank Level 2 controls include a tank used for a waste
stabilization process and a tank for which the hazardous waste in the tank
has a maximum organic vapor pressure that is equal to or greater than
the maximum organic vapor pressure limit for the tank’s design capacity
category as specified in subsection (b)(1)(A) of this Section.
c)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 1 controls must meet the requirements specified in subsections (c)(1)
through (c)(4) of this Section:
1)
The owner or operator shall determine the maximum organic vapor
pressure for a hazardous waste to be managed in the tank using Tank
Level 1 controls before the first time the hazardous waste is placed in the
tank. The maximum organic vapor pressure must be determined using
the procedures specified in Section 724.983(c). Thereafter, the owner or
operator shall perform a new determination whenever changes to the
hazardous waste managed in the tank could potentially cause the
maximum organic vapor pressure to increase to a level that is equal to or
greater than the maximum organic vapor pressure limit for the tank
design capacity category specified in subsection (b)(1)(A) of this
Section, as applicable to the tank.
2)
The tank must be equipped with a fixed roof designed to meet the
following specifications:
210
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the hazardous
waste in the tank. The fixed roof may be a separate cover
installed on the tank (e.g., a removable cover mounted on an
open-top tank) or may be an integral part of the tank structural
design (e.g., a horizontal cylindrical tank equipped with a hatch).
B)
The fixed roof must be installed in a manner such that there are
no visible cracks, holes, gaps, or other open spaces between roof
section joints or between the interface of the roof edge and the
tank wall.
C)
Each Either of the following must be true of each opening in the
fixed roof and of any manifold system associated with the fixed roof
must be either:
i)
Equipped The opening or manifold system is equipped
with a closure device designed to operate such that when
the closure device is secured in the closed position there
are no visible cracks, holes, gaps, or other open spaces in
the closure device or between the perimeter of the opening
and the closure device; or
ii)
Connected The opening or manifold system is connected
by a closed-vent system that is vented to a control device.
The control device must remove or destroy organics in the
vent stream, and it must be operating whenever hazardous
waste is managed in the tank, except as provided for in
subsection (c)(2)(E) of this Section.
D)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: the organic vapor permeability; the
effects of any contact with the hazardous waste or its vapors
managed in the tank; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices used for the
tank on which the fixed roof is installed.
E)
The control device operated pursuant to subsection (c)(2)(C) of
this Section needs not remove or destroy organics in the vent
stream under the following conditions:
211
i)
During periods when it is necessary to provide access to the
tank for performing the activities of subsection (c)(2)(E)(ii) of
this Section, venting of the vapor headspace underneath the
fixed roof to the control device is not required, opening of
closure devices is allowed, and removal of the fixed roof is
allowed. Following completion of the activity, the owner or
operator shall promptly secure the closure device in the
closed position or reinstall the cover, as applicable, and
resume operation of the control device; and
ii)
During periods of routine inspection, maintenance, or other
activities needed for normal operations, and for removal of
accumulated sludge or other residues from the bottom of the
tank.
BOARD NOTE: Subsections (c)(2)(E)(i) and (c)(2)(E)(ii) are
derived from 40 CFR 264.1084(c)(2)(iii)(B)(
1
) and
(c)(2)(iii)(B)(
2
), which the Board has codified here to comport
with Illinois Administrative Code format requirements.
3)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position, except
as follows:
A)
Opening of closure devices or removal of the fixed roof is
allowed at the following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
the liquid in the tank, or when a worker needs to open a
hatch to maintain or repair equipment. Following
completion of the activity, the owner or operator shall
promptly secure the closure device in the closed position
or reinstall the cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of the tank.
B)
Opening of a spring-loaded pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the tank internal pressure in
accordance with the tank design specifications. The device must
be designed to operate with no detectable organic emissions when
212
the device is secured in the closed position. The settings at which
the device opens must be established such that the device remains
in the closed position whenever the tank internal pressure is
within the internal pressure operating range determined by the
owner or operator based on the tank manufacturer
recommendations, applicable regulations, fire protection and
prevention codes, standard engineering codes and practices, or
other requirements for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to open are
during those times when the tank internal pressure exceeds the
internal pressure operating range for the tank as a result of
loading operations or diurnal ambient temperature fluctuations.
C)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
4)
The owner or operator shall inspect the air emission control equipment
in accordance with the following requirements.
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof sections or between the
roof and the tank wall; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
fixed roof and its closure devices on or before the date that the
tank becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year
except under the special conditions provided for in subsection (l)
of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
213
d)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 2 controls must use one of the following tanks:
1)
A fixed-roof tank equipped with an internal floating roof in accordance
with the requirements specified in subsection (e) of this Section;
2)
A tank equipped with an external floating roof in accordance with the
requirements specified in subsection (f) of this Section;
3)
A tank vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (g) of this
Section;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) of this Section; or
5)
A tank located inside an enclosure that is vented through a closed-vent
system to an enclosed combustion control device in accordance with the
requirements specified in subsection (i) of this Section.
e)
The owner or operator that controls air pollutant emissions from a tank using a
fixed roof with an internal floating roof shall meet the requirements specified in
subsections (e)(1) through (e)(3) of this Section.
1)
The tank must be equipped with a fixed roof and an internal floating roof
in accordance with the following requirements:
A)
The internal floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The internal floating roof must be equipped with a continuous
seal between the wall of the tank and the floating roof edge that
meets either of the following requirements:
i)
A single continuous seal that is either a liquid-mounted
seal or a metallic shoe seal, as defined in 35 Ill. Adm.
Code 725.981; or
ii)
Two continuous seals mounted one above the other. The
lower seal may be a vapor-mounted seal.
C)
The internal floating roof must meet the following specifications:
214
i)
Each opening in a noncontact internal floating roof except
for automatic bleeder vents (vacuum breaker vents) and
the rim space vents is to provide a projection below the
liquid surface.
ii)
Each opening in the internal floating roof must be
equipped with a gasketed cover or a gasketed lid except
for leg sleeves, automatic bleeder vents, rim space vents,
column wells, ladder wells, sample wells, and stub drains.
iii)
Each penetration of the internal floating roof for the
purpose of sampling must have a slit fabric cover that
covers at least 90 percent of the opening.
iv)
Each automatic bleeder vent and rim space vent must be
gasketed.
v)
Each penetration of the internal floating roof that allows
for passage of a ladder must have a gasketed sliding
cover.
vi)
Each penetration of the internal floating roof that allows
for passage of a column supporting the fixed roof must
have a flexible fabric sleeve seal or a gasketed sliding
cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
C)
Prior to filling the tank, each cover, access hatch, gauge float
well or lid on any opening in the internal floating roof must be
bolted or fastened closed (i.e., no visible gaps). Rim space vents
must be set to open only when the internal floating roof is not
floating or when the pressure beneath the rim exceeds the
manufacturer’s recommended setting.
215
3)
The owner or operator shall inspect the internal floating roof in
accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects that could
result in air pollutant emissions. Defects include, but are not
limited to, any of the following: when the internal floating roof
is not floating on the surface of the liquid inside the tank; when
liquid has accumulated on top of the internal floating roof; when
any portion of the roof seals have detached from the roof rim;
when holes, tears, or other openings are visible in the seal fabric;
when the gaskets no longer close off the hazardous waste surface
from the atmosphere; or when the slotted membrane has more
than 10 percent open area.
B)
The owner or operator shall inspect the internal floating roof
components as follows, except as provided in subsection
(e)(3)(C) of this Section:
i)
Visually inspect the internal floating roof components
through openings on the fixed-roof (e.g., manholes and
roof hatches) at least once every 12 months after initial
fill, and
ii)
Visually inspect the internal floating roof, primary seal,
secondary seal (if one is in service), gaskets, slotted
membranes, and sleeve seals (if any) each time the tank is
emptied and degassed and at least once every 10 years.
C)
As an alternative to performing the inspections specified in
subsection (e)(3)(B) of this Section for an internal floating roof
equipped with two continuous seals mounted one above the other,
the owner or operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted membranes,
and sleeve seals (if any) each time the tank is emptied and
degassed and at least every five years.
D)
Prior to each inspection required by subsection (e)(3)(B) or
(e)(3)(C) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
216
i)
Prior to each visual inspection of an internal floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned, as provided for in subsection
(e)(3)(D)(ii) of this Section.
ii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Agency at least seven calendar days before refilling the
tank.
E)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
F)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
4)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may be installed and
operated as necessary on any tank complying with the requirements of this
subsection (e).
f)
The owner or operator that controls air pollutant emissions from a tank using an
external floating roof must meet the requirements specified in subsections (f)(1)
through (f)(3) of this Section.
1)
The owner or operator shall design the external floating roof in
accordance with the following requirements:
A)
The external floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The floating roof must be equipped with two continuous seals,
one above the other, between the wall of the tank and the roof
217
edge. The lower seal is referred to as the primary seal, and the
upper seal is referred to as the secondary seal.
i)
The primary seal must be a liquid-mounted seal or a
metallic shoe seal, as defined in 35 Ill. Adm. Code
725.981. The total area of the gaps between the tank wall
and the primary seal must not exceed 212 square
centimeters (cm
2
) per meter (10.0 square inches (in
2
) per
foot) of tank diameter, and the width of any portion of
these gaps must not exceed 3.8 centimeters (cm) (1.5 in).
If a metallic shoe seal is used for the primary seal, the
metallic shoe seal must be designed so that one end
extends into the liquid in the tank and the other end
extends a vertical distance of at least 61 cm (24 in) above
the liquid surface.
ii)
The secondary seal must be mounted above the primary
seal and cover the annular space between the floating roof
and the wall of the tank. The total area of the gaps
between the tank wall and the secondary seal must not
exceed 21.2 cm
2
per meter (1.00 in
2
per foot) of tank
diameter, and the width of any portion of these gaps must
not exceed 1.3 cm (0.51 in).
C)
The external floating roof must meet the following specifications:
i)
Except for automatic bleeder vents (vacuum breaker
vents) and rim space vents, each opening in a noncontact
external floating roof must provide a projection below the
liquid surface.
ii)
Except for automatic bleeder vents, rim space vents, roof
drains, and leg sleeves, each opening in the roof must be
equipped with a gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must be
equipped with a cover designed to be bolted or fastened
when the cover is secured in the closed position.
iv)
Each automatic bleeder vent and each rim space vent must
be equipped with a gasket.
v)
Each roof drain that empties into the liquid managed in
the tank must be equipped with a slotted membrane fabric
218
cover that covers at least 90 percent of the area of the
opening.
vi)
Each unslotted and slotted guide pole well must be
equipped with a gasketed sliding cover or a flexible fabric
sleeve seal.
vii)
Each unslotted guide pole must be equipped with a
gasketed cap on the end of the pole.
viii) Each slotted guide pole must be equipped with a gasketed
float or other device which closes off the liquid surface
from the atmosphere.
ix)
Each gauge hatch and each sample well must be equipped
with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents, roof drains,
and leg sleeves, each opening in the roof must be secured and
maintained in a closed position at all times except when the
closure device must be open for access.
C)
Covers on each access hatch and each gauge float well must be
bolted or fastened when secured in the closed position.
D)
Automatic bleeder vents must be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
E)
Rim space vents must be set to open only at those times that the
roof is being floated off the roof leg supports or when the
pressure beneath the rim seal exceeds the manufacturer’s
recommended setting.
F)
The cap on the end of each unslotted guide pole must be secured
in the closed position at all times except when measuring the
level or collecting samples of the liquid in the tank.
219
G)
The cover on each gauge hatch or sample well must be secured in
the closed position at all times except when the hatch or well
must be opened for access.
H)
Both the primary seal and the secondary seal must completely
cover the annular space between the external floating roof and the
wall of the tank in a continuous fashion except during
inspections.
3)
The owner or operator shall inspect the external floating roof in
accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external floating roof
seal gaps in accordance with the following requirements:
i)
The owner or operator shall perform measurements of
gaps between the tank wall and the primary seal within 60
calendar days after initial operation of the tank following
installation of the floating roof and, thereafter, at least
once every five years.
ii)
The owner or operator shall perform measurements of
gaps between the tank wall and the secondary seal within
60 calendar days after initial operation of the tank
following installation of the floating roof and, thereafter,
at least once every year.
iii)
If a tank ceases to hold hazardous waste for a period of
one year or more, subsequent introduction of hazardous
waste into the tank must be considered an initial operation
for the purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) of this Section.
iv)
The owner or operator shall determine the total surface
area of gaps in the primary seal and in the secondary seal
individually using the procedure of subsection (f)(3)(D) of
this Section.
v)
In the event that the seal gap measurements do not
conform to the specifications in subsection (f)(1)(B) of
this Section, the owner or operator shall repair the defect
in accordance with the requirements of subsection (k) of
this Section.
220
vi)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 724.989(b).
B)
The owner or operator shall visually inspect the external floating
roof in accordance with the following requirements:
i)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects
include, but are not limited to, any of the following
conditions: holes, tears, or other openings in the rim seal
or seal fabric of the floating roof; a rim seal detached
from the floating roof; all or a portion of the floating roof
deck being submerged below the surface of the liquid in
the tank; broken, cracked, or otherwise damaged seals or
gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
ii)
The owner or operator shall perform an initial inspection
of the external floating roof and its closure devices on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall perform
the inspections at least once every year except for the
special conditions provided for in subsection (l) of this
Section.
iii)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k) of this Section.
iv)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 724.989(b).
C)
Prior to each inspection required by subsection (f)(3)(A) or
(f)(3)(B) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each inspection to measure external floating roof
seal gaps as required under subsection (f)(3)(A) of this
Section, written notification must be prepared and sent by
221
the owner or operator so that it is received by the Agency
at least 30 calendar days before the date the measurements
are scheduled to be performed.
ii)
Prior to each visual inspection of an external floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned as provided for in subsection
(f)(3)(C)(iii) of this Section.
iii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Agency at least seven calendar days before refilling the
tank.
D)
Procedure for determining the total surface area of gaps in the
primary seal and the secondary seal:
i)
The seal gap measurements must be performed at one or
more floating roof levels when the roof is floating off the
roof supports.
ii)
Seal gaps, if any, must be measured around the entire
perimeter of the floating roof in each place where a 0.32
cm (0.125 in) diameter uniform probe passes freely
(without forcing or binding against the seal) between the
seal and the wall of the tank and measure the
circumferential distance of each such location.
iii)
For a seal gap measured under subsection (f)(3) of this
Section, the gap surface area must be determined by using
probes of various widths to measure accurately the actual
distance from the tank wall to the seal and multiplying
each such width by its respective circumferential distance.
222
iv)
The total gap area must be calculated by adding the gap
surface areas determined for each identified gap location
for the primary seal and the secondary seal individually,
and then dividing the sum for each seal type by the
nominal perimeter diameter of the tank. These total gap
areas for the primary seal and secondary seal are then
compared to the respective standards for the seal type, as
specified in subsection (f)(1)(B) of this Section.
BOARD NOTE: Subsections (f)(3)(D)(i) through (f)(3)(D)(iv)
correspond with are derived from 40 CFR
264.1084(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4), which the Board
has codified here to comport with Illinois Administrative Code
format requirements.
4)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may be installed and
operated as necessary on any tank complying with the requirements of
subsection (f) of this Section.
g)
The owner or operator that controls air pollutant emissions from a tank by
venting the tank to a control device shall meet the requirements specified in
subsections (g)(1) through (g)(3) of this Section.
1)
The tank must be covered by a fixed roof and vented directly through a
closed-vent system to a control device in accordance with the following
requirements:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
tank.
B)
Each opening in the fixed roof not vented to the control device
must be equipped with a closure device. If the pressure in the
vapor headspace underneath the fixed roof is less than
atmospheric pressure when the control device is operating, the
closure devices must be designed to operate such that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device. If the pressure in the vapor headspace underneath
the fixed roof is equal to or greater than atmospheric pressure
when the control device is operating, the closure device must be
designed to operate with no detectable organic emissions.
C)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
223
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: organic vapor permeability; the
effects of any contact with the liquid and its vapor managed in
the tank; the effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the tank on which
the fixed roof is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 724.987.
2)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position and the
vapor headspace underneath the fixed roof vented to the control device
except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the fixed roof is allowed at the
following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to open a hatch
to maintain or repair equipment. Following completion of
the activity, the owner or operator shall promptly secure
the closure device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of a tank.
B)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to,
224
any of the following: visible cracks, holes, or gaps in the roof
sections or between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure devices; and
broken or missing hatches, access covers, caps, or other closure
devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 724.987.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the tank
becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year
except for the special conditions provided for in subsection (l) of
this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
h)
The owner or operator that controls air pollutant emissions by using a pressure
tank must meet the following requirements:
1)
The tank must be designed not to vent to the atmosphere as a result of
compression of the vapor headspace in the tank during filling of the tank
to its design capacity.
2)
All tank openings must be equipped with closure devices designed to
operate with no detectable organic emissions as determined using the
procedure specified in Section 724.983(d).
3)
Whenever a hazardous waste is in the tank, the tank must be operated as
a closed system that does not vent to the atmosphere except in the event
that a safety device, as defined in 35 Ill. Adm. Code 725.981, is
required to open to avoid an unsafe condition.
i)
The owner or operator that controls air pollutant emissions by using an
enclosure vented through a closed-vent system to an enclosed combustion
control device must meet the requirements specified in subsections (i)(1)
through (i)(4) of this Section.
225
1)
The tank must be located inside an enclosure. The enclosure must be
designed and operated in accordance with the criteria for a permanent
total enclosure, as specified in “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure” under 40
CFR 52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the verification
procedure for the enclosure, as specified in Section 5.0 to “Procedure T-
-Criteria for and Verification of a Permanent or Temporary Total
Enclosure”, initially when the enclosure is first installed and, thereafter,
annually.
2)
The enclosure must be vented through a closed-vent system to an
enclosed combustion control device that is designed and operated in
accordance with the standards for either a vapor incinerator, boiler, or
process heater specified in Section 724.987.
3)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may be
installed and operated as necessary on any enclosure, closed-vent system,
or control device used to comply with the requirements of subsections
(i)(1) and (i)(2) of this Section.
4)
The owner or operator shall inspect and monitor the closed-vent system
and control device as specified in Section 724.987.
j)
The owner or operator shall transfer hazardous waste to a tank subject to this
Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (j)(2) of
this Section, to the tank from another tank subject to this Section or from
a surface impoundment subject to Section 724.985 must be conducted
using continuous hard-piping or another closed system that does not
allow exposure of the hazardous waste to the atmosphere. For the
purpose of complying with this provision, an individual drain system is
considered to be a closed system when it meets the requirements of 40
CFR 63, subpart RR, “National Emission Standards for Individual Drain
Systems”, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) of this Section do not apply when
transferring a hazardous waste to the tank under any of the following
conditions:
226
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 724.982(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
724.982(c)(2).
C)
The hazardous waste meets the requirements of Section
724.982(c)(4).
k)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(4), (e)(3),
(f)(3), or (g)(3) of this Section, as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair must be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (k)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the tank and no alternative tank
capacity is available at the site to accept the hazardous waste normally
managed in the tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating the hazardous
waste managed in the tank stops operation. Repair of the defect must be
completed before the process or unit resumes operation.
l)
Following the initial inspection and monitoring of the cover, as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year under the following special
conditions:
1)
In the case when inspecting or monitoring the cover would expose a
worker to dangerous, hazardous, or other unsafe conditions, then the
owner or operator may designate a cover as an “unsafe to inspect and
monitor cover” and comply with all of the following requirements:
A)
Prepare a written explanation for the cover stating the reasons
why the cover is unsafe to visually inspect or to monitor, if
required.
B)
Develop and implement a written plan and schedule to inspect
and monitor the cover, using the procedures specified in the
227
applicable Section of this Subpart, as frequently as practicable
during those times when a worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely underground, an
owner or operator is required to inspect and monitor, as required by the
applicable provisions of this Section, only those portions of the tank
cover and those connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground surface.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.985
Standards: Surface Impoundments
a)
The provisions of this Section apply to the control of air pollutant emissions
from surface impoundments for which Section 724.982(b) references the use of
this Section for such air emission control.
b)
The owner or operator shall control air pollutant emissions from the surface
impoundment by installing and operating either of the following:
1)
A floating membrane cover in accordance with the provisions specified
in subsection (c) of this Section; or
2)
A cover that is vented through a closed-vent system to a control device
in accordance with the provisions specified in subsection (d) of this
Section.
c)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a floating membrane cover must meet the requirements
specified in subsections (c)(1) through (c)(3) of this Section.
1)
The surface impoundment must be equipped with a floating membrane
cover designed to meet the following specifications:
A)
The floating membrane cover must be designed to float on the
liquid surface during normal operations and form a continuous
barrier over the entire surface area of the liquid.
B)
The cover must be fabricated from a synthetic membrane material
that is either:
i)
High density polyethylene (HDPE) with a thickness no
less than 2.5 millimeters (mm) (0.098 in); or
228
ii)
A material or a composite of different materials
determined to have both organic permeability properties
that are equivalent to those of the material listed in
subsection (c)(1)(B)(i) of this Section and chemical and
physical properties that maintain the material integrity for
the intended service life of the material.
C)
The cover must be installed in such a manner that there are no
visible cracks, holes, gaps, or other open spaces between cover
section seams or between the interface of the cover edge and its
foundation mountings.
D)
Except as provided for in subsection (c)(1)(E) of this Section,
each opening in the floating membrane cover must be equipped
with a closure device so designed as to operate that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device.
E)
The floating membrane cover may be equipped with one or more
emergency cover drains for removal of stormwater. Each
emergency cover drain must be equipped with a slotted
membrane fabric cover that covers at least 90% percent of the
area of the opening or a flexible fabric sleeve seal.
F)
The closure devices must be made of suitable materials that will
minimize exposure of the hazardous waste to the atmosphere, to
the extent practical, and will maintain the integrity of the closure
devices throughout their intended service life. Factors to be
considered when selecting the materials of construction and
designing the cover and closure devices must include the
following: the organic vapor permeability; the effects of any
contact with the liquid and its vapor managed in the surface
impoundment; the effects of outdoor exposure to wind, moisture,
and sunlight; and the operating practices used for the surface
impoundment on which the floating membrane cover is installed.
2)
Whenever a hazardous waste is in the surface impoundment, the floating
membrane cover must float on the liquid and each closure device must
be secured in the closed position, except as follows:
A)
Opening of closure devices or removal of the cover is allowed at
the following times:
229
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample the liquid in the surface impoundment, or
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly replace the cover and
secure the closure device in the closed position, as
applicable.
ii)
To remove accumulated sludge or other residues from the
bottom of surface impoundment.
B)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
3)
The owner or operator shall inspect the floating membrane cover in
accordance with the following procedures:
A)
The floating membrane cover and its closure devices must be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
floating membrane cover and its closure devices on or before the
date that the surface impoundment becomes subject to this
Section. Thereafter, the owner or operator shall perform the
inspections at least once every year except for the special
conditions provided for in subsection (g) of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(c).
230
d)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a cover vented to a control device shall meet the
requirements specified in subsections (d)(1) through (d)(3) of this Section.
1)
The surface impoundment must be covered by a cover and vented
directly through a closed-vent system to a control device in accordance
with the following requirements:
A)
The cover and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
surface impoundment.
B)
Each opening in the cover not vented to the control device must
be equipped with a closure device. If the pressure in the vapor
headspace underneath the cover is less than atmospheric pressure
when the control device is operating, the closure devices must be
designed to operate such that when the closure device is secured
in the closed position there are no visible cracks, holes, gaps, or
other open spaces in the closure device or between the perimeter
of the cover opening and the closure device. If the pressure in
the vapor headspace underneath the cover is equal to or greater
than atmospheric pressure when the control device is operating,
the closure device must be designed to operate with no detectable
organic emissions using the procedure specified in Section
724.983(d).
C)
The cover and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and which will maintain
the integrity of the cover and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for of construction and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the liquid or its
vapors managed in the surface impoundment; the effects of
outdoor exposure to wind, moisture, and sunlight; and the
operating practices used for the surface impoundment on which
the cover is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 724.987.
2)
Whenever a hazardous waste is in the surface impoundment, the cover
must be installed with each closure device secured in the closed position
231
and the vapor headspace underneath the cover vented to the control
device except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the cover is allowed at the
following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample liquid in the surface impoundment, or
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as
applicable, to the surface impoundment.
ii)
To remove accumulated sludge or other residues from the
bottom of the surface impoundment.
B)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The surface impoundment cover and its closure devices shall be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 724.987.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the
surface impoundment becomes subject to this Section.
Thereafter, the owner or operator shall perform the inspections at
232
least once every year except for the special conditions provided
for in subsection (g) of this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(c).
e)
The owner or operator shall transfer hazardous waste to a surface impoundment
subject to this Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (e)(2) of
this Section, to the surface impoundment from another surface
impoundment subject to this Section or from a tank subject to Section
724.984 must be conducted using continuous hard-piping or another
closed system that does not allow exposure of the waste to the
atmosphere. For the purpose of complying with this provision, an
individual drain system is considered to be a closed system when it meets
the requirements of 40 CFR 63, Subpart RR, “National Emission
Standards for Individual Drain Systems”, incorporated by reference in
35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (e)(1) of this Section do not apply when
transferring a hazardous waste to the surface impoundment under either
any of the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 724.982(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
724.982(c)(2).
C)
The hazardous waste meets the requirements of Section
724.982(c)(4).
f)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(3) or (d)(3) of
this Section as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection and repair must be completed
233
as soon as possible but no later than 45 calendar days after detection
except as provided in subsection (f)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the surface impoundment and no
alternative capacity is available at the site to accept the hazardous waste
normally managed in the surface impoundment. In this case, the owner
or operator shall repair the defect the next time the process or unit that is
generating the hazardous waste managed in the surface impoundment
stops operation. Repair of the defect must be completed before the
process or unit resumes operation.
g)
Following the initial inspection and monitoring of the cover as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year in the case when inspecting or
monitoring the cover would expose a worker to dangerous, hazardous, or other
unsafe conditions. In this case, the owner or operator may designate the cover
as an “unsafe to inspect and monitor cover” and comply with all of the
following requirements:
1)
Prepare a written explanation for the cover stating the reasons why the
cover is unsafe to visually inspect or to monitor, if required.
2)
Develop and implement a written plan and schedule to inspect and
monitor the cover using the procedures specified in the applicable
Section of this Subpart as frequently as practicable during those times
when a worker can safely access the cover.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.986
Standards: Containers
a)
The provisions of this Section apply to the control of air pollutant emissions
from containers for which Section 724.982(b) references the use of this Section
for such air emission control.
b)
General requirements.
1)
The owner or operator shall control air pollutant emissions from each
container subject to this Section in accordance with the following
requirements, as applicable to the container, except when the special
provisions for waste stabilization processes specified in subsection (b)(2)
of this Section apply to the container.
234
A)
For a container having a design capacity greater than 0.1 m
3
(26
gal) and less than or equal to 0.46 m
3
(120 gal), the owner or
operator shall control air pollutant emissions from the container
in accordance with the Container Level 1 standards specified in
subsection (c) of this Section.
B)
For a container having a design capacity greater than 0.46 m
3
(120 gal) that is not in light material service, the owner or
operator shall control air pollutant emissions from the container
in accordance with the Container Level 1 standards specified in
subsection (c) of this Section.
C)
For a container having a design capacity greater than 0.46 m
3
(120 gal) that is in light material service, the owner or operator
shall control air pollutant emissions from the container in
accordance with the Container Level 2 standards specified in
subsection (d) of this Section.
2)
When a container having a design capacity greater than 0.1 m
3
(26 gal)
is used for treatment of a hazardous waste by a waste stabilization
process, the owner or operator shall control air pollutant emissions from
the container in accordance with the Container Level 3 standards
specified in subsection (e) of this Section at those times during the waste
stabilization process when the hazardous waste in the container is
exposed to the atmosphere.
c)
Container Level 1 standards.
1)
A container using Container Level 1 controls is one of the following:
A)
A container that meets the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous
materials for transportation, as specified in subsection (f) of this
Section.
B)
A container equipped with a cover and closure devices that form
a continuous barrier over the container openings so that when the
cover and closure devices are secured in the closed position there
are no visible holes, gaps, or other open spaces into the interior
of the container. The cover may be a separate cover installed on
the container (e.g., a lid on a drum or a suitably secured tarp on
a roll-off box) or may be an integral part of the container
structural design (e.g., a “portable tank” or bulk cargo container
equipped with a screw-type cap).
235
C)
An open-top container in which an organic-vapor suppressing
barrier is placed on or over the hazardous waste in the container
such that no hazardous waste is exposed to the atmosphere. One
example of such a barrier is application of a suitable organic-
vapor suppressing foam.
2)
A container used to meet the requirements of subsection (c)(1)(B) or
(c)(1)(C) of this Section must be equipped with covers and closure
devices, as applicable to the container, that are composed of suitable
materials to minimize exposure of the hazardous waste to the atmosphere
and to maintain the equipment integrity, for as long as it is in service.
Factors to be considered in selecting the materials of construction and
designing the cover and closure devices must include the following: the
organic vapor permeability; the effects of contact with the hazardous
waste or its vapor managed in the container; the effects of outdoor
exposure of the closure device or cover material to wind, moisture, and
sunlight; and the operating practices for which the container is intended
to be used.
3)
Whenever a hazardous waste is in a container using Container Level 1
controls, the owner or operator shall install all covers and closure
devices for the container, as applicable to the container, and secure and
maintain each closure device in the closed position except as follows:
A)
Opening of a closure device or cover is allowed for the purpose
of adding hazardous waste or other material to the container as
follows:
i)
In the case when the container is filled to the intended
final level in one continuous operation, the owner or
operator shall promptly secure the closure devices in the
closed position and install the covers, as applicable to the
container, upon conclusion of the filling operation.
ii)
In the case when discrete quantities or batches of material
intermittently are added to the container over a period of
time, the owner or operator shall promptly secure the
closure devices in the closed position and install covers, as
applicable to the container, upon either the container
being filled to the intended final level; the completion of a
batch loading after which no additional material will be
added to the container within 15 minutes; the person
performing the loading operation leaving the immediate
vicinity of the container; or the shutdown of the process
236
generating the material being added to the container,
whichever condition occurs first.
B)
Opening of a closure device or cover is allowed for the purpose
of removing hazardous waste from the container as follows:
i)
For the purpose of meeting the requirements of this
Section, an empty container, as defined in 35 Ill. Adm.
Code 721.107(b), may be open to the atmosphere at any
time (i.e., covers and closure devices are not required to
be secured in the closed position on an empty container).
ii)
In the case when discrete quantities or batches of material
are removed from the container but the container does not
meet the conditions to be an empty container as defined in
35 Ill. Adm. Code 721.107(b), the owner or operator
shall promptly secure the closure devices in the closed
position and install covers, as applicable to the container,
upon the completion of a batch removal after which no
additional material will be removed from the container
within 15 minutes or the person performing the unloading
operation leaves the immediate vicinity of the container,
whichever condition occurs first.
C)
Opening of a closure device or cover is allowed when access
inside the container is needed to perform routine activities other
than transfer of hazardous waste. Examples of such activities
include those times when a worker needs to open a port to
measure the depth of or sample the material in the container, or
when a worker needs to open a manhole hatch to access
equipment inside the container. Following completion of the
activity, the owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as applicable
to the container.
D)
Opening of a spring-loaded pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the internal pressure of the container
in accordance with the container design specifications. The
device must be designed to operate with no detectable organic
emissions when the device is secured in the closed position. The
settings at which the device opens must be established such that
the device remains in the closed position whenever the internal
pressure of the container is within the internal pressure operating
237
range determined by the owner or operator based on container
manufacturer recommendations, applicable regulations, fire
protection and prevention codes, standard engineering codes and
practices, or other requirements for the safe handling of
flammable, ignitable, explosive, reactive, or hazardous
materials. Examples of normal operating conditions that may
require these devices to open are during those times when the
internal pressure of the container exceeds the internal pressure
operating range for the container as a result of loading operations
or diurnal ambient temperature fluctuations.
E)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 1 controls
shall inspect the containers and their covers and closure devices as
follows:
A)
In the case when a hazardous waste already is in the container at
the time the owner or operator first accepts possession of the
container at the facility and the container is not emptied (i.e.,
does not meet the conditions for an empty container as specified
in 35 Ill. Adm. Code 721.107(b)) within 24 hours after the
container is accepted at the facility (i.e., it does not meet the
conditions for an empty container as specified in 35 Ill. Adm.
Code 721.107(b)), the owner or operator shall visually inspect
the container and its cover and closure devices to check for
visible cracks, holes, gaps, or other open spaces into the interior
of the container when the cover and closure devices are secured
in the closed position. The container visual inspection must be
conducted on or before the date on which the container is accepted at
the facility (i.e., the date when the container becomes subject to the
Subpart CC container standards). For the purposes of this
requirement, the date of acceptance is the date of signature that the
facility owner or operator enters on Item 20 of the Uniform Hazardous
Waste Manifest incorporated by reference in 35 Ill. Adm. Code
722.Appendix A (USEPA Forms 8700-22 and 8700-22A), as required
under Section 724.171. If a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (c)(4)(C) of this Section.
B)
In the case when a container used for managing hazardous waste
remains at the facility for a period of one year or more, the
owner or operator shall visually inspect the container and its
cover and closure devices initially and thereafter, at least once
238
every 12 months, to check for visible cracks, holes, gaps, or
other open spaces into the interior of the container when the
cover and closure devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair the defect in
accordance with the requirements of subsection (c)(4)(C) of this
Section.
C)
When a defect is detected for the container, cover, or closure
devices, the owner or operator shall make first efforts at repair of
the defect no later than 24 hours after detection and repair must
be completed as soon as possible but no later than five calendar
days after detection. If repair of a defect cannot be completed
within five calendar days, then the hazardous waste must be
removed from the container and the container must not be used to
manage hazardous waste until the defect is repaired.
5)
The owner or operator shall maintain at the facility a copy of the
procedure used to determine that containers with capacity of 0.46 m
3
(120 gal) or greater, which do not meet applicable DOT regulations, as
specified in subsection (f) of this Section, are not managing hazardous
waste in light material service.
d)
Container Level 2 standards.
1)
A container using Container Level 2 controls is one of the following:
A)
A container that meets the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous
materials for transportation as specified in subsection (f) of this
Section.
B)
A container that operates with no detectable organic emissions, as
defined in 35 Ill. Adm. Code 725.981, and determined in
accordance with the procedure specified in subsection (g) of this
Section.
C)
A container that has been demonstrated within the preceding 12
months to be vapor-tight by using 40 CFR 60, appendix A,
Method 27, incorporated by reference in 35 Ill. Adm. Code
720.111, in accordance with the procedure specified in subsection
(h) of this Section.
2)
Transfer of hazardous waste in or out of a container using Container
Level 2 controls must be conducted in such a manner as to minimize
exposure of the hazardous waste to the atmosphere, to the extent
239
practical, considering the physical properties of the hazardous waste and
good engineering and safety practices for handling flammable, ignitable,
explosive, reactive, or other hazardous materials. Examples of container
loading procedures that the USEPA considers to meet the requirements
of this subsection (d)(2) include using any one of the following: a
submerged-fill pipe or other submerged-fill method to load liquids into
the container; a vapor-balancing system or a vapor-recovery system to
collect and control the vapors displaced from the container during filling
operations; or a fitted opening in the top of a container through which
the hazardous waste is filled and subsequently purging the transfer line
before removing it from the container opening.
3)
Whenever a hazardous waste is in a container using Container Level 2
controls, the owner or operator shall install all covers and closure
devices for the container, and secure and maintain each closure device in
the closed position, except as follows:
A)
Opening of a closure device or cover is allowed for the purpose
of adding hazardous waste or other material to the container as
follows:
i)
In the case when the container is filled to the intended
final level in one continuous operation, the owner or
operator shall promptly secure the closure devices in the
closed position and install the covers, as applicable to the
container, upon conclusion of the filling operation.
ii)
In the case when discrete quantities or batches of material
intermittently are added to the container over a period of
time, the owner or operator shall promptly secure the
closure devices in the closed position and install covers, as
applicable to the container, upon either the container
being filled to the intended final level; the completion of a
batch loading after which no additional material will be
added to the container within 15 minutes; the person
performing the loading operation leaving the immediate
vicinity of the container; or the shutdown of the process
generating the material being added to the container,
whichever condition occurs first.
B)
Opening of a closure device or cover is allowed for the purpose
of removing hazardous waste from the container as follows:
i)
For the purpose of meeting the requirements of this
Section, an empty container as defined in 35 Ill. Adm.
240
Code 721.107(b) may be open to the atmosphere at any
time (i.e., covers and closure devices are not required to
be secured in the closed position on an empty container).
ii)
In the case when discrete quantities or batches of material
are removed from the container but the container does not
meet the conditions to be an empty container as defined in
35 Ill. Adm. Code 721.107(b), the owner or operator
shall promptly secure the closure devices in the closed
position and install covers, as applicable to the container,
upon the completion of a batch removal after which no
additional material will be removed from the container
within 15 minutes or the person performing the unloading
operation leaves the immediate vicinity of the container,
whichever condition occurs first.
C)
Opening of a closure device or cover is allowed when access
inside the container is needed to perform routine activities other
than transfer of hazardous waste. Examples of such activities
include those times when a worker needs to open a port to
measure the depth of or sample the material in the container, or
when a worker needs to open a manhole hatch to access
equipment inside the container. Following completion of the
activity, the owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as applicable
to the container.
D)
Opening of a spring-loaded, pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the internal pressure of the container
in accordance with the container design specifications. The device
must be designed to operate with no detectable organic emission
when the device is secured in the closed position. The settings at
which the device opens must be established such that the device
remains in the closed position whenever the internal pressure of
the container is within the internal pressure operating range
determined by the owner or operator based on container
manufacturer recommendations, applicable regulations, fire
protection and prevention codes, standard engineering codes and
practices, or other requirements for the safe handling of
flammable, ignitable, explosive, reactive, or hazardous
materials. Examples of normal operating conditions that may
require these devices to open are during those times when the
internal pressure of the container exceeds the internal pressure
241
operating range for the container as a result of loading operations
or diurnal ambient temperature fluctuations.
E)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 2 controls
shall inspect the containers and their covers and closure devices as
follows:
A)
In the case when a hazardous waste already is in the container at
the time the owner or operator first accepts possession of the
container at the facility and the container is not emptied (i.e.,
does not meet the conditions for an empty container as specified
in 35 Ill. Adm. Code 721.107(b)) within 24 hours after the
container arrives is accepted at the facility (i.e., it does not meet
the conditions for an empty container as specified in 35 Ill. Adm.
Code 721.107(b)), the owner or operator shall visually inspect
the container and its cover and closure devices to check for
visible cracks, holes, gaps, or other open spaces into the interior
of the container when the cover and closure devices are secured
in the closed position. The container visual inspection must be
conducted on or before the date on which the container is accepted at
the facility (i.e., the date when the container becomes subject to the
Subpart CC container standards). For the purposes of this
requirement, the date of acceptance is the date of signature that the
facility owner or operator enters on Item 20 of the Uniform Hazardous
Waste Manifest incorporated by reference in the appendix to 40 CFR
262 (USEPA Forms 8700-22 and 8700-22A), as required under
Section 724.171. If a defect is detected, the owner or operator
shall repair the defect in accordance with the requirements of
subsection (d)(4)(C) of this Section.
B)
In the case when a container used for managing hazardous waste
remains at the facility for a period of one year or more, the
owner or operator shall visually inspect the container and its
cover and closure devices initially and thereafter, at least once
every 12 months, to check for visible cracks, holes, gaps, or
other open spaces into the interior of the container when the
cover and closure devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair the defect in
accordance with the requirements of subsection (d)(4)(C) of this
Section.
242
C)
When a defect is detected for the container, cover, or closure
devices, the owner or operator shall make first efforts at repair of
the defect no later than 24 hours after detection, and repair must
be completed as soon as possible but no later than five calendar
days after detection. If repair of a defect cannot be completed
within five calendar days, then the hazardous waste must be
removed from the container and the container must not be used to
manage hazardous waste until the defect is repaired.
e)
Container Level 3 standards.
1)
A container using Container Level 3 controls is one of the following:
A)
A container that is vented directly through a closed-vent system
to a control device in accordance with the requirements of
subsection (e)(2)(B) of this Section.
B)
A container that is vented inside an enclosure which is exhausted
through a closed-vent system to a control device in accordance
with the requirements of subsections (e)(2)(A) and (e)(2)(B) of
this Section.
2)
The owner or operator shall meet the following requirements, as
applicable to the type of air emission control equipment selected by the
owner or operator:
A)
The container enclosure must be designed and operated in
accordance with the criteria for a permanent total enclosure as
specified in “Procedure T--Criteria for and Verification of a
Permanent or Temporary Total Enclosure” under 40 CFR
52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of containers through
the enclosure by conveyor or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow
into the enclosure. The owner or operator shall perform the
verification procedure for the enclosure as specified in Section
5.0 to “Procedure T--Criteria for and Verification of a Permanent
or Temporary Total Enclosure” initially when the enclosure is
first installed and, thereafter, annually.
B)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 724.987.
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3)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may be
installed and operated as necessary on any container, enclosure, closed-
vent system, or control device used to comply with the requirements of
subsection (e)(1) of this Section.
4)
Owners and operators using Container Level 3 controls in accordance
with the provisions of this Subpart shall inspect and monitor the closed-
vent systems and control devices as specified in Section 724.987.
5)
Owners and operators that use Container Level 3 controls in accordance
with the provisions of this Subpart shall prepare and maintain the records
specified in Section 724.989(d).
f)
For the purpose of compliance with subsection (c)(1)(A) or (d)(1)(A) of this
Section, containers must be used that meet the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous materials for
transportation as follows:
1)
The container meets the applicable requirements specified in 49 CFR
178, “Specifications for Packaging”, or 49 CFR 179, “Specifications for
Tank Cars”, both incorporated by reference in 35 Ill. Adm. Code
720.111.
2)
Hazardous waste is managed in the container in accordance with the
applicable requirements specified in 49 CFR 107, Subpart B,
“Exemptions”; 49 CFR 172, “Hazardous Materials Table, Special
Provisions, Hazardous Materials Communications, Emergency Response
Information, and Training Requirements”; 49 CFR 173, “Shippers--
General Requirements for Shipments and Packages”; and 49 CFR 180,
“Continuing Qualification and Maintenance of Packagings”, each
incorporated by reference in 35 Ill. Adm. Code 720.111.
3)
For the purpose of complying with this Subpart, no exceptions to the 49
CFR 178 or 179 regulations are allowed, except as provided for in
subsection (f)(4) of this Section.
4)
For a lab pack that is managed in accordance with the requirements of
49 CFR 178, incorporated by reference in 35 Ill. Adm. Code 720.111,
for the purpose of complying with this Subpart, an owner or operator
may comply with the exceptions for combination packagings specified in
49 CFR 173.12(b).
g)
The owner or operator shall use the procedure specified in Section 724.983(d)
for determining a container operates To determine compliance with the no
detectable organic emissions for the purpose of complying with requirement of
244
subsection (d)(1)(B) of this Section, the procedure specified in Section 724.983(d)
must be used.
1)
Each potential leak interface (i.e., a location where organic vapor
leakage could occur) on the container, its cover, and associated closure
devices, as applicable to the container, must be checked. Potential leak
interfaces that are associated with containers include, but are not limited
to, the following: the interface of the cover rim and the container wall;
the periphery of any opening on the container or container cover and its
associated closure device; and the sealing seat interface on a spring-
loaded pressure-relief valve.
2)
The test must be performed when the container is filled with a material
having a volatile organic concentration representative of the range of
volatile organic concentrations for the hazardous wastes expected to be
managed in this type of container. During the test, the container cover
and closure devices must be secured in the closed position.
h)
Procedure for determining a container to be vapor-tight using Method 27 of 40
CFR 60, appendix A for the purpose of complying with subsection (d)(1)(C) of
this Section.
1)
The test must be performed in accordance with Method 27 of 40 CFR
60, appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111.
2)
A pressure measurement device must be used that has a precision of ±
2.5 mm (0.098 in) water and that is capable of measuring above the
pressure at which the container is to be tested for vapor tightness.
3)
If the test results determined by Method 27 indicate that the container
sustains a pressure change less than or equal to 750 Pascals (0.11 psig)
within five minutes after it is pressurized to a minimum of 4,500 Pascals
(0.65 psig), then the container is determined to be vapor-tight.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.987
Standards: Closed-vent Systems and Control Devices
a)
This Section applies to each closed-vent system and control device installed and
operated by the owner or operator to control air emissions in accordance with
standards of this Subpart.
b)
The closed-vent system shall meet the following requirements:
245
1)
The closed-vent system shall route the gases, vapors, and fumes emitted
from the hazardous waste in the waste management unit to a control
device that meets the requirements specified in subsection (c) of this
Section.
2)
The closed-vent system shall be designed and operated in accordance
with the requirements specified in Section 724.933(k).
3)
When the closed-vent system includes bypass devices that could be used
to divert the gas or vapor stream to the atmosphere before entering the
control device, each bypass device must be equipped with either a flow
indicator, as specified in subsection (b)(3)(A) of this Section, or a seal or
locking device, as specified in subsection (b)(3)(B) of this Section. For
the purpose of complying with this subsection, low leg drains, high point
bleeds, analyzer vents, open-ended valves or lines, spring-loaded
pressure-relief valves, and other fittings used for safety purposes are not
considered to be bypass devices.
A)
If a flow indicator is used to comply with this subsection (b)(3),
the indicator must be installed at the inlet to the bypass line used
to divert gases and vapors from the closed-vent system to the
atmosphere at a point upstream of the control device inlet. For
the purposes of this subsection, a flow indicator means a device
that indicates the presence of either gas or vapor flow in the
bypass line.
B)
If a seal or locking device is used to comply with subsection
(b)(3) of this Section, the device must be placed on the
mechanism by which the bypass device position is controlled
(e.g., valve handle or damper lever) when the bypass device is in
the closed position such that the bypass device cannot be opened
without breaking the seal or removing the lock. Examples of
such devices include, but are not limited to, a car-seal or a lock-
and-key configuration valve. The owner or operator shall
visually inspect the seal or closure mechanism at least once every
month to verify that the bypass mechanism is maintained in the
closed position.
4)
The closed-vent system must be inspected and monitored by the owner
or operator in accordance with the procedure specified in Section
724.933(l).
c)
The control device shall meet the following requirements:
1)
The control device shall be one of the following devices:
246
A)
A control device designed and operated to reduce the total
organic content of the inlet vapor stream vented to the control
device by at least 95% percent by weight;
B)
An enclosed combustion device designed and operated in
accordance with the requirements of Section 724.933(c); or
C)
A flare designed and operated in accordance with the
requirements of Section 724.933(d).
2)
The owner or operator that elects to use a closed-vent system and control
device to comply with the requirements of this Section shall comply with
the requirements specified in subsections (c)(2)(A) through (c)(2)(F) of
this Section.
A)
Periods of planned routine maintenance of the control device,
during which the control device does not meet the specifications
of subsections (c)(1)(A), (c)(1)(B), or (c)(1)(C) of this Section,
as applicable, must not exceed 240 hours per year.
B)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during periods of planned routine maintenance.
C)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during a control device system malfunction.
D)
The owner or operator shall demonstrate compliance with the
requirements of subsection (c)(2)(A) of this Section (i.e., planned
routine maintenance of a control device, during which the control
device does not meet the specifications of subsections (c)(1)(A),
(c)(1)(B), or (c)(1)(C) of this Section, as applicable, must not
exceed 240 hours per year) by recording the information
specified in Section 724.989(e)(1)(E).
E)
The owner or operator shall correct control device system
malfunctions as soon as practicable after their occurrence in order
to minimize excess emissions of air pollutants.
F)
The owner or operator shall operate the closed-vent system so
that gases, vapors, or fumes are not actively vented to the control
device during periods of planned maintenance or control device
system malfunction (i.e., periods when the control device is not
247
operating or not operating normally), except in cases when it is
necessary to vent the gases, vapors, or fumes to avoid an unsafe
condition or to implement malfunction corrective actions or
planned maintenance actions.
3)
The owner or operator using a carbon adsorption system to comply with
subsection (c)(1) of this Section shall operate and maintain the control
device in accordance with the following requirements:
A)
Following the initial startup of the control device, all activated
carbon in the control device shall be replaced with fresh carbon
on a regular basis in accordance with the requirements of Section
724.933(g) or Section 724.933(h).
B)
All carbon that is a hazardous waste and that is removed from the
control device shall must be managed in accordance with the
requirements of Section 724.933(n), regardless of the average
volatile organic concentration of the carbon.
4)
An owner or operator using a control device other than a thermal vapor
incinerator, flare, boiler, process heater, condenser, or carbon
adsorption system to comply with subsection (c)(1) of this Section shall
operate and maintain the control device in accordance with the
requirements of Section 724.933(j).
5)
The owner or operator shall demonstrate that a control device achieves
the performance requirements of subsection (c)(1) of this Section, as
follows:
A)
An owner or operator shall demonstrate using either a
performance test, as specified in subsection (c)(5)(C) of this
Section, or a design analysis, as specified in subsection (c)(5)(D)
of this Section, the performance of each control device except for
the following:
i)
A flare;
ii)
A boiler or process heater with a design heat input
capacity of 44 megawatts or greater;
iii)
A boiler or process heater into which the vent stream is
introduced with the primary fuel;
iv)
A boiler or industrial furnace burning hazardous waste for
which the owner or operator has been issued a final
248
permit under 35 Ill. Adm. Code 702, 703, and 705 and
has designed and operates the unit in accordance with the
interim status requirements of 35 Ill. Adm. Code
726.Subpart H; or
v)
A boiler or industrial furnace burning hazardous waste
that the owner or operator has designed and operates in
accordance with the interim status requirements of 35 Ill.
Adm. Code 726.Subpart H.
B)
An owner or operator shall demonstrate the performance of each
flare in accordance with the requirements specified in Section
724.933(e).
C)
For a performance test conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the owner or operator shall
use the test methods and procedures specified in Section
724.934(c)(1) through (c)(4).
D)
For a design analysis conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the design analysis shall
meet the requirements specified in Section 724.935(b)(4)(C).
E)
The owner or operator shall demonstrate that a carbon adsorption
system achieves the performance requirements of subsection
(c)(1) of this Section based on the total quantity of organics
vented to the atmosphere from all carbon adsorption system
equipment that is used for organic adsorption, organic desorption
or carbon regeneration, organic recovery, and carbon disposal.
6)
If the owner or operator and the Agency do not agree on a demonstration
of control device performance using a design analysis then the
disagreement shall be resolved using the results of a performance test
performed by the owner or operator in accordance with the requirements
of subsection (c)(5)(C) of this Section. The Agency may choose to have
an authorized representative observe the performance test.
7)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the procedures
specified in Section 724.933(f)(2) and (l). The readings from each
monitoring device required by Section 724.933(f)(2) must be inspected
at least once each operating day to check control device operation. Any
necessary corrective measures must be immediately implemented to
ensure the control device is operated in compliance with the
requirements of this Section.
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(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.989
Recordkeeping Requirements
a)
Each owner or operator of a facility subject to the requirements in of this
Subpart shall record and maintain the information specified in subsections (b)
through (i) (j) of this Section, as applicable to the facility. Except for air
emission control equipment design documentation and information required by
subsection subsections (i) and (j) of this Section, records required by this
Section must be maintained in the operating record for a minimum of three
years. Air emission control equipment design documentation must be
maintained in the operating record until the air emission control equipment is
replaced or is otherwise no longer in service. Information required by
subsection subsections (i) and (j) of this Section must be maintained in the
operating record for as long as the tank or container waste management unit is
not using air emission controls specified in Sections 724.984 through 724.987,
in accordance with the conditions specified in Section 724.984(d) or (b)(7),
respectively.
b)
The owner or operator of a tank using air emission controls in accordance with
the requirements of Section 724.984 shall prepare and maintain records for the
tank that include the following information:
1)
For each tank using air emission controls in accordance with the
requirements of Section 724.984, the owner or operator shall record:
A)
A tank identification number (or other unique identification
description as selected by the owner or operator).
B)
A record for each inspection required by Section 724.984 that
includes the following information:
i)
Date inspection was conducted.
ii)
For each defect detected during the inspection, the
following information: the location of the defect, a
description of the defect, the date of detection, and
corrective action taken to repair the defect. In the event
that repair of the defect is delayed in accordance with the
provisions requirements of Section 724.984, the owner or
operator shall also record the reason for the delay and the
date that completion of repair of the defect is expected.
250
2)
In addition to the information required by subsection (b)(1) of this
Section, the owner or operator shall record the following information, as
applicable to the tank:
A)
The owner or operator using a fixed roof to comply with the
Tank Level 1 control requirements specified in Section
724.984(c) shall prepare and maintain records for each
determination for the maximum organic vapor pressure of the
hazardous waste in the tank performed in accordance with the
requirements of Section 724.984(c). The records must include
the date and time the samples were collected, the analysis method
used, and the analysis results.
B)
The owner or operator using an internal floating roof to comply
with the Tank Level 2 control requirements specified in Section
724.984(e) shall prepare and maintain documentation describing
the floating roof design.
C)
Owners and operators using an external floating roof to comply
with the Tank Level 2 control requirements specified in Section
724.984(f) shall prepare and maintain the following records:
i)
Documentation describing the floating roof design and the
dimensions of the tank.
ii)
Records for each seal gap inspection required by Section
724.984(f)(3) describing the results of the seal gap
measurements. The records must include the date that the
measurements were performed, the raw data obtained for
the measurements, and the calculations of the total gap
surface area. In the event that the seal gap measurements
do not conform to the specifications in Section
724.984(f)(1), the records must include a description of
the repairs that were made, the date the repairs were
made, and the date the tank was emptied, if necessary.
D)
Each owner or operator using an enclosure to comply with the
Tank Level 2 control requirements specified in Section
724.984(i) shall prepare and maintain the following records:
i)
Records for the most recent set of calculations and
measurements performed by the owner or operator to
verify that the enclosure meets the criteria of a permanent
total enclosure as specified in “Procedure T--Criteria for
and Verification of a Permanent or Temporary Total
251
Enclosure” under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code 720.111.
ii)
Records required for the closed-vent system and control
device in accordance with the requirements of subsection
(e) of this Section.
c)
The owner or operator of a surface impoundment using air emission controls in
accordance with the requirements of Section 724.985 shall prepare and maintain
records for the surface impoundment that include the following information:
1)
A surface impoundment identification number (or other unique
identification description as selected by the owner or operator).
2)
Documentation describing the floating membrane cover or cover design,
as applicable to the surface impoundment, that includes information
prepared by the owner or operator or provided by the cover
manufacturer or vendor describing the cover design, and certification by
the owner or operator that the cover meets the specifications listed in
Section 724.985(c).
3)
A record for each inspection required by Section 724.985 that includes
the following information:
A)
Date inspection was conducted.
B)
For each defect detected during the inspection the following
information: the location of the defect, a description of the
defect, the date of detection, and corrective action taken to repair
the defect. In the event that repair of the defect is delayed in
accordance with the provisions of Section 724.985(f), the owner
or operator shall also record the reason for the delay and the date
that completion of repair of the defect is expected.
4)
For a surface impoundment equipped with a cover and vented through a
closed-vent system to a control device, the owner or operator shall
prepare and maintain the records specified in subsection (e).
d)
The owner or operator of containers using Container Level 3 air emission
controls in accordance with the requirements of Section 724.986 shall prepare
and maintain records that include the following information:
1)
Records for the most recent set of calculations and measurements
performed by the owner or operator to verify that the enclosure meets
the criteria of a permanent total enclosure as specified in “Procedure T--
252
Criteria for and Verification of a Permanent or Temporary Total
Enclosure” under 40 CFR 52.741, appendix B, incorporated by
reference in 35 Ill. Adm. Code 720.111.
2)
Records required for the closed-vent system and control device in
accordance with the requirements of subsection (e) of this Section.
e)
The owner or operator using a closed-vent system and control device in
accordance with the requirements of Section 724.987 shall prepare and maintain
records that include the following information:
1)
Documentation for the closed-vent system and control device that
includes:
A)
Certification that is signed and dated by the owner or operator
stating that the control device is designed to operate at the
performance level documented by a design analysis as specified
in subsection (e)(1)(B) of this Section or by performance tests as
specified in subsection (e)(1)(C) of this Section when the tank,
surface impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to occur.
B)
If a design analysis is used, then design documentation, as
specified in Section 724.935(b)(4). The documentation must
include information prepared by the owner or operator or
provided by the control device manufacturer or vendor that
describes the control device design in accordance with Section
724.935(b)(4)(C) and certification by the owner or operator that
the control equipment meets the applicable specifications.
C)
If performance tests are used, then a performance test plan as
specified in Section 724.935(b)(3) and all test results.
D)
Information as required by Section 724.935(c)(1) and Section
724.935(c)(2), as applicable.
E)
An owner or operator shall record, on a semiannual basis, the
information specified in subsections (e)(1)(E)(i) and (e)(1)(E)(ii)
of this Section for those planned routine maintenance operations
that would require the control device not to meet the
requirements of Section 724.987(c)(1)(A), (c)(1)(B), or (c)(1)(C)
of this Section, as applicable.
i)
A description of the planned routine maintenance that is
anticipated to be performed for the control device during
253
the next six-month period. This description must include
the type of maintenance necessary, planned frequency of
maintenance, and lengths of maintenance periods.
ii)
A description of the planned routine maintenance that was
performed for the control device during the previous six-
month period. This description must include the type of
maintenance performed and the total number of hours
during those six months that the control device did not
meet the requirements of Section 724.987(c)(1)(A),
(c)(1)(B), or (c)(1)(C), as applicable, due to planned
routine maintenance.
F)
An owner or operator shall record the information specified in
subsections (e)(1)(F)(i) through (e)(1)(F)(iii) of this Section for
those unexpected control device system malfunctions that would
require the control device not to meet the requirements of Section
724.987 (c)(1)(A), (c)(1)(B), or (c)(1)(C) of this Section, as
applicable.
i)
The occurrence and duration of each malfunction of the
control device system.
ii)
The duration of each period during a malfunction when
gases, vapors, or fumes are vented from the waste
management unit through the closed-vent system to the
control device while the control device is not properly
functioning.
iii)
Actions taken during periods of malfunction to restore a
malfunctioning control device to its normal or usual
manner of operation.
G)
Records of the management of carbon removed from a carbon
adsorption system conducted in accordance with Section
724.987(c)(3)(B).
f)
The owner or operator of a tank, surface impoundment, or container exempted
from standards in accordance with the provisions of Section 724.982(c) shall
prepare and maintain the following records, as applicable:
1)
For tanks, surface impoundments, or containers exempted under the
hazardous waste organic concentration conditions specified in Section
724.982(c)(1) or (c)(2)(A) through (c)(2)(E), the owner or operator shall
record the information used for each waste determination (e.g., test
254
results, measurements, calculations, and other documentation) in the
facility operating log. If analysis results for waste samples are used for
the waste determination, then the owner or operator shall record the
date, time, and location that each waste sample is collected in
accordance with the applicable requirements of Section 724.983.
2)
For tanks, surface impoundments, or containers exempted under the
provisions of Section 724.982(c)(2)(G) or (c)(2)(H), the owner or
operator shall record the identification number for the incinerator,
boiler, or industrial furnace in which the hazardous waste is treated.
g)
An owner or operator designating a cover as “unsafe to inspect and monitor”
pursuant to Section 724.984(l) or Section 724.985(g) shall record in a log that is
kept in the facility operating record the following information: the
identification numbers for waste management units with covers that are
designated as “unsafe to inspect and monitor”, the explanation for each cover
stating why the cover is unsafe to inspect and monitor, and the plan and
schedule for inspecting and monitoring each cover.
h)
The owner or operator of a facility that is subject to this Subpart and to the
control device standards in 40 CFR 60, Subpart VV or 40 CFR 61, Subpart V,
incorporated by reference in 35 Ill. Adm. Code 720.111, may elect to
demonstrate compliance with the applicable Sections of this Subpart by
documentation either pursuant to this Subpart, or pursuant to the provisions of
40 CFR 60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
documentation required by 40 CFR 60 or 61 duplicates the documentation
required by this Section.
i)
For each tank or container not using air emission controls specified in Sections
724.984 through 724.987 in accordance with the conditions specified in Section
724.980(d), the owner or operator shall record and maintain the following
information:
1)
A list of the individual organic peroxide compounds manufactured at the
facility that meet the conditions specified in Section 724.980(d)(1).
