ILLINOIS POLLUTION CONTROL BOARD
August 20, 1998
IN THE MATTER OF:
)
)
R97-21
RCRA UPDATE, USEPA REGULATIONS
)
(Identical-in-Substance
(July 1, 1996, through December 31, 1996)
)
Rulemaking - Land)
________________________________________
IN THE MATTER OF:
)
)
R98-3
UIC UPDATE, USEPA REGULATIONS
)
(Identical-in-Substance
(January 1, 1997, through June 30, 1997)
)
Rulemaking - Land)
________________________________________
IN THE MATTER OF:
)
)
R98-5
RCRA UPDATE, USEPA REGULATIONS
)
(Identical-in-Substance
(January 1, 1997, through June 30, 1997)
)
Rulemaking - Land)
Adopted Rule. Final Order.
ORDER OF THE BOARD (by K.M. Hennessey):
Pursuant to Sections 13(c) and 22.4(a) of the Environmental Protection Act (Act) (415
ILCS 5/13(c) & 22.4(a) (1996)), the Board adopts amendments to the Illinois regulations that
are “identical-in-substance” to hazardous waste regulations adopted by the United States
Environmental Protection Agency (USEPA) to implement Subtitle C of the federal Resource
Conservation and Recovery Act of 1976 (RCRA Subtitle C), 42 U.S.C. §§ 6921
et seq
.
(1996). The Board further adopts amendments to the Illinois regulations that are “identical-in-
substance” to underground injection control (UIC) regulations adopted by the USEPA to
implement provisions of the Safe Drinking Water Act (SDWA), 42 U.S.C. § 300h
et seq
.
(1996). The nominal timeframe of this consolidated docket includes federal RCRA Subtitle C
amendments adopted by USEPA in the periods July 1, 1996, through December 31, 1996, and
January 1, 1997, through June 30, 1997. The nominal timeframe also includes federal UIC
amendments adopted in the period January 1, 1997, through June 30, 1997.
Section 22.4(a) provides for quick adoption of regulations that are “identical-in-
substance” to federal regulations adopted by USEPA to implement Sections 3001 through 3005
of RCRA, 42 U.S.C. §§ 6921-6925 (1996)) and that Title VII of the Act and Section 5 of the
Administrative Procedure Act (APA) (5 ILCS 100/5-35 & 5-40 (1996)) shall not apply.
Section 13(c) similarly provides for quick adoption of regulations that are “identical-in-
substance” to federal regulations adopted by USEPA to implement Section 1421 of SDWA, 42
U.S.C. § 300h (1996)). Because this consolidated rulemaking is not subject to Section 5 of
the APA, it is not subject to first-notice or to second-notice review by the Joint Committee on
2
Administrative Rules (JCAR). The federal RCRA Subtitle C regulations are found at 40
C.F.R. 260 through 268, 270 through 271, 279, and, more recently, 273. The federal UIC
regulations are found at 40 CFR 144 through 148.
This order is supported by an opinion adopted on the same day. The Board will wait
the 30 days for USEPA review that are provided in the state primacy agreement, then file the
Amendments with the Secretary of State and submit Notices of Adopted Amendments for
publication in the
Illinois Register
. The complete text of the adopted rules follows.
IT IS SO ORDERED.
I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control Board, do hereby certify
that the above order was adopted on the 20th day of August 1998 by a vote of 7-0.
Dorothy M. Gunn, Clerk
Illinois Pollution Control Board
3
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER b: PERMITS
PART 703
RCRA PERMIT PROGRAM
SUBPART A: GENERAL PROVISIONS
Section
703.100
Scope and Relation to Other Parts
703.101
Purpose
703.110
References
SUBPART B: PROHIBITIONS
Section
703.120
Prohibitions in General
703.121
RCRA Permits
703.122
Specific Inclusions in Permit Program
703.123
Specific Exclusions from Permit Program
703.124
Discharges of Hazardous Waste
703.125
Reapplications
703.126
Initial Applications
703.127
Federal Permits (Repealed)
SUBPART C: AUTHORIZATION BY RULE AND INTERIM STATUS
Section
703.140
Purpose and Scope
703.141
Permits by Rule
703.150
Application by Existing HWM Facilities and Interim Status Qualifications
703.151
Application by New HWM Facilities
703.152
Amended Part A Application
703.153
Qualifying for Interim Status
703.154
Prohibitions During Interim Status
703.155
Changes During Interim Status
703.156
Interim Status Standards
703.157
Grounds for Termination of Interim Status
703.158
Permits for Less Than an Entire Facility
703.159
Closure by Removal
703.160
Procedures for Closure Determination
SUBPART D: APPLICATIONS
Section
703.180
Applications in General
703.181
Contents of Part A
4
703.182
Contents of Part B
703.183
General Information
703.184
Facility Location Information
703.185
Groundwater Protection Information
703.186
Exposure Information
703.187
Solid Waste Management Units
703.188
Other Information
703.191
Public Participation: Pre-Application Public Notice and Meeting
703.192
Public Participation: Public Notice of Application
703.193
Public Participation: Information Repository
703.200
Specific Part B Application Information
703.201
Containers
703.202
Tank Systems
703.203
Surface Impoundments
703.204
Waste Piles
703.205
Incinerators that Burn Hazardous Waste
703.206
Land Treatment
703.207
Landfills
703.208
Boilers and Industrial Furnaces Burning Hazardous Waste
703.209
Miscellaneous Units
703.210
Process Vents
703.211
Equipment
703.212
Drip Pads
703.213
Air Emission Controls for Tanks, Surface Impoundments, and Containers
SUBPART E: SHORT TERM AND PHASED PERMITS
Section
703.221
Emergency Permits
703.222
Incinerator Conditions Prior to Trial Burn
703.223
Incinerator Conditions During Trial Burn
703.224
Incinerator Conditions After Trial Burn
703.225
Trial Burns for Existing Incinerators
703.230
Land Treatment Demonstration
703.231
Research, Development and Demonstration Permits
703.232
Permits for Boilers and Industrial Furnaces Burning Hazardous Waste
SUBPART F: PERMIT CONDITIONS OR DENIAL
Section
703.240
Permit Denial
703.241
Establishing Permit Conditions
703.242
Noncompliance Pursuant to Emergency Permit
703.243
Monitoring
703.244
Notice of Planned Changes (Repealed)
703.245
Twenty-four Hour Reporting
703.246
Reporting Requirements
5
703.247
Anticipated Noncompliance
703.248
Information Repository
SUBPART G: CHANGES TO PERMITS
Section
703.260
Transfer
703.270
Modification
703.271
Causes for Modification
703.272
Causes for Modification or Reissuance
703.273
Facility Siting
703.280
Permit Modification at the Request of the Permittee
703.281
Class 1 Modifications
703.282
Class 2 Modifications
703.283
Class 3 Modifications
703.Appendix A
Classification of Permit Modifications
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14289, effective October 12, 1983; amended in R83-
24 at 8 Ill. Reg. 206, effective December 27, 1983; amended in R84-9 at 9 Ill. Reg. 11899, effective July 24,
1985; amended in R85-22 at 10 Ill. Reg. 1110, effective January 2, 1986; amended in R85-23 at 10 Ill. Reg.
13284, effective July 28, 1986; amended in R86-1 at 10 Ill. Reg. 14093, effective August 12, 1986; amended in
R86-19 at 10 Ill. Reg. 20702, effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6121, effective
March 24, 1987; amended in R86-46 at 11 Ill. Reg. 13543, effective August 4, 1987; amended in R87-5 at 11 Ill.
Reg. 19383, effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2584, effective January 15, 1988;
amended in R87-39 at 12 Ill. Reg. 13069, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 447,
effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18477, effective November 13, 1989; amended in
R89-9 at 14 Ill. Reg. 6278, effective April 16, 1990; amended in R90-2 at 14 Ill. Reg. 14492, effective August
22, 1990; amended in R90-11 at 15 Ill. Reg. 9616, effective June 17, 1991; amended in R91-1 at 15 Ill. Reg.
14554, effective September 30, 1991; amended in R91-13 at 16 Ill. Reg. 9767, effective June 9, 1992; amended in
R92-10 at 17 Ill. Reg. 5774, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20794, effective
November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6898, effective April 26, 1994; amended in R94-7 at 18
Ill. Reg. 12392, effective July 29, 1994; amended in R94-5 at 18 Ill. Reg. 18316, effective December 20, 1994;
amended in R95-6 at 19 Ill. Reg. 9920, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11225,
effective August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 533, effective December 16, 1997;
amended in R98-12 at 22 Ill. Reg. 7632, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill.
Reg. ________, effective ______________________.
SUBPART B: PROHIBITIONS
Section 703.124
Discharges of Hazardous Waste
a)
A person is not required to obtain a RCRA permit for treatment or containment
activities taken during immediate response to any of the following situations:
6
1)
A discharge of a hazardous waste;
2)
An imminent and substantial threat of a discharge of hazardous waste;
3)
A discharge of a material which, when discharged, becomes a hazardous
waste.; or
4) An immediate threat to human health, public safety, property, or the
environment from the known or suspected presence of military
munitions, other explosive material, or an explosive device, as
determined by an explosive or munitions emergency response specialist
as defined in 35 Ill. Adm. Code 720.110.
b)
Any person who continues or initiates hazardous waste treatment or containment
activities after the immediate response is over is subject to all applicable
requirements of this Part for those activities.
c) In the case of an emergency response involving military munitions, the
responding military emergency response specialist’s organizational unit shall
retain records for three years after the date of the response that identify the
following: the date of the response, the responsible persons responding, the
type and description of material addressed, and the disposition of the material.
(Board NoteBOARD NOTE: See Derived from 40 CFR 270.1(c)(3) (1997).)
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART D: APPLICATIONS
Section 703.213
Air Emission Controls for Tanks, Surface Impoundments, and
Containers
Except as otherwise provided in 35 Ill. Adm. Code 724.101, owners and operators of tanks,
surface impoundments, or containers that use air emission controls in accordance with the
requirements of 35 Ill. Adm. Code 724.Subpart CC shall provide the following additional
information:
a)
Documentation for each floating roof cover installed on a tank subject to 35 Ill.
Adm. Code 724.984(d)(1) or (d)(2) that includes information prepared by the
owner or operator or provided by the cover manufacturer or vendor describing
the cover design, and certification by the owner or operator that the cover meets
the applicable design specifications, as listed in 35 Ill. Adm. Code
725.991(e)(1) or (f)(1).
7
b)
Identification of each container area subject to the requirements of 35 Ill. Adm.
Code 724.Subpart CC and certification by the owner or operator that the
requirements of this Subpart are met.
c)
Documentation for each enclosure used to control air pollutant emissions from
containers in accordance with the requirements of 35 Ill. Adm. Code
724.984(d)(5) or 724.986(e)(1)(ii) that includes records for the most recent set
of calculations and measurements performed by the owner or operator to verify
that the enclosure meets the criteria of a permanent total enclosure, as specified
in “Procedure T--Criteria for and Verification of a Permanent or Temporary
Total Enclosure” under 40 CFR 52.741, appendix B, incorporated by reference
in 35 Ill. Adm. Code 720.111.
d)
Documentation for each floating membrane cover installed on a surface
impoundment in accordance with the requirements of 35 Ill. Adm. Code
724.985(c) that includes information prepared by the owner or operator or
provided by the cover manufacturer or vendor describing the cover design, and
certification by the owner or operator that the cover meets the specifications
listed in 35 Ill. Adm. Code 264724.985(c)(1).
e)
Documentation for each closed-vent system and control device installed in
accordance with the requirements of 35 Ill. Adm. Code 724.987 that includes
design and performance information, as specified in Section 703.124(c) and (d).
f)
An emission monitoring plan for both Method 21 in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code 720.111, and control device
monitoring methods. This plan must include the following information:
monitoring points, monitoring methods for control devices, monitoring
frequency, procedures for documenting exceedances, and procedures for
mitigating noncompliances.
g)
When an owner or operator of a facility subject to 35 Ill. Adm. Code
725.Subpart CC cannot comply with 35 Ill. Adm. Code 724.Subpart CC by the
date of permit issuance, the schedule of implementation required under 35 Ill.
Adm. Code 725.982.
BOARD NOTE: Derived from 40 CFR 270.27(a) (19967), as amended at 61
Fed. Reg. 59996 (Nov. 25, 1996).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
8
SUBPART E: SHORT TERM AND PHASED PERMITS
Section 703.232
Permits for Boilers and Industrial Furnaces Burning Hazardous Waste
a)
General. Owners and operators of new boilers and industrial furnaces (those
not operating under the interim status standards of 35 Ill. Adm. Code 726.203)
are subject to subsection subsections (b) through (f) of this Section. Boilers and
industrial furnaces operating under the interim status standards of 35 Ill. Adm.
Code 726.203 are subject to subsection (g) of this Section.
b)
Permit operating periods for new boilers and industrial furnaces. A permit for a
new boiler or industrial furnace must specify appropriate conditions for the
following operating periods:
1)
Pretrial burn period. For the period beginning with initial introduction
of hazardous waste and ending with initiation of the trial burn, and only
for the minimum time required to bring the boiler or industrial furnace
to a point of operation readiness to conduct a trial burn, not to exceed
720 hours operating time when burning hazardous waste, the Agency
shall establish permit conditions in the Pretrial Burn Period of the permit
conditions, including but not limited to allowable hazardous waste feed
rates and operating conditions. The Agency shall extend the duration of
this operational period once, for up to 720 additional hours, at the
request of the applicant when good cause is shown. The permit most be
modified to reflect the extension according to Section 703.280 et seq.
A)
Applicants must submit a statement, with Part B of the permit
application, that suggests the conditions necessary to operate in
compliance with the standards of 35 Ill. Adm. Code 726.204
through 726.207 during this period. This statement should
include, at a minimum, restrictions on the applicable operating
requirements identified in 35 Ill. Adm. Code 726.202 (e).
B)
The Agency shall review this statement and any other relevant
information submitted with Part B of the permit application and
specify requirements for this period sufficient to meet the
performance standards of 35 Ill. Adm. Code 726.204 through
726.207 based on the Agency’s engineering judgment.
2)
Trial burn period. For the duration of the trial burn, the Agency shall
establish conditions in the permit for the purposes of determining
feasibility of compliance with the performance standards of 35 Ill. Adm.
Code 726.204 through 726.207 and determining adequate operating
conditions under 35 Ill. Adm. Code 726.202(e). Applicants shall
9
propose a trial burn plan, prepared under subsection (c) of this Section,
to be submitted with Part B of the permit application.
3)
Post-trial burn period.
A)
For the period immediately following completion of the trial
burn, and only for the minimum period sufficient to allow sample
analysis, data computation and submission of the trial burn results
by the applicant, and review of the trial burn results and
modification of the facility permit by the Agency to reflect the
trial burn results, the Agency shall establish the operating
requirements most likely to ensure compliance with the
performance standards of 35 Ill. Adm. Code 726.204 through
726.207 based on the Agency’s engineering judgment.
B)
Applicants shall submit a statement, with Part B of the
application, that identifies the conditions necessary to operate
during this period in compliance with the performance standards
of 35 Ill. Adm. Code 726.204 through 726.207. This statement
should include, at a minimum, restrictions on the operating
requirements provided by 35 Ill. Adm. Code 726.202 (e).
C)
The Agency shall review this statement and any other relevant
information submitted with Part B of the permit application and
specify requirements of this period sufficient to meet the
performance standards of 35 Ill. Adm. Code 726.204 through
726.207 based on the Agency’s engineering judgment.
4)
Final permit period. For the final period of operation the Agency shall
develop operating requirements in conformance with 35 Ill. Adm. Code
726.202(e) that reflect conditions in the trial burn plan and are likely to
ensure compliance with the performance standards of 35 Ill. Adm. Code
726.204 through 726.207. Based on the trial burn results, the Agency
shall make any necessary modifications to the operating requirements to
ensure compliance with the performance standards. The permit
modification must proceed according to Section 703.280 et seq.
c)
Requirements for trial burn plans. The trial burn plan must include the
following information. The Agency, in reviewing the trial burn plan, shall
evaluate the sufficiency of the information provided and may require the
applicant to supplement this information, if necessary, to achieve the purposes
of this subsection.
1)
An analysis of each feed stream, including hazardous waste, other fuels,
and industrial furnace feed stocks, as fired, that includes:
10
A)
Heating value, levels of antimony, arsenic, barium, beryllium,
cadmium, chromium, lead, mercury, silver, thallium, total
chlorine/chloride, and ash; and
B)
Viscosity or description of the physical form of the feed stream.
2)
An analysis of each hazardous waste, as fired, including:
A)
An identification of any hazardous organic constituents listed in
35 Ill. Adm. Code 721.Appendix H that are present in the feed
stream, except that the applicant need not analyze for constituents
listed in 721.Appendix H that would reasonably not be expected
to be found in the hazardous waste. The constituents excluded
from analysis must be identified as and the basis for this
exclusion explained. The analysis must be conducted in
accordance with analytical techniques specified in “Test Methods
for the Evaluation of Solid Waste, Physical/Chemical Methods”,
USEPA Publication SW-846, as incorporated by reference at 35
Ill. Adm. Code 720.111 and Section 703.110, or their
equivalent.
B)
An approximate quantification of the hazardous constituents
identified in the hazardous waste, within the precision produced
by the analytical methods specified in “Test Methods for the
Evaluation of Solid Waste, Physical/Chemical Methods”,
USEPA Publication SW-846, as incorporated by reference at 35
Ill. Adm. Code 720.111 and Section 703.110, or other
equivalent.
C)
A description of blending procedures, if applicable, prior to
firing the hazardous waste, including a detailed analysis of the
hazardous waste prior to blending, an analysis of the material
with which the hazardous waste prior to blending, an analysis of
the material with which the hazardous waste is blended, and
blending ratios.
3)
A detailed engineering description of the boiler or industrial furnace,
including:
A)
Manufacturer’s name and model number of the boiler or
industrial furnace;
B)
Type of boiler or industrial furnace;
11
C)
Maximum design capacity in appropriate units;
D)
Description of the feed system for the hazardous waste and, as
appropriate, other fuels and industrial furnace feedstocks;
E)
Capacity of hazardous waste feed system;
F)
Description of automatic hazardous waste feed cutoff system(s);
G)
Description of any pollution control system; and
H)
Description of stack gas monitoring and any pollution control
monitoring systems.
4)
A detailed description of sampling and monitoring procedures including
sampling and monitoring locations in the system, the equipment to be
used, sampling and monitoring frequency, and sample analysis.
5)
A detailed test schedule for each hazardous waste for which the trial
burn is planned, including date(s), duration, quantity of hazardous waste
to be burned, and other factors relevant to the Agency’s decision under
subsection (b)(2) of this Section.
6)
A detailed test protocol, including, for each hazardous waste identified,
the ranges of hazardous waste feed rate, and, as appropriate, the feed
rates of other fuels and industrial furnace feedstocks, and any other
relevant parameters that may affect the ability of the boiler or industrial
furnace to meet the performance standards in 35 Ill. Adm. Code 726.204
through 726.207.
7)
A description of and planned operating conditions for any emission
control equipment that will be used.
8)
Procedures for rapidly stopping the hazardous waste feed and controlling
emissions in the event of an equipment malfunction.
9)
Such other information as the Agency finds necessary to determine
whether to approve the trial burn plan in light of the purposes of this
subsection and the criteria in subsection (b)(2) of this Section.
d)
Trial burn procedures.
1)
A trial burn must be conducted to demonstrate conformance with the
standards of 35 Ill. Adm. Code 726.104 through 726.107.
12
2)
The Agency shall approve a trial burn plan if the Agency finds that:
A)
The trial burn is likely to determine whether the boiler or
industrial furnace can meet the performance standards of 35 Ill.
Adm. Code 726.104 through 726.107.;
B)
The trial burn itself will not present an imminent hazard to
human health and the environment;
C)
The trial burn will help the Agency to determine operating
requirements to be specified under 35 Ill. Adm. Code
726.102(e); and
D)
The information sought in the trial burn cannot reasonably be
developed through other means.
3)
The Agency shall send a notice to all persons on the facility mailing list,
as set forth in 35 Ill. Adm. Code 705.161(a), and to the appropriate
units of State and local government, as set forth in 35 Ill. Adm. Code
705.163(a)(5), announcing the scheduled commencement and completion
dates for the trial burn. The applicant may not commence the trial burn
until after the Agency has issued such notice.
A)
This notice must be mailed within a reasonable time period
before the trial burn. An additional notice is not required if the
trial burn is delayed due to circumstances beyond the control of
the facility or the Agency.
B)
This notice must contain:
i)
The name and telephone number of applicant’s contact
person;
ii)
The name and telephone number of the Agency regional
office appropriate for the facility;
iii)
The location where the approved trial burn plan and any
supporting documents can be reviewed and copied; and
iv)
An expected time period for commencement and
completion of the trial burn.
4)
The applicant shall submit to the Agency a certification that the trial
burn has been carried out in accordance with the approved trial burn
plan, and submit the results of all the determinations required in
13
subsection (c) of this Section. The Agency shall, in the trial burn plan,
require that the submission be made within 90 days after completion of
the trial burn, or later if the Agency determines that a later date is
acceptable.
5)
All data collected during any trial burn must be submitted to the Agency
following completion of the trial burn.
6)
All submissions required by this subsection must be certified on behalf
of the applicant by the signature of a person authorized to sign a permit
application or a report under 35 Ill. Adm. Code 702.126.
e)
Special procedures for DRE trial burns. When a DRE trial burn is required
under 35 Ill. Adm. Code 726.104, the Agency shall specify (based on the
hazardous waste analysis data and other information in the trial burn plan) as
trial Principal Organic Hazardous Constituents (POHCs) those compounds for
which destruction and removal efficiencies must be calculated during the trial
burn. These trial POHCs will be specified by the Agency based on information
including the Agency’s estimate of the difficulty of destroying the constituents
identified in the hazardous waste analysis, their concentrations or mass in the
hazardous waste feed, and, for hazardous waste containing or derived from
wastes listed in 35 Ill. Adm. Code 721.Subpart D, the hazardous waste organic
constituent(s) identified in 35 Ill. Adm. Code 721.Appendix G as the basis for
listing.
f)
Determinations based on trial burn. During each approved trial burn (or as
soon after the burn as is practicable), the applicant shall make the following
determinations:
1)
A quantitative analysis of the levels of antimony, arsenic, barium,
beryllium, cadmium, chromium, lead, mercury, thallium, silver, and
chlorine/chloride in the feed streams (hazardous waste, other fuels, and
industrial furnace feedstocks);
2)
When a DRE trial burn is required under 35 Ill. Adm. Code 726.204(a):
A)
A quantitative analysis of the trial POHCs in the hazardous waste
feed;
B)
A quantitative analysis of the stack gas for the concentration and
mass emissions of the trial POHCs; and
C)
A computation of destruction and removal efficiency (DRE), in
accordance with the DRE formula specified in 35 Ill. Adm. Code
726.204(a).;
14
3)
When a trial burn for chlorinated dioxins and furans is required under 35
Ill. Adm. Code 726.204(e), a quantitative analysis of the stack gas for
the concentration and mass emission rate of the 2,3,7,8-chlorinated tetra-
through octa-congeners of chlorinated dibenzo-p-dioxins and furans, and
a computation showing conformance with the emission standard.;
4)
When a trial burn for PM, metals, or HCl/Chlorine gas is required under
35 Ill. Adm. Code 726.205, 726.206(c) or (d), or 726.207(b)(2) or (c),
a quantitative analysis of the stack gas for the concentrations and mass
emissions of PM, metals, or HCl and chlorine gas and computations
showing conformance with the applicable emission performance
standards;
5)
When a trial burn for DRE, metals, and HCl/Chlorine gas is required
under 35 Ill. Adm. Code 726.204(a), 726.206(c) or (d), or
726.207(b)(2) or (c), a quantitative analysis of the scrubber water (if
any), ash residues, other residues, and products for the purpose of
estimating the fate of the trial POHCs, metals, and chlorine/chloride;
6)
An identification of sources of fugitive emissions and their means of
control;
7)
A continuous measurement of carbon monoxide (CO), oxygen, and,
where required, hydrocarbons (HC), in the stack gas; and
8)
Such other information as the Agency specifies as necessary to ensure
that the trial burn will determine compliance with the performance
standards 35 Ill. Adm. Code 726.204 through 726.207 and to establish
the operating conditions required by 35 Ill. Adm. Code 726.204 through
726.207 and of determining adequate operating conditions under 35 Ill.
Adm. Code 726.203, and to establish the operating conditions required
by 35 Ill. Adm. Code 726.202(e) as necessary to meet those
performance standards.
g)
Interim status boilers and industrial furnaces. For the purpose of determining
feasibility of compliance with the performance standards of 35 Ill. Adm. Code
726.204 through 726.207 and of determining adequate operating conditions
under 35 Ill. Adm. Code 726.203, applicants owning or operating existing
boilers or industrial furnaces operated under the interim status standards of 35
Ill. Adm. Code 726.203 shall either prepare and submit a trial burn plan and
perform a trial burn in accordance with the requirements of the Section or
submit other information as specified in Section 703.208(a)(6). The Agency
shall announce its intention to approve of the trial burn plan in accordance with
the timing and distribution requirements of subsection (d)(3) of this Section.
15
The contents of the notice must include: the name and telephone number of a
contact person at the facility; the name and telephone number of Agency
regional office appropriate for the facility; the location where the trial burn plan
and any supporting documents can be reviewed and copied; and a schedule of
the activities that are required prior to permit issuance, including the anticipated
time schedule for agency approval of the plan and the time periods during which
the trial burn would be conducted. Applicants that submit a trial burn plan and
receive approval before submission of the Part B permit application shall
complete the trial burn and submit the results specified in subsection (f) of this
Section with the Part B permit application. If completion of this process
conflicts with the date set for submission of the Part B application, the applicant
shall contact the Agency to establish a later date for submission of the Part B
application or the trial burn results. If the applicant submits a trial burn plan
with Part B of the permit application, the trial burn must be conducted and the
results submitted within a time period prior to permit issuance to be specified by
the Agency.
BOARD NOTE: Derived from 40 CFR 270.66 (1996).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART G: CHANGES TO PERMITS
Section 703.280
Permit Modification at the Request of the
Permittee
a)
Class 1 modifications. See Section 703.281.
b)
Class 2 modifications. See Section 703.282.
c)
Class 3 modifications. See Section 703.283.
d)
Other modifications.
1)
In the case of modifications not explicitly listed in Appendix A, the
permittee may submit a Class 3 modification request to the Agency, or
the permittee may request a determination by the Agency that the
modification be reviewed and approved as a Class 1 or Class 2
modification. If the permittee requests that the modification be classified
as a Class 1 or 2 modification, the permittee shall provide the Agency
with the necessary information to support the requested classification.
2)
The Agency shall make the determination described in subsection (d)(1),
above, as promptly as practicable. In determining the appropriate class
for a specific modification, the Agency shall consider the similarity of
16
the modification to other modifications codified in Appendix A and the
following criteria:
A)
Class 1 modifications apply to minor changes that keep the
permit current with routine changes to the facility or its
operation. These changes do not substantially alter the permit
conditions or reduce the capacity of the facility to protect human
health or the environment. In the case of Class 1 modifications,
the Agency may require prior approval.
B)
Class 2 modifications apply to changes that are necessary to
enable a permittee to respond, in a timely manner, to any of the
following:
i)
Common variations in the types and quantities of the
wastes managed under the facility permit,
ii)
Technological advances, and
iii)
Changes necessary to comply with new regulations, where
these changes can be implemented without substantially
changing design specifications or management practices in
the permit.
C)
Class 3 modifications substantially alter the facility or its
operation.
e)
Temporary authorizations.
1)
Upon request of the permittee, the Agency shall, without prior public
notice and comment, grant the permittee a temporary authorization in
accordance with this subsection. Temporary authorizations have a term
of not more than 180 days.
2)
Procedures.
A)
The permittee may request a temporary authorization for:
i)
Any Class 2 modification meeting the criteria in
subsection (e)(3)(B), below of this Section,; and
ii)
Any Class 3 modification that meets the criteria in
subsection (e)(3)(B)(i), below; or that meets the criteria in
subsection (e)(3)(B)(iii) through (v), below, and provides
17
improved management or treatment of a hazardous waste
already listed in the facility permit.
B)
The temporary authorization request must include:
i)
A description of the activities to be conducted under the
temporary authorization;
ii)
An explanation of why the temporary authorization is
necessary; and
iii)
Sufficient information to ensure compliance with 35 Ill.
Adm. Code 724 standards.
C)
The permittee shall send a notice about the temporary
authorization request to all persons on the facility mailing list
maintained by the Agency and to appropriate units of State and
local governments as specified in 35 Ill. Adm. Code
705.163(a)(5). This notification must be made within seven days
after submission of the authorization request.
3)
The Agency shall approve or deny the temporary authorization as
quickly as practical. To issue a temporary authorization, the Agency
shall find:
A)
The authorized activities are in compliance with the standards of
35 Ill. Adm. Code 724.
B)
The temporary authorization is necessary to achieve one of the
following objectives before action is likely to be taken on a
modification request:
i)
To facilitate timely implementation of closure or
corrective action activities;
ii)
To allow treatment or storage in tanks, containers or in
containment buildings in accordance with 35 Ill. Adm.
Code 728;
iii)
To prevent disruption of ongoing waste management
activities;
iv)
To enable the permittee to respond to sudden changes in
the types or quantities of the wastes managed under the
facility permit; or
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v)
To facilitate other changes to protect human health and the
environment.
4)
A temporary authorization shall be reissued for one additional term of up
to 180 days provided that the permittee has requested a Class 2 or 3
permit modification for the activity covered in the temporary
authorization, and:
A)
The reissued temporary authorization constitutes the Agency’s
decision on a Class 2 permit modification in accordance with
Section 703.282(f)(1)(D) or (f)(2)(D), or
B)
The Agency determines that the reissued temporary authorization
involving a Class 3 permit modification request is warranted to
allow the authorized activities to continue while the modification
procedures of 35 Ill. Adm. Code 703.283 are conducted.
f)
Public notice and appeals of permit modification decisions.
1)
The Agency shall notify persons on the facility mailing list and
appropriate units of State and local government within 10 days of any
decision to grant or deny a Class 2 or 3 permit modification request.
The Agency shall also notify such persons within 10 days after an
automatic authorization for a Class 2 modification goes into effect under
Section 703.282(f)(3) or (f)(5).
2)
The Agency’s decision to grant or deny a Class 2 or 3 permit
modification request may be appealed under the permit appeal
procedures of 35 Ill. Adm. Code 705.212.
3)
An automatic authorization that goes into effect under Section
703.282(f)(3) or (f)(5) may be appealed under the permit appeal
procedures of 35 Ill. Adm. Code 705.212; however, the permittee may
continue to conduct the activities pursuant to the automatic authorization
until the Board enters a final order on the appeal notwithstanding the
provisions of 35 Ill. Adm. Code 705.204.
g)
Newly regulated wastes and units.
1)
The permittee is authorized to continue to manage wastes listed or
identified as hazardous under 35 Ill. Adm. Code 721, or to continue to
manage hazardous waste in units newly regulated as hazardous waste
management units, if:
19
A)
The unit was in existence as a hazardous waste facility with
respect to the newly listed or characterized waste or newly
regulated waste management unit on the effective date of the final
rule listing or identifying the waste, or regulating the unit;
B)
The permittee submits a Class 1 modification request on or
before the date on which the waste becomes subject to the new
requirements;
C)
The permittee is in compliance with the applicable standards of
35 Ill. Adm. Code 725 and 726;
D)
The permittee also submits a complete class 2 or 3 modification
request within 180 days after the effective date of the rule listing
or identifying the waste, or subjecting the unit to management
standards under 35 Ill. Adm. Code 724, 725 or 726; and
E)
In the case of land disposal units, the permittee certifies that such
unit is in compliance with all applicable requirements of 35 Ill.
Adm. Code 725 for groundwater monitoring and financial
responsibility requirements on the date 12 months after the
effective date of the rule identifying or listing the waste as
hazardous, or regulating the unit as a hazardous waste
management unit. If the owner or operator fails to certify
compliance with all these requirements, the owner or operator
loses authority to operate under this Section.
2)
New wastes or units added to a facility’s permit under this subsection do
not constitute expansions for the purpose of the 25 percent capacity
expansion limit for Class 2 modifications.
h) Military hazardous waste munitions treatment and disposal. The permittee is
authorized to continue to accept waste military munitions notwithstanding any
permit conditions barring the permittee from accepting off-site wastes, if:
1) The facility was in existence as a hazardous waste facility and the facility
was already permitted to handle the waste military munitions on the date
when the waste military munitions became subject to hazardous waste
regulatory requirements;
2) On or before the date when the waste military munitions become subject
to hazardous waste regulatory requirements, the permittee submits a
Class 1 modification request to remove or amend the permit provision
restricting the receipt of off-site waste munitions; and
20
3) The permittee submits a complete Class 2 modification request within
180 days of the date when the waste military munitions became subject
to hazardous waste regulatory requirements.
hi)
Permit modification list. The Agency shall maintain a list of all approved
permit modifications and shall publish a notice once a year in a State-wide
newspaper that an updated list is available for review.
Board NoteBOARD NOTE: Derived from 40 CFR 270.42(d) through (hi)
(19907), as amended at 56 Fed. Reg. 7206, February 21, 1991, and at 56 Fed.
Reg. 32688, July 17, 1991.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 720
HAZARDOUS WASTE MANAGEMENT SYSTEM: GENERAL
SUBPART A: GENERAL PROVISIONS
Section
720.101
Purpose, Scope, and Applicability
720.102
Availability of Information; Confidentiality of Information
720.103
Use of Number and Gender
SUBPART B: DEFINITIONS
Section
720.110
Definitions
720.111
References
SUBPART C: RULEMAKING PETITIONS AND OTHER PROCEDURES
Section
720.120
Rulemaking
720.121
Alternative Equivalent Testing Methods
720.122
Waste Delisting
720.123
Petitions for Regulation as Universal Waste
720.130
Procedures for Solid Waste Determinations
720.131
Solid Waste Determinations
720.132
Boiler Determinations
720.133
Procedures for Determinations
21
720.140
Additional regulation of certain hazardous waste Recycling Activities on a case-
by-case Basis
720.141
Procedures for case-by-case regulation of hazardous waste Recycling Activities
720.Appendix A
Overview of 40 CFR, Subtitle C Regulations
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982; amended and codified
in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982; amended in R82-19 at 7 Ill. Reg. 14015,
effective October 12, 1983; amended in R84-9, 53 PCB 131 at 9 Ill. Reg. 11819, effective July 24, 1985;
amended in R85-22 at 10 Ill. Reg. 968, effective January 2, 1986; amended in R86-1 at 10 Ill. Reg. 13998,
effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20630, effective December 2, 1986; amended in
R86-28 at 11 Ill. Reg. 6017, effective March 24, 1987; amended in R86-46 at 11 Ill. Reg. 13435, effective
August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19280, effective November 12, 1987; amended in R87-26 at 12
Ill. Reg. 2450, effective January 15, 1988; amended in R87-39 at 12 Ill. Reg. 12999, effective July 29, 1988;
amended in R88-16 at 13 Ill. Reg. 362, effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18278,
effective November 13, 1989; amended in R89-2 at 14 Ill. Reg. 3075, effective February 20, 1990; amended in
R89-9 at 14 Ill. Reg. 6225, effective April 16, 1990; amended in R90-10 at 14 Ill. Reg. 16450, effective
September 25, 1990; amended in R90-17 at 15 Ill. Reg. 7934, effective May 9, 1991; amended in R90-11 at 15
Ill. Reg. 9323, effective June 17, 1991; amended in R91-1 at 15 Ill. Reg. 14446, effective September 30, 1991;
amended in R91-13 at 16 Ill. Reg. 9489, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17636, effective
November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5625, effective March 26, 1993; amended in R93-4 at 17
Ill. Reg. 20545, effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6720, effective April 26, 1994;
amended in R94-7 at 18 Ill. Reg. 12160, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17480,
effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9508, effective June 27, 1995; amended in R95-
20 at 20 Ill. Reg. 10929, August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 256, effective
December 16, 1997; amended in R98-12 at 22 Ill. Reg. 7590, effective April 15, 1998; amended in R97-21/R98-
3/R98-5 at 22 Ill. Reg. ________, effective ______________________.
SUBPART B: DEFINITIONS
Section 720.110
Definitions
When used in 35 Ill. Adm. Code 720 through 726 and 728 only, the following terms have the
meanings given below:
“Aboveground tank” means a device meeting the definition of “tank” that is situated
in such a way that the entire surface area of the tank is completely above the plane
of the adjacent surrounding surface and the entire surface area of the tank (including
the tank bottom) is able to be visually inspected.
“Act” or “RCRA” means the Solid Waste Disposal Act, as amended by the
Resource Conservation and Recovery Act of 1976, as amended (42 U.S.C. 6901 et
seq.)
22
“Active life” of a facility means the period from the initial receipt of hazardous
waste at the facility until the Agency receives certification of final closure.
“Active portion” means that portion of a facility where treatment, storage or
disposal operations are being or have been conducted after May 19, 1980, and
which is not a closed portion. (See also “closed portion” and “inactive portion”.)
“Administrator” means the Administrator of the U.S. Environmental Protection
Agency or the Administrator’s designee.
“Agency” means the Illinois Environmental Protection Agency.
“Ancillary equipment” means any device including, but not limited to, such devices
as piping, fittings, flanges, valves and pumps, that is used to distribute, meter or
control the flow of hazardous waste from its point of generation to storage or
treatment tank(s), between hazardous waste storage and treatment tanks to a point of
disposal onsite, or to a point of shipment for disposal off-site.
“Aquifer” means a geologic formation, group of formations or part of a formation
capable of yielding a significant amount of groundwater to wells or springs.
“Authorized representative” means the person responsible for the overall operation
of a facility or an operational unit (i.e., part of a facility), e.g., the plant manager,
superintendent or person of equivalent responsibility.