2)
A description of how the hazardous waste containing the organic
peroxide compounds identified pursuant to subsection (i)(1) of this
Section are managed at the facility in tanks and containers. This
description must include the following information:
A)
For the tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to describe the following
for each tank: a facility identification number for the tank, the
purpose and placement of this tank in the management train of
255
this hazardous waste, and the procedures used to ultimately
dispose of the hazardous waste managed in the tanks.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to describe each
tank: a facility identification number for the container or group
of containers, the purpose and placement of this container or
group of containers in the management train of this hazardous
waste, and the procedures used to ultimately dispose of the
hazardous waste managed in the containers.
3)
An explanation of why managing the hazardous waste containing the
organic peroxide compounds identified pursuant to subsection (i)(1) of
this Section in the tanks or containers identified pursuant to subsection
(i)(2) of this Section would create an undue safety hazard if the air
emission controls specified in Sections 724.984 through 724.987 were
installed and operated on these waste management units. This
explanation must include the following information:
A)
For tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to explain the following:
how use of the required air emission controls on the tanks would
affect the tank design features and facility operating procedures
currently used to prevent an undue safety hazard during
management of this hazardous waste in the tanks; and why
installation of safety devices on the required air emission
controls, as allowed under this Subpart, would not address those
situations in which evacuation of tanks equipped with these air
emission controls is necessary and consistent with good
engineering and safety practices for handling organic peroxides.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to explain the
following: how use of the required air emission controls on the
tanks would affect the container design features and handling
procedures currently used to prevent an undue safety hazard
during management of this hazardous waste in the containers; and
why installation of safety devices on the required air emission
controls, as allowed under this Subpart, would not address those
situations in which evacuation of containers equipped with these
air emission controls is necessary and consistent with good
engineering and safety practices for handling organic peroxides.
j)
For each hazardous waste management unit not using air emission controls
specified in Sections 724.984 through 724.987 in accordance with the requirements
256
of Section 724.980(b)(7), the owner and operator shall record and maintain the
following information:
1)
The certification that the waste management unit is equipped with and
operating air emission controls in accordance with the requirements of an
applicable federal Clean Air Act regulation codified under 40 CFR 60, 61, or
63.
2)
An identification of the specific federal requirements codified under 40 CFR
60, 61, or 63 with which the waste management unit is in compliance.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 725
INTERIM STATUS STANDARDS FOR OWNERS AND OPERATORS OF
HAZARDOUS WASTE TREATMENT, STORAGE, AND DISPOSAL
FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
725.101
Purpose, Scope and Applicability
725.104
Imminent Hazard Action
SUBPART B: GENERAL FACILITY STANDARDS
Section
725.110
Applicability
725.111
USEPA Identification Number
725.112
Required Notices
725.113
General Waste Analysis
725.114
Security
725.115
General Inspection Requirements
725.116
Personnel Training
725.117
General Requirements for Ignitable, Reactive, or Incompatible Wastes
725.118
Location Standards
725.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
725.130
Applicability
725.131
Maintenance and Operation of Facility
725.132
Required Equipment
257
725.133
Testing and Maintenance of Equipment
725.134
Access to Communications or Alarm System
725.135
Required Aisle Space
725.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
725.150
Applicability
725.151
Purpose and Implementation of Contingency Plan
725.152
Content of Contingency Plan
725.153
Copies of Contingency Plan
725.154
Amendment of Contingency Plan
725.155
Emergency Coordinator
725.156
Emergency Procedures
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND
REPORTING
Section
725.170
Applicability
725.171
Use of Manifest System
725.172
Manifest Discrepancies
725.173
Operating Record
725.174
Availability, Retention and Disposition of Records
725.175
Annual Report
725.176
Unmanifested Waste Report
725.177
Additional Reports
SUBPART F: GROUNDWATER MONITORING
Section
725.190
Applicability
725.191
Groundwater Monitoring System
725.192
Sampling and Analysis
725.193
Preparation, Evaluation and Response
725.194
Recordkeeping and Reporting
SUBPART G: CLOSURE AND POST-CLOSURE
Section
725.210
Applicability
725.211
Closure Performance Standard
725.212
Closure Plan; Amendment of Plan
725.213
Closure; Time Allowed for Closure
725.214
Disposal or Decontamination of Equipment, Structures and Soils
725.215
Certification of Closure
725.216
Survey Plat
725.217
Post-closure Care and Use of Property
258
725.218
Post-closure Plan; Amendment of Plan
725.219
Post-Closure Notices
725.220
Certification of Completion of Post-Closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
725.240
Applicability
725.241
Definitions of Terms as Used in this Subpart
725.242
Cost Estimate for Closure
725.243
Financial Assurance for Closure
725.244
Cost Estimate for Post-closure Care
725.245
Financial Assurance for Post-closure Monitoring and Maintenance
725.246
Use of a Mechanism for Financial Assurance of Both Closure and Post-closure
Care
725.247
Liability Requirements
725.248
Incapacity of Owners or Operators, Guarantors or Financial Institutions
725.251
Promulgation of Forms (Repealed)
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
725.270
Applicability
725.271
Condition of Containers
725.272
Compatibility of Waste with Container
725.273
Management of Containers
725.274
Inspections
725.276
Special Requirements for Ignitable or Reactive Waste
725.277
Special Requirements for Incompatible Wastes
725.278
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
725.290
Applicability
725.291
Assessment of Existing Tank System’s Integrity
725.292
Design and Installation of New Tank Systems or Components
725.293
Containment and Detection of Releases
725.294
General Operating Requirements
725.295
Inspections
725.296
Response to leaks or spills and disposition of Tank Systems
725.297
Closure and Post-Closure Care
725.298
Special Requirements for Ignitable or Reactive Waste
725.299
Special Requirements for Incompatible Wastes
725.300
Waste Analysis and Trial Tests
725.301
Generators of 100 to 1000 Kilograms of Hazardous Waste Per Month
725.302
Air Emission Standards
259
SUBPART K: SURFACE IMPOUNDMENTS
Section
725.320
Applicability
725.321
Design and Operating Requirements
725.322
Action Leakage Rate
725.323
Response Actions
725.324
Containment System
725.325
Waste Analysis and Trial Tests
725.326
Monitoring and Inspections
725.328
Closure and Post-closure Care
725.329
Special Requirements for Ignitable or Reactive Waste
725.330
Special Requirements for Incompatible Wastes
725.331
Air Emission Standards
SUBPART L: WASTE PILES
Section
725.350
Applicability
725.351
Protection from Wind
725.352
Waste Analysis
725.353
Containment
725.354
Design and Operating Requirements
725.355
Action Leakage Rates
725.356
Special Requirements for Ignitable or Reactive Waste
725.357
Special Requirements for Incompatible Wastes
725.358
Closure and Post-closure Care
725.359
Response Actions
725.360
Monitoring and Inspection
SUBPART M: LAND TREATMENT
Section
725.370
Applicability
725.372
General Operating Requirements
725.373
Waste Analysis
725.376
Food Chain Crops
725.378
Unsaturated Zone (Zone of Aeration) Monitoring
725.379
Recordkeeping
725.380
Closure and Post-closure
725.381
Special Requirements for Ignitable or Reactive Waste
725.382
Special Requirements for Incompatible Wastes
SUBPART N: LANDFILLS
Section
725.400
Applicability
725.401
Design Requirements
725.402
Action Leakage Rate
260
725.403
Response Actions
725.404
Monitoring and Inspection
725.409
Surveying and Recordkeeping
725.410
Closure and Post-closure
725.412
Special Requirements for Ignitable or Reactive Waste
725.413
Special Requirements for Incompatible Wastes
725.414
Special Requirements for Liquid Wastes
725.415
Special Requirements for Containers
725.416
Disposal of Small Containers of Hazardous Waste in Overpacked Drums (Lab
Packs)
SUBPART O: INCINERATORS
Section
725.440
Applicability
725.441
Waste Analysis
725.445
General Operating Requirements
725.447
Monitoring and Inspection
725.451
Closure
725.452
Interim Status Incinerators Burning Particular Hazardous Wastes
SUBPART P: THERMAL TREATMENT
Section
725.470
Other Thermal Treatment
725.473
General Operating Requirements
725.475
Waste Analysis
725.477
Monitoring and Inspections
725.481
Closure
725.482
Open Burning; Waste Explosives
725.483
Interim Status Thermal Treatment Devices Burning Particular Hazardous Waste
SUBPART Q: CHEMICAL, PHYSICAL AND BIOLOGICAL TREATMENT
Section
725.500
Applicability
725.501
General Operating Requirements
725.502
Waste Analysis and Trial Tests
725.503
Inspections
725.504
Closure
725.505
Special Requirements for Ignitable or Reactive Waste
725.506
Special Requirements for Incompatible Wastes
SUBPART R: UNDERGROUND INJECTION
Section
725.530
Applicability
261
SUBPART W: DRIP PADS
Section
725.540
Applicability
725.541
Assessment of existing drip pad integrity
725.542
Design and installation of new drip pads
725.543
Design and operating requirements
725.544
Inspections
725.545
Closure
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
725.930
Applicability
725.931
Definitions
725.932
Standards: Process Vents
725.933
Standards: Closed-Vent Systems and Control Devices
725.934
Test methods and procedures
725.935
Recordkeeping Requirements
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
725.950
Applicability
725.951
Definitions
725.952
Standards: Pumps in Light Liquid Service
725.953
Standards: Compressors
725.954
Standards: Pressure Relief Devices in Gas/Vapor Service
725.955
Standards: Sampling Connecting Systems
725.956
Standards: Open-ended Valves or Lines
725.957
Standards: Valves in Gas/Vapor or Light Liquid Service
725.958
Standards: Pumps, Valves, Pressure Relief Devices, Flanges and other
Connectors
725.959
Standards: Delay of Repair
725.960
Standards: Closed-vent Systems and Control Devices
725.961
Percent Leakage Alternative for Valves
725.962
Skip Period Alternative for Valves
725.963
Test Methods and Procedures
725.964
Recordkeeping Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section
725.980
Applicability
725.981
Definitions
725.982
Schedule for Implementation of Air Emission Standards
725.983
Standards: General
725.984
Waste Determination Procedures
262
725.985
Standards: Tanks
725.986
Standards: Surface Impoundments
725.987
Standards: Containers
725.988
Standards: Closed-Vent Systems and Control Devices
725.989
Inspection and Monitoring Requirements
725.990
Recordkeeping Requirements
725.991
Alternative Tank Emission Control Requirements (Repealed)
SUBPART DD: CONTAINMENT BUILDINGS
Section
725.1100
Applicability
725.1101
Design and operating standards
725.1102
Closure and Post Closure-Care
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section
725.1200
Applicability
725.1201
Design and Operating Standards
725.1202
Closure and Post-Closure Care
725.Appendix A
Recordkeeping Instructions
725.Appendix B
EPA Report Form and Instructions (Repealed)
725.Appendix C
EPA Interim Primary Drinking Water Standards
725.Appendix D
Tests for Significance
725.Appendix E
Examples of Potentially Incompatible Waste
725.Appendix F
Compounds With Henry’s Law Constant Less Than 0.1 Y/X (at 25°C)
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982; amended
and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982; amended in R82-18,
51 PCB 831, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in R82-19, 53 PCB 131, at 7
Ill. Reg. 14034, effective October 12, 1983; amended in R84-9, at 9 Ill. Reg. 11869, effective July 24,
1985; amended in R85-22 at 10 Ill. Reg. 1085, effective January 2, 1986; amended in R86-1 at 10 Ill.
Reg. 14069, effective August 12, 1986; amended in R86-28 at 11 Ill. Reg. 6044, effective March 24,
1987; amended in R86-46 at 11 Ill. Reg. 13489, effective August 4, 1987; amended in R87-5 at 11 Ill.
Reg. 19338, effective November 10, 1987; amended in R87-26 at 12 Ill. Reg. 2485, effective January
15, 1988; amended in R87-39 at 12 Ill. Reg. 13027, effective July 29, 1988; amended in R88-16 at 13
Ill. Reg. 437, effective December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18354, effective
November 13, 1989; amended in R90-2 at 14 Ill. Reg. 14447, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16498, effective September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9398,
effective June 17, 1991; amended in R91-1 at 15 Ill. Reg. 14534, effective October 1, 1991;
amended in R91-13 at 16 Ill. Reg. 9578, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg.
17672, effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5681, effective March 26,
1993; amended in R93-4 at 17 Ill. Reg. 20620, effective November 22, 1993; amended in R93-16 at
18 Ill. Reg. 6771, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg. 12190, effective July 29,
263
1994; amended in R94-17 at 18 Ill. Reg. 17548, effective November 23, 1994; amended in R95-6 at
19 Ill. Reg. 9566, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11078, effective August
1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 369, effective December 16, 1997;
amended in R98-12 at 22 Ill. Reg. 7620, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at
22 Ill. Reg. 17620, effective September 28, 1998; amended in R98-21/R99-2/R99-7 at 22 Ill. Reg.
________, effective ______________________.
SUBPART B: GENERAL FACILITY STANDARDS
Section 725.115
General Inspection Requirements
a)
The owner or operator shall inspect the facility for malfunctions and
deterioration, operator errors and discharges that may be causing—or may lead
to—the conditions listed below. The owner or operator shall conduct these
inspections often enough to identify problems in time to correct them before
they harm human health or the environment.
1)
Release of hazardous waste constituents to the environment, or
2)
A threat to human health.
b)
Written schedule.
1)
The owner or operator shall develop and follow a written schedule for
inspecting all monitoring equipment, safety and emergency equipment,
security devices, and operating and structural equipment (such as dikes
and sump pumps) that are important to preventing, detecting, or
responding to environmental or human health hazards.
2)
The owner or operator shall keep this schedule at the facility.
3)
The schedule must identify the types of problems (e.g., malfunctions or
deterioration) that are to be looked for during the inspection (e.g.,
inoperative sump pump, leaking fitting, eroding dike, etc.).
4)
The frequency of inspection may vary for the items on the schedule.
However, it the frequency should be based on the rate of deterioration of
the equipment and the probability of an environmental or human health
incident if the deterioration, malfunction, or any operator error goes
undetected between inspections. Areas subject to spills, such as loading
and unloading areas, must be inspected daily when in use. At a
minimum, the inspection schedule must include the items and
frequencies called for in Sections 725.274, 725.293, 725.295, 725.326,
725.360, 725.378, 725.404, 725.447, 725.477, 725.503, 725.933,
264
725.952, 725.953, 725.958, 725.989, and 725.991(b) 725.984 through
725.990, where applicable.
c)
The owner or operator shall remedy any deterioration or malfunction of
equipment or structure that the inspection reveals on a schedule which ensures
that the problem does not lead to an environmental or human health hazard.
Where a hazard is imminent or has already occurred, remedial action must be
taken immediately.
d)
The owner or operator shall record inspections in an inspection log or
summary. The owner or operator shall keep these records for at least three
years from the date of inspection. At a minimum, these records must include
the date and time of the inspection, the name of the inspector, a notation of the
observations made and the date, and nature of any repairs or other remedial
actions.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 725.173
Operating Record
a)
The owner or operator shall keep a written operating record at the facility.
b)
The following information must be recorded as it becomes available and
maintained in the operating record until closure of the facility.
1)
A description and the quantity of each hazardous waste received and the
method or methods and date or dates of its treatment, storage, or
disposal at the facility as required by Section 725.Appendix A;
2)
The location of each hazardous waste within the facility and the quantity
at each location. For disposal facilities the location and quantity of each
hazardous waste must be recorded on a map or diagram of each cell or
disposal area. For all facilities this information must include cross-
references to specific manifest document numbers if the waste was
accompanied by a manifest;
BOARD NOTE: See Sections 725.219, 725.379, and 725.409 for
related requirements.
3)
Records and results of waste analysis, waste determinations, and trial
tests performed as specified in Sections 725.113, 725.300, 725.325,
265
725.352, 725.373, 725.414, 725.441, 725.475, 725.502, 725.934,
725.963, and 725.984 and 35 Ill. Adm. Code 728.104(a) and 728.107;
4)
Summary reports and details of all incidents that require implementing
the contingency plan as specified in Section 725.156(j);
5)
Records and results of inspections as required by Sections 725.115(d)
(except these data need be kept only three years);
6)
Monitoring, testing, or analytical data where required by 725.Subpart F
of this Part or Sections 725.119, 725.190, 725.194, 725.291, 725.293,
725.295, 725.322, 725.323, 725.326, 725.355, 725.359, 725.360,
725.376, 725.378, 725.380(d)(1), 725.402 through 725.404, 725.447,
725.477, 725.934(c) through (f), 725.935, 725.963(d) through (i), or
725.964, and 725.989 725.1083 through 725.991 725.990;
BOARD NOTE: As required by Section 725.194, monitoring data at
disposal facilities must be kept throughout the post-closure period.
7)
All closure cost estimates under Section 725.242 and, for disposal
facilities, all post-closure cost estimates under Section 725.244;
8)
Records of the quantities (and date of placement) for each shipment of
hazardous waste placed in land disposal units under an extension of the
effective date of any land disposal restriction granted pursuant to 35 Ill.
Adm. Code 728.105, a petition pursuant to 35 Ill. Adm. Code 728.106,
or a certification under 35 Ill. Adm. Code 728.108 and the applicable
notice required of a generator under 35 Ill. Adm. Code 728.107(a);
9)
For an off-site treatment facility, a copy of the notice and the
certification and demonstration, if applicable, required of the generator
or the owner or operator under 35 Ill. Adm. Code 728.107 or 728.108;
10)
For an on-site treatment facility, the information contained in the notice
(except the manifest number) and the certification and demonstration, if
applicable, required of the generator or the owner or operator under 35
Ill. Adm. Code 728.107 or 728.108;
11)
For an off-site land disposal facility, a copy of the notice and the
certification and demonstration, if applicable, required of the generator
or the owner or operator of a treatment facility under 35 Ill. Adm. Code
728.107 or 728.108;
12)
For an on-site land disposal facility, the information contained in the
notice required of the generator or owner or operator of a treatment
266
facility under 35 Ill. Adm. Code 728.107, except for the manifest
number, and the certification and demonstration, if applicable, required
under 35 Ill. Adm. Code 728.107 or 728.108;
13)
For an off-site storage facility, a copy of the notice and the certification
and demonstration, if applicable, required of the generator or the owner
or operator under 35 Ill. Adm. Code 728.107 or 728.108; and
14)
For an on-site storage facility, the information contained in the notice
(except the manifest number) and the certification and demonstration, if
applicable, required of the generator or the owner or operator under 35
Ill. Adm. Code 728.107 or 728.108.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART J: TANK SYSTEMS
Section 725.302
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a tank in accordance with
the requirements of 724.Subparts AA, BB, and CC of this Part.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 725.930
Applicability
a)
This Subpart applies to owners and operators of facilities that treat, store or
dispose of hazardous wastes (except as provided in Section 725.101).
b)
Except for Section 725.934(d) and (e), this Subpart applies to process vents
associated with distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operations that manage hazardous wastes
with organic concentrations of at least 10 ppmw (parts per million by weight), if
these operations are conducted in one of the following:
1)
A unit that is subject to the permitting requirements of 35 Ill. Adm.
Code 702, 703, and 705; or
2)
A unit (including a hazardous waste recycling unit) that is not exempt
from permitting under the provisions of 35 Ill. Adm. Code 262.34(a)
722.134(a) (i.e., a hazardous waste recycling unit that is not a 90-day
267
tank or container) and that is located on a hazardous waste management
facility otherwise subject to the permitting requirements of 35 Ill. Adm.
Code 702, 703, and 705.; or
3)
A unit that is exempt from permitting under the provisions of 35 Ill. Adm.
Code 722.134(a) (i.e., a “90-day” tank or container) and which is not a
recycling unit under the requirements of 35 Ill. Adm. Code 721.106.
BOARD NOTE: The requirements of Sections 725.932 through 725.936 apply
to process vents on hazardous waste recycling units previously exempt under 35
Ill. Adm. Code 721.106(c)(1). Other exemptions under 35 Ill. Adm. Code
721.104 and 725.101(c) are not affected by these requirements.
c)
Agency decisions pursuant to this Part must be made in writing, are in the
nature of permit decisions pursuant to Section 39 of the Environmental
Protection Act and may be appealed to the Board pursuant to 35 Ill. Adm. Code
105.
d)
The requirements of this Subpart do not apply to the process vents at a facility where
the facility owner or operator certifies that all of the process vents which would
otherwise be subject to this Subpart are equipped with and operating air emission
controls in accordance with the process vent requirements of an applicable federal
Clean Air Act regulation codified under 40 CFR 60, 61, or 63. The documentation of
compliance under regulations at 40 CFR 60, 61, or 63 must be kept with, or made
readily available with, the facility operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.933
Standards: Closed-Vent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control devices used to
comply with provisions of this Part shall comply with the provisions of
this Section.
2)
Implementation Schedule.
A)
The owner or operator of an existing facility that cannot install a
closed-vent system and control device to comply with the
provisions of this Subpart on the effective date that the facility
becomes subject to the provisions of this Subpart shall prepare an
implementation schedule that includes dates by which the closed-
vent system and control device will be installed and in operation.
The controls must be installed as soon as possible, but the
implementation schedule may allow up to 30 months after the
268
effective date that the facility becomes subject to this Subpart for
installation and startup.
B)
All units Any unit that begin begins operation after December 21,
1990, and which is subject to the provisions of this Subpart when
operation begins, must comply with the rules immediately (i.e.,
must have control devices installed and operating on startup of
the affected unit); the 2-year 30-month implementation schedule
does not apply to these units.
C)
The owner or operator of any facility in existence on the effective date
of a statutory or regulatory amendment that renders the facility
subject to this Subpart shall comply with all requirements of this
Subpart as soon as practicable but no later than 30 months after the
effective date of the amendment. When control equipment required
by this Subpart can not be installed and begin operation by the
effective date of the amendment, the facility owner or operator shall
prepare an implementation schedule that includes the following
information: Specific calendar dates for award of contracts or
issuance of purchase orders for the control equipment, initiation of
on-site installation of the control equipment, completion of the control
equipment installation, and performance of any testing to
demonstrate that the installed equipment meets the applicable
standards of this Subpart. The owner or operator shall enter the
implementation schedule in the operating record or in a permanent,
readily available file located at the facility.
D)
An owner or operator of a facility or unit that becomes newly subject
to the requirements of this Subpart after December 8, 1997, due to an
action other than those described in subsection (a)(2)(iii) of this
Section must comply with all applicable requirements immediately
(i.e., the facility or unit must have control devices installed and
operating on the date the facility or unit becomes subject to this
Subpart; the 30-month implementation schedule does not apply).
b)
A control device involving vapor recovery (e.g., a condenser or adsorber) must
be designed and operated to recover the organic vapors vented to it with an
efficiency of 95 weight percent or greater unless the total organic emission
limits of Section 725.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler, or process
heater) must be designed and operated to reduce the organic emissions vented to
it by 95 weight percent or greater; to achieve a total organic compound
concentration of 20 ppmv, expressed as the sum of the actual compounds, not
carbon equivalents, on a dry basis corrected to three percent oxygen; or to
provide a minimum residence time of 0.50 seconds at a minimum temperature
of 760 degrees Celsius (° C). If a boiler or process heater is used as the control
269
device, then the vent stream must be introduced into the flame combustion zone
of the boiler or process heater.
d)
Flares.
1)
A flare must be designed for and operated with no visible emissions as
determined by the methods specified in subsection (e)(1) of this Section
except for periods not to exceed a total of 5 minutes during any 2
consecutive hours.
2)
A flare must be operated with a flame present at all times, as determined
by the methods specified in subsection (f)(2)(c) of this Section.
3)
A flare must be used only if the net heating value of the gas being
combusted is 11.2 MJ/scm (300 Btu/scf) or greater if the flare is steam-
assisted or air-assisted, or if the net heating value of the gas being
combusted is 7.45 MJ/scm (200 Btu/scf) or greater if the flare is
nonassisted. The net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2) of this Section.
4)
Exit Velocity.
A)
A steam-assisted or nonassisted flare must be designed for and
operated with an exit velocity, as determined by the methods
specified in subsection (e)(3) of this Section, less than 18.3 m/s
(60 ft/s), except as provided in subsections (d)(4)(B) and
(d)(4)(C) of this Section.
B)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, equal to or greater than 18.3
m/s (60 ft/s) but less than 122 m/s (400 ft/s) is allowed if the net
heating value of the gas being combusted is greater than 37.3
MJ/scm (1000 Btu/scf).
C)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, less than the velocity, V as
determined by the method specified in subsection (e)(4) and less
than 122 m/s (400 ft/s) is allowed.
5)
An air-assisted flare must be designed and operated with an exit velocity
less than the velocity, V as determined by the method specified in
subsection (e)(5) of this Section.
270
6)
A flare used to comply with this Section must be steam-assisted, air-
assisted, or nonassisted.
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be used to determine the compliance of a
flare with the visible emission provisions of this Subpart. The
observation period is 2 hours and must be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare must be
calculated using the following equation:
T
ii
i1
n
H
=K×
C
×H
=
∑
Where:
HT is the net heating value of the sample in MJ/scm; where the
net enthalpy per mole of offgas is based on combustion at 25° C
and 760 mm Hg, but the standard temperature for determining
the volume corrersponding to 1 mole is 20° C.
K = 1.74×10
-7
(1/ppm)(g mol/scm)(MJ/kcal) where the standard
temperature for (g mol/scm) is 20° C.
ΣX
i means the sum of the values of X for each component i,
from i=1 to n.
Ci is the concentration of sample component i in ppm on a wet
basis, as measured for organics by Reference Method 18 in 40
CFR 60, and for carbon monoxide, by ASTM D 1946-90,
incorporated by reference in 35 Ill. Adm. Code 720.111.
Hi is the net heat of combustion of sample component i,
kcal/gmol at 25° C and 760 mm Hg. The heats of combustion
must be determined using ASTM D 2382-88, incorporated by
reference in 35 Ill. Adm. Code 720.111, if published values are
not available or cannot be calculated.
3)
The actual exit velocity of a flare must be determined by dividing the
volumetric flow rate (in units of standard temperature and pressure), as
determined by Reference Methods 2, 2A, 2C, or 2D in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111, as appropriate,
by the unobstructed (free) cross-sectional area of the flare tip.
271
4)
The maximum allowed velocity in m/s, V for a flare complying with
subsection (d)(4)(C) of this Section must be determined by the following
equation:
log
(
V
)
H
28.8
10
max
31.7
T
=
+
log
(
V
)
H
28.8
10
max
31.7
T
=
+
Where:
log10 means logarithm to the base 10
HT is the net heating value as determined in subsection (e)(2) of
this Section.
5)
The maximum allowed velocity in m/s, V for an air-assisted flare must
be determined by the following equation:
Where:
HT is the net heating value as determined in subsection (e)(2) of
this Section.
f)
The owner or operator shall monitor and inspect each control device required to
comply with this Section to ensure proper operation and maintenance of the
control device by implementing the following requirements:
1)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a flow indicator that provides a record of vent stream flow
from each affected process vent to the control device at least once every
hour. The flow indicator sensor must be installed in the vent stream at
the nearest feasible point to the control device inlet but before being
combined with other vent streams.
V = 8.706 + 0.7084
H
T
272
2)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a device to continuously monitor control device operation
as specified below:
A)
For a thermal vapor incinerator, a temperature monitoring device
equipped with a continuous recorder. The device must have
accuracy of ±1 percent of the temperature being monitored in °
C or ± 0.5° C, whichever is greater. The temperature sensor
must be installed at a location in the combustion chamber
downstream of the combustion zone.
B)
For a catalytic vapor incinerator, a temperature monitoring
device equipped with a continuous recorder. The device must be
capable of monitoring temperature at two locations and have an
accuracy of ±1 percent of the temperature being monitored in °
C or ± 0.5° C, whichever is greater. One temperature sensor
must be installed in the vent stream at the nearest feasible point to
the catalyst bed inlet and a second temperature sensor must be
installed in the vent stream at the nearest feasible point to the
catalyst bed outlet.
C)
For a flare, a heat sensing monitoring device equipped with a
continuous recorder that indicates the continuous ignition of the
pilot flame.
D)
For a boiler or process heater having a design heat input capacity
less than 44 MW, a temperature monitoring device equipped with
a continuous recorder. The device must have an accuracy of ±1
percent of the temperature being monitored in ° C or ± 0.5° C,
whichever is greater. The temperature sensor must be installed at
a location in the furnace downstream of the combustion zone.
E)
For a boiler or process heater having a design heat input capacity
greater than or equal to 44 MW, a monitoring device equipped
with a continuous recorder to measure parameters that indicate
good combustion operating practices are being used.
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the
condenser; or
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ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable of
monitoring temperature with an accuracy of ±1 percent of
the temperature being monitored in degrees Celsius (° C)
or ±0.5° C, whichever is greater. The temperature
sensor must be installed at a location in the exhaust vent
stream from the condenser exit (i.e., product side).
G)
For a carbon adsorption system such as a fixed-bed carbon
adsorber that regenerates the carbon bed directly in the control
device, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the carbon
bed; or
ii)
A monitoring device equipped with a continuous recorder
to measure a parameter that indicates the carbon bed is
regenerated on a regular, predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsections (f)(1) and (f)(2) of this Section at least once each operating
day to check control device operation and, if necessary, immediately
implement the corrective measures necessary to ensure the control device
operates in compliance with the requirements of this Section.
g)
An owner or operator using a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
at a regular, predetermined time interval that is no longer than the carbon
service life established as a requirement of Section 725.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system, such as a carbon
canister, that does not regenerate the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
on a regular basis by using one of the following procedures:
1)
Monitor the concentration level of the organic compounds in the exhaust
vent stream from the carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon immediately when
carbon breakthrough is indicated. The monitoring frequency must be
daily or at an interval no greater than 20 percent of the time required to
consume the total carbon working capacity established as a requirement
of Section 725.935(b)(4)(C)(vii), whichever is longer.
274
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design carbon
replacement interval established as a requirement of Section
725.935(b)(4)(C)(vii).
i)
An owner or operator of an affected facility seeking to comply with the
provisions of this Part by using a control device other than a thermal vapor
incinerator, catalytic vapor incinerator, flare, boiler, process heater, condenser,
or carbon adsorption system is required to develop documentation including
sufficient information to describe the control device operation and identify the
process parameter or parameters that indicate proper operation and maintenance
of the control device.
j)
A closed-vent system must meet either of the following design requirements:
1)
A closed-vent system must be designed to operate with no detectable
emissions, as indicated by an instrument reading of less than 500 ppmv
above background, as determined by the methods specified at Section
725.934(b), and by visual inspections; or
2)
A closed-vent system must be designed to operate at a pressure below
atmospheric pressure. The system must be equipped with at least one
pressure gauge or other pressure measurement device that can be read
from a readily accessible location to verify that negative pressure is
being maintained in the closed-vent system when the control device is
operating.
k)
The owner or operator shall monitor and inspect each closed-vent system
required to comply with this Section to ensure proper operation and maintenance
of the closed-vent system by implementing the following requirements:
1)
Each closed-vent system that is used to comply with subsection (j)(1) of
this Section shall be inspected and monitored in accordance with the
following requirements:
A)
An initial leak detection monitoring of the closed-vent system
shall be conducted by the owner or operator on or before the date
that the system becomes subject to this Section. The owner or
operator shall monitor the closed-vent system components and
connections using the procedures specified in Section 725.934(b)
to demonstrate that the closed-vent system operates with no
detectable emissions, as indicated by an instrument reading of
less than 500 ppmv above background.
275
B)
After initial leak detection monitoring required in subsection
(k)(1)(A) of this Section, the owner or operator shall inspect and
monitor the closed-vent system as follows:
i)
Closed-vent system joints, seams, or other connections
that are permanently or semi-permanently sealed (e.g., a
welded joint between two sections of hard piping or a
bolted and gasketed ducting flange) must be visually
inspected at least once per year to check for defects that
could result in air pollutant emissions. The owner or
operator shall monitor a component or connection using
the procedures specified in Section 725.934(b) to
demonstrate that it operates with no detectable emissions
following any time the component is repaired or replaced
(e.g., a section of damaged hard piping is replaced with
new hard piping) or the connection is unsealed (e.g., a
flange is unbolted).
ii)
Closed-vent system components or connections other than
those specified in subsection (k)(1)(B)(i) of this Section
must be monitored annually and at other times as
requested by the Regional Administrator, except as
provided for in subsection (n) of this Section, using the
procedures specified in Section 725.934(b) to demonstrate
that the components or connections operate with no
detectable emissions.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect or leak in accordance with the
requirements of subsection (k)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 725.935.
2)
Each closed-vent system that is used to comply with subsection (j)(2) of
this Section must be inspected and monitored in accordance with the
following requirements:
A)
The closed-vent system must be visually inspected by the owner
or operator to check for defects that could result in air pollutant
emissions. Defects include, but are not limited to, visible cracks,
holes, or gaps in ductwork or piping or loose connections.
276
B)
The owner or operator shall perform an initial inspection of the
closed-vent system on or before the date that the system becomes
subject to this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 725.935.
3)
The owner or operator shall repair all detected defects as follows:
A)
Detectable emissions, as indicated by visual inspection or by an
instrument reading greater than 500 ppmv above background,
must be controlled as soon as practicable, but not later than 15
calendar days after the emission is detected, except as provided
for in subsection (k)(3)(C) of this Section.
B)
A first attempt at repair must be made no later than five calendar
days after the emission is detected.
C)
Delay of repair of a closed-vent system for which leaks have been
detected is allowed if the repair is technically infeasible without a
process unit shutdown, or if the owner or operator determines
that emissions resulting from immediate repair would be greater
than the fugitive emissions likely to result from delay of repair.
Repair of such equipment must be completed by the end of the
next process unit shutdown.
D)
The owner or operator shall maintain a record of the defect repair
in accordance with the requirements specified in Section 725.935.
l)
A closed-vent system or control device used to comply with provisions of this
Subpart must be operated at all times when emissions may be vented to it.
m)
The owner or operator using a carbon adsorption system to control air pollutant
emissions shall document that all carbon removed that is a hazardous waste and
that is removed from the control device is managed in one of the following
manners, regardless of the volatile organic concentration of the carbon:
1)
It is regenerated or reactivated in a thermal treatment unit that meets one
of the following:
277
A)
The owner or operator of the unit has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 724.Subpart X; or
B)
The unit is equipped with and operating air emission controls in
accordance with the applicable requirements of 725.Subparts AA
and CC of this Part or 35 Ill. Adm. Code 724; or
C)
The unit is equipped with and operating air emission controls in
accordance with a national emission standard for hazardous air
pollutants under 40 CFR 61 or 40 CFR 63.
2)
It is incinerated in a hazardous waste incinerator for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 724.Subpart O, or
B)
The owner or operator has designed and operates the incinerator
in accordance with the interim status requirements of 725.Subpart
O of this Part.
3)
It is burned in a boiler or industrial furnace for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 726.Subpart H, or
B)
The owner or operator has designed and operates the boiler or
industrial furnace in accordance with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
n)
Any components of a closed-vent system that are designated, as described in
Section 725.935(c)(9), as unsafe to monitor are exempt from the requirements
of subsection (k)(1)(B)(ii) of this Section if both of the following conditions are
fulfilled:
1)
The owner or operator of the closed-vent system has determined that the
components of the closed-vent system are unsafe to monitor because
monitoring personnel would be exposed to an immediate danger as a
consequence of complying with subsection (k)(1)(B)(ii) of this Section;
and
278
2)
The owner or operator of the closed-vent system adheres to a written
plan that requires monitoring the closed-vent system components using
the procedure specified in subsection (k)(1)(B)(ii) of this Section as
frequently as practicable during safe-to-monitor times.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 725.950
Applicability
a)
The regulations in this Subpart apply to owners and operators of facilities that
treat, store, or dispose of hazardous wastes (except as provided in Section
725.101).
b)
Except as provided in Section 725.964(k), this Subpart applies to equipment that
contains or contacts hazardous wastes with organic concentrations of at least
10% percent by weight that are managed in one of the following:
1)
A unit that is subject to the RCRA permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705;
2)
A unit (including a hazardous waste recycling unit) that is not exempt
from permitting under the provisions of 35 Ill. Adm. Code 722.134(a)
(i.e., a hazardous waste recycling unit that is not a “90-day” tank or
container) and that is located at a hazardous waste management facility
otherwise subject to the permitting requirements of 35 Ill. Adm. Code
702, 703, and 705; or
3)
A unit that is exempt from permitting under the provisions of 35 Ill.
Adm. Code 722.134(a) (i.e., a “90-day” tank or container) and which is
not a recycling unit under the provisions of 35 Ill. Adm. Code 721.106.
c)
Each piece of equipment to which this Subpart applies must be marked in such a
manner that it can be distinguished readily from other pieces of equipment.
d)
Equipment that is in vacuum service is excluded from the requirements of
Sections 725.952 to 725.960, if it is identified as required in Section
725.964(g)(5).
e)
Equipment that contains or contacts hazardous waste with an organic
concentration of at least 10% percent by weight for a period of less than 300
hours per calendar year is excluded from the requirements of Sections 265.952
279
725.952 through 265.960 725.960 if it is identified as required in Section
725.964(g)(6).
BOARD NOTE: The requirements of Sections 725.952 through 725.964 apply
to equipment associated with hazardous waste recycling units previously exempt
under 35 Ill. Adm. Code 721.106(c)(1). Other exemptions under 35 Ill. Adm.
Code 721.104 and 725.101(e) are not affected by these requirements.
f)
Agency decisions pursuant to this Part must be made in writing, are in the
nature of permit decisions pursuant to Section 39 of the Environmental
Protection Act and may be appealed to the Board pursuant to 35 Ill. Adm. Code
105.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.960
Standards: Closed-vent Systems and Control Devices
a)
Owners An owner or operators operator of a closed-vent systems and system or
control devices device subject to this Subpart shall comply with the provisions
of Section 725.933.
b)
Implementation Schedule.
1)
The owner or operator of an existing facility that cannot install a closed-vent
system and control device to comply with the provisions of this Subpart on
the effective date that the facility becomes subject to the provisions of this
Subpart shall prepare an implementation schedule that includes dates by
which the closed-vent system and control device will be installed and in
operation. The controls must be installed as soon as possible, but the
implementation schedule may allow up to 30 months after the effective date
that the facility becomes subject to this Subpart for installation and startup.
2)
Any unit that begins operation after December 21, 1990, and which is subject
to the provisions of this Subpart when operation begins, must comply with
the rules immediately (i.e., the unit must have control devices installed and
operating on startup of the affected unit); the 30-month implementation
schedule does not apply.
3)
The owner or operator of any facility in existence on the effective date of a
statutory or regulatory amendment that renders the facility subject to this
Subpart shall comply with all requirements of this Subpart as soon as
practicable but no later than 30 months after the effective date of the
amendment. When control equipment required by this Subpart can not be
installed and begin operation by the effective date of the amendment, the
facility owner or operator shall prepare an implementation schedule that
includes the following information: Specific calendar dates for award of
contracts or issuance of purchase orders for the control equipment, initiation
of on-site installation of the control equipment, completion of the control
equipment installation, and performance of any testing to demonstrate that
280
the installed equipment meets the applicable standards of this Subpart. The
owner or operator shall enter the implementation schedule in the operating
record or in a permanent, readily available file located at the facility.
4)
An owner or operator of a facility or unit that becomes newly subject to the
requirements of this Subpart due to an action other than those described in
subsection (b)(3) of this Section shall comply with all applicable requirements
immediately (i.e., the facility or unit must have control devices installed and
operating on the date the facility or unit becomes subject to this Subpart; the
30-month implementation schedule does not apply).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.962
Skip Period Alternative for Valves
a)
Election
1)
An owner or operator subject to the requirements of Section 725.957
may elect for all valves within a hazardous waste management unit to
comply with one of the alternative work practices specified in
subsections (b)(2) and (3).
2)
An owner or operator shall notify the Agency before implementing one
of the alternative work practices.
b)
Reduced Monitoring
1)
An owner or operator shall comply with the requirements for valves, as
described in Section 725.957, except as described in subsection
subsections (b)(2) and (b)(3).
2)
After two consecutive quarterly leak detection periods with the
percentage of valves leaking equal to or less than 2 two percent, an
owner or operator may begin to skip one of the quarterly leak detection
periods (i.e., the owner or operator may monitor for leaks once every six
months) for the valves subject to the requirements in Section 725.957.
3)
After five consecutive quarterly leak detection periods with the
percentage of valves leaking equal to or less than 2 two percent, an
owner or operator may begin to skip three of the quarterly leak detection
periods (i.e., the owner or operator may monitor for leaks once every year)
for the valves subject to the requirements in Section 725.957.
4)
If the percentage of valves leaking is greater than 2 percent, the owner
or operator shall monitor monthly in compliance with the requirements
in Section 725.957, but may again elect to use this Section after meeting
the requirements of Section 725.957(c)(1).
281
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.964
Recordkeeping Requirements
a)
Lumping Units.
1)
Each owner or operator subject to the provisions of this Subpart shall
comply with the recordkeeping requirements of this Section.
2)
An owner or operator of more than one hazardous waste management
unit subject to the provisions of this Subpart may comply with the
recordkeeping requirements for these hazardous waste management units
in one recordkeeping system if the system identifies each record by each
hazardous waste management unit.
b)
Owners and operators shall record the following information in the facility
operating record:
1)
For each piece of equipment to which this Subpart applies:
A)
Equipment identification number and hazardous waste
management unit identification.
B)
Approximate locations within the facility (e.g., identify the
hazardous waste management unit on a facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total organics in the hazardous wastestream at
the equipment.
E)
Hazardous waste state at the equipment (e.g., gas/vapor or
liquid).
F)
Method of compliance with the standard (e.g., “monthly leak
detection and repair” or “equipped with dual mechanical seals”).
2)
For facilities that comply with the provisions of Section 725.933(a)(2),
an implementation schedule as specified in that Section.
3)
Where an owner or operator chooses to use test data to demonstrate the
organic removal efficiency or total organic compound concentration
achieved by the control device, a performance test plan as specified in
Section 725.935(b)(3).
282
4)
Documentation of compliance with Section 725.960, including the
detailed design documentation or performance test results specified in
Section 725.935(b)(4).
c)
When each leak is detected as specified in Section 725.952, 725.953, 725.957,
or 725.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked with the
equipment identification number, the date evidence of a potential leak
was found in accordance with Section 725.958(a), and the date the leak
was detected, must be attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be removed after
it has been repaired.
3)
The identification on a valve may be removed after it has been
monitored for 2 successive months as specified in Section 725.957(c)
and no leak has been detected during those 2 months.
d)
When each leak is detected as specified in Sections 725.952, 725.953, 725.957
or 725.958, the following information must be recorded in an inspection log and
must be kept in the facility operating record:
1)
The instrument and operator identification numbers and the equipment
identification number.
2)
The date evidence of a potential leak was found in accordance with
Section 725.958(a).
3)
The date the leak was detected and the dates of each attempt to repair the
leak.
4)
Repair methods applied in each attempt to repair the leak.
5)
“Above 10,000”, if the maximum instrument reading measured by the
methods specified in Section 725.963(b) after each repair attempt is
equal to or greater than 10,000 ppm.
6)
“Repair delayed” and the reason for the delay if a leak is not repaired
within 15 calendar days after discovery of the leak.
7)
Documentation supporting the delay of repair of a valve in compliance
with Section 725.959(c).
283
8)
The signature of the owner or operator (or designate) whose decision it
was that repair could not be effected without a hazardous waste
management unit shutdown.
9)
The expected date of successful repair of the leak if a leak is not repaired
within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection information for
each closed-vent system and control device required to comply with the
provisions of Section 725.960 must be recorded and kept up-to-date in the
facility operating record as specified in Section 725.935(c)(1) and (c)(2), and
monitoring, operating and inspection information in Section 725.935(c)(3)
through (c)(8).
f)
For a control device other than a thermal vapor incinerator, catalytic vapor
incinerator, flare, boiler, process heater, condenser, or carbon adsorption
system, monitoring and inspection information indicating proper operation and
maintenance of the control device must be recorded in the facility operating
record.
g)
The following information pertaining to all equipment subject to the
requirements in Sections 725.952 through 725.960 must be recorded in a log
that is kept in the facility operating record:
1)
A list of identification numbers for equipment (except welded fittings)
subject to the requirements of this Subpart.
2)
List of Equipment.
A)
A list of identification numbers for equipment that the owner or
operator elects to designate for no detectable emissions, as
indicated by an instrument reading of less than 500 ppm above
background, under the provisions of Sections 725.952(e),
725.953(i) and 725.957(f).
B)
The designation of this equipment as subject to the requirements
of Section 725.952(e), 725.953(i) or 725.957(f) must be signed
by the owner or operator.
3)
A list of equipment identification numbers for pressure relief devices
required to comply with Section 725.954(a).
4)
Compliance tests.
284
A)
The dates of each compliance test required in Sections
725.952(e), 725.953(i), 725.954, and 725.957(f).
B)
The background level measured during each compliance test.
C)
The maximum instrument reading measured at the equipment
during each compliance test.
5)
A list of identification numbers for equipment in vacuum service.
6)
Identification, either by list or location (area or group) of equipment that
contains or contacts hazardous waste with an organic concentration of at
least 10 percent by weight for a period of less than 300 hours per year.
h)
The following information pertaining to all valves subject to the requirements of
Section 725.957(g) and (h) must be recorded in a log that is kept in the facility
operating record:
1)
A list of identification numbers for valves that are designated as unsafe
to monitor, an explanation for each valve stating why the valve is unsafe
to monitor, and the plan for monitoring each valve.
2)
A list of identification numbers for valves that are designated as difficult
to monitor, an explanation for each valve stating why the valve is
difficult to monitor, and the planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility operating record for
valves complying with Section 725.962:
1)
A schedule of monitoring.
2)
The percent of valves found leaking during each monitoring period.
j)
The following information must be recorded in a log that is kept in the facility
operating record:
1)
Criteria required in Sections 725.952(d)(5)(B) and 725.953(e)(2) and an
explanation of the criteria.
2)
Any changes to these criteria and the reasons for the changes.
k)
The following information must be recorded in a log that is kept in the facility
operating record for use in determining exemptions as provided in Section
725.950 and other specific Subparts:
285
1)
An analysis determining the design capacity of the hazardous waste
management unit.
2)
A statement listing the hazardous waste influent to and effluent from
each hazardous waste management unit subject to the requirements in
Section 725.960 and an analysis determining whether these hazardous
wastes are heavy liquids.
3)
An up-to-date analysis and the supporting information and data used to
determine whether or not equipment is subject to the requirements in
Sections 725.952 through 725.960. The record must include supporting
documentation as required by Section 725.963(d)(3) when application of
the knowledge of the nature of the hazardous wastestream or the process
by which it was produced is used. If the owner or operator takes any
action (e.g., changing the process that produced the waste) that could
result in an increase in the total organic content of the waste contained in
or contacted by equipment determined not to be subject to the
requirements in Sections 725.952 through 725.960, then a new
determination is required.
l)
Records of the equipment leak information required by subsection (d) of this
Section and the operating information required by subsection (e) of this Section
need be kept only three years.
m)
The owner or operator of any facility with equipment that is subject to this
Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart
V or 63, incorporated by reference in 35 Ill. Adm. Code 720.111, may elect to
determine compliance with this Subpart by documentation of compliance either
pursuant to Section 725.964, or by documentation of compliance with the
regulations at 40 CFR 60, 61, or 63, pursuant to those the relevant provisions of
40 CFR 60, or 61, or 63.to the extent that the documentation under the
regulation at 40 CFR 60 or 61 duplicates the documentation required under this
Subpart. The documentation of compliance under the regulation at 40 CFR 60,
or 61, or 63 must be kept with or made readily available with the facility
operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
286
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section 725.980
Applicability
a)
The requirements of this Subpart apply, effective October 6, 1996, to owners
and operators of all facilities that treat, store, or dispose of hazardous waste in
tanks, surface impoundments, or containers that are subject to 725.Subpart I, J,
or K of this Part, except as Section 725.101 and subsection (b) of this Section
provide otherwise.
BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
(Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828 (May 19,
1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed. Reg. 28508 (June 5,
1996), USEPA delayed the effective date until October 6, 1996. If action by
USEPA or a decision of a federal court changes the effectiveness of these
regulations, the Board does not intend that 725.Subpart CC be enforceable to
the extent that it becomes more stringent that the federal regulations upon which
they are based.
b)
The requirements of this Subpart do not apply to the following waste
management units at the facility:
1)
A waste management unit that holds hazardous waste placed in the unit
before October December 6, 1996, and in which no hazardous waste is
added to the unit on or after this date December 6, 1996.
2)
A container that has a design capacity less than or equal to 0.1 m
3
(3.5
ft
3
or 26.4 gal).
3)
A tank in which an owner or operator has stopped adding hazardous
waste and the owner or operator has begun implementing or completed
closure pursuant to an approved closure plan.
4)
A surface impoundment in which an owner or operator has stopped
adding hazardous waste (except to implement an approved closure plan)
and the owner or operator has begun implementing or completed closure
pursuant to an approved closure plan.
5)
A waste management unit that is used solely for on-site treatment or
storage of hazardous waste that is generated as the result of
implementing remedial activities required pursuant to the Act or Board
regulations or under the corrective action authorities of RCRA sections
3004(u), 3004(v) or 3008(h); CERCLA authorities; or similar federal or
state authorities.
287
6)
A waste management unit that is used solely for the management of
radioactive mixed waste in accordance with all applicable regulations
under the authority of the Atomic Energy Act (42 U.S.C. USC 2011 et
seq.) and the Nuclear Waste Policy Act.
7)
A hazardous waste management unit that the owner or operator certifies
is equipped with and operating air emission controls in accordance with
the requirements of an applicable federal Clean Air Act regulation
codified under 40 CFR 60, 61, or 63. For the purpose of complying
with this subsection (b)(7), a tank for which the air emission control
includes an enclosure, as opposed to a cover, must be in compliance
with the enclosure and control device requirements of Section
725.985(i), except as provided in Section 725.983(c)(5).
8)
A tank that has a process vent, as defined in 35 Ill. Adm. Code 725.931.
c)
For the owner and operator of a facility subject to this Subpart that has received
a final RCRA permit prior to October December 6, 1996, the following
requirements apply:
1)
The requirements of 35 Ill. Adm. Code 724.Subpart CC must be
incorporated into the permit when the permit is reissued, renewed, or
modified in accordance with the requirements of 35 Ill. Adm. Code 703
and 705.
2)
Until the date when the permit is reissued, renewed, or modified in
accordance with the requirements of 35 Ill. Adm. Code 703 and 705, the
owner and operator is subject to the requirements of this Subpart.
d)
The requirements of this Subpart, except for the recordkeeping requirements
specified in Section 725.990(i), are stayed for a tank or container used for the
management of hazardous waste generated by organic peroxide manufacturing
and its associated laboratory operations, when the owner or operator of the unit
meets all of the following conditions:
1)
The owner or operator identifies that the tank or container receives
hazardous waste generated by an organic peroxide manufacturing process
producing more than one functional family of organic peroxides or
multiple organic peroxides within one functional family, that one or
more of these organic peroxides could potentially undergo self-
accelerating thermal decomposition at or below ambient temperatures,
and that organic peroxides are the predominant products manufactured
by the process. For the purposes of this subsection, “organic peroxide”
means an organic compound that contains the bivalent -O-O- structure
288
and which may be considered to be a structural derivative of hydrogen
peroxide where one or both of the hydrogen atoms has been replaced by
an organic radical.
2)
The owner or operator prepares documentation, in accordance with
Section 725.990(i), explaining why an undue safety hazard would be
created if air emission controls specified in Sections 725.985 through
725.988 are installed and operated on the tanks and containers used at
the facility to manage the hazardous waste generated by the organic
peroxide manufacturing process or processes meeting the conditions of
subsection (d)(1) of this Section.
3)
The owner or operator notifies the Agency in writing that hazardous
waste generated by an organic peroxide manufacturing process or
processes meeting the conditions of subsection (d)(1) of this Section are
managed at the facility in tanks or containers meeting the conditions of
subsection (d)(2) of this Section. The notification must state the name
and address of the facility and be signed and dated by an authorized
representative of the facility owner or operator.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.981
Definitions
As used in this Subpart and in 35 Ill. Adm. Code 724, all terms not defined herein shall have
the meanings given to them in the Act and 35 Ill. Adm. Code 720 through 726.
“Average volatile organic concentration” or “average VO concentration” means
the mass-weighted average volatile organic concentration of a hazardous waste,
as determined in accordance with the requirements of Section 725.984.
“Closure device” means a cap, hatch, lid, plug, seal, valve, or other type of
fitting that blocks an opening in a cover so that when the device is secured in
the closed position it prevents or reduces air pollutant emissions to the
atmosphere. Closure devices include devices that are detachable from the cover
(e.g., a sampling port cap), manually operated (e.g., a hinged access lid or
hatch), or automatically operated (e.g., a spring-loaded pressure relief valve).
“Continuous seal” means a seal that forms a continuous closure that completely
covers the space between the edge of the floating roof and the wall of a tank. A
continuous seal may be a vapor-mounted seal, liquid-mounted seal, or metallic
shoe seal. A continuous seal may be constructed of fastened segments so as to
form a continuous seal.
289
“Cover” means a device that provides a continuous barrier over the hazardous
waste managed in a unit to prevent or reduce air emissions to the atmosphere.
A cover may have openings (such as access hatches, sampling ports, and gauge
wells) that are necessary for operation, inspection, maintenance, or repair of the
unit on which the cover is used. A cover may be a separate piece of equipment
which can be detached and removed from the unit or a cover may be formed by
structural features permanently integrated into the design of the unit.
“Enclosure” means a structure that surrounds a tank or container, captures
organic vapors emitted from the tank or container, and vents the captured
vapors through a closed-vent system to a control device.
“External floating roof” means a pontoon-type or double-deck type cover that
rests on the surface of a hazardous waste being managed in a tank with no fixed
roof.
“Fixed roof” means a cover that is mounted on a unit in a stationary position
and does not move with fluctuations in the level of the material managed in the
unit.
“Floating membrane cover” means a cover consisting of a synthetic flexible
membrane material that rests upon and is supported by the hazardous waste
being managed in a surface impoundment.
“Floating roof” means a cover consisting of a double-deck, pontoon single-
deck, or internal floating cover that rests upon and is supported by the material
being contained, and is equipped with a continuous seal.
“Hard-piping” means pipe or tubing that is manufactured and properly installed
in accordance with relevant standards and good engineering practices.
“In light material service” means that the container is used to manage a material
for which both of the following conditions apply: the vapor pressure of one or
more of the organic constituents in the material is greater than 0.3 kilopascals
(kPa) at 20°C (1.2 inches H2O at 68°F); and the total concentration of the pure
organic constituents having a vapor pressure greater than 0.3 kPa at 20°C (1.2
inches H2O at 68°F) is equal to or greater than 20 percent by weight.
“Internal floating roof” means a cover that rests or floats on the material surface
(but not necessarily in complete contact with it) inside a tank that has a fixed
roof.
“Liquid-mounted seal” means a foam or liquid-filled primary seal mounted in
contact with the hazardous waste between the tank wall and the floating roof,
continuously around the circumference of the tank.
290
“Malfunction” means any sudden, infrequent, and not reasonably preventable
failure of air pollution control equipment, process equipment, or a process to
operate in a normal or usual manner. A failure that is caused in part by poor
maintenance or careless operation is not a malfunction.
“Maximum organic vapor pressure” means the sum of the individual organic
constituent partial pressures exerted by the material contained in a tank at the
maximum vapor pressure-causing conditions (i.e., temperature, agitation, pH
effects of combining wastes, etc.) reasonably expected to occur in the tank. For
the purpose of this Subpart, maximum organic vapor pressure is determined
using the procedures specified in Section 725.984(c).
“Metallic shoe seal” means a continuous seal that is constructed of metal sheets
that are held vertically against the wall of the tank by springs, weighted levers,
or other mechanisms and which is connected to the floating roof by braces or
other means. A flexible coated fabric (envelope) spans the annular space
between the metal sheet and the floating roof.
“No detectable organic emissions” means no escape of organics to the
atmosphere, as determined using the procedure specified in Section 725.984(d).
“Point of waste origination” means as follows:
When the facility owner or operator is the generator of the hazardous
waste, the “point of waste origination” means the point where a solid
waste produced by a system, process, or waste management unit is
determined to be a hazardous waste, as defined in 35 Ill. Adm. Code
721.
BOARD NOTE: In this case, this term is being used in a manner
similar to the use of the term “point of generation” in air standards
established for waste management operations under authority of the
federal Clean Air Act in 40 CFR 60, 61, and 63.
When the facility owner and operator are not the generator of the
hazardous waste, “point of waste origination” means the point where the
owner or operator accepts delivery or takes possession of the hazardous
waste.
“Point of waste treatment” means the point where a hazardous waste to be
treated in accordance with Section 725.983(c)(2) exits the treatment process.
Any waste determination must be made before the waste is conveyed, handled,
or otherwise managed in a manner that allows the waste to volatilize to the
atmosphere.
291
“Safety device” means a closure device, such as a pressure relief valve,
frangible disc, fusible plug, or any other type of device, which functions
exclusively to prevent physical damage or permanent deformation to a unit or its
air emission control equipment by venting gases or vapors directly to the
atmosphere during unsafe conditions resulting from an unplanned, accidental, or
emergency event. For the purpose of this Subpart, a safety device is not used
for routine venting of gases or vapors from the vapor headspace underneath a
cover such as during filling of the unit or to adjust the pressure in this vapor
headspace in response to normal daily diurnal ambient temperature fluctuations.
A safety device is designed to remain in a closed position during normal
operations and open only when the internal pressure, or another relevant
parameter, exceeds the device threshold setting applicable to the air emission
control equipment as determined by the owner or operator based on
manufacturer recommendations, applicable regulations, fire protection and
prevention codes, standard engineering codes and practices, or other
requirements for the safe handling of flammable, ignitable, explosive, reactive,
or hazardous materials.
“Single-seal system” means a floating roof having one continuous seal. This
seal may be vapor-mounted, liquid-mounted, or a metallic shoe seal.
“Vapor-mounted seal” means a continuous seal that is mounted so that there is a
vapor space between the hazardous waste in the unit and the bottom of the seal.
“Volatile organic concentration” or “VO concentration” means the fraction by
weight of organic compounds contained in a hazardous waste expressed in terms
of parts per million (ppmw), as determined by direct measurement or by
knowledge of the waste, in accordance with the requirements of Section
725.984. For the purpose of determining the VO concentration of a hazardous
waste, organic compounds with a Henry’s law constant value of at least 0.1
mole-fraction-in-the-gas-phase/mole-fraction-in-the-liquid-phase (0.1 Y/X)
(which can also be expressed as 1.8×10
-6
atmospheres/gram-mole/m
3
) at 25° C
(77° F) must be included. Section 725.Appendix F of this Part presents a list of
compounds known to have a Henry’s law constant value less than the cutoff
level.
“Waste determination” means performing all applicable procedures in
accordance with the requirements of Section 725.984 to determine whether a
hazardous waste meets standards specified in this Subpart. Examples of a waste
determination include performing the procedures in accordance with the
requirements of Section 725.984 to determine the average VO concentration of
a hazardous waste at the point of waste origination, determining the average VO
concentration of a hazardous waste at the point of waste treatment and
comparing the results to the exit concentration limit specified for the process
292
used to treat the hazardous waste, the organic reduction efficiency and the
organic biodegradation efficiency for a biological process used to treat a
hazardous waste and comparing the results to the applicable standards, or
determining the maximum volatile organic vapor pressure for a hazardous waste
in a tank and comparing the results to the applicable standards.
“Waste stabilization process” means any physical or chemical process used to
either reduce the mobility of hazardous constituents in a hazardous waste or
eliminate free liquids as determined by Test Method 9095 (Paint Filter Liquids
Test) in “Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, incorporated by reference in Section 35 Ill. Adm. Code 720.111. A
waste stabilization process includes mixing the hazardous waste with binders or
other materials and curing the resulting hazardous waste and binder mixture.
Other synonymous terms used to refer to this process are “waste fixation” or
“waste solidification”. This does not include the addition of absorbent materials
to the surface of a waste to absorb free liquid without mixing, agitation, or
subsequent curing.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.982
Schedule for Implementation of Air Emission Standards
a)
An owner or operator of a facility in existence on October December 6, 1996
and subject to 725.Subpart I, J, or K of this Part shall meet the following
requirements:
1)
The owner or operator shall install and begin operation of all control
equipment required by to comply with this Subpart and complete
modifications of production or treatment processes to satisfy exemption
criteria in accordance with Section 725.983(c) by October December 6,
1996, except as provided in subsection (a)(2) below of this Section.
2)
When control equipment or waste management units required by to
comply with this Subpart cannot be installed and in operation or
modifications of production or treatment processes to satisfy exemption
criteria in accordance with Section 725.983(c) cannot be completed by
October December 6, 1996, the owner or operator shall:
A)
Install and begin operation of the control equipment and waste
management units, and complete modifications of production or
treatment processes as soon as possible, but in no case later than
December 8, 1997.
B)
Prepare an implementation schedule that includes the following
information: specific calendar dates for award of contracts or
issuance of purchase orders for the control equipment, waste
293
management units, and production or treatment process
modifications; the dates of initiation of on-site installation of the
control equipment, or waste management units, and modifications
of production or treatment processes; the dates of completion of the
control equipment or waste management unit installation, and
production or treatment process modifications; and the dates of
performance of any testing to demonstrate that the installed
equipment meets or waste management units, and modified
production or treatment processes meet the applicable standards of
this Subpart.
C)
For a facilities facility subject to the recordkeeping requirements
of Section 725.173, the owner or operator shall enter the
implementation schedule specified in subsection (a)(2)(B) above
of this Section in the operating record no later than October
December 6, 1996.
D)
For a facilities facility not subject to Section 725.173 above of
this Section, the owner or operator shall enter the implementation
schedule specified in subsection (a)(2)(B) of this section in a
permanent, readily available file located at the facility no later
than October December 6, 1996.
b)
An owner or operator of a facility or unit in existence on the effective date of
statutory or regulatory amendments under the Act that render the facility subject
to 725.Subpart I, J, or K of this Part shall meet the following requirements:
1)
The owner or operator shall install and begin operation of all control
equipment required by to comply with this Subpart and complete
modifications of production or treatment processes to satisfy exemption
criteria of Section 725.983(c) by the effective date of the amendment,
except as provided in subsection (b)(2) below of this Section.
2)
When control equipment or waste management units required by to
comply with this Subpart cannot be installed and begin operation or when
modifications of production or treatment processes to satisfy the exemption
criteria of Section 725.983(c) cannot be completed by the effective date of
the amendment, the owner or operator shall undertake the following
actions:
A)
Install and operate begin operation of the control equipment or
waste management unit and complete modification of production or
treatment processes as soon as possible, but in no case later than
30 months after the effective date of the amendment; and
B)
Maintenance of implementation schedule.
294
i)
For facilities subject to the recordkeeping requirements of
Section 725.173, enter and maintain the implementation
schedule specified in subsection (a)(2)(B) above of this
Section in the operating record no later than the effective
date of the amendment, or
ii)
For facilities not subject to Section 725.173, the owner or
operator shall enter and maintain the implementation
schedule specified in subsection (a)(2)(B) above of this
Section in a permanent, readily available file, located at
the facility site, no later than the effective date of the
amendment.
c)
The owner or operator of a facility or unit that becomes newly subject to the
requirements of this Subpart after December 8, 1997 due to an action other than
those described in subsection (b) of this Section shall comply with all applicable
requirements immediately (i.e., the owner or operator shall have control devices
installed and operating on the date the facility or unit becomes subject to the
requirements of this Subpart; the 30-month implementation schedule does not apply
to the owner or operator of such a facility).
cd)
The Agency may Board elect to extend will grant an adjusted standard pursuant
to Section 28.1 of the Act and 35 Ill. Adm. Code 106 that extends the
implementation date for control equipment at a facility, on a case by case basis,
to a date later than December 8, 1997 when the facility owner or operator
proves the following:
1)
When That special circumstances that are beyond the facility owner’s or
operator’s control have delayed or will delay installation or operation of
control equipment, and
2)
The That the owner or operator has made all reasonable and prudent
attempts to comply with the requirements of this Subpart.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.983
Standards: General
a)
This Section applies to the management of hazardous waste in tanks, surface
impoundments, and containers subject to this Subpart.
b)
The owner or operator shall control air pollutant emissions from each hazardous
waste management unit in accordance with the standards specified in Sections
725.985 through Section 725.988, as applicable to the hazardous waste
management unit, except as provided for in subsection (c) of this Section.
295
c)
A tank, surface impoundment, or container is exempted from standards
specified in Sections 725.985 through 725.988, provided that all hazardous
waste placed in the waste management unit is one of the following:
1)
A tank, surface impoundment, or container for which all hazardous
waste entering the unit has an average VO concentration at the point of
waste origination of less than 500 parts per million by weight (ppmw).
The average VO concentration must be determined by the procedures
specified in Section 725.984(a). The owner or operator shall review and
update, as necessary, this determination at least once every 12 months
following the date of the initial determination for the hazardous waste
streams entering the unit.
2)
A tank, surface impoundment, or container for which the organic content
of all the hazardous waste entering the waste management unit has been
reduced by an organic destruction or removal process that achieves any
one of the following conditions:
A)
The process removes or destroys the organics contained in the
hazardous waste to such a level that the average VO
concentration of the hazardous waste at the point of waste
treatment is less than the exit concentration limit (Ct) established
for the process. The average VO concentration of the hazardous
waste at the point of waste treatment and the exit concentration
limit for the process must be determined using the procedures
specified in Section 725.984(b).
B)
The process removes or destroys the organics contained in the
hazardous waste to such a level that the organic reduction
efficiency (R) for the process is equal to or greater than 95%
percent, and the average VO concentration of the hazardous
waste at the point of waste treatment is less than 100 ppmw. The
organic reduction efficiency for the process and the average VO
concentration of the hazardous waste at the point of waste
treatment must be determined using the procedures specified in
Section 725.984(b).
C)
The process removes or destroys the organics contained in the
hazardous waste to such a level that the actual organic mass
removal rate (MR) for the process is equal to or greater than the
required organic mass removal rate (RMR) established for the
process. The required organic mass removal rate and the actual
organic mass removal rate for the process must be determined
using the procedures specified in Section 725.984(b).
296
D)
The process is a biological process that destroys or degrades the
organics contained in the hazardous waste so that either of the
following conditions is met:
i)
The organic reduction efficiency (R) for the process is
equal to or greater than 95% percent, and the organic
biodegradation efficiency (Rbio) for the process is equal to
or greater than 95% percent. The organic reduction
efficiency and the organic biodegradation efficiency for
the process must be determined using the procedures
specified in Section 725.984(b).
ii)
The total actual organic mass biodegradation rate (MRbio)
for all hazardous waste treated by the process is equal to
or greater than the required organic mass removal rate
(RMR). The required organic mass removal rate and the
actual organic mass biodegradation rate for the process
must be determined using the procedures specified in
Section 725.984(b).
E)
The process is one that removes or destroys the organics
contained in the hazardous waste and meets all of the following
conditions:
i)
From the point of waste origination through the point
where the hazardous waste enters the treatment process,
the hazardous waste is continuously managed in waste
management units that use air emission controls in
accordance with the standards specified in Section
725.985 through Section 725.988, as applicable to the
waste management unit.
ii)
From the point of waste origination through the point
where the hazardous waste enters the treatment process,
any transfer of the hazardous waste is accomplished
through continuous hard-piping or other closed system
transfer that does not allow exposure of the waste to the
atmosphere.
BOARD NOTE: The USEPA considers a drain system
that meets the requirements of 40 CFR 63, subpart RR,
“National Emission Standards for Individual Drain
Systems”, to be a closed system.
297
iii)
The average VO concentration of the hazardous waste at
the point of waste treatment is less than the lowest average
VO concentration at the point of waste origination
determined for each of the individual hazardous waste
streams entering the process or 500 ppmw, whichever
value is lower. The average VO concentration of each
individual hazardous waste stream at the point of waste
origination must be determined using the procedures
specified in Section 725.984(a). The average VO
concentration of the hazardous waste at the point of waste
treatment must be determined using the procedures
specified in Section 725.984(b).
F)
A process that removes or destroys the organics contained in the
hazardous waste to a level such that the organic reduction
efficiency (R) for the process is equal to or greater than 95%
percent and the owner or operator certifies that the average VO
concentration at the point of waste origination for each of the
individual waste streams entering the process is less than 10,000
ppmw. The organic reduction efficiency for the process and the
average VO concentration of the hazardous waste at the point of
waste origination shall be determined using the procedures
specified in Section 724.983(b) and Section 724.983(a),
respectively.
G)
A hazardous waste incinerator for which either of the following
conditions is true:
i)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
724.Subpart O; or
ii)
The owner or operator has designed and operates the
incinerator in accordance with the interim status
requirements of 725.Subpart O of this Part.
H)
A boiler or industrial furnace for which either of the following
conditions is true:
i)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
726.Subpart H; or
298
ii)
The owner or operator has designed and operates the
industrial furnace or incinerator in accordance with the
interim status requirements of 35 Ill. Adm. Code
726.Subpart H.
I)
For the purpose of determining the performance of an organic
destruction or removal process in accordance with the conditions
in each of subsections (c)(2)(A) through (c)(2)(F) of this Section,
the owner or operator shall account for VO concentrations
determined to be below the limit of detection of the analytical
method by using the following VO concentration:
i)
If Method 25D in 40 CFR 60, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111, is used for
the analysis, one-half the blank value determined in the
method at Section 4.4 of Method 25D or a value of 25 ppmw,
whichever is less.
ii)
If any other analytical method is used, one-half the limit
of detection established for the method sum of the limits of
detection established for each organic constituent in the
waste that has a Henry’s law constant value at least 0.1 mole-
fraction-in-the-gas-phase/mole-fraction-in-the-liquid-phase
(0.1 Y/X) (which can also be expressed as 1.8 x 10
-6
atmospheres/gram-mole/m
3
) at 25° C .
3)
A tank or surface impoundment used for biological treatment of hazardous
waste in accordance with the requirements of subsection (c)(2)(D) of this
Section.
4)
A tank, surface impoundment, or container for which all hazardous
waste placed in the unit fulfills either of the following two conditions:
A)
It meets the numerical concentration limits for organic hazardous
constituents, applicable to the hazardous waste, as specified in 35
Ill. Adm. Code 728.Table T; or
B)
It has The organic hazardous constituents in the waste have been
treated by the treatment technology established by USEPA for the
waste, as set forth in 35 Ill. Adm. Code 728.142(a), or treated by
an equivalent method of treatment approved by the Agency
pursuant to 35 Ill. Adm. Code 728.142(b).
5)
A tank used for bulk feed of hazardous waste to a waste incinerator and
all of the following conditions are met:
299
A)
The tank is located inside an enclosure vented to a control device
that is designed and operated in accordance with all applicable
requirements specified under 40 CFR 61, subpart FF, “National
Emission Standards for Benzene Waste Operations”, incorporated
by reference in 35 Ill. Adm. Code 720.111, for a facility at
which the total annual benzene quantity from the facility waste is
equal to or greater than 10 megagrams (11 tons) per year;
B)
The enclosure and control device serving the tank were installed
and began operation prior to November 25, 1996; and
C)
The enclosure is designed and operated in accordance with the
criteria for a permanent total enclosure as specified in “Procedure
T--Criteria for and Verification of a Permanent or Temporary
Total Enclosure” under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code 720.111. The
enclosure may have permanent or temporary openings to allow
worker access; passage of material into or out of the enclosure by
conveyor, vehicles, or other mechanical or electrical equipment;
or to direct air flow into the enclosure. The owner or operator
shall perform the verification procedure for the enclosure as
specified in Section 5.0 to “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure”
annually.
d)
The Agency may at any time perform or request that the owner or operator
perform a waste determination for a hazardous waste managed in a tank, surface
impoundment, or container that is exempted from using air emission controls
under the provisions of this Section as follows:
1)
The waste determination for average VO concentration of a hazardous
waste at the point of waste origination must be performed using direct
measurement in accordance with the applicable requirements of Section
725.984(a). The waste determination for a hazardous waste at the point
of waste treatment must be performed in accordance with the applicable
requirements of Section 725.984(b).
2)
In performing a waste determination pursuant to subsection (d)(1) of this
Section, the sample preparation and analysis shall be conducted as
follows:
A)
In accordance with the method used by the owner or operator to
perform the waste analysis, except in the case specified in
subsection (d)(2)(B) of this Section.
300
B)
If the Agency determines that the method used by the owner or
operator was not appropriate for the hazardous waste managed in
the tank, surface impoundment, or container, then the Agency
may choose an appropriate method.
3)
Where the owner or operator is requested to perform the waste
determination, the Agency may elect to have an authorized
representative observe the collection of the hazardous waste samples
used for the analysis.
4)
Where the results of the waste determination performed or requested by
the Agency do not agree with the results of a waste determination
performed by the owner or operator using knowledge of the waste, then
the results of the waste determination performed in accordance with the
requirements of subsection (d)(1) of this Section must be used to
establish compliance with the requirements of this Subpart.
5)
Where the owner or operator has used an averaging period greater than
one hour for determining the average VO concentration of a hazardous
waste at the point of waste origination, the Agency may elect to establish
compliance with this Subpart by performing or requesting that the owner
or operator perform a waste determination using direct measurement,
based on waste samples collected within a 1-hour period as follows:
A)
The average VO concentration of the hazardous waste at the point
of waste origination must be determined by direct measurement
in accordance with the requirements of Section 725.984(a).
B)
Results of the waste determination performed or requested by the
Agency showing that the average VO concentration of the
hazardous waste at the point of waste origination is equal to or
greater than 500 ppmw shall constitute noncompliance with this
Subpart, except in a case as provided for in subsection (d)(4)(C)
of this Section.
C)
Where the average VO concentration of the hazardous waste at
the point of waste origination previously has been determined by
the owner or operator using an averaging period greater than one
hour to be less than 500 ppmw but because of normal operating
process variations the VO concentration of the hazardous waste
determined by direct measurement for any given 1-hour period
may be equal to or greater than 500 ppmw, information that was
used by the owner or operator to determine the average VO
concentration of the hazardous waste (e.g., test results,
measurements, calculations, and other documentation) and
301
recorded in the facility records in accordance with the
requirements of Sections 725.984(a) and 725.990 must be
considered by the Agency together with the results of the waste
determination performed or requested by the Agency in
establishing compliance with this Subpart.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.984
Waste Determination Procedures
a)
Waste determination procedure for volatile organic (VO) concentration of a
hazardous waste at the point of waste origination.
1)
An owner or operator shall determine the average VO concentration at
the point of waste origination for each hazardous waste placed in a waste
management unit exempted under the provisions of Section
725.983(c)(1) from using air emission controls in accordance with
standards specified in Section 725.985 through Section 725.988, as
applicable to the waste management unit.
2)
The For a waste determination that is required by subsection (a)(1) of this
Section, the average VO concentration of a hazardous waste at the point
of waste origination must be determined using either direct
measurement, as specified in subsection (a)(3) of this Section, or by
knowledge of the waste, as specified in subsection (a)(4) of this Section.
3)
Direct measurement to determine average VO concentration of a
hazardous waste at the point of waste origination.
A)
Identification. The owner or operator shall identify and record
the point of waste origination for the hazardous waste.
B)
Sampling. Samples of the hazardous waste stream must be
collected at the point of waste origination in a manner such that
volatilization of organics contained in the waste and in the
subsequent sample is minimized and an adequately representative
sample is collected and maintained for analysis by the selected
method.
i)
The averaging period to be used for determining the
average VO concentration for the hazardous waste stream
on a mass-weighted average basis must be designated and
recorded. The averaging period can represent any time
interval that the owner or operator determines is
302
appropriate for the hazardous waste stream but must not
exceed one year.
ii)
A sufficient number of samples, but no less fewer than
four samples, must be collected for the a hazardous waste
determination. The average of the four or more sample
results constitutes a waste determination for the waste
stream. One or more waste determinations may be required
to represent the complete range of waste compositions and
quantities that occur during the entire averaging period
due to normal variations in the operating conditions for
the source or process generating the hazardous waste
stream. Examples of such normal variations are seasonal
variations in waste quantity or fluctuations in ambient
temperature.
iii)
All samples must be collected and handled in accordance
with written procedures prepared by the owner or operator
and documented in a site sampling plan. This plan must
describe the procedure by which representative samples of
the hazardous waste stream are collected such that a
minimum loss of organics occurs throughout the sample
collection and handling process, and by which sample
integrity is maintained. A copy of the written sampling
plan must be maintained on-site in the facility operating
records. An example of an acceptable sampling plan
includes a plan incorporating sample collection and
handling procedures in accordance with the requirements
specified in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods,” USEPA Publication SW-
846, incorporated by reference in 35 Ill. Adm. Code
720.111, or in Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code 720.111.
C)
Analysis. Each collected sample must be prepared and analyzed
in accordance with one or more of the methods listed in
subsections (a)(3)(C)(i) through (a)(3)(C)(ix) of this Section,
including the appropriate quality assurance and quality control
(QA/QC) checks and use of target compounds for calibration. If
Method 25D in 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111, is not used, then one or
more methods should be chosen that are appropriate to ensure
that the waste determination accounts for and reflects all organic
compounds in the waste with Henry’s law constant values at least
0.1 mole-fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
phase (0.1 Y/X) [(which can also be expressed as 1.8×10
-6
303
atmospheres/gram-mole/m
3
]) at 25° C (77° F). Each of the
analytical methods listed in subsections (a)(3)(C)(ii) through
(a)(3)(C)(vii) of this Section has an associated list of approved
chemical compounds, for which USEPA considers the method
appropriate for measurement. If an owner or operator uses
USEPA Method 624, 625, 1624, or 1625 in 40 CFR 136,
appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111, to analyze one or more compounds that are not on that
method’s published list, the Alternative Test Procedure contained
in 40 CFR 136.4 and 136.5, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be followed. If an owner or operator
uses USEPA Method 8260(B) or 8270(C) in “Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods”, USEPA
Publication SW-846, incorporated by reference in 35 Ill. Adm.
Code 720.111, to analyze one or more compounds that are not on
that method’s published list, the procedures in subsection
(a)(3)(C)(viii) of this Section must be followed. At the owner’s
or operator’s discretion, the concentration of each individual
chemical constituent measured in the waste by a method other
than Method 25D may be corrected to the concentration it would
have had, had it been measured using Method 25D, by
multiplying the measured concentration by the constituent-
specific adjustment factor (fm25D), as specified in subsection
(a)(4)(C) of this Section. Constituent-specific adjustment factors
(fm25D) can be obtained by contacting the USEPA, Waste and
Chemical Processes Group, Office of Air Quality Planning and
Standards, Research Triangle Park, NC 27711.
i)
Method 25D in 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111.
ii)
Method 624 in 40 CFR 136, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111.
iii)
Method 625 in 40 CFR 136, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111. Perform
corrections to the compounds for which the analysis is
being conducted based on the “accuracy as recovery”
using the factors in Table 7 of the method.
iv)
Method 1624 in 40 CFR 136, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111.
v)
Method 1625 in 40 CFR 136, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111.
304
vi)
Method 8260(B) in “Test Methods for Evaluating Solid
Waste, Physical/Chemical Methods”, USEPA Publication
SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111. Maintain a formal quality assurance program
consistent with the requirements of Method 8260(B). The
quality assurance program must include the elements set
forth in subsection (a)(3)(EF) of this Section.
vii)
Method 8270(C) in “Test Methods for Evaluating Solid
Waste, Physical/Chemical Methods”, USEPA Publication
SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111. Maintain a formal quality assurance program
consistent with the requirements of Method 8270(C). The
quality assurance program must include the elements set
forth in subsection (a)(3)(EF) of this Section.
viii) Any other USEPA standard method that has been
validated in accordance with “Alternative Validation
Procedure for USEPA Waste and Wastewater Methods”,
40 CFR 63, appendix D, incorporated by reference in 35
Ill. Adm. Code 720.111. As an alternative, other USEPA
standard methods may be validated by the procedure
specified in subsection (a)(3)(C)(ix) of this Section.
ix)
Any other analysis method that has been validated in
accordance with the procedures specified in Section 5.1 or
Section 5.3, and the corresponding calculations in Section
6.1 or Section 6.3, of Method 301 in 40 CFR 63,
appendix A, incorporated by reference in 35 Ill. Adm.
Code 720.111. The data are acceptable if they meet the
criteria specified in Section 6.1.5 or Section 6.3.3 of
Method 301. If correction is required under Section 6.3.3
of Method 301, the data are acceptable if the correction
factor is within the range 0.7 to 1.30. Other Sections of
Method 301 are not required.
D)
Calculations.
i)
The average VO concentration (
C
C
) on a mass-weighted
basis must be calculated by using the results for all
samples analyzed waste determinations conducted in
accordance with subsections (a)(3)(B) and (a)(3)(C) of this
Section and the following equation:
305
C=
1
Q
x
n
i= 1
(Q xC )
T
∑
ii
C=
1
Q
x
n
i=1
(Q xC)
T
∑
ii
Where:
C
C
=
Average VO concentration of the hazardous
waste at the point of waste origination on a mass-
weighted basis, in ppmw.
i =
Individual sample waste determination “i” of the
hazardous waste.
n = Total number of samples waste determinations of
the hazardous waste collected (at least four)
conducted for the averaging period (not to exceed
one year).
Qi = Mass quantity of the hazardous waste stream
represented by Ci, in kg/hr.
QT = Total mass quantity of the hazardous waste during
the averaging period, in kg/hr.
Ci = Measured VO concentration of sample waste
determination “i”, as determined in accordance
with subsection (a)(3)(C) of this Section (i.e., the
average of the four or more samples specified in
subsection (a)(3)(B)(ii) of this Section), in ppmw.
ii)
For the purpose of determining C
i
, for individual waste
samples analyzed in accordance with subsection (a)(3)(C) of
this Section, the owner or operator shall account for VO
concentrations determined to be below the limit of detection
of the analytical method by using the VO concentration
determined according to subsection (a)(3)(G) of this Section.
E)
Provided that the test method is appropriate for the waste as required
under subsection (a)(3)(C) of this Section, the Agency must
determine compliance based on the test method used by the owner
or operator as recorded pursuant to Section 725.990(f)(1).
306
EF) The quality assurance program elements required under
subsections (a)(3)(C)(vi) and (a)(3)(C)(vii) of this Section are as
follows:
i)
Documentation of site-specific procedures to minimize the
loss of compounds due to volatilization, biodegradation,
reaction, or sorption during the sample collection,
storage, preparation, introduction, and analysis steps.
ii)
Measurement of the overall accuracy and precision of the
specific procedures.
BOARD NOTE: Subsections (a)(3)(EF)(i) and (a)(3)(EF)(ii)
correspond with are derived from 40 CFR
265.984(a)(3)(iii)(F)(1), (a)(3)(iii)(F)(2), (a)(3)(iii)(G)(1), and
(a)(3)(iii)(G)(2), which the Board has codified here to comport
with Illinois Administrative Code format requirements.
G)
VO concentrations below the limit of detection must be considered to
be as follows:
i)
If Method 25D in 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111, is used for the
analysis, the VO concentration must be considered to be one-
half the blank value determined in the method at Section 4.4
of Method 25D in 40 CFR 60, appendix A.
ii)
If any other analytical method is used, the VO concentration
must be considered to be one-half the sum of the limits of
detection established for each organic constituent in the
waste that has a Henry’s law constant value at least 0.1 mole-
fraction-in-the-gas-phase/mole-fraction-in-the-liquid-phase
(0.1 Y/X) (which can also be expressed as 1.8 x 10
-6
atmospheres/gram-mole/m
3
) at 25° C.
BOARD NOTE: Subsections (a)(3)(G)(i) and (a)(3)(G)(ii) are
derived from 40 CFR 265.984(a)(3)(iv)(A)(1) and
(a)(3)(iv)(A)(2), which the Board has codified here to comport
with Illinois Administrative Code format requirements.
4)
Use of owner or operator knowledge to determine average VO
concentration of a hazardous waste at the point of waste origination.
A)
Documentation must be prepared that presents the information
used as the basis for the owner’s or operator’s knowledge of the
hazardous waste stream’s average VO concentration. Examples
of information that may be used as the basis for knowledge
307
include the following: material balances for the source or
process generating the hazardous waste stream; constituent-
specific chemical test data for the hazardous waste stream from
previous testing that are still applicable to the current waste
stream; previous test data for other locations managing the same
type of waste stream; or other knowledge based on information
included in manifests, shipping papers, or waste certification
notices.
B)
If test data are used as the basis for knowledge, then the owner or
operator shall document the test method, sampling protocol, and
the means by which sampling variability and analytical variability
are accounted for in the determination of the average VO
concentration. For example, an owner or operator may use
organic concentration test data for the hazardous waste stream
that are validated in accordance with Method 301 in 40 CFR 63,
appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111, as the basis for knowledge of the waste.
C)
An owner or operator using chemical constituent-specific
concentration test data as the basis for knowledge of the
hazardous waste may adjust the test data to the corresponding
average VO concentration value which would have been obtained
had the waste samples been analyzed using Method 25D in 40
CFR 60, appendix A, incorporated by reference in 35 Ill. Adm.
Code 720.111. To adjust these data, the measured concentration
for each individual chemical constituent contained in the waste is
multiplied by the appropriate constituent-specific adjustment
factor (fm25D).
D)
In the event that the Agency and the owner or operator disagree
on a determination of the average VO concentration for a
hazardous waste stream using knowledge, then the results from a
determination of average VO concentration using direct
measurement, as specified in subsection (a)(3) of this Section,
must be used to establish compliance with the applicable
requirements of this Subpart. The Agency may perform or
request that the owner or operator perform this determination
using direct measurement. The owner or operator may choose one
or more appropriate methods to analyze each collected sample in
accordance with the requirements of subsection (a)(3)(C) of this
Section.
b)
Waste determination procedures for treated hazardous waste.
308
1)
An owner or operator shall perform the applicable waste determination
for each treated hazardous waste placed in a waste management unit
exempted under the provisions of Section 725.983(c)(2)(A) through
(c)(2)(F) from using air emission controls in accordance with the
standards specified in Sections 725.985 through 725.988, as applicable
to the waste management unit.
2)
The owner or operator shall designate and record the specific provision
in Section 725.983(c)(2) under which the waste determination is being
performed. The waste determination for the treated hazardous waste
must be performed using the applicable procedures specified in
subsections (b)(3) through (b)(9) of this Section.
3)
Procedure to determine the average VO concentration of a hazardous
waste at the point of waste treatment.
A)
Identification. The owner or operator shall identify and record
the point of waste treatment for the hazardous waste.
B)
Sampling. Samples of the hazardous waste stream must be
collected at the point of waste treatment in a manner such that
volatilization of organics contained in the waste and in the
subsequent sample is minimized and an adequately representative
sample is collected and maintained for analysis by the selected
method.
i)
The averaging period to be used for determining the
average VO concentration for the hazardous waste stream
on a mass-weighted average basis must be designated and
recorded. The averaging period can represent any time
interval that the owner or operator determines is
appropriate for the hazardous waste stream but must not
exceed one year.
ii)
A sufficient number of samples, but no less fewer than
four samples, must be collected and analyzed for a
hazardous waste determination. The average of the four or
more sample results constitutes a waste determination for
the hazardous waste stream. One or more waste
determinations may be required to represent the complete
range of waste compositions and quantities that occur
during the entire averaging period due to normal
variations in the operating conditions for the source or
process treating generating the hazardous waste stream.
Examples of such normal variations are seasonal
309
variations in waste quantity or fluctuations in ambient
temperature.
iii)
All samples must be collected and handled in accordance
with written procedures prepared by the owner or operator
and documented in a site sampling plan. This plan must
describe the procedure by which representative samples of
the hazardous waste stream are collected such that a
minimum loss of organics occurs throughout the sample
collection and handling process, and by which sample
integrity is maintained. A copy of the written sampling
plan must be maintained on-site in the facility operating
records. An example of an acceptable sampling plan
includes a plan incorporating sample collection and
handling procedures in accordance with the requirements
specified in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods,” USEPA Publication No.
SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111, or in Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code 720.111.
C)
Analysis. Each collected sample must be prepared and analyzed
in accordance with one or more of the methods listed in
subsections (b)(3)(C)(i) through (b)(3)(C)(ix) of this Section,
including appropriate quality assurance and quality control
(QA/QC) checks and use of target compounds for calibration.
When the owner or operator is making a waste determination for a
treated hazardous waste that is to be compared to an average VO
concentration at the point of waste origination or the point of waste
entry to the treatment system, to determine if the conditions of 35 Ill.
Adm. Code 724.982(c)(2)(A) through (c)(2)(F) or Section
725.983(c)(2)(A) through (c)(2)(F) are met, then the waste samples
shall be prepared and analyzed using the same method or methods
as were used in making the initial waste determinations at the point of
waste origination or at the point of entry to the treatment system. If
Method 25D in 40 CFR 60, appendix A is not used, then one or
more methods should be chosen that are appropriate to ensure
that the waste determination accounts for and reflects all organic
compounds in the waste with Henry’s law constant values at least
0.1 mole-fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
phase (0.1 Y/X) [which can also be expressed as 1.8×10
-6
atmospheres/gram-mole/m
3
] at 25 degrees Celsius. Each of the
analytical methods listed in subsections (b)(3)(C)(ii) through
(b)(3)(C)(vii) of this Section has an associated list of approved
chemical compounds, for which USEPA considers the method
appropriate for measurement. If an owner or operator uses
310
USEPA Method 624, 625, 1624, or 1625 in 40 CFR 136,
appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111, to analyze one or more compounds that are not on that
method’s published list, the Alternative Test Procedure contained
in 40 CFR 136.4 and 136.5, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be followed. If an owner or operator
uses USEPA Method 8260(B) or 8270(C) in “Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods”, USEPA
Publication SW-846, incorporated by reference in 35 Ill. Adm.
Code 720.111, to analyze one or more compounds that are not on
that method’s published list, the procedures in subsection
(b)(3)(C)(viii) of this Section must be followed. At the owner’s
or operator’s discretion, the concentration of each individual
chemical constituent measured in the waste by a method other
than Method 25D may be corrected to the concentration had it
been measured using Method 25D by multiplying the measured
concentration by the constituent-specific adjustment factor (fm25D)
as specified in subsection (a)(4)(C) of this Section. Constituent-
specific adjustment factors (fm25D) can be obtained by contacting
the USEPA, Waste and Chemical Processes Group, Office of Air
Quality Planning and Standards, Research Triangle Park, NC
27711.
i)
Method 25D in 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111.
ii)
Method 624 in 40 CFR 136, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111.
iii)
Method 625 in 40 CFR 136, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111. Perform
corrections to the compounds for which the analysis is
being conducted based on the “accuracy as recovery”
using the factors in Table 7 of the method.
iv)
Method 1624 in 40 CFR 136, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111.
v)
Method 1625 in 40 CFR 136, appendix A, incorporated
by reference in 35 Ill. Adm. Code 720.111.
vi)
Method 8260(B) in “Test Methods for Evaluating Solid
Waste, Physical/Chemical Methods”, USEPA Publication
SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111. Maintain a formal quality assurance program
311
consistent with the requirements of Method 8260(B). The
quality assurance program must include the elements set
forth in subsection (b)(3)(E) of this Section.
vii)
Method 8270(C) in “Test Methods for Evaluating Solid
Waste, Physical/Chemical Methods”, USEPA Publication
SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111. Maintain a formal quality assurance program
consistent with the requirements of Method 8270(C). The
quality assurance program must include the elements set
forth in subsection (b)(3)(E) of this Section.
viii) Any other USEPA standard method that has been
validated in accordance with “Alternative Validation
Procedure for EPA Waste and Wastewater Methods”, 40
CFR 63, appendix D, incorporated by reference in 35 Ill.
Adm. Code 720.111. As an alternative, other USEPA
standard methods may be validated by the procedure
specified in subsection (b)(3)(C)(ix) of this Section.
ix)
Any other analysis method that has been validated in
accordance with the procedures specified in Section 5.1 or
Section 5.3, and the corresponding calculations in Section
6.1 or Section 6.3, of Method 301 in 40 CFR 63,
appendix A. The data are acceptable if they meet the
criteria specified in Section 6.1.5 or Section 6.3.3 of
Method 301. If correction is required under Section 6.3.3
of Method 301, the data are acceptable if the correction
factor is within the range 0.7 to 1.30. Other Sections of
Method 301 are not required.
D)
Calculations. The average VO concentration (
C
) on a mass-
weighted basis must be calculated by using the results for all
samples analyzed in accordance with subsection (b)(3)(C) of this
Section and the following equation:
C=
1
Q
x
n
i= 1
(Q xC )
T
∑
ii
C=
1
Q
x
n
i=1
(Q xC)
T
∑
ii
312
Where:
C
C
=
Average VO concentration of the hazardous
waste at the point of waste treatment on a mass-
weighted basis, in ppmw.
i =
Individual sample determination “i” of the
hazardous waste.
n = Total number of samples waste determinations of
the hazardous waste collected (at least 4) for the
averaging period (not to exceed 1 year).
Qi = Mass quantity of the hazardous waste stream
represented by Ci, in kg/hr.
QT = Total mass quantity of hazardous waste during the
averaging period, in kg/hr.
Ci = Measured VO concentration of sample waste
determinations “i”, as determined in accordance
with the requirements of subsection (b)(3)(C) of
this Section (i.e., the average of the four or more
samples specified in subsection (b)(3)(B)(ii) of this
Section), in ppmw.
E)
Provided that the test method is appropriate for the waste as required
under subsection (b)(3)(C) of this Section, compliance shall be
determined based on the test method used by the owner or operator
as recorded pursuant to Section 725.990(f)(1).
4)
Procedure to determine the exit concentration limit (Ct) for a treated
hazardous waste.
A)
The point of waste origination for each hazardous waste treated
by the process at the same time must be identified.
B)
If a single hazardous waste stream is identified in subsection
(b)(4)(A) of this Section, then the exit concentration limit (Ct)
must be 500 ppmw.
C)
If more than one hazardous waste stream is identified in
subsection (b)(4)(A) of this Section, then the average VO
concentration of each hazardous waste stream at the point of
waste origination must be determined in accordance with the
requirements of subsection (a) of this Section. The exit
313
concentration limit (Ct) must be calculated by using the results
determined for each individual hazardous waste stream and the
following equation:
t
xx
y
xy
C=
m
x= 1
(Q xC )+
n
y= 1
(
Q
x 00ppmw)
m
x= 1
Q+
n
y= 1
Q
∑∑
∑∑
5
t
xx
y
xy
C=
m
x=1
(Q xC )+
n
y=1
(Q x500ppmw)
m
x=1
Q+
n
y=1
Q
∑∑
∑∑
Where:
Ct = Exit concentration limit for treated hazardous
waste, in ppmw.
x = Individual hazardous waste stream “x” that has an
average VO concentration less than 500 ppmw at
the point of waste origination, as determined in
accordance with the requirements of subsection (a)
of this Section.
y = Individual hazardous waste stream “y” that has an
average VO concentration equal to or greater than
500 ppmw at the point of waste origination, as
determined in accordance with the requirements of
subsection (a) of this Section.
m = Total number of “x” hazardous waste streams
treated by process.
n = Total number of “y” hazardous waste streams
treated by process.
314
Qx = Annual mass quantity of hazardous waste stream
“x”, in kg/yr.
Qy = Annual mass quantity of hazardous waste stream
“y”, in kg/yr.
C
x
C
x
=
Average VO concentration of hazardous
waste stream “x” at the point of waste origination,
as determined in accordance with the requirements
of subsection (a) of this Section, in ppmw.
5)
Procedure to determine the organic reduction efficiency (R) for a treated
hazardous waste.
A)
The organic reduction efficiency (R) for a treatment process must
be determined based on results for a minimum of three
consecutive runs.
B)
All hazardous waste streams entering the process and all
hazardous waste streams exiting the treatment process must be
identified. The owner or operator shall prepare a sampling plan
for measuring these streams that accurately reflects the retention
time of the hazardous waste in the process.
C)
For each run, information must be determined for each hazardous
waste stream identified in subsection (b)(5)(B) of this Section,
using the following procedures:
i)
The mass quantity of each hazardous waste stream
entering the process (Qb) and the mass quantity of each
hazardous waste stream exiting the process (Qa) must be
determined.
ii)
The average VO concentration at the point of waste
origination of each hazardous waste stream entering the
process (Cb) during the run must be determined in
accordance with the requirements of subsections (a)(3) of
this Section. The average VO concentration at the point
of waste treatment of each hazardous waste stream exiting
the process (Ca) during the run must be determined in
accordance with the requirements of subsection (b)(3) of
this Section.
D)
The waste volatile organic mass flow entering the process (Eb)
and the waste volatile organic mass flow exiting the process (Ea)
315
must be calculated by using the results determined in accordance
with subsection (b)(5)(C) of this Section and the following
equations:
E
b
=
6
bj
bj
1
10
m
j= 1
∑
(Q xC )
E
a
=
6
aj
aj
1
10
m
j= 1
∑
(Q xC )
E
b
=
6
bj
bj
1
10
m
j=1
∑
(Q xC )
E
a
=
6
aj
aj
1
10
m
j=1
∑
(Q xC )
Where:
Ea = Waste volatile organic mass flow exiting the
process, in kg/hr.
Eb = Waste volatile organic mass flow entering the
process, in kg/hr.
m = Total number of runs (at least 3)
j =
Individual run “j”
Qbj = Mass quantity of hazardous waste entering the
process during run “j”, in kg/hr.
Qaj = Average mass quantity of waste exiting the process
during run “j”, in kg/hr.
C
aj
C
aj
=
Average VO concentration of hazardous
waste exiting the process during run “j”, as
determined in accordance with the requirements of
subsection (b)(3) of this Section, in ppmw.
316
C
bj
C
bj
=
Average VO concentration of hazardous
waste entering the process during run “j”, as
determined in accordance with the requirements of
subsection 725.984 (a)(3) of this Section, in
ppmw.
E)
The organic reduction efficiency of the process must be
calculated by using the results determined in accordance with
subsection (b)(5)(D) of this Section and the following equation:
R=
E
-E
E
x100%
ba
b
R=
E
-E
E
x100%
ba
b
Where:
R = Organic reduction efficiency, in percent.
Eb = Waste volatile organic mass flow entering the
process as determined in accordance with the
requirements of subsection (b)(5)(D) of this
Section, in kg/hr.
Ea = Waste volatile organic mass flow exiting the
process as determined in accordance with the
requirements of subsection (b)(5)(D) of this
Section, in kg/hr.
6)
Procedure to determine the organic biodegradation efficiency (Rbio) for a
treated hazardous waste.
A)
The fraction of organics biodegraded (Fbio) must be determined
using the procedure specified in 40 CFR 63, Appendix C,
incorporated by reference in 35 Ill. Adm. Code 720.111.
B)
The organic biodegradation efficiency (Rbio) must be calculated by
using the following equation:
R
bio
=
F
bio
x100%
R
bio
=
F
bio
x100%
317
Where
Rbio = Organic biodegradation efficiency, in percent.
Fbio = Fraction of organic biodegraded, as determined in
accordance with the requirements of subsection
(b)(6)(A) of this Section.
7)
Procedure to determine the required organic mass removal rate (RMR)
for a treated hazardous waste.
A)
All of the hazardous waste streams entering the treatment process
must be identified.
B)
The average VO concentration of the hazardous waste stream at
the point of waste origination must be determined in accordance
with the requirements of subsection (a) of this Section.
C)
For each individual hazardous waste stream that has an average
volatile organic concentration equal to or greater than 500 ppmw
at the point of waste origination, the average volumetric flow rate
of hazardous waste and the density of the hazardous waste stream
at the point of waste origination must be determined.
D)
The required organic mass removal rate (RMR) for the hazardous
waste must be calculated by using the average VO concentration,
average volumetric flow rate, and density determined for each
individual hazardous waste stream, and the following equation:
RMR
=
n
y= 1
V
xk x
(
C
- 500ppmw)
10
yy
y
∑
6
RMR =
n
y=1
Vxk
x
(C - 500ppmw)
10
yy
y
∑
6
Where:
RMR =
Required organic mass removal rate, in kg/hr.
y = Individual hazardous waste stream “y” that has an average
volatile organic (VO) concentration equal to or greater
318
than 500 ppmw at the point of waste origination, as
determined in accordance with the requirements of
subsection (a) of this Section.
n = Total number of “y” hazardous waste streams treated by
process.
Vy = Average volumetric flow rate of hazardous waste stream
“y” at the point of waste origination, in m
3
/hr.
ky = Density of hazardous waste stream “y”, in kg/m
3
C
y
= Average VO concentration of hazardous waste stream “y”
at the point of waste origination, as determined in
accordance with the requirements of subsection (a) of this
Section, in ppmw.
8)
Procedure to determine the actual organic mass removal rate (MR) for a
treated hazardous waste.
A)
The actual organic mass removal rate (MR) must be determined
based on results for a minimum of three consecutive runs. The
sampling time for each run must be one hour.
B)
The waste volatile organic mass flow entering the process (Eb)
and the waste volatile organic mass flow exiting the process (Ea)
must be determined in accordance with the requirements of
subsection (b)(5)(D) of this Section.
C)
The actual organic mass removal rate (MR) must be calculated by
using the mass flow rate determined in accordance with the
requirements of subsection (b)(8)(B) of this Section and the
following equation:
MR
=
E
b
-E
a
MR =E
b
-E
a
Where:
MR = Actual organic mass removal rate, in kg/hr.
Eb = Waste volatile organic mass flow entering the
process, as determined in accordance with the
319
requirements of subsection (b)(5)(D) of this
Section, in kg/hr.
Ea = Waste volatile organic mass flow exiting the
process, as determined in accordance with the
requirements of subsection (b)(5)(D) of this
Section, in kg/hr.
9)
Procedure to determine the actual organic mass biodegradation rate
(MRbio) for a treated hazardous waste.
A)
The actual organic mass biodegradation rate (MRbio) must be
determined based on results for a minimum of three consecutive
runs. The sampling time for each run must be one hour.
B)
The waste organic mass flow entering the process (Eb) must be
determined in accordance with the requirements of subsection
(b)(5)(D) of this Section.
C)
The fraction of organic biodegraded (Fbio) must be determined
using the procedure specified in 40 CFR 63, Appendix C,
incorporated by reference in 35 Ill. Adm. Code 720.111.
D)
The actual organic mass biodegradation rate (MRbio) must be
calculated by using the mass flow rates and fraction of organic
biodegraded, as determined in accordance with the requirements
of subsections (b)(9)(B) and (b)(9)(C) of this Section,
respectively, and the following equation:
MR
bio
=
E
b
x
F
bio
MR
bio
=
E
b
x
F
bio
Where:
MRbio = Actual organic mass biodegradation rate, in
kg/hr.
Eb = Waste organic mass flow entering the process, as
determined in accordance with the requirements of
subsection (b)(5)(D) of this Section, in kg/hr.
Fbio = Fraction of organic biodegraded, as determined in
accordance with the requirements of subsection
(b)(9)(C) of this Section.
320
c)
Procedure to determine the maximum organic vapor pressure of a hazardous
waste in a tank.
1)
An owner or operator shall determine the maximum organic vapor
pressure for each hazardous waste placed in a tank using Tank Level 1
controls in accordance with standards specified in Section 725.985(c).
2)
An owner or operator shall use either direct measurement, as specified in
subsection (c)(3) of this Section, or knowledge of the waste, as specified
by subsection (c)(4) of this Section, to determine the maximum organic
vapor pressure that is representative of the hazardous waste composition
stored or treated in the tank.
3)
Direct measurement to determine the maximum organic vapor pressure
of a hazardous waste.
A)
Sampling. A sufficient number of samples must be collected to
be representative of the waste contained in the tank. All samples
must be conducted and handled in accordance with written
procedures prepared by the owner or operator and documented in
a site sampling plan. This plan must describe the procedure by
which representative samples of the hazardous waste are collected
such that a minimum loss of organics occurs throughout the
sample collection and handling process and by which sample
integrity is maintained. A copy of the written sampling plan
must be maintained on-site in the facility operating records. An
example of an acceptable sampling plan includes a plan
incorporating sample collection and handling procedures in
accordance with the requirements specified in “Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods”, USEPA
Publication No. SW-846, incorporated by reference in 35 Ill.
Adm. Code 720.111, or in Method 25D in 40 CFR 60, appendix
A, incorporated by reference in 35 Ill. Adm. Code 720.111.
B)
Analysis. Any appropriate one of the following methods may be
used to analyze the samples and compute the maximum organic
vapor pressure of the hazardous waste:
i)
Method 25E in 40 CFR 60, Appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111;
ii)
Methods described in American Petroleum Institute
Publication 2517, incorporated by reference in 35 Ill.
Adm. Code 720.111;
321
iii)
Methods obtained from standard reference texts;
iv)
ASTM Method D 2879-92, incorporated by reference in
35 Ill. Adm. Code 720.111; or
v)
Any other method approved by the Agency.
4)
Use of knowledge to determine the maximum organic vapor pressure of
the hazardous waste. Documentation must be prepared and recorded that
presents the information used as the basis for the owner’s or operator’s
knowledge that the maximum organic vapor pressure of the hazardous
waste is less than the maximum vapor pressure limit listed in Section
725.985(b)(1)(A) for the applicable tank design capacity category. An
example of information that may be used is documentation that the
hazardous waste is generated by a process for which at other locations it
previously has been determined by direct measurement that the waste
maximum organic vapor pressure is less than the maximum vapor
pressure limit for the appropriate tank design capacity category.
d)
Procedure for determining no detectable organic emissions for the purpose of
complying with this Subpart:
1)
The test must be conducted in accordance with the procedures specified
in Method 21 of 40 CFR 60, appendix A, incorporated by reference in
35 Ill. Adm. Code 720.111. Each potential leak interface (i.e., a
location where organic vapor leakage could occur) on the cover and
associated closure devices must be checked. Potential leak interfaces
that are associated with covers and closure devices include, but are not
limited to any of the following: the interface of the cover and its
foundation mounting, the periphery of any opening on the cover and its
associated closure device, and the sealing seat interface on a spring-
loaded pressure relief valve.
2)
The test must be performed when the unit contains a hazardous waste
having an organic concentration representative of the range of
concentrations for the hazardous waste expected to be managed in the
unit. During the test, the cover and closure devices must be secured in
the closed position.
3)
The detection instrument must meet the performance criteria of Method
21 of 40 CFR 60, appendix A, incorporated by reference in 35 Ill. Adm.
Code 720.111, except the instrument response factor criteria in Section
3.1.2(a) of Method 21 must be for the average composition of the
322
organic constituents in the hazardous waste placed in the waste
management unit, not for each individual organic constituent.
4)
The detection instrument must be calibrated before use on each day of its
use by the procedures specified in Method 21 of 40 CFR 60, appendix
A, incorporated by reference in 35 Ill. Adm. Code 720.111.
5)
Calibration gases must be as follows:
A)
Zero air (less than 10 ppmv hydrocarbon in air), and
B)
A mixture of methane or n-hexane in air at a concentration of
approximately, but less than, 10,000 ppmv methane or n-hexane.
6)
The background level must be determined according to the procedures in
Method 21 of 40 CFR 60, appendix A, incorporated by reference in 35
Ill. Adm. Code 720.111.
7)
Each potential leak interface must be checked by traversing the
instrument probe around the potential leak interface as close to the
interface as possible, as described in Method 21 of 40 CFR 60, appendix
A, incorporated by reference in 35 Ill. Adm. Code 720.111. In the case
when the configuration of the cover or closure device prevents a
complete traverse of the interface, all accessible portions of the interface
must be sampled. In the case when the configuration of the closure
device prevents any sampling at the interface and the device is equipped
with an enclosed extension or horn (e.g., some pressure relief devices),
the instrument probe inlet must be placed at approximately the center of
the exhaust area to the atmosphere.
8)
The arithmetic difference between the maximum organic concentration
indicated by the instrument and the background level must be compared
with the value of 500 ppmv except when monitoring a seal around a
rotating shaft that passes through a cover opening, in which case the
comparison must be as specified in subsection (d)(9) of this Section. If
the difference is less than 500 ppmv, then the potential leak interface is
determined to operate with no detectable organic emissions.
9)
For the seals around a rotating shaft that passes through a cover opening,
the arithmetic difference between the maximum organic concentration
indicated by the instrument and the background level must be compared
with the value of 10,000 ppmw. If the difference is less than 10,000
ppmw, then the potential leak interface is determined to operate with no
detectable organic emissions.
323
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.985
Standards: Tanks
a)
The provisions of this Section apply to the control of air pollutant emissions
from tanks for which Section 725.983(b) references the use of this Section for
such air emission control.
b)
The owner or operator shall control air pollutant emissions from each tank
subject to this Section in accordance with the following requirements, as
applicable:
1)
For a tank that manages hazardous waste which meets all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank in accordance with the Tank Level 1 controls specified in
subsection (c) of this Section or the Tank Level 2 controls specified in
subsection (d) of this Section.
A)
The hazardous waste in the tank has a maximum organic vapor
pressure that is less than the maximum organic vapor pressure
limit for the tank’s design capacity category, as follows:
i)
For a tank design capacity equal to or greater than 151 m
3
(5333 ft
3
or 39,887 gal), the maximum organic vapor
pressure limit for the tank is 5.2 kPa (0.75 psia or 39 mm
Hg);
ii)
For a tank design capacity equal to or greater than 75 m
3
(2649 ft
3
or 19,810 gal) but less than 151 m
3
(5333 ft
3
or
39,887 gal), the maximum organic vapor pressure limit
for the tank is 27.6 kPa (4.0 psia or 207 mm Hg); or
iii)
For a tank design capacity less than 75 m
3
(2649 ft
3
or
19,810 gal), the maximum organic vapor pressure limit
for the tank is 76.6 kPa (11.1 psia or 574 mm Hg).
B)
The hazardous waste in the tank is not heated by the owner or
operator to a temperature that is greater than the temperature at
which the maximum organic vapor pressure of the hazardous
waste is determined for the purpose of complying with subsection
(b)(1)(A) of this Section.
324
C)
The hazardous waste in the tank is not treated by the owner or
operator using a waste stabilization process, as defined in Section
725.981.
2)
For a tank that manages hazardous waste that does not meet all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank by using Tank Level 2 controls in accordance with the
requirements of subsection (d) of this Section. Examples of tanks
required to use Tank Level 2 controls include the following: a tank used
for a waste stabilization process and a tank for which the hazardous
waste in the tank has a maximum organic vapor pressure that is equal to
or greater than the maximum organic vapor pressure limit for the tank’s
design capacity category, as specified in subsection (b)(1)(A) of this
Section.
c)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 1 controls shall meet the requirements specified in subsections (c)(1)
through (c)(4) of this Section:
1)
The owner or operator shall determine the maximum organic vapor
pressure for a hazardous waste to be managed in the tank using Tank
Level 1 controls before the first time the hazardous waste is placed in the
tank. The maximum organic vapor pressure must be determined using
the procedures specified in Section 725.984(c). Thereafter, the owner or
operator shall perform a new determination whenever changes to the
hazardous waste managed in the tank could potentially cause the
maximum organic vapor pressure to increase to a level that is equal to or
greater than the maximum organic vapor pressure limit for the tank
design capacity category specified in subsection (b)(1)(A) of this
Section, as applicable to the tank.
2)
The tank must be equipped with a fixed roof designed to meet the
following specifications:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the hazardous
waste in the tank. The fixed roof may be a separate cover
installed on the tank (e.g., a removable cover mounted on an
open-top tank) or may be an integral part of the tank structural
design (e.g., a horizontal cylindrical tank equipped with a hatch).
B)
The fixed roof must be installed in a manner such that there are
no visible cracks, holes, gaps, or other open spaces between roof
325
section joints or between the interface of the roof edge and the
tank wall.
C)
Each Either of the following must be true of each opening in the
fixed roof and of any manifold system associated with the fixed roof
must be either:
i)
Equipped The opening or manifold system is equipped
with a closure device designed to operate such that when
the closure device is secured in the closed position there
are no visible cracks, holes, gaps, or other open spaces in
the closure device or between the perimeter of the opening
and the closure device; or
ii)
Connected The opening or manifold system is connected
by a closed-vent system that is vented to a control device.
The control device must remove or destroy organics in the
vent stream, and it must be operating whenever hazardous
waste is managed in the tank, except as provided for in
subsection (c)(2)(E).
D)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and which will maintain
the integrity of the fixed roof and closure devices throughout
their intended service life. Factors to be considered when
selecting the materials for and designing the fixed roof and
closure devices must include the following: organic vapor
permeability; the effects of any contact with the hazardous waste
or its vapors managed in the tank; the effects of outdoor exposure
to wind, moisture, and sunlight; and the operating practices used
for the tank on which the fixed roof is installed.
E)
The control device operated pursuant to subsection (c)(2)(C) of
this Section needs not remove or destroy organics in the vent
stream under the following conditions:
i)
During periods when it is necessary to provide access to the
tank for performing the activities of subsection (c)(2)(E)(ii) of
this Section, venting of the vapor headspace underneath the
fixed roof to the control device is not required, opening of
closure devices is allowed, and removal of the fixed roof is
allowed. Following completion of the activity, the owner or
operator shall promptly secure the closure device in the
closed position or reinstall the cover, as applicable, and
resume operation of the control device; and
326
ii)
During periods of routine inspection, maintenance, or other
activities needed for normal operations, and for the removal
of accumulated sludge or other residues from the bottom of
the tank.
BOARD NOTE: Subsections (c)(2)(E)(i) and (c)(2)(E)(ii) are
derived from 40 CFR 265.985(c)(2)(iii)(B)(1) and
(c)(2)(iii)(B)(2), which the Board has codified here to comport
with Illinois Administrative Code format requirements.
3)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position, except
as follows:
A)
Opening of closure devices or removal of the fixed roof is
allowed at the following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
the liquid in the tank, or when a worker needs to open a
hatch to maintain or repair equipment. Following
completion of the activity, the owner or operator shall
promptly secure the closure device in the closed position
or reinstall the cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of tank.
B)
Opening of a spring-loaded pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the tank internal pressure in
accordance with the tank design specifications. The device must
be designed to operate with no detectable organic emissions when
the device is secured in the closed position. The settings at which
the device opens must be established such that the device remains
in the closed position whenever the tank internal pressure is
within the internal pressure operating range determined by the
owner or operator based on the tank manufacturer
recommendations; applicable regulations; fire protection and
prevention codes; standard engineering codes and practices; or
other requirements for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples of normal
327
operating conditions that may require these devices to open are
during those times when the tank internal pressure exceeds the
internal pressure operating range for the tank as a result of
loading operations or diurnal ambient temperature fluctuations.
C)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
4)
The owner or operator shall inspect the air emission control equipment
in accordance with the following requirements.
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof sections or between the
roof and the tank wall; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
fixed roof and its closure devices on or before the date that the
tank becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year,
except under the special conditions provided for in subsection (l)
of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
d)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 2 controls shall use one of the following tanks:
1)
A fixed-roof tank equipped with an internal floating roof in accordance
with the requirements specified in subsection (e) of this Section;
2)
A tank equipped with an external floating roof in accordance with the
requirements specified in subsection (f) of this Section;
328
3)
A tank vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (g) of this
Section;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) of this Section; or
5)
A tank located inside an enclosure that is vented through a closed-vent
system to an enclosed combustion control device in accordance with the
requirements specified in subsection (i) of this Section.
e)
The owner or operator that controls air pollutant emissions from a tank using a
fixed roof with an internal floating roof shall meet the requirements specified in
subsections (e)(1) through (e)(3) of this Section.
1)
The tank must be equipped with a fixed roof and an internal floating roof
in accordance with the following requirements:
A)
The internal floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The internal floating roof must be equipped with a continuous
seal between the wall of the tank and the floating roof edge that
meets either of the following requirements:
i)
A single continuous seal that is either a liquid-mounted
seal or a metallic shoe seal, as defined in Section
725.981; or
ii)
Two continuous seals mounted one above the other. The
lower seal may be a vapor-mounted seal.
C)
The internal floating roof must meet the following specifications:
i)
Each opening in a noncontact internal floating roof except
for automatic bleeder vents (vacuum breaker vents) and
the rim space vents is to provide a projection below the
liquid surface.
ii)
Each opening in the internal floating roof must be
equipped with a gasketed cover or a gasketed lid except
for leg sleeves, automatic bleeder vents, rim space vents,
column wells, ladder wells, sample wells, and stub drains.
329
iii)
Each penetration of the internal floating roof for the
purpose of sampling must have a slit fabric cover that
covers at least 90 percent of the opening.
iv)
Each automatic bleeder vent and rim space vent must be
gasketed.
v)
Each penetration of the internal floating roof that allows
for passage of a ladder must have a gasketed sliding
cover.
vi)
Each penetration of the internal floating roof that allows
for passage of a column supporting the fixed roof must
have a flexible fabric sleeve seal or a gasketed sliding
cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
C)
Prior to filling the tank, each cover, access hatch, gauge float
well or lid on any opening in the internal floating roof must be
bolted or fastened closed (i.e., no visible gaps). Rim space vents
are to be set to open only when the internal floating roof is not
floating or when the pressure beneath the rim exceeds the
manufacturer’s recommended setting.
3)
The owner or operator shall inspect the internal floating roof in
accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects that could
result in air pollutant emissions. Defects include, but are not
limited to, the following: when the internal floating roof is not
floating on the surface of the liquid inside the tank; when liquid
has accumulated on top of the internal floating roof; when any
portion of the roof seals have detached from the roof rim; when
holes, tears, or other openings are visible in the seal fabric; when
330
the gaskets no longer close off the hazardous waste surface from
the atmosphere; or when the slotted membrane has more than 10
percent open area.
B)
The owner or operator shall inspect the internal floating roof
components as follows, except as provided in subsection
(e)(3)(C) of this Section:
i)
Visually inspect the internal floating roof components
through openings on the fixed roof (e.g., manholes and
roof hatches) at least once every 12 months after initial
fill, and
ii)
Visually inspect the internal floating roof, primary seal,
secondary seal (if one is in service), gaskets, slotted
membranes, and sleeve seals (if any) each time the tank is
emptied and degassed and at least once every 10 years.
C)
As an alternative to performing the inspections specified in
subsection (e)(3)(B) of this Section for an internal floating roof
equipped with two continuous seals mounted one above the other,
the owner or operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted membranes,
and sleeve seals (if any) each time the tank is emptied and
degassed and at least every five years.
D)
Prior to each inspection required by subsection (e)(3)(B) or
(e)(3)(C) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each visual inspection of an internal floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned, as provided for in subsection
(e)(3)(D)(ii) of this Section.
ii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
331
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Regional Administrator at least seven calendar days before
refilling the tank.
E)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
F)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
4)
Safety devices, as defined in Section 725.981, may be installed and operated
as necessary on any tank complying with the requirements of this subsection
(e).
f)
The owner or operator that controls air pollutant emissions from a tank using an
external floating roof shall meet the requirements specified in subsections (f)(1)
through (f)(3) of this Section.