“Battery” means a device consisting of one or more electrically connected
electrochemical cells that is designed to receive, store, and deliver electric energy.
An electrochemical cell is a system consisting of an anode, cathode, and an
electrolyte, plus such connections (electrical and mechanical) as may be needed to
allow the cell to deliver or receive electrical energy. The term battery also includes
an intact, unbroken battery from which the electrolyte has been removed.
“Board” means the Illinois Pollution Control Board.
“Boiler” means an enclosed device using controlled flame combustion and having
the following characteristics:
Physical characteristics.
The unit must have physical provisions for recovering and exporting
thermal energy in the form of steam, heated fluids or heated gases;
and the unit’s combustion chamber and primary energy recovery
Section(s) section(s) must be of integral design. To be of integral
design, the combustion chamber and the primary energy recovery
Section(s) section(s) (such as waterwalls and superheaters) must be
23
physically formed into one manufactured or assembled unit. A unit
in which the combustion chamber and the primary energy recovery
Section(s) section(s) are joined only by ducts or connections carrying
flue gas is not integrally designed; however, secondary energy
recovery equipment (such as economizers or air preheaters) need not
be physically formed into the same unit as the combustion chamber
and the primary energy recovery Section section. The following
units are not precluded from being boilers solely because they are
not of integral design: process heaters (units that transfer energy
directly to a process stream), and fluidized bed combustion units;
and
While in operation, the unit must maintain a thermal energy
recovery efficiency of at least 60 percent, calculated in terms of the
recovered energy compared with the thermal value of the fuel; and
The unit must export and utilize at least 75 percent of the recovered
energy, calculated on an annual basis. In this calculation, no credit
shall be given for recovered heat used internally in the same unit.
(Examples of internal use are the preheating of fuel or combustion
air, and the driving of induced or forced draft fans or feedwater
pumps); or
Boiler by designation. The unit is one which the Board has determined, on
a case-by-case basis, to be a boiler, after considering the standards in Section
720.132.
“Carbon regeneration unit” means any enclosed thermal treatment device used to
regenerate spent activated carbon.
“Certification” means a statement of professional opinion based upon knowledge
and belief.
“Closed Portion portion” means that portion of a facility which an owner or
operator has closed in accordance with the approved facility closure plan and all
applicable closure requirements. (See also “active portion” and “inactive portion”.)
“Component” means either the tank or ancillary equipment of a tank system.
“Confined aquifer” means an aquifer bounded above and below by impermeable
beds or by beds of distinctly lower permeability than that of the aquifer itself; an
aquifer containing confined groundwater.
“Container” means any portable device in which a material is stored, transported,
treated, disposed of or otherwise handled.
24
“Containment Building building” means a hazardous waste management unit that is
used to store or treat hazardous waste under the provisions of 35 Ill. Adm. Code
724.Subpart DD and 35 Ill. Adm. Code 725.Subpart DD.
“Contingency plan” means a document setting out an organized, planned and
coordinated course of action to be followed in case of a fire, explosion or release of
hazardous waste or hazardous waste constituents which could threaten human health
or the environment.
“Corrective action management unit” or “CAMU” means an area within a facility
that is designated by the Agency under 35 Ill. Adm. Code 724.Subpart S for the
purpose of implementing corrective action requirements under 35 Ill. Adm. Code
724.201 and RCRA section 3008(h). A CAMU shall only be used for the
management of remediation wastes pursuant to implementing such corrective action
requirements at the facility.
BOARD NOTE: USEPA must also designate a CAMU until it grants this authority
to the Agency. See the note following 35 Ill. Adm. Code 724.652.
“Corrosion expert” means a person who, by reason of knowledge of the physical
sciences and the principles of engineering and mathematics, acquired by a
professional education and related practical experience, is qualified to engage in the
practice of corrosion control on buried or submerged metal piping systems and
metal tanks. Such a person must be certified as being qualified by the National
Association of Corrosion Engineers (NACE) or be a registered professional engineer
who has certification or licensing that includes education and experience in
corrosion control on buried or submerged metal piping systems and metal tanks.
“Designated facility” means a hazardous waste treatment, storage or disposal
facility,
Which:
Has received a RCRA permit (or interim status) pursuant to 35 Ill.
Adm. Code 702, 703 and 705;
Has received a RCRA permit from USEPA pursuant to 40 CFR 124
and 270 (1992);
Has received a RCRA permit from a state authorized by USEPA
pursuant to 40 CFR 271 (1992); or
Is regulated under 35 Ill. Adm. Code 721.106(c)(2) or 266.Subpart
F; and
25
Which has been designated on the manifest by the generator pursuant to 35
Ill. Adm. Code 722.120.
If a waste is destined to a facility in a state, other than Illinois, which has
been authorized by USEPA pursuant to 40 CFR 271, but which has not yet
obtained authorization to regulate that waste as hazardous, then the
designated facility must be a facility allowed by the receiving state to accept
such waste.
“Destination facility” means a facility that treats, disposes of, or recycles a
particular category of universal waste, except those management activities described
in 35 Ill. Adm. Code 733.113(a) and (c) and 733.133(a) and (c). A facility at
which a particular category of universal waste is only accumulated is not a
destination facility for the purposes of managing that category of universal waste.
“Dike” means an embankment or ridge of either natural or manmade materials used
to prevent the movement of liquids, sludges, solids or other materials.
“Director” means the Director of the Illinois Environmental Protection Agency.
“Discharge” or “hazardous waste discharge” means the accidental or intentional
spilling, leaking, pumping, pouring, emitting, emptying or dumping of hazardous
waste into or on any land or water.
“Disposal” means the discharge, deposit, injection, dumping, spilling, leaking or
placing of any solid waste or hazardous waste into or on any land or water so that
such solid waste or hazardous waste or any constituent thereof may enter the
environment or be emitted into the air or discharged into any waters, including
groundwaters.
“Disposal facility” means a facility or part of a facility at which hazardous waste is
intentionally placed into or on any land or water and at which waste will remain
after closure. The term disposal facility does not include a corrective action
management unit (CAMU) into which remediation wastes are placed.
“Drip pad” means an engineered structure consisting of a curbed, free-draining
base, constructed of non-earthen materials and designed to convey preservative kick-
back or drippage from treated wood, precipitation and surface water run-on to an
associated collection system at wood preserving plants.
“Electric lamp” means the bulb or tube portion of a lighting device specifically
designed to produce radiant energy, most often in the ultraviolet, visible, and
infrared regions of the electromagnetic spectrum.
26
BOARD NOTE: The definition of “electric lamp” was added pursuant to
Section 22.23a of the Act [415 ILCS 5/22.23a] (see P.A. 90-502, effective
August 19, 1997).
“Elementary neutralization unit” means a device which:
Is used for neutralizing wastes which are hazardous only because they
exhibit the corrosivity characteristic defined in 35 Ill. Adm. Code 721.122
or are listed in 35 Ill. Adm. Code 721.Subpart D only for this reason; and
Meets the definition of tank, tank system, container, transport vehicle or
vessel in this Section.
“EPA hazardous waste number” or “USEPA hazardous waste number” means the
number assigned by USEPA to each hazardous waste listed in 35 Ill. Adm. Code
721.Subpart D and to each characteristic identified in 35 Ill. Adm. Code
721.Subpart C.
“EPA identification number” or “USEPA identification number” means the number
assigned by USEPA pursuant to 35 Ill. Adm. Code 722 through 725 to each
generator, transporter and treatment, storage or disposal facility.
“EPA region” or “USEPA region” means the states and territories found in any
one of the following ten regions:
Region I: Maine, Vermont, New Hampshire, Massachusetts, Connecticut
and Rhode Island
Region II: New York, New Jersey, Commonwealth of Puerto Rico and the
U.S. Virgin Islands
Region III: Pennsylvania, Delaware, Maryland, West Virginia, Virginia
and the District of Columbia
Region IV: Kentucky, Tennessee, North Carolina, Mississippi, Alabama,
Georgia, South Carolina and Florida
Region V: Minnesota, Wisconsin, Illinois, Michigan, Indiana and Ohio
Region VI: New Mexico, Oklahoma, Arkansas, Louisiana and Texas
Region VII: Nebraska, Kansas, Missouri and Iowa
Region VIII: Montana, Wyoming, North Dakota, South Dakota, Utah and
Colorado
27
Region IX: California, Nevada, Arizona, Hawaii, Guam, American Samoa
and Commonwealth of the Northern Mariana Islands
Region X: Washington, Oregon, Idaho and Alaska
“Equivalent method” means any testing or analytical method approved by the Board
pursuant to Section 720.120.
“Existing hazardous waste management (HWM) facility” or “existing facility”
means a facility which was in operation or for which construction commenced on or
before November 19, 1980. A facility had commenced construction if the owner or
operator had obtained the federal, state, and local approvals or permits necessary to
begin physical construction and either:
A continuous on-site, physical construction program had begun or
The owner or operator had entered into contractual obligations -- -- which
could not be canceled or modified without substantial loss -- -- for physical
construction of the facility to be completed within a reasonable time.
“Existing portion” means that land surface area of an existing waste management
unit, included in the original Part A permit application, on which wastes have been
placed prior to the issuance of a permit.
“Existing tank system” or “existing component” means a tank system or component
that is used for the storage or treatment of hazardous waste and that is in operation,
or for which installation has commenced on or prior to July 14, 1986. Installation
will be considered to have commenced if the owner or operator has obtained all
federal, State state, and local approvals or permits necessary to begin physical
construction of the site or installation of the tank system and if either
A continuous on-site physical construction or installation program has
begun; or
The owner or operator has entered into contractual obligations -- -- which
cannot be canceled or modified without substantial loss -- -- for physical
construction of the site or installation of the tank system to be completed
within a reasonable time.
“Explosives or munitions emergency” means a situation involving the suspected
or detected presence of unexploded ordnance (UXO), damaged or deteriorated
explosives or munitions, an improvised explosive device (IED), other
potentially explosive material or device, or other potentially harmful military
chemical munitions or device, that creates an actual or potential imminent threat
28
to human health, including safety, or the environment, including property, as
determined by an explosives or munitions emergency response specialist. Such
situations may require immediate and expeditious action by an explosives or
munitions emergency response specialist to control, mitigate, or eliminate the
threat.
“Explosives or munitions emergency response” means all immediate response
activities by an explosives and munitions emergency response specialist to
control, mitigate, or eliminate the actual or potential threat encountered during
an explosives or munitions emergency. An explosives or munitions emergency
response may include in-place render-safe procedures, treatment, or destruction
of the explosives or munitions and/or transporting those items to another
location to be rendered safe, treated, or destroyed. Any reasonable delay in the
completion of an explosives or munitions emergency response caused by a
necessary, unforeseen, or uncontrollable circumstance will not terminate the
explosives or munitions emergency. Explosives and munitions emergency
responses can occur on either public or private lands and are not limited to
responses at RCRA facilities.
“Explosives or munitions emergency response specialist” means an individual
trained in chemical or conventional munitions or explosives handling,
transportation, render-safe procedures, or destruction techniques. Explosives or
munitions emergency response specialists include U.S. Department of Defense
(U.S. DOD) emergency explosive ordnance disposal (EOD), technical escort
unit (TEU), and U.S. DOD-certified civilian or contractor personnel and other
federal, state, or local government or civilian personnel who are similarly
trained in explosives or munitions emergency responses.
“Facility” means:
All contiguous land and structures, other appurtenances, and improvements
on the land used for treating, storing, or disposing of hazardous waste. A
facility may consist of several treatment, storage, or disposal operational
units (e.g., one or more landfills, surface impoundments, or combinations of
them).
For the purpose of implementing corrective action under 35 Ill. Adm. Code
724.201, all contiguous property under the control of the owner or operator
seeking a permit under Subtitle C of RCRA. This definition also applies to
facilities implementing corrective action under RCRA Section 3008(h).
“Federal agency” means any department, agency or other instrumentality of the
federal government, any independent agency or establishment of the federal
government including any government corporation and the Government Printing
Office.
29
“Federal, state, and local approvals or permits necessary to begin physical
construction” means permits and approvals required under federal, state, or local
hazardous waste control statutes, regulations or ordinances.
“Final closure” means the closure of all hazardous waste management units at the
facility in accordance with all applicable closure requirements so that hazardous
waste management activities under 35 Ill. Adm. Code 724 and 725 are no longer
conducted at the facility unless subject to the provisions of 35 Ill. Adm. Code
722.134.
“Food-chain crops” means tobacco, crops grown for human consumption and crops
grown for feed for animals whose products are consumed by humans.
“Freeboard” means the vertical distance between the top of a tank or surface
impoundment dike and the surface of the waste contained therein.
“Free liquids” means liquids which readily separate from the solid portion of a
waste under ambient temperature and pressure.
“Generator” means any person, by site, whose act or process produce hazardous
waste identified or listed in 35 Ill. Adm. Code 721 or whose act first causes a
hazardous waste to become subject to regulation.
“Groundwater” means water below the land surface in a zone of saturation.
“Hazardous waste” means a hazardous waste as defined in 35 Ill. Adm. Code
721.103.
“Hazardous waste constituent” means a constituent which caused the hazardous
waste to be listed in 35 Ill. Adm. Code 721.Subpart D, or a constituent listed in of
35 Ill. Adm. Code 721.124.
“Hazardous waste management unit” is a contiguous area of land on or in which
hazardous waste is placed, or the largest area in which there is significant likelihood
of mixing hazardous waste constituents in the same area. Examples of hazardous
waste management units include a surface impoundment, a waste pile, a land
treatment area, a landfill cell, an incinerator, a tank and its associated piping and
underlying containment system and a container storage area. A container alone does
not constitute a unit; the unit includes containers and the land or pad upon which
they are placed.
“Inactive portion” means that portion of a facility which is not operated after
November 19, 1980. (See also “active portion” and “closed portion”.)
30
“Incinerator” means any enclosed device that:
Uses controlled flame combustion and neither:
Meets the criteria for classification as a boiler, sludge dryer or
carbon regeneration unit, nor
Is listed as an industrial furnace; or
Meets the definition of infrared incinerator or plasma arc incinerator.
“Incompatible waste” means a hazardous waste which is unsuitable for:
Placement in a particular device or facility because it may cause corrosion or
decay of containment materials (e.g., container inner liners or tank walls);
or
Commingling with another waste or material under uncontrolled conditions
because the commingling might produce heat or pressure, fire or explosion,
violent reaction, toxic dusts, mists, fumes or gases or flammable fumes or
gases.
(See 35 Ill. Adm. Code 725.Appendix E for examples.)
“Industrial furnace” means any of the following enclosed devices that are integral
components of manufacturing processes and that use thermal treatment to
accomplish recovery of materials or energy:
Cement kilns
Lime kilns
Aggregate kilns
Phosphate kilns
Coke ovens
Blast furnaces
Smelting, melting and refining furnaces (including pyrometallurgical devices
such as cupolas, reverberator furnaces, sintering machines, roasters and
foundry furnaces)
Titanium dioxide chloride process oxidation reactors
31
Methane reforming furnaces
Pulping liquor recovery furnaces
Combustion devices used in the recovery of sulfur values from spent sulfuric
acid
Halogen acid furnaces (HAFs) for the production of acid from halogenated
hazardous waste generated by chemical production facilities where the
furnace is located on the site of a chemical production facility, the acid
product has a halogen acid content of at least 3% three percent, the acid
product is used in a manufacturing process and, except for hazardous waste
burned as fuel, hazardous waste fed to the furnace has a minimum halogen
content of 20% percent, as generated
Any other such device as the Agency determines to be an “Industrial
Furnace” on the basis of one or more of the following factors:
The design and use of the device primarily to accomplish recovery of
material products;
The use of the device to burn or reduce raw materials to make a
material product;
The use of the device to burn or reduce secondary materials as
effective substitutes for raw materials, in processes using raw
materials as principal feedstocks;
The use of the device to burn or reduce secondary materials as
ingredients in an industrial process to make a material product;
The use of the device in common industrial practice to produce a
material product; and
Other relevant factors.
“Individual generation site” means the contiguous site at or on which one or more
hazardous wastes are generated. An individual generation site, such as a large
manufacturing plant, may have one or more sources of hazardous waste but is
considered a single or individual generation site if the site or property is contiguous.
“Infrared incinerator” means any enclosed device which uses electric powered
resistance heaters as a source of radiant heat followed by an afterburner using
controlled flame combustion and which is not listed as an industrial furnace.
32
“Inground tank” means a device meeting the definition of “tank” whereby a portion
of the tank wall is situated to any degree within the ground, thereby preventing
visual inspection of that external surface area of the tank that is in the ground.
“In operation” refers to a facility which is treating, storing or disposing of
hazardous waste.
“Injection well” means a well into which fluids are being injected. (See also
“underground injection”.)
“Inner liner” means a continuous layer of material placed inside a tank or container
which protects the construction materials of the tank or container from the contained
waste or reagents used to treat the waste.
“Installation inspector” means a person who, by reason of knowledge of the
physical sciences and the principles of engineering, acquired by a professional
education and related practical experience, is qualified to supervise the installation of
tank systems.
“International shipment” means the transportation of hazardous waste into or out of
the jurisdiction of the United States.
“Land treatment facility” means a facility or part of a facility at which hazardous
waste is applied onto or incorporated into the soil surface; such facilities are disposal
facilities if the waste will remain after closure.
“Landfill” means a disposal facility or part of a facility where hazardous waste is
placed in or on land and which is not a pile, a land treatment facility, a surface
impoundment, an underground injection well, a salt dome formation, a salt bed
formation, an underground mine, a cave, or a corrective action management unit
(CAMU).
“Landfill cell” means a discrete volume of a hazardous waste landfill which uses a
liner to provide isolation of wastes from adjacent cells or wastes. Examples of
landfill cells are trenches and pits.
“LDS” means leak detection system.
“Leachate” means any liquid, including any suspended components in the liquid,
that has percolated through or drained from hazardous waste.
“Liner” means a continuous layer of natural or manmade materials beneath or on
the sides of a surface impoundment, landfill or landfill cell, which restricts the
33
downward or lateral escape of hazardous waste, hazardous waste constituents or
leachate.
“Leak-detection system” means a system capable of detecting the failure of either
the primary or secondary containment structure or the presence of a release of
hazardous waste or accumulated liquid in the secondary containment structure.
Such a system must employ operational controls (e.g., daily visual inspections for
releases into the secondary containment system of aboveground tanks) or consist of
an interstitial monitoring device designed to detect continuously and automatically
the failure of the primary or secondary containment structure or the presence of a
release of hazardous waste into the secondary containment structure.
“Management” or “hazardous waste management” means the systematic control of
the collection, source separation, storage, transportation, processing, treatment,
recovery and disposal of hazardous waste.
“Manifest” means the shipping document originated and signed by the generator
which contains the information required by 35 Ill. Adm. Code 722.Subpart B.
“Manifest document number” means the USEPA twelve digit identification number
assigned to the generator plus a unique five digit document number assigned to the
manifest by the generator for recording and reporting purposes.
“Mercury-containing lamp” means an electric lamp into which mercury is
purposely introduced by the manufacturer for the operation of the lamp.
Mercury-containing lamps include, but are not limited to, fluorescent lamps and
high-intensity discharge lamps.
BOARD NOTE: The definition of “mercury-containing lamp” was added
pursuant to Section 22.23a of the Act [415 ILCS 5/22.23a] (see P.A. 90-502,
effective August 19, 1997).
“Military munitions” means all ammunition products and components produced
or used by or for the U.S. Department of Defense or the U.S. Armed Services
for national defense and security, including military munitions under the control
of the U.S. Department of Defense, the U.S. Coast Guard, the U.S.
Department of Energy (U.S. DOE), and National Guard personnel. The term
military munitions includes: confined gaseous, liquid, and solid propellants,
explosives, pyrotechnics, chemical and riot control agents, smokes, and
incendiaries used by U.S. DOD components, including bulk explosives and
chemical warfare agents, chemical munitions, rockets, guided and ballistic
missiles, bombs, warheads, mortar rounds, artillery ammunition, small arms
ammunition, grenades, mines, torpedoes, depth charges, cluster munitions and
dispensers, demolition charges, and devices and components of these items and
devices. Military munitions do not include wholly inert items, improvised
explosive devices, and nuclear weapons, nuclear devices, and nuclear
34
components of these items and devices. However, the term does include non-
nuclear components of nuclear devices, managed under U.S. DOE's nuclear
weapons program after all sanitization operations required under the Atomic
Energy Act of 1954, as amended, have been completed.
“Mining overburden returned to the mine site” means any material overlying an
economic mineral deposit which is removed to gain access to that deposit and is then
used for reclamation of a surface mine.
“Miscellaneous unit” means a hazardous waste management unit where hazardous
waste is treated, stored or disposed of and which is not a container, tank, tank
system, surface impoundment, pile, land treatment unit, landfill, incinerator, boiler,
industrial furnace, underground injection well with appropriate technical standards
under 35 Ill. Adm. Code 730, containment building, corrective action management
unit (CAMU), or a unit eligible for a research, development and demonstration
permit under 35 Ill. Adm. Code 703.231.
“Movement” means that hazardous waste transported to a facility in an individual
vehicle.
“New hazardous waste management facility” or “new facility” means a facility
which began operation, or for which construction commenced, after November 19,
1980. (See also “Existing hazardous waste management facility”.)
“New tank system” or “new tank component” means a tank system or component
that will be used for the storage or treatment of hazardous waste and for which
installation commenced after July 14, 1986; except, however, for purposes of 35 Ill.
Adm. Code 724.293(g)(2) and 725.293(g)(2), a new tank system is one for which
construction commences after July 14, 1986. (See also “existing tank system”.)
“Onground tank” means a device meeting the definition of “tank” that is situated in
such a way that the bottom of the tank is on the same level as the adjacent
surrounding surfaces so that the external tank bottom cannot be visually inspected.
“On-site” means the same or geographically contiguous property which may be
divided by public or private right-of-way, provided the entrance and exit between
the properties is at a crossroads intersection and access is by crossing as opposed to
going along the right-of-way. Noncontiguous properties owned by the same person
but connected by a right-of-way which he controls and to which the public does not
have access is also considered on-site property.
“Open burning” means the combustion of any material without the following
characteristics:
35
Control of combustion air to maintain adequate temperature for efficient
combustion;
Containment of the combustion reaction in an enclosed device to provide
sufficient residence time and mixing for complete combustion; and
Control of emission of the gaseous combustion products.
(See also “incineration” and “thermal treatment”.)
“Operator” means the person responsible for the overall operation of a facility.
“Owner” means the person who owns a facility or part of a facility.
“Partial closure” means the closure of a hazardous waste management unit in
accordance with the applicable closure requirements of 35 Ill. Adm. Code 724 or
725 at a facility which contains other active hazardous waste management units.
For example, partial closure may include the closure of a tank (including its
associated piping and underlying containment systems), landfill cell, surface
impoundment, waste pile or other hazardous waste management unit, while other
units of the same facility continue to operate.
“Person” means an individual, trust, firm, joint stock company, federal agency,
corporation (including a government corporation), partnership, association, state,
municipality, commission, political subdivision of a state or any interstate body.
“Personnel” or “facility personnel” means all persons who work at or oversee the
operations of a hazardous waste facility and whose actions or failure to act may
result in noncompliance with the requirements of 35 Ill. Adm. Code 724 or 725.
“Pesticide” means any substance or mixture of substances intended for preventing,
destroying, repelling, or mitigating any pest or intended for use as a plant regulator,
defoliant, or desiccant, other than any article that fulfills one of the following
descriptions:
It is a new animal drug under Section 201(v) of the Federal Food, Drug and
Cosmetic Act (FFDCA; 21 U.S.C. § 321(v)), incorporated by reference in
Section 720.111,
It is an animal drug that has been determined by regulation of the federal
Secretary of Health and Human Services pursuant to FFDCA Section 512,
incorporated by reference in Section 720.111, to be an exempted new
animal drug, or
36
It is an animal feed under FFDCA Section 201(w) (21 U.S.C. § 321(w)),
incorporated by reference in Section 720.111 that bears or contains any
substances described in either of the two preceding subsections of this
definition.
BOARD NOTE: The second exception of corresponding 40 CFR 260.10
reads as follows: “Is an animal drug that has been determined by regulation
of the Secretary of Health and Human Services not to be a new animal
drug”. This is very similar to the language of Section 2(u) of the Federal
Insecticide, Fungicide, and Rodenticide Act (FIFRA; 7 U.S.C. § 136(u)).
The three exceptions, taken together, appear intended not to include as
“pesticide” any material within the scope of federal Food and Drug
Administration regulation. The Board codified this provision with the intent
of retaining the same meaning as its federal counterpart while adding the
definiteness required under Illinois law.
“Pile” means any noncontainerized accumulation of solid, non-flowing hazardous
waste that is used for treatment or storage, and that is not a containment building.
“Plasma arc incinerator” means any enclosed device which uses a high intensity
electrical discharge or arc as a source of heat followed by an afterburner using
controlled flame combustion and which is not listed as an industrial furnace.
“Point source” means any discernible, confined and discrete conveyance including,
but not limited to, any pipe, ditch, channel, tunnel, conduit, well, discrete fissure,
container, rolling stock, concentrated animal feeding operation or vessel or other
floating craft from which pollutants are or may be discharged. This term does not
include return flows from irrigated agriculture.
“Publicly owned treatment works” or “POTW” is as defined in 35 Ill. Adm. Code
310.110.
“Qualified groundwater scientist” means a scientist or engineer who has received a
baccalaureate or postgraduate degree in the natural sciences or engineering, and has
sufficient training and experience in groundwater hydrology and related fields, as
demonstrated by state registration, professional certifications or completion of
accredited university courses that enable the individual to make sound professional
judgments regarding groundwater monitoring and contaminant fate and transport.
BOARD NOTE: “State registration” includes, but is not limited to, registration as
a professional engineer with the Department of Professional Regulation, pursuant to
225 ILCS 325/1 and 68 Ill. Adm. Code 1380. “Professional certification” includes,
but is not limited to, certification under the certified ground water professional
program of the National Ground Water Association.
“Regional Administrator” means the Regional Administrator for the EPA Region in
which the facility is located or the Regional Administrator’s designee.
37
“Remediation waste” means all solid and hazardous wastes, and all media
(including groundwater, surface water, soils, and sediments) and debris that contain
listed hazardous wastes or which themselves exhibit a hazardous waste characteristic
which are managed for the purpose of implementing corrective action requirements
under 35 Ill. Adm. Code 724.201 and RCRA Section 3008(h). For a given facility,
remediation wastes may originate only from within the facility boundary, but may
include waste managed in implementing RCRA sections 3004(v) or 3008(h) for
releases beyond the facility boundary.
“Replacement unit” means a landfill, surface impoundment or waste pile unit from
which all or substantially all of the waste is removed, and which is subsequently
reused to treat, store or dispose of hazardous waste. “Replacement unit” does not
include a unit from which waste is removed during closure, if the subsequent reuse
solely involves the disposal of waste from that unit and other closing units or
corrective action areas at the facility, in accordance with a closure or corrective
action plan approved by USEPA or the Agency.
“Representative sample” means a sample of a universe or whole (e.g., waste pile,
lagoon, groundwater) which can be expected to exhibit the average properties of the
universe or whole.
“Runoff” means any rainwater, leachate or other liquid that drains over land from
any part of a facility.
“Runon” means any rainwater, leachate or other liquid that drains over land onto
any part of a facility.
“Saturated zone” or “zone of saturation” means that part of the earth’s crust in
which all voids are filled with water.
“SIC Code” means Standard Industrial Code as defined in Standard Industrial
Classification Manual, incorporated by reference in Section 720.111.
“Sludge” means any solid, semi-solid or liquid waste generated from a municipal,
commercial or industrial wastewater treatment plant, water supply treatment plant or
air pollution control facility exclusive of the treated effluent from a wastewater
treatment plant.
“Sludge dryer” means any enclosed thermal treatment device which is used to
dehydrate sludge and which has a total thermal input, excluding the heating value of
the sludge itself, of 2500 Btu/lb or less of sludge treated on a wet weight basis.
“Small Quantity Generator” means a generator which generates less than 1000 kg of
hazardous waste in a calendar month.
38
“Solid waste” means a solid waste as defined in 35 Ill. Adm. Code 721.102.
“Sorbent” means a material that is used to soak up free liquids by either adsorption
or absorption, or both. “Sorb” means to either adsorb or absorb, or both.
“Sump” means any pit or reservoir that meets the definition of tank and those
troughs or trenches connected to it that serve to collect hazardous waste for transport
to hazardous waste storage, treatment or disposal facilities; except that, as used in
the landfill, surface impoundment and waste pile rules, “sump” means any lined pit
or reservoir that serves to collect liquids drained from a leachate collection and
removal system or leak detection system for subsequent removal from the system.
“State” means any of the several states, the District of Columbia, the
Commonwealth of Puerto Rico, the Virgin Islands, Guam, American Samoa and the
Commonwealth of the Northern Mariana Islands.
“Storage” means the holding of hazardous waste for a temporary period, at the end
of which the hazardous waste is treated, disposed of or stored elsewhere.
“Surface impoundment” or “impoundment” means a facility or part of a facility
which is a natural topographic depression, manmade excavation or diked area
formed primarily of earthen materials (although it may be lined with manmade
materials) which is designed to hold an accumulation of liquid wastes or wastes
containing free liquids and which is not an injection well. Examples of surface
impoundments are holding, storage, settling and aeration pits, ponds and lagoons.
“Tank” means a stationary device, designed to contain an accumulation of
hazardous waste which is constructed primarily of nonearthen materials (e.g., wood,
concrete, steel, plastic) which provide structural support.
“Tank system” means a hazardous waste storage or treatment tank and its associated
ancillary equipment and containment system.
“Thermal treatment” means the treatment of hazardous waste in a device which uses
elevated temperatures as the primary means to change the chemical, physical or
biological character or composition of the hazardous waste. Examples of thermal
treatment processes are incineration, molten salt, pyrolysis, calcination, wet air
oxidation and microwave discharge. (See also “incinerator” and “open burning”.)
“Thermostat” means a temperature control device that contains metallic mercury in
an ampule attached to a bimetal sensing element and mercury-containing ampules
that have been removed from such a temperature control device in compliance with
the requirements of 35 Ill. Adm. Code 733.113(c)(2) or 733.133(c)(2).
39
“Totally enclosed treatment facility” means a facility for the treatment of hazardous
waste which is directly connected to an industrial production process and which is
constructed and operated in a manner which prevents the release of any hazardous
waste or any constituent thereof into the environment during treatment. An example
is a pipe in which waste acid is neutralized.
“Transfer facility” means any transportation related facility including loading docks,
parking areas, storage areas and other similar areas where shipments of hazardous
waste are held during the normal course of transportation.
“Transport vehicle” means a motor vehicle or rail car used for the transportation of
cargo by any mode. Each cargo-carrying body (trailer, railroad freight car, etc.) is
a separate transport vehicle.
“Transportation” means the movement of hazardous waste by air, rail, highway or
water.
“Transporter” means a person engaged in the off-site transportation of hazardous
waste by air, rail, highway or water.
“Treatability study” means:
A study in which a hazardous waste is subjected to a treatment process to
determine:
Whether the waste is amenable to the treatment process.
What pretreatment (if any) is required.
The optimal process conditions needed to achieve the desired
treatment.
The efficiency of a treatment process for a specific waste or wastes.
Or,
The characteristics and volumes of residuals from a particular
treatment process.
Also included in this definition for the purpose of 35 Ill. Adm. Code
721.104(e) and (f) exemptions are liner compatibility, corrosion and other
material compatibility studies and toxicological and health effects studies. A
“treatability study” is not a means to commercially treat or dispose of
hazardous waste.
40
“Treatment” means any method, technique or process, including neutralization,
designed to change the physical, chemical or biological character or composition of
any hazardous waste so as to neutralize such waste, or so as to recover energy or
material resources from the waste or so as to render such waste non-hazardous or
less hazardous; safer to transport, store or dispose of; or amenable for recovery,
amenable for storage or reduced in volume.
“Treatment zone” means a soil area of the unsaturated zone of a land treatment unit
within which hazardous constituents are degraded, transformed or immobilized.
“Underground injection” means the subsurface emplacement of fluids through a
bored, drilled or driven well; or through a dug well, where the depth of the dug
well is greater than the largest surface dimension. (See also “injection well”.)
“Underground tank” means a device meeting the definition of “tank” whose entire
surface area is totally below the surface of and covered by the ground.
“Unfit-for-use tank system” means a tank system that has been determined through
an integrity assessment or other inspection to be no longer capable of storing or
treating hazardous waste without posing a threat of release of hazardous waste to the
environment.
“United States” means the 50 States states, the District of Columbia, the
Commonwealth of Puerto Rico, the U.S. Virgin Islands, Guam, American Samoa
and the Commonwealth of the Northern Mariana Islands.
“Universal waste” means any of the following hazardous wastes that are managed
under the universal waste requirements of 35 Ill. Adm. Code 733:
Batteries, as described in 35 Ill. Adm. Code 733.102;
Pesticides, as described in 35 Ill. Adm. Code 733.103;
Thermostats, as described in 35 Ill. Adm. Code 733.104; and
Mercury-containing lamps, as described in 35 Ill. Adm. Code 733.107.
BOARD NOTE: Mercury-containing lamps were added as universal
waste pursuant to Section 22.23a of the Act [415 ILCS 5/22.23a] (see
P.A. 90-502, effective August 19, 1997).
“Universal waste handler” means either of the following:
A generator (as defined in this Section) of universal waste; or
41
The owner or operator of a facility, including all contiguous property, that
receives universal waste from other universal waste handlers, accumulates
the universal waste, and sends that universal waste to another universal
waste handler, to a destination facility, or to a foreign destination.
“Universal waste handler” does not mean:
A person that treats (except under the provisions of Section
733.113(a) or (c) or 733.133(a) or (c)), disposes of, or recycles
universal waste; or
A person engaged in the off-site transportation of universal waste by
air, rail, highway, or water, including a universal waste transfer
facility.
“Universal waste transporter” means a person engaged in the off-site transportation
of universal waste by air, rail, highway, or water.
“Unsaturated zone” or “zone of aeration” means the zone between the land surface
and the water table.
“Uppermost aquifer” means the geologic formation nearest the natural ground
surface that is an aquifer, as well as lower aquifers that are hydraulically
interconnected with this aquifer within the facility’s property boundary.
“USDOT” or “Department of Transportation” means the United States Department
of Transportation.
“Used oil” means any oil that has been refined from crude oil, or any synthetic oil,
that has been used and as a result of such use is contaminated by physical or
chemical impurities.
“USEPA” or “EPA” or “U.S. EPA” means the United States Environmental
Protection Agency.
“Vessel” includes every description of watercraft, used or capable of being used as
a means of transportation on the water.
“Wastewater treatment unit” means a device which:
Is part of a wastewater treatment facility which has an NPDES permit
pursuant to 35 Ill. Adm. Code 309 or a pretreatment permit or authorization
to discharge pursuant to 35 Ill. Adm. Code 310; and
42
Receives and treats or stores an influent wastewater which is a hazardous
waste as defined in 35 Ill. Adm. Code 721.103, or generates and
accumulates a wastewater treatment sludge which is a hazardous waste as
defined in 35 Ill. Adm. Code 721.103, or treats or stores a wastewater
treatment sludge which is a hazardous waste as defined in 35 Ill. Adm. Code
721.103; and
Meets the definition of tank or tank system in this Section.
“Water (bulk shipment)” means the bulk transportation of hazardous waste which is
loaded or carried on board a vessel without containers or labels.
“Well” means any shaft or pit dug or bored into the earth, generally of a cylindrical
form, and often walled with bricks or tubing to prevent the earth from caving in.
“Well injection” (See “underground injection”).
“Zone of engineering control” means an area under the control of the owner or
operator that, upon detection of a hazardous waste release, can be readily cleaned up
prior to the release of hazardous waste or hazardous constituents to groundwater or
surface water.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 720.111
References
a)
The following publications are incorporated by reference for the purposes of this
Part and 35 Ill. Adm. Code 703 through 705, 721 through 726, 728, 730, 731,
733, 738, and 739:
ACI. Available from the American Concrete Institute, Box 19150,
Redford Station, Detroit, Michigan 48219:
ACI 318-83: “Building Code Requirements for Reinforced
Concrete”, adopted September, 1983.
ANSI. Available from the American National Standards Institute, 1430
Broadway, New York, New York 10018, 212-354-3300:
ANSI B31.3 and B31.4. See ASME/ANSI B31.3 and B31.4.
API. Available from the American Petroleum Institute, 1220 L Street,
N.W., Washington, D.C. 20005, 202-682-8000:
43
“Cathodic Protection of Underground Petroleum Storage Tanks
and Piping Systems”, API Recommended Practice 1632, Second
Edition, December, 1987.
“Evaporative Loss from External Floating-Roof Tanks”, API
Publication 2517, Third Edition, February, 1989.
“Guide for Inspection of Refinery Equipment, Chapter XIII,
Atmospheric and Low Pressure Storage Tanks”, 4th Edition,
1981, reaffirmed December, 1987.
“Installation of Underground Petroleum Storage Systems”, API
Recommended Practice 1615, Fourth Edition, November, 1987.
APTI. Available from the Air and Waste Management Association, Box
2861, Pittsburgh, PA 15230, 412-232-3444:
APTI Course 415: Control of Gaseous Emissions, USEPA
Publication EPA-450/2-81-005, December, 1981.
ASME. Available from the American Society of Mechanical Engineers,
345 East 47th Street, New York, NY 10017, 212-705-7722:
“Chemical Plant and Petroleum Refinery Piping”, ASME/ANSI
B31.3-1987, as supplemented by B31.3a-1988 and B31.3b-1988.
Also available from ANSI.
“Liquid Transportation Systems for Hydrocarbons, Liquid
Petroleum Gas, Anhydrous Ammonia, and Alcohols”,
ASME/ANSI B31.4-1986, as supplemented by B31.4a-1987.
Also available from ANSI.
ASTM. Available from American Society for Testing and Materials,
1916 Race Street, Philadelphia, PA 19103, 215-299-5400:
ASTM C 94-90, Standard Specification for Ready-Mixed
Concrete, approved March 30, 1990.