1)
The owner or operator shall design the external floating roof in
accordance with the following requirements:
A)
The external floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The floating roof must be equipped with two continuous seals,
one above the other, between the wall of the tank and the roof
edge. The lower seal is referred to as the primary seal, and the
upper seal is referred to as the secondary seal.
i)
The primary seal must be a liquid-mounted seal or a
metallic shoe seal, as defined in Section 725.981. The
total area of the gaps between the tank wall and the
primary seal must not exceed 212 square centimeters
(cm
2
) per meter (10.0 in
2
per foot) of tank diameter, and
the width of any portion of these gaps must not exceed
3.8 centimeters (cm) (1.5 inches). If a metallic shoe seal
is used for the primary seal, the metallic shoe seal must be
designed so that one end extends into the liquid in the tank
332
and the other end extends a vertical distance of at least 61
centimeters above the liquid surface.
ii)
The secondary seal must be mounted above the primary
seal and cover the annular space between the floating roof
and the wall of the tank. The total area of the gaps
between the tank wall and the secondary seal must not
exceed 21.2 cm
2
per meter (1.0 in
2
per foot) of tank
diameter, and the width of any portion of these gaps must
not exceed 1.3 cm (0.5 inch).
C)
The external floating roof must meet the following specifications:
i)
Except for automatic bleeder vents (vacuum breaker
vents) and rim space vents, each opening in a noncontact
external floating roof must provide a projection below the
liquid surface.
ii)
Except for automatic bleeder vents, rim space vents, roof
drains, and leg sleeves, each opening in the roof must be
equipped with a gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must be
equipped with a cover designed to be bolted or fastened
when the cover is secured in the closed position.
iv)
Each automatic bleeder vent and each rim space vent must
be equipped with a gasket.
v)
Each roof drain that empties into the liquid managed in
the tank must be equipped with a slotted membrane fabric
cover that covers at least 90 percent of the area of the
opening.
vi)
Each unslotted and slotted guide pole well must be
equipped with a gasketed sliding cover or a flexible fabric
sleeve seal.
vii)
Each unslotted guide pole must be equipped with a
gasketed cap on the end of the pole.
viii) Each slotted guide pole must be equipped with a gasketed
float or other device which closes off the liquid surface
from the atmosphere.
333
ix)
Each gauge hatch and each sample well must be equipped
with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents, roof drains,
and leg sleeves, each opening in the roof must be secured and
maintained in a closed position at all times except when the
closure device must be open for access.
C)
Covers on each access hatch and each gauge float well must be
bolted or fastened when secured in the closed position.
D)
Automatic bleeder vents must be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
E)
Rim space vents must be set to open only at those times that the
roof is being floated off the roof leg supports or when the
pressure beneath the rim seal exceeds the manufacturer’s
recommended setting.
F)
The cap on the end of each unslotted guide pole must be secured
in the closed position at all times except when measuring the
level or collecting samples of the liquid in the tank.
G)
The cover on each gauge hatch or sample well must be secured in
the closed position at all times except when the hatch or well
must be opened for access.
H)
Both the primary seal and the secondary seal must completely
cover the annular space between the external floating roof and the
wall of the tank in a continuous fashion except during
inspections.
3)
The owner or operator shall inspect the external floating roof in
accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external floating roof
seal gaps in accordance with the following requirements:
334
i)
The owner or operator shall perform measurements of
gaps between the tank wall and the primary seal within 60
calendar days after initial operation of the tank following
installation of the floating roof and, thereafter, at least
once every five years.
ii)
The owner or operator shall perform measurements of
gaps between the tank wall and the secondary seal within
60 calendar days after initial operation of the tank
following installation of the floating roof and, thereafter,
at least once every year.
iii)
If a tank ceases to hold hazardous waste for a period of
one year or more, subsequent introduction of hazardous
waste into the tank must be considered an initial operation
for the purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) of this Section.
iv)
The owner or operator shall determine the total surface
area of gaps in the primary seal and in the secondary seal
individually using the procedure set forth in subsection
(f)(4)(D) of this Section.
v)
In the event that the seal gap measurements do not
conform to the specifications in subsection (f)(1)(B) of
this Section, the owner or operator must repair the defect
in accordance with the requirements of subsection (k) of
this Section.
vi)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 725.990(b).
B)
The owner or operator shall visually inspect the external floating
roof in accordance with the following requirements:
i)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects
include, but are not limited to any of the following:
holes, tears, or other openings in the rim seal or seal
fabric of the floating roof; a rim seal detached from the
floating roof; all or a portion of the floating roof deck
being submerged below the surface of the liquid in the
335
tank; broken, cracked, or otherwise damaged seals or
gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
ii)
The owner or operator shall perform an initial inspection
of the external floating roof and its closure devices on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall perform
the inspections at least once every year except for the
special conditions provided for in subsection (l) of this
Section.
iii)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k) of this Section.
iv)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 725.990(b).
C)
Prior to each inspection required by subsection (f)(3)(A) or
(f)(3)(B) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each inspection to measure external floating roof
seal gaps as required under subsection (f)(3)(A) of this
Section, written notification must be prepared and sent by
the owner or operator so that it is received by the Agency
at least 30 calendar days before the date the measurements
are scheduled to be performed.
ii)
Prior to each visual inspection of an external floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank except when an
inspection is not planned, as provided for in subsection
(f)(3)(C)(iii) of this Section.
iii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
336
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Regional Administrator at least seven calendar days before
refilling the tank.
D)
Procedure for determining gaps in the primary seal and in the
secondary seal for the purposes of subsection (f)(3)(A)(iv) of this
Section:
i)
The seal gap measurements must be performed at one or
more floating roof levels when the roof is floating off the
roof supports.
ii)
Seal gaps, if any, must be measured around the entire
perimeter of the floating roof in each place where a 0.32-
cm (¼-inch) diameter uniform probe passes freely
(without forcing or binding against the seal) between the
seal and the wall of the tank and measure the
circumferential distance of each such location.
iii)
For a seal gap measured under this subsection (f)(3), the
gap surface area must be determined by using probes of
various widths to measure accurately the actual distance
from the tank wall to the seal and multiplying each such
width by its respective circumferential distance.
iv)
The total gap area must be calculated by adding the gap
surface areas determined for each identified gap location
for the primary seal and the secondary seal individually,
and then dividing the sum for each seal type by the
nominal perimeter diameter of the tank. These total gap
areas for the primary seal and secondary seal are then
compared to the respective standards for the seal type, as
specified in subsection (f)(1)(B) of this Section.
BOARD NOTE: Subsections (f)(3)(D)(i) through (f)(3)(D)(iv)
correspond with are derived from 40 CFR
265.1085(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4), which the Board
has codified here to comport with Illinois Administrative Code
format requirements.
337
4)
Safety devices, as defined in Section 725.981, may be installed and operated
as necessary on any tank complying with the requirements of this subsection
(f).
g)
The owner or operator that controls air pollutant emissions from a tank by
venting the tank to a control device shall meet the requirements specified in
subsections (g)(1) through (g)(3) of this Section.
1)
The tank must be covered by a fixed roof and vented directly through a
closed-vent system to a control device in accordance with the following
requirements:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
tank.
B)
Each opening in the fixed roof not vented to the control device
must be equipped with a closure device. If the pressure in the
vapor headspace underneath the fixed roof is less than
atmospheric pressure when the control device is operating, the
closure devices must be designed to operate such that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device. If the pressure in the vapor headspace underneath
the fixed roof is equal to or greater than atmospheric pressure
when the control device is operating, the closure device must be
designed to operate with no detectable organic emissions.
C)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: organic vapor permeability; the
effects of any contact with the liquid and its vapor managed in
the tank; the effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the tank on which
the fixed roof is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 725.988.
338
2)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position and the
vapor headspace underneath the fixed roof vented to the control device
except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the fixed roof is allowed at the
following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to open a hatch
to maintain or repair equipment. Following completion of
the activity, the owner or operator shall promptly secure
the closure device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of a tank.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to
any of the following: visible cracks, holes, or gaps in the roof
sections or between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure devices; and
broken or missing hatches, access covers, caps, or other closure
devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 725.988.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the tank
becomes subject to this Section. Thereafter, the owner or
339
operator shall perform the inspections at least once every year
except for the special conditions provided for in subsection (l) of
this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
h)
The owner or operator that controls air pollutant emissions by using a pressure
tank must meet the following requirements.
1)
The tank shall be designed not to vent to the atmosphere as a result of
compression of the vapor headspace in the tank during filling of the tank
to its design capacity.
2)
All tank openings must be equipped with closure devices designed to
operate with no detectable organic emissions as determined using the
procedure specified in Section 725.984(d).
3)
Whenever a hazardous waste is in the tank, the tank must be operated as
a closed system that does not vent to the atmosphere except in the event
that a safety device, as defined in Section 725.981, is required to open to
avoid an unsafe condition.
i)
The owner or operator that controls air pollutant emissions by using an
enclosure vented through a closed-vent system to an enclosed combustion
control device shall meet the requirements specified in subsections (i)(1) through
(i)(4) of this Section.
1)
The tank must be located inside an enclosure. The enclosure must be
designed and operated in accordance with the criteria for a permanent
total enclosure, as specified in “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure” under 40
CFR 52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the verification
procedure for the enclosure as specified in Section 5.0 to “Procedure T--
Criteria for and Verification of a Permanent or Temporary Total
340
Enclosure” initially when the enclosure is first installed and, thereafter,
annually.
2)
The enclosure must be vented through a closed-vent system to an
enclosed combustion control device that is designed and operated in
accordance with the standards for either a vapor incinerator, boiler, or
process heater specified in Section 725.988.
3)
Safety devices, as defined in Section 725.981, may be installed and
operated as necessary on any enclosure, closed-vent system, or control
device used to comply with the requirements of subsections (i)(1) and
(i)(2) of this Section.
4)
The owner or operator shall inspect and monitor the closed-vent system
and control device, as specified in Section 725.988.
j)
The owner or operator shall transfer hazardous waste to a tank subject to this
Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (j)(2) of
this Section, to the tank from another tank subject to this Section or from
a surface impoundment subject to Section 725.986 must be conducted
using continuous hard-piping or another closed system that does not
allow exposure of the hazardous waste to the atmosphere. For the
purpose of complying with this provision, an individual drain system is
considered to be a closed system when it meets the requirements of 40
CFR 63, subpart RR, “National Emission Standards for Individual Drain
Systems”, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) of this Section do not apply when
transferring a hazardous waste to the tank under any of the following
conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
725.983(c)(2).
C)
The hazardous waste meets the requirements of Section
725.983(c)(4).
341
k)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(4), (e)(3),
(f)(3), or (g)(3) of this Section as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair shall be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (k)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the tank and no alternative tank
capacity is available at the site to accept the hazardous waste normally
managed in the tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating the hazardous
waste managed in the tank stops operation. Repair of the defect must be
completed before the process or unit resumes operation.
l)
Following the initial inspection and monitoring of the cover as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year under the following special
conditions:
1)
Where inspecting or monitoring the cover would expose a worker to
dangerous, hazardous, or other unsafe conditions, then the owner or
operator may designate a cover as an “unsafe to inspect and monitor
cover” and comply with all of the following requirements:
A)
Prepare a written explanation for the cover stating the reasons
why the cover is unsafe to visually inspect or to monitor, if
required.
B)
Develop and implement a written plan and schedule to inspect
and monitor the cover, using the procedures specified in the
applicable Section of this Subpart, as frequently as practicable
during those times when a worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely underground, an
owner or operator is required to inspect and monitor, as required by the
applicable provisions of this Section, only those portions of the tank
cover and those connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground surface.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
342
Section 725.986
Standards: Surface Impoundments
a)
The provisions of this Section apply to the control of air pollutant emissions
from surface impoundments for which Section 725.983(b) of this Subpart
references the use of this Section for such air emission control.
b)
The owner or operator shall control air pollutant emissions from the surface
impoundment by installing and operating either of the following:
1)
A floating membrane cover in accordance with the provisions specified
in subsection (c) of this Section; or
2)
A cover that is vented through a closed-vent system to a control device
in accordance with the provisions requirements specified in subsection (d)
of this Section.
c)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a floating membrane cover must meet the requirements
specified in subsections (c)(1) through (c)(3) of this Section.
1)
The surface impoundment must be equipped with a floating membrane
cover designed to meet the following specifications:
A)
The floating membrane cover must be designed to float on the
liquid surface during normal operations and form a continuous
barrier over the entire surface area of the liquid.
B)
The cover must be fabricated from a synthetic membrane material
that is either:
i)
High density polyethylene (HDPE) with a thickness no
less than 2.5 millimeters (mm) (0.10 inch); or
ii)
A material or a composite of different materials
determined to have both organic permeability properties
that are equivalent to those of the material listed in
subsection (c)(1)(B)(i) of this Section and chemical and
physical properties that maintain the material integrity for
the intended service life of the material.
C)
The cover must be installed in a manner such that there are no
visible cracks, holes, gaps, or other open spaces between cover
section seams or between the interface of the cover edge and its
foundation mountings.
343
D)
Except as provided for in subsection (c)(1)(E) of this Section,
each opening in the floating membrane cover must be equipped
with a closure device so designed as to operate that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device.
E)
The floating membrane cover may be equipped with one or more
emergency cover drains for removal of stormwater. Each
emergency cover drain must be equipped with a slotted
membrane fabric cover that covers at least 90 percent of the area
of the opening or a flexible fabric sleeve seal.
F)
The closure devices must be made of suitable materials that will
minimize exposure of the hazardous waste to the atmosphere, to
the extent practical, and will maintain the integrity of the closure
devices throughout their intended service life. Factors to be
considered when selecting the materials of construction and
designing the cover and closure devices must include the
following: the organic vapor permeability; the effects of any
contact with the liquid and its vapor managed in the surface
impoundment; the effects of outdoor exposure to wind, moisture,
and sunlight; and the operating practices used for the surface
impoundment on which the floating membrane cover is installed.
2)
Whenever a hazardous waste is in the surface impoundment, the floating
membrane cover must float on the liquid and each closure device must
be secured in the closed position except as follows:
A)
Opening of closure devices or removal of the cover is allowed at
the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample the liquid in the surface impoundment, or
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly replace the cover and
secure the closure device in the closed position, as
applicable.
344
ii)
To remove accumulated sludge or other residues from the
bottom of surface impoundment.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect the floating membrane cover in
accordance with the following procedures:
A)
The floating membrane cover and its closure devices must be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
floating membrane cover and its closure devices on or before the
date that the surface impoundment becomes subject to this
Section. Thereafter, the owner or operator shall perform the
inspections at least once every year except for the special
conditions provided for in subsection (g) of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(c).
d)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a cover vented to a control device shall meet the
requirements specified in subsections (d)(1) through (d)(3) of this Section.
1)
The surface impoundment must be covered by a cover and vented
directly through a closed-vent system to a control device in accordance
with the following requirements:
A)
The cover and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
surface impoundment.
345
B)
Each opening in the cover not vented to the control device must
be equipped with a closure device. If the pressure in the vapor
headspace underneath the cover is less than atmospheric pressure
when the control device is operating, the closure devices must be
designed to operate such that when the closure device is secured
in the closed position there are no visible cracks, holes, gaps, or
other open spaces in the closure device or between the perimeter
of the cover opening and the closure device. If the pressure in
the vapor headspace underneath the cover is equal to or greater
than atmospheric pressure when the control device is operating,
the closure device must be designed to operate with no detectable
organic emissions using the procedure specified in Section
725.984(d).
C)
The cover and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and which will maintain
the integrity of the cover and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for of construction and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the liquid or its
vapors managed in the surface impoundment; the effects of
outdoor exposure to wind, moisture, and sunlight; and the
operating practices used for the surface impoundment on which
the cover is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 725.988.
2)
Whenever a hazardous waste is in the surface impoundment, the cover
must be installed with each closure device secured in the closed position
and the vapor headspace underneath the cover vented to the control
device except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the cover is allowed at the
following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample liquid in the surface impoundment, or
346
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as
applicable, to the surface impoundment.
ii)
To remove accumulated sludge or other residues from the
bottom of the surface impoundment.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The surface impoundment cover and its closure devices must be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 725.988.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the
surface impoundment becomes subject to this Section.
Thereafter, the owner or operator shall perform the inspections at
least once every year except for the special conditions provided
for in subsection (g) of this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(c).
347
e)
The owner or operator shall transfer hazardous waste to a surface impoundment
subject to this Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (e)(2) of
this Section, to the surface impoundment from another surface
impoundment subject to this Section or from a tank subject to Section
725.985 must be conducted using continuous hard-piping or another
closed system that does not allow exposure of the waste to the
atmosphere. For the purpose of complying with this provision, an
individual drain system is considered to be a closed system when it meets
the requirements of 40 CFR 63, Subpart RR, “National Emission
Standards for Individual Drain Systems”, incorporated by reference in
35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (e)(1) of this Section do not apply when
transferring a hazardous waste to the surface impoundment under either
any of the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
725.983(c)(2).
C)
The hazardous waste meets the requirements of Section
725.983(c)(4).
f)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(3) or (d)(3) of
this Section as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair must be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (f)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the surface impoundment and no
alternative capacity is available at the site to accept the hazardous waste
normally managed in the surface impoundment. In this case, the owner
or operator shall repair the defect the next time the process or unit that is
generating the hazardous waste managed in the tank stops operation.
348
Repair of the defect must be completed before the process or unit
resumes operation.
g)
Following the initial inspection and monitoring of the cover as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year in the case when inspecting or
monitoring the cover would expose a worker to dangerous, hazardous, or other
unsafe conditions. In this case, the owner or operator may designate the cover
as an “unsafe to inspect and monitor cover” and comply with all of the
following requirements:
1)
Prepare a written explanation for the cover stating the reasons why the
cover is unsafe to visually inspect or to monitor, if required.
2)
Develop and implement a written plan and schedule to inspect and
monitor the cover using the procedures specified in the applicable
Section of this Subpart as frequently as practicable during those times
when a worker can safely access the cover.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.987
Standards: Containers
a)
The provisions of this Section apply to the control of air pollutant emissions
from containers for which Section 725.983(b) references the use of this Section
for such air emission control.
b)
General requirements.
1)
The owner or operator shall control air pollutant emissions from each
container subject to this Section in accordance with the following
requirements, as applicable to the container, except when the special
provisions for waste stabilization processes specified in subsection (b)(2)
of this Section apply to the container.
A)
For a container having a design capacity greater than 0.1 m
3
(26
gal) and less than or equal to 0.46 m
3
(120 gal), the owner or
operator shall control air pollutant emissions from the container
in accordance with the Container Level 1 standards specified in
subsection (c) of this Section.
B)
For a container having a design capacity greater than 0.46 m
3
(120 gal) that is not in light material service, the owner or
operator shall control air pollutant emissions from the container
349
in accordance with the Container Level 1 standards specified in
subsection (c) of this Section.
C)
For a container having a design capacity greater than 0.46 m
3
(120 gal) that is in light material service, the owner or operator
shall control air pollutant emissions from the container in
accordance with the Container Level 2 standards specified in
subsection (d) of this Section.
2)
When a container having a design capacity greater than 0.1 m
3
(26 gal)
is used for treatment of a hazardous waste by a waste stabilization
process, the owner or operator shall control air pollutant emissions from
the container in accordance with the Container Level 3 standards
specified in subsection (e) of this Section at those times during the waste
stabilization process when the hazardous waste in the container is
exposed to the atmosphere.
c)
Container Level 1 standards.
1)
A container using Container Level 1 controls is one of the following:
A)
A container that meets the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous
materials for transportation, as specified in subsection (f) of this
Section.
B)
A container equipped with a cover and closure devices that form
a continuous barrier over the container openings so that when the
cover and closure devices are secured in the closed position there
are no visible holes, gaps, or other open spaces into the interior
of the container. The cover may be a separate cover installed on
the container (e.g., a lid on a drum or a suitably secured tarp on
a roll-off box) or may be an integral part of the container
structural design (e.g., a “portable tank” or bulk cargo container
equipped with a screw-type cap).
C)
An open-top container in which an organic-vapor suppressing
barrier is placed on or over the hazardous waste in the container
such that no hazardous waste is exposed to the atmosphere. One
example of such a barrier is application of a suitable organic-
vapor suppressing foam.
2)
A container used to meet the requirements of subsection (c)(1)(B) or
(c)(1)(C) of this Section must be equipped with covers and closure
devices, as applicable to the container, that are composed of suitable
350
materials to minimize exposure of the hazardous waste to the atmosphere
and to maintain the equipment integrity for as long as it is in service.
Factors to be considered in selecting the materials of construction and
designing the cover and closure devices must include the following: the
organic vapor permeability, the effects of contact with the hazardous
waste or its vapor managed in the container; the effects of outdoor
exposure of the closure device or cover material to wind, moisture, and
sunlight; and the operating practices for which the container is intended
to be used.
3)
Whenever a hazardous waste is in a container using Container Level 1
controls, the owner or operator shall install all covers and closure
devices for the container, as applicable to the container, and secure and
maintain each closure device in the closed position except as follows:
A)
Opening of a closure device or cover is allowed for the purpose
of adding hazardous waste or other material to the container as
follows:
i)
In the case when the container is filled to the intended
final level in one continuous operation, the owner or
operator shall promptly secure the closure devices in the
closed position and install the covers, as applicable to the
container, upon conclusion of the filling operation.
ii)
In the case when discrete quantities or batches of material
intermittently are added to the container over a period of
time, the owner or operator shall promptly secure the
closure devices in the closed position and install covers, as
applicable to the container, upon either the container
being filled to the intended final level; the completion of a
batch loading after which no additional material will be
added to the container within 15 minutes; the person
performing the loading operation leaving the immediate
vicinity of the container; or the shutdown of the process
generating the material being added to the container,
whichever condition occurs first.
B)
Opening of a closure device or cover is allowed for the purpose
of removing hazardous waste from the container as follows:
i)
For the purpose of meeting the requirements of this
Section, an empty container, as defined in 35 Ill. Adm.
Code 721.107(b), may be open to the atmosphere at any
351
time (i.e., covers and closure devices are not required to
be secured in the closed position on an empty container).
ii)
In the case when discrete quantities or batches of material
are removed from the container but the container does not
meet the conditions to be an empty container, as defined
in 35 Ill. Adm. Code 721.107(b), the owner or operator
shall promptly secure the closure devices in the closed
position and install covers, as applicable to the container,
upon the completion of a batch removal after which no
additional material will be removed from the container
within 15 minutes or the person performing the unloading
operation leaves the immediate vicinity of the container,
whichever condition occurs first.
C)
Opening of a closure device or cover is allowed when access
inside the container is needed to perform routine activities other
than transfer of hazardous waste. Examples of such activities
include those times when a worker needs to open a port to
measure the depth of or sample the material in the container, or
when a worker needs to open a manhole hatch to access
equipment inside the container. Following completion of the
activity, the owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as applicable
to the container.
D)
Opening of a spring-loaded, pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the container internal pressure in
accordance with the design specifications of the container. The
device must be designed to operate with no detectable organic
emissions when the device is secured in the closed position. The
settings at which the device opens must be established such that
the device remains in the closed position whenever the internal
pressure of the container is within the internal pressure operating
range determined by the owner or operator based on container
manufacturer recommendations, applicable regulations, fire
protection and prevention codes, standard engineering codes and
practices, or other requirements for the safe handling of
flammable, ignitable, explosive, reactive, or hazardous
materials. Examples of normal operating conditions that may
require these devices to open are during those times when the
internal pressure of the container exceeds the internal pressure
352
operating range for the container as a result of loading operations
or diurnal ambient temperature fluctuations.
E)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
4)
The owner or operator of containers using Container Level 1 controls
must inspect the containers and their covers and closure devices as
follows:
A)
In the case when a hazardous waste already is in the container at
the time the owner or operator first accepts possession of the
container at the facility and the container is not emptied (i.e.,
does not meet the conditions for an empty container as specified
in 35 Ill. Adm. Code 721.107(b)) within 24 hours after the
container is accepted at the facility (i.e., it does not meet the
conditions for an empty container as specified in 35 Ill. Adm.
Code 721.107(b)), the owner or operator shall visually inspect
the container and its cover and closure devices to check for
visible cracks, holes, gaps, or other open spaces into the interior
of the container when the cover and closure devices are secured
in the closed position. The container visual inspection must be
conducted on or before the date on which the container is accepted at
the facility (i.e., the date when the container becomes subject to the
Subpart CC container standards). For the purposes of this
requirement, the date of acceptance is the date of signature that the
facility owner or operator enters on Item 20 of the Uniform Hazardous
Waste Manifest incorporated by reference in 35 Ill. Adm. Code
722.Appendix A (USEPA Forms 8700-22 and 8700-22A), as required
under Section 725.171. If a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (c)(4)(C) of this Section.
B)
In the case when a container used for managing hazardous waste
remains at the facility for a period of one year or more, the
owner or operator shall visually inspect the container and its
cover and closure devices initially and thereafter, at least once
every 12 months, to check for visible cracks, holes, gaps, or
other open spaces into the interior of the container when the
cover and closure devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair the defect in
accordance with the requirements of subsection (c)(4)(C) of this
Section.
353
C)
When a defect is detected for the container, cover, or closure
devices, the owner or operator shall make first efforts at repair of
the defect no later than 24 hours after detection, and repair must
be completed as soon as possible but no later than five calendar
days after detection. If repair of a defect cannot be completed
within five calendar days, then the hazardous waste must be
removed from the container and the container must not be used to
manage hazardous waste until the defect is repaired.
5)
The owner or operator shall maintain at the facility a copy of the
procedure used to determine that containers with capacity of 0.46 m
3
(120 gal) or greater, which do not meet applicable USDOT regulations
as specified in subsection (f) of this Section, are not managing hazardous
waste in light material service.
d)
Container Level 2 standards.
1)
A container using Container Level 2 controls is one of the following:
A)
A container that meets the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous
materials for transportation as specified in subsection (f) of this
Section.
B)
A container that operates with no detectable organic emissions, as
defined in Section 725.981, and determined in accordance with
the procedure specified in subsection (g) of this Section.
C)
A container that has been demonstrated within the preceding 12
months to be vapor-tight by using 40 CFR 60, appendix A,
Method 27, incorporated by reference in 35 Ill. Adm. Code
720.111, in accordance with the procedure specified in subsection
(h) of this Section.
2)
Transfer of hazardous waste in or out of a container using Container
Level 2 controls must be conducted in such a manner as to minimize
exposure of the hazardous waste to the atmosphere, to the extent
practical, considering the physical properties of the hazardous waste and
good engineering and safety practices for handling flammable, ignitable,
explosive, reactive or other hazardous materials. Examples of container
loading procedures that the USEPA considers to meet the requirements
of this subsection (d)(2) include using any one of the following: a
submerged-fill pipe or other submerged-fill method to load liquids into
the container; a vapor-balancing system or a vapor-recovery system to
collect and control the vapors displaced from the container during filling
354
operations; or a fitted opening in the top of a container through which
the hazardous waste is filled and subsequently purging the transfer line
before removing it from the container opening.
3)
Whenever a hazardous waste is in a container using Container Level 2
controls, the owner or operator shall install all covers and closure
devices for the container, and secure and maintain each closure device in
the closed position except as follows:
A)
Opening of a closure device or cover is allowed for the purpose
of adding hazardous waste or other material to the container as
follows:
i)
In the case when the container is filled to the intended
final level in one continuous operation, the owner or
operator shall promptly secure the closure devices in the
closed position and install the covers, as applicable to the
container, upon conclusion of the filling operation.
ii)
In the case when discrete quantities or batches of material
intermittently are added to the container over a period of
time, the owner or operator shall promptly secure the
closure devices in the closed position and install covers, as
applicable to the container, upon either the container
being filled to the intended final level; the completion of a
batch loading after which no additional material will be
added to the container within 15 minutes; the person
performing the loading operation leaving the immediate
vicinity of the container; or the shutdown of the process
generating the material being added to the container,
whichever condition occurs first.
B)
Opening of a closure device or cover is allowed for the purpose
of removing hazardous waste from the container as follows:
i)
For the purpose of meeting the requirements of this
Section, an empty container as defined in 35 Ill. Adm.
Code 721.107(b) may be open to the atmosphere at any
time (i.e., covers and closure devices are not required to
be secured in the closed position on an empty container).
ii)
In the case when discrete quantities or batches of material
are removed from the container but the container does not
meet the conditions to be an empty container as defined in
35 Ill. Adm. Code 721.107(b), the owner or operator
355
shall promptly secure the closure devices in the closed
position and install covers, as applicable to the container,
upon the completion of a batch removal after which no
additional material will be removed from the container
within 15 minutes or the person performing the unloading
operation leaves the immediate vicinity of the container,
whichever condition occurs first.
C)
Opening of a closure device or cover is allowed when access
inside the container is needed to perform routine activities other
than transfer of hazardous waste. Examples of such activities
include those times when a worker needs to open a port to
measure the depth of or sample the material in the container, or
when a worker needs to open a manhole hatch to access
equipment inside the container. Following completion of the
activity, the owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as applicable
to the container.
D)
Opening of a spring-loaded, pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the internal pressure of the container
in accordance with the container design specifications. The
device must be designed to operate with no detectable organic
emission when the device is secured in the closed position. The
settings at which the device opens must be established such that
the device remains in the closed position whenever the internal
pressure of the container is within the internal pressure operating
range determined by the owner or operator based on container
manufacturer recommendations, applicable regulations, fire
protection and prevention codes, standard engineering codes and
practices, or other requirements for the safe handling of
flammable, ignitable, explosive, reactive, or hazardous
materials. Examples of normal operating conditions that may
require these devices to open are during those times when the
internal pressure of the container exceeds the internal pressure
operating range for the container as a result of loading operations
or diurnal ambient temperature fluctuations.
E)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
356
4)
The owner or operator of containers using Container Level 2 controls
shall inspect the containers and their covers and closure devices as
follows:
A)
In the case when a hazardous waste already is in the container at
the time the owner or operator first accepts possession of the
container at the facility and the container is not emptied (i.e.,
does not meet the conditions for an empty container as specified
in 35 Ill. Adm. Code 721.107(b)) within 24 hours after the
container is accepted at the facility (i.e., it does not meet the
conditions for an empty container as specified in 35 Ill. Adm.
Code 721.107(b)), the owner or operator shall visually inspect
the container and its cover and closure devices to check for
visible cracks, holes, gaps, or other open spaces into the interior
of the container when the cover and closure devices are secured
in the closed position. The container visual inspection must be
conducted on or before the date on which the container is accepted at
the facility (i.e., the date when the container becomes subject to the
Subpart CC container standards). For the purposes of this
requirement, the date of acceptance is the date of signature that the
facility owner or operator enters on Item 20 of the Uniform Hazardous
Waste Manifest incorporated by reference in 35 Ill. Adm. Code
722.Appendix A (USEPA Forms 8700-22 and 8700-22A), as required
under Section 725.171. If a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (d)(4)(C) of this Section.
B)
In the case when a container used for managing hazardous waste
remains at the facility for a period of one year or more, the
owner or operator shall visually inspect the container and its
cover and closure devices initially and thereafter, at least once
every 12 months, to check for visible cracks, holes, gaps, or
other open spaces into the interior of the container when the
cover and closure devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair the defect in
accordance with the requirements of subsection (d)(4)(C) of this
Section.
C)
When a defect is detected for the container, cover, or closure
devices, the owner or operator shall make first efforts at repair of
the defect no later than 24 hours after detection, and repair must
be completed as soon as possible but no later than five calendar
days after detection. If repair of a defect cannot be completed
within five calendar days, then the hazardous waste must be
removed from the container and the container must not be used to
manage hazardous waste until the defect is repaired.
357
e)
Container Level 3 standards.
1)
A container using Container Level 3 controls is one of the following:
A)
A container that is vented directly through a closed-vent system
to a control device in accordance with the requirements of
subsection (e)(2)(B) of this Section.
B)
A container that is vented inside an enclosure which is exhausted
through a closed-vent system to a control device in accordance
with the requirements of subsections (e)(2)(A) and (e)(2)(B) of
this Section.
2)
The owner or operator shall meet the following requirements, as
applicable to the type of air emission control equipment selected by the
owner or operator:
A)
The container enclosure must be designed and operated in
accordance with the criteria for a permanent total enclosure as
specified in “Procedure T--Criteria for and Verification of a
Permanent or Temporary Total Enclosure” under 40 CFR
52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of containers through
the enclosure by conveyor or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow
into the enclosure. The owner or operator shall perform the
verification procedure for the enclosure as specified in Section
5.0 to “Procedure T--Criteria for and Verification of a Permanent
or Temporary Total Enclosure” initially when the enclosure is
first installed and, thereafter, annually.
B)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 725.988.
3)
Safety devices, as defined in Section 725.981, may be installed and
operated as necessary on any container, enclosure, closed-vent system,
or control device used to comply with the requirements of subsection
(e)(1) of this Section.
4)
Owners and operators using Container Level 3 controls in accordance
with the provisions of this Subpart shall inspect and monitor the closed-
vent systems and control devices, as specified in Section 725.988.
358
5)
Owners and operators that use Container Level 3 controls in accordance
with the provisions of this Subpart shall prepare and maintain the records
specified in Section 725.990(d).
f)
For the purpose of compliance with subsection (c)(1)(A) or (d)(1)(A) of this
Section, containers must be used that meet the applicable U.S. Department of
Transportation (USDOT) regulations on packaging hazardous materials for
transportation as follows:
1)
The container meets the applicable requirements specified in 49 CFR
178, “Specifications for Packaging”, or 49 CFR 179, “Specifications for
Tank Cars”, both incorporated by reference in 35 Ill. Adm. Code
720.111.
2)
Hazardous waste is managed in the container in accordance with the
applicable requirements specified in 49 CFR 107, subpart B,
“Exemptions”; 49 CFR 172, “Hazardous Materials Table, Special
Provisions, Hazardous Materials Communications, Emergency Response
Information, and Training Requirements”; 49 CFR 173, “Shippers--
General Requirements for Shipments and Packages”; and 49 CFR 180,
“Continuing Qualification and Maintenance of Packagings”, each
incorporated by reference in 35 Ill. Adm. Code 720.111.
3)
For the purpose of complying with this Subpart, no exceptions to the 49
CFR 178 or 179 regulations are allowed, except as provided for in
subsection (f)(4) of this Section.
4)
For a lab pack that is managed in accordance with the requirements of
49 CFR 178 for the purpose of complying with this Subpart, an owner
or operator may comply with the exceptions for combination packagings
specified in 49 CFR 173.12(b), incorporated by reference in 35 Ill.
Adm. Code 720.111.
g)
The owner or operator shall use the procedure specified in Section 725.984(d)
for determining a container operates To determine compliance with the no
detectable organic emissions for the purpose of complying with requirements of
subsection (d)(1)(B) of this Section, the procedure specified in Section 725.984(d)
must be used.
1)
Each potential leak interface (i.e., a location where organic vapor
leakage could occur) on the container, its cover, and associated closure
devices, as applicable to the container, must be checked. Potential leak
interfaces that are associated with containers include, but are not limited
to: the interface of the cover rim and the container wall; the periphery
of any opening on the container or container cover and its associated
359
closure device; and the sealing seat interface on a spring-loaded
pressure-relief valve.
2)
The test must be performed when the container is filled with a material
having a volatile organic concentration representative of the range of
volatile organic concentrations for the hazardous wastes expected to be
managed in this type of container. During the test, the container cover
and closure devices must be secured in the closed position.
h)
Procedure for determining a container to be vapor-tight using Method 27 of 40
CFR 60, appendix A for the purpose of complying with subsection (d)(1)(C) of
this Section.
1)
The test must be performed in accordance with Method 27 of 40 CFR
60, appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111.
2)
A pressure measurement device must be used that has a precision of
±2.5 mm (0.10 inch) water and that is capable of measuring above the
pressure at which the container is to be tested for vapor tightness.
3)
If the test results determined by Method 27 indicate that the container
sustains a pressure change less than or equal to 750 Pascals (0.11 psig)
within five minutes after it is pressurized to a minimum of 4,500 Pascals
(0.65 psig), then the container is determined to be vapor-tight.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.988
Standards: Closed-Vent Systems and Control Devices
a)
This Section applies to each closed-vent system and control device installed and
operated by the owner or operator to control air emissions in accordance with
standards of this Subpart.
b)
The closed-vent system must meet the following requirements:
1)
The closed-vent system must route the gases, vapors, and fumes emitted
from the hazardous waste in the waste management unit to a control
device that meets the requirements specified in subsection (c) of this
Section.
2)
The closed-vent system must be designed and operated in accordance
with the requirements specified in Section 725.933(j).
360
3)
When the closed-vent system includes bypass devices that could be used
to divert the gas or vapor stream to the atmosphere before entering the
control device, each bypass device must be equipped with either a flow
indicator as specified in subsection (b)(3)(A) of this Section or a seal or
locking device as specified in subsection (b)(3)(B) of this Section. For
the purpose of complying with this subsection, low leg drains, high point
bleeds, analyzer vents, open-ended valves or lines, spring-loaded
pressure relief valves, and other fittings used for safety purposes are not
considered to be bypass devices.
A)
If a flow indicator is used to comply with this subsection (b)(3),
the indicator must be installed at the inlet to the bypass line used
to divert gases and vapors from the closed-vent system to the
atmosphere at a point upstream of the control device inlet. For
the purposes of this subsection, a flow indicator means a device
which indicates the presence of either gas or vapor flow in the
bypass line.
B)
If a seal or locking device is used to comply with this subsection
(b)(3), the device must be placed on the mechanism by which the
bypass device position is controlled (e.g., valve handle or damper
lever) when the bypass device is in the closed position such that
the bypass device cannot be opened without breaking the seal or
removing the lock. Examples of such devices include, but are
not limited to, a car-seal or a lock-and-key configuration valve.
The owner or operator shall visually inspect the seal or closure
mechanism at least once every month to verify that the bypass
mechanism is maintained in the closed position.
4)
The closed-vent system must be inspected and monitored by the owner
or operator in accordance with the procedure specified in Section
725.933(k).
c)
The control device must meet the following requirements:
1)
The control device must be one of the following devices:
A)
A control device designed and operated to reduce the total
organic content of the inlet vapor stream vented to the control
device by at least 95 percent by weight;
B)
An enclosed combustion device designed and operated in
accordance with the requirements of Section 725.933(c); or
361
C)
A flare designed and operated in accordance with the
requirements of Section 725.933(d).
2)
The owner or operator that elects to use a closed-vent system and control
device to comply with the requirements of this Section shall comply with
the requirements specified in subsections (c)(2)(A) through (c)(2)(G) of
this Section.
A)
Periods of planned routine maintenance of the control device,
during which the control device does not meet the specifications
of subsections subsection (c)(1)(A), (c)(1)(B), or (c)(1)(C) of this
Section, as applicable, must not exceed 240 hours per year.
B)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during periods of planned routine maintenance.
C)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during a control device system malfunction.
D)
The owner or operator shall demonstrate compliance with the
requirements of subsection (c)(2)(A) of this Section (i.e., planned
routine maintenance of a control device, during which the control
device does not meet the specifications of subsections subsection
(c)(1)(A), (c)(1)(B), or (c)(1)(C) of this Section, as applicable,
must not exceed 240 hours per year) by recording the information
specified in Section 725.990(e)(1)(E).
E)
The owner or operator shall correct control device system
malfunctions as soon as practicable after their occurrence in order
to minimize excess emissions of air pollutants.
F)
The owner or operator shall operate the closed-vent system so
that gases, vapors, or fumes are not actively vented to the control
device during periods of planned maintenance or control device
system malfunction (i.e., periods when the control device is not
operating or not operating normally), except in cases when it is
necessary to vent the gases, vapors, or fumes to avoid an unsafe
condition or to implement malfunction corrective actions or
planned maintenance actions.
3)
The owner or operator using a carbon adsorption system to comply with
subsection (c)(1) of this Section shall operate and maintain the control
device in accordance with the following requirements:
362
A)
Following the initial startup of the control device, all activated
carbon in the control device must be replaced with fresh carbon
on a regular basis in accordance with the requirements of Section
725.933(g) or 725.933(h).
B)
All carbon that is a hazardous waste and that is removed from the
control device must be managed in accordance with the
requirements of Section 725.933(m), regardless of the average
volatile organic concentration of the carbon.
4)
An owner or operator using a control device other than a thermal vapor
incinerator, flare, boiler, process heater, condenser, or carbon
adsorption system to comply with subsection (c)(1) of this Section shall
operate and maintain the control device in accordance with the
requirements of Section 725.933(i).
5)
The owner or operator shall demonstrate that a control device achieves
the performance requirements of subsection (c)(1) of this Section as
follows:
A)
An owner or operator shall demonstrate using either a
performance test, as specified in subsection (c)(5)(C) of this
Section, or a design analysis, as specified in subsection (c)(5)(D)
of this Section, the performance of each control device except for
the following:
i)
A flare;
ii)
A boiler or process heater with a design heat input
capacity of 44 megawatts or greater;
iii)
A boiler or process heater into which the vent stream is
introduced with the primary fuel;
iv)
A boiler or industrial furnace burning hazardous waste for
which the owner or operator has been issued a final
permit under 35 Ill. Adm. Code 702, 703, and 705 and
has designed and operates in accordance with the
requirements of 35 Ill. Adm. Code 726.Subpart H; or
v)
A boiler or industrial furnace burning hazardous waste for
which the owner or operator has designed and operates in
accordance with the interim status requirements of 35 Ill.
Adm. Code 726.Subpart H.
363
B)
An owner or operator shall demonstrate the performance of each
flare in accordance with the requirements specified in Section
725.933(e).
C)
For a performance test conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the owner or operator shall
use the test methods and procedures specified in Section
725.934(c)(1) through (c)(4).
D)
For a design analysis conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the design analysis must
meet the requirements specified in Section 725.935(b)(4)(C).
E)
The owner or operator shall demonstrate that a carbon adsorption
system achieves the performance requirements of subsection
(c)(1) of this Section based on the total quantity of organics
vented to the atmosphere from all carbon adsorption system
equipment that is used for organic adsorption, organic desorption
or carbon regeneration, organic recovery, and carbon disposal.
6)
If the owner or operator and the Agency do not agree on a demonstration
of control device performance using a design analysis, then the
disagreement must be resolved using the results of a performance test
performed by the owner or operator in accordance with the requirements
of subsection (c)(5)(C) of this Section. The Agency may choose to have
an authorized representative observe the performance test.
7)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the procedures
specified in Section 725.933(f)(2) and (k). The readings from each
monitoring device required by Section 725.933(f)(2) must be inspected
at least once each operating day to check control device operation. Any
necessary corrective measures must be immediately implemented to
ensure the control device is operated in compliance with the
requirements of this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.989
Inspection and Monitoring Requirements
a)
The owner or operator shall inspect and monitor air emission control equipment
used to comply with this Subpart in accordance with the requirements specified
in Sections 725.985 through 725.988.
364
b)
The owner or operator shall develop and implement a written plan and schedule
to perform the inspections and monitoring required by subsection (a) of this
Section. The owner or operator shall incorporate this plan and schedule into the
facility inspection plan required under Section 725.115.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.990
Recordkeeping Requirements
a)
Each owner or operator of a facility subject to the requirements in this Subpart
shall record and maintain the information specified in subsections (b) through
(ij) of this Section, as applicable to the facility. Except for air emission control
equipment design documentation and information required by subsection (ij) of
this Section, records required by this Section must be maintained in the
operating record for a minimum of three years. Air emission control equipment
design documentation must be maintained in the operating record until the air
emission control equipment is replaced or is otherwise no longer in service.
Information required by subsection subsections (i) and (j) of this Section must
be maintained in the operating record for as long as the tank or container waste
management unit is not using air emission controls specified in Sections 724.984
through 724.987 725.985 through 725.988, in accordance with the conditions
specified in Section 724.984(d) 725.980(d) or (b)(7), respectively.
b)
The owner or operator of a tank using air emission controls in accordance with
the requirements of Section 725.985 shall prepare and maintain records for the
tank that include the following information:
1)
For each tank using air emission controls in accordance with the
requirements of Section 725.985 of this Subpart, the owner or operator
shall record:
A)
A tank identification number (or other unique identification
description as selected by the owner or operator).
B)
A record for each inspection required by Section 725.985 that
includes the following information:
i)
Date inspection was conducted.
ii)
For each defect detected during the inspection, the
following information: the location of the defect, a
description of the defect, the date of detection, and
corrective action taken to repair the defect. In the event
that repair of the defect is delayed in accordance with the
provisions of Section 725.985, the owner or operator shall
365
also record the reason for the delay and the date that
completion of repair of the defect is expected.
2)
In addition to the information required by subsection (b)(1) of this
Section, the owner or operator shall record the following information, as
applicable to the tank:
A)
The owner or operator using a fixed roof to comply with the
Tank Level 1 control requirements specified in Section
725.985(c) shall prepare and maintain records for each
determination for the maximum organic vapor pressure of the
hazardous waste in the tank performed in accordance with the
requirements of Section 725.985(c). The records must include
the date and time the samples were collected, the analysis method
used, and the analysis results.
B)
The owner or operator using an internal floating roof to comply
with the Tank Level 2 control requirements specified in Section
725.985(e) shall prepare and maintain documentation describing
the floating roof design.
C)
Owners and operators using an external floating roof to comply
with the Tank Level 2 control requirements specified in Section
725.985(f) shall prepare and maintain the following records:
i)
Documentation describing the floating roof design and the
dimensions of the tank.
ii)
Records for each seal gap inspection required by Section
725.985(f)(3) describing the results of the seal gap
measurements. The records must include the date that the
measurements were performed, the raw data obtained for
the measurements, and the calculations of the total gap
surface area. In the event that the seal gap measurements
do not conform to the specifications in Section
725.985(f)(1), the records must include a description of
the repairs that were made, the date the repairs were
made, and the date the tank was emptied, if necessary.
D)
Each owner or operator using an enclosure to comply with the
Tank Level 2 control requirements specified in Section
725.985(i) shall prepare and maintain the following records:
i)
Records for the most recent set of calculations and
measurements performed by the owner or operator to
366
verify that the enclosure meets the criteria of a permanent
total enclosure as specified in “Procedure T--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure” under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code 720.111.
ii)
Records required for the closed-vent system and control
device in accordance with the requirements of subsection
(e) of this Section.
c)
The owner or operator of a surface impoundment using air emission controls in
accordance with the requirements of Section 725.986 shall prepare and maintain
records for the surface impoundment that include the following information:
1)
A surface impoundment identification number (or other unique
identification description as selected by the owner or operator).
2)
Documentation describing the floating membrane cover or cover design,
as applicable to the surface impoundment, that includes information
prepared by the owner or operator or provided by the cover
manufacturer or vendor describing the cover design, and certification by
the owner or operator that the cover meets the specifications listed in
Section 725.986(c).
3)
A record for each inspection required by Section 725.986 that includes
the following information:
A)
Date inspection was conducted.
B)
For each defect detected during the inspection the following
information: the location of the defect, a description of the
defect, the date of detection, and corrective action taken to repair
the defect. In the event that repair of the defect is delayed in
accordance with the provisions of Section 725.986(f), the owner
or operator shall also record the reason for the delay and the date
that completion of repair of the defect is expected.
4)
For a surface impoundment equipped with a cover and vented through a
closed-vent system to a control device, the owner or operator shall
prepare and maintain the records specified in subsection (e) of this
Section.
d)
The owner or operator of containers using Container Level 3 air emission
controls in accordance with the requirements of Section 725.987 shall prepare
and maintain records that include the following information:
367
1)
Records for the most recent set of calculations and measurements
performed by the owner or operator to verify that the enclosure meets
the criteria of a permanent total enclosure as specified in “Procedure T--
Criteria for and Verification of a Permanent or Temporary Total
Enclosure” under 40 CFR 52.741, appendix B, incorporated by
reference in 35 Ill. Adm. Code 720.111.
2)
Records required for the closed-vent system and control device in
accordance with the requirements of subsection (e) of this Section.
e)
The owner or operator using a closed-vent system and control device in
accordance with the requirements of Section 725.988 shall prepare and maintain
records that include the following information:
1)
Documentation for the closed-vent system and control device that
includes:
A)
Certification that is signed and dated by the owner or operator
stating that the control device is designed to operate at the
performance level documented by a design analysis as specified
in subsection (e)(1)(B) of this Section or by performance tests as
specified in subsection (e)(1)(C) of this Section when the tank,
surface impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to occur.
B)
If a design analysis is used, then design documentation, as
specified in Section 725.935(b)(4). The documentation must
include information prepared by the owner or operator or
provided by the control device manufacturer or vendor that
describes the control device design in accordance with Section
725.935(b)(4)(C) and certification by the owner or operator that
the control equipment meets the applicable specifications.
C)
If performance tests are used, then a performance test plan as
specified in Section 725.935(b)(3) and all test results.
D)
Information as required by Section 725.935(c)(1) and (c)(2), as
applicable.
E)
An owner or operator shall record, on a semiannual basis, the
information specified in subsections (e)(1)(E)(i) and (e)(1)(E)(ii)
of this Section for those planned routine maintenance operations
that would require the control device not to meet the
368
requirements of Section 725.988(c)(1)(A), (c)(1)(B), or
(c)(1)(C), as applicable.
i)
A description of the planned routine maintenance that is
anticipated to be performed for the control device during
the next six-month period. This description must include
the type of maintenance necessary, planned frequency of
maintenance, and lengths of maintenance periods.
ii)
A description of the planned routine maintenance that was
performed for the control device during the previous six-
month period. This description must include the type of
maintenance performed and the total number of hours
during those six months that the control device did not
meet the requirements of Section 725.988(c)(1)(A),
(c)(1)(B), or (c)(1)(C), as applicable, due to planned
routine maintenance.
F)
An owner or operator shall record the information specified in
subsections (e)(1)(F)(i) through (e)(1)(F)(iii) of this Section for
those unexpected control device system malfunctions that would
require the control device not to meet the requirements of Section
725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as applicable.
i)
The occurrence and duration of each malfunction of the
control device system.
ii)
The duration of each period during a malfunction when
gases, vapors, or fumes are vented from the waste
management unit through the closed-vent system to the
control device while the control device is not properly
functioning.
iii)
Actions taken during periods of malfunction to restore a
malfunctioning control device to its normal or usual
manner of operation.
G)
Records of the management of carbon removed from a carbon
adsorption system conducted in accordance with Section
725.988(c)(3)(B).
f)
The owner or operator of a tank, surface impoundment, or container exempted
from standards in accordance with the provisions of Section 725.983(c) of this
Subpart shall prepare and maintain the following records, as applicable:
369
1)
For tanks, surface impoundments, or containers exempted under the
hazardous waste organic concentration conditions specified in Section
725.983 (c)(1) or (c)(2) of this Subpart 725.984(c)(2)(A) through (c)(2)(F),
the owner or operator shall record the information used for each waste
determination (e.g., test results, measurements, calculations, and other
documentation) in the facility operating log. If analysis results for waste
samples are used for the waste determination, then the owner or operator
shall record the date, time, and location that each waste sample is
collected in accordance with the applicable requirements of Section
725.984 of this Subpart.
2)
For tanks, surface impoundments, or containers exempted under the
provisions of Section 725.983(c)(2)(G) or (c)(2)(H) of this Subpart, the
owner or operator shall record the identification number for the
incinerator, boiler, or industrial furnace in which the hazardous waste is
treated.
g)
An owner or operator designating a cover as “unsafe to inspect and monitor”
pursuant to Section 725.985(l) shall record in a log that is kept in the facility
operating record the following information: the identification numbers for
waste management units with covers that are designated as “unsafe to inspect
and monitor”, the explanation for each cover stating why the cover is unsafe to
inspect and monitor, and the plan and schedule for inspecting and monitoring
each cover.
h)
The owner or operator of a facility that is subject to this Subpart and to the
control device standards in 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart V,
incorporated by reference in 35 Ill. Adm. Code 270.111, may elect to
demonstrate compliance with the applicable Sections of this Subpart by
documentation either pursuant to this Subpart, or pursuant to the provisions of
40 CFR 60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
documentation required by 40 CFR 60 or 61 duplicates the documentation
required by this Section.
i)
For each tank or container not using air emission controls specified in Sections
725.985 through 725.988 in accordance with the conditions specified in Section
725.980(d), the owner or operator shall record and maintain the following
information:
1)
A list of the individual organic peroxide compounds manufactured at the
facility that meet the conditions specified in Section 725.980(d)(1).
2)
A description of how the hazardous waste containing the organic
peroxide compounds identified pursuant to subsection (i)(1) are managed
370
at the facility in tanks and containers. This description must include the
following information:
A)
For the tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to describe each tank: a
facility identification number for the tank, the purpose and
placement of this tank in the management train of this hazardous
waste, and the procedures used to ultimately dispose of the
hazardous waste managed in the tanks.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to describe the
following for each container: a facility identification number for
the container or group of containers; the purpose and placement
of this container or group of containers in the management train
of this hazardous waste; and the procedures used to ultimately
dispose of the hazardous waste handled in the containers.
3)
An explanation of why managing the hazardous waste containing the
organic peroxide compounds identified pursuant to subsection (i)(1) of
this Section in the tanks or containers identified pursuant to subsection
(i)(2) of this Section would create an undue safety hazard if the air
emission controls specified in Sections 725.985 through 725.988 were
installed and operated on these waste management units. This
explanation must include the following information:
A)
For tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to explain: how use of
the required air emission controls on the tanks would affect the
tank design features and facility operating procedures currently
used to prevent an undue safety hazard during the management of
this hazardous waste in the tanks; and why installation of safety
devices on the required air emission controls, as allowed under
this Subpart, would not address those situations in which
evacuation of tanks equipped with these air emission controls is
necessary and consistent with good engineering and safety
practices for handling organic peroxides.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to explain: how
use of the required air emission controls on the containers would
affect the container design features and handling procedures
currently used to prevent an undue safety hazard during
management of this hazardous waste in the containers; and why
installation of safety devices on the required air emission
371
controls, as allowed under this Subpart, would not address those
situations in which evacuation of containers equipped with these
air emission controls is necessary and consistent with good
engineering and safety practices for handling organic peroxides.
j)
For each hazardous waste management unit not using air emission controls
specified in Sections 725.985 through 725.988 in accordance with the provisions of
Section 725.980(b)(7), the owner and operator shall record and maintain the
following information:
1)
The certification that the waste management unit is equipped with and
operating air emission controls in accordance with the requirements of an
applicable federal Clean Air Act regulation codified under 40 CFR 60, 61, or
63.
2)
An identification of the specific federal requirements codified under 40 CFR
60, 61, or 63 with which the waste management unit is in compliance.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.Appendix F
Compounds With Henry’s Law Constant Less Than 0.1 Y/X (at
25° C)
Compound name
CAS No.