ASTM D 88-87, Standard Test Method for Saybolt Viscosity,
April 24, 1981, reapproved January, 1987.
ASTM D 93-85, Standard Test Methods for Flash Point by
Pensky-Martens Closed Tester, approved October 25, 1985.
44
ASTM D 1946-90, Standard Practice for Analysis of Reformed
Gas by Gas Chromatography, Aapproved March 30, 1990.
ASTM D 2161-87, Standard Practice for Conversion of
Kinematic Viscosity to Saybolt Universal or to Saybolt Furol
Viscosity, March 27, 1987.
ASTM D 2267-88, Standard Test Method for Aromatics in Light
Naphthas and Aviation Gasolines by Gas Chromatography,
approved November 17, 1988.
ASTM D 2382-88, Standard Test Method for Heat of
Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High
Precision Method), approved October 31, 1988.
ASTM D 2879-86, Standard Test Method for Vapor Pressure-
Temperature Relationship and Initial Decomposition Temperature
of Liquids by Isoteniscope, approved October 31, 1986.
ASTM D 2879-92, Standard Test Method for Vapor Pressure-
Temperature Relationship and Initial Decomposition Temperature
of Liquids by Isoteniscope, approved 1992.
ASTM D 3828-87, Standard Test Methods for Flash Point of
Liquids by Setaflash Closed Tester, approved December 14,
1988.
ASTM E 168-88, Standard Practices for General Techniques of
Infrared Quantitative Analysis, approved May 27, 1988.
ASTM E 169-87, Standard Practices for General Techniques of
Ultraviolet-Visible Quantitative Analysis, approved February 1,
1987.
ASTM E 260-85, Standard Practice for Packed Column Gas
Chromatography, approved June 28, 1985.
ASTM E 926-88 C, Standard Test Methods for Preparing Refuse-
Derived Fuel (RDF) Samples for Analysis of Metals, Bomb-Acid
Digestion Method, approved March 25, 1988.
ASTM Method G 21-70 (1984a) -- Standard Practice for
Determining Resistance of Synthetic Polymer Materials to Fungi.
45
ASTM Method G 22-76 (1984b) -- Standard Practice for
Determining Resistance of Plastics to Bacteria.
GPO. Available from the Superintendent of Documents, U.S.
Government Printing Office, Washington, D.C. 20402, 202-783-3238:
Standard Industrial Classification Manual (1972), and 1977
Supplement, republished in 1983.
“Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, USEPA Publication number SW-846 (Third Edition,
November, 1986), as amended by Updates I (July, 1992), II
(September, 1994), IIA (August, 1993), and IIB (January, 1995),
and III (December, 1996) (Document Number 955-001-00000-1).
NACE. Available from the National Association of Corrosion
Engineers, 1400 South Creek Dr., Houston, TX 77084, 713-492-0535:
“Control of External Corrosion on Metallic Buried, Partially
Buried, or Submerged Liquid Storage Systems”, NACE
Recommended Practice RP0285-85 RP-02-85, approved March,
1985.
NFPA. Available from the National Fire Protection Association,
Batterymarch Park, Boston, MA 02269, 617-770-3000 or 800-344-
3555:
“Flammable and Combustible Liquids Code” NFPA 30, issued
July 17, 1987. Also available from ANSI.
NTIS. Available from the U.S. Department of Commerce, National
Technical Information Service, 5285 Port Royal Road, Springfield, VA
22161, 703-487-4600:
APTI Course 415: Control of Gaseous Emissions, USEPA
Publication EPA-450/2-81-005, December, 1981.
“Generic Quality Assurance Project Plan for Land Disposal
Restrictions Program”, EPA/530-SW-87-011, March 15, 1987.
(Document number PB 88-170766.)
“Guidance Guideline on Air Quality Models”, Revised 1986.
(Document number PB86-245-248 (Guideline) and PB88-150-958
(Supplement), also set forth at 40 CFR 51, Appendix W).
46
“Methods for Chemical Analysis of Water and Wastes”, Third
Edition, March, 1983. (Document number PB 84-128677).
“Methods Manual for Compliance with BIF Regulations”,
December, 1990. (Document number PB91-120-006).
“Petitions to Delist Hazardous Wastes -- A Guidance Manual,
Second Edition”, EPA/530-R-93-007, March, 1993. (Document
Number PB 93-169 365).
“Procedures Manual for Ground Water Monitoring at Solid
Waste Disposal Facilities”, EPA-530/SW-611, 1977. (Document
number PB 84-174820).
“Screening Procedures for Estimating the Air Quality Impact of
Stationary Sources”, October, 1992, Publication Number EPA-
450/R-92-019.
“Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, USEPA Publication number SW-846 (Third Edition,
November, 1986), as amended by Updates I (July, 1992), II
(September, 1994), IIA (August, 1993), IIB (January, 1995), and
III (December, 1996) (Document Number 955-001-00000-1).
OECD. Organisation for Economic Co-operation and Development,
Environment Directorate, 2 rue Andre Pascal, 75775 Paris Cedex 16,
France):
OECD Guideline for Testing of Chemicals, Method 301B: “CO
2
Evolution (Modified Sturm Test)”, adopted 17 July 1992.
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) of 27 May 1988.
STI. Available from the Steel Tank Institute, 728 Anthony Trail,
Northbrook, IL 60062, 708-498-1980:
“Standard for Dual Wall Underground Steel Storage Tanks”
(1986).
U.S. DOD. Available from the United States Department of Defense:
“DOD Ammunition and Explosive Safety Standards” (DOD
6055.9-STD), as in effect on November 8, 1995.
47
The Motor Vehicle Inspection Report (DD Form 626), as in
effect on November 8, 1995.
Requisition Tracking Form (DD Form 1348), as in effect on
November 8, 1995.
The Signature and Talley Record (DD Form 1907), as in effect
on November 8, 1995.
Special Instructions for Motor Vehicle Drivers (DD Form 836),
as in effect on November 8, 1995.
USEPA. Available from United States Environmental Protection
Agency, Office of Drinking Water, State Programs Division, WH 550
E, Washington, D.C. 20460:
“Technical Assistance Document: Corrosion, Its Detection and
Control in Injection Wells”, EPA 570/9-87-002, August, 1987.
USEPA. Available from Receptor Analysis Branch, USEPA (MD-14),
Research Triangle Park, NC 27711:
“Screening Procedures for Estimating the Air Quality Impact of
Stationary Sources, Revised”, October, 1992, Publication
Number EPA-450/R-92-019.
USEPA. Available from RCRA Information Center (RIC), 1235
Jefferson-Davis Highway, first floor, Arlington, VA 22203 (Docket # F-
94-IEHF-FFFFF):
OECD Amber List of Wastes, Appendix 4 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1993).
OECD Green List of Wastes, Appendix 3 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1994).
OECD Red List of Wastes, Appendix 5 to the OECD Council
Decision C(92)39/FINAL (Concerning the Control of
Transfrontier Movements of Wastes Destined for Recovery
Operations) (May 1993).
48
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) (May 27, 1988).
U.S. GSA. Available from the United States Government Services
Administration:
Government Bill of Lading (GBL) (GSA Standard Form 1109),
as in effect on November 8, 1995.
b)
Code of Federal Regulations. Available from the Superintendent of Documents,
U.S. Government Printing Office, Washington, D.C. 20401, 202-783-3238:
10 CFR 20, Appendix B (1997)
40 CFR 51.100(ii) (1997)
40 CFR 51, Subpart Appendix W (1997)
40 CFR 52.741, Appendix B (1997)
40 CFR 60 (1997)
40 CFR 61, Subpart V (1997)
40 CFR 136 (1997)
40 CFR 142 (1997)
40 CFR 220 (1997)
40 CFR 260.20 (1997)
40 CFR 264 (1997)
40 CFR 268.Appendix IX (1997)
40 CFR 302.4, 302.5 and 302.6 (1997)
40 CFR 761 (1997)
49 CFR 171 (1997)
49 CFR 173 (1997)
49 CFR 178 (1997)
49
c)
Federal Statutes
Section 3004 of the Resource Conservation and Recovery Act (42
U.S.C. 6901 et seq.), as amended through December 31, 1987.
Sections 201(v), 201(w), and 360b(j) of the Federal Food, Drug, and
Cosmetic Act (FFDCA; 21 U.S.C. §§ 321(v), 321(w) & 512(j)), as
amended through October 25, 1994.
Section 1412 of the Department of Defense Authorization Act of 1986,
Pub. L. 99-145, 50 U.S.C. 1521(j)(1) (1997).
d)
This Section incorporates no later editions or amendments.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 721
IDENTIFICATION AND LISTING OF HAZARDOUS WASTE
SUBPART A: GENERAL PROVISIONS
Section
721.101
Purpose and Scope
721.102
Definition of Solid Waste
721.103
Definition of Hazardous Waste
721.104
Exclusions
721.105
Special Requirements for Hazardous Waste Generated by Small Quantity
Generators
721.106
Requirements for Recyclable Materials
721.107
Residues of Hazardous Waste in Empty Containers
721.108
PCB Wastes Regulated under TSCA
721.109
Requirements for Universal Waste
SUBPART B: CRITERIA FOR IDENTIFYING THE CHARACTERISTICS
OF HAZARDOUS WASTE AND FOR LISTING HAZARDOUS WASTES
Section
721.110
Criteria for Identifying the Characteristics of Hazardous Waste
721.111
Criteria for Listing Hazardous Waste
50
SUBPART C: CHARACTERISTICS OF HAZARDOUS WASTE
Section
721.120
General
721.121
Characteristic of Ignitability
721.122
Characteristic of Corrosivity
721.123
Characteristic of Reactivity
721.124
Toxicity Characteristic
SUBPART D: LISTS OF HAZARDOUS WASTE
Section
721.130
General
721.131
Hazardous Wastes From Nonspecific Sources
721.132
Hazardous Waste from Specific Sources
721.133
Discarded Commercial Chemical Products, Off-Specification Species, Container
Residues, and Spill Residues Thereof
721.135
Wood Preserving Wastes
721.Appendix A
Representative Sampling Methods
721.Appendix B
Method 1311 Toxicity Characteristic Leaching Procedure (TCLP)
721.Appendix C
Chemical Analysis Test Methods
Table A
Analytical Characteristics of Organic Chemicals (Repealed)
Table B
Analytical Characteristics of Inorganic Species (Repealed)
Table C
Sample Preparation/Sample Introduction Techniques (Repealed)
721.Appendix G
Basis for Listing Hazardous Wastes
721.Appendix H
Hazardous Constituents
721.Appendix I
Wastes Excluded by Administrative Action
Table A
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22 from
Non-Specific Sources
Table B
Wastes Excluded by USEPA under 40 CFR 260.20 and 260.22 from
Specific Sources
Table C
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22 from
Commercial Chemical Products, Off-Specification Species, Container
Residues, and Soil Residues Thereof
Table D
Wastes Excluded by the Board by Adjusted Standard
721.Appendix J
Method of Analysis for Chlorinated Dibenzo-p-Dioxins and
Dibenzofurans (Repealed)
721.Appendix Z
Table to Section 721.102
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982;
amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982;
amended in R82-18, 51 PCB 31, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in
R82-19, 53 PCB 131, at 7 Ill. Reg. 13999, effective October 12, 1983; amended in R84-34,
51
61 PCB 247, at 8 Ill. Reg. 24562, effective December 11, 1984; amended in R84-9, at 9 Ill.
Reg. 11834, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 998, effective January
2, 1986; amended in R85-2 at 10 Ill. Reg. 8112, effective May 2, 1986; amended in R86-1 at
10 Ill. Reg. 14002, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20647,
effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6035, effective March 24,
1987; amended in R86-46 at 11 Ill. Reg. 13466, effective August 4, 1987; amended in R87-32
at 11 Ill. Reg. 16698, effective September 30, 1987; amended in R87-5 at 11 Ill. Reg. 19303,
effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2456, effective January 15,
1988; amended in R87-30 at 12 Ill. Reg. 12070, effective July 12, 1988; amended in R87-39
at 12 Ill. Reg. 13006, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 382,
effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18300, effective November
13, 1989; amended in R90-2 at 14 Ill. Reg. 14401, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16472, effective September 25, 1990; amended in R90-17 at 15 Ill.
Reg. 7950, effective May 9, 1991; amended in R90-11 at 15 Ill. Reg. 9332, effective June 17,
1991; amended in R91-1 at 15 Ill. Reg. 14473, effective September 30, 1991; amended in
R91-12 at 16 Ill. Reg. 2155, effective January 27, 1992; amended in R91-26 at 16 Ill. Reg.
2600, effective February 3, 1992; amended in R91-13 at 16 Ill. Reg. 9519, effective June 9,
1992; amended in R92-1 at 16 Ill. Reg. 17666, effective November 6, 1992; amended in R92-
10 at 17 Ill. Reg. 5650, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20568,
effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6741, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12175, effective July 29, 1994; amended in R94-17 at
18 Ill. Reg. 17490, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9522,
effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10963, effective August 1, 1996;
amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 275, effective December 16, 1997; amended
in R98-12 at 22 Ill. Reg. 7615, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at
22 Ill. Reg. ________, effective ______________________.
SUBPART A: GENERAL PROVISIONS
Section 721.101
Purpose and Scope
a)
This Part identifies those solid wastes which are subject to regulation as
hazardous wastes under 35 Ill. Adm. Code 702, 703, 705 and 722 through 725
and 728, and which are subject to the notification requirements of Section 3010
of the Resource Conservation and Recovery Act (RCRA) (42 U.S.C. 6901 et
seq.). In this Part:
1)
Subpart A defines the terms “solid waste” and “hazardous waste,”
identifies those wastes which are excluded from regulation under 35 Ill.
Adm. Code 702, 703, 705 and 722 through 726 and 728, and establishes
special management requirements for hazardous waste produced by
conditionally exempt small quantity generators and hazardous waste
which is recycled.
52
2)
Subpart B sets forth the criteria used to identify characteristics of
hazardous waste and to list particular hazardous wastes.
3)
Subpart C identifies characteristics of hazardous wastes.
4)
Subpart D lists particular hazardous wastes.
b)
Limitations on definition of solid waste:
1)
The definition of solid waste contained in this Part applies only to wastes
that also are hazardous for purposes of the regulations implementing
Subtitle C of the Resource Conservation and Recovery Act RCRA. For
example, it does not apply to materials (such as non-hazardous scrap,
paper, textiles or rubber) that are not otherwise hazardous wastes and
that are recycled.
2)
This Part identifies only some of the materials which are solid wastes
and hazardous wastes under Sections 1004(5), 1004(27) and 7003 of
RCRA. A material which is not defined as a solid waste in this Part, or
is not a hazardous waste identified or listed in this Part, is still a
hazardous waste for purposes of those Sections if, in the case of Section
7003 of RCRA, the statutory elements are established.
c)
For the purposes of Sections 721.102 and 721.106:
1)
A “spent material” is any material that has been used and as a result of
contamination can no longer serve the purpose for which it was produced
without processing.
2)
“Sludge” has the same meaning used in 35 Ill. Adm. Code 720.110.
3)
A “by-product” is a material that is not one of the primary products of a
production process and is not solely or separately produced by the
production process. Examples are process residues such as slags or
distillation column bottoms. The term does not include a co-product that
is produced for the general public’s use and is ordinarily used in the
form it is produced by the process.
4)
A material is “reclaimed” if it is processed to recover a usable product,
or if it is regenerated. Examples are recovery of lead values from spent
batteries and regeneration of spent solvents.
5)
A material is “used or reused” if it is either:
53
A)
Employed as an ingredient (including use as an intermediate) in
an industrial process to make a product (for example, distillation
bottoms from one process used as feedstock in another process).
However, a material will not satisfy this condition if distinct
components of the material are recovered as separate end
products (as when metals are recovered from metal-containing
secondary materials); or
B)
Employed in a particular function or application as an effective
substitute for a commercial product (for example, spent pickle
liquor used as phosphorus precipitant and sludge conditioner in
wastewater treatment).
6)
“Scrap metal” is bits and pieces of metal parts (e.g., bars, turnings,
rods, sheets, wire) or metal pieces that may be combined together with
bolts or soldering (e.g., radiators, scrap automobiles, railroad box cars)
which when worn or superfluous can be recycled.
7)
A material is “recycled” if it is used, reused or reclaimed.
8)
A material is “accumulated speculatively” if it is accumulated before
being recycled. A material is not accumulated speculatively, however, if
the person accumulating it can show that the material is potentially
recyclable and has a feasible means of being recycled; and that -- —
during the calendar year (commencing on January 1) -- —the amount of
material that is recycled, or transferred to a different site for recycling,
equals at least 75 percent by weight or volume of the amount of that
material accumulated at the beginning of the period. In calculating the
percentage of turnover, the 75 percent requirement is to be applied to
each material of the same type (e.g., slags from a single smelting
process) that is recycled in the same way (i.e., from which the same
material is recovered or that is used in the same way). Materials
accumulating in units that would be exempt from regulation under
Section 721.104(c) are not to be included in making the calculation.
(Materials that are already defined as solid wastes also are not to be
included in making the calculation.). Materials are no longer in this
category once they are removed from accumulation for recycling,
however.
9) “Excluded scrap metal” is processed scrap metal, unprocessed home
scrap metal, and unprocessed prompt scrap metal.
10) “Processed scrap metal” is scrap metal that has been manually or
physically altered to either separate it into distinct materials to enhance
economic value or to improve the handling of materials. Processed
54
scrap metal includes, but is not limited to, scrap metal that has been
baled, shredded, sheared, chopped, crushed, flattened, cut, melted, or
separated by metal type (i.e., sorted), and fines, drosses and related
materials that have been agglomerated. (Note: shredded circuit boards
being sent for recycling are not considered processed scrap metal. They
are covered under the exclusion from the definition of solid waste for
shredded circuit boards being recycled (Section 721.104(a)(13))).
11) “Home scrap metal” is scrap metal as generated by steel mills,
foundries, and refineries, such as turnings, cuttings, punchings, and
borings.
12) “Prompt scrap metal” is scrap metal as generated by the metal
working/fabrication industries, and it includes such scrap metal as
turnings, cuttings, punchings, and borings. Prompt scrap metal is also
known as industrial or new scrap metal.
d)
The Agency has inspection authority pursuant to Section 3007 of Resource
Conservation and Recovery Act RCRA and Section 4 of the Environmental
Protection Act.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.102
Definition of Solid Waste
a)
Solid waste.
1)
A solid waste is any discarded material that is not excluded by Section
721.104(a) or that is not excluded pursuant to 35 Ill. Adm. Code
720.130 and 720.131.
2)
A discarded material is any material that is:
A)
Abandoned, as explained in subsection (b) below of this Section;
or
B)
Recycled, as explained in subsection (c) below of this Section; or
C)
Considered inherently waste-like, as explained in subsection (d)
below. of this Section; or
D) A military munition identified as a solid waste in 35 Ill. Adm.
Code 726.302.
b)
Materials are solid waste if they are abandoned by being:
55
1)
Disposed of; or
2)
Burned or incinerated; or
3)
Accumulated, stored or treated (but not recycled) before or in lieu of
being abandoned by being disposed of, burned or incinerated.
c)
Materials are solid wastes if they are recycled--or accumulated, stored or treated
before recycling--as specified in subsections (c)(1) through (c)(4) below of this
Section if they are:
1)
Used in a manner constituting disposal.
A)
Materials noted with a “yes” in column 1 of the table in Section
721.Appendix Z are solid wastes when they are:
i)
Applied to or placed on the land in a manner that
constitutes disposal; or
ii)
Used to produce products that are applied to or placed on
the land or are otherwise contained in products that are
applied to or placed on the land (in which cases the
product itself remains a solid waste).
B)
However, commercial chemical products listed in Section
721.133 are not solid wastes if they are applied to the land and
that is their ordinary manner of use.
2)
Burned for energy recovery.
A)
Materials noted with a “yes” in column 2 of the table in Section
721.Appendix Z are solid wastes when they are:
i)
bBurned to recover energy;
ii)
Used to produce a fuel or are otherwise contained in fuels
(in which case the fuel itself remains a solid waste);
iii)
Contained in fuels (in which case the fuel itself remains a
solid waste).
B)
However, commercial chemical products listed in Section
721.133 are not solid wastes if they are themselves fuels.
56
3)
Reclaimed. Materials noted with a “yes” in column 3 of the table in
Section 721.Appendix Z are solid wastes when reclaimed.
4)
Accumulated speculatively. Materials noted with “yes” in column 4 of
the table in Section 721.Appendix Z are solid wastes when accumulated
speculatively.
d)
Inherently waste-like materials. The following materials are solid wastes when
they are recycled in any manner:
1)
Hazardous waste numbers F020, F021 (unless used as an ingredient to
make a product at the site of generation), F022, F023, F026, and F028.
2)
Secondary materials fed to a halogen acid furnace that exhibit a
characteristic of a hazardous waste or are listed as a hazardous waste as
defined in 721.Subparts C or D of this Part, except for brominated
material that meets the following criteria:
A)
The material must contain a bromine concentration of at least
45% percent;
B)
The material must contain less than a total of 1% one percent of
toxic organic compounds listed in Section 721.Appendix H; and
C)
The material is processed continually on-site in the halogen acid
furnace via direct conveyance (hard piping).
3)
The following criteria are used to add wastes to the list:
A)
Disposal method or toxicity.
i)
The materials are ordinarily disposed of, burned, or
incinerated; or
ii)
The materials contain toxic constituents listed in Section
721.Appendix H and these constituents are not ordinarily
found in raw materials or products for which the materials
substitute (or are found in raw materials or products in
smaller concentrations) and are not used or reused during
the recycling process; and
B)
The material may pose a substantial hazard to human health and
the environment when recycled.
e)
Materials that are not solid waste when recycled.
57
1)
Materials are not solid wastes when they can be shown to be recycled by
being:
A)
Used or reused as ingredients in an industrial process to make a
product, provided the materials are not being reclaimed; or
B)
Used or reused as effective substitutes for commercial products;
or
C)
Returned to the original process from which they are generated
without first being reclaimed. The materials must be returned as
a substitute for feedstock materials. In cases where the original
process to which the material is returned is a secondary process,
the materials must be managed so there is no placement on the
land.
2)
The following materials are solid wastes, even if the recycling involves
use, reuse, or return to the original process (described in subsections
(e)(1)(A) through (e)(1)(C) above of this Section):
A)
Materials used in a manner constituting disposal or used to
produce products that are applied to the land; or
B)
Materials burned for energy recovery, used to produce a fuel, or
contained in fuels; or
C)
Materials accumulated speculatively; or
D)
Materials listed in subsections (d)(1) and (d)(2) above of this
Section.
f)
Documentation of claims that materials are not solid wastes or are conditionally
exempt from regulation. Respondents in actions to enforce regulations
implementing Subtitle C of the Resource Conservation Recovery Act RCRA or
Section 21 of the Environmental Protection Act that raise a claim that a certain
material is not a solid waste or that the material is conditionally exempt from
regulation must demonstrate that there is a known market or disposition for the
material and that they meet the terms of the exclusion or exemption. In doing
so, the person must provide appropriate documentation (such as contracts
showing that a second person uses the material as an ingredient in a production
process) to demonstrate that the material is not a waste or that the material is
exempt from regulation. In addition, owners or operators of facilities claiming
that they actually are recycling materials must show that they have the necessary
equipment to do so.
58
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.104
Exclusions
a)
Materials that are not solid wastes. The following materials are not solid wastes
for the purpose of this Part:
1)
Sewage:
A)
Domestic sewage (untreated sanitary wastes that pass through a
sewer system); and
B)
Any mixture of domestic sewage and other waste that passes
through a sewer system to publicly-owned treatment works for
treatment.
C) “Domestic sewage” means untreated sanitary wastes that pass
through a sewer system.
2)
Industrial wastewater discharges that are point source discharges with
National Pollutant Discharge Elimination System (NPDES) permits
issued by the Agency pursuant to Section 12(f) of the Environmental
Protection Act and 35 Ill. Adm. Code 309.
BOARD NOTE: This exclusion applies only to the actual point source
discharge. It does not exclude industrial wastewaters while they are
being collected, stored, or treated before discharge, nor does it exclude
sludges that are generated by industrial wastewater treatment.
3)
Irrigation return flows.
4)
Source, special nuclear, or by-product material as defined by the Atomic
Energy Act of 1954, as amended (42 U.S.C. 2011 et seq.).
5)
Materials subjected to in-situ mining techniques that are not removed
from the ground as part of the extraction process.
6)
Pulping liquors (i.e., black liquor liquors) that are reclaimed in a
pulping liquor recovery furnace and then reused in the pulping process,
unless accumulated speculatively, as defined in Section 721.101(c).
7)
Spent sulfuric acid used to produce virgin sulfuric acid unless it is
accumulated speculatively, as defined in Section 721.101(c).
59
8)
Secondary materials that are reclaimed and returned to the original
process or processes in which they were generated where they are reused
in the production process, provided:
A)
Only tank storage is involved, and the entire process through
completion of reclamation is closed by being entirely connected
with pipes or other comparable enclosed means of conveyance;
B)
Reclamation does not involve controlled flame combustion (such
as occurs in boilers, industrial furnaces or incinerators);
C)
The secondary materials are never accumulated in such tanks for
over twelve months without being reclaimed; and
D)
The reclaimed material is not used to produce a fuel or used to
produce products that are used in a manner constituting disposal.
9)
Wood preserving wastes.
A)
Spent wood preserving solutions that have been used and which
are reclaimed and reused for their original intended purpose; and
B)
Wastewaters from the wood preserving process that have been
reclaimed and which are reused to treat wood.
10)
Hazardous waste numbers K060, K087, K141, K142, K143, K144,
K145, K147, and K148, and any wastes from the coke by-products
processes that are hazardous only because they exhibit the toxicity
characteristic specified in Section 721.124, when subsequent to
generation these materials are recycled to coke ovens, to the tar recovery
process as a feedstock to produce coal tar, or are mixed with coal tar
prior to the tar’s sale or refining. This exclusion is conditioned on there
being no land disposal of the waste from the point it is generated to the
point it is recycled to coke ovens, to tar recovery, to the tar refining
processes, or prior to when it is mixed with coal.
11)
Nonwastewater splash condenser dross residue from the treatment of
hazardous waste number K061 in high temperature metals recovery
units, provided it is shipped in drums (if shipped) and not land disposed
before recovery.
12)
Recovered oil from petroleum refining, exploration, and production and
from transportation incident thereto that is to be inserted into the
petroleum refining process (SIC Code 2911) at or before a point (other
than direct insertion into a coker) where contaminants are removed.
60
This exclusion applies to recovered oil stored or transported prior to
insertion, except that the oil must not be stored in a manner involving
placement on the land and the oil must not be accumulated speculatively
before being recycled. Recovered oil is oil that has been reclaimed from
secondary materials (such as wastewater) generated from normal
petroleum refining, exploration, and production, and from transportation
practices. Recovered oil includes oil that is recovered from refinery
wastewater collection and treatment systems, oil recovered from oil and
gas drilling operations, and oil recovered from wastes removed from
crude oil storage tanks. Recovered oil does not include (among other
things) oil-bearing hazardous wastes listed in Subpart D of this Part
(e.g., K048 through K052, F037, and F038). However, oil recovered
from such wastes may be considered recovered oil. Recovered oil also
does not include used oil as defined in 35 Ill. Adm. Code 739.100.
13) Excluded scrap metal (processed scrap metal, unprocessed home scrap
metal, and unprocessed prompt scrap metal) being recycled.
14) Shredded circuit boards being recycled, provided that they meet the
following conditions:
A) The circuit boards are stored in containers sufficient to prevent a
release to the environment prior to recovery; and
B) The circuit boards are free of mercury switches, mercury relays
and nickel-cadmium batteries and lithium batteries.
b)
Solid wastes that are not hazardous wastes. The following solid wastes are not
hazardous wastes:
1)
Household waste, including household waste that has been collected,
transported, stored, treated, disposed, recovered (e.g., refuse-derived
fuel), or reused. “Household waste” means any waste material
(including garbage, trash, and sanitary wastes in septic tanks) derived
from households (including single and multiple residences, hotels, and
motels, bunkhouses, ranger stations, crew quarters, campgrounds, picnic
grounds, and day-use recreation areas). A resource recovery facility
managing municipal solid waste shall not be deemed to be treating,
storing, disposing of, or otherwise managing hazardous wastes for the
purposes of regulation under this Part, if such facility:
A)
Receives and burns only:
i)
Household waste (from single and multiple dwellings,
hotels, motels, and other residential sources); and
61
ii)
Solid waste from commercial or industrial sources that
does not contain hazardous waste,; and
B)
Such facility does not accept hazardous waste and the owner or
operator of such facility has established contractual requirements
or other appropriate notification or inspection procedures to
assure that hazardous wastes are not received at or burned in such
facility.
BOARD NOTE: The U.S. Supreme Court determined, in City
of Chicago v. Environmental Defense Fund, Inc., -- 511 U.S. --
328, 114 S. Ct. 1588, 128 L. Ed. 2d 302 (1994), that this
exclusion and RCRA section 3001(i) (42 U.S.C. § 6921(i)) do
not exclude the ash from facilities covered by this subsection
from regulation as a hazardous waste. At 59 Fed. Reg. 29372
(June 7, 1994), USEPA granted facilities managing ash from
such facilities that is determined a hazardous waste under Subpart
C of this Part until December 7, 1994 to file a Part A permit
application pursuant to 35 Ill. Adm. Code 703.181. At 60 Fed.
Reg. 6666 (Feb. 3, 1995), USEPA stated that it interpreted that
the point at which ash becomes subject to RCRA Subtitle C
regulation is when that material leaves the combustion building
(including connected air pollution control equipment).
2)
Solid wastes generated by any of the following that are returned to the
soil as fertilizers:
A)
The growing and harvesting of agricultural crops, or
B)
The raising of animals, including animal manures.
3)
Mining overburden returned to the mine site.
4)
Fly ash waste, bottom ash waste, slag waste, and flue gas emission
control waste generated primarily from the combustion of coal or other
fossil fuels, except as provided in 35 Ill. Adm. Code 726.212 for
facilities that burn or process hazardous waste.
5)
Drilling fluids, produced waters, and other wastes associated with the
exploration, development, or production of crude oil, natural gas, or
geothermal energy.
6)
Chromium wastes:
62
A)
Wastes that fail the test for the toxicity characteristic (Sections
721.124 and 721.Appendix B) because chromium is present or
which are listed in Subpart D of this Part due to the presence of
chromium, that do not fail the test for the toxicity characteristic
for any other constituent or which are not listed due to the
presence of any other constituent, and that do not fail the test for
any other characteristic, if it is shown by a waste generator or by
waste generators that:
i)
The chromium in the waste is exclusively (or nearly
exclusively) trivalent chromium;
ii)
The waste is generated from an industrial process that uses
trivalent chromium exclusively (or nearly exclusively) and
the process does not generate hexavalent chromium; and
iii)
The waste is typically and frequently managed in non-
oxidizing environments.
B)
Specific wastes that meet the standard in subsection (b)(6)(A) of
this Section (so long as they do not fail the test for the toxicity
characteristic for any other constituent and do not exhibit any
other characteristic) are:
i)
Chrome (blue) trimmings generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
ii)
Chrome (blue) shavings generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
iii)
Buffing dust generated by the following subcategories of
the leather tanning and finishing industry: hair
pulp/chrome tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no beamhouse,
through-the-blue;
iv)
Sewer screenings generated by the following subcategories
of the leather tanning and finishing industry: hair
pulp/chrome tan/retan/wet finish, hair save/chrome
63
tan/retan/wet finish, retan/wet finish, no beamhouse,
through-the-blue, and shearling;
v)
Wastewater treatment sludges generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
vi)
Wastewater treatment sludges generated by the following
subcategories of the leather tanning and finishing
industry: hair pulp/chrome tan/retan/wet finish, hair
save/chrome tan/retan/wet finish, and through-the-blue;
vii)
Waste scrap leather from the leather tanning industry, the
shoe manufacturing industry, and other leather product
manufacturing industries; and
viii)
Wastewater treatment sludges from the production of
titanium dioxide pigment using chromium-bearing ores by
the chloride process.
7)
Solid waste from the extraction, beneficiation, and processing of ores
and minerals (including coal, phosphate rock, and overburden from the
mining of uranium ore), except as provided by 35 Ill. Adm. Code
726.212 for facilities that burn or process hazardous waste. For
purposes of this subsection (b)(7), beneficiation of ores and minerals is
restricted to the following activities: crushing, grinding, washing,
dissolution, crystallization, filtration, sorting, sizing, drying, sintering,
pelletizing, briquetting, calcining to remove water or carbon dioxide,
roasting, autoclaving or chlorination in preparation for leaching (except
where the roasting or autoclaving or chlorination and leaching sequence
produces a final or intermediate product that does not undergo further
beneficiation or processing), gravity concentration, magnetic separation,
electrostatic separation, floatation, ion exchange, solvent extraction,
electrowinning, precipitation, amalgamation, and heap, dump, vat tank,
and in situ leaching. For the purposes of this subsection (b)(7), solid
waste from the processing of ores and minerals includes only the
following wastes:
A)
Slag from primary copper processing,
B)
Slag from primary lead processing,
C)
Red and brown muds from bauxite refining,
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D)
Phosphogypsum from phosphoric acid production,
E)
Slag from elemental phosphorus production,
F)
Gasifier ash from coal gasification,
G)
Process wastewater from coal gasification,
H)
Calcium sulfate wastewater treatment plant sludge from primary
copper processing,
I)
Slag tailings from primary copper processing,
J)
Fluorogypsum from hydrofluoric acid production,
K)
Process wastewater from hydrofluoric acid production,
L)
Air pollution control dust or sludge from iron blast furnaces,
M)
Iron blast furnace slag,
N)
Treated residue from roasting and leaching of chrome ore,
O)
Process wastewater from primary magnesium processing by the
anhydrous process,
P)
Process wastewater from phosphoric acid production,
Q)
Basic oxygen furnace and open hearth furnace air pollution
control dust or sludge from carbon steel production,
R)
Basic oxygen furnace and open hearth furnace slag from carbon
steel production,
S)
Chloride processing waste solids from titanium tetrachloride
production, and
T)
Slag from primary zinc smelting.
8)
Cement kiln dust waste, except as provided by 35 Ill. Adm. Code
726.212 for facilities that burn or process hazardous waste.
9)
Solid waste that consists of discarded arsenical-treated wood or wood
products that fails the test for the toxicity characteristic for hazardous
65
waste codes D004 through D017 and which is not a hazardous waste for
any other reason if the waste is generated by persons that utilize the
arsenical-treated wood and wood products for these materials’ intended
end use.
10)
Petroleum-contaminated media and debris that fail the test for the
toxicity characteristic of Section 721.124 (hazardous waste codes D018
through D043 only) and which are subject to corrective action
regulations under 35 Ill. Adm. Code 731.
11)
This subsection corresponds with 40 CFR 261.4(b)(11), which expired
by its own terms on January 25, 1993. This statement maintains
structural parity with USEPA regulations.
12)
Used chlorofluorocarbon refrigerants from totally enclosed heat transfer
equipment, including mobile air conditioning systems, mobile
refrigeration, and commercial and industrial air conditioning and
refrigeration systems, that uses chlorofluorocarbons as the heat transfer
fluid in a refrigeration cycle, provided the refrigerant is reclaimed for
further use.
13)
Non-terne plated used oil filters that are not mixed with wastes listed in
Subpart D of this Part, if these oil filters have been gravity hot-drained
using one of the following methods:
A)
Puncturing the filter anti-drain back valve or the filter dome end
and hot-draining;
B)
Hot-draining and crushing;
C)
Dismantling and hot-draining; or
D)
Any other equivalent hot-draining method that will remove used
oil.
14)
Used oil re-refining distillation bottoms that are used as feedstock to
manufacture asphalt products.
c)
Hazardous wastes that are exempted from certain regulations. A hazardous
waste that is generated in a product or raw material storage tank, a product or
raw material transport vehicle or vessel, a product or raw material pipeline, or
in a manufacturing process unit, or an associated non-waste-treatment
manufacturing unit, is not subject to regulation under 35 Ill. Adm. Code 702,
703, 705, and 722 through 725, and 728 or to the notification requirements of
Section section 3010 of RCRA until it exits the unit in which it was generated,
66
unless the unit is a surface impoundment, or unless the hazardous waste remains
in the unit more than 90 days after the unit ceases to be operated for
manufacturing or for storage or transportation of product or raw materials.
d)
Samples
1)
Except as provided in subsection (d)(2) of this Section, a sample of solid
waste or a sample of water, soil, or air that is collected for the sole
purpose of testing to determine its characteristics or composition is not
subject to any requirements of this Part or 35 Ill. Adm. Code 702, 703,
705, and 722 through 728. The sample qualifies when:
A)
The sample is being transported to a laboratory for the purpose of
testing;
B)
The sample is being transported back to the sample collector after
testing;
C)
The sample is being stored by the sample collector before
transport to a laboratory for testing;
D)
The sample is being stored in a laboratory before testing;
E)
The sample is being stored in a laboratory for testing but before it
is returned to the sample collector; or
F)
The sample is being stored temporarily in the laboratory after
testing for a specific purpose (for example, until conclusion of a
court case or enforcement action where further testing of the
sample may be necessary).
2)
In order to qualify for the exemption in subsection (d)(1)(A) or (d)(1)(B)
of this Section, a sample collector shipping samples to a laboratory and a
laboratory returning samples to a sample collector shall:
A)
Comply with U.S. Department of Transportation (USDOT), U.S.
Postal Service (USPS), or any other applicable shipping
requirements; or
B)
Comply with the following requirements if the sample collector
determines that USDOT, USPS, or other shipping requirements
do not apply to the shipment of the sample:
i)
Assure that the following information accompanies the
sample: The sample collector’s name, mailing address,
67
and telephone number; the laboratory’s name, mailing
address, and telephone number; the quantity of the
sample; the date of the shipment; and a description of the
sample.
ii)
Package the sample so that it does not leak, spill, or
vaporize from its packaging.
3)
This exemption does not apply if the laboratory determines that the waste
is hazardous but the laboratory is no longer meeting any of the
conditions stated in subsection (d)(1) of this Section.
e)
Treatability study samples.
1)
Except as is provided in subsection (e)(2) of this Section, a person that
generates or collects samples for the purpose of conducting treatability
studies, as defined in 35 Ill. Adm. Code 720.110, are not subject to any
requirement of 35 Ill. Adm. Code 721 through 723 or to the notification
requirements of Section section 3010 of the Resource Conservation and
Recovery Act. Nor are such samples included in the quantity
determinations of Section 721.105 and 35 Ill. Adm. Code 722.134(d)
when:
A)
The sample is being collected and prepared for transportation by
the generator or sample collector;
B)
The sample is being accumulated or stored by the generator or
sample collector prior to transportation to a laboratory or testing
facility; or
C)
The sample is being transported to the laboratory or testing
facility for the purpose of conducting a treatability study.
2)
The exemption in subsection (e)(1) of this Section is applicable to
samples of hazardous waste being collected and shipped for the purpose
of conducting treatability studies provided that:
A)
The generator or sample collector uses (in “treatability studies”)
no more than 10,000 kg of media contaminated with non-acute
hazardous waste, 1000 kg of non-acute hazardous waste other
than contaminated media, 1 kg of acute hazardous waste, or 2500
kg of media contaminated with acute hazardous waste for each
process being evaluated for each generated wastestream;
68
B)
The mass of each shipment does not exceed 10,000 kg; the
10,000 kg quantity may be all media contaminated with non-
acute hazardous waste, or may include 2500 kg of media
contaminated with acute hazardous waste, 1000 kg of hazardous
waste, and 1 kg of acute hazardous waste;
C)
The sample must be packaged so that it does not leak, spill, or
vaporize from its packaging during shipment and the
requirements of subsections (e)(2)(C)(i) or (e)(2)(C)(ii) of this
Section are met.
i)
The transportation of each sample shipment complies with
U.S. Department of Transportation (USDOT), U.S.
Postal Service (USPS), or any other applicable shipping
requirements; or
ii)
If the USDOT, USPS, or other shipping requirements do
not apply to the shipment of the sample, the following
information must accompany the sample: The name,
mailing address, and telephone number of the originator
of the sample; the name, address, and telephone number
of the facility that will perform the treatability study; the
quantity of the sample; the date of the shipment; and, a
description of the sample, including its USEPA hazardous
waste number;
D)
The sample is shipped to a laboratory or testing facility that is
exempt under subsection (f) of this Section, or has an appropriate
RCRA permit or interim status;
E)
The generator or sample collector maintains the following records
for a period ending three years after completion of the treatability
study:
i)
Copies of the shipping documents;
ii)
A copy of the contract with the facility conducting the
treatability study;
iii)
Documentation showing: The amount of waste shipped
under this exemption; the name, address, and USEPA
identification number of the laboratory or testing facility
that received the waste; the date the shipment was made;
and whether or not unused samples and residues were
returned to the generator; and
69
F)
The generator reports the information required in subsection
(e)(2)(E)(iii) of this Section in its report under 35 Ill. Adm. Code
722.141.
3)
The Agency may grant requests on a case-by-case basis for up to an
additional two years for treatability studies involving bioremediation.
The Agency may grant requests, on a case-by-case basis, for quantity
limits in excess of those specified in subsections (e)(2)(A), (e)(2)(B), and
(f)(4) of this Section, for up to an additional 5000 kg of media
contaminated with non-acute hazardous waste, 500 kg of non-acute
hazardous waste, 2500 kg of media contaminated with acute hazardous
waste, and 1 kg of acute hazardous waste:
A)
In response to requests for authorization to ship, store, and
conduct further treatability studies on additional quantities in
advance of commencing treatability studies. Factors to be
considered in reviewing such requests include the nature of the
technology, the type of process (e.g., batch versus continuous),
the size of the unit undergoing testing (particularly in relation to
scale-up considerations), the time or quantity of material required
to reach steady-state operating conditions, or test design
considerations, such as mass balance calculations.
B)
In response to requests for authorization to ship, store, and
conduct treatability studies on additional quantities after initiation
or completion of initial treatability studies when: There has been
an equipment or mechanical failure during the conduct of the
treatability study, there is need to verify the results of a
previously-conducted treatability study, there is a need to study
and analyze alternative techniques within a previously-evaluated
treatment process, or there is a need to do further evaluation of
an ongoing treatability study to determine final specifications for
treatment.
C)
The additional quantities allowed and timeframes allowed in
subsections (e)(3)(A) and (e)(3)(B) of this Section are subject to
all the provisions in subsections (e)(1) and (e)(2)(B) through
(e)(2)(F) of this Section. The generator or sample collector shall
apply to the Agency and provide in writing the following
information:
i)
The reason why the generator or sample collector requires
additional time or quantity of sample for the treatability
70
study evaluation and the additional time or quantity
needed;
ii)
Documentation accounting for all samples of hazardous
waste from the wastestream that have been sent for or
undergone treatability studies, including the date each
previous sample from the waste stream was shipped, the
quantity of each previous shipment, the laboratory or
testing facility to which it was shipped, what treatability
study processes were conducted on each sample shipped,
and the available results of each treatability study;
iii)
A description of the technical modifications or change in
specifications that will be evaluated and the expected
results;
iv)
If such further study is being required due to equipment or
mechanical failure, the applicant shall include information
regarding the reason for the failure or breakdown and also
include what procedures or equipment improvements have
been made to protect against further breakdowns; and
v)
Such other information as the Agency determines is
necessary.
4)
Final Agency determinations pursuant to this subsection (e) may be
appealed to the Board.
f)
Samples undergoing treatability studies at laboratories or testing facilities.
Samples undergoing treatability studies and the laboratory or testing facility
conducting such treatability studies (to the extent such facilities are not
otherwise subject to RCRA requirements) are not subject to any requirement of
this Part, or of 35 Ill. Adm. Code 702, 703, 705, 722 through 726, and 728 or
to the notification requirements of Section 3010 of the Resource Conservation
and Recovery Act, provided that the requirements of subsections (f)(1) through
(f)(11) of this Section are met. A mobile treatment unit may qualify as a testing
facility subject to subsections (f)(1) through (f)(11) of this Section. Where a
group of mobile treatment units are located at the same site, the limitations
specified in subsections (f)(1) through (f)(11) of this Section apply to the entire
group of mobile treatment units collectively as if the group were one mobile
treatment unit.
1)
No less than 45 days before conducting treatability studies, the facility
notifies the Agency in writing that it intends to conduct treatability
studies under this subsection (f).
71
2)
The laboratory or testing facility conducting the treatability study has a
USEPA identification number.
3)
No more than a total of 10,000 kg of “as received” media contaminated
with non-acute hazardous waste, 2500 kg of media contaminated with
acute hazardous waste, or 250 kg of other “as received” hazardous waste
is subject to initiation of treatment in all treatability studies in any single
day. “As received” waste refers to the waste as received in the shipment
from the generator or sample collector.
4)
The quantity of “as received” hazardous waste stored at the facility for
the purpose of evaluation in treatability studies does not exceed 10,000
kg, the total of which can include 10,000 kg of media contaminated with
non-acute hazardous waste, 2500 kg of media contaminated with acute
hazardous waste, 1000 kg of non-acute hazardous wastes other than
contaminated media, and 1 kg of acute hazardous waste. This quantity
limitation does not include treatment materials (including nonhazardous
solid waste) added to “as received” hazardous waste.
5)
No more than 90 days have elapsed since the treatability study for the
sample was completed, or no more than one year (two years for
treatability studies involving bioremediation) has elapsed since the
generator or sample collector shipped the sample to the laboratory or
testing facility, whichever date first occurs. Up to 500 kg of treated
material from a particular waste stream from treatability studies may be
archived for future evaluation up to five years from the date of initial
receipt. Quantities of materials archived are counted against the total
storage limit for the facility.
6)
The treatability study does not involve the placement of hazardous waste
on the land or open burning of hazardous waste.
7)
The facility maintains records for three years following completion of
each study that show compliance with the treatment rate limits and the
storage time and quantity limits. The following specific information
must be included for each treatability study conducted:
A)
The name, address, and USEPA identification number of the
generator or sample collector of each waste sample;
B)
The date the shipment was received;
C)
The quantity of waste accepted;
72
D)
The quantity of “as received” waste in storage each day;
E)
The date the treatment study was initiated and the amount of “as
received” waste introduced to treatment each day;
F)
The date the treatability study was concluded;
G)
The date any unused sample or residues generated from the
treatability study were returned to the generator or sample
collector or, if sent to a designated facility, the name of the
facility and the USEPA identification number.
8)
The facility keeps, on-site, a copy of the treatability study contract and
all shipping papers associated with the transport of treatability study
samples to and from the facility for a period ending three years from the
completion date of each treatability study.
9)
The facility prepares and submits a report to the Agency by March 15 of
each year that estimates the number of studies and the amount of waste
expected to be used in treatability studies during the current year, and
includes the following information for the previous calendar year:
A)
The name, address, and USEPA identification number of the
facility conducting the treatability studies;
B)
The types (by process) of treatability studies conducted;
C)
The names and addresses of persons for whom studies have been
conducted (including their USEPA identification numbers);
D)
The total quantity of waste in storage each day;
E)
The quantity and types of waste subjected to treatability studies;
F)
When each treatability study was conducted; and
G)
The final disposition of residues and unused sample from each
treatability study.
10)
The facility determines whether any unused sample or residues generated
by the treatability study are hazardous waste under Section 721.103 and,
if so, are subject to 35 Ill. Adm. Code 702, 703, and 721 through 728,
unless the residues and unused samples are returned to the sample
originator under the exemption of subsection (e) of this Section.
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11)
The facility notifies the Agency by letter when the facility is no longer
planning to conduct any treatability studies at the site.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.105
Special Requirements for Hazardous Waste Generated by Small Quantity
Generators
a)
A generator is a conditionally exempt small quantity generator in a calendar
month if it generates no more than 100 kilograms of hazardous waste in that
month. 35 Ill. Adm. Code 700 explains the relation of this to the 100 kg/mo
exception of 35 Ill. Adm. Code 809.
b)
Except for those wastes identified in subsections (e), (f), (g) and (j) of this
Section, a conditionally exempt small quantity generator’s hazardous wastes are
not subject to regulation under 35 Ill. Adm. Code 702, 703, 705 and 722
through 726 and 728, and the notification requirements of Section section 3010
of Resource Conservation and Recovery Act, provided the generator complies
with the requirements of subsections (f), (g) and (j) of this Section.
c)
When making the quantity determinations of this Part and 35 Ill. Adm. Code
722, the generator must include all hazardous waste that it generates, except the
following hazardous waste:
1)
Hazardous waste that is exempt from regulation under Section
721.104(c) through (f), 721.106(a)(3), 721.107(a)(1), or 721.108;
2)
Hazardous waste that is managed immediately upon generation only in
on-site elementary neutralization units, wastewater treatment units, or
totally enclosed treatment facilities, as defined in 35 Ill. Adm. Code
720.110;
3)
Hazardous waste that is recycled, without prior storage or accumulation,
only in an on-site process subject to regulation under Section
721.106(c)(2);
4)
Hazardous waste that is used oil managed under the requirements of
Section 721.106(a)(4) and 35 Ill. Adm. Code 739;
5)
Hazardous waste that is spent lead-acid batteries managed under the
requirements of 35 Ill. Adm. Code 726.Subpart G; and
6)
Hazardous waste that is universal waste managed under Section 721.109
and 35 Ill. Adm. Code 733.
74
d)
In determining the quantity of hazardous waste it generates, a generator need
not include:
1)
Hazardous waste when it is removed from on-site storage; or
2)
Hazardous waste produced by on-site treatment (including reclamation)
of its hazardous waste so long as the hazardous waste that is treated was
counted once; or
3)
Spent materials that are generated, reclaimed and subsequently reused
on-site, so long as such spent materials have been counted once.
e)
If a generator generates acute hazardous waste in a calendar month in quantities
greater than set forth below, all quantities of that acute hazardous waste are
subject to full regulation under 35 Ill. Adm. Code 702, 703, 705 and 722
through 726 and 728, and the notification requirements of Section section 3010
of the Resource Conservation and Recovery Act:
1)
A total of one kilogram of one or more of the acute hazardous wastes
listed in Section 721.131, 721.132, or 721.133(e); or
2)
A total of 100 kilograms of any residue or contaminated soil, waste or
other debris resulting from the clean-up of a spill, into or on any land or
water, of any one or more of the acute hazardous wastes listed in Section
721.131, 721.132, or 721.133(e).
BOARD NOTE: “Full regulation” means those regulations applicable to
generators of greater than 1000 kg of non-acute hazardous waste in a
calendar month.
f)
In order for acute hazardous wastes generated by a generator of acute hazardous
wastes in quantities equal to or less than those set forth in subsection (e)(1) or
(e)(2) of this Section to be excluded from full regulation under this Section, the
generator must comply with the following requirements:
1)
35 Ill. Adm. Code 722.111.
2)
The generator may accumulate acute hazardous waste on-site. If the
generator accumulates at any time acute hazardous wastes in quantities
greater than set forth in subsection (e)(1) or (e)(2) of this Section, all of
those accumulated wastes are subject to regulation under 35 Ill. Adm.
Code 702, 703, 705 and 722 through 726 and 728, and the applicable
notification requirements of Section section 3010 of the Resource
Conservation and Recovery Act. The time period of 35 Ill. Adm. Code
75
722.134(a), for accumulation of wastes on-site, begins when the
accumulated wastes exceed the applicable exclusion limit.
3)
A conditionally exempt small quantity generator may either treat or
dispose of its acute hazardous waste in an on-site facility or ensure
delivery to an off-site treatment, storage, or disposal facility, , any of
which, if located in the United States, meets any of the following
conditions:
A)
The facility is permitted under 35 Ill. Adm. Code 702 and 703;
B)
The facility has interim status under 35 Ill. Adm. Code 702, 703
and 725;
C)
The facility is authorized to manage hazardous waste by a state
with a hazardous waste management program approved by
USEPA pursuant to 40 CFR 271;
D)
The facility is permitted, licensed, or registered by a state to
manage municipal or industrial solid waste and, if managed in a
municipal solid waste landfill facility, the landfill is subject to 35
Ill. Adm. Code 810 through 814 or 40 CFR 258;
E)
The facility is permitted, licensed, or registered by a state to
manage non-municipal non-hazardous waste and, if managed in a
non-municipal non-hazardous waste disposal unit, the unit is
subject to the requirements of 40 CFR 257.5 through 257.30;
BOARD NOTE: The Illinois non-hazardous waste landfill
regulations, 35 Ill. Adm. Code 810 through 814, do not allow the
disposal of hazardous waste in a landfill regulated under those
rules. The Board intends that subsections (f)(3)(D) and (f)(3)(E)
of this Section impose a federal requirement on the hazardous
waste generator. The Board specifically does not intend that
these subsections authorize any disposal of conditionally-exempt
small quantity generator waste in a landfill not specifically
permitted to accept the particular hazardous waste.
EF)
The facility is a facility one that:
i)
Beneficially uses or reuses or legitimately recycles or
reclaims its waste; or
ii)
Treats its waste prior to beneficial use or reuse, or
legitimate recycling or reclamation; or
76
FG)
For universal waste managed under 35 Ill. Adm. Code 733 or 40
CFR 273, the facility is a universal waste handler or destination
facility subject to the requirements of 35 Ill. Adm. Code 733 or
40 CFR 273.
g)
In order for hazardous waste generated by a conditionally exempt small quantity
generator in quantities of less than 100 kilograms of hazardous waste during a
calendar month to be excluded from full regulation under this Section, the
generator must comply with the following requirements:
1)
35 Ill. Adm. Code 722.111;
2)
The conditionally exempt small quantity generator may accumulate
hazardous waste on-site. If it accumulates at any time more than a total
of 1000 kilograms of the generator’s hazardous waste, all of those
accumulated wastes are subject to regulation under the special provisions
of 35 Ill. Adm. Code 722 applicable to generators of between 100 kg
and 1000 kg of hazardous waste in a calendar month as well as the
requirements of 35 Ill. Adm. Code 702, 703, 705 and 723 through 726
and 728, and the applicable notification requirements of Section 3010 of
the Resource Conservation and Recovery Act. The time period of 35 Ill.
Adm. Code 722.134(d) for accumulation of wastes on-site begins for a
small quantity generator when the accumulated wastes exceed 1000
kilograms;
3)
A conditionally exempt small quantity generator may either treat or
dispose of its hazardous waste in an on-site facility or ensure delivery to
an off-site treatment, storage, or disposal facility, any of which, if
located in the United States, meets any of the following conditions:
A)
The facility is permitted under 35 Ill. Adm. Code 702 and 703;
B)
The facility has interim status under 35 Ill. Adm. Code 702, 703
and 725;
C)
The facility is authorized to manage hazardous waste by a state
with a hazardous waste management program approved by
USEPA under 40 CFR 271 (1986);
D)
The facility is permitted, licensed, or registered by a state to
manage municipal or industrial solid waste and, if managed in a
municipal solid waste landfill facility, the landfill is subject to 35
Ill. Adm. Code 810 through 814 or 40 CFR 258;
77
E)
The facility is permitted, licensed, or registered by a state to
manage non-municipal non-hazardous waste and, if managed in a
non-municipal non-hazardous waste disposal unit, the unit is
subject to the requirements of 40 CFR 257.5 through 257.30;
BOARD NOTE: The Illinois non-hazardous waste landfill
regulations, 35 Ill. Adm. Code 810 through 814, do not allow the
disposal of hazardous waste in a landfill regulated under those
rules. The Board intends that subsections (g)(3)(D) and (g)(3)(E)
of this Section impose a federal requirement on the hazardous
waste generator. The Board specifically does not intend that
these subsections authorize any disposal of conditionally-exempt
small quantity generator waste in a landfill not specifically
permitted to accept the particular hazardous waste.
EF)
The facility is a facility one that:
i)
Beneficially uses or re-uses, or legitimately recycles or
reclaims the small quantity generator’s waste; or
ii)
Treats its waste prior to beneficial use or re-use, or
legitimate recycling or reclamation; or
FG)
For universal waste managed under 35 Ill. Adm. Code 733 or 40
CFR 273, the facility is a universal waste handler or destination
facility subject to the requirements of 35 Ill. Adm. Code 733 or
40 CFR 273.
h)
Hazardous waste subject to the reduced requirements of this Section may be
mixed with non-hazardous waste and remain subject to these reduced
requirements even though the resultant mixture exceeds the quantity limitations
identified in this Section, unless the mixture meets any of the characteristics of
hazardous wastes identified in Subpart C.
i)
If a small quantity generator mixes a solid waste with a hazardous waste that
exceeds a quantity exclusion level of this Section, the mixture is subject to full
regulation.
j)
If a conditionally exempt small quantity generator’s hazardous wastes are mixed
with used oil, the mixture is subject to 35 Ill. Adm. Code 739, if it is destined
to be burned for energy recovery. Any material produced from such a mixture
by processing, blending, or other treatment is also so regulated if it is destined
to be burned for energy recovery.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
78
Section 721.106
Requirements for Recyclable Materials
a)
Recyclable materials:
1)
Hazardous wastes that are recycled are subject to the requirements for
generators, transporters, and storage facilities of subsections (b) and (c)
of this Section, except for the materials listed in subsections (a)(2) and
(a)(3) of this Section. Hazardous wastes that are recycled will be known
as “recyclable materials”.
2)
The following recyclable materials are not subject to the requirements of
this Section but are regulated under 35 Ill. Adm. Code 726.Subparts C
through H and all applicable provisions in 35 Ill. Adm. Code 702, 703,
and 705.
A)
Recyclable materials used in a manner constituting disposal (35
Ill. Adm. Code 726.Subpart C);
B)
Hazardous wastes burned for energy recovery in boilers and
industrial furnaces that are not regulated under 35 Ill. Adm. Code
724.Subpart O or 725.Subpart O (35 Ill. Adm. Code 726.Subpart
H);
C)
Recyclable materials from which precious metals are reclaimed
(35 Ill. Adm. Code 726.Subpart F);
D)
Spent lead-acid batteries that are being reclaimed (35 Ill. Adm.
Code 726.Subpart G).
3)
The following recyclable materials are not subject to regulation under 35
Ill. Adm. Code 722 through 726, 728, or 702, 703, or 705 and are not
subject to the notification requirements of Section section 3010 of the
Resource Conservation and Recovery Act:
A)
Industrial ethyl alcohol that is reclaimed except that, unless
provided otherwise in an international agreement as specified in
35 Ill. Adm. Code 722.158:
i)
A person initiating a shipment for reclamation in a foreign
country and any intermediary arranging for the shipment
shall comply with the requirements applicable to a
primary exporter in 35 Ill. Adm. Code 722.153;
722.156(a)(1) through (a)(4), (a)(6), and (b); and
722.157; shall export such materials only upon consent of
79
the receiving country and in conformance with the
USEPA Acknowledgment of Consent, as defined in 35 Ill.
Adm. Code 722.Subpart E; and shall provide a copy of
the USEPA Acknowledgment of Consent to the shipment
to the transporter transporting the shipment for export;
ii)
Transporters transporting a shipment for export shall not
accept a shipment if the transporter knows that the
shipment does not conform to the USEPA
Acknowledgement of Consent, shall ensure that a copy of
the USEPA Acknowledgement of Consent accompanies
the shipment, and shall ensure that it is delivered to the
facility designated by the person initiating the shipment;
B)
Scrap metal that is not excluded under Section 721.104(a)(13);
C)
Fuels produced from the refining of oil-bearing hazardous wastes
along with normal process streams at a petroleum refining facility
if such wastes result from normal petroleum refining, production,
and transportation practices (this exemption does not apply to
fuels produced from oil recovered from oil-bearing hazardous
waste where such recovered oil is already excluded under Section
721.104(a)(12));
D)
Petroleum refining wastes.
i)
Hazardous waste fuel produced from oil-bearing
hazardous wastes from petroleum refining, production, or
transportation practices or produced from oil reclaimed
from such hazardous wastes, where such hazardous wastes
are reintroduced into a process that does not use
distillation or does not produce products from crude oil,
so long as the resulting fuel meets the used oil
specification under 35 Ill. Adm. Code 726.140(e) and so
long as no other hazardous wastes are used to produce the
hazardous waste fuel;
ii)
Hazardous waste fuel produced from oil-bearing
hazardous waste from petroleum refining production, and
transportation practices, where such hazardous wastes are
reintroduced into a refining process after a point at which
contaminants are removed, so long as the fuel meets the
used oil fuel specification under 35 Ill. Adm. Code
726.140(e); and
80
iii)
Oil reclaimed from oil-bearing hazardous wastes from
petroleum refining, production, and transportation
practices, which reclaimed oil is burned as a fuel without
reintroduction to a refining process, so long as the
reclaimed oil meets the used oil fuel specification under
35 Ill. Adm. Code 726.140(e); and
E)
Petroleum coke produced from petroleum refinery hazardous
wastes containing oil by the same person that generated the
wastes unless the resulting coke product exceeds one or more of
the characteristics of hazardous waste in 721.Subpart C.
4)
Used oil that is recycled and is also a hazardous waste solely because it
exhibits a hazardous characteristic is not subject to the requirements of
35 Ill. Adm. Code 720 through 728, but it is regulated under 35 Ill.
Adm. Code 739. Used oil that is recycled includes any used oil that is
reused for any purpose following its original use (including the purpose
for which the oil was originally used). Such term includes, but is not
limited to, oil that is re-refined, reclaimed, burned for energy recovery,
or reprocessed.
5)
Hazardous waste that is exported to or imported from designated
member countries of the Organization for Economic Cooperation and
Development (OECD), as defined in Section 722.158(a)(1), for the
purpose of recovery is subject to the requirements of 35 Ill. Adm. Code
722.Subpart H if it is subject to either the hazardous waste manifesting
requirements of 35 Ill. Adm. Code 722 or the universal waste
management standards of 35 Ill. Adm. Code 733.
b)
Generators and transporters of recyclable materials are subject to the applicable
requirements of 35 Ill. Adm. Code 722 and 723 and the notification
requirements under Section section 3010 of the Resource Conservation and
Recovery Act, except as provided in subsection (a) of this Section.
c)
Storage and recycling:
1)
Owners or operators of facilities that store recyclable materials before
they are recycled are regulated under all applicable provisions of 35 Ill.
Adm. Code 702, 703, and 705; 724.Subparts A through L, AA, BB, and
CC; and 725.Subparts A through L, AA, BB, and CC; 726; 728; and
the notification requirement under Section section 3010 of the Resource
Conservation and Recovery Act, except as provided in subsection (a) of
this Section. (The recycling process itself is exempt from regulation,
except as provided in subsection (d) of this Section.)
81
2)
Owners or operators of facilities that recycle recyclable materials without
storing them before they are recycled are subject to the following
requirements, except as provided in subsection (a) of this Section:
A)
Notification requirements under Section section 3010 of the
Resource Conservation and Recovery Act,
B)
35 Ill. Adm. Code 725.171 and 725.172 (dealing with the use of
the manifest and manifest discrepancies), and
C)
subsection (d) of this Section.
d)
Owners or operators of facilities required to have a RCRA permit pursuant to 35
Ill. Adm. Code 703 with hazardous waste management units that recycle
hazardous wastes are subject to 35 Ill. Adm. Code 724.Subparts AA and BB
and 725.Subparts AA and BB.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART C: CHARACTERISTICS OF HAZARDOUS WASTE
Section 721.121
Characteristic of Ignitability
a)
A solid waste exhibits the characteristic of ignitability if a representative sample
of the waste has any of the following properties:
1)
It is a liquid, other than an aqueous solution containing less than 24
percent alcohol by volume, and has a flash point less than 60°C
(140°F), as determined by a Pensky-Martens Closed Cup Tester, using
the test method specified in ASTM D-93, incorporated by reference in
35 Ill. Adm. Code 720.111, or a Setaflash Closed Cup Tester, using the
test method specified in ASTM Standard D-3228 D-3828, incorporated
by reference in 35 Ill. Adm. Code 720.111, or as determined by an
equivalent test method approved by the Board (35 Ill. Adm. Code
720.120).
2)
It is not a liquid and is capable, under standard temperature and
pressure, of causing fire through friction, absorption of moisture or
spontaneous chemical changes and, when ignited, burns so vigorously
and persistently that it creates a hazard.
3)
It is an ignitable compressed gas as defined in 49 CFR 173.300,
incorporated by reference in 35 Ill. Adm. Code 720.111, and as
82
determined by the test methods described in that regulation or equivalent
test methods approved by the Board (35 Ill. Adm. Code 720.120).
4)
It is an oxidizer as defined in 49 CFR 173.151, incorporated by
reference in 35 Ill. Adm. Code 720.111.
b)
A solid waste that exhibits the characteristic of ignitability has the EPA
Hazardous Waste Number of D001.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART D: LISTS OF HAZARDOUS WASTE
Section 721.132
Hazardous Waste from Specific Sources
The following solid wastes are listed hazardous wastes from specific sources unless they are
excluded under 35 Ill. Adm. Code 720.120 and 720.122 and listed in Section 721.Appendix I.
EPA
Hazardous
Waste No.
Industry and Hazardous Waste
Hazard
Code
Wood Preservation:
K001
Bottom sediment sludge from the treatment of wastewaters from
wood preserving processes that use creosote or pentachloro-
phenol.
(T)
Inorganic Pigments:
K002
Wastewater treatment sludge from the production of chrome
yellow and orange pigments.
(T)
K003
Wastewater treatment sludge from the production of molybdate
orange pigments.
(T)
K004
Wastewater treatment sludge from the production of zinc yellow
pigments.
(T)
K005
Wastewater treatment sludge from the production of chrome
green pigments.
(T)
K006
Wastewater treatment sludge from the production of chrome
oxide green pigments (anhydrous and hydrated).
(T)
83
K007
Wastewater treatment sludge from the production of iron blue
pigments.
(T)
K008
Oven residue from the production of chrome oxide green
pigments.
(T)
Organic Chemicals:
K009
Distillation bottoms from the production of acetaldehyde from
ethylene.
(T)
K010
Distillation side cuts from the production of acetaldehyde from
ethylene.
(T)
K011
Bottom stream from the wastewater stripper in the production of
acrylonitrile.
(R,T)
K013
Bottom stream from the acetonitrile column in the production of
acrylonitrile.
(T)
K014
Bottoms from the acetonitrile purification column in the
production of acrylonitrile.
(T)
K015
Still bottoms from the distillation of benzyl chloride.
(T)
K016
Heavy ends or distillation residues from the production of
carbon tetrachloride.
(T)
K017
Heavy ends (still bottoms) from the purification column in the
production of epichlorohydrin.
(T)
K018
Heavy ends from the fractionation column in ethyl chloride
production.
(T)
K019
Heavy ends from the distillation of ethylene dichloride in
ethylene dichloride production.
(T)
K020
Heavy ends from the distillation of vinyl chloride in vinyl
chloride monomer production.
(T)
K021
Aqueous spent antimony catalyst waste from fluoromethanes
production.
(T)
K022
Distillation bottom tars from the production of phenol/acetone
(T)
84
from cumene.
K023
Distillation light ends from the production of phthalic anhydride
from naphthalene.
(T)
K024
Distillation bottoms from the production of phthalic anhydride
from naphthalene.
(T)
K093
Distillation light ends from the production of phthalic anhydride
from ortho-xylene.
(T)
K094
Distillation bottoms from the production of phthalic anhydride
from ortho-xylene.
(T)
K025
Distillation bottoms from the production of nitrobenzene by the
nitration of benzene.
(T)
K026
Stripping still tails from the production of methyl ethyl
pyridines.
(T)
K027
Centrifuge and distillation residues from toluene diisocyanate
production.
(R,T)
K028
Spent catalyst from the hydrochlorinator reactor in the
production of 1,1,1-trichloroethane.
(T)
K029
Waste from the product stream stripper in the production of
1,1,1-trichloroethane.
(T)
K095
Distillation bottoms from the production of 1,1,1-trichloro-
ethane.
(T)
K096
Heavy ends from the heavy ends column from the production of
1,1,1-trichloroethane.
(T)
K030
Column bottoms or heavy ends from the combined production
of trichloroethylene and perchloroethylene.
(T)
K083
Distillation bottoms from aniline production.
(T)
K103
Process residues from aniline extraction from the production of
aniline.
(T)
K104
Combined wastewater streams generated from
nitrobenzene/aniline production.
(T)
85
K085
Distillation or fractionation column bottoms
from the production of chlorobenzenes.
(T)
K105
Separated aqueous stream from the reactor product washing step
in the production of chlorobenzenes.
(T)
K107
Column bottoms from product separation from the production
of 1,1-dimethylhydrazine (UDMH) from carboxylic acid
hydrazides.
(C,T)
K108
Condensed column overheads from product separation and
condensed reactor vent gases from the production of 1,1-di-
methylhydrazine (UDMH) from carboxylic acid hydrazides.
(I,T)
K109
Spent filter cartridges from the product purification from the
production of 1,1-dimethylhydrazine (UDMH) from carboxylic
acid hydrazides.
(T)
K110
Condensed column overheads from intermediate separation from
the production of 1,1-dimethylhydrazine (UDMH) from
carboxylic acid hydrazides.
(T)
K111
Product wastewaters from the production of dinitrotoluene via
nitration of toluene.
(C,T)
K112
Reaction by-product water from the drying column in the
production of toluenediamine via hydrogenation of di-
nitrotoluene.
(T)
K113
Condensed liquid light ends from the purification of toluenedi-
amine in the production of toluenediamine via hydrogenation of
dinitrotoluene.
(T)
K114
Vicinals from the purification of toluenediamine in the
production of toluenediamine via hydrogenation of
dinitrotoluene.
(T)
K115
Heavy ends from the purification of toluenediamine in the
production of toluenediamine via hydrogenation of di-
nitrotoluene.
(T)
K116
Organic condensate from the solvent recovery column in the
production of toluene diisocyanate via phosgenation of
toluenediamine.
(T)
86
K117
Wastewater from the reactor vent gas scrubber in the production
of ethylene dibromide via bromination of ethene.
(T)
K118
Spent adsorbent solids from purification of ethylene dibromide
in the production of ethylene dibromide via bromination of
ethene.
(T)
K136
Still bottoms from the purification of ethylene dibromide in the
production of ethylene dibromide via bromination of ethene.
(T)
K156
Organic waste (including heavy ends, still bottoms, light ends,
spent solvents, filtrates, and decantates) from the production of
carbamates and carbamoyl oximes. (This listing does not apply
to wastes generated from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
K157
Wastewaters (including scrubber waters, condenser waters,
washwaters, and separation waters) from the production of
carbamates and carbamoyl oximes. (This listing does not apply
to wastes generated from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
K158
Bag house dusts and filter/separation solids from the production
of carbamates and carbamoyl oximes. (This listing does not
apply to wastes generated from the manufacture of 3-iodo-2-
propynyl n-butylcarbamate.)
(T)
K159
Organics from the treatment of thiocarbamate wastes.
(T)
K161
Purification solids (including filtration, evaporation, and
centrifugation solids), bag house dust and floor sweepings from
the production of dithiocarbamate acids and their salts. (This
listing does not include K125 or K126.)
(R,T)
Inorganic Chemicals:
K071
Brine purification muds from the mercury cell process in
chlorine production, where separately prepurified brine is not
used.
(T)
K073
Chlorinated hydrocarbon waste from the purification step of the
diaphragm cell process using graphite anodes in chlorine
production.
(T)
87
K106
Wastewater treatment sludge from the mercury cell process in
chlorine production.
(T)
Pesticides:
K031
By-product salts generated in the production of MSMA and
cacodylic acid.
(T)
K032
Wastewater treatment sludge from the production of chlordane.
(T)
K033
Wastewater and scrub water from the chlorination of
cyclopentadiene in the production of chlordane.
(T)
K034
Filter solids from the filtration of hexachlorocyclopentadiene in
the production of chlordane.
(T)
K097
Vacuum stripper discharge from the chlordane chlorinator in the
production of chlordane.
(T)
K035
Wastewater treatment sludges generated in the production of
creosote.
(T)
K036
Still bottoms from toluene reclamation distillation in the
production of disulfoton.
(T)
K037
Wastewater treatment sludges from the production of disulfoton.
(T)
K038
Wastewater from the washing and stripping of phorate
production.
(T)
K039
Filter cake from the filtration of diethylphosphorodithioic acid
in the production of phorate.
(T)
K040
Wastewater treatment sludge from the production of phorate.
(T)
K041
Wastewater treatment sludge from the production of toxaphene.
(T)
K098
Untreated process wastewater from the production of
toxaphene.
(T)
K042
Heavy ends or distillation residues from the distillation of tetra-
chlorobenzene in the production of 2,4,5-T.
(T)
K043
2,6-Dichlorophenol waste from the production of 2,4-D.
(T)
88
K099
Untreated wastewater from the production of 2,4-D.
(T)
K123
Process wastewater (including supernates, filtrates and
washwaters) from the production of ethylenebisdithiocarbamic
acid and its salts.
(T)
K124
Reactor vent scrubber water from the production of ethylenebis-
dithiocarbamic acid and its salts.
(C,T)
K125
Filtration, evaporation and centrifugation solids from the
production of ethylenebisdithiocarbamic acid and its salts.
(T)
K126
Baghouse dust and floor sweepings in milling and packaging
operations from the production or formulation of ethylenebisdi-
thiocarbamic acid and its salts.
(T)
K131
Wastewater from the reactor and spent sulfuric acid from the
acid dryer from the production of methyl bromide.
(C,T)
K132
Spent absorbent and wastewater separator solids from the
production of methyl bromide.
(T)
Explosives:
K044
Wastewater treatment sludges from the manufacturing and
processing of explosives.
(R)
K045
Spent carbon from the treatment of wastewater containing
explosives.
(R)
K046
Wastewater treatment sludges from the manufacturing,
formulation and loading of lead-based initiating compounds.
(T)
K047
Pink/red water from TNT operations.
(R)
Petroleum Refining:
K048
Dissolved air flotation (DAF) float from the petroleum refining
industry.
(T)
K049
Slop oil emulsion solids from the petroleum refining industry.
(T)
K050
Heat exchanger bundle cleaning sludge from the petroleum
refining industry.
(T)
89
K051
API separator sludge from the petroleum refining industry.
(T)
K052
Tank bottoms (leaded) from the petroleum refining industry.
(T)
Iron and Steel:
K061
Emission control dust/sludge from the primary production of
steel in electric furnaces.
(T)
K062
Spent pickle liquor generated by steel finishing operations of
facilities within the iron and steel industry (SIC Codes 331 and
332) (as defined in 35 Ill. Adm. Code 720.110).
(C,T)
Primary Copper:
K064
Acid plant blowdown slurry or sludge resulting from the
thickening of blowdown slurry from primary copper production.
(T)
Primary Lead:
K065
Surface impoundment solids contained in and dredged from
surface impoundments at primary lead smelting facilities.
(T)
Primary Zinc:
K066
Sludge from treatment of process wastewater or acid plant
blowdown from primary zinc production.
(T)
BOARD NOTE: This waste listing is the subject of a judicial
remand in American Mining Congress v. EPA, 907 F.2d 1179
(D.D.C. 1990). The Board intends that this listing not become
enforceable in Illinois until the first date upon which the Board
RCRA program becomes “not equivalent to the Federal
program”, within the meaning of Section section 3006(b) of the
RCRA Act, 42 U.S.C. 6926(b), the Board RCRA rules become
“less stringent” than the USEPA rules, as this phrase is used in
Section section 3009, 42 U.S.C. 6929, or the Board RCRA
rules are not “identical in substance” with the federal rules as
that term is intended by 415 ILCS 5/7.2 and 22.4 as a result of
some action by USEPA with regard to this listing in response to
the American Mining Congress remand.
Primary Aluminum:
K088
Spent potliners from primary aluminum reduction.