Acetaldol
107-89-1
Acetamide
60-35-5
2-Acetylaminofluorene
53-96-3
3-Acetyl-5-hydroxypiperidine
3-Acetylpiperidine
618-42-8
1-Acetyl-2-thiourea
591-08-2
Acrylamide
79-06-1
Acrylic acid
79-10-7
Adenine
73-24-5
Adipic acid
124-04-9
Adiponitrile
111-69-3
Alachlor
15972-60-8
Aldicarb
116-06-3
Ametryn
834-12-8
4-Aminobiphenyl
92-67-1
4-Aminopyridine
504-24-5
Aniline
62-53-3
o-Anisidine
90-04-0
Anthraquinone
84-65-1
Atrazine
1912-24-9
Benzenearsonic acid
98-05-5
372
Benzenesulfonic acid
98-11-3
Benzidine
92-87-5
Benzo(a)anthracene
56-55-3
Benzo(k)fluoranthene
207-08-9
Benzoic acid
65-85-0
Benzo(g,h,i)perylene
191-24-2
Benzo(a)pyrene
50-32-8
Benzyl alcohol
100-51-6
γ-BHC
58-89-9
Bis(2-ethylhexyl)phthalate
117-81-7
Bromochloromethyl acetate
Bromoxynil (3,5-Dibromo-4-hydroxybenzonitrile)
1689-84-5
Butyric acid
107-92-6
Caprolactam (hexahydro-2H-azepin-2-one)
105-60-2
Catechol (o-dihydroxybenzene)
120-80-9
Cellulose
9004-34-6
Cell wall
Chlorhydrin (3-Chloro-1,2-propanediol)
96-24-2
Chloroacetic acid
79-11-8
2-Chloroacetophenone
93-76-5
p-Chloroaniline
106-47-8
p-Chlorobenzophenone
134-85-0
ChlorobenzylateChlorobenzilate
510-15-6
p-Chloro-m-cresol (6-chloro-m-cresol)
59-50-7
3-Chloro-2,5-diketopyrrolidine
Chloro-1,2-ethane diol
4-Chlorophenol
106-48-9
Chlorophenol polymers (2-chlorophenol & 4-chlorophenol)
95-57-8 &
106-48-9
1-(o-Chlorophenyl)thiourea
5344-82-1
Chrysene
218-01-9
Citric acid
77-92-9
Creosote
8001-58-9
m-Cresol
108-39-4
o-Cresol
95-48-7
p-Cresol
106-44-5
Cresol (mixed isomers)
1319-77-3
4-Cumylphenol
27576-86
Cyanide
57-12-5
4-Cyanomethyl benzoate
Diazinon
333-41-5
Dibenzo(a,h)anthracene
53-70-3
3,5-Dibromo-4-hydroxybenzonitrile
1689-84-5
Dibutylphthalate
84-74-2
2,5-Dichloroaniline (N,N’-dichloroaniline)
95-82-9
373
2,6-Dichlorobenzonitrile
1194-65-6
2,6-Dichloro-4-nitroaniline
99-30-9
2,5-Dichlorophenol
333-41-5
3,4-Dichlorotetrahydrofuran
3511-19
Dichlorvos (DDVP)
106-47-8
62-73-7
Diethanolamine
111-42-2
N,N-Diethylaniline
91-66-7
Diethylene glycol
111-46-6
Diethylene glycol dimethyl ether (dimethyl Carbitol)
111-96-6
Diethylene glycol monobutyl ether (butyl Carbitol)
112-34-5
Diethylene glycol monoethyl ether acetate (Carbitol acetate)
112-15-2
Diethylene glycol monoethyl ether (Carbitol Cellosolve)
111-90-0
Diethylene glycol monomethyl ether (methyl Carbitol)
111-77-3
N,N’-Diethylhydrazine
1615-80-1
Diethyl(4-methylumbelliferyl)thionophosphate
299-45-6
Diethylphosphorothioate
126-75-0
N,N’-Diethylpropionamide
15299-99-7
Dimethoate
60-51-5
2,3-Dimethoxystrychnidin-10-one
357-57-3
4-Dimethylaminoazobenzene
60-11-7
7,12-Dimethylbenz(a)anthracene
57-97-6
3,3-Dimethylbenzidine
119-93-7
Dimethylcarbamoyl chloride
79-44-7
Dimethyldisulfide
624-92-0
Dimethylformamide
68-12-2
1,1-Dimethylhydrazine
57-14-7
Dimethylphthalate
131-11-3
Dimethylsulfone
67-71-0
Dimethylsulfoxide
67-68-5
2,3-Dimethoxystrychnidin-10-one
357-57-3
4,6-Dinitro-o-cresol
534-52-1
1,2-Diphenylhydrazine
122-66-7
Dipropylene glycol (1,1'-oxydi-2-propanol)
110-98-5
Endrin
72-20-8
Epinephrine
51-43-4
mono-Ethanolamine
141-43-5
Ethyl carbamate (urethane)
51-79-6
Ethylene glycol
107-21-1
Ethylene glycol monobutyl ether (butyl Cellosolve)
111-76-2
Ethylene glycol monoethyl ether (Cellosolve)
110-80-5
Ethylene glycol monoethyl ether acetate (Cellosolve acetate)
111-15-9
Ethylene glycol monomethyl ether (methyl Cellosolve)
109-86-4
Ethylene glycol monophenyl ether (phenyl Cellosolve)
122-99-6
Ethylene glycol monopropyl ether (propyl Cellosolve)
2807-30-9
374
Ethylene thiourea (2-imidazolidinethione)
9-64-57
4-Ethylmorpholine
100-74-3
3-Ethylphenol
620-17-7
Fluoroacetic acid, sodium salt
62-74-8
Formaldehyde
50-00-0
Formamide
75-12-7
Formic acid
64-18-6
Fumaric acid
110-17-8
Glutaric acid
110-94-1
Glycerin (Glycerol)
56-81-5
Glycidol
556-52-5
Glycinamide
598-41-4
Glyphosate
1071-83-6
Guthion
86-50-0
Hexamethylene-1,6-diisocyanate (1,6-diisocyanatohexane)
822-06-0
Hexamethyl phosphoramide
680-31-9
Hexanoic acid
142-62-1
Hydrazine
302-01-2
Hydrocyanic acid
74-90-8
Hydroquinone
123-31-9
Hydroxy-2-propionitrile (hydracrylonitrile)
109-78-4
Indeno(1,2,3-cd)pyrene
193-39-5
Lead acetate
301-04-2
Lead subacetate (lead acetate, monobasic)
1335-32-6
Leucine
61-90-5
Malathion
121-75-5
Maleic acid
110-16-7
Maleic anhydride
108-31-6
Mesityl oxide
141-79-7
Methane sulfonic acid
75-75-2
Methomyl
16752-77-5
p-Methoxyphenol
150-76-5
Methylacrylate
96-33-3
4,4'-Methylene-bis-(2-chloroaniline)
101-14-4
4,4'-Methylenediphenyl diisocyanate (diphenyl methane diisocyanate) 101-68-8
4,4'-Methylenedianiline
101-77-9
Methylene diphenylamine (MDA)
5-Methylfurfural
620-02-0
Methylhydrazine
60-34-4
Methyliminoacetic acid
Methyl methane sulfonate
66-27-3
1-Methyl-2-methoxyaziridine
Methylparathion
298-00-0
Methyl sulfuric acid (sulfuric acid, dimethyl ester)
77-78-1
4-Methylthiophenol
106-45-6
375
Monoethanolamine
141-43-5
Monomethylformamide (N-methylformamide)
123-39-7
Nabam
142-59-6
α-Naphthol
90-15-3
β-Naphthol
135-19-3
α-Naphthylamine
134-32-7
β-Naphthylamine
91-59-8
Neopentyl glycol
126-30-7
Niacinamide
98-92-0
o-Nitroaniline
88-74-4
Nitroglycerin
55-63-0
2-Nitrophenol
88-75-5
4-Nitrophenol
100-02-7
N-Nitrosodimethylamine
62-75-9
Nitrosoguanidine
674-81-7
N-Nitroso-n-methylurea
684-93-5
N-Nitrosomorpholine (4-nitrosomorpholine)
59-89-2
Oxalic acid
144-62-7
Parathion
56-38-2
Pentaerythritol
115-77-5
Phenacetin
62-44-2
Phenol
108-95-2
Phenylacetic acid
103-82-2
m-Phenylene diamine
108-45-2
o-Phenylene diamine
95-54-5
p-Phenylene diamine
106-50-3
Phenyl mercuric acetate
62-38-4
Phorate
298-02-2
Phthalic anhydride
85-44-9
α-Picoline
(2-methyl pyridine)
109-06-8
1,3-Propane sulfone
1120-71-4
β-Propiolactone
57-57-8
Proporur (Baygon)
Propylene glycol
57-55-6
Pyrene
129-00-0
Pyridinium bromide
39416-48-3
Quinoline
91-22-5
Quinone (p-benzoquinone)
106-51-4
Resorcinol
108-46-3
Simazine
122-34-9
Sodium acetate
127-09-3
Sodium formate
141-53-7
Strychnine
57-24-9
Succinic acid
110-15-6
Succinimide
123-56-8
376
Sulfanilic acid
121-47-1
Terephthalic acid
100-21-0
Tetraethyldithiopyrophosphate
3689-24-5
Tetraethylenepentamine
112-57-2
Thiofanox
39196-18-4
Thiosemicarbazide
79-19-6
2,4-Toluenediamine
95-80-7
2,6-Toluenediamine
823-40-5
3,4-Toluenediamine
496-72-0
2,4-Toluene diisocyanate
584-84-9
p-Toluic acid
99-94-5
m-Toluidine
108-44-1
1,1,2-Trichloro-1,2,2-trifluoroethane
76-13-1
Triethanolamine
102-71-6
Triethylene glycol dimethyl ether
Tripropylene glycol
24800-44-0
Warfarin
81-81-2
3,4-Xylenol (3,4-dimethylphenol)
95-65-8
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 728
LAND DISPOSAL RESTRICTIONS
SUBPART A: GENERAL
Section
728.101
Purpose, Scope and Applicability
728.102
Definitions
728.103
Dilution Prohibited as a Substitute for Treatment
728.104
Treatment Surface Impoundment Exemption
728.105
Procedures for case-by-case Extensions to an Effective Date
728.106
Petitions to Allow Land Disposal of a Waste Prohibited under Subpart C
728.107
Testing, Tracking, and Recordkeeping Requirements for Generators, Treaters,
and Disposal Facilities
728.108
Landfill and Surface Impoundment Disposal Restrictions (Repealed)
728.109
Special Rules for Characteristic Wastes
377
SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION AND
ESTABLISHMENT OF TREATMENT STANDARDS
Section
728.110
First Third (Repealed)
728.111
Second Third (Repealed)
728.112
Third Third (Repealed)
728.113
Newly Listed Wastes
728.114
Surface Impoundment exemptions
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section
728.130
Waste Specific Prohibitions -- Wood Preserving Wastes
728.131
Waste Specific Prohibitions -- Dioxin-Containing Wastes
728.132
Waste Specific Prohibitions -- California List Wastes (Repealed)
728.133
Waste Specific Prohibitions -- First Third Wastes (Repealed)
728.133
Waste-Specific Prohibitions -- Organobromine Wastes
728.134
Waste Specific Prohibitions -- Second Third Wastes (Repealed)
728.134
Waste-Specific Prohibitions -- Toxicity Characteristic Metal Wastes
728.135
Waste Specific Prohibitions -- Third Third Wastes (Repealed)
728.135
Waste Specific Prohibitions -- Petroleum Refining Wastes
728.136
Waste Specific Prohibitions -- Newly Listed Wastes (Repealed)
728.137
Waste Specific Prohibitions -- Ignitable and Corrosive Characteristic Wastes
Whose Treatment Standards Were Vacated
728.138
Waste-Specific Prohibitions: Newly-Identified Organic Toxicity Characteristic
Wastes and Newly-Listed Coke By-Product and Chlorotoluene Production
Wastes
728.139
Waste-Specific Prohibitions: End-of-pipe CWA, CWA-Equivalent, and Class I
Nonhazardous Waste Injection Well Treatment Standards; Spent Aluminum
Potliners; and Carbamate Wastes
SUBPART D: TREATMENT STANDARDS
Section
728.140
Applicability of Treatment Standards
728.141
Treatment Standards Expressed as Concentrations in Waste Extract
728.142
Treatment Standards Expressed as Specified Technologies
728.143
Treatment Standards Expressed as Waste Concentrations
728.144
Adjustment of Treatment Standard
728.145
Treatment Standards for Hazardous Debris
728.146
Alternative Treatment Standards Based on HTMR
728.148
Universal Treatment Standards
728.149
Alternative LDR Treatment Standards for Contaminated Soil
SUBPART E: PROHIBITIONS ON STORAGE
Section
728.150
Prohibitions on Storage of Restricted Wastes
378
728.Appendix A
Toxicity Characteristic Leaching Procedure (TCLP) (Repealed)
728.Appendix B
Treatment Standards (As concentrations in the Treatment Residual
Extract) (Repealed)
728.Appendix C
List of Halogenated Organic Compounds (Repealed)
728.Appendix D
Wastes Excluded from Lab Packs
728.Appendix E
Organic Lab Packs (Repealed)
728.Appendix F
Technologies to Achieve Deactivation of Characteristics
728.Appendix G
Federal Effective Dates
728.Appendix H
National Capacity LDR Variances for UIC Wastes
728.Appendix I
EP Toxicity Test Method and Structural Integrity Test
728.Appendix J
Recordkeeping, Notification, and Certification Requirements (Repealed)
728.Appendix K
Metal Bearing Wastes Prohibited From Dilution in a Combustion Unit
According to Section 728.103(c)
728.Table A
Constituent Concentrations in Waste Extract (CCWE)
728.Table B
Constituent Concentrations in Wastes (CCW)
728.Table C
Technology Codes and Description of Technology-Based Standards
728.Table D
Technology-Based Standards by RCRA Waste Code
728.Table E
Standards for Radioactive Mixed Waste
728.Table F
Alternative Treatment Standards for Hazardous Debris
728.Table G
Alternative Treatment Standards Based on HMTR
728.Table H
Wastes Excluded from CCW Treatment Standards
728.Table I
Generator Paperwork Requirements
728.Table T
Treatment Standards for Hazardous Wastes
728.Table U
Universal Treatment Standards (UTS)
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R87-5 at 11 Ill. Reg. 19354, effective November 12, 1987; amended
in R87-39 at 12 Ill. Reg. 13046, effective July 29, 1988; amended in R89-1 at 13 Ill. Reg.
18403, effective November 13, 1989; amended in R89-9 at 14 Ill. Reg. 6232, effective April
16, 1990; amended in R90-2 at 14 Ill. Reg. 14470, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16508, effective September 25, 1990; amended in R90-11 at 15 Ill.
Reg. 9462, effective June 17, 1991; amendment withdrawn at 15 Ill. Reg. 14716, October 11,
1991; amended in R91-13 at 16 Ill. Reg. 9619, effective June 9, 1992; amended in R92-10 at
17 Ill. Reg. 5727, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20692,
effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6799, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12203, effective July 29, 1994; amended in R94-17 at
18 Ill. Reg. 17563, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9660,
effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11100, August 1, 1996; amended
in R96-10/R97-3/R97-5 at 22 Ill. Reg. 783, effective December 16, 1997; amended in R98-12
at 22 Ill. Reg. 7685, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill.
379
Reg. 17706, effective September 28, 1998; amended in R98-21/R99-2/R99-7 at 22 Ill. Reg.
________, effective ______________________.
SUBPART A: GENERAL
Section 728.102
Definitions
When used in this Part, the following terms have the meanings given below. All other terms
have the meanings given under 35 Ill. Adm. Code 702.110, 720.110, or 721.102 through
721.104.
“Agency” means the Illinois Environmental Protection Agency.
“Board” means the Illinois Pollution Control Board.
“CERCLA” means the Comprehensive Environmental Response,
Compensation, and Liability Act of 1980 (42 U.S.C. USC 9601 et seq.)
“Debris” means solid material exceeding a 60 mm particle size that is intended
for disposal and that is: a manufactured object; plant or animal matter; or
natural geologic material. However, the following materials are not debris:
any material for which a specific treatment standard is provided in Subpart D of
this Part, namely lead acid batteries, cadmium batteries, and radioactive lead
solids; process residuals, such as smelter slag and residues from the treatment of
waste, wastewater, sludges, or air emission residues; and intact containers of
hazardous waste that are not ruptured and that retain at least 75% percent of
their original volume. A mixture of debris that has not been treated to the
standards provided by Section 728.145 of this Part and other material is subject
to regulation as debris if the mixture is comprised primarily of debris, by
volume, based on visual inspection.
“End-of-pipe” refers to the point where effluent is discharged to the
environment.
“Halogenated organic compounds” or “HOCs” means those compounds having
a carbon-halogen bond that are listed under Section 728.Appendix C.
“Hazardous constituent or constituents” means those constituents listed in 35 Ill.
Adm. Code 721.Appendix H.
“Hazardous debris” means debris that contains a hazardous waste listed in 35
Ill. Adm. Code 721.Subpart D or that exhibits a characteristic of hazardous
waste identified in 35 Ill. Adm. Code 721.Subpart C.
380
“Inorganic metal-bearing waste” is one for which USEPA has established
treatment standards for metal hazardous constituents that does not otherwise
contain significant organic or cyanide content, as described in Section
728.103(b)(1), and which is specifically listed in Section 728.Appendix K.
“Inorganic solid debris” are nonfriable inorganic solids that are incapable of
passing through a 9.5 mm standard sieve and that require cutting or crushing
and grinding in mechanical sizing equipment prior to stabilization, limited to the
following inorganic or metal materials:
Metal slags (either dross or scoria).
Glassified slag.
Glass.
Concrete (excluding cementitious or pozzolanic stabilized hazardous
wastes).
Masonry and refractory bricks.
Metal cans, containers, drums, or tanks.
Metal nuts, bolts, pipes, pumps, valves, appliances, or industrial
equipment.
Scrap metal, as defined in 35 Ill. Adm. Code 721.101(c)(6).
“Land disposal” means placement in or on the land, except in a corrective
action management unit, and includes, but is not limited to, placement in a
landfill, surface impoundment, waste pile, injection well, land treatment
facility, salt dome formation, salt bed formation, underground mine, or cave or
placement in a concrete vault or bunker intended for disposal purposes.
“Nonwastewaters” are wastes that do not meet the criteria for “wastewaters” in
this Section.
“Polychlorinated biphenyls” or “PCBs” are halogenated organic compounds
defined in accordance with 40 CFR 761.3, incorporated by reference in 35 Ill.
Adm. Code 720.111.
“ppm” means parts per million.
“RCRA corrective action” means corrective action taken under 35 Ill. Adm.
Code 724.200 or 725.193, 40 CFR 264.100 or 265.93 (1996), or similar
381
regulations in other States with RCRA programs authorized by USEPA pursuant
to 40 CFR 271 (1996).
“Soil” means unconsolidated earth material composing the superficial geologic
strata (material overlying bedrock), consisting of clay, silt, sand, or gravel size
particles, as classified by the U.S. Soil Conservation Service, or a mixture of
such materials with liquids, sludges, or solids that is inseparable by simple
mechanical removal processes and which is made up primarily of soil by
volume based on visual inspection.
“Stormwater impoundments” are surface impoundments that receive wet
weather flow and which receive process waste only during wet weather events.
“Underlying hazardous constituent” means any constituent listed in Section
728.Table U of this Part, “Universal Treatment Standards (UTS)”, except
fluoride, selenium, sulfides, vanadium, and zinc, that can reasonably be
expected to be present at the point of generation of the hazardous waste at a
concentration above the constituent-specific UTS treatment standard.
“U.S. EPA” or “USEPA” means the United States Environmental Protection
Agency.
“Wastewaters” are wastes that contain less than 1% percent by weight total
organic carbon (TOC) and less than 1% percent by weight total suspended solids
(TSS).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.103
Dilution Prohibited as a Substitute for Treatment
a)
Except as provided in subsection (b) of this Section, no generator, transporter,
handler, or owner or operator of a treatment, storage, or disposal facility shall
in any way dilute a restricted waste or the residual from treatment of a restricted
waste as a substitute for adequate treatment to achieve compliance with Subpart
D of this Part, to circumvent the effective date of a prohibition in Subpart C of
this Part, to otherwise avoid a prohibition in Subpart C of this Part, or to
circumvent a land disposal restriction imposed by RCRA section 3004.
b)
Dilution of waste that is hazardous only because it exhibits a characteristic of
hazardous waste in a treatment system that treats wastes subsequently discharged
to a water of the State pursuant to an NPDES permit issued under 35 Ill. Adm.
Code 309, that treats wastes in a CWA-equivalent treatment system, that treats
wastes for purposes of pretreatment requirements under 35 Ill. Adm. Code 310
is not impermissible dilution for purposes of this Section unless a method other
382
than DEACT has been specified in Section 728.140 as the treatment standard or
unless the waste is a D003 reactive cyanide wastewater or nonwastewater.
c)
Combustion of waste designated by any of the USEPA hazardous waste codes
listed in Section 728.Appendix J is prohibited, unless the waste can be
demonstrated to comply with one or more of the following criteria at the point
of generation or after any bona fide treatment, such as cyanide destruction prior
to combustion (unless otherwise specifically prohibited from combustion):
1)
The waste contains hazardous organic constituents or cyanide at levels
exceeding the constituent-specific treatment standard found in Section
728.148;
2)
The waste consists of organic, debris-like materials (e.g., wood, paper,
plastic, or cloth) contaminated with an inorganic metal-bearing
hazardous waste;
3)
The waste has reasonable heating value, such as greater than or equal to
5000 BTU Btu per pound, at the point of generation;
4)
The waste is co-generated with wastes for which combustion is a
required method of treatment;
5)
The waste is subject to any federal or state requirements necessitating
reduction of organics (including biological agents); or
6)
The waste contains greater than one percent Total Organic Carbon
(TOC).
d)
It is a form of impermissible dilution, and therefore prohibited, to add iron
filings or other metallic forms of iron to lead-containing hazardous wastes in
order to achieve any land disposal restriction treatment standard for lead. Lead-
containing wastes include D008 wastes (wastes exhibiting a characteristic due to
the presence of lead), all characteristic wastes containing lead as an underlying
hazardous constituent, listed wastes containing lead as a regulated constitutent,
and hazardous media containing any of the aforementioned lead-containing
wastes.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.104
Treatment Surface Impoundment Exemption
a)
Wastes which are otherwise prohibited from land disposal under this Part may
be treated in a surface impoundment or series of impoundments provided that all
of the following conditions are fulfilled:
383
1)
Treatment of such wastes occurs in the impoundments;
2)
The following conditions are met:
A)
Sampling and testing. For wastes with treatment standards in
Subpart D or prohibition levels in Subpart C, the residues from
treatment are analyzed, as specified in Section 728.107 or
728.132, to determine if they meet the applicable treatment
standards or, where no treatment standards have been established
for the waste, the applicable prohibition levels. The sampling
method, specified in the waste analysis plan under 35 Ill. Adm.
Code 724.113 or 725.113, must be designed such that
representative samples of the sludge and the supernatant are
tested separately rather than mixed to form homogeneous
samples.
B)
Removal. The following treatment residues (including any liquid
waste) must be removed at least annually: residues which do not
meet the treatment standards promulgated under Subpart D of this
Part; residues which do not meet the prohibition levels
established under Subpart C of this Part or Section 728.139
imposed by federal statute (where no treatment standards have
been established); residues which that are from the treatment of
wastes prohibited from land disposal under Subpart C of this Part
(where no treatment standards have been established and no
prohibition levels apply); or residues from managing listed wastes
which that are not delisted under 35 Ill. Adm. Code 720.122.
However, residues which are the subject of a valid certification
under Section 728.108 made no later than a year after placement
of the wastes in an impoundment are not required to be removed
annually. If the volume of liquid flowing through the
impoundment or series of impoundments annually is greater than
the volume of the impoundment or impoundments, this flow-
through constitutes removal of the supernatant for the purpose of
this requirement.
C)
Subsequent management. Treatment residues must not be placed
in any other surface impoundment for subsequent management
unless the residues are the subject of a valid certification under
Section 728.108 which allows disposal in surface impoundments
meeting the requirements of Section 728.108(a).
D)
Recordkeeping. Sampling, testing, and recordkeeping provisions
of 35 Ill. Adm. Code 724.113 or 725.113 apply;
384
3)
The impoundment meets the design requirements of 35 Ill. Adm. Code
724.321(c) or 725.321(a) even though the unit may not be new,
expanded or a replacement, and must be in compliance with applicable
groundwater monitoring requirements of 35 Ill. Adm. Code 724.Subpart
F or 725.Subpart F of this Part, unless any of the following conditions is
fulfilled:
A)
The impoundment is exempted pursuant to 35 Ill. Adm. Code
724.321(d) or (e), or to 35 Ill. Adm. Code 725.321(c) or (d);
B)
Upon application by the owner or operator, the Agency has by
permit provided that the requirements of this Part do not apply on
the basis that the surface impoundment fulfills all of the
following conditions:
i)
The impoundment has at least one liner, for which there is
no evidence that such liner is leaking;
ii)
The impoundment is located more than one-quarter mile
from an underground source of drinking water; and
iii)
The impoundment is in compliance with generally
applicable groundwater monitoring requirements for
facilities with permits; or
C)
Upon application by the owner or operator, the Board has,
pursuant to 35 Ill. Adm. Code 106, granted an adjusted standard
from the requirements of this Part. The justification for such an
adjusted standard shall be a demonstration that the surface
impoundment is located, designed and operated so as to assure
that there will be no migration of any hazardous constituent into
groundwater or surface water at any future time; and
4)
The owner or operator submits to the Agency a written certification that
the requirements of subsection (a)(3)of this Section have been met. The
following certification is required:
I certify under penalty of law that the requirements of 35 Ill.
Adm. Code 728.104(a)(3) have been met for all surface
impoundments being used to treat restricted wastes. I believe
that the submitted information is true, accurate and complete. I
am aware that there are significant penalties for submitting false
information, including the possibility of fine and imprisonment.
385
b)
Evaporation of hazardous constituents as the principal means of treatment is not
considered to be a treatment for purposes of an exemption under this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.107
Testing, Tracking, and Recordkeeping Requirements for Generators,
Treaters, and Disposal Facilities
a)
Requirements for generators:
1)
A generator of a hazardous waste shall determine if the waste has to be
treated before it can be land disposed. This is done by determining if
the hazardous waste meets the treatment standards in Section 728.140, or
Section 728.145, or 728.149. This determination can be made in either
of two ways: testing the waste or using knowledge of the waste.
Testing If the generator tests the waste, testing determines the total
concentration of hazardous constituents, or the concentration of
hazardous constituents in an extract of the waste obtained using SW-846
Method 1311 (the Toxicity Characteristic Leaching Procedure),
incorporated by reference in 35 Ill. Adm. Code 720.111, depending on
whether the treatment standard for the waste is expressed as a total
concentration or concentration of hazardous constituent in the waste’s
extract. In addition, some hazardous wastes must be treated by
particular treatment methods before they can be land disposed and some
soils are contaminated by such hazardous wastes. These treatment
standards are also found in Sections Section 728.140 and 728.Table T of
this Part, and are described in detail in Section 728.Table C of this Part.
These wastes and soils contaminated with such wastes do not need to be
tested (however, if they are in a waste mixture, other wastes with
concentration level treatment standards shall must be tested). If a
generator determines that it is managing a waste or soil contaminated
with a waste that displays a hazardous characteristic of ignitability,
corrosivity, reactivity, or toxicity, the generator shall comply with the
special requirements of Section 728.109 in addition to any applicable
requirements in this Section.
2)
If the waste or contaminated soil does not meet the treatment standard:
With the initial shipment of waste to each treatment or storage facility,
the generator shall send a one-time written notice to each treatment or
storage facility receiving the waste with the initial shipment of waste to
each treatment or storage facility, and the generator shall place a copy of
the one-time notice in the file. The notice must include the information
in column “728.107(a)(2)” of the Generator Paperwork Requirements
Table in Section 728.Table I of this Part. No further notification is
necessary until such time that the waste or facility changes, in which
386
case a new notification must be sent and a copy placed in the generator’s
file.
A)
For contaminated soil, the following certification statement
should be included, signed by an authorized representative:
I certify under penalty of law that I personally have
examined this contaminated soil and it (does/does not)
contain listed hazardous waste and (does/does not) exhibit
a characteristic of hazardous waste and requires treatment
to meet the soil treatment standards as provided by 35 Ill.
Adm. Code 728.149(c).
B)
This subsection (a)(2)(B) corresponds with 40 CFR
268.7(a)(2)(ii), which is marked “reserved” by USEPA. This
statement maintains structural consistency with USEPA rules.
3)
If the waste or contaminated soil meets the treatment standard at the
original point of generation:
A)
With the initial shipment of waste to each treatment, storage, or
disposal facility, the generator shall send a one-time written
notice to each treatment, storage, or disposal facility receiving
the waste, and place a copy in its own file. The notice must
include the information indicated in column “728.107(a)(3)” of
the Generator Paperwork Requirements Table in Section
728.Table I of this Part and the following certification statement,
signed by an authorized representative:
I certify under penalty of law that I personally have
examined and am familiar with the waste through analysis
and testing or through knowledge of the waste to support
this certification that the waste complies with the
treatment standards specified in 35 Ill. Adm. Code
728.Subpart D. I believe that the information I submitted
is true, accurate, and complete. I am aware that there are
significant penalties for submitting a false certification,
including the possibility of a fine and imprisonment.
B)
If the waste changes, the generator shall send a new notice and
certification to the receiving facility, and place a copy in its file.
Generators of hazardous debris excluded from the definition of
hazardous waste under 35 Ill. Adm. Code 721.103(f) are not
subject to these requirements.
387
B)
For contaminated soil, with the initial shipment of wastes to each
treatment, storage, or disposal facility, the generator must send a
one-time written notice to each facility receiving the waste and
place a copy in the file. The notice must include the information
in the column headed “(a)(3)” in Table I of this Part.
4)
For reporting, tracking and recordkeeping when exceptions allow certain
wastes or contaminated soil that do not meet the treatment standards to
be land disposed,: There there are certain exemptions from the
requirement that hazardous wastes or contaminated soil meet treatment
standards before they can be land disposed. These include, but are not
limited to, case-by-case extensions under Section 728.105, disposal in a
no-migration unit under Section 728.106, or a national capacity variance
or case-by-case capacity variance under Subpart C of this Part. If a
generator’s waste is so exempt, then with the initial shipment of waste,
the generator shall send a one-time written notice to each land disposal
facility receiving the waste. The notice must include the information
indicated in column “728.107(a)(4)” of the Generator Paperwork
Requirements Table in Section 728.Table I of this Part. If the waste
changes, the generator shall send a new notice to the receiving facility,
and place a copy in its file.
5)
If a generator is managing and treating prohibited waste or contaminated
soil in tanks, containers, or containment buildings regulated under 35 Ill.
Adm. Code 722.134 to meet applicable LDR treatment standards found
at Section 728.140, the generator shall develop and follow a written
waste analysis plan that describes the procedures it will carry out to
comply with the treatment standards. (Generators treating hazardous
debris under the alternative treatment standards of Section 728.Table F
of this Part, however, are not subject to these waste analysis
requirements.) The plan must be kept on site in the generator’s records,
and the following requirements must be met:
A)
The waste analysis plan must be based on a detailed chemical and
physical analysis of a representative sample of the prohibited
wastes being treated, and contain all information necessary to
treat the wastes in accordance with the requirements of this Part,
including the selected testing frequency;
B)
Such plan must be kept in the facility’s on-site files and made
available to inspectors; and
C)
Wastes shipped off-site pursuant to this subsection (a)(5) of this
Section must comply with the notification requirements of
subsection (a)(3) of this Section.
388
6)
If a generator determines that the waste or contaminated soil is restricted
based solely on its knowledge of the waste, all supporting data used to
make this determination must be retained on-site in the generator’s files.
If a generator determines that the waste is restricted based on testing this
waste or an extract developed using SW-846 Method 1311 (the Toxicity
Characteristic Leaching Procedure), incorporated by reference in 35 Ill.
Adm. Code 720.111, and all waste analysis data must be retained on-site
in the generator’s files.
7)
If a generator determines that it is managing a restricted prohibited waste
which is excluded from the definition of hazardous or solid waste or
which is exempt from Subtitle C regulation under 35 Ill. Adm. Code
721.102 through 721.106 subsequent to the point of generation
(including deactivated characteristic hazardous wastes that are managed
in wastewater treatment systems subject to the CWA, as specified at 35
Ill. Adm. Code 721.104(a)(2),; or which that are CWA-equivalent; or
that are managed in an underground injection well regulated under 35
Ill. Adm. Code 730), the generator shall place a one-time notice stating
such generation, subsequent exclusion from the definition of hazardous
or solid waste or exemption from RCRA Subtitle C regulation, and the
disposition of the waste in the generating facility’s on-site file.
8)
A generator shall retain a copy of all notices, certifications, waste
analysis data, and other documentation produced pursuant to this Section
on-site for at least three years from the date that the waste that is the
subject of such documentation was last sent to on-site or off-site
treatment, storage, or disposal. The three year record retention period is
automatically extended during the course of any unresolved enforcement
action regarding the regulated activity or as requested by the Agency.
The requirements of this subsection (a)(8) apply to solid wastes even
when the hazardous characteristic is removed prior to disposal, or when
the waste is excluded from the definition of hazardous or solid waste
under 35 Ill. Adm. Code 721.102 through 721.106, or exempted from
RCRA Subtitle C regulation, subsequent to the point of generation.
9)
If a generator is managing a lab pack containing hazardous wastes and
wishes to use the alternative treatment standard for lab packs found at
Section 728.142(c), the generator shall fulfill the following conditions:
A)
With the initial shipment of waste to a treatment facility, the
generator shall submit a notice that provides the information in
column “Section 728.107(a)(9)” in the Generator Paperwork
Requirements Table of Section 728.Table I of this Part and the
following certification. The certification, which must be signed
389
by an authorized representative and must be placed in the
generator’s files, must say the following:
I certify under penalty of law that I personally have
examined and am familiar with the waste and that the lab
pack contains only wastes that have not been excluded
under 35 Ill. Adm. Code 728.Appendix D and that this
lab pack will be sent to a combustion facility in
compliance with the alternative treatment standards for lab
packs at 35 Ill. Adm. Code 728.142(c). I am aware that
there are significant penalties for submitting a false
certification, including the possibility of fine or
imprisonment.
B)
No further notification is necessary until such time as the wastes
in the lab pack change, or the receiving facility changes, in which
case a new notice and certification must be sent and a copy
placed in the generator’s file.
C)
If the lab pack contains characteristic hazardous wastes (D001-
D043), underlying hazardous constituents (as defined in Section
728.102(i)) need not be determined.
D)
The generator shall also comply with the requirements in
subsections (a)(6) and (a)(7) of this Section.
10)
Small quantity generators with tolling agreements pursuant to 35 Ill.
Adm. Code 722.120(e) shall comply with the applicable notification and
certification requirements of subsection (a) of this Section for the initial
shipment of the waste subject to the agreement. Such generators shall
retain on-site a copy of the notification and certification, together with
the tolling agreement, for at least three years after termination or
expiration of the agreement. The three-year record retention period is
automatically extended during the course of any unresolved enforcement
action regarding the regulated activity or as requested by the Agency.
b)
The owner or operator of a treatment facility shall test its wastes according to
the frequency specified in its waste analysis plan, as required by 35 Ill. Adm.
Code 724.113 (for permitted TSDs) or 725.113 (for interim status facilities).
Such testing must be performed as provided in subsections (b)(1), (b)(2), and
(b)(3) of this Section.
1)
For wastes or contaminated soil with treatment standards expressed as
concentrations in the waste extract (TCLP), the owner or operator of the
treatment facility shall test an extract of the treatment residues using SW-
390
846 Method 1311 (the Toxicity Characteristic Leaching Procedure),
incorporated by reference in 35 Ill. Adm. Code 720.111, to assure that
the treatment residues extract meets the applicable treatment standards.
2)
For wastes or contaminated soil with treatment standards expressed as
concentrations in the waste, the owner or operator of the treatment
facility shall test the treatment residues (not an extract of such residues)
to assure that the treatment residues meet the applicable treatment
standards.
3)
A one-time notice must be sent with the initial shipment of waste or
contaminated soil to the land disposal facility. A copy of the notice must
be placed in the treatment facility’s file.
A)
No further notification is necessary until such time that the waste
or receiving facility changes, in which case a new notice must be
sent and a copy placed in the treatment facility’s file.
B)
The one-time notice must include the requirements indicated in
the following table:
Treatment Facility Paperwork Requirements Table
Required information
Section
728.107(b)
1. USEPA Hazardous Waste hazardous
waste number and Manifest numbers
manifest number of first shipment.
ü
2. The waste is subject to the LDRs. The
constituents of concern for F001- through
F005 and F039 waste and underlying
hazardous constituents in characteristic
wastes (for wastes that are not managed in a
Clean Water Act (CWA) or CWA-equiva-
lent facility), unless the waste will be treat-
ed and monitored for all constituents. If all
constituents will be treated and monitored,
there is no need to put them all on the LDR
notice.
ü
3. The notice must include the applicable
wastewater/ nonwastewater category (see
Section Section 728.102(d) and (f)) and
subdivisions made within a waste code
based on waste-specific criteria (such as
D003 reactive cyanide).
ü
391
4. Waste analysis data (when available).
ü
5. For contaminated soil subject to LDRs as
provided in Section 728.149(a), the
constituents subject to treatment as
described in Section 728.149(d) and the
following statement, “this contaminated soil
(does/does not) contain listed hazardous
waste and (does/does not) exhibit a
characteristic of hazardous waste and (is
subject to/complies with) the soil treatment
standards as provided by Section
728.149(c).
ü
56. A certification statement is needed (see
applicable section for exact wording).
ü
4)
The owner or operator of a treatment facility shall submit a certification
signed by an authorized representative with the initial shipment of waste
or treatment residue of a restricted waste to the land disposal facility.
The certification must state as follows:
I certify under penalty of law that I have personally examined
and am familiar with the treatment technology and operation of
the treatment process used to support this certification. Based on
my inquiry of those individuals immediately responsible for
obtaining this information, I believe that the treatment process
has been operated and maintained properly so as to comply with
the treatment standards specified in 35 Ill. Adm. Code 728.140
without impermissible dilution of the prohibited waste. I am
aware there are significant penalties for submitting a false
certification, including the possibility of fine and imprisonment.
A certification is also necessary for contaminated soil and it must state:
I certify under penalty of law that I have personally examined
and am familiar with the treatment technology and operation of
the treatment process used to support this certification and believe
that it has been maintained and operated properly so as to comply
with treatment standards specified in 35 Ill. Adm. Code 728.149
without impermissible dilution of the prohibited wastes. I am
aware there are significant penalties for submitting a false
certification, including the possibility of fine and imprisonment.
A)
A copy of the certification must be placed in the treatment
facility’s on-site files. If the waste or treatment residue changes,
or the receiving facility changes, a new certification must be sent
392
to the receiving facility, and a copy placed in the treatment
facility’s file.
B)
Debris excluded from the definition of hazardous waste under 35
Ill. Adm. Code 721.103(e) (i.e., debris treated by an extraction
or destruction technology listed in Section 728.Table F of this
Part and debris that the Agency has determined does not contain
hazardous waste) is subject to the notification and certification
requirements of subsection (d) of this Section rather than the
certification requirements of this subsection (b)(4).
C)
For wastes with organic constituents having treatment standards
expressed as concentration levels, if compliance with the
treatment standards is based in part or in whole on the analytical
detection limit alternative specified in Section 728.140(d), the
certification must be signed by an authorized representative and
must state the following:
I certify under penalty of law that I have personally
examined and am familiar with the treatment technology
and operation of the treatment process used to support this
certification. Based on my inquiry of those individuals
immediately responsible for obtaining this information, I
believe that the nonwastewater organic constituents have
been treated by combustion units as specified in 35 Ill.
Adm. Code 728.Table C. I have been unable to detect
the nonwastewater organic constituents, despite having
used best good faith efforts to analyze for such
constituents. I am aware that there are significant
penalties for submitting a false certification, including the
possibility of fine and imprisonment.
D)
For characteristic wastes that are subject to the treatment
standards in Section 728.140 and Table T of this Part (other than
those expressed as a required method of treatment) that are
reasonably expected to contain underlying hazardous constituents
as defined in 35 Ill. Adm. Code 728.102(i); that are treated on-
site to remove the hazardous characteristic; and that are then sent
off-site for treatment of underlying hazardous constituents, the
certification must state the following:
I certify under penalty of law that the waste has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.140 and Table T of that Part to remove
the hazardous characteristic. This decharacterized waste
393
contains underlying hazardous constituents that require
further treatment to meet universal treatment standards. I
am aware that there are significant penalties for
submitting a false certification, including the possibility of
fine and imprisonment.
E)
For characteristic wastes that contain underlying hazardous
constituents as defined in Section 728.102(i) that are treated on-
site to remove the hazardous characteristic and to treat underlying
hazardous constituents to levels in Section 728.148 and Table U
of this Part universal treatment standards, the certification must
state the following:
I certify under penalty of law that the waste has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.140 and Table T of that Part to remove
the hazardous characteristic and that underlying hazardous
constituents, as defined in 35 Ill. Adm. Code 728.102(i)
have been treated on-site to meet the 35 Ill. Adm. Code
728.148 and Table U of that Part universal treatment
standards. I am aware that there are significant penalties
for submitting a false certification, including the
possibility of fine and imprisonment.
5)
If the waste or treatment residue will be further managed at a different
treatment, or storage, or disposal facility, the treatment, storage, or
disposal facility sending the waste or treatment residue off-site must
comply with the notice and certification requirements applicable to
generators under this Section.
6)
Where the wastes are recyclable materials used in a manner constituting
disposal subject to the provisions of 35 Ill. Adm. Code 726.120(b),
regarding treatment standards and prohibition levels, the owner or
operator of a treatment facility (i.e., the recycler) is not required to
notify the receiving facility pursuant to subsection (b)(4)(3)) of this
Section. With each shipment of such wastes the owner or operator of
the recycling facility shall submit a certification described in subsection
(b)(5)(4) of this Section and a notice that includes the information listed
in subsection (b)(4)(3) of this Section (except the manifest number) to
the Agency. The recycling facility also shall keep records of the name
and location of each entity receiving the hazardous waste-derived
product.
c)
Except where the owner or operator is disposing of any waste that is a
recyclable material used in a manner constituting disposal pursuant to 35 Ill.
394
Adm. Code 726.120(b), the owner or operator of any land disposal facility
disposing any waste subject to restrictions under this Part shall:
1)
Maintain in its files copies of the notice and certifications specified in
subsection (a) or (b) of this Section.
2)
Test the waste or an extract of the waste or treatment residue developed
using SW-846 Method 1311 (the Toxicity Characteristic Leaching
Procedure), incorporated by reference in 35 Ill. Adm. Code 720.111), to
assure that the waste or treatment residue is in compliance with the
applicable treatment standards set forth in Subpart D of this Part. Such
testing must be performed according to the frequency specified in the
facility’s waste analysis plan as required by 35 Ill. Adm. Code 724.113
or 725.113.
3)
Where the owner or operator is disposing of any waste that is subject to
the prohibitions under Section 728.133(f) but not subject to the
prohibitions set forth in Section 728.132, the owner or operator shall
ensure that such waste is the subject of a certification according to the
requirements of Section 728.108 prior to disposal in a landfill or surface
impoundment unit, and that such disposal is in accordance with the
requirements of Section 728.105(h)(2). The same requirement applies to
any waste that is subject to the prohibitions under Section 728.133(f) and
also is subject to the statutory prohibitions in the codified prohibitions in
Section 728.139 or Section 728.132.
4)
Where the owner or operator is disposing of any waste that is a
recyclable material used in a manner constituting disposal subject to the
provisions of 35 Ill. Adm. Code 726.120(b), the owner or operator is
not subject to subsections (c)(1) through (c)(3) of this Section with
respect to such waste.
d)
A generator or treater that first claims that hazardous debris is excluded from
the definition of hazardous waste under 35 Ill. Adm. Code 721.103(e) (i.e.,
debris treated by an extraction or destruction technology provided by Section
728.Table F of this Part, and debris that has been delisted) is subject to the
following notification and certification requirements:
1)
A one-time notification must be submitted to the Agency including the
following information:
A)
The name and address of the RCRA Subtitle D (municipal solid
waste landfill) facility receiving the treated debris;
395
B)
A description of the hazardous debris as initially generated,
including the applicable USEPA hazardous waste numbers; and
C)
For debris excluded under 35 Ill. Adm. Code 721.103(e)(1), the
technology from Section 728.Table F of this Part used to treat the
debris.
2)
The notification must be updated if the debris is shipped to a different
facility and, for debris excluded under 35 Ill. Adm. Code 721.102(e)(1),
if a different type of debris is treated or if a different technology is used
to treat the debris.
3)
For debris excluded under 35 Ill. Adm. Code 721.103(e)(1), the owner
or operator of the treatment facility shall document and certify
compliance with the treatment standards of Section 728.Table F of this
Part, as follows:
A)
Records must be kept of all inspections, evaluations, and analyses
of treated debris that are made to determine compliance with the
treatment standards;
B)
Records must be kept of any data or information the treater
obtains during treatment of the debris that identifies key operating
parameters of the treatment unit; and
C)
For each shipment of treated debris, a certification of compliance
with the treatment standards must be signed by an authorized
representative and placed in the facility’s files. The certification
must state the following:
I certify under penalty of law that the debris has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.145. I am aware that there are
significant penalties for making a false certification,
including the possibility of fine and imprisonment.
e)
A generator or treater that first receives a determination from USEPA or the
Agency that a given contaminated soil subject to LDRs, as provided in Section
728.149(a), no longer contains a listed hazardous waste and generators and
treaters that first determine that a contaminated soil subject to LDRs, as
provided in Section 728.149(a), no longer exhibits a characteristic of hazardous
waste shall do the following:
1)
Prepare a one-time only documentation of these determinations including
all supporting information; and
396
2)
Maintain that information in the facility files and other records for a
minimum of three years.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section 728.133
Waste-Specific Prohibitions -- First Third Wastes (Repealed)
Section 728.133
Waste-Specific Prohibitions -- Organobromine Wastes
a)
The waste specified in 35 Ill. Adm. Code 721.132 as USEPA hazardous waste
number K140 and in 35 Ill. Adm. Code 721.133 as USEPA hazardous waste
number U408 are prohibited from land disposal. In addition, soils and debris
contaminated with these wastes, radioactive wastes mixed with these hazardous
wastes, and soils and debris contaminated with these radioactive mixed wastes
are prohibited from land disposal.
b)
The requirements of subsection (a) of this Section do not apply if:
1)
The wastes meet the applicable treatment standards specified in Subpart
D of this Part;
2)
The Board has granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to the wastes and units
covered by the petition;
3)
The wastes meet the applicable treatment standards established pursuant
to a petition granted under Section 728.144;
4)
Hazardous debris that has met treatment standards in Section 728.140
and Table T of this Part or, in the alternative, the treatment standards in
Section 728.145; or
5)
USEPA has granted an extension to the effective date of a prohibition, as
described in Section 728.105, with respect to those wastes covered by
the extension.
c)
To determine whether a hazardous waste identified in this Section exceeds the
applicable treatment standards specified in Section 728.140 and Table T of this
Part, the initial generator shall test a sample of the waste extract or the entire
waste, depending on whether the treatment standards are expressed as
concentrations in the waste extract or in the waste, or the generator may use
knowledge of the waste. If the waste contains constituents in excess of the
397
applicable universal treatment standard levels of Section 728.148 and Table U of
this Part, the waste is prohibited from land disposal, and all requirements of this
Part are applicable, except as otherwise specified.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 728.134
Waste Specific Prohibitions -- Second Third Wastes (Repealed)
Section 728.134
Waste-Specific Prohibitions -- Toxicity Characteristic Metal Wastes
a)
The following wastes are prohibited from land disposal: the wastes specified in
35 Ill. Adm. Code 721 as USEPA hazardous waste numbers D004 through
D011 that are newly identified (i.e., wastes, soil, or debris identified as
hazardous by the Toxic Characteristic Leaching Procedure but not the
Extraction Procedure), and waste, soil, or debris from mineral processing
operations that is identified as hazardous by the specifications at 35 Ill. Adm.
Code 721.
b)
The following waste is prohibited from land disposal: slag from secondary lead
smelting that exhibits the characteristic of toxicity due to the presence of one or
more metals.
c)
Effective May 26, 2000, the following wastes are prohibited from land
disposal: newly identified characteristic wastes from elemental phosphorus
processing; radioactive wastes mixed with USEPA hazardous waste numbers
D004 through D011 wastes that are newly identified (i.e., wastes, soil, or
debris identified as hazardous by the Toxic Characteristic Leaching Procedure
but not the Extraction Procedure); or mixed with newly identified characteristic
mineral processing wastes, soil, or debris.
d)
Until May 26, 2000, newly identified characteristic wastes from elemental
phosphorus processing, radioactive waste mixed with USEPA hazardous waste
numbers D004 through D011 wastes that are newly identified (i.e., wastes, soil,
or debris identified as hazardous by the Toxic Characteristic Leaching
Procedure but not the Extraction Procedure), or mixed with newly identified
characteristic mineral processing wastes, soil, or debris may be disposed in a
landfill or surface impoundment only if such unit is in compliance with the
requirements specified in Section 728.105(h)(2).
e)
The requirements of subsections (a) and (b) of this Section do not apply if any
of the following applies to the waste:
1)
The wastes meet the applicable treatment standards specified in Subpart
D of this Part;
398
2)
The Board has granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to those wastes and units
covered by the petition;
3)
The wastes meet the applicable alternate treatment standards established
pursuant to a petition granted under Section 728.144; or
4)
USEPA has granted an extension to the effective date of a prohibition
pursuant to 40 CFR 268.5, with respect to those wastes covered by the
extension.
f)
To determine whether a hazardous waste identified in this Section exceeds the
applicable treatment standards specified in Section 728.140 and Table T of this
Part, the initial generator must test a sample of the waste extract or the entire
waste, depending on whether the treatment standards are expressed as
concentrations in the waste extract or the waste, or the generator may use
knowledge of the waste. If the waste contains constituents (including
underlying hazardous constituents in characteristic wastes) in excess of the
applicable universal treatment standard levels of Section 728.148 and Table U of
this Part, the waste is prohibited from land disposal, and all requirements of this
Part are applicable, except as otherwise specified.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 728.135
Waste Specific Prohibitions -- Third Third Wastes (Repealed)
Section 728.135
Waste Specific Prohibitions -- Petroleum Refining Wastes
a)
Effective February 8, 1999, the wastes specified in 35 Ill. Adm. Code 721.132
as USEPA hazardous wastes numbers K169, K170, K171, and K172; soils and
debris contaminated with these wastes; radioactive wastes mixed with these
hazardous wastes; and soils and debris contaminated with these radioactive
mixed wastes are prohibited from land disposal.
b)
The requirements of subsection (a) of this Section do not apply under any of the
following circumstances:
1)
The wastes meet the applicable treatment standards specified in Subpart
D of this Part;
2)
The Board has granted an adjusted standard that exempts waste from a
prohibition pursuant to Section 728.106, with respect to those wastes and
units covered by the adjusted standard;
3)
The wastes meet an adjusted standard from an applicable treatment
standard granted under Section 728.144;
399
4)
The waste is hazardous debris that has met the treatment standards set
forth in Section 728.140 and Table T of this Part or the alternative
treatment standards in Section 728.145; or
5)
USEPA has granted an extension to the effective date of a prohibition
pursuant to 40 CFR 268.5, with respect to these wastes covered by the
extension.
c)
To determine whether a hazardous waste identified in this section exceeds the
applicable treatment standards specified in Section 728.140, the initial generator
must test a sample of the waste extract or the entire waste, depending on
whether the treatment standards are expressed as concentrations in the waste
extract or the waste, or the generator may use knowledge of the waste. If the
waste contains constituents in excess of the applicable universal treatment
standard levels of Section 728.148 and Table U of this Part, the waste is
prohibited from land disposal, and all requirements of this Part are applicable,
except as otherwise specified.
SUBPART D: TREATMENT STANDARDS
Section 728.140
Applicability of Treatment Standards
a)
A prohibited waste identified in Section 728.Table T of this Part, “Treatment
Standards for Hazardous Wastes”, may be land disposed only if it meets the
requirements found in that Section. For each waste, Section 728.Table T of this
Part identifies one of three types of treatment standard requirements:
1)
All hazardous constituents in the waste or in the treatment residue must
be at or below the values found in that Section for that waste (“total
waste standards”);
2)
The hazardous constituents in the extract of the waste or in the extract of
the treatment residue must be at or below the values found in that
Section (“waste extract standards”); or
3)
The waste must be treated using the technology specified in that Section
(“technology standard”), which is described in detail in Section
728.Table C of this Part, “Technology Codes and Description of
Technology-Based Standards”.
b)
For wastewaters, compliance with concentration level standards is based on
maximums for any one day, except for D004 through D011 wastes for which
the previously promulgated treatment standards based on grab samples remain in
400
effect. For all nonwastewaters, compliance with concentration level standards is
based on grab sampling. For wastes covered by the waste extract standards, the
test Method 1311, the Toxicity Characteristic Leaching Procedure, found in
“Test Methods for Evaluating Solid Waste, Physical/Chemical Methods”,
USEPA Publication SW-846, incorporated by reference in Section 720.111,
must be used to measure compliance. An exception is made for D004 and
D008, for which either of two test methods may be used: Method 1311 or
Method 1310, the Extraction Procedure Toxicity Test, found in “Test Methods
for Evaluating Solid Waste, Physical/Chemical Methods”, USEPA Publication
SW-846, incorporated by reference in Section 720.111. For wastes covered by
a technology standard, the wastes may be land disposed after being treated using
that specified technology or an equivalent treatment technology approved by the
Agency pursuant to Section 728.142(b).
c)
When wastes with differing treatment standards for a constituent of concern are
combined for purposes of treatment, the treatment residue must meet the lowest
treatment standard for the constituent of concern.
d)
Notwithstanding the prohibitions specified in subsection (a) of this Section,
treatment and disposal facilities may demonstrate (and certify pursuant to 35 Ill.
Adm. Code 728.107(b)(5)) compliance with the treatment standards for organic
constituents specified by a footnote in Section 728.Table T of this Part,
provided the following conditions are satisfied:
1)
The treatment standards for the organic constituents were established
based on incineration in units operated in accordance with the technical
requirements of 35 Ill. Adm. Code 724.Subpart O, or based on
combustion in fuel substitution units operating in accordance with
applicable technical requirements;
2)
The treatment or disposal facility has used the methods referenced in
subsection (d)(1) of this Section to treat the organic constituents; and
3)
The treatment or disposal facility may demonstrate compliance with
organic constituents if good-faith analytical efforts achieve detection
limits for the regulated organic constituents that do not exceed the
treatment standards specified in this Section and Section 728.Table T of
this Part by an order of magnitude.
e)
For a characteristic wastes waste (USEPA hazardous waste numbers number
D001 through D003 and D018 through D043) that are is subject to treatment
standards set forth in Section 728.Table T of this Part, “Treatment Standards
for Hazardous Wastes”, and the waste is not managed in a wastewater treatment
system that is either regulated under the Clean Water Act (CWA) or one that is
CWA-equivalent or the waste is injected into a Class I nonhazardous deep
401
injection well, all underlying hazardous constituents (as defined in Section
728.102(i)) must meet the universal treatment standards, set forth in Section
728.Table U of this Part prior to land disposal, as defined in Section
728.102(c).
f)
The treatment standards for USEPA hazardous waste numbers F001 through
F005 nonwastewater constituents carbon disulfide, cyclohexanone, or methanol
apply to wastes that contain only one, two, or three of these constituents.
Compliance is measured for these constituents in the waste extract from test
Method 1311, the Toxicity Characteristic Leaching Procedure found in “Test
Methods for Evaluating Solid Waste, Physical/Chemical Methods”, USEPA
Publication SW-846, incorporated by reference in Section 720.111. If the waste
contains any of these three constituents along with any of the other 25
constituents found in USEPA hazardous waste numbers F001 through F005,
then compliance with treatment standards for carbon disulfide, cyclohexanone,
or methanol are not required.
g)
This subsection corresponds with 40 CFR 268.40(g), added at 61 Fed. Reg.
43927 (Aug. 26, 1996), which has expired. This statement maintains structural
consistency with the federal rules.
h)
Prohibited USEPA hazardous waste numbers D004 through D011, mixed
radioactive wastes, and mixed radioactive listed wastes containing metal
constituents that were previously treated by stabilization to the treatment
standards in effect at that time and then put into storage do not have to be re-
treated to meet treatment standards in this Section prior to land disposal.
i)
Zinc-containing fertilizers that are produced for the use of the general public
and which are produced from or contain recycled characteristic hazardous
wastes (D004 through D011) are subject to the applicable treatment standards
set forth in 40 CFR 268.41 (1990), incorporated by reference in 35 Ill. Adm.
Code 720.111(b).
BOARD NOTE: USEPA added 40 CFR 268.40(i) at 63 Fed. Reg. 46331
(Aug. 31, 1998) to stay the Phase IV land disposal restrictions (LDRs) as they
apply to zinc-containing fertilizers while it develops a more comprehensive set
of regulations applicable to use of hazardous waste in making fertilizers. To
effect the stay, USEPA applied the 1990 LDR standards to the affected
materials.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
402
Section 728.142
Treatment Standards Expressed as Specified Technologies
a)
The following wastes listed in subsections (a)(1) and (b)(2) below and Section
728.Table T of this Part, “Treatment Standards for Hazardous Wastes,”, for which
standards are expressed as a treatment method rather than a concentration level,
must be treated using the technology or technologies specified in subsections (a)(1)
and (a)(2) below and Section 728.Table T C of this Part.
1)
Liquid hazardous wastes containing PCBs at concentrations greater than or
equal to 50 ppm but less than 500 ppm must be incinerated in accordance
with the technical requirements of 40 CFR 761.70, incorporated by
reference in 35 Ill. Adm. Code 720.111, or burned in high efficiency boilers
in accordance with the technical requirements of 40 CFR 761.60. Liquid
hazardous wastes containing PCBs at concentrations greater than or equal to
500 ppm must be incinerated in accordance with the technical requirements
of 40 CFR 761.70. Thermal treatment in accordance with this Section must
be in compliance with applicable regulations in 35 Ill. Adm. Code 724, 725,
and 726.
2)
Nonliquid hazardous wastes containing halogenated organic compounds
(HOCs) in total concentrations greater than or equal to 1000 mg/kg and
liquid HOC-containing wastes that are prohibited under Section
728.132(e)(1) must be incinerated in accordance with the requirements of 35
Ill. Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O. These
treatment standards do not apply where the waste is subject to a treatment
standard codified in 728.Subpart C of this Part for a specific HOC (such as
a hazardous waste chlorinated solvent for which a treatment standard is
established under Section 728.141(a)).
3)
A mixture consisting of wastewater, the discharge of which is subject to
regulation under 35 Ill. Adm. Code 309 or 310, and de minimis losses of
materials from manufacturing operations in which these materials are used as
raw materials or are produced as products in the manufacturing process that
meet the criteria of the D001 ignitable liquids containing greater than 10%
percent total organic constituents (TOC) subcategory are subject to the
DEACT treatment standard described in Section 728.Table C of this Part.
For purposes of this subsection, “de minimis losses” include:
A)
Those from normal material handling operations (e.g., spills from
the unloading or transfer of materials from bins or other containers,
or leaks from pipes, valves, or other devices used to transfer
materials);
B)
Minor leaks from process equipment, storage tanks, or containers;
403
C)
Leaks from well-maintained pump packings and seals;
D)
Sample purgings; and
E)
Relief device discharges.
b)
Any person may submit an application to the Agency demonstrating that an
alternative treatment method can achieve a level of performance equivalent to that
achievable by methods specified in subsections (a), above and (c), and (d) below of
this Section for wastes or specififed specified in Section 728.Table F of this Part
for hazardous debris. The applicant shall submit information demonstrating that the
applicant’s treatment method is in compliance with federal and state requirements,
including this Part; 35 Ill. Adm. Code 709, 724, 725, 726, and 729; and Sections
22.6 and 39(h) of the Environmental Protection Act [415 ILCS 5/22.6 and 39(h)]
and that the treatment method is protective of human health and the environment.
On the basis of such information and any other available information, the Agency
shall approve the use of the alternative treatment method if the Agency finds that the
alternative treatment method provides a measure of performance equivalent to that
achieved by methods specified in subsections (a) above of this Section and (c) and
(d) below of this Section and in Section 728.Table F of this Part, for hazardous
debris. Any approval must be stated in writing and may contain such provisions
and conditions as the Agency determines to be appropriate. The person to whom
such approval is issued shall comply with all limitations contained in such
determination.
c)
As an alternative to the otherwise applicable treatment standards of 728.Subpart D
of this Part, lab packs are eligible for land disposal provided the following
requirements are met:
1)
The lab packs comply with the applicable provisions of 35 Ill. Adm. Code
724.416 and 725.416;
BOARD NOTE: 35 Ill. Adm. Code 729.301 and 729.312 include
additional restrictions on the use of lab packs.
2)
The lab pack does not contain any of the wastes listed in Section
728.Appendix D of this Part;
3)
The lab packs are incinerated in accordance with the requirements of 35 Ill.
Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O; and
4)
Any incinerator residues from lab packs containing D004, D005, D006,
D007, D008, D010, and D011 are treated in compliance with the applicable
treatment standards specified for such wastes in 728.Subpart D of this Part.
404
d)
Radioactive hazardous mixed wastes are subject to the treatment standards in
Sections Section 728.140 and 728.Table T of this Part. Where treatment standards
are specified for radioactive mixed wastes in Section 728.Table T of this Part,
“Table of Treatment Standards”, those treatment standards will govern. Where
there is no specific treatment standard for radioactive mixed waste, the treatment
standard for the hazardous waste (as designated by EPA waste code) applies.
Hazardous debris containing radioactive waste is subject to the treatment standards
specified in Section 728.145.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.144
Adjustment of Treatment Standard
a)
Where the treatment standard is expressed as a concentration in a waste or waste
extract and a waste cannot be treated to the specified level, or where the
treatment technology is not appropriate to the waste, the generator or treatment
facility may petition to the Board for an adjusted treatment standard. As
justification, the petitioner shall demonstrate that, because the physical or
chemical properties of the waste differ significantly from wastes analyzed in
developing the treatment standard, the waste cannot be treated to specified
levels or by the specified methods.
a)
Based on a petition filed by a generator or treater of hazardous waste, the Board
will grant an adjusted standard from an applicable treatment standard if the
petitioner can demonstrate that either of the following applies to treatment of the
waste:
1)
It is not physically possible to treat the waste to the level specified in the
treatment standard, or by the method specified as the treatment
standard. To show that this is the case, the petitioner must demonstrate
that because the physical or chemical properties of the waste differ
significantly from waste analyzed in developing the treatment standard,
the waste cannot be treated to the specified level or by the specified
method; or
2)
It is inappropriate to require the waste to be treated to the level specified
in the treatment standard or by the method specified as the treatment
standard, even though such treatment is technically possible. To show
that this is the case, the petitioner must demonstrate that either of the
following applies to treatment of the waste:
A)
Treatment to the specified level or by the specified method is
technically inappropriate (for example, resulting in combustion of
large amounts of mildly contaminated environmental media); or
405
B)
For remediation waste only, treatment to the specified level or by
the specified method is environmentally inappropriate because it
would likely discourage aggressive remediation.
BOARD NOTE: 40 CFR 268.44 refers to these as “treatability
variances”. The Board has not used this term in its rules to avoid
confusion with the Board variances under Title IX of the Environmental
Protection Act. The equivalent Board procedures are an “adjusted
treatment standard from a treatment standard” pursuant to subsections (a)
through (l) of this Section, or a “treatability exception” adopted pursuant
to subsections (m) et seq. of this Section. While the latter is adopted by
“identical in substance” rulemaking following a USEPA action, the
former is an original Board action which will be the only mechanism
following authorization to the State of this component of the RCRA
program.
b)
Each petition must be submitted in accordance with the procedures in 35 Ill.
Adm. Code 106.Subpart G.
c)
Each petition must include the following statement signed by the petitioner or an
authorized representative:
I certify under penalty of law that I have personally examined and am
familiar with the information submitted in this petition and all attached
documents, and that, based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that the
submitted information is true, accurate and complete. I am aware that
there are significant penalties for submitting false information, including
the possibility of fine and imprisonment.
d)
After receiving a petition for an adjusted treatment standard, the Board may
request any additional information or samples which are necessary to evaluate
the petition.
e)
The Board will give public notice and provide an opportunity for public
comment, as provided in 35 Ill. Adm. Code 106. In conjunction with any
updating of the RCRA regulations, the Board will maintain, in this Part, a
listing of all adjusted treatment standards granted by the Board pursuant to this
Section. A LISTING OF ALL ADJUSTED STANDARDS GRANTED
PURSUANT TO THIS SECTION WILL BE PUBLISHED IN THE ILLINOIS
REGISTER AND ENVIRONMENTAL REGISTER AT THE END OF EACH
FISCAL YEAR. (Section 28.1(d)(3) of the Environmental Protection Act [415
ILCS 5/28.1(d)(3)].)
406
f)
A generator, treatment facility or disposal facility that is managing a waste
covered by an adjusted treatment standard shall comply with the waste analysis
requirements for restricted wastes found under Section 728.107.
g)
During the petition review process, the applicant is required to comply with all
restrictions on land disposal under this Part once the effective date for the waste
has been reached.
h)
Where the treatment standard is expressed as a concentration in a waste or waste
extract and a waste generated under conditions specific to only one site cannot
be treated to the specified level, or where treatment technology is not
appropriate to the waste, the generator or treatment facility may petition the
Board for a site-specific adjusted treatment standard. The petitioner shall
demonstrate that, because the physical or chemical properties of the waste
differs significantly from the waste analyzed in developing the treatment
standard, the waste cannot be treated to specified levels or by the specified
methods.
h)
Based on a petition filed by a generator or treater of hazardous waste, the Board
will grant an andjusted standard from an applicable treatment standard if the
petitioner can demonstrate that either of the following applies to treatment of the
waste:
1)
It is not physically possible to treat the waste to the level specified in the
treatment standard, or by the method specified as the treatment
standard. To show that this is the case, the petitioner must demonstrate
that because the physical or chemical properties of the waste differ
significantly from waste analyzed in developing the treatment standard,
the waste cannot be treated to the specified level or by the specified
method; or
2)
It is inappropriate to require the waste to be treated to the level specified
in the treatment standard or by the method specified as the treatment
standard, even though such treatment is technically possible. To show
that this is the case, the petitioner must demonstrate that either of the
following applies to treatment of the waste:
A)
Treatment to the specified level or by the specified method is
technically inappropriate (for example, resulting in combustion of
large amounts of mildly contaminated environmental media
where the treatment standard is not based on combustion of such
media); or
407
B)
For remediation waste only, treatment to the specified level or by
the specified method is environmentally inappropriate because it
would likely discourage aggressive remediation.
3)
For contaminated soil only, treatment to the level or by the method specified
in the soil treatment standards would result in concentrations of hazardous
constituents that are below (i.e., lower than) the concentrations necessary to
minimize short- and long-term threats to human health and the environment.
An adjusted standard from a treatment standard granted under this
subsection (h)(3) will include the following features:
A)
At a minimum, the adjusted standard from the treatment standard will
impose an alternative land disposal restriction treatment standard that
will achieve the following, using a reasonable maximum exposure
scenario:
i)
For carcinogens, it will achieve constituent concentrations that
result in the total excess risk to an individual exposed over a
lifetime, generally falling within a range from 10
-4
to 10
-6
; and
ii)
For constituents with non-carcinogenic effects, it will achieve
constituent concentrations that an individual could be exposed
to on a daily basis without appreciable risk of deleterious
effect during a lifetime.
B)
The treatment adjusted standard will not consider post-land-disposal
controls.
4)
For contaminated soil only, treatment to the level or by the method specified
in the soil treatment standards would result in concentrations of hazardous
constituents that are below (i.e., lower than) natural background
concentrations at the site where the contaminated soil will land disposed.
5)
The Board will follow the procedures of Section 28.1 of the Act and 35
Ill. Adm. Code 106 pertaining to public notice and a reasonable
opportunity for public comment before granting or denying a petition.
i)
Each petition for a site-specific adjusted treatment standard must include the
information in 35 Ill. Adm. Code 720.120(b)(1) through (b)(4).
j)
After receiving a petition for a site-specific adjusted treatment standard, the
Board may request any additional information or samples which the Board
determines are necessary to evaluate the petition.
k)
A generator, treatment facility or disposal facility which is managing a waste
covered by a site-specific adjusted treatment standard shall comply with the
waste analysis requirements for restricted wastes in Section 728.107.
408
l)
During the petition review process, the petitioner for a site-specific adjusted
treatment standard shall comply with all restrictions on land disposal under this
Part once the effective date for the waste has been reached.
m)
If USEPA grants a treatability exception by regulatory action pursuant to 40
CFR 268.44 (1996) and a person demonstrates that the treatability exception
needs to be adopted as part of the Illinois RCRA program because the waste is
generated or managed in Illinois, the Board will adopt the treatability exception
by identical in substance rulemaking pursuant to Section 22.4(a) of the
Environmental Protection Act.
BOARD NOTE: The Board will adopt the treatability exception during a
RCRA update Docket if a timely demonstration is made. Otherwise, the Board
will assign the matter to a separate Docket. This subsection (m) is not derived
directly from a federal regulation. Corresponding 40 CFR 264.1030(m) is
marked “reserved” by USEPA.
m)
For any adjusted standard from a treatment standard, the petitioner must also
demonstrate that compliance with the requested adjusted standard is sufficient to
minimize threats to human health and the environment posed by land disposal of
the waste. In evaluating this demonstration, the Board will take into account
whether the adjusted standard should be granted if the subject waste is to be
used in a manner constituting disposal pursuant to Sections 728.120 through
728.123.
n)
This subsection (n) corresponds with 40 CFR 264.1030(n), marked “reserved”
by USEPA. This statement maintains structural consistency with USEPA rules.
o)
The facilities listed in Section 728.Table H of this Part are excluded from the
treatment standards under Sections 728.143(a) and 728.Table B of this Part, and
are subject to the constituent concentrations listed in Section 728.Table H of this
Part.
p)
This subsection (p) corresponds with 40 CFR 264.1030(p), which is a site-
specific regulation that applies to a facility outside Illinois. This statement
maintains structural consistency with USEPA rules.
p)
If USEPA grants a treatability exception by regulatory action pursuant to 40
CFR 268.44 (1996) and a person demonstrates that the treatability exception
needs to be adopted as part of the Illinois RCRA program because the waste is
generated or managed in Illinois, the Board will adopt the treatability exception
by identical in substance rulemaking pursuant to Section 22.4(a) of the
Environmental Protection Act.
409
BOARD NOTE: The Board will adopt the treatability exception during a
RCRA update Docket if a timely demonstration is made. Otherwise, the Board
will assign the matter to a separate Docket.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.145
Treatment Standards for Hazardous Debris
a)
Treatment standards. Hazardous debris must be treated prior to land disposal as
follows, unless the Board has determined, under 35 Ill. Adm. Code
721.103(d)(f)(2), that the debris is no longer contaminated with hazardous waste or
the debris is treated to the waste-specific treatment standard provided in this Subpart
for the waste contaminating the debris:
1)
General. Hazardous debris must be treated for each “contaminant subject to
treatment”, defined by subsection (b) below of this Section, using the
technology or technologies identified in Section 728.Table F of this Part.
2)
Characteristic debris. Hazardous debris that exhibits the characteristic of
ignitability, corrosivity, or reactivity identified under 35 Ill. Adm. Code
721.121, 721.122, or 721.123, respectively, must be deactivated by
treatment using one of the technologies identified in Section 728.Table F of
this Part.
3)
Mixtures of debris types. The treatment standards of Section 728.Table F
of this Part must be achieved for each type of debris contained in a mixture
of debris types. If an immobilization technology is used in a treatment train,
it must be the last treatment technology used.
4)
Mixtures of contaminant types. Debris that is contaminated with two or
more contaminants subject to treatment identified under subsection (b)
below of this Section must be treated for each contaminant using one or
more treatment technologies identified in Section 728.Table F of this Part.
If an immobilization technology is used in a treatment train, it must be the
last treatment technology used.
5)
Waste PCBs. Hazardous debris that is also a waste PCB under 40 CFR 761
is subject to the requirements of either 40 CFR 761 or the requirements of
this Section, whichever are more stringent.
b)
Contaminants subject to treatment. Hazardous debris must be treated for each
“contaminant subject to treatment”. The contaminants subject to treatment must be
determined as follows:
410
1)
Toxicity characteristic debris. The contaminants subject to treatment for
debris that exhibits the Toxicity Characteristic (TC) by 35 Ill. Adm. Code
721.124 are those EP constituents for which the debris exhibits the TC
toxicity characteristic.
2)
Debris contaminated with listed waste. The contaminants subject to
treatment for debris that is contaminated with a prohibited listed hazardous
waste are those constituents or wastes for which treatment standards are
established for the waste under Sections Section 728.140 and 728.Table T of
this Part.
3)
Cyanide reactive debris. Hazardous debris that is reactive because of
cyanide must be treated for cyanide.
c)
Conditioned exclusion of treated debris. Hazardous debris that has been treated
using one of the specified extraction or destruction technologies in Section
728.Table F of this Part and that does not exhibit a characteristic of hazardous
waste identified under 35 Ill. Adm. Code 721.Subpart C after treatment is not a
hazardous waste and need not be managed in a subtitle C facility. Hazardous debris
contaminated with a listed waste that is treated by an immobilization technology
specified in Section 728.Table F of this Part is a hazardous waste and must be
managed in a RCRA Subtitle C treatment, storage, or disposal facility.
d)
Treatment residuals
1)
General requirements. Except as provided by subsections (d)(2) and (d)(4)
below of this Section:
A)
Residue from the treatment of hazardous debris must be separated
from the treated debris using simple physical or mechanical means;
and
B)
Residue from the treatment of hazardous debris is subject to the
waste-specific treatment standards provided by 728.Subpart D of
this Part for the waste contaminating the debris.
2)
Nontoxic debris. Residue from the deactivation of ignitable, corrosive, or
reactive characteristic hazardous debris (other than cyanide-reactive) that is
not contaminated with a contaminant subject to treatment defined by
subsection (b) above of this Section, must be deactivated prior to land
disposal and is not subject to the waste-specific treatment standards of
728.Subpart D of this Part.
3)
Cyanide-reactive debris. Residue from the treatment of debris that is
reactive because of cyanide must meet the standards for U.S. EPA USEPA
411
hazardous waste number D003 under Section 728.143 728.140 and Table T
of this Part.
4)
Ignitable nonwastewater residue. Ignitable nonwastewater residue
containing equal to or greater than 10% percent total organic carbon is
subject to the technology-based specified in the treatment standards for U.S.
EPA USEPA hazardous waste number D001: “Ignitable Liquids based on
35 Ill. Adm. Code 721.121(a)(1)”, under Section 728.142.
5)
Residue from spalling. Layers of debris removed by spalling are hazardous
debris that remain subject to the treatment standards of this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.149
Alternative LDR Treatment Standards for Contaminated Soil
a)
Applicability. An owner or operator shall comply with LDRs prior to placing soil that
exhibits a characteristic of hazardous waste or which exhibited a characteristic of
hazardous waste at the time it was generated into a land disposal unit. The following
chart describes whether an owner or operator must comply with LDRs prior to
placing soil contaminated by listed hazardous waste into a land disposal unit:
If the LDRs
And if the LDRs
And if
Then the owner or
operator
Applied to the
listed waste when
it contaminated the
soil*.
Apply to the listed
waste now.
—
Must comply with
LDRs.
Did not apply to the
listed waste when
it contaminated the
soil*.
Apply to the listed
waste now.
The soil is deter-
mined to contain
the listed waste
when the soil is
first generated.
Must comply with
LDRs.
Did not apply to the
listed waste when
it contaminated the
soil*.
Apply to the listed
waste now.
The soil is deter-
mined to contain
the listed waste
when the soil is
first generated.
Needs not comply
with LDRs.
Did not apply to the
listed waste when
it contaminated the
soil*.
Do not apply to the
listed waste now.
—
Needs not comply
with LDRs.
* For dates of LDR applicability, see Appendix G of this Part. To determine the date
any given listed hazardous waste contaminated any given volume of soil, use the
last date any given listed hazardous waste was placed into any given land disposal
unit or, in the case of an accidental spill, the date of the spill.
b)
Prior to land disposal, contaminated soil identified by subsection (a) of this Section as
needing to comply with LDRs must be treated according to the applicable treatment
412
standards specified in subsection (c) of this Section or according to the universal
treatment standards specified in Section 728.148 and Table U of this Part applicable
to the contaminating listed hazardous waste or the applicable characteristic of
hazardous waste if the soil is characteristic. The treatment standards specified in
subsection (c) of this Section and the universal treatment standards may be modified
through a treatment variance approved in accordance with Section 728.144.
c)
Treatment standards for contaminated soils. Prior to land disposal, contaminated soil
identified by subsection (a) of this Section as needing to comply with LDRs must be
treated according to all the standards specified in this subsection or according to the
universal treatment standards specified in Section 728.148 and Table U of this Part.
1)
All soils. Prior to land disposal, all constituents subject to treatment must be
treated as follows:
A)
For non-metals, treatment must achieve 90 percent reduction in total
constituent concentrations, except as provided by subsection
(c)(1)(C) of this Section.
B)
For metals, treatment must achieve 90 percent reduction in
constituent concentrations as measured in leachate from the treated
media (tested according to the TCLP) or 90 percent reduction in total
constituent concentrations (when a metal removal treatment
technology is used), except as provided by subsection (c)(1)(C) of
this Section.
C)
When treatment of any constituent subject to treatment to a 90
percent reduction standard would result in a concentration less than
10 times the universal treatment standard for that constituent,
treatment to achieve constituent concentrations less than 10 times the
universal treatment standard is not required. The universal treatment
standards are identified in Table U of this Part.
2)
Soils that exhibit the characteristic of ignitability, corrosivity or reactivity. In
addition to the treatment required by subsection (c)(1) of this Section, prior to
land disposal, soils that exhibit the characteristic of ignitability, corrosivity, or
reactivity must be treated to eliminate these characteristics.
3)
Soils that contain nonanalyzable constituents. In addition to the treatment
requirements of subsections (c)(1) and (c)(2) of this Section, prior to land
disposal, the following treatment is required for soils that contain
nonanalyzable constituents:
A)
For soil that also contains analyzable constituents, treatment of those
analyzable constituents to the levels specified in subsections (c)(1)
and (c)(2) of this Section; or
B)
For soil that contains only nonanalyzable constituents, treatment by
the method specified in Section 728.142 for the waste contained in
the soil.
413
d)
Constituents subject to treatment. When applying the soil treatment standards in
subsection (c) of this Section, constituents subject to treatment are any constituents
listed in Table U of this Part universal treatment standards that are reasonably
expected to be present in any given volume of contaminated soil, except fluoride,
selenium, sulfides, vanadium and zinc, and are present at concentrations greater
than ten times the universal treatment standard.
e)
Management of treatment residuals. Treatment residuals from treating contaminated
soil identified by subsection (a) of this Section as needing to comply with LDRs must
be managed as follows:
1)
Soil residuals are subject to the treatment standards of this Section;
2)
Non-soil residuals are subject to the following requirements:
A)
For soils contaminated by listed hazardous waste, the RCRA Subtitle
C standards applicable to the listed hazardous waste; and
B)
For soils that exhibit a characteristic of hazardous waste, if the non-
soil residual also exhibits a characteristic of hazardous waste, the
treatment standards applicable to the characteristic hazardous waste.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix G
Federal Effective Dates
The following are the effective dates for the USEPA rules in 40 CFR 268. These generally became
effective as Illinois rules at a later date.
TABLE 1
EFFECTIVE DATES OF SURFACE DISPOSED WASTES (NON-SOIL AND
DEBRIS) REGULATED IN THE LDRS
a
—COMPREHENSIVE LIST
Waste code
Waste category
Effective date
D001
c
All (except High TOC Ignitable Liquids)
Aug. 9, 1993.
D001
High TOC Ignitable Liquids
Aug. 8, 1990.
D002
c
All
Aug. 9, 1993.
D003
e
All
July 8, 1996.
D003
e
Newly identified surface-disposed elemental
phosphorus processing wastes
May 26, 2000.
D004
Nonwastewater
May 8, 1992.
D004
Newly identified D004 and mineral processing
wastes
Aug. 24, 1998.
D004
Wastewater
Aug. 8, 1992.
D004
Mixed radioactive/newly identified D004 or
mineral processing wastes
May 26, 2000.
D005
All
Aug. 8, 1990.
414
D005
Newly identified D005 and mineral processing
wastes
Aug. 24, 1998.
D005
Mixed radioactive/newly identified D005 or
mineral processing wastes
May 26, 2000.
D006
All
Aug. 8, 1990.
D006
Newly identified D006 and mineral processing
wastes
Aug. 24, 1998.
D006
Mixed radioactive/newly identified D006 or
mineral processing wastes
May 26, 2000.
D007
All
Aug. 8, 1990.
D007
Newly identified D007 and mineral processing
wastes
Aug. 24, 1998.
D007
Mixed radioactive/newly identified D007or mineral
processing wastes
May 26, 2000.
D008
Lead materials before secondary smelting
May 8, 1992.
D008
Newly identified D008 and mineral processing
waste
Aug. 24, 1998.
D008
All others
Aug. 8, 1990.
D008
Mixed radioactive/newly identified D008 or
mineral processing wastes
May 26, 2000.
D009
Nonwastewater
May 8, 1992.
D009
Newly identified D009 and mineral processing
waste
Aug. 24, 1998.
D009
All others
Aug. 8, 1990.
D009
Mixed radioactive/newly identified D009or mineral
processing wastes
May 26, 2000.
D010
All
Aug. 8, 1990.
D010
Newly identified D010 and mineral processing
wastes
Aug. 24, 1998.
D010
Mixed radioactive/newly identified D010 or
mineral processing wastes
May 26, 2000.
D011
All
Aug. 8, 1990.
D011
Newly identified D011 and mineral processing
wastes
Aug. 24, 1998.
D011
Mixed radioactive/newly identified D011or mineral
processing wastes
May 26, 2000.
D012 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
D013 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
D014 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
D015 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
415
D016 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
D017 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Dec. 14, 1994.
D018
Mixed with radioactive wastes
Sep. 19, 1996.
D018
All others
Dec. 19, 1994.
D019
Mixed with radioactive wastes
Sep. 19, 1996.
D019
All others
Dec. 19, 1994.
D020
Mixed with radioactive wastes
Sep. 19, 1996.
D020
All others
Dec. 19, 1994.
D021
Mixed with radioactive wastes
Sep. 19, 1996.
D021
All others
Dec. 19, 1994.
D022
Mixed with radioactive wastes
Sep. 19, 1996.
D022
All others
Dec. 19, 1994.
D023
Mixed with radioactive wastes
Sep. 19, 1996.
D023
All others
Dec. 19, 1994.
D024
Mixed with radioactive wastes
Sep. 19, 1996.
D024
All others
Dec. 19, 1994.
D025
Mixed with radioactive wastes
Sep. 19, 1996.
D025
All others
Dec. 19, 1994.
D026
Mixed with radioactive wastes
Sep. 19, 1996.
D026
All others
Dec. 19, 1994.
D027
Mixed with radioactive wastes
Sep. 19, 1996.
D027
All others
Dec. 19, 1994.
D028
Mixed with radioactive wastes
Sep. 19, 1996.
D028
All others
Dec. 19, 1994.
D029
Mixed with radioactive wastes
Sep. 19, 1996.
D029
All others
Dec. 19, 1994.
D030
Mixed with radioactive wastes
Sep. 19, 1996.
D030
All others
Dec. 19, 1994.
D031
Mixed with radioactive wastes
Sep. 19, 1996.
D031
All others
Dec. 19, 1994.
D032
Mixed with radioactive wastes
Sep. 19, 1996.
D032
All others
Dec. 19, 1994.
D033
Mixed with radioactive wastes
Sep. 19, 1996.
D033
All others
Dec. 19, 1994.
D034
Mixed with radioactive wastes
Sep. 19, 1996.
D034
All others
Dec. 19, 1994.
D035
Mixed with radioactive wastes
Sep. 19, 1996.
D035
All others
Dec. 19, 1994.
D036
Mixed with radioactive wastes
Sep. 19, 1996.
D036
All others
Dec. 19, 1994.
D037
Mixed with radioactive wastes
Sep. 19, 1996.
416
D037
All others
Dec. 19, 1994.
D038
Mixed with radioactive wastes
Sep. 19, 1996.
D038
All others
Dec. 19, 1994.
D039
Mixed with radioactive wastes
Sep. 19, 1996.
D039
All others
Dec. 19, 1994.
D040
Mixed with radioactive wastes
Sep. 19, 1996.
D040
All others
Dec. 19, 1994.
D041
Mixed with radioactive wastes
Sep. 19, 1996.
D041
All others
Dec. 19, 1994.
D042
Mixed with radioactive wastes
Sep. 19, 1996.
D042
All others
Dec. 19, 1994.
D043
Mixed with radioactive wastes
Sep. 19, 1996.
D043
All others
Dec. 19, 1994.
F001
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F001
All others
Nov. 8, 1986.
F002 (1,1,2-trichloroethane)
Wastewater and Nonwastewater
Aug. 8, 1990.
F002
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F002
All others
Nov. 8, 1986.
F003
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F003
All others
Nov. 8, 1986.
F004
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F004
All others
Nov. 8, 1986.
F005 (benzene, 2-ethoxy
ethanol, 2-nitropropane)
Wastewater and Nonwastewater
Aug. 8, 1990.
F005
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F005
All others
Nov. 8, 1986.
F006
Wastewater
Aug. 8, 1990.
F006
Nonwastewater
Aug. 8, 1988.
F006 (cyanides)
Nonwastewater
July 8, 1989.
F007
All
July 8, 1989.
417
F008
All
July 8, 1989.
F009
All
July 8, 1989.
F010
All
June 8, 1989.
F011 (cyanides)
Nonwastewater
Dec. 8, 1989.
F011
All others
July 8, 1989.
F012 (cyanides)
Nonwastewater
Dec. 8, 1989.
F012
All others
July 8, 1989.
F019
All
Aug. 8, 1990.
F020
All
Nov. 8, 1988.
F021
All
Nov. 8, 1988.
F025
All
Aug. 8, 1990.
F026
All
Nov. 8, 1988.
F027
All
Nov. 8, 1988.
F028
All
Nov. 8, 1988.
F032
Mixed with radioactive wastes
May 12, 1999.
F032
All others
May Aug. 12,
1997.
F033
Mixed with radioactive wastes
May 12, 1999.
F033
All others
May 12, 1997.
F034
Mixed with radioactive wastes
May 12, 1999.
F034
All others
May Aug. 12,
1997.
F035
Mixed with radioactive wastes
May 12, 1999.
F035
All others
Aug. 12, 1997.
F037
Not generated from surface impoundment
cleanouts or closures
June 30, 1993.
F037
Generated from surface impoundment
cleanouts or closures
June 30, 1994.
F037
Mixed with radioactive wastes
June 30, 1994.
F038
Not generated from surface impoundment
cleanouts or closures
June 30, 1993.
F038
Generated from surface impoundment
cleanouts or closures
June 30, 1994.
F038
Mixed with radioactive wastes
June 30, 1994.
F039
Wastewater
Aug. 8, 1990.
F039
Nonwastewater
May 8, 1992.
K001 (organics)
b
All
Aug. 8, 1988.
K001
All others
Aug. 8, 1988.
K002
All
Aug. 8, 1990.
K003
All
Aug. 8, 1990.
418
K004
Wastewater
Aug. 8, 1990.
K004
Nonwastewater
Aug. 8, 1988.
K005
Wastewater
Aug. 8, 1990.
K005
Nonwastewater
June 8, 1989.
K006
All
Aug. 8, 1990.
K007
Wastewater
Aug. 8, 1990.
K007
Nonwastewater
June 8, 1989.
K008
Wastewater
Aug. 8, 1990.
K008
Nonwastewater
Aug. 8, 1988.
K009
All
June 8, 1989.
K010
All
June 8, 1989.
K011
Wastewater
Aug. 8, 1990.
K011
Nonwastewater
June 8, 1989.
K013
Wastewater
Aug. 8, 1990.
K013
Nonwastewater
June 8, 1989.
K014
Wastewater
Aug. 8, 1990.
K014
Nonwastewater
June 8, 1989.
K015
Wastewater
Aug. 8, 1988.
K015
Nonwastewater
Aug. 8, 1990.
K016
All
Aug. 8, 1988.
K017
All
Aug. 8, 1990.
K018
All
Aug. 8, 1988.
K019
All
Aug. 8, 1988.
K020
All
Aug. 8, 1988.
K021
Wastewater
Aug. 8, 1990.
K021
Nonwastewater
Aug. 8, 1988.
K022
Wastewater
Aug. 8, 1990.
K022
Nonwastewater
Aug. 8, 1988.
K023
All
June 8, 1989.
K024
All
Aug. 8, 1988.
K025
Wastewater
Aug. 8, 1990.
K025
Nonwastewater
Aug. 8, 1988.
K026
All
Aug. 8, 1990.
K027
All
June 8, 1989.
K028 (metals)
Nonwastewater
Aug. 8, 1990.
K028
All others
June 8, 1989.
K029
Wastewater
Aug. 8, 1990.
K029
Nonwastewater
June 8, 1989.
K030
All
Aug. 8, 1988.
K031
Wastewater
Aug. 8, 1990.
K031
Nonwastewater
May 8, 1992.
K032
All
Aug. 8, 1990.
K033
All
Aug. 8, 1990.
K034
All
Aug. 8, 1990.
K035
All
Aug. 8, 1990.
419
K036
Wastewater
June 8, 1989.
K036
Nonwastewater
Aug. 8, 1988.
K037
b
Wastewater
Aug. 8, 1988.
K037
Nonwastewater
Aug. 8, 1988.
K038
All
June 8, 1989.
K039
All
June 8, 1989.
K040
All
June 8, 1989.
K041
All
Aug. 8, 1990.
K042
All
Aug. 8, 1990.
K043
All
June 8, 1989.
K044
All
Aug. 8, 1988.
K045
All
Aug. 8, 1988.
K046 (Nonreactive)
Nonwastewater
Aug. 8, 1988.
K046
All others
Aug. 8, 1990.
K047
All
Aug. 8, 1988.
K048
Wastewater
Aug. 8, 1990.
K048
Nonwastewater
Nov. 8, 1990.
K049
Wastewater
Aug. 8, 1990.
K049
Nonwastewater
Nov. 8, 1990.
K050
Wastewater
Aug. 8, 1990.
K050
Nonwastewater
Nov. 8, 1990.
K051
Wastewater
Aug. 8, 1990.
K051
Nonwastewater
Nov. 8, 1990.
K052
Wastewater
Aug. 8, 1990.
K052
Nonwastewater
Nov. 8, 1990.
K060
Wastewater
Aug. 8, 1990.
K060
Nonwastewater
Aug. 8, 1988.
K061
Wastewater
Aug. 8, 1990.
K061
Nonwastewater
June 30, 1992.
K062
All
Aug. 8, 1988.
K069 (Non-Calcium Sulfate) Nonwastewater
Aug. 8, 1988.
K069
All others
Aug. 8, 1990.
K071
All
Aug. 8, 1990.
K073
All
Aug. 8, 1990.
K083
All
Aug. 8, 1990.
K084
Wastewater
Aug. 8, 1990.
K084
Nonwastewater
May 8, 1992.
K085
All
Aug. 8, 1990.
K086 (organics)
b
All
Aug. 8, 1988.
K086
All others
Aug. 8, 1988.
K087
All
Aug. 8, 1988.
K088
Mixed with radioactive wastes
Apr. 8, 1998.
K088
All others
Jan. Oct. 8,
1997.
K093
All
June 8, 1989.
420
K094
All
June 8, 1989.
K095
Wastewater
Aug. 8, 1990.
K095
Nonwastewater
June 8, 1989.
K096
Wastewater
Aug. 8, 1990.
K096
Nonwastewater
June 8, 1989.
K097
All
Aug. 8, 1990.
K098
All
Aug. 8, 1990.
K099
All
Aug. 8, 1988.
K100
Wastewater
Aug. 8, 1990.
K100
Nonwastewater
Aug. 8, 1988.
K101 (organics)
Wastewater
Aug. 8, 1988.
K101 (metals)
Wastewater
Aug. 8, 1990.
K101 (organics)
Nonwastewater
Aug. 8, 1988.
K101 (metals)
Nonwastewater
May 8, 1992.
K102 (organics)
Wastewater
Aug. 8, 1988.
K102 (metals)
Wastewater
Aug. 8, 1990.
K102 (organics)
Nonwastewater
Aug. 8, 1988.
K102 (metals)
Nonwastewater
May 8, 1992.
K103
All
Aug. 8, 1988.
K104
All
Aug. 8, 1988.
K105
All
Aug. 8, 1990.
K106
Wastewater
Aug. 8, 1990.
K106
Nonwastewater
May 8, 1992.
K107
Mixed with radioactive wastes
June 30, 1994.
K107
All others
Nov. 9, 1992.
K108
Mixed with radioactive wastes
June 30, 1994.
K108
All others
Nov. 9, 1992.
K109
Mixed with radioactive wastes
June 30, 1994.
K109
All others
Nov. 9, 1992.
K110
Mixed with radioactive wastes
June 30, 1994.
K110
All others
Nov. 9, 1992.
K111
Mixed with radioactive wastes
June 30, 1994.
K111
All others
Nov. 9, 1992.
K112
Mixed with radioactive wastes
June 30, 1994.
K112
All others
Nov. 9, 1992.
K113
All
June 8, 1989.
K114
All
June 8, 1989.
K115
All
June 8, 1989.
K116
All
June 8, 1989.
K117
Mixed with radioactive wastes
June 30, 1994.
K117
All others
Nov. 9, 1992.
K118
Mixed with radioactive wastes
June 30, 1994.
K118
All others
Nov. 9, 1992.
K123
Mixed with radioactive wastes
June 30, 1994.
K123
All others
Nov. 9, 1992.
421
K124
Mixed with radioactive wastes
June 30, 1994.
K124
All others
Nov. 9, 1992.
K125
Mixed with radioactive wastes
June 30, 1994.
K125
All others
Nov. 9, 1992.
K126
Mixed with radioactive wastes
June 30, 1994.
K126
All others
Nov. 9, 1992.
K131
Mixed with radioactive wastes
June 30, 1994.
K131
All others
Nov. 9, 1992.
K132
Mixed with radioactive wastes
June 30, 1994.
K132
All others
Nov. 9, 1992.
K136
Mixed with radioactive wastes
June 30, 1994.
K136
All others
Nov. 9, 1992.
K141
Mixed with radioactive wastes
Sep. 19, 1996.
K141
All others
Dec. 19, 1994.
K142
Mixed with radioactive wastes
Sep. 19, 1996.
K142
All others
Dec. 19, 1994.
K143
Mixed with radioactive wastes
Sep. 19, 1996.
K143
All others
Dec. 19, 1994.
K144
Mixed with radioactive wastes
Sep. 19, 1996.
K144
All others
Dec. 19, 1994.
K145
Mixed with radioactive wastes
Sep. 19, 1996.
K145
All others
Dec. 19, 1994.
K147
Mixed with radioactive wastes
Sep. 19, 1996.
K147
All others
Dec. 19, 1994.
K148
Mixed with radioactive wastes
Sep. 19, 1996.
K148
All others
Dec. 19, 1994.
K149
Mixed with radioactive wastes
Sep. 19, 1996.
K149
All others
Dec. 19, 1994.
K150
Mixed with radioactive wastes
Sep. 19, 1996.
K150
All others
Dec. 19, 1994.
K151
Mixed with radioactive wastes
Sep. 19, 1996.
K151
All others
Dec. 19, 1994.
K156
Mixed with radioactive wastes
Apr. 8, 1998.
K156
All others
July 8, 1996.
K157
Mixed with radioactive wastes
Apr. 8, 1998.
K157
All others
July 8, 1996.
K158
Mixed with radioactive wastes
Apr. 8, 1998.
K158
All others
July 8, 1996.
K159
Mixed with radioactive wastes
Apr. 8, 1998.
K159
All others
July 8, 1996.
K160
Mixed with radioactive wastes
Apr. 8, 1998.
K160
All others
July 8, 1996.
K161
Mixed with radioactive wastes
Apr. 8, 1998.
K161
All others
July 8, 1996.
P001
All
Aug. 8, 1990.
422
P002
All
Aug. 8, 1990.
P003
All
Aug. 8, 1990.
P004
All
Aug. 8, 1990.
P005
All
Aug. 8, 1990.
P006
All
Aug. 8, 1990.
P007
All
Aug. 8, 1990.
P008
All
Aug. 8, 1990.
P009
All
Aug. 8, 1990.
P010
Wastewater
Aug. 8, 1990.
P010
Nonwastewater
May 8, 1992.
P011
Wastewater
Aug. 8, 1990.
P011
Nonwastewater
May 8, 1992.
P012
Wastewater
Aug. 8, 1990.
P012
Nonwastewater
May 8, 1992.
P013 (barium)
Nonwastewater
Aug. 8, 1990.
P013
All others
June 8, 1989.
P014
All
Aug. 8, 1990.
P015
All
Aug. 8, 1990.
P016
All
Aug. 8, 1990.
P017
All
Aug. 8, 1990.
P018
All
Aug. 8, 1990.
P020
All
Aug. 8, 1990.
P021
All
June 8, 1989.
P022
All
Aug. 8, 1990.
P023
All
Aug. 8, 1990.
P024
All
Aug. 8, 1990.
P026
All
Aug. 8, 1990.
P027
All
Aug. 8, 1990.
P028
All
Aug. 8, 1990.
P029
All
June 8, 1989.
P030
All
June 8, 1989.
P031
All
Aug. 8, 1990.
P033
All
Aug. 8, 1990.
P034
All
Aug. 8, 1990.
P036
Wastewater
Aug. 8, 1990.
P036
Nonwastewater
May 8, 1992.
P037
All
Aug. 8, 1990.
P038
Wastewater
Aug. 8, 1990.
P038
Nonwastewater
May 8, 1992.
P039
All
June 8, 1989.
P040
All
June 8, 1989.
P041
All
June 8, 1989.
P042
All
Aug. 8, 1990.
P043
All
June 8, 1989.
P044
All
June 8, 1989.
423
P045
All
Aug. 8, 1990.
P046
All
Aug. 8, 1990.
P047
All
Aug. 8, 1990.
P048
All
Aug. 8, 1990.
P049
All
Aug. 8, 1990.
P050
All
Aug. 8, 1990.
P051
All
Aug. 8, 1990.
P054
All
Aug. 8, 1990.
P056
All
Aug. 8, 1990.
P057
All
Aug. 8, 1990.
P058
All
Aug. 8, 1990.
P059
All
Aug. 8, 1990.
P060
All
Aug. 8, 1990.
P062
All
June 8, 1989.
P063
All
June 8, 1989.
P064
All
Aug. 8, 1990.
P065
Wastewater
Aug. 8, 1990.
P065
Nonwastewater
May 8, 1992.
P066
All
Aug. 8, 1990.
P067
All
Aug. 8, 1990.
P068
All
Aug. 8, 1990.
P069
All
Aug. 8, 1990.
P070
All
Aug. 8, 1990.
P071
All
June 8, 1989.
P072
All
Aug. 8, 1990.
P073
All
Aug. 8, 1990.
P074
All
June 8, 1989.
P075
All
Aug. 8, 1990.
P076
All
Aug. 8, 1990.
P077
All
Aug. 8, 1990.
P078
All
Aug. 8, 1990.
P081
All
Aug. 8, 1990.
P082
All
Aug. 8, 1990.
P084
All
Aug. 8, 1990.
P085
All
June 8, 1989.
P087
All
May 8, 1992.
P088
All
Aug. 8, 1990.
P089
All
June 8, 1989.
P092
Wastewater
Aug. 8, 1990.
P092
Nonwastewater
May 8, 1992.
P093
All
Aug. 8, 1990.
P094
All
June 8, 1989.
P095
All
Aug. 8, 1990.
P096
All
Aug. 8, 1990.
P097
All
June 8, 1989.
424
P098
All
June 8, 1989.
P099 (silver)
Wastewater
Aug. 8, 1990.
P099
All others
June 8, 1989.
P101
All
Aug. 8, 1990.
P102
All
Aug. 8, 1990.
P103
All
Aug. 8, 1990.
P104 (silver)
Wastewater
Aug. 8, 1990.
P104
All others
June 8, 1989.
P105
All
Aug. 8, 1990.
P106
All
June 8, 1989.
P108
All
Aug. 8, 1990.
P109
All
June 8, 1989.
P110
All
Aug. 8, 1990.
P111
All
June 8, 1989.
P112
All
Aug. 8, 1990.
P113
All
Aug. 8, 1990.
P114
All
Aug. 8, 1990.
P115
All
Aug. 8, 1990.
P116
All
Aug. 8, 1990.
P118
All
Aug. 8, 1990.
P119
All
Aug. 8, 1990.
P120
All
Aug. 8, 1990.
P121
All
June 8, 1989.
P122
All
Aug. 8, 1990.
P123
All
Aug. 8, 1990.
P127
Mixed with radioactive wastes
Apr. 8, 1998.
P127
All others
July 8, 1996.
P128
Mixed with radioactive wastes
Apr. 8, 1998.
P128
All others
July 8, 1996.
P185
Mixed with radioactive wastes
Apr. 8, 1998.
P185
All others
July 8, 1996.
P188
Mixed with radioactive wastes
Apr. 8, 1998.
P188
All others
July 8, 1996.
P189
Mixed with radioactive wastes
Apr. 8, 1998.
P189
All others
July 8, 1996.
P190
Mixed with radioactive wastes
Apr. 8, 1998.
P190
All others
July 8, 1996.
P191
Mixed with radioactive wastes
Apr. 8, 1998.
P191
All others
July 8, 1996.
P192
Mixed with radioactive wastes
Apr. 8, 1998.
P192
All others
July 8, 1996.
P194
Mixed with radioactive wastes
Apr. 8, 1998.
P194
All others
July 8, 1996.
P196
Mixed with radioactive wastes
Apr. 8, 1998.
P196
All others
July 8, 1996.
425
P197
Mixed with radioactive wastes
Apr. 8, 1998.
P197
All others
July 8, 1996.
P198
Mixed with radioactive wastes
Apr. 8, 1998.
P198
All others
July 8, 1996.
P199
Mixed with radioactive wastes
Apr. 8, 1998.
P199
All others
July 8, 1996.
P201
Mixed with radioactive wastes
Apr. 8, 1998.
P201
All others
July 8, 1996.
P202
Mixed with radioactive wastes
Apr. 8, 1998.
P202
All others
July 8, 1996.
P203
Mixed with radioactive wastes
Apr. 8, 1998.
P203
All others
July 8, 1996.
P204
Mixed with radioactive wastes
Apr. 8, 1998.
P204
All others
July 8, 1996.
P205
Mixed with radioactive wastes
Apr. 8, 1998.
P205
All others
July 8, 1996.
U001
All
Aug. 8, 1990.
U002
All
Aug. 8, 1990.
U003
All
Aug. 8, 1990.
U004
All
Aug. 8, 1990.
U005
All
Aug. 8, 1990.
U006
All
Aug. 8, 1990.
U007
All
Aug. 8, 1990.
U008
All
Aug. 8, 1990.
U009
All
Aug. 8, 1990.
U010
All
Aug. 8, 1990.
U011
All
Aug. 8, 1990.
U012
All
Aug. 8, 1990.
U014
All
Aug. 8, 1990.
U015
All
Aug. 8, 1990.
U016
All
Aug. 8, 1990.
U017
All
Aug. 8, 1990.
U018
All
Aug. 8, 1990.
U019
All
Aug. 8, 1990.
U020
All
Aug. 8, 1990.
U021
All
Aug. 8, 1990.
U022
All
Aug. 8, 1990.
U023
All
Aug. 8, 1990.
U024
All
Aug. 8, 1990.
U025
All
Aug. 8, 1990.
U026
All
Aug. 8, 1990.
U027
All
Aug. 8, 1990.
U028
All
June 8, 1989.
U029
All
Aug. 8, 1990.
U030
All
Aug. 8, 1990.
426
U031
All
Aug. 8, 1990.
U032
All
Aug. 8, 1990.
U033
All
Aug. 8, 1990.
U034
All
Aug. 8, 1990.
U035
All
Aug. 8, 1990.
U036
All
Aug. 8, 1990.
U037
All
Aug. 8, 1990.
U038
All
Aug. 8, 1990.
U039
All
Aug. 8, 1990.
U041
All
Aug. 8, 1990.
U042
All
Aug. 8, 1990.
U043
All
Aug. 8, 1990.
U044
All
Aug. 8, 1990.
U045
All
Aug. 8, 1990.
U046
All
Aug. 8, 1990.
U047
All
Aug. 8, 1990.
U048
All
Aug. 8, 1990.
U049
All
Aug. 8, 1990.
U050
All
Aug. 8, 1990.
U051
All
Aug. 8, 1990.
U052
All
Aug. 8, 1990.
U053
All
Aug. 8, 1990.
U055
All
Aug. 8, 1990.
U056
All
Aug. 8, 1990.
U057
All
Aug. 8, 1990.
U058
All
June 8, 1989.
U059
All
Aug. 8, 1990.
U060
All
Aug. 8, 1990.
U061
All
Aug. 8, 1990.
U062
All
Aug. 8, 1990.
U063
All
Aug. 8, 1990.
U064
All
Aug. 8, 1990.
U066
All
Aug. 8, 1990.
U067
All
Aug. 8, 1990.
U068
All
Aug. 8, 1990.
U069
All
June 30, 1992.
U070
All
Aug. 8, 1990.
U071
All
Aug. 8, 1990.
U072
All
Aug. 8, 1990.
U073
All
Aug. 8, 1990.
U074
All
Aug. 8, 1990.
U075
All
Aug. 8, 1990.
U076
All
Aug. 8, 1990.
U077
All
Aug. 8, 1990.
U078
All
Aug. 8, 1990.
427
U079
All
Aug. 8, 1990.
U080
All
Aug. 8, 1990.
U081
All
Aug. 8, 1990.
U082
All
Aug. 8, 1990.
U083
All
Aug. 8, 1990.
U084
All
Aug. 8, 1990.
U085
All
Aug. 8, 1990.
U086
All
Aug. 8, 1990.
U087
All
June 8, 1989.
U088
All
June 8, 1989.
U089
All
Aug. 8, 1990.
U090
All
Aug. 8, 1990.
U091
All
Aug. 8, 1990.
U092
All
Aug. 8, 1990.
U093
All
Aug. 8, 1990.
U094
All
Aug. 8, 1990.
U095
All
Aug. 8, 1990.
U096
All
Aug. 8, 1990.
U097
All
Aug. 8, 1990.
U098
All
Aug. 8, 1990.
U099
All
Aug. 8, 1990.
U101
All
Aug. 8, 1990.
U102
All
June 8, 1989.
U103
All
Aug. 8, 1990.
U105
All
Aug. 8, 1990.
U106
All
Aug. 8, 1990.
U107
All
June 8, 1989.
U108
All
Aug. 8, 1990.
U109
All
Aug. 8, 1990.
U110
All
Aug. 8, 1990.
U111
All
Aug. 8, 1990.
U112
All
Aug. 8, 1990.
U113
All
Aug. 8, 1990.
U114
All
Aug. 8, 1990.
U115
All
Aug. 8, 1990.
U116
All
Aug. 8, 1990.
U117
All
Aug. 8, 1990.
U118
All
Aug. 8, 1990.
U119
All
Aug. 8, 1990.
U120
All
Aug. 8, 1990.
U121
All
Aug. 8, 1990.
U122
All
Aug. 8, 1990.
U123
All
Aug. 8, 1990.
U124
All
Aug. 8, 1990.
U125
All
Aug. 8, 1990.
428
U126
All
Aug. 8, 1990.
U127
All
Aug. 8, 1990.
U128
All
Aug. 8, 1990.
U129
All
Aug. 8, 1990.
U130
All
Aug. 8, 1990.
U131
All
Aug. 8, 1990.
U132
All
Aug. 8, 1990.
U133
All
Aug. 8, 1990.
U134
All
Aug. 8, 1990.
U135
All
Aug. 8, 1990.
U136
Wastewater
Aug. 8, 1990.
U136
Nonwastewater
May 8, 1992.
U137
All
Aug. 8, 1990.
U138
All
Aug. 8, 1990.
U140
All
Aug. 8, 1990.
U141
All
Aug. 8, 1990.
U142
All
Aug. 8, 1990.
U143
All
Aug. 8, 1990.
U144
All
Aug. 8, 1990.
U145
All
Aug. 8, 1990.
U146
All
Aug. 8, 1990.
U147
All
Aug. 8, 1990.
U148
All
Aug. 8, 1990.
U149
All
Aug. 8, 1990.
U150
All
Aug. 8, 1990.
U151
Wastewater
Aug. 8, 1990.
U151
Nonwastewater
May 8, 1992.
U152
All
Aug. 8, 1990.
U153
All
Aug. 8, 1990.
U154
All
Aug. 8, 1990.
U155
All
Aug. 8, 1990.
U156
All
Aug. 8, 1990.
U157
All
Aug. 8, 1990.
U158
All
Aug. 8, 1990.
U159
All
Aug. 8, 1990.
U160
All
Aug. 8, 1990.
U161
All
Aug. 8, 1990.
U162
All
Aug. 8, 1990.
U163
All
Aug. 8, 1990.
U164
All
Aug. 8, 1990.
U165
All
Aug. 8, 1990.
U166
All
Aug. 8, 1990.
U167
All
Aug. 8, 1990.
U168
All
Aug. 8, 1990.
U169
All
Aug. 8, 1990.
429
U170
All
Aug. 8, 1990.
U171
All
Aug. 8, 1990.
U172
All
Aug. 8, 1990.
U173
All
Aug. 8, 1990.
U174
All
Aug. 8, 1990.
U176
All
Aug. 8, 1990.
U177
All
Aug. 8, 1990.
U178
All
Aug. 8, 1990.
U179
All
Aug. 8, 1990.
U180
All
Aug. 8, 1990.
U181
All
Aug. 8, 1990.
U182
All
Aug. 8, 1990.
U183
All
Aug. 8, 1990.
U184
All
Aug. 8, 1990.
U185
All
Aug. 8, 1990.
U186
All
Aug. 8, 1990.
U187
All
Aug. 8, 1990.
U188
All
Aug. 8, 1990.
U189
All
Aug. 8, 1990.
U190
All
June 8, 1989.
U191
All
Aug. 8, 1990.
U192
All
Aug. 8, 1990.
U193
All
Aug. 8, 1990.
U194
All
June 8, 1989.
U196
All
Aug. 8, 1990.
U197
All
Aug. 8, 1990.
U200
All
Aug. 8, 1990.
U201
All
Aug. 8, 1990.
U202
All
Aug. 8, 1990.
U203
All
Aug. 8, 1990.
U204
All
Aug. 8, 1990.
U205
All
Aug. 8, 1990.
U206
All
Aug. 8, 1990.
U207
All
Aug. 8, 1990.
U208
All
Aug. 8, 1990.
U209
All
Aug. 8, 1990.
U210
All
Aug. 8, 1990.
U211
All
Aug. 8, 1990.
U213
All
Aug. 8, 1990.
U214
All
Aug. 8, 1990.
U215
All
Aug. 8, 1990.
U216
All
Aug. 8, 1990.
U217
All
Aug. 8, 1990.
U218
All
Aug. 8, 1990.
U219
All
Aug. 8, 1990.
430
U220
All
Aug. 8, 1990.
U221
All
June 8, 1989.
U222
All
Aug. 8, 1990.
U223
All
June 8, 1989.
U225
All
Aug. 8, 1990.
U226
All
Aug. 8, 1990.
U227
All
Aug. 8, 1990.
U228
All
Aug. 8, 1990.
U234
All
Aug. 8, 1990.
U235
All
June 8, 1989.
U236
All
Aug. 8, 1990.
U237
All
Aug. 8, 1990.
U238
All
Aug. 8, 1990.
U239
All
Aug. 8, 1990.
U240
All
Aug. 8, 1990.
U243
All
Aug. 8, 1990.
U244
All
Aug. 8, 1990.
U246
All
Aug. 8, 1990.
U247
All
Aug. 8, 1990.
U248
All
Aug. 8, 1990.
U249
All
Aug. 8, 1990.
U271
Mixed with radioactive wastes
Apr. 8, 1998.
U271
All others
July 8, 1996.
U277
Mixed with radioactive wastes
Apr. 8, 1998.
U277
All others
July 8, 1996.
U278
Mixed with radioactive wastes
Apr. 8, 1998.
U278
All others
July 8, 1996.
U279
Mixed with radioactive wastes
Apr. 8, 1998.
U279
All others
July 8, 1996.
U280
Mixed with radioactive wastes
Apr. 8, 1998.
U280
All others
July 8, 1996.
U328
Mixed with radioactive wastes
June 30, 1994.
U328
All others
Nov. 9, 1992.
U353
Mixed with radioactive wastes
June 30, 1994.
U353
All others
Nov. 9, 1992.
U359
Mixed with radioactive wastes
June 30, 1994.
U359
All others
Nov. 9, 1992.
U364
Mixed with radioactive wastes
Apr. 8, 1998.
U364
All others
July 8, 1996.
U365
Mixed with radioactive wastes
Apr. 8, 1998.
U365
All others
July 8, 1996.
U366
Mixed with radioactive wastes
Apr. 8, 1998.
U366
All others
July 8, 1996.
U367
Mixed with radioactive wastes
Apr. 8, 1998.
U367
All others
July 8, 1996.
431
U372
Mixed with radioactive wastes
Apr. 8, 1998.
U372
All others
July 8, 1996.
U373
Mixed with radioactive wastes
Apr. 8, 1998.
U373
All others
July 8, 1996.
U375
Mixed with radioactive wastes
Apr. 8, 1998.
U375
All others
July 8, 1996.
U376
Mixed with radioactive wastes
Apr. 8, 1998.
U376
All others
July 8, 1996.
U377
Mixed with radioactive wastes
Apr. 8, 1998.
U377
All others
July 8, 1996.
U378
Mixed with radioactive wastes
Apr. 8, 1998.
U378
All others
July 8, 1996.
U379
Mixed with radioactive wastes
Apr. 8, 1998.
U379
All others
July 8, 1996.
U381
Mixed with radioactive wastes
Apr. 8, 1998.
U381
All others
July 8, 1996.
U382
Mixed with radioactive wastes
Apr. 8, 1998.
U382
All others
July 8, 1996.
U383
Mixed with radioactive wastes
Apr. 8, 1998.
U383
All others
July 8, 1996.
U384
Mixed with radioactive wastes
Apr. 8, 1998.
U384
All others
July 8, 1996.
U385
Mixed with radioactive wastes
Apr. 8, 1998.
U385
All others
July 8, 1996.
U386
Mixed with radioactive wastes
Apr. 8, 1998.
U386
All others
July 8, 1996.
U387
Mixed with radioactive wastes
Apr. 8, 1998.
U387
All others
July 8, 1996.
U389
Mixed with radioactive wastes
Apr. 8, 1998.
U389
All others
July 8, 1996.
U390
Mixed with radioactive wastes
Apr. 8, 1998.
U390
All others
July 8, 1996.
U391
Mixed with radioactive wastes
Apr. 8, 1998.
U391
All others
July 8, 1996.
U392
Mixed with radioactive wastes
Apr. 8, 1998.
U392
All others
July 8, 1996.
U393
Mixed with radioactive wastes
Apr. 8, 1998.
U393
All others
July 8, 1996.
U394
Mixed with radioactive wastes
Apr. 8, 1998.
U394
All others
July 8, 1996.
U395
Mixed with radioactive wastes
Apr. 8, 1998.
U395
All others
July 8, 1996.
U396
Mixed with radioactive wastes
Apr. 8, 1998.
U396
All others
July 8, 1996.
U400
Mixed with radioactive wastes
Apr. 8, 1998.
432
U400
All others
July 8, 1996.
U401
Mixed with radioactive wastes
Apr. 8, 1998.
U401
All others
July 8, 1996.
U402
Mixed with radioactive wastes
Apr. 8, 1998.
U402
All others
July 8, 1996.
U403
Mixed with radioactive wastes
Apr. 8, 1998.
U403
All others
July 8, 1996.
U404
Mixed with radioactive wastes
Apr. 8, 1998.
U404
All others
July 8, 1996.
U407
Mixed with radioactive wastes
Apr. 8, 1998.
U407
All others
July 8, 1996.
U409
Mixed with radioactive wastes
Apr. 8, 1998.
U409
All others
July 8, 1996.
U410
Mixed with radioactive wastes
Apr. 8, 1998.
U410
All others
July 8, 1996.
U411
Mixed with radioactive wastes
Apr. 8, 1998.
U411
All others
July 8, 1996.
a
This table does not include mixed radioactive wastes (from the First, Second, and Third
rules) which are receiving a national capacity variance until May 8, 1992. This table
also does not include contaminated soil and debris wastes.
b
The standard was revised in the Third Third Final Rule (adopted by USEPA at 55 Fed.
Reg. 22520 (June 1, 1990) and by the Board in docket R90-11 by orders dated April
11, May 23, and August 8 and 22, 1991).
c
USEPA amended the standard in the Third Third Emergency Rule (at 58 Fed. Reg.
29860 (May 24, 1993), which the Board adopted in docket R93-16 on March 17,
1994); the original effective date was August 8, 1990.
d
The standard was revised in the Phase II Final Rule (which USEPA adopted at 59 Fed.
Reg. 47982 (Sept. 19, 1994) and the Board adopted in docket R95-6 by orders dated
June 1 and 15, 1995); the original effective date was August 8, 1990.
e
The standards for selected reactive wastes was revised in the Phase III Final Rule
(which USEPA adopted at 61 Fed. Reg. 15566 (Apr. 8, 1996) and the Board adopted
in docket R96-10/R97-3/R97-5 (consolidated) by an order dated November 6, 1997);
the original effective date was August 8, 1990.
TABLE 2
SUMMARY OF EFFECTIVE DATES OF LAND DISPOSAL
RESTRICTIONS FOR CONTAMINATED SOIL AND DEBRIS (CSD)
Restricted hazardous waste in CSD
Effective date
433
1. Solvent-(F001-F005) and dioxin-(F020-F023 and F026-F028) containing soil
and debris from CERCLA response of RCRA corrective actions.
Nov. 8, 1990.
2. Soil and debris not from CERCLA response or RCRA corrective actions
contaminated with less than one percent total solvents (F001-F005) or dioxins
(F020-F023 and F026-F028).
Nov. 8, 1988.
3. All soil and debris contaminated with First Third wastes for which treatment
standards are based on incineration.
Aug. 8, 1990.
4. All soil and debris contaminated with Second Third wastes for which treatment
standards are based on incineration.
June 8, 1991.
5. All soil and debris contaminated with Third Third wastes or, First or Second
Third “soft hammer” wastes which had treatment standards promulgated in the
Third Third rule, for which treatment standards are based on incineration,
vitrification, or mercury retorting, acid leaching followed by chemical
precipitation, or thermal recovery of metals, as well as all inorganic solids
debris contaminated with D004-D011 wastes, and all soil and debris
contaminated with mixed RCRA/radioactive wastes.
May 8, 1992.
6. Soil and debris contaminated with D012-D043, K141-K145, and K147-151
wastes.
Dec. 19, 1994.
7. Debris (only) contaminated with F037, F038, K107-K112, K117, K118,
K123-K126, K131, K132, K136, U328, U353, U359.
Dec. 19, 1994
8. Soil and debris contaminated with K156- K161, P127, P128, P188-P192,
P194, P196- P199, P201-P205, U271, U277-U280, U364-U367, U372,
U373, U375-U379, U381-U387, U389-U396, U400-U404, U407, and
U409-U411 wastes.
July 8, 1996.
9. Soil and debris contaminated with K088 wastes.
Jan. Oct. 8,
1997.
10. Soil and debris contaminated with radioactive wastes mixed with K088,
K156-K161, P127, P128, P188-P192, P194, P196-P199, P201-P205,
U271, U277-U280, U364-U367,U372, U373, U375-U379, U381-U387,
U389-U396, U400-U404, U407, and U409-U411 wastes.
April 8, 1998.
11. Soil and debris contaminated with F032, F034, and F035.
May 12, 1997.
12. Soil and debris contaminated with newly identified D004-D011 toxicity
characteristic wastes and mineral processing wastes.
Aug. 24, 1998.
13. Soil and debris contaminated with mixed radioactive newly identified D011
characteristic wastes and mineral processing wastes.
May 26, 2000.
BOARD NOTE: This table is provided for the convenience of the reader.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix H
National Capacity LDR Variances for UIC Wastes
See Note
a
Waste code
Waste category
Effective date
434
D001 (except High
TOC Ignitable Liquids
Subcategory)
c
All
Feb. 10, 1994.
D001 (High TOC
Ignitable Characteristic
Liquids Subcategory)
Nonwastewater
Sep. 19, 1995.
D002
b
All
May 8, 1992.
D002
c
All
Feb. 10, 1994.
D003 (cyanides)
All
May 8, 1992.
D003 (sulfides)
All
May 8, 1992.
D003 (explosives,
reactives).
All
May 8, 1992.
D007
All
May 8, 1992.
D009
Nonwastewater
May 8, 1992.
D012
All
Sep. 19, 1995.
D013
All
Sep. 19, 1995.
D014
All
Sep. 19, 1995.
D015
All
Sep. 19, 1995.
D016
All
Sep. 19, 1995.
D017
All
Sep. 19, 1995.
D018
All, including mixed with radioactive wastes
Apr. 8, 1998.
D019
All, including mixed with radioactive wastes
Apr. 8, 1998.
D020
All, including mixed with radioactive wastes
Apr. 8, 1998.
D021
All, including mixed with radioactive wastes
Apr. 8, 1998.
D022
All, including mixed with radioactive wastes
Apr. 8, 1998.
D023
All, including mixed with radioactive wastes
Apr. 8, 1998.
D024
All, including mixed with radioactive wastes
Apr. 8, 1998.
D025
All, including mixed with radioactive wastes
Apr. 8, 1998.
D026
All, including mixed with radioactive wastes
Apr. 8, 1998.
D027
All, including mixed with radioactive wastes
Apr. 8, 1998.
D028
All, including mixed with radioactive wastes
Apr. 8, 1998.
D029
All, including mixed with radioactive wastes
Apr. 8, 1998.
D030
All, including mixed with radioactive wastes
Apr. 8, 1998.
D031
All, including mixed with radioactive wastes
Apr. 8, 1998.
D032
All, including mixed with radioactive wastes
Apr. 8, 1998.
D033
All, including mixed with radioactive wastes
Apr. 8, 1998.
D034
All, including mixed with radioactive wastes
Apr. 8, 1998.
D035
All, including mixed with radioactive wastes
Apr. 8, 1998.
D036
All, including mixed with radioactive wastes
Apr. 8, 1998.
D037
All, including mixed with radioactive wastes
Apr. 8, 1998.
D038
All, including mixed with radioactive wastes
Apr. 8, 1998.
D039
All, including mixed with radioactive wastes
Apr. 8, 1998.
D040
All, including mixed with radioactive wastes
Apr. 8, 1998.
D041
All, including mixed with radioactive wastes
Apr. 8, 1998.
D042
All, including mixed with radioactive wastes
Apr. 8, 1998.
435
D043
All, including mixed with radioactive wastes
Apr. 8, 1998.
F001-F005
All spent F001-F005 solvent containing less than 1
percent total F001-F005 solvent constituents
Aug. 8, 1990.
F007
All
June 8, 1991.
F032
All, including mixed with radioactive wastes
May 12, 1999.
F034
All, including mixed with radioactive wastes
May 12,1999.
F035
All, including mixed with radioactive wastes
May 12, 1999.
F037
All
Nov. 8, 1992.
F038
All
Nov. 8, 1992.
F039
Wastewater
May 8, 1992.
K009
Wastewater
June 8, 1991.
K011
Nonwastewater
June 8, 1991.
K011
Wastewater
May 8, 1992.
K013
Nonwastewater
June 8, 1991.
K013
Wastewater
May 8, 1992.
K014
All
May 8, 1992.
K016 (dilute)
All
June 8, 1991.
K049
All
Aug. 8, 1990.
K050
All
Aug. 8, 1990.
K051
All
Aug. 8, 1990.
K052
All
Aug. 8, 1990.
K062
All
Aug. 8, 1990.
K071
All
Aug. 8, 1990.
K088
All
Jan. 8, 1997.
K104
All
Aug. 8, 1990.
K107
All
Nov. 8, 1992.
K108
All
Nov. 9, 1992.
K109
All
Nov. 9, 1992.
K110
All
Nov. 9, 1992.
K111
All
Nov. 9, 1992.
K112
All
Nov. 9, 1992.
K117
All
June 30, 1995.
K118
All
June 30, 1995.
K123
All
Nov. 9, 1992.
K124
All
Nov. 9, 1992.
K125
All
Nov. 9, 1992.
K126
All
Nov. 9, 1992.
K131
All
June 30, 1995.
K132
All
June 30, 1995.
K136
All
Nov. 9, 1992.
K141
All
Dec. 19, 1994.
K142
All
Dec. 19, 1994.
K143
All
Dec. 19, 1994.
K144
All
Dec. 19, 1994.
K145
All
Dec. 19, 1994.