(T)
90
Ferroalloys:
K090
Emission control dust or sludge from ferrochromiumsilicon
production.
(T)
K091
Emission control dust or sludge from ferrochromium
production.
(T)
Secondary Lead:
K069
Emission control dust/sludge from secondary lead smelting.
(T)
BOARD NOTE: This listing is administratively stayed for
sludge generated from secondary acid scrubber systems. The
stay will remain in effect until this note is removed.
K100
Waste leaching solution from acid leaching of emission control
dust/sludge from secondary lead smelting.
(T)
Veterinary Pharmaceuticals:
K084
Wastewater treatment sludges generated during the production
of veterinary pharmaceuticals from arsenic or organo-arsenic
compounds.
(T)
K101
Distillation tar residues from the distillation of aniline-based
compounds in the production of veterinary pharmaceuticals
from arsenic or organoarsenic organo-arsenic compounds.
(T)
K102
Residue from use of activated carbon for decolorization in the
production of veterinary pharmaceuticals from arsenic or
organo-arsenic compounds.
(T)
Ink Formulation:
K086
Solvent washes and sludges, caustic washes and sludges, or
water washes and sludges from cleaning tubs and equipment
used in the formulation of ink from pigments, dryers, soaps and
stabilizers containing chromium and lead.
(T)
Coking:
K060
Ammonia still lime sludge from coking operations.
(T)
K087
Decanter tank tar sludge from coking operations.
(T)
91
K141
Process residues from the recovery of coal tar, including, but
not limited to, collecting sump residues from the production of
coke from coal or the recovery of coke by-products produced
from coal. This listing does not include K087 (decanter tank tar
sludges from coking operations).
(T)
K142
Tar storage tank residues from the production of coke from coal
or from the recovery of coke by-products produced from coal.
(T)
K143
Process residues from the recovery of light oil, including, but
not limited to, those generated in stills, decanters, and wash oil
recovery units from the recovery of coke by-products produced
from coal.
(T)
K144
Wastewater sump residues from light oil refining, including, but
not limited to, intercepting or contamination sump sludges from
the recovery of coke by-products produced from coal.
(T)
K145
Residues from naphthalene collection and recovery operations
from the recovery of coke by-products produced from coal.
(T)
K147
Tar storage tank residues from coal tar refining.
(T)
K148
Residues from coal tar distillation, including but not limited to,
still bottoms.
(T)
K149
Distillation bottoms from the production of alpha
α
- (or methyl-)
chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional
groups. (This waste does not include still bottoms from the
distillation of benzyl chloride.)
(T)
K150
Organic residuals, excluding spent carbon adsorbent, from the
spent chlorine gas and hydrochloric acid recovery processes
associated with the production of alpha
α
- (or methyl-)
chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional
groups.
(T)
K151
Wastewater treatment sludges, excluding neutralization and
biological sludges, generated during the treatment of
wastewaters from the production of alpha-
α
- (or methyl-)
chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional
(T)
92
groups.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.133
Discarded Commercial Chemical Products, Off-Specification Species,
Container Residues, and Spill Residues Thereof
The following materials or items are hazardous wastes if and when they are discarded or
intended to be discarded as described in Section 721.102(a)(2)(A), when they are mixed with
waste oil or used oil or other material and applied to the land for dust suppression or road
treatment, when they are otherwise applied to the land in lieu of their original intended use or
when they are contained in products that are applied to land in lieu of their original intended
use, or when, in lieu of their original intended use, they are produced for use as (or as a
component of) a fuel, distributed for use as a fuel, or burned as a fuel.
a)
Any commercial chemical product, or manufacturing chemical intermediate
having the generic name listed in subsection (e) or (f) of this Section.
b)
Any off-specification commercial chemical product or manufacturing chemical
intermediate which, if it met specifications, would have the generic name listed
in subsection (e) or (f) of this Section.
c)
Any residue remaining in a container or inner liner removed from a container
that has held any commercial chemical product or manufacturing chemical
intermediate having the generic name listed in subsection (e) or (f) of this
Section, unless the container is empty as defined in Section 721.107(b)(3).
BOARD NOTE: Unless the residue is being beneficially used or reused, or
legitimately recycled or reclaimed, or being accumulated, stored, transported,
or treated prior to such use, reuse, recycling, or reclamation, the Board
considers the residue to be intended for discard, and thus a hazardous waste.
An example of a legitimate reuse of the residue would be where the residue
remains in the container and the container is used to hold the same commercial
chemical product or manufacturing chemical intermediate it previously held.
An example of the discard of the residue would be where the drum is sent to a
drum reconditioner that reconditions the drum but discards the residue.
d)
Any residue or contaminated soil, water, or other debris resulting from the
cleanup of a spill into or on any land or water of any commercial chemical
product or manufacturing chemical intermediate having the generic name listed
in subsection (e) or (f) of this Section, or any residue or contaminated soil,
water, or other debris resulting from the cleanup of a spill into or on any land
or water, of any off-specification chemical product or manufacturing chemical
intermediate which, if it met specifications, would have the generic name listed
in subsection (e) or (f) of this Section.
93
BOARD NOTE: The phrase “commercial chemical product or manufacturing
chemical intermediate having the generic name listed in ...” refers to a chemical
substance that is manufactured or formulated for commercial or manufacturing
use which consists of the commercially pure grade of the chemical, any
technical grades of the chemical that are produced or marketed, and all
formulations in which the chemical is the sole active ingredient. It does not
refer to a material, such as a manufacturing process waste, that contains any of
the substances listed in subsection (e) or (f) of this Section. Where a
manufacturing process waste is deemed to be a hazardous waste because it
contains a substance listed in subsection (e) or (f) of this Section, such waste
will be listed in either Sections 721.131 or 721.132 or will be identified as a
hazardous waste by the characteristics set forth in Subpart C.
e)
The commercial chemical products, manufacturing chemical intermediates, or
off-specification commercial chemical products or manufacturing chemical
intermediates referred to in subsections (a) through (d) of this Section, are
identified as acute hazardous waste (H) and are subject to the small quantity
exclusion defined in Section 721.105(e). These wastes and their corresponding
USEPA Hazardous Waste Numbers are:
BOARD NOTE: For the convenience of the regulated community the primary
hazardous properties of these materials have been indicated by the letters T
(Toxicity), and R (Reactivity). The absence of a letter indicates that the
compound only is listed for acute toxicity.
Hazardous
Waste No.
Chemical
Abstracts No.
Substance
P023
107-20-0
Acetaldehyde, chloro-
P002
591-08-2
Acetamide, N-(aminothioxomethyl)
P057
640-19-7
Acetamide, 2-fluoro-
P058
62-74-8
Acetic acid, fluoro-, sodium salt
P002
591-08-2
1-Acetyl-2-thiourea
P003
107-02-8
Acrolein
P070
116-06-3
Aldicarb
P203
1646-88-4
Aldicarb sulfone
P004
309-00-2
Aldrin
P005
107-18-6
Allyl alcohol
P006
20859-73-8
Aluminum phosphide (R,T)
P007
2763-96-4
5-(Aminomethyl)-3-isoxazolol
P008
504-24-5
4-Aminopyridine
P009
131-74-8
Ammonium picrate (R)
P119
7803-55-6
Ammonium vanadate
94
P099
506-61-6
Argentate(1-), bis(cyano-C)-, potassium
P010
7778-39-4
Arsenic acid H
3
AsO
4
P012
1327-53-3
Arsenic oxide As
2
O
3
P011
1303-28-2
Arsenic oxide As
2
O
5
P011
1303-28-2
Arsenic pentoxide
P012
1327-53-3
Arsenic trioxide
P038
692-42-2
Arsine, diethyl-
P036
696-28-6
Arsonous dichloride, phenyl-
P054
151-56-4
Aziridine
P067
75-55-8
Aziridine, 2-methyl
P013
542-62-1
Barium cyanide
P024
106-47-8
Benzenamine, 4-chloro-
P077
100-01-6
Benzenamine, 4-nitro-
P028
100-44-7
Benzene, (chloromethyl)-
P042
51-43-4
1,2-Benzenediol, 4-[1-hydroxy-2-(methyl-
amino)ethyl]-, (R)-
P046
122-09-8
Benzeneethanamine, alpha
α
,alpha
α
-dimethyl-
P014
108-98-5
Benzenethiol
P127
1563-66-2
7-Benzofuranol, 2,3-dihydro-2,2-dimethyl-,
methylcarbamate
P188
57-64-7
Benzoic acid, 2-hydroxy-, compound with (3aS-
cis)-1,2,3,3a,8,8a-hexahydro-1,3a,8-trimethyl-
pyrrolo[2,3-b]indol-5-yl methylcarbamate ester
(1:1)
P001
81-81-2
*
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-
phenylbutyl)-, and salts, when present at
concentrations greater than 0.3% percent
P028
100-44-7
Benzyl chloride
P015
7440-41-7
Beryllium powder
P017
598-31-2
Bromoacetone
P018
357-57-3
Brucine
P045
39196-18-6
2-Butanone,3,3-dimethyl-1-(methylthio)-, O-
[methylamino)carbonyl] oxime
P021
592-01-8
Calcium cyanide
P021
592-01-8
Calcium cyanide Ca(CN)
2
P189
55285-14-8
Carbamic acid, [(dibutylamino)- thio]methyl-,
2,3-dihydro-2,2-dimethyl-7-benzofuranyl ester
P191
644-64-4
Carbamic acid, dimethyl-, 1-[(dimethyl-amino)-
carbonyl]-5-methyl-1H-pyrazol-3-yl ester
P192
119-38-0
Carbamic acid, dimethyl-, 3-methyl-1-(1-
methylethyl)-1H-pyrazol-5-yl ester
P190
1129-41-5
Carbamic acid, methyl-, 3-methylphenyl ester
P127
1563-66-2
Carbofuran
P022
75-15-0
Carbon disulfide
P095
75-44-5
Carbonic dichloride
95
P189
55285-14-8
Carbosulfan
P023
107-20-0
Chloroacetaldehyde
P024
106-47-8
p-Chloroaniline
P026
5344-82-1
1-(o-Chlorophenyl)thiourea
P027
542-76-7
3-Chloropropionitrile
P029
544-92-3
Copper cyanide
P029
544-92-3
Copper cyanide CuCN
P202
64-00-6
m-Cumenyl methylcarbamate
P030
Cyanides (soluble cyanide salts), not otherwise
specified
P031
460-19-5
Cyanogen
P033
506-77-4
Cyanogen chloride
P033
506-77-4
Cyanogen chloride CNCl
P034
131-89-5
2-Cyclohexyl-4,6-dinitrophenol
P016
542-88-1
Dichloromethyl ether
P036
696-28-6
Dichlorophenylarsine
P037
60-57-1
Dieldrin
P038
692-42-2
Diethylarsine
P041
311-45-5
Diethyl-p-nitrophenyl phosphate
P040
297-97-2
O,O-Diethyl O-pyrazinyl phosphorothioate
P043
55-91-4
Diisopropylfluorophosphate (DFP)
P191
644-64-4
Dimetilan
P004
309-00-2
1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-hexahydro-,
(1alpha
α
,4alpha
α
,4abeta
β
,5alpha
α
,8alpha
α
,8ab
eta
β
)-
P060
465-73-6
1,4,5,8-Di-methanonaphthalene, 1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-hexahydro-,
(1alpha
α
,4alpha
α
,4abeta
β
,5beta
β
,8beta
β
,8abeta
β
)-
P037
60-57-1
2,7:3,6-Dimethanonaphth[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-1a,2,2a,3,6,6a,7,7a-
octahydro-,
(1aalpha
α
,2beta
β
,2aalpha
α
,3beta
β
,6beta
β
,6aalp
ha
α
,7beta
β
,7aalpha
α
)-
P051
72-20-8
*
2,7:3,6-Dimethanonaphth[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-1a,2,2a,3,6,6a,7,7a-
octahydro-,
(1aalpha
α
,2beta
β
,2abeta
β
,3alpha
α
,6alpha
α
,6ab
eta
β
,7beta
β
,7aalpha
α
)-, and metabolites
P044
60-51-5
Dimethoate
P046
122-09-8
alpha
α
,alpha
α
-Dimethylphenethylamine
P047
534-52-1
*
4,6-Dinitro-o-cresol and salts
P048
51-28-5
2,4-Dinitrophenol
P020
88-85-7
Dinoseb
96
P085
152-16-9
Diphosphoramide, octamethyl-
P111
107-49-3
Diphosphoric acid, tetraethyl ester
P039
298-04-4
Disulfoton
P049
541-53-7
Dithiobiuret
P185
26419-73-8
1,3-Dithiolane-2-carboxaldehyde, 2,4-dimethyl-
, O-[(methylamino)- carbonyl]oxime
P050
115-29-7
Endosulfan
P088
145-73-3
Endothall
P051
72-20-8
Endrin
P051
72-20-8
Endrin, and metabolites
P042
51-43-4
Epinephrine
P031
460-19-5
Ethanedinitrile
P194
23135-22-0
Ethanimidothioc acid, 2-(dimethylamino)-N-
[[(methylamino)carbonyl]oxy]-2-oxo-, methyl
ester
P066
16752-77-5
Ethanimidothioic acid, N-[[(methylamino)-
carbonyl]oxy]-, methyl ester
P101
107-12-0
Ethyl cyanide
P054
151-56-4
Ethylenimine
P097
52-85-7
Famphur
P056
7782-41-4
Fluorine
P057
640-19-7
Fluoroacetamide
P058
62-74-8
Fluoroacetic acid, sodium salt
P198
23422-53-9
Formetanate hydrochloride
P197
17702-57-7
Formparanate
P065
628-86-4
Fulminic acid, mercury (2+) salt (R,T)
P059
76-44-8
Heptachlor
P062
757-58-4
Hexaethyl tetraphosphate
P116
79-19-6
Hydrazinecarbothioamide
P068
60-34-4
Hydrazine, methyl-
P063
74-90-8
Hydrocyanic acid
P063
74-90-8
Hydrogen cyanide
P096
7803-51-2
Hydrogen phosphide
P060
465-73-6
Isodrin
P192
119-38-0
Isolan
P202
64-00-6
3-Isopropylphenyl-N-methylcarbamate
P007
2763-96-4
3(2H)-Isoxazolone, 5-(aminomethyl)-
P196
15339-36-3
Manganese, bis(dimethylcarbamodithioato-
S,S')-
P196
15339-36-3
Manganese dimethyldithiocarbamate
P092
62-38-4
Mercury, (acetato-O)phenyl-
P065
628-86-4
Mercury fulminate (R,T)
P082
62-75-9
Methanamine, N-methyl-N-nitroso-
P064
624-83-9
Methane, isocyanato-
P016
542-88-1
Methane, oxybis[chloro-
97
P112
509-14-8
Methane, tetranitro- (R)
P118
75-70-7
Methanethiol, trichloro-
P198
23422-53-9
Methanimidamide, N,N-dimethyl-N'-[3-
[[(methylamino)-carbonyl]oxy]phenyl]-,
monohydrochloride
P197
17702-57-7
Methanimidamide, N,N-dimethyl-N'-[2-methyl-
4-[[(methylamino)carbonyl]oxy]phenyl]-
P199
2032-65-7
Methiocarb
P050
115-29-7
6,9-Methano-2,4,3-benzodioxathiepen,
6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexa-
hydro-, 3-oxide
P059
76-44-8
4,7-Methano-1H-indene, 1,4,5,6,7,8,8-hepta-
chloro-3a,4,7,7a-tetrahydro-
P066
16752-77-5
Methomyl
P068
60-34-4
Methyl hydrazine
P064
624-83-9
Methyl isocyanate
P069
75-86-5
2-Methyllactonitrile
P071
298-00-0
Methyl parathion
P190
1129-41-5
Metolcarb
P129
315-8-4
Mexacarbate
P072
86-88-4
alpha
α
-Naphthylthiourea
P073
13463-39-3
Nickel carbonyl
P073
13463-39-3
Nickel carbonyl Ni(CO)
4
, (T-4)-
P074
557-19-7
Nickel cyanide
P074
557-19-7
Nickel cyanide Ni(CN)
2
P075
54-11-5
*
Nicotine, and salts
P076
10102-43-9
Nitric oxide
P077
100-01-6
p-Nitroaniline
P078
10102-44-0
Nitrogen dioxide
P076
10102-43-9
Nitrogen oxide NO
P078
10102-44-0
Nitrogen oxide NO
2
P081
55-63-0
Nitroglycerine (R)
P082
62-75-9
N-Nitrosodimethylamine
P084
4549-40-0
N-Nitrosomethylvinylamine
P085
152-16-9
Octamethylpyrophosphoramide
P087
20816-12-0
Osmium oxide OsO
4
, (T-4)-
P087
20816-12-0
Osmium tetroxide
P088
145-73-3
7-Oxabicyclo[2.2.1]heptane-2,3-dicarboxylic
acid
P194
23135-22-0
Oxamyl
P089
56-38-2
Parathion
P034
131-89-5
Phenol, 2-cyclohexyl-4,6-dinitro-
P128
315-18-4
Phenol, 4-(dimethylamino)-3,5-dimethyl-,
methylcarbamate (ester)
P199
2032-65-7
Phenol, (3,5-dimethyl-4-(methylthio)-, methyl-
98
carbamate
P048
51-28-5
Phenol, 2,4-dinitro-
P047
534-52-1
*
Phenol, 2-methyl-4,6-dinitro-, and salts
P202
64-00-6
Phenol, 3-(1-methylethyl)-, methyl carbamate
P201
2631-37-0
Phenol, 3-methyl-5-(1-methylethyl)-, methyl
carbamate
P020
88-85-7
Phenol, 2-(1-methylpropyl)-4,6-dinitro-
P009
131-74-8
Phenol, 2,4,6-trinitro-, ammonium salt (R)
P092
62-38-4
Phenylmercury acetate
P093
103-85-5
Phenylthiourea
P094
298-02-2
Phorate
P095
75-44-5
Phosgene
P096
7803-51-2
Phosphine
P041
311-45-5
Phosphoric acid, diethyl 4-nitrophenyl ester
P039
298-04-4
Phosphorodithioic acid, O,O-diethyl S-[2-
(ethylthio)ethyl] ester
P094
298-02-2
Phosphorodithioic acid, O,O-diethyl S-[(ethyl-
thio)methyl] ester
P044
60-51-5
Phosphorodithioic acid, O,O-dimethyl S-[2-
(methylamino)-2-oxoethyl]ester
P043
55-91-4
Phosphorofluoridic acid, bis(1-methylethyl)ester
P089
56-38-2
Phosphorothioic acid, O,O-diethyl O-(4-
nitrophenyl) ester
P040
297-97-2
Phosphorothioic acid, O,O-diethyl O-pyrazinyl
ester
P097
52-85-7
Phosphorothioic acid, O-[4-[(dimethylamino)-
sulfonyl)]phenyl] O,O-dimethyl ester
P071
298-00-0
Phosphorothioic acid, O,O-dimethyl O-(4-
nitrophenyl) ester
P204
57-47-6
Physostigmine
P188
57-64-7
Physostigmine salicylate
P110
78-00-2
Plumbane, tetraethyl-
P098
151-50-8
Potassium cyanide
P098
151-50-8
Potassium cyanide KCN
P099
506-61-6
Potassium silver cyanide
P201
2631-37-0
Promecarb
P203
1646-88-4
Propanal, 2-methyl-2-(methyl-sulfonyl)-, O-
[(methylamino)carbonyl] oxime
P070
116-06-3
Propanal, 2-methyl-2-(methylthio)-, O-
[(methylamino)carbonyl]oxime
P101
107-12-0
Propanenitrile
P027
542-76-7
Propanenitrile, 3-chloro-
P069
75-86-5
Propanenitrile, 2-hydroxy-2-methyl-
P081
55-63-0
1,2,3-Propanetriol, trinitrate- (R)
P017
598-31-2
2-Propanone, 1-bromo-
99
P102
107-19-7
Propargyl alcohol
P003
107-02-8
2-Propenal
P005
107-18-6
2-Propen-1-ol
P067
75-55-8
1,2-Propylenimine
P102
107-19-7
2-Propyn-1-ol
P008
504-24-5
4-Pyridinamine
P075
54-11-5
*
Pyridine, 3-(1-methyl-2-pyrrolidinyl)-, (S)- and
salts
P204
57-47-6
Pyrrolo[2,3-b]indol-5-ol, 1,2,3,3a,8,8a-hexa-
hydro-1,3a,8-trimethyl-, methylcarbamate
(ester), (3aS-cis)-
P114
12039-52-0
Selenious acid, dithallium (1+) salt
P103
630-10-4
Selenourea
P104
506-64-9
Silver cyanide
P104
506-64-9
Silver cyanide AgCN
P105
26628-22-8
Sodium azide
P106
143-33-9
Sodium cyanide
P106
143-33-9
Sodium cyanide NaCN
P108
57-24-9
*
Strychnidin-10-one, and salts
P018
357-57-3
Strychnidin-10-one, 2,3-dimethoxy-
P108
57-24-9
*
Strychnine and salts
P115
7446-18-6
Sulfuric acid, dithallium (1+) salt
P109
3689-24-5
Tetraethyldithiopyrophosphate
P110
78-00-2
Tetraethyl lead
P111
107-49-3
Tetraethylpyrophosphate
P112
509-14-8
Tetranitromethane (R)
P062
757-58-4
Tetraphosphoric acid, hexaethyl ester
P113
1314-32-5
Thallic oxide
P113
1314-32-5
Thallium oxide Tl
2
O
3
P114
12039-52-0
Thallium (I) selenite
P115
7446-18-6
Thallium (I) sulfate
P109
3689-24-5
Thiodiphosphoric acid, tetraethyl ester
P045
39196-18-4
Thiofanox
P049
541-53-7
Thioimidodicarbonic diamide [(H
2
N)C(S)]
2
NH
P014
108-98-5
Thiophenol
P116
79-19-6
Thiosemicarbazide
P026
5344-82-1
Thiourea, (2-chlorophenyl)-
P072
86-88-4
Thiourea, 1-naphthalenyl-
P093
103-85-5
Thiourea, phenyl-
P123
8001-35-2
Toxaphene
P185
26419-73-8
Tirpate
P118
75-70-7
Trichloromethanethiol
P119
7803-55-6
Vanadic acid, ammonium salt
P120
1314-62-1
Vanadium oxide V
2
O
5
P120
1314-62-1
Vanadium pentoxide
100
P084
4549-40-0
Vinylamine, N-methyl-N-nitroso-
P001
81-81-2
*
Warfarin, and salts, when present at
concentrations greater than 0.3% percent
P121
557-21-1
Zinc cyanide
P121
557-21-1
Zinc cyanide Zn(CN)
2
P205
137-30-4
Zinc, bis(dimethylcarbamodithioato-S,S')-
P122
1314-84-7
Zinc phosphide Zn
3
P
2
, when present at
concentrations greater than 10% percent (R,T)
P205
137-30-4
Ziram
BOARD NOTE: An asterisk (*) following the CAS number indicates that the
CAS number is given for the parent compound only.
f)
The commercial chemical products, manufacturing chemical intermediates, or
off-specification commercial chemical products referred to in subsections (a)
through (d) of this Section, are identified as toxic wastes (T) unless otherwise
designated and are subject to the small quantity exclusion defined in Section
721.105(a) and (g). These wastes and their corresponding USEPA Hazardous
Waste Numbers are:
BOARD NOTE: For the convenience of the regulated community, the primary
hazardous properties of these materials have been indicated by the letters T
(Toxicity), R (Reactivity), I (Ignitability), and C (Corrosivity). The absence of
a letter indicates that the compound is only listed for toxicity.
Hazardous
Waste No.
Chemical
Abstracts No.
Substance
U394
30558-43-1
A2213
U001
75-07-0
Acetaldehyde (I)
U034
75-87-6
Acetaldehyde, trichloro-
U187
62-44-2
Acetamide, N-(4-ethoxyphenyl)-
U005
53-96-3
Acetamide, N-9H-fluoren-2-yl-
U240
P 94-75-7
Acetic acid, (2,4-dichlorophenoxy)-, salts and
esters
U112
141-78-6
Acetic acid, ethyl ester (I)
U144
301-04-2
Acetic acid, lead (2+) salt
U214
563-68-8
Acetic acid, thallium (1+) salt
See F027
93-76-5
Acetic acid, (2,4,5-trichlorophenoxy)-
UOO2U002
67-64-1
Acetone (I)
UOO3U003
75-05-8
Acetonitrile (I,T)
U004
98-86-2
Acetophenone
U005
53-96-3
2-Acetylaminofluorene
U006
75-36-5
Acetyl chloride (C,R,T)
101
U007
79-06-1
Acrylamide
U008
79-10-7
Acrylic acid (I)
U009
107-13-1
Acrylonitrile
U011
61-82-5
Amitrole
U012
62-53-3
Aniline (I,T)
U136
75-60-5
Arsinic acid, dimethyl-
U014
492-80-8
Auramine
U015
115-02-6
Azaserine
U010
50-07-7
Azirino[2',3':3,4]pyrrolo[1,2-a]indole-4,7-di-
one, 6-amino-8-[[(aminocarbonyl)oxy]methyl]-
1,1a,2,8,8a,8b-hexahydro-8a-methoxy-5-
methyl-, [1a-S-
(1aalpha
α
,8beta
β
,8aalpha
α
,8balpha
α
)]-
U280
101-27-9
Barban
U278
22781-23-3
Bendiocarb
U364
22961-82-6
Bendiocarb phenol
U271
17804-35-2
Benomyl
U157
56-49-5
Benz[j]aceanthrylene, 1,2-dihydro-3-methyl-
U016
225-51-4
Benz(c)acridine
U017
98-87-3
Benzal chloride
U192
23950-58-5
Benzamide, 3,5-dichloro-N-(1,1-dimethyl-2-
propynyl)-
U018
56-55-3
Benz[a]anthracene
U094
57-97-6
Benz[a]anthracene, 7,12-dimethyl-
U012
62-53-3
Benzenamine (I,T)
U014
492-80-8
Benzenamine, 4,4'-carbonimidoylbis[N,N-di-
methyl-
U049
3165-93-3
Benzenamine, 4-chloro-2-methyl-,
hydrochloride
U093
60-11-7
Benzenamine, N,N-dimethyl-4-(phenylazo)-
U328
95-53-4
Benzenamine, 2-methyl-
U353
106-49-0
Benzenamine, 4-methyl-
U158
101-14-4
Benzenamine, 4,4'-methylenebis[2-chloro-
U222
636-21-5
Benzenamine, 2-methyl-, hydrochloride
U181
99-55-8
Benzenamine, 2-methyl-5-nitro-
U019
71-43-2
Benzene (I,T)
U038
510-15-6
Benzeneacetic acid, 4-chloro-alpha
α
-(4-chloro-
phenyl)-alpha
α
-hydroxy-, ethyl ester
U030
101-55-3
Benzene, 1-bromo-4-phenoxy-
U035
305-03-3
Benzenebutanoic acid, 4-[bis(2-chloroethyl)-
amino]-
U037
108-90-7
Benzene, chloro-
U221
25376-45-8
Benzenediamine, ar-methyl-
U028
117-81-7
1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl)
ester
102
U069
84-74-2
1,2-Benzenedicarboxylic acid, dibutyl ester
U088
84-66-2
1,2-Benzenedicarboxylic acid, diethyl ester
U102
131-11-3
1,2-Benzenedicarboxylic acid, dimethyl ester
U107
117-84-0
1,2-Benzenedicarboxylic acid, dioctyl ester
U070
95-50-1
Benzene, 1,2-dichloro-
U071
541-73-1
Benzene, 1,3-dichloro-
U072
106-46-7
Benzene, 1,4-dichloro-
U060
72-54-8
Benzene, 1,1'-(2,2-dichloroethylidene)bis[4-
chloro-
U017
98-87-3
Benzene, (dichloromethyl)-
U223
26471-62-5
Benzene, 1,3-diisocyanatomethyl- (R,T)
U239
1330-20-7
Benzene, dimethyl- (I,T)
U201
108-46-3
1,3-Benzenediol
U127
118-74-1
Benzene, hexachloro-
U056
110-82-7
Benzene, hexahydro- (I)
U220
108-88-3
Benzene, methyl-
U105
121-14-2
Benzene, 1-methyl-2,4-dinitro-
U106
606-20-2
Benzene, 2-methyl-1,3-dinitro-
U055
98-82-8
Benzene, (1-methylethyl)- (I)
U169
98-95-3
Benzene, nitro-
U183
608-93-5
Benzene, pentachloro-
U185
82-68-8
Benzene, pentachloronitro-
U020
98-09-9
Benzenesulfonic acid chloride (C,R)
U020
98-09-9
Benzenesulfonyl chloride (C,R)
U207
95-94-3
Benzene, 1,2,4,5-tetrachloro-
U061
50-29-3
Benzene, 1,1'-(2,2,2-trichloroethylidene)bis[4-
chloro-
U247
72-43-5
Benzene, 1,1'-(2,2,2-trichloroethylidene)bis[4-
methoxy-
U023
98-07-7
Benzene, (trichloromethyl)-
U234
99-35-4
Benzene, 1,3,5-trinitro-
U021
92-87-5
Benzidene
U202
P 81-07-2
1,2-Benzisothiazol-3(2H)-one, 1,1-dioxide, and
salts
U203
94-59-7
1,3-Benzodioxole, 5-(2-propenyl)-
U141
120-58-1
1,3-Benzodioxole, 5-(1-propenyl)-
U090
94-58-6
1,3-Benzodioxole, 5-propyl-
U278
22781-23-3
1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl
carbamate
U364
22961-82-6
1,3-Benzodioxol-4-ol, 2,2-dimethyl-
U367
1563-38-8
7-Benzofuranol, 2,3-dihydro-2,2-dimethyl-
U064
189-55-9
Benzo[rst]pentaphene
U248
P 81-81-2
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-oxo-1-
phenylbutyl)-, and salts, when present at
concentrations of 0.3% percent or less
103
U022
50-32-8
Benzo[a]pyrene
U197
106-51-4
p-Benzoquinone
U023
98-07-7
Benzotrichloride (C,R,T)
U085
1464-53-5
2,2'-Bioxirane
U021
92-87-5
[1,1'-Biphenyl]-4,4'-diamine
U073
91-94-1
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dichloro-
U091
119-90-4
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethoxy-
U095
119-93-7
[1,1'-Biphenyl]-4,4'-diamine, 3,3'-dimethyl-
U225
75-25-2
Bromoform
U030
101-55-3
4-Bromophenyl phenyl ether
U128
87-68-3
1,3-Butadiene, 1,1,2,3,4,4-hexachloro-
U172
924-16-3
1-Butanamine, N-butyl-N-nitroso-
U031
71-36-3
1-Butanol (I)
U159
78-93-3
2-Butanone (I,T)
U160
1338-23-4
2-Butanone, peroxide (R,T)
U053
4170-30-3
2-Butenal
U074
764-41-0
2-Butene, 1,4-dichloro- (I,T)
U143
303-34-4
2-Butenoic acid, 2-methyl-, 7-[[2,3-dihydroxy-
2-(1-methoxyethyl)-3-methyl-1-oxobutoxy]-
methyl]-2,3,5,7a-tetrahydro-1H-pyrrolizin-1-yl
ester, [1S-[1alpha
α
(Z), 7(2S*,3R*),
7aalpha
α
]]-
U031
71-36-3
n-Butyl alcohol (I)
U136
75-60-5
Cacodylic acid
U032
13765-19-0
Calcium chromate
U372
10605-21-7
Carbamic acid, 1H-benzimidazol-2-yl, methyl
ester
U271
17804-35-2
Carbamic acid, [1-[(butylamino)carbonyl]-1H-
benzimidazol-2-yl]-, methyl ester
U280
101-27-9
Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-
butynyl ester
U238
51-79-6
Carbamic acid, ethyl ester
U178
615-53-2
Carbamic acid, methylnitroso-, ethyl ester
U373
122-42-9
Carbamic acid, phenyl-, 1-methylethyl ester
U409
23564-05-8
Carbamic acid, [1,2-phenylenebis(imino-
carbonothioyl)]bis-, dimethyl ester
U097
79-44-7
Carbamic chloride, dimethyl-
U114
P 111-54-6
Carbamodithioic acid, 1,2-ethanediylbis-, salts
and esters
U062
2303-16-4
Carbamothioic acid, bis(1-methylethyl)-, S-
(2,3-dichloro-2-propenyl) ester
U389
2303-17-5
Carbamothioic acid, bis(1-methylethyl)-, S-
(2,3,3-trichloro-2-propenyl) ester
U387
52888-80-9
Carbamothioic acid, dipropyl-, S-(phenyl-
methyl) ester
104
U279
63-25-2
Carbaryl
U372
10605-21-7
Carbendazim
U367
1563-38-8
Carbofuran phenol
U215
6533-73-9
Carbonic acid, dithallium (1+) salt
U033
353-50-4
Carbonic difluoride
U156
79-22-1
Carbonochloridic acid, methyl ester (I,T)
U033
353-50-4
Carbon oxyfluoride (R,T)
U211
56-23-5
Carbon tetrachloride
U034
75-87-6
Chloral
U035
305-03-3
Chlorambucil
U036
57-74-9
Chlordane, alpha
α
and gamma
γ
isomers
U026
494-03-1
Chlornaphazin
U037
108-90-7
Chlorobenzene
U038
510-15-6
Chlorobenzilate
U039
59-50-7
p-Chloro-m-cresol
U042
110-75-8
2-Chloroethyl vinyl ether
U044
67-66-3
Chloroform
U046
107-30-2
Chloromethyl methyl ether
U047
91-58-7
beta
β
-Chloronaphthalene
U048
95-57-8
o-Chlorophenol
U049
3165-93-3
4-Chloro-o-toluidine, hydrochloride
U032
13765-19-0
Chromic acid H
2
CrO
4
, calcium salt
U050
218-01-9
Chrysene
U051
Creosote
U052
1319-77-3
Cresol (Cresylic acid)
U053
4170-30-3
Crotonaldehyde
U055
98-82-8
Cumeme (I)
U246
506-68-3
Cyanogen bromide CNBr
U197
106-51-4
2,5-Cyclohexadiene-1,4-dione
U056
110-82-7
Cyclohexane (I)
U129
58-89-9
Cyclohexane, 1,2,3,4,5,6-hexachloro-,
(1alpha
α
,2alpha
α
,3beta
β
,4alpha
α
,5alpha
α
,6bet
a
β
)-
U057
108-94-1
Cyclohexanone (I)
U130
77-47-4
1,3-Cyclopentadiene, 1,2,3,4,5,5-hexachloro-
U058
50-18-0
Cyclophosphamide
U240
P 94-75-7
2,4-D, salts and esters
U059
20830-81-3
Daunomycin
U060
72-54-8
DDD
U061
50-29-3
DDT
U062
2303-16-4
Diallate
U063
53-70-3
Dibenz[a,h]anthracene
U064
189-55-9
Dibenzo[a,i]pyrene
U066
96-12-8
1,2-Dibromo-3-chloropropane
U069
84-74-2
Dibutyl phthalate
105
U070
95-50-1
o-Dichlorobenzene
U071
541-73-1
m-Dichlorobenzene
U072
106-46-7