436
K147
All
Dec. 19, 1994.
K148
All
Dec. 19, 1994.
K149
All
Dec. 19, 1994.
K150
All
Dec. 19, 1994.
K151
All
Dec. 19, 1994.
K156
All
July 8, 1996.
K157
All
July 8, 1996.
K158
All
July 8, 1996.
K159
All
July 8, 1996.
K160
All
July 8, 1996.
K161
All
July 8, 1996.
NA
Newly identified mineral processing wastes from
titanium dioxide production and mixed
radioactive/newly identified D004-D011 characteristic
wastes and mineral processing wastes.
May 26, 2000.
P127
All
July 8, 1996.
P128
All
July 8, 1996.
P185
All
July 8, 1996.
P188
All
July 8, 1996.
P189
All
July 8, 1996.
P190
All
July 8, 1996.
P191
All
July 8, 1996.
P192
All
July 8, 1996.
P194
All
July 8, 1996.
P196
All
July 8, 1996.
P197
All
July 8, 1996.
P198
All
July 8, 1996.
P199
All
July 8, 1996.
P201
All
July 8, 1996.
P202
All
July 8, 1996.
P203
All
July 8, 1996.
P204
All
July 8, 1996.
P205
All
July 8, 1996.
U271
All
July 8, 1996.
U277
All
July 8, 1996.
U278
All
July 8, 1996.
U279
All
July 8, 1996.
U280
All
July 8, 1996.
U328
All
Nov. 9, 1992.
U353
All
Nov. 9, 1992.
U359
All
Nov. 9, 1992.
U364
All
July 8, 1996.
U365
All
July 8, 1996.
U366
All
July 8, 1996.
U367
All
July 8, 1996.
U372
All
July 8, 1996.
437
U373
All
July 8, 1996.
U375
All
July 8, 1996.
U376
All
July 8, 1996.
U377
All
July 8, 1996.
U378
All
July 8, 1996.
U379
All
July 8, 1996.
U381
All
July 8, 1996.
U382
All
July 8, 1996.
U383
All
July 8, 1996.
U384
All
July 8, 1996.
U385
All
July 8, 1996.
U386
All
July 8, 1996.
U387
All
July 8, 1996.
U389
All
July 8, 1996.
U390
All
July 8, 1996.
U391
All
July 8, 1996.
U392
All
July 8, 1996.
U395
All
July 8, 1996.
U396
All
July 8, 1996.
U400
All
July 8, 1996.
U401
All
July 8, 1996.
U402
All
July 8, 1996.
U403
All
July 8, 1996.
U404
All
July 8, 1996.
U407
All
July 8, 1996.
U409
All
July 8, 1996.
U410
All
July 8, 1996.
U411
All
July 8, 1996.
a
Wastes that are deep well disposed on-site receive a six-month variance, with
restrictions effective in November 1990.
b
Deep well injected D002 liquids with a pH less than 2 must meet the California List
treatment standards on August 8, 1990.
c
Managed in systems defined in 35 Ill. Adm. Code 730.105(e) as Class V injection
wells that do not engage in CWA-equivalent treatment before injection.
BOARD NOTE: This table is provided for the convenience of the reader.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table I Generator Paperwork Requirements
438
Subsection of Section 728.107 under
Which the Paperwork is Required:
Required information
(a)(2)
(a)(3)
(a)(4)
(a)(9)
1. USEPA hazardous waste and manifest number
of first shipment
üüüü
2. Statement: this waste is not prohibited from
land disposal
ü
3. The waste is subject to the LDRs. The
constituents of concern for USEPA hazardous
waste numbers F001 through F005 and F039
waste, and underlying hazardous constituents (for
wastes that are not managed in a Clean Water Act
(CWA) or CWA-equivalent facility) in
characteristic waste, unless the waste will be
treated and monitored for all constituents. If all
constituents will be treated and monitored, there
is no need to put them all on the LDR notice
üü
4. The notice must include the applicable
wastewater/ nonwastewater category (see Section
728.102(d) and (f)) and subdivisions made within
a waste code based on waste-specific criteria
(such as D003 reactive cyanide)
üü
5. Waste analysis data (when available)
ü
ü
ü
6. Date the waste is subject to the prohibition
ü
7. For hazardous debris, when treating with the
alternative treatment technologies provided by
Section 728.145: the contaminants subject to
treatment, as described in Section 728.145(b);
and an indication that these contaminants are
being treated to comply with Section 728.145
üü
439
8. For contaminated soil subject to LDRs as
provided in Section 728.149(a), the constituents
subject to treatment as described in Section
728.149(d), and the following statement: This
contaminated soil (does/does not) contain listed
hazardous waste and (does/does not) exhibit a
characteristic of hazardous waste and (is subject
to/complies with) the soil treatment standards as
provided by Section 728.149(c) or the universal
treatment standards
ü
89. A certification is needed (see applicable
subsection for exact wording)
üü
BOARD NOTE: Derived from Table 1 to 40 CFR 268.7(a)(4) (1997), as amended at 63 Fed.
Reg. 28639 (May 26, 1998).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table T Treatment Standards for Hazardous Wastes
Note: The treatment standards that heretofore appeared in tables in Sections 728.141,
728.142, and 728.143 have been consolidated into this table.
Waste Code
Waste Description and Treatment or Regulatory Subcategory
1
Regulated Hazardous Constituent
Wastewaters
Nonwastewaters
Common Name
CAS
2
Number
Concentration in
mg/l
3
; or Techno-
logy Code
4
Concentration in
mg/kg
5
unless
noted as “mg/l
TCLP”; or Tech-
nology Code
4
D001
9
Ignitable Characteristic Wastes, except for the 35 Ill. Adm. Code 721.121(a)(1) High TOC
Subcategory.
NA
NA
DEACT and meet
Section 728.148
standards;
8
or
RORGS; or
CMBST
DEACT and meet
Section 728.148
standards;
8
or
RORGS; or
CMBST
440
D001
9
High TOC Ignitable Characteristic Liquids Subcategory based on 35 Ill. Adm. Code
721.121(a)(1) - Greater than or equal to 10 percent total organic carbon.
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
RORGS;
CMBST; or
POLYM
D002
9
Corrosive Characteristic Wastes.
NA
NA
DEACT and meet
Section 728.148
standards
8
DEACT and meet
Section 728.148
standards
8
D002, D004, D005, D006, D007, D008, D009, D010, D011
Radioactive high level wastes generated during the reprocessing of fuel rods.
(Note: This subcategory consists of nonwastewaters only.)
Corrosivity (pH)
NA
NA
HLVIT
Arsenic
7440-38-2
NA
HLVIT
Barium
7440-39-3
NA
HLVIT
Cadmium
7440-43-9
NA
HLVIT
Chromium (Total)
7440-47-3
NA
HLVIT
Lead
7439-92-1
NA
HLVIT
Mercury
7439-97-6
NA
HLVIT
Selenium
7782-49-2
NA
HLVIT
Silver
7440-22-4
NA
HLVIT
D003
9
Reactive Sulfides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
NA
NA
DEACT
DEACT
D003
9
Explosive subcategory based on 35 Ill. Adm. Code 721.123(a)(6), (a)(7), and (a)(8).
NA
NA
DEACT and meet
Section 728.148
standards
8
DEACT and meet
Section 728.148
standards
8
D003
9
Unexploded ordnance and other explosive devices that have been the subject of an emergency
response.
NA
NA
DEACT
DEACT
441
D003
9
Other Reactives Subcategory based on 35 Ill. Adm. Code 721.123(a)(1).
NA
NA
DEACT and meet
Section 728.148
standards
8
DEACT and meet
Section 728.148
standards
8
D003
9
Water Reactive Subcategory based on 35 Ill. Adm. Code 721.123(a)(2), (a)(3), and (a)(4).
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
DEACT and
meet Section
728.148
standards
8
D003
9
Reactive Cyanides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
Cyanides (Total)
7
57-12-5
--
590
Cyanides (Amenable)
7
57-12-5
0.86
30
D004
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for arsenic based
on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method
1310 1311.
Arsenic
7440-38-2
5.01.4 and meet
Section 728.148
standards
8
5.0 mg/l EP
TCLP and meet
Section 728.148
standards
8
Arsenic; alternative
6
standard for
nonwastewaters only.
7440-38-2
NA
5.0 mg/l TCLP
D005
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for barium based
on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method
1310 1311.
Barium
7440-39-3
1001.2 and meet
Section 728.148
standards
8
100 21 mg/l
TCLP and meet
Section 728.148
standards
8
442
D006
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for cadmium based
on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method
1310 1311.
Cadmium
7440-43-9
1.00.69 and meet
Section 728.148
standards
8
1.0 0.11 mg/l
TCLP and meet
Section 728.148
standards
8
D006
9
Cadmium-Containing Batteries Subcategory
(Note: This subcategory consists of nonwastewaters only.)
Cadmium
7440-43-9
NA
RTHRM
D007
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for chromium
based on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846
Method 1310 1311.
Chromium (Total)
7440-47-3
5.02.77 and meet
Section 728.148
standards
8
5.0 0.60 mg/l
TCLP and meet
Section 728.148
standards
8
D008
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for lead based on
the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method 1310
1311.
Lead
7439-92-1
5.00.69 and meet
Section 728.148
standards
8
5.0 0.75 mg/l EP
TCLP and meet
Section 728.148
standards
8
Lead; alternative
6
standard for
nonwastewaters only
7439-92-1
NA
5.0 mg/l TCLP
D008
9
Lead Acid Batteries Subcategory
(Note: This standard only applies to lead acid batteries that are identified as RCRA hazardous
wastes and that are not excluded elsewhere from regulation under the land disposal restrictions
of this Part or exempted under other regulations (see 35 Ill. Adm. Code 726.180). This
subcategory consists of nonwastewaters only.)
Lead
7439-92-1
NA
RLEAD
443
D008
9
Radioactive Lead Solids Subcategory
(Note: These lead solids include, but are not limited to, all forms of lead shielding and other
elemental forms of lead. These lead solids do not include treatment residuals such as
hydroxide sludges, other wastewater treatment residuals, or incinerator ashes that can undergo
conventional pozzolanic stabilization, nor do they include organo-lead materials that can be
incinerated and stabilized as ash. This subcategory consists of nonwastewaters only.)
Lead
7439-92-1
NA
MACRO
D009
9
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-
846 Method 1310 1311; and contain greater than or equal to 260 mg/kg total mercury that also
contain organics and are not incinerator residues. (High Mercury-Organic Subcategory)
Mercury
7439-97-6
NA
IMERC; or
RMERC
D009
9
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-
846 Method 1310 1311; and contain greater than or equal to 260 mg/kg total mercury that are
inorganic, including incinerator residues and residues from RMERC. (High Mercury-
Inorganic Subcategory)
Mercury
7439-97-6
NA
RMERC
D009
9
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-
846 Method 1310 1311; and contain less than 260 mg/kg total mercury. (Low Mercury
Subcategory)
Mercury
7439-97-6
NA
0.20 mg/l TCLP
and meet Section
728.148
standards
8
D009
9
All other nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity
for mercury based on the toxicity characteristic leaching procedure (TCLP) in SW-846 Method
1311; and contain less than 260 mg/kg total mercury and that are not residues from RMERC.
(Low Mercury Subcategory)
Mercury
7439-97-6
NA
0.025 mg/l TCLP
and meet Section
728.148
standards
8
444
D009
9
All D009 wastewaters.
Mercury
7439-97-6
0.200.15 and
meet Section
728.148
standards
8
NA
D009
9
Elemental mercury contaminated with radioactive materials.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
AMLGM
D009
9
Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
IMERC
D010
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for selenium based
on the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method
1310 1311.
Selenium
7782-49-2
1.00.82
5.7 mg/l TCLP
and meet Section
728.148
standards
8
D011
9
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for silver based on
the extraction toxicity characteristic leaching procedure (EP) (TCLP) in SW-846 Method 1310
1311.
Silver
7440-22-4
5.00.43
5.0 0.14 mg/l
TCLP and meet
Section 728.148
standards
8
D012
9
Wastes that are TC for Endrin based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
Endrin
72-20-8
BIODG; or
CMBST
0.13 and meet
Section 728.148
standards
8
Endrin aldehyde
7421-93-4
BIODG; or
CMBST
0.13 and meet
Section 728.148
standards
8
445
D013
9
Wastes that are TC for Lindane based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
α-BHC
319-84-6
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
β-BHC
319-85-7
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
δ-BHC
319-86-8
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
χ-BHC
(Lindane)
58-89-9
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
D014
9
Wastes that are TC for Methoxychlor based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Methoxychlor
72-43-5
WETOX or
CMBST
0.18 and meet
Section 728.148
standards
8
D015
9
Wastes that are TC for Toxaphene based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Toxaphene
8001-35-2
BIODG or
CMBST
2.6 and meet
Section 728.148
standards
8
D016
9
Wastes that are TC for 2,4-D (2,4-Dichlorophenoxyacetic acid) based on the toxicity
characteristic leaching procedure (TCLP) in SW-846 Method 1311.
2,4-D (2,4-Dichlorophenoxy-
acetic acid)
94-75-7
CHOXD;
BIODG; or
CMBST
10 and meet
Section 728.148
standards
8
D017
9
Wastes that are TC for 2,4,5-TP (Silvex) based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
2,4,5-TP (Silvex)
93-72-1
CHOXD or
CMBST
7.9 and meet
Section 728.148
standards
8
446
D018
9
Wastes that are TC for Benzene based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
Benzene
71-43-2
0.14 and meet
Section 728.148
standards
8
10 and meet
Section 728.148
standards
8
D019
9
Wastes that are TC for Carbon tetrachloride based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Carbon tetrachloride
56-23-5
0.057 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D020
9
Wastes that are TC for Chlordane based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Chlordane (α and
χ
isomers)
57-74-9
0.0033 and meet
Section 728.148
standards
8
0.26 and meet
Section 728.148
standards
8
D021
9
Wastes that are TC for Chlorobenzene based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Chlorobenzene
108-90-7
0.057 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D022
9
Wastes that are TC for Chloroform based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Chloroform
67-66-3
0.046 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D023
9
Wastes that are TC for o-Cresol based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
o-Cresol
95-48-7
0.11 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
447
D024
9
Wastes that are TC for m-Cresol based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
m-Cresol
(difficult to distinguish from p-
cresol)
108-39-4
0.77 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D025
9
Wastes that are TC for p-Cresol based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
p-Cresol
(difficult to distinguish from m-
cresol)
106-44-5
0.77 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D026
9
Wastes that are TC for Cresols (Total) based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Cresol-mixed isomers (Cresylic
acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88 and meet
Section 728.148
standards
8
11.2 and meet
Section 728.148
standards
8
D027
9
Wastes that are TC for p-Dichlorobenzene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
p-Dichlorobenzene (1,4-
Dichlorobenzene)
106-46-7
0.090 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D028
9
Wastes that are TC for 1,2-Dichloroethane based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
1,2-Dichloroethane
107-06-2
0.21 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D029
9
Wastes that are TC for 1,1-Dichloroethylene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
1,1-Dichloroethylene
75-35-4
0.025 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
448
D030
9
Wastes that are TC for 2,4-Dinitrotoluene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
2,4-Dinitrotoluene
121-14-2
0.32 and meet
Section 728.148
standards
8
140 and meet
Section 728.148
standards
8
D031
9
Wastes that are TC for Heptachlor based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Heptachlor
76-44-8
0.0012 and meet
Section 728.148
standards
8
0.066 and meet
Section 728.148
standards
8
Heptachlor epoxide
1024-57-3
0.016 and meet
Section 728.148
standards
8
0.066 and meet
Section 728.148
standards
8
D032
9
Wastes that are TC for Hexachlorobenzene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Hexachlorobenzene
118-74-1
0.055 and meet
Section 728.148
standards
8
10 and meet
Section 728.148
standards
8
D033
9
Wastes that are TC for Hexachlorobutadiene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Hexachlorobutadiene
87-68-3
0.055 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D034
9
Wastes that are TC for Hexachloroethane based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Hexachloroethane
67-72-1
0.055 and meet
Section 728.148
standards
8
30 and meet
Section 728.148
standards
8
D035
9
Wastes that are TC for Methyl ethyl ketone based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Methyl ethyl ketone
78-93-3
0.28 and meet
Section 728.148
standards
8
36 and meet
Section 728.148
standards
8
449
D036
9
Wastes that are TC for Nitrobenzene based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Nitrobenzene
98-95-3
0.068 and meet
Section 728.148
standards
8
14 and meet
Section 728.148
standards
8
D037
9
Wastes that are TC for Pentachlorophenol based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Pentachlorophenol
87-86-5
0.089 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
D038
9
Wastes that are TC for Pyridine based on the toxicity characteristic leaching procedure (TCLP)
in SW-846 Method 1311.
Pyridine
110-86-1
0.014 and meet
Section 728.148
standards
8
16 and meet
Section 728.148
standards
8
D039
9
Wastes that are TC for Tetrachloroethylene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Tetrachloroethylene
127-18-4
0.056 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D040
9
Wastes that are TC for Trichloroethylene based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
Trichloroethylene
79-01-6
0.054 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D041
9
Wastes that are TC for 2,4,5-Trichlorophenol based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
2,4,5-Trichlorophenol
95-95-4
0.18 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
450
D042
9
Wastes that are TC for 2,4,6-Trichlorophenol based on the toxicity characteristic leaching
procedure (TCLP) in SW-846 Method 1311.
2,4,6-Trichlorophenol
88-06-2
0.035 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
D043
9
Wastes that are TC for Vinyl chloride based on the toxicity characteristic leaching procedure
(TCLP) in SW-846 Method 1311.
Vinyl chloride
75-01-4
0.27 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
F001, F002, F003, F004 & F005
F001, F002, F003, F004, or F005 solvent wastes that contain any combination of one or more
of the following spent solvents: acetone, benzene, n-butyl alcohol, carbon disulfide, carbon
tetrachloride, chlorinated fluorocarbons, chlorobenzene, o-cresol, m-cresol, p-cresol, cyclo-
hexanone, o-dichlorobenzene, 2-ethoxyethanol, ethyl acetate, ethyl benzene, ethyl ether,
isobutyl alcohol, methanol, methylene chloride, methyl ethyl ketone, methyl isobutyl ketone,
nitrobenzene, 2-nitropropane, pyridine, tetrachloroethylene, toluene, 1,1,1-trichloroethane,
1,1,2-trichloroethane, 1,1,2-trichloro-1,2,2-trifluoroethane, trichloroethylene, trichloromono-
fluoromethane, or xylenes (except as specifically noted in other subcategories). See further
details of these listings in 35 Ill. Adm. Code 721.131
Acetone
67-64-1
0.28
160
Benzene
71-43-2
0.14
10
n-Butyl alcohol
71-36-3
5.6
2.6
Carbon disulfide
75-15-0
3.8
NA
Carbon tetrachloride
56-23-5
0.057
6.0
Chlorobenzene
108-90-7
0.057
6.0
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from m-
cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers (Cresylic
acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88
11.2
Cyclohexanone
108-94-1
0.36
NA
o-Dichlorobenzene
95-50-1
0.088
6.0
Ethyl acetate
141-78-6
0.34
33
Ethyl benzene
100-41-4
0.057
10
451
Ethyl ether
60-29-7
0.12
160
Isobutyl alcohol
78-83-1
5.6
170
Methanol
67-56-1
5.6
NA
Methylene chloride
75-9-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Nitrobenzene
98-95-3
0.068
14
Pyridine
110-86-1
0.014
16
Tetrachloroethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
1,1,2-Trichloro-1,2,2-trifluoro-
ethane
76-13-1
0.057
30
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane
75-69-4
0.020
30
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
F001, F002, F003, F004 & F005
F003 and F005 solvent wastes that contain any combination of one or more of the following
three solvents as the only listed F001 through F005 solvents: carbon disulfide, cyclohexanone,
or methanol. (Formerly Section 728.141(c))
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
Methanol
67-56-1
5.6
0.75 mg/l TCLP
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Nitropropane as the only listed F001 through F005 solvent.
2-Nitropropane
79-46-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Ethoxyethanol as the only listed F001 through F005 solvent.
2-Ethoxyethanol
110-80-5
BIODG; or
CMBST
CMBST
F006
Wastewater treatment sludges from electroplating operations except from the following
processes: (1) Sulfuric acid anodizing of aluminum; (2) tin plating on carbon steel; (3) zinc
plating (segregated basis) on carbon steel; (4) aluminum or zinc-aluminum plating on carbon
452
steel; (5) cleaning or stripping associated with tin, zinc, and aluminum plating on carbon steel;
and (6) chemical etching and milling of aluminum.
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
F007
Spent cyanide plating bath solutions from electroplating operations.
Cadmium
7440-43-9
NA
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
F008
Plating bath residues from the bottom of plating baths from electroplating operations where
cyanides are used in the process.
Cadmium
7440-43-9
NA
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
453
F009
Spent stripping and cleaning bath solutions from electroplating operations where cyanides are
used in the process.
Cadmium
7440-43-9
NA
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
F010
Quenching bath residues from oil baths from metal heat treating operations where cyanides are
used in the process.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
NA
F011
Spent cyanide solutions from salt bath pot cleaning from metal heat treating operations.
Cadmium
7440-43-9
NA
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
F012
Quenching wastewater treatment sludges from metal heat treating operations where cyanides
are used in the process.
Cadmium
7440-43-9
NA
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
454
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
F019
Wastewater treatment sludges from the chemical conversion coating of aluminum except from
zirconium phosphating in aluminum can washing when such phosphating is an exclusive
conversion coating process.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
F020, F021, F022, F023, F026
Wastes (except wastewater and spent carbon from hydrogen chloride purification) from the
production or manufacturing use (as a reactant, chemical intermediate, or component in a
formulating process) of: (1) tri- or tetrachlorophenol, or of intermediates used to produce
their pesticide derivatives, excluding wastes from the production of Hexachlorophene from
highly purified 2,4,5-trichlorophenol (i.e., F020); (2) pentachlorophenol, or of intermediates
used to produce its derivatives (i.e., F021); (3) tetra-, penta-, or hexachlorobenzenes under
alkaline conditions (i.e., F022) and wastes (except wastewater and spent carbon from hydrogen
chloride purification) from the production of materials on equipment previously used for the
production or manufacturing use (as a reactant, chemical intermediate, or component in a
formulating process) of: (1) tri- or tetrachlorophenols, excluding wastes from equipment used
only for the production of Hexachlorophene from highly purified 2,4,5-trichlorophenol (F023)
or (2) tetra-, penta-, or hexachlorobenzenes under alkaline conditions (i.e., F026).
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
455
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F024
Process wastes, including but not limited to, distillation residues, heavy ends, tars, and reactor
clean-out wastes, from the production of certain chlorinated aliphatic hydrocarbons by free
radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon
chain lengths ranging from one to and including five, with varying amounts and positions of
chlorine substitution. (This listing does not include wastewaters, wastewater treatment
sludges, spent catalysts, and wastes listed in 35 Ill. Adm. Code 721.131 or 721.132.)
All F024 wastes
NA
CMBST
11
CMBST
11
2-Chloro-1,3-butadiene
126-99-8
0.057
0.28
3-Chloropropylene
107-05-1
0.036
30
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
bis(2-Ethylhexyl)phthalate
117-81-7
0.28
28
Hexachloroethane
67-72-1
0.055
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
F025
Condensed light ends from the production of certain chlorinated aliphatic hydrocarbons by free
radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon
chain lengths ranging from one up to and including five, with varying amounts and positions
of chlorine substitution. F025--Light Ends Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
456
F025
Spent filters and filter aids, and spent desiccant wastes from the production of certain
chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These chlorinated
aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and
including five, with varying amounts and positions of chlorine substitution. F025--Spent
Filters/Aids and Desiccants Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F027
Discarded unused formulations contianing tri-, tetra-, or pentachlorophenol or discarded
unused formulations containing compounds derived from these chlorophenols. (This listing
does not include formulations containing hexachlorophene synthesized from prepurified 2,4,5-
trichlorophenol as the sole component.)
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F028
Residues resulting from the incineration or thermal treatment of soil contaminated with
USEPA hazardous waste numbers F020, F021, F023, F026, and F027.
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
457
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F032
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes
generated at plants that currently use or have previously used chlorophenolic formulations
(except potentially cross-contaminated wastes that have had the F032 waste code deleted in
accordance with 35 Ill. Adm. Code 721.135 or potentially cross-contaminated wastes that are
otherwise currently regulated as hazardous wastes (i.e., F034 or F035), where the generator
does not resume or initiate use of chlorophenolic formulations). This listing does not include
K001 bottom sediment sludge from the treatment of wastewater from wood preserving
processes that use creosote and/or penta-chlorophenol.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)
fluoranthene)
207-08-9
0.11
6.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
2-4-Dimethyl phenol
105-67-9
0.036
14
Fluorene
86-73-7
0.059
3.4
Hexachlorodibenzo-p-dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Hexachlorodibenzofurans
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Pentachlorodibenzo-p-dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
458
Pentachlorodibenzofurans
NA
0.000035 or
CMBST
11
0.001 or
CMBST
11
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Tetrachlorodibenzo-p-dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Tetrachlorodibenzofurans
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
F034
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes
generated at plants that use creosote formulations. This listing does not include K001 bottom
sediment sludge from the treatment of wastewater from wood preserving processes that use
creosote or pentachlorophenol.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene (difficult
to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Fluorene
86-73-7
0.059
3.4
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
459
F035
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes that
are generated at plants that use inorganic preservatives containing arsenic or chromium. This
listing does not include K001 bottom sediment sludge from the treatment of wastewater from
wood preserving processes that use creosote or pentachlorophenol.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
F037
Petroleum refinery primary oil/water/solids separation sludge--Any sludge generated from the
gravitational separation of oil/water/solids during the storage or treatment of process
wastewaters and oily cooling wastewaters from petroleum refineries. Such sludges include,
but are not limited to, those generated in: oil/water/solids separators; tanks and
impoundments; ditches and other conveyances; sumps; and stormwater units receiving dry
weather flow. Sludge generated in stormwater units that do not receive dry weather flow,
sludges generated from non-contact once-through cooling waters segregated for treatment from
other process or oily cooling waters, sludges generated in agressive biological treatment units
as defined in 35 Ill. Adm. Code 721.131(b)(2) (including sludges generated in one or more
additional units after wastewaters have been treated in agressive biological treatment units) and
K051 wastes are not included in this listing.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
460
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
F038
Petroleum refinery secondary (emulsified) oil/water/solids separation sludge or float generated
from the physical or chemical separation of oil/water/solids in process wastewaters and oily
cooling wastewaters from petroleum refineries. Such wastes include, but are not limited to, all
sludges and floats generated in: induced air floatation (IAF) units, tanks and impoundments,
and all sludges generated in DAF units. Sludges generated in stormwater units that do not
receive dry weather flow, sludges generated from non-contact once-through cooling waters
segregated for treatment from other process or oily cooling waters, sludges and floats
generated in agressive biological treatment units as defined in 35 Ill. Adm. Code
721.131(b)(2) (including sludges and floats generated in one or more additional units after
wastewaters have been treated in agressive biological units) and F037, K048, and K051 are not
included in this listing.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
F039
Leachate (liquids that have percolated through land disposed wastes) resulting from the
disposal of more than one restricted waste classified as hazardous under Subpart D of this
Part. (Leachate resulting from the disposal of one or more of the following USEPA hazardous
wastes and no other hazardous wastes retains its USEPA hazardous waste numbers: F020,
F021, F022, F026, F027, or F028.).
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
461
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
NA
Acetophenone
96-86-2
0.010
9.7
2-Acetylaminofluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylonitrile
107-13-1
0.24
84
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
α-BHC
319-84-6
0.00014
0.066
β-BHC
319-85-7
0.00014
0.066
δ-BHC
319-86-8
0.023
0.066
χ-BHC
58-89-9
0.0017
0.066
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloromethane
75-27-4
0.35
15
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
4-Bromophenyl phenyl ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitrophenol
(Dinoseb)
88-85-7
0.066
2.5
Carbon disulfide
75-15-0
3.8
NA
Carbon tetrachloride
56-23-5
0.057
6.0
Chlordane (α and
χ
isomers)
57-74-9
0.0033
0.26
p-Chloroaniline
106-47-8
0.46
16
Chlorobenzene
108-90-7
0.057
6.0
Chlorobenzilate
510-15-6
0.10
NA
2-Chloro-1,3-butadiene
126-99-8
0.057
NA
Chlorodibromomethane
124-48-1
0.057
15
Chloroethane
75-00-3
0.27
6.0
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
Chloroform
67-66-3
0.046
6.0
462
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
2-Chloronaphthalene
91-58-7
0.055
5.6
2-Chlorophenol
95-57-8
0.044
5.7
3-Chloropropylene
107-05-1
0.036
30
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from m-
cresol)
106-44-5
0.77
5.6
Cyclohexanone
108-94-1
0.36
NA
1,2-Dibromo-3-chloropropane
96-12-8
0.11
15
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
Dibromomethane
74-95-3
0.11
15
2,4-D (2,4-Dichlorophenoxy-
acetic acid)
94-75-7
0.72
10
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
p,p’-DDE
72-55-9
0.031
0.087
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Dibenz(a,e)pyrene
192-65-4
0.061
NA
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Dichlorodifluoromethane
75-71-8
0.23
7.2
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
87-65-0
0.044
14
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethyl phthalate
84-66-2
0.20
28
463
2-4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
1,4-Dinitrobenzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitrophenol
51-28-5
0.12
160
2,4-Dinitrotoluene
121-14-2
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
Di-n-propylnitrosamine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
12.0
170
Diphenylamine (difficult to
distinguish from diphenylnitros-
amine)
122-39-4
0.92
NA
Diphenylnitrosamine (difficult to
distinguish from diphenylamine)
86-30-6
0.92
NA
1,2-Diphenylhydrazine
122-66-7
0.087
NA
Disulfoton
298-04-4
0.017
6.2
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
Ethyl acetate
141-78-6
0.34
33
Ethyl cyanide (Propanenitrile)
107-12-0
0.24
360
Ethyl benzene
100-41-4
0.057
10
Ethyl ether
60-29-7
0.12
160
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
464
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-8
0.0011
0.13
Methacrylonitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
NA
Methapyrilene
91-80-5
0.081
1.5
Methoxychlor
72-43-5
0.25
0.18
3-Methylcholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methyl methacrylate
80-62-6
0.14
160
Methyl methansulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
p-Nitroaniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
p-Nitrophenol
100-02-7
0.12
29
N-Nitrosodiethylamine
55-18-5
0.40
28
N-Nitrosodimethylamine
62-75-9
0.40
NA
N-Nitroso-di-n-butylamine
924-16-3
0.40
17
N-Nitrosomethylethylamine
10595-95-6
0.40
2.3
N-Nitrosomorpholine
59-89-2
0.40
2.3
N-Nitrosopiperidine
100-75-4
0.013
35
N-Nitrosopyrrolidine
930-55-2
0.013
35
Parathion
56-38-2
0.014
4.6
Total PCBs
(sum of all PCB isomers, or all
Aroclors)
1336-36-3
0.10
10
Pentachlorobenzene
608-93-5
0.055
10
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachloronitrobenzene
82-68-8
0.055
4.8
Pentachlorophenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
465
Phorate
298-02-2
0.021
4.6
Phthalic anhydride
85-44-9
0.055
NA
Pronamide
23950-58-5
0.093
1.5
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
2,4,5-T
93-76-5
0.72
7.9
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Bromoform (Tribromomethane) 75-25-2
0.63
15
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane
75-69-4
0.020
30
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
1,2,3-Trichloropropane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-trifluoro-
ethane
76-13-1
0.057
30
tris(2,3-Dibromopropyl)
phosphate
126-72-7
0.11
NA
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 1.15 mg/l
TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 21 mg/l
TCLP
Beryllium
7440-41-7
0.82
NA
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
466
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
NA
Fluoride
16964-48-8
35
NA
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Mercury
7439-97-6
0.15
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
Silver
7440-22-4
0.43
0.30 0.14 mg/l
TCLP
Sulfide
8496-25-8
14
NA
Thallium
7440-28-0
1.4
NA
Vanadium
7440-62-2
4.3
NA
K001
Bottom sediment sludge from the treatment of wastewaters from wood preserving processes
that use creosote or pentachlorophenol.
Naphthalene
91-20-3
0.059
5.6
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K002
Wastewater treatment sludge from the production of chrome yellow and orange pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K003
Wastewater treatment sludge from the production of molybdate orange pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
467
K004
Wastewater treatment sludge from the production of zinc yellow pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K005
Wastewater treatment sludge from the production of chrome green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
K006
Wastewater treatment sludge from the production of chrome oxide green pigments
(anhydrous).
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K006
Wastewater treatment sludge from the production of chrome oxide green pigments (hydrated).
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
NA
K007
Wastewater treatment sludge from the production of iron blue pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
K008
Oven residue from the production of chrome oxide green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
468
K009
Distillation bottoms from the production of acetaldehyde from ethylene.
Chloroform
67-66-3
0.046
6.0
K010
Distillation side cuts from the production of acetaldehyde from ethylene.
Chloroform
67-66-3
0.046
6.0
K011
Bottom stream from the wastewater stripper in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K013
Bottom stream from the acetonitrile column in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K014
Bottoms from the acetonitrile purification column in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K015
Still bottoms from the distillation of benzyl chloride.
Anthracene
120-12-7
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
469
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
K016
Heavy ends or distillation residues from the production of carbon tetrachloride.
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
Hexachloroethane
67-72-1
0.055
30
Tetrachloroethylene
127-18-4
0.056
6.0
K017
Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
1,2-Dichloropropane
78-87-5
0.85
18
1,2,3-Trichloropropane
96-18-4
0.85
30
K018
Heavy ends from the fractionation column in ethyl chloride production.
Chloroethane
75-00-3
0.27
6.0
Chloromethane
74-87-3
0.19
NA
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
NA
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K019
Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
p-Dichlorobenzene
106-46-7
0.090
NA
1,2-Dichloroethane
107-06-2
0.21
6.0
Fluorene
86-73-7
0.059
NA
Hexachloroethane
67-72-1
0.055
30
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
NA
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
470
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K020
Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
K021
Aqueous spent antimony catalyst waste from fluoromethanes production.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Antimony
7440-36-0
1.9
2.1 1.15 mg/l
TCLP
K022
Distillation bottom tars from the production of phenol or acetone from cumene.
Toluene
108-88-3
0.080
10
Acetophenone
96-86-2
0.010
9.7
Diphenylamine (difficult to
distinguish from diphenylnitros-
amine)
122-39-4
0.92
13
Diphenylnitrosamine (difficult to
distinguish from diphenylamine)
86-30-6
0.92
13
Phenol
108-95-2
0.039
6.2
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
K023
Distillation light ends from the production of phthalic anhydride from naphthalene.
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
85-44-9
0.055
28
K024
Distillation bottoms from the production of phthalic anhydride from naphthalene.
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
100-21-0
0.055
28
471
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
85-44-9
0.055
28
K025
Distillation bottoms from the production of nitrobenzene by the nitration of benzene.
NA
NA
LLEXT fb
SSTRP fb
CARBN; or
CMBST
CMBST
K026
Stripping still tails from the production of methyl ethyl pyridines.
NA
NA
CMBST
CMBST
K027
Centrifuge and distillation residues from the toluene diisocyanate production.
NA
NA
CARBN; or
CMBST
CMBST
K028
Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1-trichloroethane.
1,1-Dichloroethane
75-34-3
0.059
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
NA
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Cadmium
7440-43-9
0.69
NA
Chromium(Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
K029
Waste from the product steam stripper in the production of 1,1,1-trichloroethane.
Chloroform
67-66-3
0.046
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
472
1,1,1-Trichloroethane
71-55-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
K030
Column bodies or heavy ends from the combined production of trichloroethylene and
perchloroethylene.
o-Dichlorobenzene
95-50-1
0.088
NA
p-Dichlorobenzene
106-46-7
0.090
NA
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
NA
30
Pentachlorobenzene
608-93-5
NA
10
Pentachloroethane
76-01-7
NA
6.0
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K031
By-product salts generated in the production of MSMA and cacodylic acid.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K032
Wastewater treatment sludge from the production of chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
Chlordane (α and
χ
isomers)
57-74-9
0.0033
0.26
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
K033
Wastewater and scrub water from the chlorination of cyclopentadiene in the production of
chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K034
Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K035
Wastewater treatment sludges generated in the production of creosote.
Acenaphthene
83-32-9
NA
3.4
Anthracene
120-12-7
NA
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
473
m-Cresol
(difficult to distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from m-
cresol)
106-44-5
0.77
5.6
Dibenz(a,h)anthracene
53-70-3
NA
8.2
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
NA
3.4
Indeno(1,2,3-cd)pyrene
193-39-5
NA
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
K036
Still bottoms from toluene reclamation distillaiton in the production of disulfoton.
Disulfoton
298-04-4
0.017
6.2
K037
Wastewater treatment sludges from the production of disulfoton.
Disulfoton
298-04-4
0.017
6.2
Toluene
108-88-3
0.080
10
K038
Wastewater from the washing and stripping of phorate production.
Phorate
298-02-2
0.021
4.6
K039
Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.
NA
NA
CARBN; or
CMBST
CMBST
K040
Wastewater treatment sludge from the production of phorate.
Phorate
298-02-2
0.021
4.6
K041
Wastewater treatment sludge from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K042
Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production
of 2,4,5-T.
o-Dichlorobenzene
95-50-1
0.088
6.0
474
p-Dichlorobenzene
106-46-7
0.090
6.0
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K043
2,6-Dichlorophenol waste from the production of 2,4-D.
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
187-65-0
0.044
14
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Pentachlorophenol
87-86-5
0.089
7.4
Tetrachloroethylene
127-18-4
0.056
6.0
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
K044
Wastewater treatment sludges from the manufacturing and processing of explosives.
NA
NA
DEACT
DEACT
K045
Spent carbon from the treatment of wastewater containing explosives.
NA
NA
DEACT
DEACT
K046
Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based
initiating compounds.
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K047
Pink or red water from TNT operations.
NA
NA
DEACT
DEACT
475
K048
Dissolved air flotation (DAF) float from the petroleum refining industry.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-33
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
K049
Slop oil emulsion solids from the petroleum refining industry.
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Carbon disulfide
75-15-0
3.8
NA
Chrysene
2218-01-9
0.059
3.4
2,4-Dimethylphenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
476
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
K050
Heat exchanger bundle cleaning sludge from the petroleum refining industry.
Benzo(a)pyrene
50-32-8
0.061
3.4
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
K051
API separator sludge from the petroleum refining industry.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
2218-01-9
0.059
3.4
Di-n-butyl phthalate
105-67-9
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
K052
Tank bottoms (leaded) from the petroleum refining industry.
Benzene
71-43-2
0.14
10
477
Benzo(a)pyrene
50-32-8
0.061
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from m-
cresol)
106-44-5
0.77
5.6
2,4-Dimethylphenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 11 mg/l
TCLP
K060
Ammonia still lime sludge from coking operations.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
Naphthalene
91-20-3
0.059
5.6
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K061
Emission control dust or sludge from the primary production of steel in electric furnaces.
Antimony
7440-36-0
NA
2.1 1.15 mg/l
TCLP
Arsenic
7440-38-2
NA
5.0 mg/l TCLP
Barium
7440-39-3
NA
7.6 21 mg/l
TCLP
Beryllium
7440-41-7
NA
0.014 1.22 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
478
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Mercury
7439-97-6
NA
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Selenium
7782-49-2
NA
0.16 5.7 mg/l
TCLP
Silver
7440-22-4
NA
0.30 0.14 mg/l
TCLP
Thallium
7440-28-0
NA
0.078 0.20 mg/l
TCLP
Zinc
7440-66-6
NA
5.3 4.3 mg/l
TCLP
K062
Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel
industry (SIC Codes 331 and 332).
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
NA
K069
Emission control dust or sludge from secondary lead smelting. - Calcium sulfate (Low Lead)
Subcategory
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K069
Emission control dust or sludge from secondary lead smelting. - Non-Calcium sulfate (High
Lead) Subcategory
NA
NA
NA
RLEAD
K071
K071 (Brine purification muds from the mercury cell process in chlorine production, where
separately prepurified brine is not used) nonwastewaters that are residues from RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
K071
K071 (Brine purification muds from the mercury cell process in chlorine production, where
separately prepurified brine is not used) nonwastewaters that are not residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l TCLP
479
K071
All K071 wastewaters.
Mercury
7439-97-6
0.15
NA
K073
Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using
graphite anodes in chlorine production.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachloroethane
67-72-1
0.055
30
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K083
Distillation bottoms from aniline production.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
Cyclohexanone
108-94-1
0.36
NA
Diphenylamine
(difficult to distinguish from
diphenylnitrosamine)
122-39-4
0.92
13
Diphenylnitrosamine (difficult to
distinguish from diphenylamine)
86-30-6
0.92
13
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
K084
Wastewater treatment sludges generated during the production of veterinary pharmaceuticals
from arsenic or organo-arsenic compounds.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K085
Distillation or fractionation column bottoms from the production of chlorobenzenes.
Benzene
71-43-2
0.14
10
Chlorobenzene
108-90-7
0.057
6.0
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Total PCBs
(sum of all PCB isomers, or all
Aroclors)
1336-36-3
0.10
10
480
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K086
Solvent wastes and sludges, caustic washes and sludges, or water washes and sludges from
cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and
stabilizers containing chromium and lead.
Acetone
67-64-1
0.28
160
Acetophenone
96-86-2
0.010
9.7
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
n-Butyl alcohol
71-36-3
5.6
2.6
Butylbenzyl phthalate
85-68-7
0.017
28
Cyclohexanone
108-94-1
0.36
NA
o-Dichlorobenzene
95-50-1
0.088
6.0
Diethyl phthalate
84-66-2
0.20
28
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
Di-n-octyl phthalate
117-84-0
0.017
28
Ethyl acetate
141-78-6
0.34
33
Ethylbenzene
100-41-4
0.057
10
Methanol
67-56-1
5.6
NA
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methylene chloride
75-09-2
0.089
30
Naphthalene
91-20-3
0.059
5.6
Nitrobenzene
98-95-3
0.068
14
Toluene
108-88-3
0.080
10
1,1,1-Trichloroethane
71-55-6
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K087
Decanter tank tar sludge from coking operations.
Acenaphthylene
208-96-8
0.059
3.4
Benzene
71-43-2
0.14
10
Chrysene
218-01-9
0.059
3.4
Fluoranthene
206-44-0
0.068
3.4
481
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K088
Spent potliners from primary aluminum reduction.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
205-99-2
0.11
6.8
Benzo(k)fluoranthene
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Fluoranthene
206-44-0
0.068
3.4
Indeno(1,2,3-c,d)pyrene
193-39-5
0.0055
3.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Antimony
7440-36-0
1.9
2.1 1.15 mg/l
TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 21 mg/l
TCLP
Beryllium
7440-41-7
0.82
0.014 1.22 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Mercury
7439-97-6
0.15
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
Silver
7440-22-4
0.43
0.30 0.14 mg/l
TCLP
482
Cyanide (Total)
7
57-12-5
1.2
590
Cyanide (Amenable)
7
57-12-5
0.86
30
Fluoride
16984-48-8
35
48 mg/l TCLP
K093
Distillation light ends from the production of phthalic anhydride from ortho-xylene.
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
85-44-9
0.055
28
K094
Distillation bottoms from the production of phthalic anhydride from ortho-xylene.
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
85-44-9
0.055
28
K095
Distillation bottoms from the production of 1,1,1-trichloroethane.
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
0.055
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
K096
Heavy ends from the heavy ends column from the production of 1,1,1-trichloroethane.
m-Dichlorobenzene
541-73-1
0.036
6.0
Pentachloroethane
76-01-7
0.055
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
483
K097
Vacuum stripper discharge from the chlordane chlorinator in the production of chlordane.
Chlordane (α and
χ
isomers)
57-74-9
0.0033
0.26
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K098
Untreated process wastewater from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K099
Untreated wastewater from the production of 2,4-D.
2,4-Dichlorophenoxyacetic acid 94-75-7
0.72
10
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachlorodibenzo-
furans)
NA
0.000063
0.001
K100
Waste leaching solution from acid leaching of emission control dust or sludge from secondary
lead smelting.
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
K101
Distillation tar residues from the distillation of aniline-based compounds in the production of
veterinary pharmaceuticals from arsenic or organo-arsenic compounds.
o-Nitroaniline
88-74-4
0.27
14
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
484
K102
Residue from the use of activated carbon for decolorization in the production of veterinary
pharmaceuticals from arsenic or organo-arsenic compounds.
o-Nitrophenol
88-75-5
0.028
13
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
K103
Process residues from aniline extraction from the production of aniline.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
2,4-Dinitrophenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
K104
Combined wastewater streams generated from nitrobenzene or aniline production.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
2,4-Dinitrophenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K105
Separated aqueous stream from the reactor product washing step in the production of chloro-
benzenes.
Benzene
71-43-2
0.14
10
Chlorobenzene
108-90-7
0.057
6.0
2-Chlorophenol
95-57-8
0.044
5.7
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Phenol
108-95-2
0.039
6.2
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine production)
nonwastewaters that contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
485
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine production)
nonwastewaters that contain less than 260 mg/kg total mercury that are residues from
RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
K106
Other K106 nonwastewaters that contain less than 260 mg/kg total mercury and are not
residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l TCLP
K106
All K106 wastewaters.
Mercury
7439-97-6
0.15
NA
K107
Column bottoms from product separation from the production of 1,1-dimethylhydrazine
(UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K108
Condensed column overheads from product separation and condensed reactor vent gases from
the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K109
Spent filter cartridges from product purification from the production of 1,1-dimethylhydrazine
(UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
486
K110
Condensed column overheads from intermediate separation from the production of 1,1-
dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K111
Product washwaters from the production of dinitrotoluene via nitration of toluene
2,4-Dinitrotoluene
121-1-1
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
K112
Reaction by-product water from the drying column in the production of toluenediamine via
hydrogenation of dinitrotoluene.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K113
Condensed liquid light ends from the purification of toluenediamine in the production of
toluenediamine via hydrogenation of dinitrotoluene.
NA
NA
CARBN; or
CMBST
CMBST
K114
Vicinals from the purification of toluenediamine in the production of toluenediamine via
hydrogenation of dinitrotoluene.
NA
NA
CARBN; or
CMBST
CMBST
K115
Heavy ends from the purification of toluenediamine in the production of toluenediamine via
hydrogenation of dinitrotoluene.
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
NA
NA
CARBN; or
CMBST
CMBST
487
K116
Organic condensate from the solvent recovery column in the production of toluene diisocyanate
via phosgenation of toluenediamine.
NA
NA
CARBN; or
CMBST
CMBST
K117
Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via
bromination of ethene.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K118
Spent absorbent solids from purification of ethylene dibromide in the production of ethylene
dibromide via bromination of ethene.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K123
Process wastewater (including supernates, filtrates, and washwaters) from the production of
ethylenebisdithiocarbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K124
Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its
salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
488
K125
Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithio-
carbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K126
Baghouse dust and floor sweepings in milling and packaging operations from the production or
formulation of ethylenebisdithiocarbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K131
Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of
methyl bromide.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
K132
Spent absorbent and wastewater separator solids from the production of methyl bromide.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
K136
Still bottoms from the purification of ethylene dibromide in the production of ethylene
dibromide via bromination of ethene.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K140
Floor sweepings, off-specification product, and spent filter media from the production of
2,4,6-tribromophenol.
2,4,6-Tribromophenol
118-79-6
0.035
7.4
489
K141
Process residues from the recovery of coal tar, including, but not limited to, collecting sump
residues from the production of coke or the recovery of coke by-products produced from coal.
This listing does not include K087 (decanter tank tar sludge from coking operations).
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-2-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K142
Tar storage tank residues from the production of coke from coal or from the recovery of coke
by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Ideno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K143
Process residues from the recovery of light oil, including, but not limited to, those generated
in stills, decanters, and wash oil recovery units from the recovery of coke by-products
produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
490
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
K144
Wastewater sump residues from light oil refining, including, but not limited to, intercepting or
contamination sump sludges from the recovery of coke by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
K145
Residues from naphthalene collection and recovery operations from the recovery of coke by-
products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Naphthalene
91-20-3
0.059
5.6
K147
Tar storage tank residues from coal tar refining.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
491
K148
Residues from coal tar distillation, including, but not limited to, still bottoms.
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene (difficult
to distinguish from benzo(k)-
fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene (difficult
to distinguish from benzo(b)-
fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K149
Distillation bottoms from the production of
α-
(or methyl-) chlorinated toluenes, ring-
chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional
groups. (This waste does not include still bottoms from the distillations of benzyl chloride.)
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Toluene
108-88-3
0.080
10
K150
Organic residuals, excluding spent carbon adsorbent, from the spent chlorine gas and hydro-
chloric acid recovery processes associated with the production of
α-
(or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these
functional groups.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,1,2,2- Tetrachloroethane
79-34-5
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
492
K151
Wastewater treatment sludges, excluding neutralization and biological sludges, generated
during the treatment of wastewaters from the production of
α-
(or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these
functional groups.
Benzene
71-43-2
0.14
10
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Tetrachloroethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
K156
Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and
decantates) from the production of carbamates and carbamoyl oximes. (This listing does not
apply to wastes generated from the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Acetonitrile
75-05-8
5.6
38
Acetophenone
96-86-2
0.010
9.7
Aniline
62-53-3
0.81
14
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbaryl
63-25-21
0.006
0.14
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Naphthalene
91-20-3
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyridine
110-86-1
0.014
16
Toluene
108-88-3
0.080
10
Triethylamine
121-44-8
0.081
1.5
K157
Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters)
from the production of carbamates and carbamoyl oximes. (This listing does not apply to
wastes generated from the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
493
Chloromethane
74-87-3
0.19
30
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
o-Phenylenediamine
95-54-5
0.056
5.6
Pyridine
110-86-1
0.014
16
Triethylamine
121-44-8
0.081
1.5
K158
Baghouse dusts and filter/separation solids from the production of carbamates and carbamoyl
oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-
propyl-n-butylcarbamate.)
10
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chloroform
67-66-3
0.046
6.0
Methylene chloride
75-09-2
0.089
30
Phenol
108-95-2
0.039
6.2
K159
Organics from the treatment of thiocarbamate wastes.
10
Benzene
71-43-2
0.14
10
Butylate
2008-41-5
0.042
1.4
EPTC (Eptam)
759-94-4
0.042
1.4
Molinate
2212-67-1
0.042
1.4
Pebulate
1114-71-2
0.042
1.4
Vernolate
1929-77-7
0.042
1.4
K161
Purification solids (including filtration, evaporation, and centrifugation solids), baghouse dust
and floor sweepings from the production of dithiocarbamate acids and their salts.
10
Antimony
7440-36-0
1.9
2.1 1.15 mg/l
TCLP
Arsenic
7440-38-2
1.91.4
5.0 mg/l TCLP
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Dithiocarbamates (total)
NA
0.028
28
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
494
K169
Crude oil tank sediment from petroleum refining operations.
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Chrysene
218-01-9
0.059
3.4
Ethyl benzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
81-05-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene (Methyl Benzene)
108-88-3
0.080
10
Xylene(s) (Total)
1330-20-7
0.32
30
K170
Clarified slurry oil sediment from petroleum refining operations.
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Ethyl benzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
3.4
Indeno(1,2,3,-cd)pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
81-05-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene (Methyl Benzene)
108-88-3
0.080
10
Xylene(s) (Total
1330-20-7
0.32
30
K171
Spent hydrotreating catalyst from petroleum refining operations, including guard beds used to
desulfurize feeds to other catalytic reactors. (This listing does not include inert support
media.)
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Chrysene
218-01-9
0.059
3.4
Ethyl benzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
81-05-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene (Methyl Benzene)
108-88-3
0.080
10
Xylene(s) (Total)
1330-20-7
0.32
30
Arsenic
7740-38-2
1.4
5 mg/L TCLP
Nickel
7440-02-0
3.98
11.0 mg/L TCLP
495
Vanadium
7440-62-2
4.3
1.6 mg/L TCLP
Reactive sulfides
NA
DEACT
DEACT
K172
Spent hydrorefining catalyst from petroleum refining operations, including guard beds used to
desulfurize feeds to other catalytic reactors. (This listing does not include inert support
media.)
Benzene
71-43-2
0.14
10
Ethyl benzene
100-41-4
0.057
10
Toluene (Methyl Benzene)
108-88-3
0.080
10
Xylene(s) (Total)
1330-20-7
0.32
30
Antimony
7740-36-0
1.9
1.15 mg/L TCLP
Arsenic
7740-38-2
1.4
5 mg/L TCLP
Nickel
7440-02-0
3.98
11.0 mg/L TCLP
Vanadium
7440-62-2
4.3
1.6 mg/L TCLP
Reactive Sulfides
NA
DEACT
DEACT
P001
Warfarin, & salts, when present at concentrations greater than 0.3 percent
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P002
1-Acetyl-2-thiourea
1-Acetyl-2-thiourea
591-08-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P003
Acrolein
Acrolein
107-02-8
0.29
CMBST
P004
Aldrin
Aldrin
309-00-2
0.021
0.066
P005
Allyl alcohol
Allyl alcohol
107-18-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
496
P006
Aluminum phosphide
Aluminum phosphide
20859-73-8
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
P007
5-Aminomethyl-3-isoxazolol
5-Aminomethyl-3-isoxazolol
2763-96-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P008
4-Aminopyridine
4-Aminopyridine
504-24-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P009
Ammonium picrate
Ammonium picrate
131-74-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P010
Arsenic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P011
Arsenic pentoxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P012
Arsenic trioxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P013
Barium cyanide
Barium
7440-39-3
NA
7.6 21 mg/l
TCLP
497
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P014
Thiophenol (Benzene thiol)
Thiophenol (Benzene thiol)
108-98-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P015
Beryllium dust
Beryllium
7440-41-7
RMETL;or
RTHRM
RMETL; or
RTHRM
P016
Dichloromethyl ether (Bis(chloromethyl)ether)
Dichloromethyl ether
542-88-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P017
Bromoacetone
Bromoacetone
598-31-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P018
Brucine
Brucine
357-57-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P020
2-sec-Butyl-4,6-dinitrophenol (Dinoseb)
2-sec-Butyl-4,6-dinitrophenol
(Dinoseb)
88-85-7
0.066
2.5
P021
Calcium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
498
P022
Carbon disulfide
Carbon disulfide
75-15-0
3.8
CMBST
Carbon disulfide; alternate
6
standard for nonwastewaters
only
75-15-0
NA
4.8 mg/l TCLP
P023
Chloroacetaldehyde
Chloroacetaldehyde
107-20-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P024
p-Chloroaniline
p-Chloroaniline
106-47-8
0.46
16
P026
1-(o-Chlorophenyl)thiourea
1-(o-Chlorophenyl)thiourea
5344-82-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P027
3-Chloropropionitrile
3-Chloropropionitrile
542-76-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P028
Benzyl chloride
Benzyl chloride
100-44-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P029
Copper cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
499
P030
Cyanides (soluble salts and complexes)
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P031
Cyanogen
Cyanogen
460-19-5
CHOXD;
WETOX; or
CMBST
CHOXD;
WETOX; or
CMBST
P033
Cyanogen chloride
Cyanogen chloride
506-77-4
CHOXD;
WETOX; or
CMBST
CHOXD;
WETOX; or
CMBST
P034
2-Cyclohexyl-4,6-dinitrophenol
2-Cyclohexyl-4,6-dinitrophenol
131-89-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P036
Dichlorophenylarsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P037
Dieldrin
Dieldrin
60-57-1
0.017
0.13
P038
Diethylarsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P039
Disulfoton
Disulfoton
298-04-4
0.017
6.2
P040
O,O-Diethyl-O-pyrazinyl-phosphorothioate
O,O-Diethyl-O-pyrazinyl-
phosphorothioate
297-97-2
CARBN; or
CMBST
CMBST
500
P041
Diethyl-p-nitrophenyl phosphate
Diethyl-p-nitrophenyl phosphate 311-45-5
CARBN; or
CMBST
CMBST
P042
Epinephrine
Epinephrine
51-43-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P043
Diisopropylfluorophosphate (DFP)
Diisopropylfluorophosphate
(DFP)
55-91-4
CARBN; or
CMBST
CMBST
P044
Dimethoate
Dimethoate
60-51-5
CARBN; or
CMBST
CMBST
P045
Thiofanox
Thiofanox
39196-18-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P046
α
,
α-Dimethylphenethylamine
α
,
α-Dimethylphenethylamine
122-09-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P047
4,6-Dinitro-o-cresol
4,6-Dinitro-o-cresol
543-52-1
0.28
160
501
P047
4,6-Dinitro-o-cresol salts
NA
NA
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P048
2,4-Dinitrophenol
2,4-Dinitrophenol
51-28-5
0.12
160
P049
Dithiobiuret
Dithiobiuret
541-53-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P050
Endosulfan
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
P051
Endrin
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
P054
Aziridine
Aziridine
151-56-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P056
Fluorine
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb
NEUTR
502
P057
Fluoroacetamide
Fluoroacetamide
640-19-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P058
Fluoroacetic acid, sodium salt
Fluoroacetic acid, sodium salt
62-74-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P059
Heptachlor
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
P060
Isodrin
Isodrin
465-73-6
0.021
0.066
P062
Hexaethyl tetraphosphate
Hexaethyl tetraphosphate
757-58-4
CARBN; or
CMBST
CMBST
P063
Hydrogen cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P064
Isocyanic acid, ethyl ester
Isocyanic acid, ethyl ester
624-83-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P065
P065 (mercury fulminate) nonwastewaters, regardless of their total mercury content, that are
not incinerator residues or are not residues from RMERC.
Mercury
7439-97-6
NA
IMERC
503
P065
P065 (mercury fulminate) nonwastewaters that are either incinerator residues or are residues
from RMERC; and contain greater than or equal to 260 mg/kg total mercury.
Mercury
7339-97-6
NA
RMERC
P065
P065 (mercury fulminate) nonwastewaters that are residues from RMERC and contain less
than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
P065
P065 (mercury fulminate) nonwastewaters that are incinerator residues and contain less than
260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l TCLP
P065
All P065 (mercury fulminate) wastewaters.
Mercury
7439-97-6
0.15
NA
P066
Methomyl
Methomyl
16752-77-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P067
2-Methyl-aziridine
2-Methyl-aziridine
75-55-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P068
Methyl hydrazine
Methyl hydrazine
60-34-4
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED, or
CMBST
504
P069
2-Methyllactonitrile
2-Methyllactonitrile
75-86-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P070
Aldicarb
Aldicarb
116-06-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P071
Methyl parathion
Methyl parathion
298-00-0
0.014
4.6
P072
1-Naphthyl-2-thiourea
1-Naphthyl-2-thiourea
86-88-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P073
Nickel carbonyl
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
P074
Nickel cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Nickel
7440-02-0
3.98
5.0 11 mg/l
TCLP
P075
Nicotine and salts
Nicotine and salts
54-11-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
505
P076
Nitric oxide
Nitric oxide
10102-43-9
ADGAS
ADGAS
P077
p-Nitroaniline
p-Nitroaniline
100-01-6
0.028
28
P078
Nitrogen dioxide
Nitrogen dioxide
10102-44-0
ADGAS
ADGAS
P081
Nitroglycerin
Nitroglycerin
55-63-0
CHOXD;
CHRED;
CARBN; BIODG
or CMBST
CHOXD;
CHRED; or
CMBST
P082
N-Nitrosodimethylamine
N-Nitrosodimethylamine
62-75-9
0.40
2.3
P084
N-Nitrosomethylvinylamine
N-Nitrosomethylvinylamine
4549-40-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P085
Octamethylpyrophosphoramide
Octamethylpyrophosphoramide
152-16-9
CARBN; or
CMBST
CMBST
P087
Osmium tetroxide
Osmium tetroxide
20816-12-0
RMETL; or
RTHRM
RMETL; or
RTHRM
506
P088
Endothall
Endothall
145-73-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P089
Parathion
Parathion
56-38-2
0.014
4.6
P092
P092 (phenyl mercuric acetate) nonwastewaters, regardless of their total mercury content, that
are not incinerator residues or are not residues from RMERC.