p-Dichlorobenzene
U073
91-94-1
3,3'-Dichlorobenzidine
U074
764-41-0
1,4-Dichloro-2-butene (I,T)
U075
75-71-8
Dichlorodifluoromethane
U078
75-35-4
1,1-Dichloroethylene
U079
156-60-5
1,2-Dichloroethylene
U025
111-44-4
Dichloroethyl ether
U027
108-60-1
Dichloroisopropyl ether
U024
111-91-1
Dichloromethoxy ethane
U081
120-83-2
2,4-Dichlorophenol
U082
87-65-0
2,6-Dichlorophenol
U084
542-75-6
1,3-Dichloropropene
U085
1464-53-5
1,2:3,4-Diepoxybutane (I,T)
U395
5952-26-1
Diethylene glycol, dicarbamate
U108
123-91-1
1,4-Diethyleneoxide
U028
117-81-7
Diethylhexyl phthalate
U086
1615-80-1
N,N'-Diethylhydrazine
U087
3288-58-2
O,O-Diethyl S-methyl dithiophosphate
U088
84-66-2
Diethyl phthalate
U089
56-53-1
Diethylstilbestrol
U090
94-58-6
Dihydrosafrole
U091
119-90-4
3,3'-Dimethoxybenzidine
U092
124-40-3
Dimethylamine (I)
U093
60-11-7
p-Dimethylaminoazobenzene
U094
57-97-6
7,12-Dimethylbenz[a]anthracene
U095
119-93-7
3,3'-Dimethylbenzidine
U096
80-15-9
alpha
α
, alpha
α
-Dimethylbenzylhydroperoxide
(R)
U097
79-44-7
Dimethylcarbamoyl chloride
U098
57-14-7
1,1-Dimethylhydrazine
U099
540-73-8
1,2-Dimethylhydrazine
U101
105-67-9
2,4-Dimethylphenol
U102
131-11-3
Dimethyl phthalate
U103
77-78-1
Dimethyl sulfate
U105
121-14-2
2,4-Dinitrotoluene
U106
606-20-2
2,6-Dinitrotoluene
U107
117-84-0
Di-n-octyl phthalate
U108
123-91-1
1,4-Dioxane
U109
122-66-7
1,2-Diphenylhydrazine
U110
142-84-7
Dipropylamine (I)
U111
621-64-7
Di-n-propylnitrosamine
U041
106-89-8
Epichlorohydrin
U001
75-07-0
Ethanal (I)
106
U404
121-44-8
Ethanamine, N,N-diethyl-
U174
55-18-5
Ethanamine, N-ethyl-N-nitroso-
U155
91-80-5
1,2-Ethanediamine, N,N-dimethyl-N'-2-
pyridinyl-N'-(2-thienylmethyl)-
U067
106-93-4
Ethane, 1,2-dibromo-
U076
75-34-3
Ethane, 1,1-dichloro-
U077
107-06-2
Ethane, 1,2-dichloro-
U131
67-72-1
Ethane, hexachloro-
U024
111-91-1
Ethane, 1,1'-[methylenebis(oxy)]bis[2-chloro-
U117
60-29-7
Ethane, 1,1'-oxybis- (I)
U025
111-44-4
Ethane, 1,1'-oxybis[2-chloro-
U184
76-01-7
Ethane, pentachloro-
U208
630-20-6
Ethane, 1,1,1,2-tetrachloro-
U209
79-34-5
Ethane, 1,1,2,2-tetrachloro-
U218
62-55-5
Ethanethioamide
U226
71-55-6
Ethane, 1,1,1-trichloro-
U227
79-00-5
Ethane, 1,1,2-trichloro-
U410
59669-26-0
Ethanimidothioic acid, N,N'- [thiobis[(methyl-
imino)carbonyloxy]]bis-, dimethyl ester
U394
30558-43-1
Ethanimidothioic acid, 2-(dimethylamino)-N-
hydroxy-2-oxo-, methyl ester
U359
110-80-5
Ethanol, 2-ethoxy-
U173
1116-54-7
Ethanol, 2,2'-(nitrosoimino)bis-
U395
5952-26-1
Ethanol, 2,2'-oxybis-, dicarbamate
U004
98-86-2
Ethanone, 1-phenyl-
U043
75-01-4
Ethene, chloro-
U042
110-75-8
Ethene, (2-chloroethoxy)-
U078
75-35-4
Ethene, 1,1-dichloro-
U079
156-60-5
Ethene, 1,2-dichloro-, (E)-
U210
127-18-4
Ethene, tetrachloro-
U228
79-01-6
Ethene, trichloro-
U112
141-78-6
Ethyl acetate (I)
U113
140-88-5
Ethyl acrylate (I)
U238
51-79-6
Ethyl carbamate (urethane)
U117
60-29-7
Ethyl ether
U114
P 111-54-6
Ethylenebisdithiocarbamic acid, salts and esters
U067
106-93-4
Ethylene dibromide
U077
107-06-2
Ethylene dichloride
U359
110-80-5
Ethylene glycol monoethyl ether
U115
75-21-8
Ethylene oxide (I,T)
U116
96-45-7
Ethylenethiourea
U076
75-34-3
Ethylidene dichloride
U118
97-63-2
Ethyl methacrylate
U119
62-50-0
Ethyl methanesulfonate
U120
206-44-0
Fluoranthene
107
U122
50-00-0
Formaldehyde
U123
64-18-6
Formic acid (C,T)
U124
110-00-9
Furan (I)
U125
98-01-1
2-Furancarboxaldehyde (I)
U147
108-31-6
2,5-Furandione
U213
109-99-9
Furan, tetrahydro- (I)
U125
98-01-1
Furfural (I)
U124
110-00-9
Furfuran (I)
U206
18883-66-4
Glucopyranose, 2-deoxy-2-(3-methyl-3-nitroso-
ureido)-, D-
U206
18883-66-4
D-Glucose, 2-deoxy-2-[[(methylnitrosoamino)-
carbonyl]amino]-
U126
765-34-4
Glycidylaldehyde
U163
70-25-7
Guanidine, N-methyl-N'-nitro-N-nitroso-
U127
118-74-1
Hexachlorobenzene
U128
87-68-3
Hexachlorobutadiene
U130
77-47-4
Hexachlorocyclopentadiene
U131
67-72-1
Hexachloroethane
U132
70-30-4
Hexachlorophene
U243
1888-71-7
Hexachloropropene
U133
302-01-2
Hydrazine (R,T)
U086
1615-80-1
Hydrazine, 1,2-diethyl-
U098
57-14-7
Hydrazine, 1,1-dimethyl-
U099
540-73-8
Hydrazine, 1,2-dimethyl-
U109
122-66-7
Hydrazine, 1,2-diphenyl-
U134
7664-39-3
Hydrofluoric acid (C,T)
U134
7664-39-3
Hydrogen fluoride (C,T)
U135
7783-06-4
Hydrogen sulfide
U135
7783-06-4
Hydrogen sulfide H
2
S
U096
80-15-9
Hydroperoxide, 1-methyl-1-phenylethyl- (R)
U116
96-45-7
2-Imidazolidinethione
U137
193-39-5
Indeno[1,2,3-cd]pyrene
U190
85-44-9
1,3-Isobenzofurandione
U140
78-83-1
Isobutyl alcohol (I,T)
U141
120-58-1
Isosafrole
U142
143-50-0
Kepone
U143
303-34-4
Lasiocarpene
U144
301-04-2
Lead acetate
U146
1335-32-6
Lead, bis(acetato-O)tetrahydroxytri-
U145
7446-27-7
Lead phosphate
U146
1335-32-6
Lead subacetate
U129
58-89-9
Lindane
U163
70-25-7
MNNG
U147
108-31-6
Maleic anhydride
U148
123-33-1
Maleic hydrazide
108
U149
109-77-3
Malononitrile
U150
148-82-3
Melphalan
U151
7439-97-6
Mercury
U152
126-98-7
Methacrylonitrile (I,T)
U092
124-40-3
Methanamine, N-methyl- (I)
U029
74-83-9
Methane, bromo-
U045
74-87-3
Methane, chloro- (I,T)
U046
107-30-2
Methane, chloromethoxy-
U068
74-95-3
Methane, dibromo-
U080
75-09-2
Methane, dichloro-
U075
75-71-8
Methane, dichlorodifluoro-
U138
74-88-4
Methane, iodo-
U119
62-50-0
Methanesulfonic acid, ethyl ester
U211
56-23-5
Methane, tetrachloro-
U153
74-93-1
Methanethiol (I,T)
U225
75-25-2
Methane, tribromo-
U044
67-66-3
Methane, trichloro-
U121
75-69-4
Methane, trichlorofluoro-
U036
57-74-9
4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8-
octachloro-2,3,3a,4,7,7a-hexahydro-
U154
67-56-1
Methanol (I)
U155
91-80-5
Methapyrilene
U142
143-50-0
1,3,4-Metheno-2H-cyclobuta[cd]pentalen-2-
one, 1,1a,3,3a,4,5,5,5a,5b,6-decachloro-
octahydro-
U247
72-43-5
Methoxychlor
U154
67-56-1
Methyl alcohol (I)
U029
74-83-9
Methyl bromide
U186
504-60-9
1-Methylbutadiene (I)
U045
74-87-3
Methyl chloride (I,T)
U156
79-22-1
Methyl chlorocarbonate (I,T)
U226
71-55-6
Methylchloroform
U157
56-49-5
3-Methylcholanthrene
U158
101-14-4
4,4'-Methylenebis(2-chloroaniline)
U068
74-95-3
Methylene bromide
U080
75-09-2
Methylene chloride
U159
78-93-3
Methyl ethyl ketone (MEK) (I,T)
U160
1338-23-4
Methyl ethyl ketone peroxide (R,T)
U138
74-88-4
Methyl iodide
U161
108-10-1
Methyl isobutyl ketone (I)
U162
80-62-6
Methyl methacrylate (I,T)
U161
108-10-1
4-Methyl-2-pentanone (I)
U164
56-04-2
Methylthiouracil
U010
50-07-7
Mitomycin C
U059
20830-81-3
5,12-Naphthacenedione, 8-acetyl-10-[(3-amino-
109
2,3,6-trideoxy)-alpha
α
-L-lyxo-hexapyranosyl)-
oxyl]-7,8,9,10-tetrahydro-6,8,11-trihydroxy-1-
methoxy-, (8S-cis)-
U167
134-32-7
1-Naphthalenamine
U168
91-59-8
2-Naphthalenamine
U026
494-03-1
Naphthaleneamine, N,N'-bis(2-chloroethyl)-
U165
91-20-3
Naphthalene
U047
91-58-7
Naphthalene, 2-chloro-
U166
130-15-4
1,4-Naphthalenedione
U236
72-57-1
2,7-Naphthalenedisulfonic acid, 3,3'-[(3,3'-di-
methyl-[1,1'-biphenyl]-4,4'-diyl)bis(azo)bis[5-
amino-4-hydroxy]-, tetrasodium salt
U279
63-25-2
1-Naphthalenol, methylcarbamate
U166
130-15-4
1,4-Naphthoquinone
U167
134-32-7
alpha
α
-Naphthylamine
U168
91-59-8
beta
β
-Naphthylamine
U217
10102-45-1
Nitric acid, thallium (1+) salt
U169
98-95-3
Nitrobenzene (I,T)
U170
100-02-7
p-Nitrophenol
U171
79-46-9
2-Nitropropane (I,T)
U172
924-16-3
N-Nitrosodi-n-butylamine
U173
1116-54-7
N-Nitrosodiethanolamine
U174
55-18-5
N-Nitrosodiethylamine
U176
759-73-9
N-Nitroso-N-ethylurea
U177
684-93-5
N-Nitroso-N-methylurea
U178
615-53-2
N-Nitroso-N-methylurethane
U179
100-75-4
N-Nitrosopiperidine
U180
930-55-2
N-Nitrosopyrrolidine
U181
99-55-8
5-Nitro-o-toluidine
U193
1120-71-4
1,2-Oxathiolane, 2,2-dioxide
U058
50-18-0
2H-1,3,2-Oxazaphosphorin-2-amine, N,N-bis-
(2-chloroethyl)tetrahydro-, 2-oxide
U115
75-21-8
Oxirane (I,T)
U126
765-34-4
Oxiranecarboxyaldehyde
U041
106-89-8
Oxirane, (chloromethyl)-
U182
123-63-7
Paraldehyde
U183
608-93-5
Pentachlorobenzene
U184
76-01-7
Pentachloroethane
U185
82-68-8
Pentachloronitrobenzene (PCNB)
See F027
87-86-5
Pentachlorophenol
U161
108-10-1
Pentanol, 4-methyl-
U186
504-60-9
1,3-Pentadiene (I)
U187
62-44-2
Phenacetin
U188
108-95-2
Phenol
U048
95-57-8
Phenol, 2-chloro-
110
U039
59-50-7
Phenol, 4-chloro-3-methyl-
U081
120-83-2
Phenol, 2,4-dichloro-
U082
87-65-0
Phenol, 2,6-dichloro-
U089
56-53-1
Phenol, 4,4'-(1,2-diethyl-1,2-ethenediyl)bis-,
(E)-
U101
105-67-9
Phenol, 2,4-dimethyl-
U052
1319-77-3
Phenol, methyl-
U132
70-30-4
Phenol, 2,2'-methylenebis[3,4,6-trichloro-
U411
114-26-1
Phenol, 2-(1-methylethoxy)-, methylcarbamate
U170
100-02-7
Phenol, 4-nitro-
See F027
87-86-5
Phenol, pentachloro-
See F027
58-90-2
Phenol, 2,3,4,6-tetrachloro-
See F027
95-95-4
Phenol, 2,4,5-trichloro-
See F027
88-06-2
Phenol, 2,4,6-trichloro-
U150
148-82-3
L-Phenylalanine, 4-[bis(2-chloroethyl)amino]-
U145
7446-27-7
Phosphoric acid, lead (2+) salt (2:3)
U087
3288-58-2
Phosphorodithioic acid, O,O-diethyl S-methyl
ester
U189
1314-80-3
Phosphorus sulfide (R)
U190
85-44-9
Phthalic anhydride
U191
109-06-8
2-Picoline
U179
100-75-4
Piperidine, 1-nitroso-
U192
23950-58-5
Pronamide
U194
107-10-8
1-Propanamine (I,T)
U111
621-64-7
1-Propanamine, N-nitroso-N-propyl-
U110
142-84-7
1-Propanamine, N-propyl- (I)
U066
96-12-8
Propane, 1,2-dibromo-3-chloro-
U083
78-87-5
Propane, 1,2-dichloro-
U149
109-77-3
Propanedinitrile
U171
79-46-9
Propane, 2-nitro- (I,T)
U027
108-60-1
Propane, 2,2'-oxybis[2-chloro-
See F027
93-72-1
Propanoic acid, 2-(2,4,5-trichlorophenoxy)-
U193
1120-71-4
1,3-Propane sultone
U235
126-72-7
1-Propanol, 2,3-dibromo-, phosphate (3:1)
U140
78-83-1
1-Propanol, 2-methyl- (I,T)
U002
67-64-1
2-Propanone (I)
U007
79-06-1
2-Propenamide
U084
542-75-6
1-Propene, 1,3-dichloro-
U243
1888-71-7
1-Propene, 1,1,2,3,3,3-hexachloro-
U009
107-13-1
2-Propenenitrile
U152
126-98-7
2-Propenenitrile, 2-methyl- (I,T)
U008
79-10-7
2-Propenoic acid (I)
U113
140-88-5
2-Propenoic acid, ethyl ester (I)
U118
97-63-2
2-Propenoic acid, 2-methyl-, ethyl ester
U162
80-62-6
2-Propenoic acid, 2-methyl-, methyl ester (I,T)
111
U373
122-42-9
Propham
U411
114-26-1
Propoxur
See F027
93-72-1
Propionic acid, 2-(2,4,5-trichlorophenoxy)-
U194
107-10-8
n-Propylamine (I,T)
U083
78-87-5
Propylene dichloride
U387
52888-80-9
Prosulfocarb
U148
123-33-1
3,6-Pyridazinedione, 1,2-dihydro-
U196
110-86-1
Pyridine
U191
109-06-8
Pyridine, 2-methyl-
U237
66-75-1
2,4-(1H,3H)-Pyrimidinedione, 5-[bis(2-chloro-
ethyl)amino]-
U164
58-04-2
4(1H)-Pyrimidinone, 2,3-dihydro-6-methyl-2-
thioxo-
U180
930-55-2
Pyrrolidine, 1-nitroso-
U200
50-55-5
Reserpine
U201
108-46-3
Resorcinol
U202
P 81-07-2
Saccharin and salts
U203
94-59-7
Safrole
U204
7783-00-8
Selenious acid
U204
7783-00-8
Selenium dioxide
U205
7488-56-4
Selenium sulfide
U205
7488-56-4
Selenium sulfide SeS
2
(R,T)
U015
115-02-6
L-Serine, diazoacetate (ester)
See F027
93-72-1
Silvex (2,4,5-TP)
U206
18883-66-4
Streptozotocin
U103
77-78-1
Sulfuric acid, dimethyl ester
U189
1314-80-3
Sulfur phosphide (R)
See F027
93-76-5
2,4,5-T
U207
95-94-3
1,2,4,5-Tetrachlorobenzene
U208
630-20-6
1,1,1,2-Tetrachloroethane
U209
79-34-5
1,1,2,2-Tetrachloroethane
U210
127-18-4
Tetrachloroethylene
See F027
58-90-2
2,3,4,6-Tetrachlorophenol
U213
109-99-9
Tetrahydrofuran (I)
U214
563-68-8
Thallium (I) acetate
U215
6533-73-9
Thallium (I) carbonate
U216
7791-12-0
Thallium (I) chloride
U216
7791-12-0
Thallium chloride TlCl
U217
10102-45-1
Thallium (I) nitrate
U218
62-55-5
Thioacetamide
U410
59669-26-0
Thiodicarb
U153
74-93-1
Thiomethanol (I,T)
U244
137-26-8
Thioperoxydicarbonic diamide [(H
2
N)C(S)]
2
S
2
,
tetramethyl-
U409
23564-05-8
Thiophanate-methyl
112
U219
62-56-6
Thiourea
U244
137-26-8
Thiram
U220
108-88-3
Toluene
U221
25376-45-8
Toluenediamine
U223
26471-62-5
Toluene diisocyanate (R,T)
U328
95-53-4
o-Toluidine
U353
106-49-0
p-Toluidine
U222
636-21-5
o-Toluidine hydrochloride
U389
2303-17-5
Triallate
U011
61-82-5
1H-1,2,4-Triazol-3-amine
U227
79-00-5
1,1,2-Trichloroethane
U228
79-01-6
Trichloroethylene
U121
75-69-4
Trichloromonofluoromethane
See F027
95-95-4
2,4,5-Trichlorophenol
See F027
88-06-2
2,4,6-Trichlorophenol
U404
121-44-8
Triethylamine
U234
99-35-4
1,3,5-Trinitrobenzene (R,T)
U182
123-63-7
1,3,5-Trioxane, 2,4,6-trimethyl-
U235
126-72-7
Tris(2,3-dibromopropyl) phosphate
U236
72-57-1
Trypan blue
U237
66-75-1
Uracil mustard
U176
759-73-9
Urea, N-ethyl-N-nitroso-
U177
684-93-5
Urea, N-methyl-N-nitroso-
U043
75-01-4
Vinyl chloride
U248
P 81-81-2
Warfarin, and salts, when present at
concentrations of 0.3% percent or less
U239
1330-20-7
Xylene (I)
U200
50-55-5
Yohimban-16-carboxylic acid, 11,17-dimeth-
oxy-18-[(3,4,5-trimethoxybenzoyl)oxy]-,
methyl ester,
(3beta
β
,16beta
β
,17alpha
α
,18beta
β
,20alpha
α
)-
U249
1314-84-7
Zinc phosphide Zn
3
P
2
, when present at
concentrations of 10% percent or less
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.Appendix H
Hazardous Constituents
Common Name
Chemical Abstracts Name
Chemical
Abstracts
Number
Hazard
ous
Waste
Numbe
r
113
A2213
Ethanimidothioic acid, 2-
(dimethylamino)-N-hydroxy-2-
oxo-, methyl ester
30558-43-1
U394
Acetonitrile
Same
75-05-8
U003
Acetophenone
Ethanone, 1-phenyl-
98-86-2
U004
2-Acetylaminofluorene
Acetamide, N-9H-fluoren-2-yl-
53-96-3
UOO5
U005
Acetyl chloride
Same
75-36-5
U006
1-Acetyl-2-thiourea
Acetamide, N-
(aminothioxomethyl)-
591-08-2
P002
Acrolein
2-Propenal
107-02-8
P003
Acrylamide
2-Propenamide
79-06-1
U007
Acrylonitrile
2-Propenenitrile
107-13-1
U009
Aflatoxins
Same
1402-68-2
Aldicarb
Propanal, 2-methyl-2-
(methylthio)-, O-
[(methylamino)carbonyl]oxime
116-06-3
P070
Aldicarb sulfone
Propanal, 2-methyl-2- (methyl-
sulfonyl)-, O-[(methylamino)-
carbonyl]oxime
1646-88-4
P203
Aldrin
1,4,5,8-Dimethanonaphthalene,
1,2,3,4,10,10-hexachloro-
1,4,4a,5,8,8a-hexahydro-, (1-
alpha
α
,4-alpha
α
,4a-beta
β
,5-
alpha
α
,8-alpha
α
,8a-beta
β
)-
309-00-2
P004
Allyl alcohol
2-Propen-1-ol
107-18-6
P005
Allyl chloride
1-Propene, 3-chloro-
107-18-6
Aluminum phosphide
Same
20859-73-8
P006
4-Aminobiphenyl
[1,1'-Biphenyl]-4-amine
92-67-1
5-(Aminomethyl)-3-isoxazolol
3(2H)-Isoxazolone, 5-(amino-
methyl)-
2763-96-4
P007
4-Aminopyridine
4-Pyridinamine
504-24-5
P008
Amitrole
1H-1,2,4-Triazol-3-amine
61-82-5
U011
Ammonium vanadate
Vanadic acid, ammonium salt
7803-55-6
U119
Aniline
Benzenamine
62-53-3
U012
Antimony
Same
7440-36-0
Antimony compounds, N.O.S. (not
otherwise specified)
Aramite
Sulfurous acid, 2-chloroethyl-,
2-[4-(1,1-dimethylethyl)-
phenoxy]-1-methylethyl ester
140-57-8
Arsenic
Arsenic
7440-38-2
Arsenic compounds, N.O.S.
Arsenic acid
Arsenic acid H
3
AsO
4
7778-39-4
P010
114
Arsenic pentoxide
Arsenic oxide As
2
O
5
1303-28-2
PO11P
011
Arsenic trioxide
Arsenic oxide As
2
O
3
1327-53-3
P012
Auramine
Benzenamine, 4,4'-carbon-
imidoylbis[N, N-dimethyl-
492-80-8
U014
Azaserine
L-Serine, diazoacetate (ester)
115-02-6
U015
Barban
Carbamic acid, (3-chloro-
phenyl)-, 4-chloro-2-butynyl
ester
101-27-9
U280
Barium
Same
7440-39-3
Barium compounds, N.O.S.
Barium cyanide
Same
542-62-1
P013
Bendiocarb
1,3-Benzodioxol-4-ol-2,2-
dimethyl-, methyl carbamate
22781-23-3
U278
Bendiocarb phenol
1,3-Benzodioxol-4-ol-2,2-
dimethyl-,
22961-82-6
U364
Benomyl
Carbamic acid, [1- [(butyl-
amino)carbonyl]-1H-benz-
imidazol-2-yl]-, methyl ester
17804-35-2
U271
Benz[c]acridine
Same
225-51-4
U016
Benz[a]anthracene
Same
56-55-3
U018
Benzal chloride
Benzene, (dichloromethyl)-
98-87-3
U017
Benzene
Same
71-43-2
U018
Benzenearsonic acid
Arsonic acid, phenyl-
98-05-5
Benzidine
[1,1'-Biphenyl]-4,4'-diamine
92-87-5
U021
Benzo[b]fluoranthene
Benz[e]acephenanthrylene
205-99-2
Benzo[j]fluoranthene
Same
205-82-3
Benzo(k)fluoranthene
Same
207-08-9
Benzo[a]pyrene
Same
50-32-8
U022
p-Benzoquinone
2,5-Cyclohexadiene-1,4-dione
106-51-4
U197
Benzotrichloride
Benzene, (trichloromethyl)-
98-07-7
U023
Benzyl chloride
Benzene, (chloromethyl)-
100-44-7
P028
Beryllium powder
Same
7440-41-7
P015
Beryllium compounds, N.O.S.
Bis(pentamethylene)thiuram
tetrasulfide
Piperidine, 1,1'-(tetrathio-
dicarbonothioyl)-bis-
120-54-7
Bromoacetone
2-Propanone, 1-bromo-
598-31-2
P017
Bromoform
Methane, tribromo-
75-25-2
U225
4-Bromophenyl phenyl ether
Benzene, 1-bromo-4-phenoxy-
101-55-3
U030
Brucine
Strychnidin-10-one, 2,3-
dimethoxy-
357-57-3
P018
Butylate
Carbamothioic acid, bis(2-
methylpropyl)-, S-ethyl ester
2008-41-5
Butyl benzyl phthalate
1,2-Benzenedicarboxylic acid,
butyl phenylmethyl ester
85-68-7
115
Cacodylic acid
Arsenic acid, dimethyl-
75-60-5
U136
Cadmium
Same
7440-43-9
Cadmium compounds, N.O.S.
Calcium chromate
Chromic acid H
2
CrO
4
, calcium
salt
13765-19-0
U032
Calcium cyanide
Calcium cyanide Ca(CN)
2
592-01-8
P021
Carbaryl
1-Naphthalenol, methyl-
carbamate
63-25-2
U279
Carbendazim
Carbamic acid, 1H-benz-
imidazol-2-yl, methyl ester
10605-21-7
U372
Carbofuran
7-Benzofuranol, 2,3-dihydro-
2,2-dimethyl-, methylcarbamate
1563-66-2
P127
Carbofuran phenol
7-Benzofuranol, 2,3-dihydro-
2,2-dimethyl-
1563-38-8
U367
Carbosulfan
Carbamic acid, [(dibutyl-
amino)thio] methyl-, 2,3-
dihydro-2,2-dimethyl-7-benzo-
furanyl ester
55285-14-8
P189
Carbon disulfide
Same
75-15-0
P022
Carbon oxyfluoride
Carbonic difuoride
353-50-4
U033
Carbon tetrachloride
Methane, tetrachloro-
56-23-5
U211
Chloral
Acetaldehyde, trichloro-
75-87-6
U034
Chlorambucil
Benzenebutanoic acid, 4[bis-(2-
chloroethyl)amino]-
305-03-3
U035
Chlordane
4,7-Methano-1H-indene,
1,2,4,5,6,7,8,8-octachloro-
2,3,3a,4,7,7a-hexahydro-
57-74-9
U036
Chlordane, alpha
α
and gamma
γ
isomers
U036
Chlorinated benzenes, N.O.S.
Chlorinated ethane, N.O.S.
Chlorinated fluorocarbons, N.O.S.
Chlorinated naphthalene, N.O.S.
Chlorinated phenol, N.O.S.
Chlornaphazine
Naphthalenamine, N,N'-bis(2-
chloroethyl)-
494-03-1
U026
Chloroacetaldehyde
Acetaldehyde, chloro-
107-20-0
P023
Chloroalkyl ethers, N.O.S.
p-Chloroaniline
Benzenamine, 4-chloro-
106-47-8
P024
Chlorobenzene
Benzene, chloro-
108-90-7
U037
Chlorobenzilate
Benzeneacetic acid, 4-chloro-
alpha
α
-(4-chlorophenyl)-
alpha
α
-hydroxy-, ethyl ester
510-15-6
U038
p-Chloro-m-cresol
Phenol, 4-chloro-3-methyl-
59-50-7
U039
2-Chloroethyl vinyl ether
Ethene, (2-chloroethoxy)-
110-75-8
U042
116
Chloroform
Methane, trichloro-
67-66-3
U044
Chloromethyl methyl ether
Methane, chloromethoxy-
107-30-2
U046
beta
β
-Chloronaphthalene
Naphthalene, 2-chloro-
91-58-7
U047
o-Chlorophenol
Phenol, 2-chloro-
95-57-8
U048
1-(o-Chlorophenyl)thiourea
Thiourea, (2-chlorophenyl)-
5344-82-1
P026
Chloroprene
1,3-Butadiene, 2-chloro-
126-99-8
3-Chloropropionitrile
Propanenitrile, 3-chloro-
542-76-7
P027
Chromium
Same
7440-47-3
Chromium compounds, N.O.S.
Chrysene
Same
218-01-9
U050
Citrus red No. 2
2-Naphthalenol, 1-[(2,5-
dimethoxyphenyl)azo]-
6358-53-8
Coal tar creosote
Same
8007-45-2
Copper cyanide
Copper cyanide CuCN
544-92-3
P029
Copper dimethyldithiocarbamate
Copper, bis(dimethylcarbamo-
dithioato-S,S')-,
137-29-1
Creosote
Same
U051
Cresols (Cresylic acid)
Phenol, methyl-
1319-77-3
U052
Crotonaldehyde
2-Butenal
4170-30-3
U053
m-Cumenyl methylcarbamate
Phenol, 3-(methylethyl)-,
methyl carbamate
64-00-6
P202
Cyanides (soluble salts and
complexes), N.O.S.
P030
Cyanogen
Ethanedinitrile
460-19-5
P031
Cyanogen bromide
Cyanogen bromide (CN)Br
506-68-3
U246
Cyanogen chloride
Cyanogen chloride (CN)Cl
506-77-4
P033
Cycasin
Beta
β
-D-glucopyranoside,
(methyl-ONN-azoxy)methyl-
14901-08-7
Cycloate
Carbamothioic acid, cyclo-
hexylethyl-, S-ethyl ester
1134-23-2
2-Cyclohexyl-4,6-dinitrophenol
Phenol, 2-cyclohexyl-4,6-
dinitro-
131-89-5
P034
Cyclophosphamide
2H-1,3,2-Oxazaphosphorin-2-
amine, N,N-bis(2-chloro-
ethyl)tetrahydro-, 2-oxide
50-18-0
U058
2,4-D
Acetic acid, (2,4-dichloro-
phenoxy)-
94-75-7
U240
2,4-D, salts and esters
Acetic acid, (2,4-
dichlorophenoxy)-, salts and
esters
U240
Daunomycin
5, 12-Naphthacenedione, 8-
acetyl-10-[(3-amino-2,3,6-
trideoxy-alpha
α
-L-lyxo-hexo-
pyranosyl)oxy]-7,8,9,10-
tetrahydro-6,8,11-trihydroxy-l-
20830-81-3
U059
117
methoxy-, 8S-cis)-
Dazomet
2H-1,3,5-thiadiazine-2-thione,
tetrahydro-3,5-dimethyl
533-74-4
DDD
Benzene, 1,1'-(2,2-dichloro-
ethylidene)bis[4-chloro-
72-54-8
U060
DDE
Benzene, 1,1'-(dichloroethenyl-
idene)bis[4-chloro-
72-55-9
DDT
Benzene, 1,1'-(2,2,2-trichloro-
ethylidene)bis[4-chloro-
50-29-3
U061
Diallate
Carbamothioic acid, bis(1-
methylethyl)-, S-(2,3-dichloro-
2-propenyl) ester
2303-16-4
U062
Dibenz[a,h]acridine
Same
226-36-8
Dibenz[a,j]acridine
Same
224-42-0
Dibenz[a,h]anthracene
Same
53-70-3
U063
7H-Dibenzo[c,g]carbazole
Same
194-59-2
Dibenzo[a,e]pyrene
Naphtho[1,2,3,4-def]chrysene
192-65-4
Dibenzo[a,h]pyrene
Dibenzo[b,def]chrysene
189-64-0
Dibenzo[a,i]pyrene
Benzo[rst]pentaphene
189-55-9
U064
1,2-Dibromo-3-chloropropane
Propane, 1,2-dibromo-3-chloro-
96-12-8
U066
Dibutyl phthalate
1,2-Benzenedicarboxylic acid,
dibutyl ester
84-74-2
U069
o-Dichlorobenzene
Benzene, 1,2-dichloro-
95-50-1
U070
m-Dichlorobenzene
Benzene, 1,3-dichloro-
541-73-1
U071
p-Dichlorobenzene
Benzene, 1,4-dichloro-
106-46-7
U072
Dichlorobenzene, N.O.S.
Benzene, dichloro-
25321-22-6
3,3'-Dichlorobenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dichloro-
91-94-1
U073
1,4-Dichloro-2-butene
2-Butene, 1,4-dichloro-
764-41-0
U074
Dichlorodifluoromethane
Methane, dichlorodifluoro-
75-71-8
U075
Dichloroethylene, N.O.S.
Dichloroethylene
25323-30-2
1,1-Dichloroethylene
Ethene, 1,1-dichloro-
75-35-4
U078
1,2-Dichloroethylene
Ethene, 1,2-dichloro-, (E)-
156-60-5
U079
Dichloroethyl ether
Ethane, 1,1'-oxybis[2-chloro-
111-44-4
U025
Dichloroisopropyl ether
Propane, 2,2'-oxybis[2-chloro-
108-60-1
U027
Dichloromethoxyethane
Ethane, 1,1'-[methylenebis-
(oxy)bis[2-chloro-
111-91-1
U024
Dichloromethyl ether
Methane, oxybis[chloro-
542-88-1
P016
2,4-Dichlorophenol
Phenol, 2,4-dichloro-
120-83-2
U081
2,6-Dichlorophenol
Phenol, 2,6-dichloro-
87-65-0
U082
Dichlorophenylarsine
Arsonous dichloride, phenyl-
696-28-6
P036
Dichloropropane, N.O.S.
Propane, dichloro-
26638-19-7
Dichloropropanol, N.O.S.
Propanol, dichloro-
26545-73-3
Dichloropropene, N.O.S.
1-Propene, dichloro-
26952-23-8
1,3-Dichloropropene
1-Propene, 1,3-dichloro-
542-75-6
U084
118
Dieldrin
2,7:3,6-Dimethanonaphth[2, 3-
b]oxirene,3,4,5,6,9,9-hexa-
chloro-1a,2,2a,3,6, 6a,7,7a-
octahydro-,
(1aalpha
α
,2beta
β
,2aalpha
α
,3be
ta
β
,6beta
β
,6aalpha
α
,7beta
β
,7aa
lpha
α
)-
60-57-1
P037
1,2:3,4-Diepoxybutane
2,2'-Bioxirane
1464-53-5
U085
Diethylarsine
Arsine, diethyl-
692-42-2
P038
Diethylene glycol, dicarbamate
Ethanol, 2,2'-oxybis-,
dicarbamate
5952-26-1
U395
1,4-Diethyleneoxide
1,4-Dioxane
123-91-1
U108
Diethylhexyl phthalate
1,2-Benzenedicarboxylic acid,
bis(2-ethylhexyl) ester
117-81-7
U028
N,N'-Diethylhydrazine
Hydrazine, 1,2-diethyl-
1615-80-1
U086
O,O-Diethyl-S-methyl dithio-
phosphate
Phosphorodithioic acid, O,O-
diethyl S-methyl ester
3288-58-2
U087
Diethyl-p-nitrophenyl phosphate
Phosphoric acid, diethyl 4-
nitrophenyl ester
311-45-5
P041
Diethyl phthalate
1,2-Benzenedicarboxylic acid,
diethyl ester
84-66-2
U088
O,O-Diethyl O-pyrazinyl
phosphorothioate
Phosphorothioic acid, O,O-
diethyl O-pyrazinyl ester
297-97-2
P040
Diethylstilbestrol
Phenol, 4,4'-(1,2-diethyl-1,2-
ethenediyl)bis-, (E)-
56-53-1
U089
Dihydrosafrole
1,3-Benzodioxole, 5-propyl-
94-58-6
U090
Diisopropylfluorophosphate (DFP)
Phosphorofluoridic acid, bis(1-
methylethyl) ester
55-91-4
P043
Dimethoate
Phosphorodithioic acid, O,O-
dimethyl S-[2-(methylamino)-2-
oxoethyl] ester
60-51-5
P044
Dimetilan
Carbamic acid, dimethyl-, 1-
[(dimethylamino) carbonyl]-5-
methyl-1H-pyrazol-3-yl ester
644-64-4
P191
3,3'-Dimethoxybenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dimethoxy-
119-90-4
U091
p-Dimethylaminoazobenzene
Benzenamine, N,N-dimethyl-4-
(phenylazo)-
60-11-7
U093
7,12-Dimethylbenz[a]anthracene
Benz[a]anthracene, 7,12-
dimethyl-
57-97-6
U094
3,3'-Dimethylbenzidine
[1,1'-Biphenyl]-4,4'-diamine,
3,3'-dimethyl-
119-93-7
U095
Dimethylcarbamoyl chloride
Carbamic chloride, dimethyl-
79-44-7
U097
1,1-Dimethylhydrazine
Hydrazine, 1,1-dimethyl-
57-14-7
U098
1,2-Dimethylhydrazine
Hydrazine, 1,2-dimethyl-
540-73-8
U099
119
alpha
α
,alpha
α
-Dimethylphen-
ethylamine
Benzeneethanamine, alpha
α
,
alpha
α
-dimethyl-
122-09-8
P046
2,4-Dimethylphenol
Phenol, 2,4-dimethyl-
105-67-9
U101
Dimethylphthalate
1,2-Benzenedicarboxylic acid,
dimethyl ester
131-11-3
U102
Dimethyl sulfate
Sulfuric acid, dimethyl ester
77-78-1
U103
Dinitrobenzene, N.O.S.
Benzene, dinitro-
25154-54-5
4,6-Dinitro-o-cresol
Phenol, 2-methyl-4,6-dinitro-
534-52-1
P047
4,6-Dinitro-o-cresol salts
P047
2,4-Dinitrophenol
Phenol, 2,4-dinitro-
51-28-5
P048
2,4-Dinitrotoluene
Benzene, 1-methyl-2,4-dinitro-
121-14-2
U105
2,6-Dinitrotoluene
Benzene, 2-methyl-1,3-dinitro-
606-20-2
U106
Dinoseb
Phenol, 2-(1-methylpropyl)-
4,6-dinitro-
88-85-7
P020
Di-n-octyl phthalate
1,2-Benzenedicarboxylic acid,
dioctyl ester
117-84-0
U107
Diphenylamine
Benzenamine, N-phenyl-
122-39-4
1,2-Diphenylhydrazine
Hydrazine, 1,2-diphenyl-
122-66-7
U109
Di-n-propylnitrosamine
1-Propanamine, N-nitroso-N-
propyl-
621-64-7
U111
Disulfiram
Thioperoxydicarbonic diamide,
tetraethyl
97-77-8
Disulfoton
Phosphorodithioic acid, O,O-
diethyl S-[2-(ethylthio)ethyl]
ester
298-04-4
P039
Dithiobiuret
Thioimidodicarbonic diamide
[(H
2
N)C(S)]
2
NH
541-53-7
P049
Endosulfan
6, 9-Methano-2,4,3-benzo-
dioxathiepen,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-oxide,
115-29-7
P050
Endothal
7-Oxabicyclo[2.2.1]heptane-
2,3-dicarboxylic acid
145-73-3
P088
Endrin
2,7:3,6-Dimethanonaphth[2,3-
b]oxirene, 3,4,5,6,9,9-hexa-
chloro-1a,2,2a,3,6,6a,7,7a-
octahydro-, (1a
alpha
α
,2beta
β
,2abeta
β
,3alpha
α
,6alpha
α
,6abeta
β
,7beta
β
,7aalph
a
α
)-,
72-20-8
P051
Endrin metabolites
P051
Epichlorohydrin
Oxirane, (chloromethyl)-
106-89-8
U041
Epinephrine
1,2-Benzenediol, 4-[1-hydroxy-
2-(methylamino)ethyl]-, (R)-
51-43-4
P042
EPTC
Carbamothioic acid, dipropyl-,
759-94-4
120
S-ethyl ester
Ethyl carbamate (urethane)
Carbamic acid, ethyl ester
51-79-6
U238
Ethyl cyanide
Propanenitrile
107-12-0
P101
Ethylenebisdithiocarbamic acid
Carbamodithioic acid, 1,2-
ethanediylbis-
111-54-6
U114
Ethylenebisdithiocarbamic acid,
salts and esters
U114
Ethylene dibromide
Ethane, 1,2-dibromo-
106-93-4
U067
Ethylene dichloride
Ethane, 1,2-dichloro-
107-06-2
Ethylene glycol monoethyl ether
Ethanol, 2-ethoxy-
110-80-5
U359
Ethyleneimine
Aziridine
151-56-4
P054
Ethylene oxide
Oxirane
75-21-8
U115
Ethylenethiourea
2-Imidazolidinethione
96-45-7
U116
Ethylidine dichloride
Ethane, 1,1-dichloro-
75-34-3
U076
Ethyl methacrylate
2-Propenoic acid, 2-methyl-,
ethyl ester
97-63-2
U118
Ethyl methanesulfonate
Methanesulfonic acid, ethyl
ester
62-50-0
U119
Ethyl Ziram
Zinc, bis(diethylcarbamo-
dithioato-S,S')-
14324-55-1
U407
Famphur
Phosphorothioc acid, O-[4-
[(dimethylamino)sulfonyl]-
phenyl] O,O-dimethyl ester
52-85-7
P097
Ferbam
Iron, tris(dimethylcarbamo-
dithioato-S,S')-,
14484-64-1
Fluoranthene
Same
206-44-0
U120
Fluorine
Same
7782-41-4
P056
Fluoroacetamide
Acetamide, 2-fluoro-
640-19-7
P057
Fluoroacetic acid, sodium salt
Acetic acid, fluoro-, sodium
salt
62-74-8
P058
Formaldehyde
Same
50-00-0
U122
Formetanate hydrochloride
Methanimidamide, N,N-
dimethyl-N'-[3-[[(methyl-
amino)carbonyl]oxy]phenyl]-,
monohydrochloride
23422-53-9
P198
Formic acid
Same
64-18-16
U123
Formparanate
Methanimidamide, N,N-
dimethyl-N'-[2-methyl-4-
[[(methylamino)carbonyl]oxy]-
phenyl]-
17702-57-7
P197
Glycidylaldehyde
Oxiranecarboxaldehyde
765-34-4
U126
Halomethanes, N.O.S.