Mercury
7439-97-6
NA
IMERC; or
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are either incinerator residues or are
residues from RMERC; and still contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are residues from RMERC and contain
less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
P092
P092 (phenyl mercuric acetate) nonwastewaters that are incinerator residues and contain less
than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l TCLP
P092
All P092 (phenyl mercuric acetate) wastewaters.
Mercury
7439-97-6
0.15
NA
P093
Phenylthiourea
Phenylthiourea
103-85-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
507
P094
Phorate
Phorate
298-02-2
0.021
4.6
P095
Phosgene
Phosgene
75-44-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P096
Phosphine
Phosphine
7803-51-2
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
P097
Famphur
Famphur
52-85-7
0.017
15
P098
Potassium cyanide.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P099
Potassium silver cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 0.14 mg/l
TCLP
P101
Ethyl cyanide (Propanenitrile)
Ethyl cyanide (Propanenitrile)
107-12-0
0.24
360
P102
Propargyl alcohol
Propargyl alcohol
107-19-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
508
P103
Selenourea
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
P104
Silver cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 0.14 mg/l
TCLP
P105
Sodium azide
Sodium azide
26628-22-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P106
Sodium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P108
Strychnine and salts
Strychnine and salts
57-24-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P109
Tetraethyldithiopyrophosphate
Tetraethyldithiopyrophosphate
3689-24-5
CARBN; or
CMBST
CMBST
P110
Tetraethyl lead
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
509
P111
Tetraethylpyrophosphate
Tetraethylpyrophosphate
107-49-3
CARBN; or
CMBST
CMBST
P112
Tetranitromethane
Tetranitromethane
509-14-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P113
Thallic oxide
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P114
Thallium selenite
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
P115
Thallium (I) sulfate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P116
Thiosemicarbazide
Thiosemicarbazide
79-19-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P118
Trichloromethanethiol
Trichloromethanethiol
75-70-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
510
P119
Ammonium vanadate
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P120
Vanadium pentoxide
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P121
Zinc cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P122
Zinc phosphide Zn3P2, when present at concentrations greater than 10 percent
Zinc Phosphide
1314-84-7
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
P123
Toxaphene
Toxaphene
8001-35-2
0.0095
2.6
P127
Carbofuran
10
Carbofuran
1563-66-2
0.006
0.14
P128
Mexacarbate
10
Mexacarbate
315-18-4
0.056
1.4
P185
Tirpate
10
Tirpate
26419-73-8
0.056
0.28
P188
Physostigimine salicylate
10
Physostigmine salicylate
57-64-7
0.056
1.4
P189
Carbosulfan
10
Carbosulfan
55285-14-8
0.028
1.4
511
P190
Metolcarb
10
Metolcarb
1129-41-5
0.056
1.4
P191
Dimetilan
10
Dimetilan
644-64-4
0.056
1.4
P192
Isolan
10
Isolan
119-38-0
0.056
1.4
P194
Oxamyl
10
Oxamyl
23135-22-0
0.056
0.28
P196
Manganese dimethyldithiocarbamates (total)
10
Dithiocarbamates (total)
NA
0.028
28
P197
Formparanate
10
Formparanate
17702-57-7
0.056
1.4
P198
Formetanate hydrochloride
10
Formetanate hydrochloride
23422-53-9
0.056
1.4
P199
Methiocarb
10
Methiocarb
2032-65-7
0.056
1.4
P201
Promecarb
10
Promecarb
2631-37-0
0.056
1.4
P202
m-Cumenyl methylcarbamate
10
m-Cumenyl methylcarbamate
64-00-6
0.056
1.4
P203
Aldicarb sulfone
10
Aldicarb sulfone
1646-88-4
0.056
0.28
512
P204
Physostigmine
10
Physostigmine
57-47-6
0.056
1.4
P205
Ziram
10
Dithiocarbamates (total)
NA
0.028
28
U001
Acetaldehyde
Acetaldehyde
75-07-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U002
Acetone
Acetone
67-64-1
0.28
160
U003
Acetonitrile
Acetonitrile
75-05-8
5.6
CMBST
Acetonitrile; alternate
6
standard
for nonwastewaters only
75-05-8
NA
38
U004
Acetophenone
Acetophenone
98-86-2
0.010
9.7
U005
2-Acetylaminofluorene
2-Acetylaminofluorene
53-96-3
0.059
140
U006
Acetyl chloride
Acetyl chloride
75-36-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
513
U007
Acrylamide
Acrylamide
79-06-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U008
Acrylic acid
Acrylic acid
79-10-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U009
Acrylonitrile
Acrylonitrile
107-13-1
0.24
84
U010
Mitomycin C
Mitomycin C
50-07-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U011
Amitrole
Amitrole
61-82-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U012
Aniline
Aniline
62-53-3
0.81
14
U014
Auramine
Auramine
492-80-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
514
U015
Azaserine
Azaserine
115-02-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U016
Benz(c)acridine
Benz(c)acridine
225-51-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U017
Benzal chloride
Benzal chloride
98-87-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U018
Benz(a)anthracene
Benz(a)anthracene
56-55-3
0.059
3.4
U019
Benzene
Benzene
71-43-2
0.14
10
U020
Benzenesulfonyl chloride
Benzenesulfonyl chloride
98-09-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U021
Benzidine
Benzidine
92-87-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
515
U022
Benzo(a)pyrene
Benzo(a)pyrene
50-32-8
0.061
3.4
U023
Benzotrichloride
Benzotrichloride
98-07-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U024
bis(2-Chloroethoxy)methane
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
U025
bis(2-Chloroethyl)ether
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
U026
Chlornaphazine
Chlornaphazine
494-03-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U027
bis(2-Chloroisopropyl)ether
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
U028
bis(2-Ethylhexyl)phthalate
bis(2-Ethylhexyl)phthalate
117-81-7
0.28
28
U029
Methyl bromide (Bromomethane)
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
U030
4-Bromophenyl phenyl ether
4-Bromophenyl phenyl ether
101-55-3
0.055
15
516
U031
n-Butyl alcohol
n-Butyl alcohol
71-36-3
5.6
2.6
U032
Calcium chromate
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
U033
Carbon oxyfluoride
Carbon oxyfluoride
353-50-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U034
Trichloroacetaldehyde (Chloral)
Trichloroacetaldehyde (Chloral) 75-87-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U035
Chlorambucil
Chlorambucil
305-03-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U036
Chlordane
Chlordane (α and
χ
isomers)
57-74-9
0.0033
0.26
U037
Chlorobenzene
Chlorobenzene
108-90-7
0.057
6.0
U038
Chlorobenzilate
Chlorobenzilate
510-15-6
0.10
CMBST
U039
p-Chloro-m-cresol
p-Chloro-m-cresol
59-50-7
0.018
14
517
U041
Epichlorohydrin (1-Chloro-2,3-epoxypropane)
Epichlorohydrin (1-Chloro-2,3-
epoxypropane)
106-89-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U042
2-Chloroethyl vinyl ether
2-Chloroethyl vinyl ether
110-75-8
0.062
CMBST
U043
Vinyl chloride
Vinyl chloride
75-01-4
0.27
6.0
U044
Chloroform
Chloroform
67-66-3
0.046
6.0
U045
Chloromethane (Methyl chloride)
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
U046
Chloromethyl methyl ether
Chloromethyl methyl ether
107-30-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U047
2-Chloronaphthalene
2-Chloronaphthalene
91-58-7
0.055
5.6
U048
2-Chlorophenol
2-Chlorophenol
95-57-8
0.044
5.7
518
U049
4-Chloro-o-toluidine hydrochloride
4-Chloro-o-toluidine hydro-
chloride
3165-93-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U050
Chrysene
Chrysene
218-01-9
0.059
3.4
U051
Creosote
Naphthalene
91-20-3
0.059
5.6
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
U052
Cresols (Cresylic acid)
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to distinguish
from p-cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to distinguish
from m-cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers (Cresylic
acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88
11.2
U053
Crotonaldehyde
Crotonaldehyde
4170-30-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
519
U055
Cumene
Cumene
98-82-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U056
Cyclohexane
Cyclohexane
110-82-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U057
Cyclohexanone
Cyclohexanone
108-94-1
0.36
CMBST
Cyclohexanone; alternate
6
standard for nonwastewaters
only
108-94-1
NA
0.75 mg/l TCLP
U058
Cyclophosphamide
Cyclophosphamide
50-18-0
CARBN; or
CMBST
CMBST
U059
Daunomycin
Daunomycin
20830-81-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U060
DDD
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
U061
DDT
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
520
p,p’-DDE
72-55-9
0.031
0.087
U062
Diallate
Diallate
2303-16-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U063
Dibenz(a,h)anthracene
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
U064
Dibenz(a,i)pyrene
Dibenz(a,i)pyrene
189-55-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U066
1,2-Dibromo-3-chloropropane
1,2-Dibromo-3-chloropropane
96-12-8
0.11
15
U067
Ethylene dibromide (1,2-Dibromoethane)
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
U068
Dibromomethane
Dibromomethane
74-95-3
0.11
15
U069
Di-n-butyl phthalate
Di-n-butyl phthalate
84-74-2
0.057
28
U070
o-Dichlorobenzene
o-Dichlorobenzene
95-50-1
0.088
6.0
U071
m-Dichlorobenzene
m-Dichlorobenzene
541-73-1
0.036
6.0
521
U072
p-Dichlorobenzene
p-Dichlorobenzene
106-46-7
0.090
6.0
U073
3,3'-Dichlorobenzidine
3,3'-Dichlorobenzidine
91-94-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U074
1,4-Dichloro-2-butene
cis-1,4-Dichloro-2-butene
1476-11-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
trans-1,4-Dichloro-2-butene
764-41-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U075
Dichlorodifluoromethane
Dichlorodifluoromethane
75-71-8
0.23
7.2
U076
1,1-Dichloroethane
1,1-Dichloroethane
75-34-3
0.059
6.0
U077
1,2-Dichloroethane
1,2-Dichloroethane
107-06-2
0.21
6.0
U078
1,1-Dichloroethylene
1,1-Dichloroethylene
75-35-4
0.025
6.0
U079
1,2-Dichloroethylene
trans-1,2-Dichloroethylene
156-60-5
0.054
30
U080
Methylene chloride
Methylene chloride
75-09-2
0.089
30
522
U081
2,4-Dichlorophenol
2,4-Dichlorophenol
120-83-2
0.044
14
U082
2,6-Dichlorophenol
2,6-Dichlorophenol
87-65-0
0.044
14
U083
1,2-Dichloropropane
1,2-Dichloropropane
78-87-5
0.85
18
U084
1,3-Dichloropropylene
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
U085
1,2:3,4-Diepoxybutane
1,2:3,4-Diepoxybutane
1464-53-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U086
N,N’-Diethylhydrazine
N,N’-Diethylhydrazine
1615-80-1
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U087
O,O-Diethyl-S-methyldithiophosphate
O,O-Diethyl-S-methyldithio-
phosphate
3288-58-2
CARBN; or
CMBST
CMBST
U088
Diethyl phthalate
Diethyl phthalate
84-66-2
0.20
28
523
U089
Diethyl stilbestrol
Diethyl stilbestrol
56-53-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U090
Dihydrosafrole
Dihydrosafrole
94-58-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U091
3,3'-Dimethoxybenzidine
3,3'-Dimethoxybenzidine
119-90-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U092
Dimethylamine
Dimethylamine
124-40-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U093
p-Dimethylaminoazobenzene
p-Dimethylaminoazobenzene
60-11-7
0.13
CMBST
U094
7,12-Dimethylbenz(a)anthracene
7,12-Dimethylbenz(a)anthracene 57-97-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U095
3,3'-Dimethylbenzidine
3,3'-Dimethylbenzidine
119-93-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
524
U096
α
,
α-Dimethyl
benzyl hydroperoxide
α
,
α-Dimethyl
benzyl hydro-
peroxide
80-15-9
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U097
Dimethylcarbamoyl chloride
Dimethylcarbamoyl chloride
79-44-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U098
1,1-Dimethylhydrazine
1,1-Dimethylhydrazine
57-14-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U099
1,2-Dimethylhydrazine
1,2-Dimethylhydrazine
540-73-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U101
2,4-Dimethylphenol
2,4-Dimethylphenol
105-67-9
0.036
14
U102
Dimethyl phthalate
Dimethyl phthalate
131-11-3
0.047
28
525
U103
Dimethyl sulfate
Dimethyl sulfate
77-78-1
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U105
2,4-Dinitrotoluene
2,4-Dinitrotoluene
121-14-2
0.32
140
U106
2,6-Dinitrotoluene
2,6-Dinitrotoluene
606-20-2
0.55
28
U107
Di-n-octyl phthalate
Di-n-octyl phthalate
117-84-0
0.017
28
U108
1,4-Dioxane
1,4-Dioxane
123-91-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
1,4-Dioxane; alternate
6
standard
for nonwastewaters only
123-91-1
NA12.0
170
U109
1,2-Diphenylhydrazine
1,2-Diphenylhydrazine
122-66-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
1,2-Diphenylhydrazine;
alternate
6
standard for
wastewaters only
122-66-7
0.087
NA
526
U110
Dipropylamine
Dipropylamine
142-84-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U111
Di-n-propylnitrosamine
Di-n-propylnitrosamine
621-64-7
0.40
14
U112
Ethyl acetate
Ethyl acetate
141-78-6
0.34
33
U113
Ethyl acrylate
Ethyl acrylate
140-88-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U114
Ethylenebisdithiocarbamic acid salts and esters
Ethylenebisdithiocarbamic acid
111-54-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U115
Ethylene oxide
Ethylene oxide
75-21-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CHOXD; or
CMBST
Ethylene oxide; alternate
6
standard for wastewaters only
75-21-8
0.12
NA
U116
Ethylene thiourea
Ethylene thiourea
96-45-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
527
U117
Ethyl ether
Ethyl ether
60-29-7
0.12
160
U118
Ethyl methacrylate
Ethyl methacrylate
97-63-2
0.14
160
U119
Ethyl methane sulfonate
Ethyl methane sulfonate
62-50-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U120
Fluoranthene
Fluoranthene
206-44-0
0.068
3.4
U121
Trichloromonofluoromethane
Trichloromonofluoromethane
75-69-4
0.020
30
U122
Formaldehyde
Formaldehyde
50-00-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U123
Formic acid
Formic acid
64-18-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U124
Furan
Furan
110-00-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
528
U125
Furfural
Furfural
98-01-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U126
Glycidylaldehyde
Glycidylaldehyde
765-34-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U127
Hexachlorobenzene
Hexachlorobenzene
118-74-1
0.055
10
U128
Hexachlorobutadiene
Hexachlorobutadiene
87-68-3
0.055
5.6
U129
Lindane
α-BHC
319-84-6
0.00014
0.066
β-BHC
319-85-7
0.00014
0.066
δ-BHC
319-86-8
0.023
0.066
χ-BHC
(Lindane)
58-89-9
0.0017
0.066
U130
Hexachlorocyclopentadiene
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
U131
Hexachloroethane
Hexachloroethane
67-72-1
0.055
30
U132
Hexachlorophene
Hexachlorophene
70-30-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
529
U133
Hydrazine
Hydrazine
302-01-2
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U134
Hydrogen fluoride
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb
NEUTR; or
NEUTR
U135
Hydrogen sulfide
Hydrogen sulfide
7783-06-4
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U136
Cacodylic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
U137
Indeno(1,2,3-c,d)pyrene
Indeno(1,2,3-c,d)pyrene
193-39-5
0.0055
3.4
U138
Iodomethane
Iodomethane
74-88-4
0.19
65
U140
Isobutyl alcohol
Isobutyl alcohol
78-83-1
5.6
170
U141
Isosafrole
Isosafrole
120-58-1
0.081
2.6
U142
Kepone
Kepone
143-50-8
0.0011
0.13
530
U143
Lasiocarpine
Lasiocarpine
303-34-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U144
Lead acetate
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
U145
Lead phosphate
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
U146
Lead subacetate
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
U147
Maleic anhydride
Maleic anhydride
108-31-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U148
Maleic hydrazide
Maleic hydrazide
123-33-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U149
Malononitrile
Malononitrile
109-77-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
531
U150
Melphalan
Melphalan
148-82-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U151
U151 (mercury) nonwastewaters that contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury and that are
residues from RMERC only.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury and that are
not residues from RMERC only.
Mercury
7439-97-6
NA
0.025 mg/l TCLP
U151
All U151 (mercury) wastewater.
Mercury
7439-97-6
0.15
NA
U151
Element Mercury Contaminated with Radioactive Materials
Mercury
7439-97-6
NA
AMLGM
U152
Methacrylonitrile
Methacrylonitrile
126-98-7
0.24
84
U153
Methanethiol
Methanethiol
74-93-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
532
U154
Methanol
Methanol
67-56-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
Methanol; alternate
6
set of
standards for both wastewaters
and nonwastewaters
67-56-1
5.6
0.75 mg/l TCLP
U155
Methapyrilene
Methapyrilene
91-80-5
0.081
1.5
U156
Methyl chlorocarbonate
Methyl chlorocarbonate
79-22-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U157
3-Methylcholanthrene
3-Methylcholanthrene
56-49-5
0.0055
15
U158
4,4'-Methylene bis(2-chloroaniline)
4,4'-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
U159
Methyl ethyl ketone
Methyl ethyl ketone
78-93-3
0.28
36
U160
Methyl ethyl ketone peroxide
Methyl ethyl ketone peroxide
1338-23-4
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U161
Methyl isobutyl ketone
Methyl isobutyl ketone
108-10-1
0.14
33
533
U162
Methyl methacrylate
Methyl methacrylate
80-62-6
0.14
160
U163
N-Methyl-N’-nitro-N-nitrosoguanidine
N-Methyl-N’-nitro-N-nitroso-
guanidine
70-25-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U164
Methylthiouracil
Methylthiouracil
56-04-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U165
Naphthalene
Naphthalene
91-20-3
0.059
5.6
U166
1,4-Naphthoquinone
1,4-Naphthoquinone
130-15-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U167
1-Naphthylamine
1-Naphthylamine
134-32-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U168
2-Naphthylamine
2-Naphthylamine
91-59-8
0.52
CMBST
U169
Nitrobenzene
Nitrobenzene
98-95-3
0.068
14
534
U170
p-Nitrophenol
p-Nitrophenol
100-02-7
0.12
29
U171
2-Nitropropane
2-Nitropropane
79-46-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U172
N-Nitrosodi-n-butylamine
N-Nitrosodi-n-butylamine
924-16-3
0.40
17
U173
N-Nitrosodiethanolamine
N-Nitrosodiethanolamine
1116-54-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U174
N-Nitrosodiethylamine
N-Nitrosodiethylamine
55-18-5
0.40
28
U176
N-Nitroso-N-ethylurea
N-Nitroso-N-ethylurea
759-73-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U177
N-Nitroso-N-methylurea
N-Nitroso-N-methylurea
684-93-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
535
U178
N-Nitroso-N-methylurethane
N-Nitroso-N-methylurethane
615-53-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U179
N-Nitrosopiperidine
N-Nitrosopiperidine
100-75-4
0.013
35
U180
N-Nitrosopyrrolidine
N-Nitrosopyrrolidine
930-55-2
0.013
35
U181
5-Nitro-o-toluidine
5-Nitro-o-toluidine
99-55-8
0.32
28
U182
Paraldehyde
Paraldehyde
123-63-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U183
Pentachlorobenzene
Pentachlorobenzene
608-93-5
0.055
10
U184
Pentachloroethane
Pentachloroethane
76-01-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
Pentachloroethane; alternate
6
standards for both wastewaters
and nonwastewaters
76-01-7
0.055
6.0
U185
Pentachloronitrobenzene
Pentachloronitrobenzene
82-68-8
0.055
4.8
536
U186
1,3-Pentadiene
1,3-Pentadiene
504-60-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U187
Phenacetin
Phenacetin
62-44-2
0.081
16
U188
Phenol
Phenol
108-95-2
0.039
6.2
U189
Phosphorus sulfide
Phosphorus sulfide
1314-80-3
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U190
Phthalic anhydride
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride (measured as
Phthalic acid or Terephthalic
acid)
85-44-9
0.055
28
U191
2-Picoline
2-Picoline
109-06-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U192
Pronamide
Pronamide
23950-58-5
0.093
1.5
537
U193
1,3-Propane sultone
1,3-Propane sultone
1120-71-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U194
n-Propylamine
n-Propylamine
107-10-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U196
Pyridine
Pyridine
110-86-1
0.014
16
U197
p-Benzoquinone
p-Benzoquinone
106-51-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U200
Reserpine
Reserpine
50-55-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U201
Resorcinol
Resorcinol
108-46-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U202
Saccharin and salts
Saccharin
81-07-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
538
U203
Safrole
Safrole
94-59-7
0.081
22
U204
Selenium dioxide
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
U205
Selenium sulfide
Selenium
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
U206
Streptozotocin
Streptozotocin
18883-66-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U207
1,2,4,5-Tetrachlorobenzene
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
U208
1,1,1,2-Tetrachloroethane
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
U209
1,1,2,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
79-34-5
0.057
6.0
U210
Tetrachloroethylene
Tetrachloroethylene
127-18-4
0.056
6.0
U211
Carbon tetrachloride
Carbon tetrachloride
56-23-5
0.057
6.0
539
U213
Tetrahydrofuran
Tetrahydrofuran
109-99-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U214
Thallium (I) acetate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U215
Thallium (I) carbonate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U216
Thallium (I) chloride
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U217
Thallium (I) nitrate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U218
Thioacetamide
Thioacetamide
62-55-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U219
Thiourea
Thiourea
62-56-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U220
Toluene
Toluene
108-88-3
0.080
10
540
U221
Toluenediamine
Toluenediamine
25376-45-8
CARBN; or
CMBST
CMBST
U222
o-Toluidine hydrochloride
o-Toluidine hydrochloride
636-21-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U223
Toluene diisocyanate
Toluene diisocyanate
26471-62-5
CARBN; or
CMBST
CMBST
U225
Bromoform (Tribromomethane)
Bromoform (Tribromomethane) 75-25-2
0.63
15
U226
1,1,1-Trichloroethane
1,1,1-Trichloroethane
71-55-6
0.054
6.0
U227
1,1,2-Trichloroethane
1,1,2-Trichloroethane
79-00-5
0.054
6.0
U228
Trichloroethylene
Trichloroethylene
79-01-6
0.054
6.0
U234
1,3,5-Trinitrobenzene
1,3,5-Trinitrobenzene
99-35-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U235
tris-(2,3-Dibromopropyl)-phosphate
tris-(2,3-Dibromopropyl)-
phosphate
126-72-7
0.11
0.10
541
U236
Trypan Blue
Trypan Blue
72-57-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U237
Uracil mustard
Uracil mustard
66-75-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U238
Urethane (Ethyl carbamate)
Urethane (Ethyl carbamate)
51-79-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U239
Xylenes
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
U240
2,4-D (2,4-Dichlorophenoxyacetic acid)
2,4-D (2,4-Dichloro-
phenoxyacetic acid)
94-75-7
0.72
10
2,4-D (2,4-Dichloro-
phenoxyacetic acid) salts and
esters
NA
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U243
Hexachloropropylene
Hexachloropropylene
1888-71-7
0.035
30
542
U244
Thiram
Thiram
137-26-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U246
Cyanogen bromide
Cyanogen bromide
506-68-3
CHOXD;
WETOX; or
CMBST
CHOXD;
WETOX; or
CMBST
U247
Methoxychlor
Methoxychlor
72-43-5
0.25
0.18
U248
Warfarin, & salts, when present at concentrations of 0.3 percent or less
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U249
Zinc phosphide, Zn3P2, when present at concentrations of 10 percent or less
Zinc Phosphide
1314-84-7
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U271
Benomyl
10
Benomyl
17804-35-2
0.056
1.4
U278
Bendiocarb
10
Bendiocarb
22781-23-3
0.056
1.4
U279
Carbaryl
10
Carbaryl
63-25-2
0.006
0.14
U280
Barban
10
Barban
101-27-9
0.056
1.4
543
U328
o-Toluidine
o-Toluidine
95-53-4
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
U353
p-Toluidine
p-Toluidine
106-49-0
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
U359
2-Ethoxyethanol
2-Ethoxyethanol
110-80-5
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
U364
Bendiocarb phenol
10
Bendiocarb phenol
22961-82-6
0.056
1.4
U367
Carbofuran phenol
10
Carbofuran phenol
1563-38-8
0.056
1.4
U372
Carbendazim
10
Carbendazim
10605-21-7
0.056
1.4
U373
Propham
10
Propham
122-42-9
0.056
1.4
544
U387
Prosulfocarb
10
Prosulfocarb
52888-80-9
0.042
1.4
U389
Triallate
10
Triallate
2303-17-5
0.042
1.4
U394
A2213
10
A2213
30558-43-1
0.042
1.4
U395
Diethylene glycol, dicarbamate
10
Diethylene glycol, dicarbamate
5952-26-1
0.056
1.4
U404
Triethylamine
10
Triethylamine
101-44-8
0.081
1.5
U408
2,4,6-Tribromophenol
2,4,6-Tribromophenol
118-79-6
0.035
7.4
U409
Thiophanate-methyl
10
Thiophanate-methyl
23564-05-8
0.056
1.4
U410
Thiodicarb
10
Thiodicarb
59669-26-0
0.019
1.4
U411
Propoxur
10
Propoxur
114-26-1
0.056
1.4
Notes:
1
The waste descriptions provided in this table do not replace waste descriptions in 35 Ill.
Adm. Code 721. Descriptions of Treatment or Regulatory Subcategories are provided,
as needed, to distinguish between applicability of different standards.
2
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts or esters, the
CAS number is given for the parent compound only.
545
3
Concentration standards for wastewaters are expressed in mg/l and are based on
analysis of composite samples.
4
All treatment standards expressed as a Technology Code or combination of Technology
Codes are explained in detail in 35 Ill. Adm. Code 728.Table C of this Part,
“Technology Codes and Descriptions of Technology-Based Standards”. “fb” inserted
between waste codes denotes “followed by”, so that the first-listed treatment is
followed by the second-listed treatment. “;” separates alternative treatment schemes.
5
Except for Metals (EP or TCLP) and Cyanides (Total and Amenable) the
nonwastewater treatment standards expressed as a concentration were established, in
part, based upon incineration in units operated in accordance with the technical
requirements of 35 Ill. Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O
or based upon combustion in fuel substitution units operating in accordance with
applicable technical requirements. A facility may comply with these treatment
standards according to provisions in 35 Ill. Adm. Code 728.140(d). All concentration
standards for nonwastewaters are based on analysis of grab samples.
6
Where an alternate treatment standard or set of alternate standards has been indicated, a
facility may comply with this alternate standard, but only for the Treatment or
Regulatory Subcategory or physical form (i.e., wastewater or nonwastewater) specified
for that alternate standard.
7
Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to be analyzed
using Method 9010 or 9012, found in “Test Methods for Evaluating Solid Waste,
Physical or Chemical Methods”, USEPA Publication SW-846, incorporated by
reference in 35 Ill. Adm. Code 720.111, with a sample size of 10 grams and a
distillation time of one hour and 15 minutes.
8
These wastes, when rendered nonhazardous and then subsequently managed in CWA or
CWA-equivalent systems, are not subject to treatment standards. (See Section
728.101(c)(3) and (c)(4).)
9
These wastes, when rendered nonhazardous and then subsequently injected in a Class I
SDWA well, are not subject to treatment standards. (See 35 Ill. Adm. Code
738.101(d).)
10
This footnote corresponds with note 10 to the table to 40 CFR 268.40, which has
already expired by its own terms. This statement maintains structural consistency with
the federal regulations.
11
For these wastes, the definition of CMBST is limited to any of the following that have
obtained a determination of equivalent treatment under Section 728.142(b): (1)
combustion units operating under 35 Ill. Adm. Code 726, (2) combustion units
546
permitted under 35 Ill. Adm. Code 724.Subpart O, or (3) combustion units operating
under 35 Ill. Adm. Code 725.Subpart O.
BOARD NOTE: Derived from table to 40 CFR 268.40 (1997), as amended at 63 Fed. Reg.
24626 (May 4, 1998), 63 Fed. Reg. 28643 (May 26, 1998), and 63 Fed. Reg. 35149 (June
29, 1998).
NA
means not applicable.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table U Universal Treatment Standards (UTS)
Regulated Constituent-
Common Name
CAS
1
No.
Wastewater
Standard
Concentration (in
mg/l
2
)
Nonwastewater
Standard
Concentration (in
mg/kg
3
unless
noted as “mg/l
TCLP”)
A2213
6
30558-43-1
0.042
1.4
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
38
Acetophenone
96-86-2
0.010
9.7
2-Acetylaminofluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylamide
79-06-1
19
23
Acrylonitrile
107-13-1
0.24
84
Aldicarb sulfone
6
1646-88-4
0.056
0.28
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
α-BHC
319-84-6
0.00014
0.066
β-BHC
319-85-7
0.00014
0.066
δ-BHC
319-86-8
0.023
0.066
χ-BHC
58-89-9
0.0017
0.066
Barban
6
101-27-9
0.056
1.4
Bendiocarb
6
22781-23-3
0.056
1.4
Bendiocarb phenol
6
22961-82-6
0.056
1.4
Benomyl
6
17804-35-2
0.056
1.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
547
Benzene
71-43-2
0.14
10
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloromethane
75-27-4
0.35
15
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
4-Bromophenyl phenyl ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butylate
6
2008-41-5
0.042
1.4
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitro-
phenol (Dinoseb)
88-85-7
0.066
2.5
Carbaryl
6
63-25-2
0.006
0.14
Carbenzadim
6
10605-21-7
0.056
1.4
Carbofuran
6
1563-66-2
0.006
0.14
Carbofuran phenol
6
1563-38-8
0.056
1.4
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Carbon tetrachloride
56-23-5
0.057
6.0
Carbosulfan
6
55285-14-8
0.028
1.4
Chlordane (α and
χ
isomers)
57-74-9
0.0033
0.26
p-Chloroaniline
106-47-8
0.46
16
Chlorobenzene
108-90-7
0.057
6.0
Chlorobenzilate
510-15-6
0.10
NA
2-Chloro-1,3-butadiene
126-99-8
0.057
0.28
p-Chloro-m-cresol
59-50-7
0.018
14
Chlorodibromomethane
124-48-1
0.057
15
Chloroethane
75-00-3
0.27
6.0
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
2-Chloroethyl vinyl ether
110-75-8
0.062
NA
Chloroform
67-66-3
0.046
6.0
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
2-Chloronaphthalene
91-58-7
0.055
5.6
2-Chlorophenol
95-57-8
0.044
5.7
3-Chloropropylene
107-05-1
0.036
30
Chrysene
218-01-9
0.059
3.4
548
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to
distinguish from p-cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to
distinguish from m-cresol)
106-44-5
0.77
5.6
m-Cumenyl methyl
-
carbamate
6
64-00-6
0.056
1.4
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
p,p’-DDE
72-55-9
0.031
0.087
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Dibenz(a,e)pyrene
192-65-4
0.061
NA
1,2-Dibromo-3-chloro-
propane
96-12-8
0.11
15
1,2-Dibromoethane/Ethylene
dibromide
106-93-4
0.028
15
Dibromomethane
74-95-3
0.11
15
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Dichlorodifluoromethane
75-71-8
0.23
7.2
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
87-65-0
0.044
14
2,4-Dichlorophenoxyacetic
acid/2,4-D
94-75-7
0.72
10
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethylene glycol,
dicarbamate
6
5952-26-1
0.056
1.4
Diethyl phthalate
84-66-2
0.20
28
p-Dimethylaminoazobenzene 60-11-7
0.13
NA
2,4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Dimetilan
6
644-64-4
0.056
1.4
Di-n-butyl phthalate
84-74-2
0.057
28
549
1,4-Dinitrobenzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitrophenol
51-28-5
0.12
160
2,4-Dinitrotoluene
121-14-2
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
Di-n-propylnitrosamine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
12.0
170
Diphenylamine (difficult to
distinguish from
diphenylnitrosamine)
122-39-4
0.92
13
Diphenylnitrosamine
(difficult to distinguish from
diphenylamine)
86-30-6
0.92
13
1,2-Diphenylhydrazine
122-66-7
0.087
NA
Disulfoton
298-04-4
0.017
6.2
Dithiocarbamates (total)
6
137-30-4
0.028
28
Endosulfan I
959-98-8
0.023
0.066
Endosulfan II
33213-65-9
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
EPTC
6
759-94-4
0.042
1.4
Ethyl acetate
141-78-6
0.34
33
Ethyl benzene
100-41-4
0.057
10
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
Ethylene oxide
75-21-8
0.12
NA
Ethyl ether
60-29-7
0.12
160
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Formetanate hydrochloride
6
23422-53-9
0.056
1.4
Formparanate
6
17702-57-7
0.056
1.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
550
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isolan
6
119-38-0
0.056
1.4
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-0
0.0011
0.13
Methacrylonitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
0.75 mg/l TCLP
Methapyrilene
91-80-5
0.081
1.5
Methiocarb
6
2032-65-7
0.056
1.4
Methomyl
6
16752-77-5
0.028
0.14
Methoxychlor
72-43-5
0.25
0.18
3-Methylcholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methyl methacrylate
80-62-6
0.14
160
Methyl methansulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Metolcarb
6
1129-41-5
0.056
1.4
Mexacarbate
6
315-18-4
0.056
1.4
Molinate
6
2212-67-1
0.042
1.4
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
o-Nitroaniline
88-74-4
0.27
14
p-Nitroaniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
o-Nitrophenol
88-75-5
0.028
13
p-Nitrophenol
100-02-7
0.12
29
N-Nitrosodiethylamine
55-18-5
0.40
28
N-Nitrosodimethylamine
62-75-9
0.40
2.3
N-Nitroso-di-n-butylamine
924-16-3
0.40
17
N-Nitrosomethylethylamine
10595-95-6
0.40
2.3
N-Nitrosomorpholine
59-89-2
0.40
2.3
N-Nitrosopiperidine
100-75-4
0.013
35
N-Nitrosopyrrolidine
930-55-2
0.013
35
Oxamyl
6
23135-22-0
0.056
0.28
551
Parathion
56-38-2
0.014
4.6
Total PCBs (sum of all PCB
isomers, or all Aroclors)
1336-36-3
0.10
10
Pebulate
6
1114-71-2
0.042
1.4
Pentachlorobenzene
608-93-5
0.055
10
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachloroethane
76-01-7
0.055
6.0
Pentachloronitrobenzene
82-68-8
0.055
4.8
Pentachlorophenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
o-Phenylenediamine
6
95-54-5
0.056
5.6
Phorate
298-02-2
0.021
4.6
Phthalic acid
100-21-0
0.055
28
Phthalic anhydride
85-44-9
0.055
28
Physostigmine
6
57-47-6
0.056
1.4
Physostigmine salicylate
6
57-64-7
0.056
1.4
Promecarb
6
2631-37-0
0.056
1.4
Pronamide
23950-58-5
0.093
1.5
Propham
6
122-42-9
0.056
1.4
Propoxur
6
114-26-1
0.056
1.4
Prosulfocarb
6
52888-80-9
0.042
1.4
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-5
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Thiodicarb
6
59669-26-0
0.019
1.4
Thiophanate-methyl
6
23564-05-8
0.056
1.4
Tirpate
6
26419-73-8
0.056
0.28
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Triallate
6
2303-17-5
0.042
1.4
552
Tribromomethane
(Bromoform)
75-25-2
0.63
15
2,4,6-Tribromophenol
118-79-6
0.035
7.4
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane 75-69-4
0.020
30
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,4,5-Trichlorophenoxy-
acetic acid/2,4,5-T
93-76-5
0.72
7.9
1,2,3-Trichloropropane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-
trifluoroethane
76-13-1
0.057
30
Triethylamine
6
101-44-8
0.081
1.5
tris-(2,3-Dibromopropyl)
phosphate
126-72-7
0.11
0.10
Vernolate
6
1929-77-7
0.042
1.4
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers (sum
of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 1.15 mg/l
TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 21 mg/l TCLP
Beryllium
7440-41-7
0.82
0.014 1.22 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 0.11 mg/l
TCLP
Chromium (Total)
7440-47-3
2.77
0.86 0.60 mg/l
TCLP
Cyanides (Total)
4
57-12-5
1.2
590
Cyanides (Amenable)
4
57-12-5
0.86
30
Fluoride
5
16984-48-8
35
NA
Lead
7439-92-1
0.69
0.37 0.75 mg/l
TCLP
Mercury-Nonwastewater
from Retort
7439-97-6
NA
0.20 mg/l TCLP
Mercury-All Others
7439-97-6
0.15
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 11 mg/l TCLP
Selenium
7
7782-49-2
0.82
0.16 5.7 mg/l
TCLP
553
Silver
7440-22-4
0.43
0.30 0.14 mg/l
TCLP
Sulfide
18496-25-8
14
NA
Thallium
7440-28-0
1.4
0.078 0.20 mg/l
TCLP
Vanadium
5
7440-62-2
4.3
0.23 1.6 mg/l
TCLP
Zinc
5
7440-66-6
2.61
5.3 4.3 mg/l
TCLP
1
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts or esters, the
CAS number is given for the parent compound only.
2
Concentration standards for wastewaters are expressed in mg/l are based on analysis of
composite samples.
3
Except for metals (EP or TCLP) and cyanides (total and amenable), the nonwastewater
treatment standards expressed as a concentration were established, in part, based on
incineration in units operated in accordance with the technical requirements of 35 Ill.
Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O or on combustion in
fuel substitution units operating in accordance with applicable technical requirements.
A facility may comply with these treatment standards according to provisions in 40
CFR 268.40(d) Section 728.140(d). All concentration standards for nonwastewaters
are based on analysis of grab samples.
4
Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to be analyzed
using Method 9010 or 9012, found in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods”, USEPA Publication SW-846, incorporated by reference
in 35 Ill. Adm. Code 720.111, with a sample size of 10 grams and a distillation time of
one hour and 15 minutes.
5
These constituents are not “underlying hazardous constituents” in characteristic wastes,
according to the definition at Section 728.102(i).
6
This footnote corresponds with note 6 to the table to 40 CFR 268.48(a), which has
already expired by its own terms. This statement maintains structural consistency with
the federal regulations.
7
This constituent is not an underlying hazardous constituent, as defined at Section
728.102(i), because its UTS level is greater than its TC level. Thus, a treated selenium
waste would always be characteristically hazardous unless it is treated to below its
characteristic level.
Note: NA means not applicable.
554
BOARD NOTE: Derived from table to 40 CFR 268.48(a) (1997), as amended at 63 Fed.
Reg. 24626 (May 4, 1998) and 63 Fed. Reg. 28739 (May 26, 1998).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER d: UNDERGROUND INJECTION CONTROL AND
UNDERGROUND STORAGE TANK PROGRAMS
PART 738
HAZARDOUS WASTE INJECTION RESTRICTIONS
SUBPART A: GENERAL
Section
738.101
Purpose, Scope, and Applicability
738.102
Definitions
738.103
Dilution Prohibited as a Substitute for Treatment
738.104
Case-by-Case Extensions of an Effective Date
738.105
Waste Analysis
SUBPART B: PROHIBITIONS ON INJECTION
Section
738.110
Waste Specific Prohibitions - Solvent Wastes
738.111
Waste Specific Prohibitions - Dioxin-Containing Wastes
738.112
Waste Specific Prohibitions - California List Wastes
738.114
Waste Specific Prohibitions - First Third Wastes
738.115
Waste Specific Prohibitions - Second Third Wastes
738.116
Waste Specific Prohibitions - Third Third Wastes
738.117
Waste-Specific Prohibitions - Newly-Listed Wastes
738.118
Waste-Specific Prohibitions - Newly-Listed and Identified Wastes
SUBPART C: PETITION STANDARDS AND PROCEDURES
Section
738.120
Petitions to Allow Injection of a Prohibited Waste
738.121
Required Information to Support Petitions
738.122
Submission, Review and Approval or Denial of Petitions
738.123
Review of Adjusted Standards
738.124
Termination of Adjusted Standards
AUTHORITY: Implementing Sections 13 and 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
555
SOURCE: Adopted in R89-2 at 14 Ill. Reg. 3059, effective February 20, 1990; amended in R89-11
at 14 Ill. Reg. 11948, effective July 9, 1990; amended in R90-14 at 15 Ill. Reg. 11425, effective July
24, 1991; amended in R92-13 at 17 Ill. Reg. 6190, effective April 5, 1993; amended in R93-6 at 17 Ill.
Reg. 15641, effective September 14, 1993; amended in R95-4 at 19 Ill. Reg. 9501, effective June 27,
1995; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 238, effective December 16, 1997; amended
in R97-21/R98-3/R98-5 at 22 Ill. Reg. 17486, effective September 28, 1998; amended in R98-
21/R99-2/R99-7 at 22 Ill. Reg. ________, effective ______________________.
SUBPART B: PROHIBITIONS ON INJECTION
Section 738.118
Waste-Specific Prohibitions - Newly-Listed and Identified Wastes
a)
All newly identified D004 through D011 wastes and characteristic mineral
processing wastes, except those identified in subsection (b) of this Section, are
prohibited from underground injection.
b)
Effective May 26, 2000, characteristic hazardous wastes from titanium dioxide
mineral processing, and radioactive wastes mixed with newly identified D004
through D011 or mixed with newly identified characteristic mineral processing
wastes, are prohibited from underground injection.
ac)
Effective August 11, 1997, the The wastes specified in 35 Ill. Adm. Code 721
as USEPA hazardous waste numbers F032, F034, F035 are prohibited from
underground injection.
bd)
Effective May 12, 1999, the wastes specified in 35 Ill. Adm. Code 721 as
USEPA hazardous waste numbers F032, F034, F035 that are mixed with
radioactive wastes are prohibited from underground injection.
ce)
The wastes specified in 35 Ill. Adm. Code 721.132 as having the following
USEPA hazardous waste numbers are prohibited from underground injection:
K156
K157
K158
K159
K160
K161
P127
P128
P185
P188
P189
P190
556
P191
P192
P194
P196
P197
P198
P199
P201
P202
P203
P204
P205
U271
U277
U278
U279
U280
U364
U365
U366
U367
U372
U373
U375
U376
U377
U378
U379
U381
U382
U383
U384
U385
U386
U387
U389
U390
U391
U392
U393
U394
U395
U396
U400
U401
557
U402
U403
U404
U407
U409
U410
U411
df)
The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA hazardous waste
number K088 is prohibited from underground injection.
eg)
The wastes specified in 35 Ill. Adm. Code 721 as having the following USEPA
hazardous waste numbers and Mixed TC/Radioactive wastes are prohibited from
underground injection:
D018
D019
D020
D021
D022
D023
D024
D025
D026
D027
D028
D029
D030
D031
D032
D033
D034
D035
D036
D037
D038
D039
D040
D041
D042
D043
f)
The wastes specified in 35 Ill. Adm. Code 721 as having the following USEPA
hazardous waste numbers are prohibited from underground injection:
558
D001
D002
D003
h)
The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA hazardous waste
number K140, and in 35 Ill. Adm. Code 721.133(f) as USEPA hazardous waste
number U408 are prohibited from underground injection.
i)
Effective February 8, 1999, the wastes specified in 35 Ill. Adm. Code 721.132
as USEPA hazardous waste numbers K169 through K172 are prohibited from
underground injection.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 739
STANDARDS FOR THE MANAGEMENT OF USED OIL
SUBPART A: DEFINITIONS
Section
739.100
Definitions
SUBPART B: APPLICABILITY
Section
739.110
Applicability
739.111
Used oil specifications
739.112
Prohibitions
SUBPART C: STANDARDS FOR USED OIL GENERATORS
Section
739.120
Applicability
739.121
Hazardous waste mixing
739.122
Used oil storage
739.123
On-site burning in space heaters
739.124
Off-site shipments
SUBPART D: STANDARDS FOR USED OIL COLLECTION CENTERS
AND AGGREGATION POINTS
Section
739.130
Do-it-yourselfer used oil collection centers
559
739.131
Used oil collection centers
739.132
Used oil aggregate points owned by the generator
SUBPART E: STANDARDS FOR USED OIL TRANSPORTER AND
TRANSFER FACILITIES
Section
739.140
Applicability
739.141
Restrictions on transporters that are not also processors
739.142
Notification
739.143
Used oil transportation
739.144
Rebuttable presumption for used oil
739.145
Used oil storage at transfer facilities
739.146
Tracking
739.147
Management of residues
SUBPART F: STANDARDS FOR USED OIL PROCESSORS
Section
739.150
Applicability
739.151
Notification
739.152
General facility standards
739.153
Rebuttable presumption for used oil
739.154
Used oil management
739.155
Analysis plan
739.156
Tracking
739.157
Operating record and reporting
739.158
Off-site shipments of used oil
739.159
Management of residues
SUBPART G: STANDARDS FOR USED OIL BURNERS THAT BURN
OFF-SPECIFICATION USED OIL FOR ENERGY RECOVERY
Section
739.160
Applicability
739.161
Restriction on burning
739.162
Notification
739.163
Rebuttable presumption for used oil
739.164
Used oil storage
739.165
Tracking
739.166
Notices
739.167
Management of residues
SUBPART H: STANDARDS FOR USED OIL FUEL MARKETERS
Section
739.170
Applicability
739.171
Prohibitions
739.172
On-specification used oil fuel
560
739.173
Notification
739.174
Tracking
739.175
Notices
SUBPART I: STANDARDS FOR USE AS A DUST SUPPRESSANT
DISPOSAL OF USED OIL
Section
739.180
Applicability
739.181
Disposal
739.182
Use as a dust suppressant
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993; amended
in R93-16 at 18 Ill. Reg. 6931, effective April 26, 1994; amended in R94-17 at 18 Ill. Reg.
17616, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 10036, effective June
27, 1995; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 767, effective December 16, 1997;
amended in R98-21/R99-2/R99-7 at 22 Ill. Reg. ________, effective ______________________.
SUBPART C: STANDARDS FOR USED OIL GENERATORS
Section 739.122
Used oil storage
Used oil generators are subject to all applicable federal Spill Prevention, Control and
Countermeasures (40 CFR 112) in addition to the requirements of this Subpart. Used oil generators
are also subject to the Underground Storage Tank (35 Ill. Adm. Code 731) standards for used oil
stored in underground tanks whether or not the used oil exhibits any characteristics of hazardous
waste, in addition to the requirements of this Subpart.
a)
Storage units. Used oil generators shall not store used oil in units other than tanks,
containers, or units subject to regulation under 35 Ill. Adm. Code 724 or 725.
b)
Condition of units. Containers and aboveground tanks used to store used oil at
generator facilities must be:
1)
In good condition (no severe rusting, apparent structural defects or
deterioration); and
2)
Not leaking (no visible leaks).
c)
Labels.
561
1)
Containers and aboveground tanks used to store used oil at generator
facilities must be labeled or marked clearly with the words “Used Oil.”
2)
Fill pipes used to transfer used oil into underground storage tanks at
generator facilities must be labeled or marked clearly with the words “Used
Oil.”
d)
Response to releases. Upon detection of a release of used oil to the environment
that is not subject to the federal requirements of Part 40 CFR 280, Subpart F and
which has occurred after the effective date of the authorized used oil program for
the State in which the release is located October 4, 1996, a generator shall perform
the following cleanup steps:
BOARD NOTE: Corresponding 40 CFR 279.22(d) applies to releases that
“occurred after the effective date of the authorized used oil program for the State in
which the release is located.” The Board adopted the used oil standards in docket
R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993. USEPA approved
the Illinois standards at 61 Fed. Reg. 40521 (Aug. 5, 1996), effective October
4, 1996. The Board has interpreted “the effective date of the authorized used oil
program” to mean the October 4, 1996 date of federal authorization of the Illinois
program, and we substituted that date for the federal effective date language. Had
USEPA written something like “the effective date of the used oil program in the
authorized State in which the release is located,” the Board would have used the
November 22, 1993 effective date of the Illinois used oil standards.
1)
Stop the release;
2)
Contain the released used oil;
3)
Clean Properly clean up and manage properly the released used oil and other
materials; and
4)
If necessary to prevent future releases, repair or replace any leaking used oil
storage containers or tanks prior to returning them to service.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: STANDARDS FOR USED OIL TRANSPORTER AND
TRANSFER FACILITIES
Section 739.145
Used oil storage at transfer facilities
A used oil transporter is subject to all applicable Spill Prevention, Control and Countermeasures (40
CFR 112) in addition to the requirements of this Subpart. A used oil transporter is also subject to
562
the Underground Storage Tank (35 Ill. Adm. Code 731) standards for used oil stored in
underground tanks whether or not the used oil exhibits any characteristics of hazardous waste, in
addition to the requirements of this Subpart.
a)
Applicability. This Section applies to used oil transfer facilities. Used oil transfer
facilities are transportation related facilities including loading docks, parking areas,
storage areas, and other areas where shipments of used oil are held for more than 24
hours during the normal course of transportation and not longer than 35 days.
Transfer facilities that store used oil for more than 35 days are subject to regulation
under Subpart F.
b)
Storage units. Owners or operators of used oil transfer facilities may not store used
oil in units other than tanks, containers, or units subject to regulation under 35 Ill.
Adm. Code 724 or 725.
c)
Condition of units. Containers and aboveground tanks used to store used oil at
transfer facilities must be:
1)
In good condition (no severe rusting, apparent structural defects or
deterioration); and
2)
Not leaking (no visible leaks).
d)
Secondary containment for containers. Containers used to store used oil at transfer
facilities must be equipped with a secondary containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dikes, berms, or retaining walls; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floors, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
e)
Secondary containment for existing aboveground tanks. Existing aboveground tanks
used to store used oil at transfer facilities must be equipped with a secondary
containment system.
563
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall except areas where existing
portions of the tank meet the ground; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floors, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
f)
Secondary containment for new aboveground tanks. New aboveground tanks used
to store used oil at transfer facilities must be equipped with a secondary containment
system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floors, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
g)
Labels.
1)
Containers and aboveground tanks used to store used oil at transfer facilities
must be labeled or marked clearly with the words “Used Oil.”
2)
Fill pipes used to transfer used oil into underground storage tanks at transfer
facilities must be labeled or marked clearly with the words “Used Oil.”
564
h)
Response to releases. Upon detection of a release of used oil to the environment
that is not subject to the federal requirements of 35 Ill. Adm. Code 731.Subpart F
40 CFR 280, Subpart F and which has occurred after the effective date of the
authorized used oil program for the State in which the release is located October 4,
1996, a an owner or operator of a transfer facility shall perform the following
cleanup steps:
BOARD NOTE: Corresponding 40 CFR 279.45(h) applies to releases that
“occurred after the effective date of the authorized used oil program for the State in
which the release is located.” The Board adopted the used oil standards in docket
R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993. USEPA approved
the Illinois standards at 61 Fed. Reg. 40521 (Aug. 5, 1996), effective October
4, 1996. The Board has interpreted “the effective date of the authorized used oil
program” to mean the October 4, 1996 date of federal authorization of the Illinois
program, and we substituted that date for the federal effective date language. Had
USEPA written something like “the effective date of the used oil program in the
authorized State in which the release is located,” the Board would have used the
November 22, 1993 effective date of the Illinois used oil standards.
1)
Stop the release;
2)
Contain the released used oil;
3)
Clean Properly clean up and manage properly the released used oil and other
materials; and
4)
If necessary to prevent future releases, repair or replace any leaking used oil
storage containers or tanks prior to returning them to service.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART F: STANDARDS FOR USED OIL PROCESSORS
Section 739.154
Used oil management
A used oil processor is subject to all applicable Spill Prevention, Control and Countermeasures (40
CFR 112) in addition to the requirements of this Subpart. A used oil processor or re-refiner is also
subject to the Underground Storage Tank (35 Ill. Adm. Code 731) standards for used oil stored in
underground tanks whether or not the used oil exhibits any characteristics of hazardous waste, in
addition to the requirements of this Subpart.
565
a)
Management units. Used oil processors shall not store used oil in units other than
tanks, containers, or units subject to regulation under 35 Ill. Adm. Code 724 or
725.
b)
Condition of units. Containers and aboveground tanks used to store or process used
oil at processing facilities must be:
1)
In good condition (no severe rusting, apparent structural defects or
deterioration); and
2)
Not leaking (no visible leaks).
c)
Secondary containment for containers. Containers used to store or process used oil
at processing and re-refining facilities must be equipped with a secondary
containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
d)
Secondary containment for existing aboveground tanks. Existing aboveground tanks
used to store or process used oil at processing and re-refining facilities must be
equipped with a secondary containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall except areas where existing
portions of the tank meet the ground; or
566
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
e)
Secondary containment for new aboveground tanks. New aboveground tanks used
to store or process used oil at processing and re-refining facilities must be equipped
with a secondary containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
f)
Labels.
1)
Containers and aboveground tanks used to store used oil at processing
facilities must be labeled or marked clearly with the words “Used Oil.”
2)
Fill pipes used to transfer used oil into underground storage tanks at
processing facilities must be labeled or marked clearly with the words “Used
Oil.”
g)
Response to releases. Upon detection of a release of used oil to the environment
that is not subject to the federal requirements of 35 Ill. Adm. Code 731.Subpart F
40 CFR 280, Subpart F and which has occurred after the effective date of the
authorized used oil program for the State in which the release is located October 4,
1996, a processor shall perform the following cleanup steps:
BOARD NOTE: Corresponding 40 CFR 279.54(g) applies to releases that
“occurred after the effective date of the authorized used oil program for the State in
567
which the release is located.” The Board adopted the used oil standards in docket
R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993. USEPA approved
the Illinois standards at 61 Fed. Reg. 40521 (Aug. 5, 1996), effective October
4, 1996. The Board has interpreted “the effective date of the authorized used oil
program” to mean the October 4, 1996 date of federal authorization of the Illinois
program, and we substituted that date for the federal effective date language. Had
USEPA written something like “the effective date of the used oil program in the
authorized State in which the release is located,” the Board would have used the
November 22, 1993 effective date of the Illinois used oil standards.
1)
Stop the release;
2)
Contain the released used oil;
3)
Clean Properly clean up and manage properly the released used oil and other
materials; and
4)
If necessary to prevent future releases, repair or replace any leaking used oil
storage containers or tanks prior to returning them to service.
h)
Closure.
1)
Aboveground tanks. Owners and operators that store or process used oil in
aboveground tanks shall comply with the following requirements:
A)
At closure of a tank system, the owner or operator shall remove or
decontaminate used oil residues in tanks, contaminated containment
system components, contaminated soils, and structures and
equipment contaminated with used oil, and manage them as
hazardous waste, unless the materials are not hazardous waste under
this chapter.
B)
If the owner or operator demonstrates that not all contaminated soils
can be practicably removed or decontaminated as required in
subsection (h)(1)(A) above of this Section, then the owner or
operator shall close the tank system and perform post-closure care in
accordance with the closure and post-closure care requirements that
apply to hazardous waste landfills (35 Ill. Adm. Code 725.410).
2)
Containers. Owners and operators that store used oil in containers shall
comply with the following requirements:
A)
At closure, containers holding used oils or residues of used oil must
be removed from the site;
568
B)
The owner or operator shall remove or decontaminate used oil
residues, contaminated containment system components,
contaminated soils, and structures and equipment contaminated with
used oil, and manage them as hazardous waste, unless the materials
are not hazardous waste 35 Ill. Adm. Code 721.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART G: STANDARDS FOR USED OIL BURNERS THAT BURN
OFF-SPECIFICATION USED OIL FOR ENERGY RECOVERY
Section 739.164
Used oil storage
A used oil burner is subject to all applicable Spill Prevention, Control and Countermeasures (40
CFR 112) in addition to the requirements of this Subpart. A used oil burner is also subject to the
Underground Storage Tank (35 Ill. Adm. Code 731) standards for used oil stored in underground
tanks whether or not the used oil exhibits any characteristics of hazardous waste, in addition to the
requirements of this Subpart.
a)
Storage units. Used oil burners may not store used oil in units other than tanks,
containers, or units subject to regulation under 35 Ill. Adm. Code 724 or 725.
b)
Condition of units. Containers and aboveground tanks used to store oil at burner
facilities must be:
1)
In good condition (no severe rusting, apparent structural defects or
deterioration); and
2)
Not leaking (no visible leaks).
c)
Secondary containment for containers. Containers used to store used oil at burner
facilities must be equipped with a secondary containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Dikes, berms or retaining walls; and
B)
A floor. The floor must cover the entire area within the dike, berm,
or retaining wall.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
569
d)
Secondary containment for existing aboveground tanks. Existing aboveground tanks
used to store used oil at burner facilities must be equipped with a secondary
containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall except areas where existing
portions of the tank meet the ground; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
e)
Secondary containment for existing aboveground tanks. New aboveground tanks
used to store used oil at burner facilities must be equipped with a secondary
containment system.
1)
The secondary containment system must consist of, at a minimum:
A)
Both:
i)
Dikes, berms or retaining walls; and
B)ii) A floor. The floor must cover the entire area within the
dike, berm, or retaining wall; or
C)B) An equivalent secondary containment system.
2)
The entire containment system, including walls and floor, must be
sufficiently impervious to used oil to prevent any used oil released into the
containment system from migrating out of the system to the soil,
groundwater, or surface water.
f)
Labels.
570
1)
Containers and aboveground tanks used to store used oil at burner facilities
must be labeled or marked clearly with the words “Used Oil.”
2)
Fill pipes used to transfer used oil into underground storage tanks at burner
facilities must be labeled or marked clearly with the words “Used Oil.”
g)
Response to releases. Upon detection of a release of used oil to the environment
that is not subject to the federal requirements of 35 Ill. Adm. Code 731.Subpart F
40 CFR 280, Subpart F and which has occurred after the effective date of the
authorized used oil program for the State in which the release is located October 4,
1996, a burner shall perform the following cleanup steps:
BOARD NOTE: Corresponding 40 CFR 279.64(g) applies to releases that
“occurred after the effective date of the authorized used oil program for the State in
which the release is located.” The Board adopted the used oil standards in docket
R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993. USEPA approved
the Illinois standards at 61 Fed. Reg. 40521 (Aug. 5, 1996), effective October
4, 1996. The Board has interpreted “the effective date of the authorized used oil
program” to mean the October 4, 1996 date of federal authorization of the Illinois
program, and we substituted that date for the federal effective date language. Had
USEPA written something like “the effective date of the used oil program in the
authorized State in which the release is located,” the Board would have used the
November 22, 1993 effective date of the Illinois used oil standards.
1)
Stop the release;
2)
Contain the released used oil;
3)
Clean Properly clean up and manage properly the released used oil and other
materials; and
4)
If necessary, repair or replace any leaking used oil storage containers or
tanks prior to returning them to service.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART H: STANDARDS FOR USED OIL FUEL MARKETERS
Section 739.174
Tracking
a)
Off-specification used oil delivery. Any used oil fuel marketer that directs a
shipment of off-specification used oil to a burner shall keep a record of each
shipment of used oil to a used oil burner. These records may take the form of a
571
log, invoice, manifest, bill of lading or other shipping documents. Records for each
shipment must include the following information:
1)
The name and address of the transporter that delivers the used oil to the
burner;
2)
The name and address of the burner that will receive the used oil;
3)
The U.S. EPA USEPA identification number and Illinois special waste
identification number of the transporter that delivers the used oil to the
burner;
4)
The U.S. EPA USEPA identification number and Illinois special waste
identification number of the burner;
5)
The quantity of used oil shipped; and
6)
The date of shipment.
b)
On-specification used oil delivery. A generator, transporter, processor or re-refiner,
or burner that first claims that used oil that is to be burned for energy recovery
meets the fuel specifications under Section 739.111 shall keep a record of each
shipment of used oil to an on-specification used oil burner. Records for each
shipment must include the following information:
1)
The name and address of the facility receiving the shipment;
2)
The quantity of used oil fuel delivered;
3)
The date of shipment or delivery; and
4)
A cross-reference to the record of used oil analysis or other information used
to make the determination that the oil meets the specification as required
under Section 739.172(a).
c)
Record retention. The records described in subsections (a) and (b) above of this
Section must be maintained for at least three years.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