Heptachlor
4,7-Methano-1H-
indene,1,4,5,6,7,8,8-
heptachloro-3a,4,7,7a-tetra-
76-44-8
P059
121
hydro-
Heptachlor epoxide
2,5-Methano-2H-indeno[1,
2b]oxirene, 2,3,4,5,6,7,7-
heptachloro-1a,1b,5,5a,6,6a-
hexahydro-,
(1aalpha
α
,1bbeta
β
,2alpha
α
,5al
pha
α
,5abeta
β
,6beta
β
,6aalpha
α
)
-
1024-57-3
Heptachlor epoxide (alpha
α
, beta
β
,
and gamma
γ
isomers)
Heptachlorodibenzofurans
Heptachlorodibenzo-p-dioxins
Hexachlorobenzene
Benzene, hexachloro-
118-74-1
U127
Hexachlorobutadiene
1,3-Butadiene, 1,1,2,3,4,4-
hexachloro-
87-68-3
U128
Hexachlorocyclo-pentadiene
1,3-Cyclopentadiene,
1,2,3,4,5,5-hexachloro-
77-47-4
U130
Hexachlorodibenzo-p-dioxins
Hexachlorodibenzofurans
Hexachloroethane
Ethane, hexachloro-
67-72-1
U131
Hexachlorophene
Phenol, 2,2'-methylene-
bis[3,4,6-trichloro-
70-30-4
U132
Hexachloropropene
1-Propene, 1,1,2,3,3,3-
hexachloro-
1888-71-7
U243
Hexaethyltetraphosphate
Tetraphosphoric acid, hexaethyl
ester
757-58-4
P062
Hydrazine
Same
302-01-2
U133
Hydrogen cyanide
Hydrocyanic acid
74-90-8
P063
Hydrogen fluoride
Hydrofluoric acid
7664-39-3
U134
Hydrogen sulfide
Hydrogen sulfide H2SH
2
S
7783-06-4
U135
Indeno[1,2,3-cd]pyrene
Same
193-39-5
U137
3-Iodo-2-propynyl-n-butylcarbamate
Carbamic acid, butyl-, 3-iodo-
2-propynyl ester
55406-53-6
Isobutyl alcohol
1-Propanol, 2-methyl-
78-83-1
U140
Isodrin
1,4:5,8-Dimethanonaph-
thalene,1,2,3,4,10,10-hexa-
chloro-1,4,4a,5,8,8a-
hexahydro-,
(1alpha
α
,4alpha
α
,4abeta
β
,5bet
a
β
,8beta
β
,8abeta
β
)-,
465-73-6
P060
Isolan
Carbamic acid, dimethyl-, 3-
methyl-1-(1-methylethyl)-1H-
pyrazol-5-yl ester
119-38-0
P192
Isosafrole
1,3-Benzodioxole, 5-(1-
propenyl)-
120-58-1
U141
122
Kepone
1,3,4-Metheno-2H-cyclobuta-
[cd]pentalen-2-one,
1,1a,3,3a,4,5,5,5a,5b,6-
decachlorooctahydro-,
143-50-0
U142
Lasiocarpine
2-Butenoic acid, 2-methyl-, 7-
[[2,3-dihydroxy-2-(1-
methoxyethyl)-3-methyl-1-
oxobutoxy]methyl]-2,3,5,7a-
tetrahydro-1H-pyrrolizin-l-yl
ester, [1S-[1-
alpha
α
(Z),7(2S*,3R*),7aalpha
α
]]-
303-34-1
U143
Lead
Same
7439-92-1
Lead and compounds, N.O.S.
Lead acetate
Acetic acid, lead (2+) salt
301-04-2
U144
Lead phosphate
Phosphoric acid, lead (2+) salt
(2:3)
7446-27-7
U145
Lead subacetate
Lead, bis(acetato-O)tetra-
hydroxytri-
1335-32-6
U146
Lindane
Cyclohexane, 1,2,3,4,5,6-hexa-
chloro-,
1alpha
α
,2alpha
α
,3beta
β
,4alpha
α
,5alpha
α
,6beta
β
)-
58-89-9
U129
Maleic anhydride
2,5-Furandione
108-31-6
U147
Maleic hydrazide
3,6-Pyridazinedione, 1,2-
dihydro-
123-33-1
U148
Malononitrile
Propanedinitrile
109-77-3
U149
Manganese dimethyldithiocarbamate
Manganese, bis(dimethyl-
carbamodithioato-S,S')-,
15339-36-3
P196
Melphalan
L-Phenylalanine, 4-[bis(2-
chloroethyl)amino]-
148-82-3
U150
Mercury
Same
7439-97-6
U151
Mercury compounds, N.O.S.
Mercury fulminate
Fulminic acid, mercury (2+)
salt
628-86-4
P065
Metam Sodium
Carbamodithioic acid, methyl-,
monosodium salt
137-42-8
Methacrylonitrile
2-Propenenitrile, 2-methyl-
126-98-7
U152
Methapyrilene
1,2-Ethanediamine, N,N-
dimethyl-N'-2-pyridinyl-N'-(2-
thienylmethyl)-
91-80-5
U155
Methiocarb
Phenol, (3,5-dimethyl-4-
(methylthio)-, methylcarbamate
2032-65-7
P199
Metholmyl
Ethanimidothioic acid, N-
[[(methylamino)carbonyl]oxy]-,
16752-77-5
P066
123
methyl ester
Methoxychlor
Benzene, 1,1'-(2,2,2-trichloro-
ethylidene)bis[4-methoxy-
72-43-5
U247
Methyl bromide
Methane, bromo-
74-83-9
U029
Methyl chloride
Methane, chloro-
74-87-3
U045
Methylchlorocarbonate
Carbonochloridic acid, methyl
ester
79-22-1
U156
Methyl chloroform
Ethane, 1,1,1-trichloro-
71-55-6
U226
3-Methylcholanthrene
Benz[j]aceanthrylene, 1,2-
dihydro-3-methyl-
56-49-5
U157
4,4'-Methylenebis(2-chloroaniline)
Benzenamine, 4,4'-methylene-
bis[2-chloro-
101-14-4
U158
Methylene bromide
Methane, dibromo-
74-95-3
U068
Methylene chloride
Methane, dichloro-
75-09-2
U080
Methyl ethyl ketone (MEK)
2-Butanone
78-93-3
U159
Methyl ethyl ketone peroxide
2-Butanone, peroxide
1338-23-4
U160
Methyl hydrazine
Hydrazine, methyl-
60-34-4
P068
Methyl iodide
Methane, iodo-
74-88-4
U138
Methyl isocyanate
Methane, isocyanato-
624-83-9
P064
2-Methyllactonitrile
Propanenitrile, 2-hydroxy-2-
methyl-
75-86-5
P069
Methyl methacrylate
2-Propenoic acid, 2-methyl-,
methyl ester
80-62-6
U162
Methyl methanesulfonate
Methanesulfonic acid, methyl
ester
66-27-3
Methyl parathion
Phosphorothioic acid, O,O-
dimethyl O-(4-nitrophenyl)
ester
298-00-0
P071
Methylthiouracil
4-(1H)-Pyrimidinone, 2,3-
dihydro-6-methyl-2-thioxo-
56-04-2
U164
Metolcarb
Carbamic acid, methyl-, 3-
methylphenyl ester
1129-41-5
P190
Mexacarbate
Phenol, 4-(dimethylamino)-3,5-
dimethyl-, methylcarbamate
(ester)
315-18-4
P128
Mitomycin C
Azirino[2', 3':3, 4]pyrrolo[1,
2-a]indole-4, 7-dione, 6-amino-
8-[[(aminocarbonyl)oxy]-
methyl]-1,1a,2,8,8a,8b-
hexahydro-8a-methoxy-5-
methyl-, [1a-S-
(1aalpha
α
,8beta
β
,8aalpha
α
,8ba
lpha
α
)]-,
50-07-7
U010
Molinate
1H-Azepine-1-carbothioic acid,
hexahydro-, S-ethyl ester
2212-67-1
124
MNNG
Guanidine, N-methyl-N'-nitro-
N-nitroso-
70-25-7
U163
Mustard gas
Ethane, 1,1'-thiobis[2-chloro-
505-60-2
U165
Naphthalene
Same
91-20-3
U165
1,4-Naphthoquinone
1,4-Naphthalenedione
130-15-4
U166
alpha
α
-Naphthylamine
1-Naphthalenamine
134-32-7
U167
beta
β
-Naphthylamine
2-Naphthalenamine
91-59-8
U168
alpha
α
-Naphthylthiourea
Thiourea, 1-naphthalenyl-
86-88-4
P072
Nickel
Same
7440-02-0
Nickel compounds, N.O.S.
Nickel carbonyl
Nickel carbonyl Ni(CO)
4
, (T-
4)-
13463-39-3
P073
Nickel cyanide
Nickel cyanide Ni(CN)
2
557-19-7
P074
Nicotine
Pyridine, 3-(1-methyl-2-
pyrrolidinyl)-, (S)-
54-11-5
P075
Nicotine salts
P075
Nitric oxide
Nitrogen oxide NO
10102-43-9
P076
p-Nitroaniline
Benzenamine, 4-nitro-
100-01-6
P077
Nitrobenzene
Benzene, nitro-
98-95-3
P078
Nitrogen dioxide
Nitrogen oxide NO
2
10102-44-0
P078
Nitrogen mustard
Ethanamine, 2-chloro-N-(2-
chloroethyl)-N-methyl-
51-75-2
Nitrogen mustard, hydrochloride
salt
Nitrogen mustard N-oxide
Ethanamine, 2-chloro-N-(2-
chloroethyl)-N-methyl-, N-
oxide
126-85-2
Nitrogen mustard, N-oxide,
hydrochloride salt
Nitroglycerin
1,2,3-Propanetriol, trinitrate
55-63-0
P081
p-Nitrophenol
Phenol, 4-nitro-
100-02-7
U170
2-Nitropropane
Propane, 2-nitro-
79-46-9
U171
Nitrosamines, N.O.S.
35576-91-1
N-Nitrosodi-n-butylamine
1-Butanamine, N-butyl-N-
nitroso-
924-16-3
U172
N-Nitrosodiethanolamine
Ethanol, 2,2'-(nitrosoimino)bis-
1116-54-7
U173
N-Nitrosodiethylamine
Ethanamine, N-ethyl-N-nitroso-
55-18-5
U174
N-Nitrosodimethylamine
Methanamine, N-methyl-N-
nitroso-
62-75-9
P082
N-Nitroso-N-ethylurea
Urea, N-ethyl-N-nitroso-
759-73-9
U176
N-Nitrosomethylethylamine
Ethanamine, N-methyl-N-
nitroso-
10595-95-6
N-Nitroso-N-methylurea
Urea, N-methyl-N-nitroso-
684-93-5
U177
N-Nitroso-N-methylurethane
Carbamic acid, methylnitroso-,
ethyl ester
615-53-2
U178
125
N-Nitrosomethylvinylamine
Vinylamine, N-methyl-N-
nitroso-
4549-40-0
P084
N-Nitrosomorpholine
Morpholine, 4-nitroso-
59-89-2
N-Nitrosonornicotine
Pyridine, 3-(1-nitroso-2-
pyrrolidinyl)-, (S)-
16543-55-8
N-Nitrosopiperidine
Piperidine, 1-nitroso-
100-75-4
U179
N-Nitrosopyrrolidine
Pyrrolidine, 1-nitroso-
930-55-2
U180
N-Nitrososarcosine
Glycine, N-methyl-N-nitroso-
13256-22-9
5-Nitro-o-toluidine
Benzenamine, 2-methyl-5-nitro-
99-55-8
U181
Octamethylpyrophosphoramide
Diphosphoramide, octamethyl-
152-16-9
P085
Osmium tetroxide
Osmium oxide OsO
4
, (T-4)
20816-12-0
P087
Oxamyl
Ethanimidothioc acid, 2-
(dimethylamino)-N-[[(methyl-
amino)carbonyl]oxy]-2-oxo-,
methyl ester
23135-22-0
P194
Paraldehyde
1,3,5-Trioxane, 2,4,6-tri-
methyl-
123-63-7
U182
Parathion
Phosphorothioic acid, O,O-
diethyl O-(4-nitrophenyl) ester
56-38-2
P089
Pebulate
Carbamothioic acid, butylethyl-
, S-propyl ester
1114-71-2
Pentachlorobenzene
Benzene, pentachloro-
608-93-5
U183
Pentachlorodibenzo-p-dioxins
Pentachlorodibenzofurans
Pentachloroethane
Ethane, pentachloro-
76-01-7
U184
Pentachloronitrobenzene (PCNB)
Benzene, pentachloronitro-
82-68-8
U185
Pentachlorophenol
Phenol, pentachloro-
87-86-5
See
F027
Phenacetin
Acetamide, N-(4-
ethoxyphenyl)-
62-44-2
U187
Phenol
Same
108-95-2
U188
Phenylenediamine
Benzenediamine
25265-76-3
Phenylmercury acetate
Mercury, (acetato-O)phenyl-
62-38-4
P092
Phenylthiourea
Thiourea, phenyl-
103-85-5
P093
Phosgene
Carbonic dichloride
75-44-5
P095
Phosphine
Same
7803-51-2
P096
Phorate
Phosphorodithioic acid, O,O-
diethyl S-[(ethylthio)methyl]
ester
298-02-2
P094
Phthalic acid esters, N.O.S.
Phthalic anhydride
1,3-Isobenzofurandione
85-44-9
U190
Physostigmine
Pyrrolo[2,3-b]indol-5-ol,
1,2,3,3a,8,8a-hexahydro-
1,3a,8-trimethyl-, methyl-
carbamate (ester), (3aS-cis)-
57-47-6
P204
126
Physostigmine salicylate
Benzoic acid, 2-hydroxy-,
compound with (3aS-cis)-
1,2,3,3a,8,8a-hexahydro-
1,3a,8-trimethylpyrrolo[2,3-b]-
indol-5-yl methylcarbamate
ester (1:1)
57-64-7
P188
2-Picoline
Pyridine, 2-methyl-
109-06-8
U191
Polychlorinated biphenyls, N.O.S.
Potassium cyanide
Same
151-50-8
P098
Potassium dimethyldithiocarbamate
Carbamodithioc acid, dimethyl,
potassium salt
128-03-0
Potassium n-hydroxymethyl-n-
methyl-dithiocarbamate
Carbamodithioc acid, (hydroxy-
methyl)methyl-, monopotassium
salt
51026-28-9
Potassium n-methyldithiocarbamate
Carbamodithioc acid, methyl-
monopotassium salt
137-41-7
Potassium silver cyanide
Argentate(1-), bis(cyano-C)-,
potassium)
506-61-6
P099
Potassium pentachlorophenate
Pentachlorophenol, potassium
salt
7778736
None
Promecarb
Phenol, 3-methyl-5-(1-methyl-
ethyl)-, methyl carbamate
2631-37-0
P201
Pronamide
Benzamide, 3,5-dichloro-N-
(1,1-dimethyl-2-propynyl)-
23950-58-5
U192
1,3-Propane sultone
1,2-Oxathiolane, 2,2-dioxide
1120-71-4
U193
Propham
Carbamic acid, phenyl-, 1-
methylethyl ester
122-42-9
U373
Propoxur
Phenol, 2-(1-methylethoxy)-,
methylcarbamate
114-26-1
U411
n-Propylamine
1-Propanamine
107-10-8
U194
Propargyl alcohol
2-Propyn-1-ol
107-19-7
P102
Propylene dichloride
Propane, 1,2-dichloro-
78-87-5
U083
1,2-Propylenimine
Aziridine, 2-methyl-
75-55-8
P067
Propylthiouracil
4(1H)-Pyrimidinone, 2,3-
dihydro-6-propyl-2-thioxo-
51-52-5
Prosulfocarb
Carbamothioic acid, dipropyl-,
S-(phenylmethyl) ester
52888-80-9
U387
Pyridine
Same
110-86-1
U196
Reserpine
Yohimban-16-carboxylic acid,
11,17-dimethoxy-18-[(3,4,5-tri-
methoxybenzoyl)oxy]-, methyl
ester,
(3beta
β
,16beta
β
,17alpha
α
,18be
ta
β
,20alpha
α
)-,
50-55-5
U200
Resorcinol
1,3-Benzenediol
108-46-3
U201
127
Saccharin
1,2-Benzisothiazol-3(2H)-one,
1,1-dioxide
81-07-2
U202
Saccharin salts
U202
Safrole
1,3-Benzodioxole, 5-(2-
propenyl)-
94-59-7
U203
Selenium
Same
7782-49-2
Selenium compounds, N.O.S.
Selenium dioxide
Selenious acid
7783-00-8
U204
Selenium sulfide
Selenium sulfide SeS
2
7488-56-4
U205
Selenium, tetrakis(dimethyl-
dithiocarbamate
Carbamodithioic acid,
dimethyl-, tetraanhydrosulfide
with orthothioselenious acid
144-34-3
Selenourea
Same
630-10-4
P103
Silver
Same
7440-22-4
Silver compounds, N.O.S.
Silver cyanide
Silver cyanide AgCN
506-64-9
P104
Silvex (2,4,5-TP)
Propanoic acid, 2-(2,4,5-
trichlorophenoxy)-
93-72-1
See
F027
Sodium cyanide
Sodium cyanide NaCN
143-33-9
P106
Sodium dibutyldithiocarbamate
Carbamodithioic acid, dibutyl-,
sodium salt
136-30-1
Sodium diethyldithiocarbamate
Carbamodithioic acid, diethyl-,
sodium salt
148-18-5
Sodium dimethyldithiocarbamate
Carbamodithioic acid,
dimethyl-, sodium salt
128-04-1
Sodium pentachlorophenate
Pentachlorophenol, sodium salt
131522
None
Streptozotocin
D-Glucose, 2-deoxy-2-
[[(methylnitrosoamino)ca-
rbonyl]amino]-
18883-66-4
U206
Strychnine
Strychnidin-10-one
57-24-9
P108
Strychnine salts
P108
Sulfallate
Carbamodithioic acid, diethyl-,
2-chloro-2-propenyl ester
95-06-7
TCDD
Dibenzo[b,e][1,4]dioxin,
2,3,7,8-tetrachloro-
1746-01-6
Tetrabutylthiuram disulfide
Thioperoxydicarbonic diamide,
tetrabutyl
1634-02-2
Tetramethylthiuram monosulfide
Bis(dimethylthiocarbamoyl)
sulfide
97-74-5
1,2,4,5-Tetrachlorobenzene
Benzene, 1,2,4,5-tetrachloro-
95-94-3
U207
Tetrachlorodibenzo-p-dioxins
Tetrachlorodibenzofurans
Tetrachloroethane, N.O.S.
Ethane, tetrachloro-, N.O.S.
25322-20-7
1,1,1,2-Tetrachloroethane
Ethane, 1,1,1,2-tetrachloro-
630-20-6
U208
1,1,2,2-Tetrachloroethane
Ethane, 1,1,2,2-tetrachloro-
79-34-5
U209
128
Tetrachloroethylene
Ethene, tetrachloro-
127-18-4
U210
2,3,4,6-Tetrachlorophenol
Phenol, 2,3,4,6-tetrachloro-
58-90-2
See
F027
2,3,4,6-Tetrachlorophenol,
potassium salt
Same
53535276
None
2,3,4,6-Tetrachlorophenol, sodium
salt
Same
25567559
None
Tetraethyldithiopyrophosphate
Thiodiphosphoric acid,
tetraethyl ester
3689-24-5
P109
Tetraethyl lead
Plumbane, tetraethyl-
78-00-2
P110
Tetraethylpyrophosphate
Diphosphoric acid, tetraethyl
ester
107-49-3
P111
Tetranitromethane
Methane, tetranitro-
509-14-8
P112
Thallium
Same
7440-28-0
Thallium compounds
Thallic oxide
Thallium oxide Tl
2
O
3
1314-32-5
P113
Thallium (I) acetate
Acetic acid, thallium (1+) salt
563-68-8
U214
Thallium (I) carbonate
Carbonic acid, dithallium (1+)
salt
6533-73-9
U215
Thallium (I) chloride
Thallium chloride TlCl
7791-12-0
U216
Thallium (I) nitrate
Nitric acid, thallium (1+) salt
10102-45-1
U217
Thallium selenite
Selenious acid, dithallium (1+)
salt
12039-52-0
P114
Thallium (I) sulfate
Sulfuric acid, dithallium (1+)
salt
7446-18-6
P115
Thioacetamide
Ethanethioamide
62-55-5
U218
Thiodicarb
Ethanimidothioic acid, N,N'-
[thiobis[(methylimino)-
carbonyloxy]]-bis-, dimethyl
ester
59669-26-0
U410
Thiofanox
2-Butanone, 3,3-dimethyl-1-
(methylthio)-, O-
[(methylamino)carbonyl]oxime
39196-18-4
P045
Thiophanate-methyl
Carbamic acid, [1,2-
phyenylenebis(iminocarbono-
thioyl)]-bis-, dimethyl ester
23564-05-8
U409
Thiomethanol
Methanethiol
74-93-1
U153
Thiophenol
Benzenethiol
108-98-5
P014
Thiosemicarbazide
Hydrazinecarbothioamide
79-19-6
P116
Thiourea
Same
62-56-6
P219
Thiram
Thioperoxydicarbonic diamide
[(H
2
N)C(S)]
2
S
2
, tetramethyl-
137-26-8
U244
Tirpate
1,3-Dithiolane-2-carbox-
aldehyde, 2,4-dimethyl-, O-
[(methylamino)carbonyl] oxime
26419-73-8
P185
129
Toluene
Benzene, methyl-
108-88-3
U220
Toluenediamine
Benzenediamine, ar-methyl-
25376-45-8
U221
Toluene-2,4-diamine
1,3-Benzenediamine, 4-methyl-
95-80-7
Toluene-2,6-diamine
1,3-Benzenediamine, 2-methyl-
823-40-5
Toluene-3,4-diamine
1,2-Benzenediamine, 4-methyl-
496-72-0
Toluene diisocyanate
Benzene, 1,3-diisocyanato-
methyl-
26471-62-5
U223
o-Toluidine
Benzenamine, 2-methyl-
95-53-4
U328
o-Toluidine hydrochloride
Benzeneamine, 2-methyl-,
hydrochloride
636-21-5
U222
p-Toluidine
Benzenamine, 4-methyl-
106-49-0
U353
Toxaphene
Same
8001-35-2
P123
Triallate
Carbamothioic acid, bis(1-
methylethyl)-, S-(2,3,3-tri-
chloro-2-propenyl) ester
2303-17-5
U389
1,2,4-Trichlorobenzene
Benzene, 1,2,4-trichloro-
120-82-1
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
79-00-5
U227
Trichloroethylene
Ethene, trichloro-
79-01-6
U228
Trichloromethanethiol
Methanethiol, trichloro-
75-70-7
P118
Trichloromonofluoromethane
Methane, trichlorofluoro-
75-69-4
U121
2,4,5-Trichlorophenol
Phenol, 2,4,5-trichloro-
95-95-4
See
F027
2,4,6-Trichlorophenol
Phenol, 2,4,6-trichloro-
88-06-2
See
F027
2,4,5-T
Acetic acid, (2,4,5-trichloro-
phenoxy)-
93-76-5
See
F027
Trichloropropane, N.O.S.
25735-29-9
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
96-18-4
Triethylamine
Ethanamine, N,N-diethyl-
121-44-8
U404
O,O,O-Triethylphosphorothioate
Phosphorothioic acid, O,O,O-
triethyl ester
126-68-1
1,3,5-Trinitrobenzene
Benzene, 1,3,5-trinitro-
99-35-4
U234
Tris(l-aziridinyl)phosphine sulfide
Aziridine, 1,1',1”-phosphino-
thioylidynetris-
52-24-4
Tris(2,3-dibromopropyl) phosphate
1-Propanol, 2,3-dibromo-,
phosphate (3:1)
126-72-7
U235
Trypan blue
2,7-Naphthalenedisulfonic acid,
3,3'-[(3,3'-dimethyl[1,1'-
biphenyl]-4,4'-diyl)-
bis(azo)]bis[5-amino-4-
hydroxy]-, tetrasodium salt
72-57-1
U236
Uracil mustard
2,4-(1H,3H)-Pyrimidinedione,
5-[bis(2-chloroethyl)amino]-
66-75-1
U237
Vanadium pentoxide
Vanadium oxide V
2
O
5
1314-62-1
P120
Vernolate
Carbamothioc acid, dipropyl-,
1929-77-7
130
S-propyl ester
Vinyl chloride
Ethene, chloro-
75-01-4
U043
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl-
butyl)-, when present at
concentrations less than 0.3%
percent
81-81-2
U248
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl-
butyl)-, when present at
concentrations greater than
0.3% percent
81-81-2
P001
Warfarin salts, when present at
concentrations less than 0.3%
percent
U248
Warfarin salts, when present at
concentrations greater than 0.3%
percent
P001
Zinc cyanide
Zinc cyanide Zn(CN)
2
557-21-1
P121
Zinc phosphide
Zinc phosphide P
2
Zn
3
, when
present at concentrations greater
than 10% percent
1314-84-7
P122
Zinc phosphide
Zinc phosphide P
2
Zn
3
, when
present at concentrations of
10% percent or less
1314-84-7
U249
Ziram
Zinc, bis(dimethylcarbamo-
dithioato-S,S')- (T-4)-
137-30-4
P205
Note: The abbreviation N.O.S. (not otherwise specified) signifies those members of the
general class not specifically listed by name in this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 721.Appendix Z
Table to Section 721.102
Table
*1
*2
*3
*4
Spent materials
Yes
Yes
Yes
Yes
Sludges (listed in Section 721.131
or 721.132)
Yes
Yes
Yes
Yes
131
Sludges exhibiting a characteristic
of hazardous waste
Yes
Yes
No
Yes
By-products (listed in Section
721.131 or 721.132)
Yes
Yes
Yes
Yes
By-products exhibiting a
characteristic of hazardous waste
Yes
Yes
No
Yes
Commercial chemical products
listed in Section 721.133
Yes
Yes
No
No
Scrap metal other than excluded
scrap metal (see Section
721.101(c)(9))
Yes
Yes
Yes
Yes
Yes - Defined as a solid waste
No - Not defined as a solid waste
*1 - Use constituting disposal (Section 721.102(c)(1))
*2 - Burning for energy recovery or use to produce a fuel (Section 721.102(c)(2))
*3 - Reclamation (Section 721.102(c)(3))
*4 - Speculative accumulation (Section 721.102(c)(4))
BOARD NOTE: Derived from Table 1 to 40 CFR 261.2(c)(4) (19947). The terms “spent
materials”, “sludges”, “by-products”, “scrap metal”, and “processed scrap metal” are defined
in Section 721.101.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 722
STANDARDS APPLICABLE TO GENERATORS OF HAZARDOUS WASTE
SUBPART A: GENERAL
Section
722.110
Purpose, Scope and Applicability
722.111
Hazardous Waste Determination
722.112
USEPA Identification Numbers
132
SUBPART B: THE MANIFEST
Section
722.120
General Requirements
722.121
Acquisition of Manifests
722.122
Number of Copies
722.123
Use of the Manifest
SUBPART C: PRE-TRANSPORT REQUIREMENTS
Section
722.130
Packaging
722.131
Labeling
722.132
Marking
722.133
Placarding
722.134
Accumulation Time
SUBPART D: RECORDKEEPING AND REPORTING
Section
722.140
Recordkeeping
722.141
Annual Reporting
722.142
Exception Reporting
722.143
Additional Reporting
722.144
Special Requirements for Generators of between 100 and 1000 kilograms per
month
SUBPART E: EXPORTS OF HAZARDOUS WASTE
Section
722.150
Applicability
722.151
Definitions
722.152
General Requirements
722.153
Notification of Intent to Export
722.154
Special Manifest Requirements
722.155
Exception Report
722.156
Annual Reports
722.157
Recordkeeping
722.158
International Agreements
SUBPART F: IMPORTS OF HAZARDOUS WASTE
Section
722.160
Imports of Hazardous Waste
SUBPART G: FARMERS
Section
722.170
Farmers
133
SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
FOR RECOVERY WITHIN THE OECD
Section
722.180
Applicability
722.181
Definitions
722.182
General Conditions
722.183
Notification and Consent
722.184
Tracking Document
722.185
Contracts
722.186
Provisions Relating to Recognized Traders
722.187
Reporting and Recordkeeping
722.189
OECD Waste Lists
722.Appendix A
Hazardous Waste Manifest
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982;
amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982;
amended in R82-18, 51 PCB 31, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in
R84-9 at 9 Ill. Reg. 11950, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1131,
effective January 2, 1986; amended in R86-1 at 10 Ill. Reg. 14112, effective August 12, 1986;
amended in R86-19 at 10 Ill. Reg. 20709, effective December 2, 1986; amended in R86-46 at
11 Ill. Reg. 13555, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19392,
effective November 12, 1987; amended in R87-39 at 12 Ill. Reg. 13129, effective July 29,
1988; amended in R88-16 at 13 Ill. Reg. 452, effective December 27, 1988; amended in R89-
1 at 13 Ill. Reg. 18523, effective November 13, 1989; amended in R90-10 at 14 Ill. Reg.
16653, effective September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9644, effective June
17, 1991; amended in R91-1 at 15 Ill. Reg. 14562, effective October 1, 1991; amended in
R91-13 at 16 Ill. Reg. 9833, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17696,
effective November 6, 1992; amended in R93-4 at 17 Ill. Reg. 20822, effective November 22,
1993; amended in R95-6 at 19 Ill. Reg. 9935, effective June 27, 1995; amended in R95-20 at
20 Ill. Reg. 11236, effective August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg.
603, effective December 16, 1997; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg.
________, effective ______________________.
SUBPART A: GENERAL
Section 722.110
Purpose, Scope and Applicability
a)
These regulations establish standards for generators of hazardous waste.
134
b)
35 Ill. Adm. Code 721.105(c) and (d) must be used to determine the
applicability of provisions of this Part that are dependent on calculations of the
quantity of hazardous waste generated per month.
c)
A generator that treats, stores or disposes of hazardous waste on-site must only
comply with the following Sections of this Part with respect to that waste:
Section 722.111 for determining whether or not the generator has a hazardous
waste, Section 722.112 for obtaining an USEPA identification number, Section
722.140(c) and (d) for recordkeeping, Section 722.143 for additional reporting
and, if applicable, Section 722.170 for farmers.
d)
Any person that exports or imports hazardous waste subject to the hazardous
waste manifesting requirements of this Part or subject to the universal waste
management standards of 35 Ill. Adm. Code 733 to or from countries listed in
Section 722.158(a)(1) for recovery must comply with Subpart H of this Part.
e) This subsection corresponds with 40 CFR 262.10(e), a federal provision
imposing the generator standards on a person importing hazardous waste into
the United States. The regulation of international trade is a matter within the
exclusive authority of the federal government. This statement maintains
structural consistency with USEPA rules.
ef)
A farmer that generates waste pesticides which are hazardous waste and that
complies with all of the requirements of Section 722.151722.170 is not required
to comply with other standards in this Part, or 35 Ill. Adm. Code 702, 703, 724
725 or 728 with respect to such pesticides.
fg)
A person that generates a hazardous waste as defined by 35 Ill. Adm. Code 721
is subject to the compliance requirements and penalties prescribed in Title VIII
and XII of the Environmental Protection Act if he does not comply with the
requirements of this Part.
gh)
An owner or operator that initiates a shipment of hazardous waste from a
treatment, storage or disposal facility must comply with the generator standards
established in this Part.
i) A person responding to an explosives or munitions emergency in accordance
with 35 Ill. Adm. Code 724.101(g)(8)(A)(iv) or (g)(8)(D) or 35 Ill. Adm. Code
725.101(c)(11)(A)(iv) or (c)(11)(D) and 35 Ill. Adm. Code 703.121(a)(4) or (c)
is not required to comply with the standards of this Part.
BOARD NOTE: The provisions of Section 722.134 are applicable to the on-
site accumulation of hazardous waste by generators. Therefore, the provisions
of Section 722.134 only apply to owners or operators that are shipping
hazardous waste which they generated at that facility. A generator that treats,
135
stores or disposes of hazardous waste on-site must comply with the applicable
standards and permit requirements set forth in 35 Ill. Adm. Code 702, 703,
724, 725, 726 and 728.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART B: THE MANIFEST
Section 722.120
General Requirements
a)
A generator who transports, or offers for transportation, hazardous waste for
off-site treatment, storage or disposal must prepare a manifest before
transporting the waste off-site.
b)
A generator must designate on the manifest one facility which is permitted to
handle the waste described on the manifest.
c)
A generator may also designate on the manifest one alternate facility which is
permitted to handle his waste in the event an emergency prevents delivery of the
waste to the primary designated facility.
d)
If the transporter is unable to deliver the hazardous waste to the designated
facility or the alternate facility, the generator must either designate another
facility or instruct the transporter to return the waste.
e)
The requirements of this Subpart do not apply to hazardous waste produced by
generators of greater than 100 kg but less than 1000 kg in a calendar month
where:
1)
The waste is reclaimed under a contractual agreement pursuant to which:
A)
The type of waste and frequency of shipments are specified in the
agreement:
B)
The vehicle used to transport the waste to the recycling facility
and to deliver regenerated material back to the generator is
owned and operated by the reclaimer of the waste; and
2)
The generator maintains a copy of the reclamation agreement in his files
for a period of at least three years after termination or expiration of the
agreement.
f) The requirements of this Subpart B and Section 722.132(b) do not apply to the
transport of hazardous wastes on a public or private right-of-way within or
along the border of contiguous property under the control of the same person,
136
even if such contiguous property is divided by a public or private right-of-way.
Notwithstanding 35 Ill. Adm. Code 723.110(a), the generator or transporter
shall comply with the requirements for transporters set forth in 35 Ill. Adm.
Code 723.130 and 723.131 in the event of a discharge of hazardous waste on a
public or private right-of-way.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: EXPORTS OF HAZARDOUS WASTE
Section 722.158
International Agreements
a)
Any person that exports or imports hazardous waste subject to either the
manifest requirements of this Part or the universal waste management standards
of 35 Ill. Adm. Code 733 which is shipped to or from designated member
countries of the Organization for Economic Cooperation and Development
(OECD), as defined in subsection (a)(1) of this Section, for purposes of
recovery is subject to the requirements of 722.Subpart H of this Part. The
requirements of Subparts E and F of this Part do not apply where 722.Subpart
H of this Part applies.
1)
For the purposes of this Subpart, the designated OECD countries are
Australia, Austria, Belgium, Denmark, Finland, France, Germany,
Greece, Iceland, Ireland, Italy, Japan, Luxembourg, Netherlands, New
Zealand, Norway, Portugal, Spain, Sweden, Switzerland, Turkey, the
United Kingdom, and the United States.
2)
Only for the purposes of transit under this Subpart, Canada and Mexico
are considered OECD member countries.
b)
Any person that exports hazardous waste to or imports hazardous waste from
any designated OECD member country for purposes other than recovery (e.g.,
incineration, disposal), Mexico (for any purpose), or Canada (for any purpose)
remains subject to the requirements of Subparts E and F of this Part.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
137
SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
FOR RECOVERY WITHIN THE OECD
Section 722.180
Applicability
a)
The requirements of this Subpart apply to imports and exports of wastes that are
considered hazardous under U.S. national procedures and which are destined for
recovery operations in any of the countries listed in Section 722.158(a)(1). A
waste is considered hazardous under U.S. national procedures if it meets the
definition of hazardous waste in 35 Ill. Adm. Code 721.103 and it is subject to
either the manifesting requirements in Subpart B of this Part, or to the universal
waste management standards of 35 Ill. Adm. Code 733.
b)
Any person (notifier, consignee, or recovery facility operator) that mixes two or
more wastes (including hazardous and non-hazardous wastes) or otherwise
subjects two or more wastes (including hazardous and non-hazardous wastes) to
physical or chemical transformation operations, and thereby creates a new
hazardous waste, becomes a generator and assumes all subsequent generator
duties under this Subchapter and any notifier duties under this Subpart, as
applicable.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 722.184
Tracking Document
a)
All U.S. parties subject to the contract provisions of Section 722.185 must
ensure that a tracking document meeting the conditions of subsection (b) of this
Section accompanies each transfrontier shipment of wastes subject to amber-list
or red-list controls from the initiation of the shipment until it reaches the final
recovery facility, including cases in which the waste is stored or exchanged by
the consignee prior to shipment to the final recovery facility, except as provided
in Section 262.184 this subsection (a)(1) and (a)(2).
1)
For shipments of hazardous waste within the U.S. solely by water (bulk
shipments only), the generator must forward the tracking document with
the manifest to the last water (bulk shipment) transporter to handle the
waste in the U.S. if exported by water (in accordance with the manifest
routing procedures at Section 722.123(c)).
2)
For rail shipments of hazardous waste within the U.S. which originate at
the site of generation, the generator must forward the tracking document
with the manifest (in accordance with the routing procedures for the
manifest in Section 722.123(d)) to the next non-rail transporter, if any,
or the last rail transporter to handle the waste in the U.S. if exported by
rail.
138
b)
The tracking document must include all information required under Section
722.183 (for notification) and the following:
1)
The date shipment commenced;
2)
The name (if not notifier), address, and telephone and telefax numbers
of primary exporter;
3)
The company name and USEPA identification number of all
transporters;
4)
Identification (license, registered name or registration number) of means
of transport, including types of packaging;
5)
Any special precautions to be taken by transporters;
6)
A certification or declaration signed by notifier that no objection to the
shipment has been lodged as follows:
“I certify that the above information is complete and correct to the best
of my knowledge. I also certify that legally-enforceable written
contractual obligations have been entered into, that any applicable
insurance or other financial guarantees are or shall be in force covering
the transfrontier movement, and that:”
“1. All necessary consents have been received;” OR
“2. The shipment is directed at a recovery facility within the OECD area
and no objection has been received from any of the concerned countries
within the 30 day tacit consent period;” OR
“3. The shipment is directed at a recovery facility pre-authorized for that
type of waste within the OECD area, such an authorization has not been
revoked, and no objection has been received from any of the concerned
countries.”
(delete sentences that are not applicable)
“Name: _____________________________________
Signature: __________________________________
Date: _____________________________________”; and
139
7)
The appropriate signatures for each custody transfer (e.g., transporter,
consignee, and owner or operator of the recovery facility).
c)
Notifiers also must comply with the special manifest requirements of Section
722.154(a), (b), (c), (e), and (i) and consignees must comply with the import
requirements of Subpart F of this Part.
d)
Each U.S. person that has physical custody of the waste from the time the
movement commences until it arrives at the recovery facility must sign the
tracking document (e.g., transporter, consignee, and owner or operator of the
recovery facility).
e)
Within three working days of the receipt of imports subject to this Subpart, the
owner or operator of the U.S. recovery facility must send signed copies of the
tracking document to the notifier, to the Office of Enforcement and Compliance
Assurance, Office of Compliance, Enforcement Planning, Targeting and Data
Division (2222A), Environmental Protection Agency, 401 M St., SW.,
Washington, DC 20460, and to the competent authorities of the exporting and
transit countries.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 722.187
Reporting and Recordkeeping
a)
Annual reports. For all waste movements subject to this Subpart, persons (e.g.,
notifiers, recognized traders) that meet the definition of primary exporter in
Section 722.151 shall file an annual report with the Office of Enforcement and
Compliance Assurance, Office of Compliance, Enforcement Planning,
Targeting and Data Division (2222A), U.S. Environmental Protection Agency,
401 M St., SW., Washington, DC 20460 and the Illinois Environmental
Protection Agency, Bureau of Land, Division of Land Pollution Control, P.O.
Box 19276, Springfield, IL 62706-927662794, no later than March 1 of each
year summarizing the types, quantities, frequency, and ultimate destination of
all such hazardous waste exported during the previous calendar year. (If the
primary exporter is required to file an annual report for waste exports that are
not covered under this Subpart, the person filing may include all export
information in one report provided the following information on exports of
waste destined for recovery within the designated OECD member countries is
contained in a separate Section). Such reports shall include the following
information:
1)
The USEPA identification number, name, and mailing and site address
of the notifier filing the report;
2)
The calendar year covered by the report;
140
3)
The name and site address of each final recovery facility;
4)
By final recovery facility, for each hazardous waste exported, a
description of the hazardous waste, the USEPA hazardous waste number
(from 35 Ill. Adm. Code 721.Subpart C or 721.Subpart D), the
designation of waste type(s) from the OECD waste list and applicable
waste code from the OECD lists, DOT hazard class, the name and
USEPA identification number (where applicable) for each transporter
used, the total amount of hazardous waste shipped pursuant to this
Subpart, and number of shipments pursuant to each notification;
5)
In even numbered years, for each hazardous waste exported, except for
hazardous waste produced by exporters of greater than 100 kilograms
(kg) but less than 1000 kg in a calendar month, and except for hazardous
waste for which information was already provided pursuant to Section
722.141:
A)
A description of the efforts undertaken during the year to reduce
the volume and toxicity of waste generated; and
B)
A description of the changes in volume and toxicity of the waste
actually achieved during the year in comparison to previous years
to the extent such information is available for years prior to
1984; and
6)
A certification signed by the person acting as primary exporter that states
as follows:
“I certify under penalty of law that I have personally examined and am
familiar with the information submitted in this and all attached
documents, and that based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that the
submitted information is true, accurate, and complete. I am aware that
there are significant penalties for submitting false information including
the possibility of fine and imprisonment.”
b)
Exception reports. Any person that meets the definition of primary exporter in
Section 722.151 shall file with USEPA and the Agency an exception report in
lieu of the requirements of Section 722.142 if any of the following occurs:
1)
The person has not received a copy of the tracking documentation signed
by the transporter stating point of departure of the waste from the United
States within 45 days from the date it was accepted by the initial
transporter;
141
2)
Within 90 days from the date the waste was accepted by the initial
transporter, the notifier has not received written confirmation from the
recovery facility that the hazardous waste was received; or
3)
The waste is returned to the United States.
c)
Recordkeeping.
1)
Persons that meet the definition of primary exporter in Section 722.151
shall keep the following records:
A)
A copy of each notification of intent to export and all written
consents obtained from the competent authorities of concerned
countries, for a period of at least three years from the date the
hazardous waste was accepted by the initial transporter;
B)
A copy of each annual report, for a period of at least three years
from the due date of the report; and
C)
A copy of any exception reports and a copy of each confirmation
of delivery (i.e., tracking documentation) sent by the recovery
facility to the notifier, for at least three years from the date the
hazardous waste was accepted by the initial transporter or
received by the recovery facility, whichever is applicable.
2)
The periods of retention referred to in this Section are extended
automatically during the course of any unresolved enforcement action
regarding the regulated activity or as requested by USEPA or the
Agency.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 722.Appendix A
Hazardous Waste Manifest
The Board incorporates by reference 40 CFR 262, Appendix (198897), as amended at 53 Fed.
Reg. 45090, November 8, 1988. This Part incorporates no later amendments or editions. The
Agency shall prepare manifest forms based on 40 CFR 262, Appendix, with such changes as are
necessary under Illinois law.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
142
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 723
STANDARDS APPLICABLE TO TRANSPORTERS OF HAZARDOUS
WASTE
SUBPART A: GENERAL
Section
723.110
Scope
723.111
USEPA Identification Number
723.112
Transfer Facility Requirements
SUBPART B: COMPLIANCE WITH THE MANIFEST SYSTEM AND
RECORDKEEPING
Section
723.120
The Manifest System
723.121
Compliance with the Manifest
723.122
Recordkeeping
SUBPART C: HAZARDOUS WASTE DISCHARGES
Section
723.130
Immediate Action
723.131
Discharge Clean Up
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982;
amended and codified in R81-22, 45 PCB 17, at 6 Ill. Reg. 4828, effective May 17, 1982;
amended in R84-9, at 9 Ill. Reg. 11961, effective July 24, 1985; amended in R86-19, at 10
Ill. Reg. 20718, effective December 2, 1986; amended in R86-46 at 11 Ill. Reg. 13570,
effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19412, effective November 12,
1987; amended in R95-6 at 19 Ill. Reg. 9945, effective June 27, 1995; amended in R96-
10/R97-3/R97-5 at 22 Ill. Reg. 589, effective December 16, 1997; amended in R97-21/R98-
3/R98-5 at 22 Ill. Reg. ________, effective ______________________.
143
SUBPART A: GENERAL
Section 723.110
Scope
a)
These regulations establish standards which apply to persons transporting
hazardous waste into, out of or through Illinois if the transportation requires a
manifest under 35 Ill. Adm. Code 722.
b)
These regulations do not apply to on-site transportation of hazardous waste by
generators or by owners or operators of permitted hazardous waste management
facilities.
c)
A transporter of hazardous waste must also comply with 35 Ill. Adm. Code
722, “Standards Applicable to Generators of Hazardous Waste”, if he:
1)
Transports hazardous waste into the United States from abroad; or
2)
Mixes hazardous waste of different DOT shipping descriptions by
placing them into a single container.
BOARD NOTE: Transporters that store hazardous waste are required to
comply with the storage standards in 35 Ill. Adm. Code 724 and 725 and
the permit requirements of 40 CFR 122.
d)
A transporter of hazardous waste subject to the manifesting requirements of 35
Ill. Adm. Code 722 or the waste management standards of 35 Ill. Adm. Code
733 that is being imported from or exported to any of the countries listed in 35
Ill. Adm. Code 722.158(a)(1) for purposes of recovery is subject to this Subpart
and to all other relevant requirements of 35 Ill. Adm. Code 722.Subpart H,
including, but not limited to, 35 Ill. Adm. Code 722.184 for tracking
documents.
e) The regulations in this Part do not apply to transportation during an explosives
or munitions emergency response, conducted in accordance with 35 Ill. Adm.
Code 724.101(g)(8)(A)(iv) or (g)(8)(D) or 35 Ill. Adm. Code
725.101(c)(11)(A)(iv) or (c)(11)(D), and 35 Ill. Adm. Code 703.121(a)(4) or
(c).
f) 35 Ill. Adm. Code 726.303 identifies how the requirements of this Part apply to
military munitions classified as solid waste under 35 Ill. Adm. Code 726.302.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
144
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 724
STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS
WASTE TREATMENT, STORAGE, AND DISPOSAL FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
724.101
Purpose, Scope and Applicability
724.103
Relationship to Interim Status Standards
SUBPART B: GENERAL FACILITY STANDARDS
Section
724.110
Applicability
724.111
Identification Number
724.112
Required Notices
724.113
General Waste Analysis
724.114
Security
724.115
General Inspection Requirements
724.116
Personnel Training
724.117
General Requirements for Ignitable, Reactive or Incompatible Wastes
724.118
Location Standards
724.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
724.130
Applicability
724.131
Design and Operation of Facility
724.132
Required Equipment
724.133
Testing and Maintenance of Equipment
724.134
Access to Communications or Alarm System
724.135
Required Aisle Space
724.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
724.150
Applicability
724.151
Purpose and Implementation of Contingency Plan
724.152
Content of Contingency Plan
724.153
Copies of Contingency Plan
724.154
Amendment of Contingency Plan
724.155
Emergency Coordinator
724.156
Emergency Procedures
145
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND
REPORTING
Section
724.170
Applicability
724.171
Use of Manifest System
724.172
Manifest Discrepancies
724.173
Operating Record
724.174
Availability, Retention and Disposition of Records
724.175
Annual Report
724.176
Unmanifested Waste Report
724.177
Additional Reports
SUBPART F: RELEASES FROM SOLID WASTE MANAGEMENT UNITS
Section
724.190
Applicability
724.191
Required Programs
724.192
Groundwater Protection Standard
724.193
Hazardous Constituents
724.194
Concentration Limits
724.195
Point of Compliance
724.196
Compliance Period
724.197
General Groundwater Monitoring Requirements
724.198
Detection Monitoring Program
724.199
Compliance Monitoring Program
724.200
Corrective Action Program
724.201
Corrective Action for Solid Waste Management Units
SUBPART G: CLOSURE AND POST-CLOSURE
Section
724.210
Applicability
724.211
Closure Performance Standard
724.212
Closure Plan; Amendment of Plan
724.213
Closure; Time Allowed For Closure
724.214
Disposal or Decontamination of Equipment, Structures and Soils
724.215
Certification of Closure
724.216
Survey Plat
724.217
Post-closure Care and Use of Property
724.218
Post-closure Plan; Amendment of Plan
724.219
Post-closure Notices
724.220
Certification of Completion of Post-closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
724.240
Applicability
146
724.241
Definitions of Terms As Used In This Subpart
724.242
Cost Estimate for Closure
724.243
Financial Assurance for Closure
724.244
Cost Estimate for Post-closure Care
724.245
Financial Assurance for Post-closure Care
724.246
Use of a Mechanism for Financial Assurance of Both Closure and Post-closure
Care
724.247
Liability Requirements
724.248
Incapacity of Owners or Operators, Guarantors or Financial Institutions
724.251
Wording of the Instruments
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
724.270
Applicability
724.271
Condition of Containers
724.272
Compatibility of Waste With Container
724.273
Management of Containers
724.274
Inspections
724.275
Containment
724.276
Special Requirements for Ignitable or Reactive Waste
724.277
Special Requirements for Incompatible Wastes
724.278
Closure
724.279
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
724.290
Applicability
724.291
Assessment of Existing Tank System’s Integrity
724.292
Design and Installation of New Tank Systems or Components
724.293
Containment and Detection of Releases
724.294
General Operating Requirements
724.295
Inspections
724.296
Response to Leaks or Spills and Disposition of Leaking or unfit-for-use Tank
Systems
724.297
Closure and Post-Closure Care
724.298
Special Requirements for Ignitable or Reactive Waste
724.299
Special Requirements for Incompatible Wastes
724.300
Air Emission Standards
SUBPART K: SURFACE IMPOUNDMENTS
Section
724.320
Applicability
724.321
Design and Operating Requirements
724.322
Action Leakage Rate
724.323
Response Actions
147
724.326
Monitoring and Inspection
724.327
Emergency Repairs; Contingency Plans
724.328
Closure and Post-closure Care
724.329
Special Requirements for Ignitable or Reactive Waste
724.330
Special Requirements for Incompatible Wastes
724.331
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
724.332
Air Emission Standards
SUBPART L: WASTE PILES
Section
724.350
Applicability
724.351
Design and Operating Requirements
724.352
Action Leakage Rate
724.353
Response Action Plan
724.354
Monitoring and Inspection
724.356
Special Requirements for Ignitable or Reactive Waste
724.357
Special Requirements for Incompatible Wastes
724.358
Closure and Post-closure Care
724.359
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
SUBPART M: LAND TREATMENT
Section
724.370
Applicability
724.371
Treatment Program
724.372
Treatment Demonstration
724.373
Design and Operating Requirements
724.376
Food-chain Crops
724.378
Unsaturated Zone Monitoring
724.379
Recordkeeping
724.380
Closure and Post-closure Care
724.381
Special Requirements for Ignitable or Reactive Waste
724.382
Special Requirements for Incompatible Wastes
724.383
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
SUBPART N: LANDFILLS
Section
724.400
Applicability
724.401
Design and Operating Requirements
724.402
Action Leakage Rate
724.403
Monitoring and Inspection
724.404
Response Actions
724.409
Surveying and Recordkeeping
148
724.410
Closure and Post-closure Care
724.412
Special Requirements for Ignitable or Reactive Waste
724.413
Special Requirements for Incompatible Wastes
724.414
Special Requirements for Bulk and Containerized Liquids
724.415
Special Requirements for Containers
724.416
Disposal of Small Containers of Hazardous Waste in Overpacked Drums (Lab
Packs)
724.417
Special Requirements for Hazardous Wastes F020, F021, F022, F023, F026
and F027
SUBPART O: INCINERATORS
Section
724.440
Applicability
724.441
Waste Analysis
724.442
Principal Organic Hazardous Constituents (POHCs)
724.443
Performance Standards
724.444
Hazardous Waste Incinerator Permits
724.445
Operating Requirements
724.447
Monitoring and Inspections
724.451
Closure
SUBPART S: CORRECTIVE ACTION FOR SOLID WASTE
MANAGEMENT UNITS
Section
724.652
Corrective Action Management Units
724.653
Temporary Units
SUBPART W: DRIP PADS
Section
724.670
Applicability
724.671
Assessment of existing drip pad integrity
724.672
Design and installation of new drip pads
724.673
Design and operating requirements
724.674
Inspections
724.675
Closure
SUBPART X: MISCELLANEOUS UNITS
Section
724.700
Applicability
724.701
Environmental Performance Standards
724.702
Monitoring, Analysis, Inspection, Response, Reporting and Corrective Action
724.703
Post-closure Care
149
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
724.930
Applicability
724.931
Definitions
724.932
Standards: Process Vents
724.933
Standards: Closed-ventVent Systems and Control Devices
724.934
Test methods Methods and procedures Procedures
724.935
Recordkeeping requirements
724.936
Reporting Requirements
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
724.950
Applicability
724.951
Definitions
724.952
Standards: Pumps in Light Liquid Service
724.953
Standards: Compressors
724.954
Standards: Pressure Relief Devices in Gas/Vapor Service
724.955
Standards: Sampling Connecting Systems
724.956
Standards: Open-ended Valves or Lines
724.957
Standards: Valves in Gas/Vapor or Light Liquid Service
724.958
Standards: Pumps, Valves, Pressure Relief Devices and Other Connectors
724.959
Standards: Delay of Repair
724.960
Standards: Closed-vent Systems and Control Devices
724.961
Alternative Percentage Standard for Valves
724.962
Skip Period Alternative for Valves
724.963
Test Methods and Procedures
724.964
Recordkeeping Requirements
724.965
Reporting Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section
724.980
Applicability
724.981
Definitions
724.982
Standards: General
724.983
Waste Determination Procedures
724.984
Standards: Tanks
724.985
Standards: Surface Impoundments
724.986
Standards: Containers
724.987
Standards: Closed-vent Systems and Control Devices
724.988
Inspection and Monitoring Requirements
724.989
Recordkeeping Requirements
724.990
Reporting Requirements
724.991
Alternative Control Requirements for Tanks
150
SUBPART DD: CONTAINMENT BUILDINGS
Section
724.1100
Applicability
724.1101
Design and operating standards
724.1102
Closure and Post-closure Care
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section
724.1200 Applicability
724.1201 Design and Operating Standards
724.1202 Closure and Post-Closure Care
724.Appendix A
Recordkeeping Instructions
724.Appendix B
EPA Report Form and Instructions (Repealed)
724.Appendix D
Cochran’s Approximation to the Behrens-Fisher Student’s T-Test
724.Appendix E
Examples of Potentially Incompatible Waste
724.Appendix I
Groundwater Monitoring List
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14059, effective October 12, 1983; amended in R84-9
at 9 Ill. Reg. 11964, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1136, effective January 2, 1986;
amended in R86-1 at 10 Ill. Reg. 14119, effective August 12, 1986; amended in R86-28 at 11 Ill. Reg. 6138,
effective March 24, 1987; amended in R86-28 at 11 Ill. Reg. 8684, effective April 21, 1987; amended in R86-46
at 11 Ill. Reg. 13577, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19397, effective November 12,
1987; amended in R87-39 at 12 Ill. Reg. 13135, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 458,
effective December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18527, effective November 13, 1989; amended in
R90-2 at 14 Ill. Reg. 14511, effective August 22, 1990; amended in R90-10 at 14 Ill. Reg. 16658, effective
September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9654, effective June 17, 1991; amended in R91-1 at 15
Ill. Reg. 14572, effective October 1, 1991; amended in R91-13 at 16 Ill. Reg. 9833, effective June 9, 1992;
amended in R92-1 at 16 Ill. Reg. 17702, effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5806,
effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20830, effective November 22, 1993; amended in
R93-16 at 18 Ill. Reg. 6973, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg. 12487, effective July 29,
1994; amended in R94-17 at 18 Ill. Reg. 17601, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg.
9951, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11244, August 1, 1996; amended in R96-
10/R97-3/R97-5 at 22 Ill. Reg. 636, effective December 16, 1997; amended in R98-12 at 22 Ill. Reg. 7638,
effective April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg. ________, effective
______________________.
SUBPART A: GENERAL PROVISIONS
Section 724.101
Purpose, Scope and Applicability
a)
The purpose of this Part is to establish minimum standards that define the
acceptable management of hazardous waste.
151
b)
The standards in this Part apply to owners and operators of all facilities that
treat, store, or dispose of hazardous waste, except as specifically provided
otherwise in this Part or 35 Ill. Adm. Code 721.
c)
The requirements of this Part apply to a person disposing of hazardous waste by
means of ocean disposal subject to a permit issued under the Marine Protection,
Research and Sanctuaries Act (16 U.S.C. 1431-1434, 33 U.S.C. 1401) only to
the extent they are included in a RCRA permit by rule granted to such a person
under 35 Ill. Adm. Code 703.141. A “RCRA permit” is a permit required by
Section 21(f) of the Environmental Protection Act and 35 Ill. Adm. Code
703.121.
BOARD NOTE: This Part does apply to the treatment or storage of hazardous
waste before it is loaded onto an ocean vessel for incineration or disposal at sea.
d)
The requirements of this Part apply to a person disposing of hazardous waste by
means of underground injection subject to a permit issued by the Agency
pursuant to Section 12(g) of the Environmental Protection Act only to the extent
they are required by 35 Ill. Adm. Code 704.Subpart F.
BOARD NOTE: This Part does apply to the above-ground treatment or storage
of hazardous waste before it is injected underground.
e)
The requirements of this Part apply to the owner or operator of a POTW
(publicly owned treatment works) that treats, stores, or disposes of hazardous
waste only to the extent included in a RCRA permit by rule granted to such a
person under 35 Ill. Adm. Code 703.141.
f)
This subsection corresponds with 40 CFR 264.1(f), which provides that the
federal regulations do not apply to T/S/D activities in authorized states, except
under limited, enumerated circumstances. This statement maintains structural
consistency with USEPA rules.
g)
The requirements of this Part do not apply to:
1)
The owner or operator of a facility permitted by the Agency under
Section 21 of the Environmental Protection Act to manage municipal or
industrial solid waste, if the only hazardous waste the facility treats,
stores, or disposes of is excluded from regulation under this Part by 35
Ill. Adm. Code 721.105.
BOARD NOTE: The owner or operator may be subject to 35 Ill. Adm.
Code 807 and may have to have a supplemental permit under 35 Ill.
Adm. Code 807.210.
152
2)
The owner or operator of a facility managing recyclable materials
described in 35 Ill. Adm. Code 721.106(a)(2) through (a)(4) (except to
the extent that requirements of this Part are referred to in 35 Ill. Adm.
Code 726.Subparts C, F, G, or H or 35 Ill. Adm. Code 739).
3)
A generator accumulating waste on-site in compliance with 35 Ill. Adm.
Code 722.134.
4)
A farmer disposing of waste pesticides from the farmer’s own use in
compliance with 35 Ill. Adm. Code 722.170.
5)
The owner or operator of a totally enclosed treatment facility, as defined
in 35 Ill. Adm. Code 720.110.
6)
The owner or operator of an elementary neutralization unit or a
wastewater treatment unit, as defined in 35 Ill. Adm. Code 720.110,
provided that if the owner or operator is diluting hazardous ignitable
(D001) wastes (other than the D001 High TOC Subcategory defined in
35 Ill. Adm. Code 728.Table T) or reactive (D003) waste to remove the
characteristic before land disposal, the owner or operator must comply
with the requirements set out in Section 724.117(b).
7)
This subsection corresponds with 40 CFR 264.1(g)(7), reserved by
USEPA. This statement maintains structural consistency with USEPA
rules.
8)
Immediate response:
A)
Except as provided in subsection (g)(8)(B) below of this Section,
a person engaged in treatment or containment activities during
immediate response to any of the following situations:
i)
A discharge of a hazardous waste;
ii)
An imminent and substantial threat of a discharge of
hazardous waste;
iii)
A discharge of a material that becomes a hazardous waste
when discharged.; or
iv) An immediate threat to human health, public safety,
property, or the environment from the known or suspected
presence of military munitions, other explosive material,
or an explosive device, as determined by an explosives or
153
munitions emergency response specialist as defined in 35
Ill. Adm. Code 720.110.
B)
An owner or operator of a facility otherwise regulated by this
Part must comply with all applicable requirements of
724.Subparts C and D.
C)
Any person that is covered by subsection (g)(8)(A) above of this
Section and that continues or initiates hazardous waste treatment
or containment activities after the immediate response is over is
subject to all applicable requirements of this Part and 35 Ill.
Adm. Code 702, 703, and 705 for those activities.
D) In the case of an explosives or munitions emergency response, if
a federal, state, or local official acting within the scope of his or
her official responsibilities or an explosives or munitions
emergency response specialist determines that immediate removal
of the material or waste is necessary to protect human health or
the environment, that official or specialist may authorize the
removal of the material or waste by transporters who do not have
USEPA identification numbers and without the preparation of a
manifest. In the case of emergencies involving military
munitions, the responding military emergency response
specialist's organizational unit shall retain records for three years
identifying the dates of the response, the responsible persons
responding, the type and description of material addressed, and
its disposition.
9)
A transporter storing manifested shipments of hazardous waste in
containers meeting the requirements of 35 Ill. Adm. Code 722.130 at a
transfer facility for a period of ten days or less.
10)
The addition of absorbent materials to waste in a container (as defined in
35 Ill. Adm. Code 720) or the addition of waste to absorbent material in
a container, provided these actions occur at the time waste is first placed
in the container, and Sections 724.117(b), 724.271, and 724.272 are
complied with.
11)
A universal waste handler or universal waste transporter (as defined in
35 Ill. Adm. Code 720.110) that handles any of the wastes listed below
is subject to regulation under 35 Ill. Adm. Code 733 when handling the
following universal wastes:
A)
Batteries, as described in 35 Ill. Adm. Code 733.102;
154
B)
Pesticides, as described in 35 Ill. Adm. Code 733.103;
C)
Thermostats, as described in 35 Ill. Adm. Code 733.104; and
D)
Mercury-containing lamps, as described in 35 Ill. Adm. Code
733.107.
BOARD NOTE: Subsection (g)(11)(D) of this Section was
added pursuant to Section 22.23a of the Act [415 ILCS 5/22.23a]
(see P.A. 90-502, effective August 19, 1997).
h)
This Part applies to owners and operators of facilities that treat, store, or
dispose of hazardous wastes referred to in 35 Ill. Adm. Code 728.
i) 35 Ill. Adm. Code 726.505 identifies when the requirements of this Part apply
to the storage of military munitions classified as solid waste under 35 Ill. Adm.
Code 726.302. The treatment and disposal of hazardous waste military
munitions are subject to the applicable permitting, procedural, and technical
standards in 35 Ill. Adm. Code 702, 703, 705, 720 through 726, and 728.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 724.170
Applicability
The regulations in this Subpart apply to owners and operators of both on-site and off-site
facilities, except as Section 724.101 provides otherwise. Sections 724.171, 724.172 and
724.176 do not apply to owners and operators of on-site facilities that do not receive any
hazardous waste from off-site sources, nor do they apply to owners and operators of off-site
facilities with respect to waste military munitions exempted from manifest requirements under
35 Ill. Adm. Code 726.303(a). Section 724.173(b) only applies to permittees which treat,
store or dispose of hazardous wastes on-site where such wastes were generated.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART J: TANK SYSTEMS
Section 724.298
Special Requirements for Ignitable or Reactive Waste
a)
Ignitable or reactive waste must not be placed in tank systems unless:
1)
The waste is treated, rendered or mixed before or immediately after
placement in the tank system so that:
155
A)
The resulting waste, mixture or dissolved material no longer
meets the definition of ignitable or reactive waste under 35 Ill.
Adm. Code 721.121 or 721.123, and
B)
Section 724.117(b) is complied with; or
2)
The waste is stored or treated in such a way that it is protected from any
material or conditions which may cause the waste to ignite or react; or
3)
The tank is used solely for emergencies.
b)
The owner or operator of a facility where ignitable or reactive waste is stored or
treated in a tank must comply with the requirements for the maintenance of
protective distances between the waste management area and any public ways,
streets, alleys or an adjoining property line that can be built upon as required.in
tables 2-1 through 2-6 of the National Fire Protection Association’s “Flammable
and Combustible Liquids Code,” NFPA 30, incorporated by reference in 35 Ill.
Adm. Code 720.111).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 724.933
Standards: Closed-ventVent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control devices used to
comply with provisions of this Part shall comply with the provisions of
this Section.
2)
The owner or operator of an existing facility that cannot install a closed-
vent system and control device to comply with the provisions of this
Subpart on the effective date that the facility becomes subject to the
provisions of this Subpart shall prepare an implementation schedule that
includes dates by which the closed-vent system and control device will
be installed and in operation. The controls must be installed as soon as
possible, but the implementation schedule may allow up to 30 months
after the effective date that the facility becomes subject to this Subpart
for installation and startup. All units that begin operation after
December 21, 1990, must comply with the rules immediately (i.e., must
have control devices installed and operating on startup of the affected
unit); the 2-year implementation schedule does not apply to these units.
156
b)
A control device involving vapor recovery (e.g., a condenser or adsorber) must
be designed and operated to recover the organic vapors vented to it with an
efficiency of 95 weight percent or greater unless the total organic emission
limits of Section 724.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler, or process
heater) must be designed and operated to reduce the organic emissions vented to
it by 95 weight percent or greater; to achieve a total organic compound
concentration of 20 ppmv, expressed as the sum of the actual compounds and
not in carbon equivalents, on a dry basis, corrected to three percent oxygen; or
to provide a minimum residence time of 0.50 seconds at a minimum
temperature of 760° C. If a boiler or process heater is used as the control
device, then the vent stream must be introduced into the flame zone of the
boiler or process heater.
d)
Flares:
1)
A flare must be designed for and operated with no visible emissions, as
determined by the methods specified in subsection (e)(1), except for
periods not to exceed a total of 5 minutes during any 2 consecutive
hours.
2)
A flare must be operated with a flame present at all times, as determined
by the methods specified in subsection (f)(2)(C) of this Section.
3)
A flare must be used only if the net heating value of the gas being
combusted is 11.2 MJ/scm (300 Btu/scf) or greater and the flare is
steam-assisted or air-assisted or if the net heating value of the gas being
combusted is 7.45 MJ/scm (200 Btu/scf) or greater and the flare is
nonassisted. The net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2) of this Section.
4)
Exit Velocity.
A)
A steam-assisted or nonassisted flare must be designed for and
operated with an exit velocity, as determined by the methods
specified in subsection (e)(3) of this Section, less than 18.3 m/s
(60 ft/s), except as provided in subsections (d)(4)(B) and
(d)(4)(C) of this Section.
B)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, equal to or greater than 18.3
157
m/s (60 ft/s) but less than 122 m/s (400 ft/s) is allowed if the net
heating value of the gas being combusted is greater than 37.3
MJ/scm (1000 Btu/scf).
C)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, less than the velocity, V, as
determined by the method specified in subsection (e)(4) of this
Section and less than 122 m/s (400 ft/s) is allowed.
5)
An air-assisted flare must be designed and operated with an exit velocity
less than the velocity, V, as determined by the method specified in
subsection (e)(5) of this Section.
6)
A flare used to comply with this Section must be steam-assisted, air-
assisted, or nonassisted.
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be used to determine the compliance of a
flare with the visible emission provisions of this Subpart. The
observation period is 2 hours and must be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare must be
calculated using the following equation:
T
i
i
H = K
i
n
C
H
×
=
∑
×
1
T
i
i
H
= K
i
1
n
C
H
×
=
∑
×
Where:
H
T
is the net heating value of the sample in MJ/scm; where the
net enthalpy per mole of offgas is based on combustion at 25° C
and 760 mm Hg, but the standard temperature for determining
the volume corrersponding corresponding to 1 mole is 20° C.
158
K = 1.74
×
10
7
(1/ppm)(g mol/scm)(MJ/kcal) where standard
temperature for (g mol/scm) 20° C.
S
Σ
(Xi) means the sum of the values of X for each component i,
from i=1 to n.
C
i
is the concentration of sample component i in ppm on a wet
basis, as measured for organics by Reference Method 18 in 40
CFR 60, and for carbon monoxide, by ASTM D 1946-90,
incorporated by reference in 35 Ill. Adm. Code 720.111.
H
i
is the net heat of combustion of sample component i,
kcal/gmol at 25° C and 760 mm Hg. The heats of combustion
must be determined using ASTM D 2382, incorporated by
reference in 35 Ill. Adm. Code 720.111, if published values are
not available or cannot be calculated.
3)
The actual exit velocity of a flare must be determined by dividing the
volumetric flow rate (in units of standard temperature and pressure), as
determined by Reference Methods 2, 2A, 2C, or 2D in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111, as appropriate,
by the unobstructed (free) cross-sectional area of the flare tip.
4)
The maximum allowed velocity in m/s, V
max
, for a flare complying with
subsection (d)(4)(C) must be determined by the following equation:
(
)
(
)
log
.
.
max
10
288
317
V
H
T
=
+
(
)
log
V
H
28.8
31.7
10
max
T
=
+
Where:
log
10
means logarithm to the base 10
H
T
is the net heating value as determined in subsection (e)(2).
5)
The maximum allowed velocity in m/s, V
max
, for an air-assisted flare
must be determined by the following equation:
max
.
.
V
H
T
=
+
8 706
0 7084
159
max
T
V
8.706
0.7084H
=
+
Where:
H
T
is the net heating value as determined in subsection (e)(2) of
this Section.
f)
The owner or operator shall monitor and inspect each control device required to
comply with this Section to ensure proper operation and maintenance of the
control device by implementing the following requirements:
1)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a flow indicator that provides a record of stream flow from
each affected process vent to the control device at least once every hour.
The flow indicator sensor must be installed in the vent stream at the
nearest feasible point to the control device inlet but before the point at
which the vent streams are combined.
2)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a device to continuously monitor control device operation
as specified below:
A)
For a thermal vapor incinerator, a temperature monitoring device
equipped with a continuous recorder. The device must have
accuracy of ±1% percent of the temperature being monitored in
° C or ±0.5° C, whichever is greater. The temperature sensor
must be installed at a location in the combustion chamber
downstream of the combustion zone.
B)
For a catalytic vapor incinerator, a temperature monitoring
device equipped with a continuous recorder. The device must be
capable of monitoring temperature at two locations and have an
accuracy of ±1% percent of the temperature being monitored in
° C or ±0.5° C, whichever is greater. One temperature sensor
must be installed in the vent stream at the nearest feasible point to
the catalyst bed inlet and a second temperature sensor must be
installed in the vent stream at the nearest feasible point to the
catalyst bed outlet.
C)
For a flare, a heat sensing monitoring device equipped with a
continuous recorder that indicates the continuous ignition of the
pilot flame.
D)
For a boiler or process heater having a design heat input capacity
less than 44 MW, a temperature monitoring device equipped with
160
a continuous recorder. The device must have an accuracy of
±1% percent of the temperature being monitored in ° C or
±0.5° C, whichever is greater. The temperature sensor must be
installed at a location in the furnace downstream of the
combustion zone.
E)
For a boiler or process heater having a design heat input capacity
greater than or equal to 44 MW, a monitoring device equipped
with a continuous recorder to measure parameters that indicate
good combustion operating practices are being used.
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the
condenser; or
ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable of
monitoring temperature with an accuracy of ±1% percent
of the temperature being monitored in ° C or ±0.5° C,
whichever is greater. The temperature sensor must be
installed at a location in the exhaust vent stream from the
condenser exit (i.e., product side).
G)
For a carbon adsorption system that regenerates the carbon bed
directly in the control device such as a fixed-bed carbon
adsorber, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the carbon
bed, or
ii)
A monitoring device equipped with a continuous recorder
to measure a parameter that indicates the carbon bed is
regenerated on a regular, predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsections (f)(1) and (f)(2) at least once each operating day to check
control device operation and, if necessary, immediately implement the
corrective measures necessary to ensure the control device operates in
compliance with the requirements of this Section.
161
g)
An owner or operator using a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
at a regular, predetermined time interval that is no longer than the carbon
service life established as a requirement of Section 724.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system such as a carbon
canister that does not regenerate the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
on a regular basis by using one of the following procedures:
1)
Monitor the concentration level of the organic compounds in the exhaust
vent stream from the carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon immediately when
carbon breakthrough is indicated. The monitoring frequency must be
daily or at an interval no greater than 20% percent of the time required
to consume the total carbon working capacity established as a
requirement of Section 724.935(b)(4)(C)(vii), whichever is longer.
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design carbon
replacement interval established as a requirement of Section
724.935(b)(4)(C)(vii).
i)
An alternative operational or process parameter may be monitored if the
operator demonstrates that the parameter will ensure that the control device is
operated in conformance with these standards and the control device’s design
specifications.
j)
An owner or operator of an affected facility seeking to comply with the
provisions of this Part by using a control device other than a thermal vapor
incinerator, catalytic vapor incinerator, flare, boiler, process heater, condenser,
or carbon adsorption system is required to develop documentation including
sufficient information to describe the control device operation and identify the
process parameter or parameters that indicate proper operation and maintenance
of the control device.
k)
A closed-vent system must meet either of the following design requirements:
1)
A closed-vent system must be designed to operate with no detectable
emissions, as indicated by an instrument reading of less than 500 ppmv
above background, as determined by the methods specified at Section
724.934(b), and by visual inspections; or
162
2)
A closed-vent system must be designed to operate at a pressure below
atmospheric pressure. The system must be equipped with at least one
pressure gauge or other pressure measurement device that can be read
from a readily accessible location to verify that negative pressure is
being maintained in the closed-vent system when the control device is
operating.
l)
The owner or operator shall monitor and inspect each closed-vent system
required to comply with this Section to ensure proper operation and maintenance
of the closed-vent system by implementing the following requirements:
1)
Each closed-vent system that is used to comply with subsection (k)(1) of
this Section shall be inspected and monitored in accordance with the
following requirements:
A)
An initial leak detection monitoring of the closed-vent system
shall be conducted by the owner or operator on or before the date
that the system becomes subject to this Section. The owner or
operator shall monitor the closed-vent system components and
connections using the procedures specified in Section 724.934(b)
to demonstrate that the closed-vent system operates with no
detectable emissions, as indicated by an instrument reading of
less than 500 ppmv of this Section above background.
B)
After initial leak detection monitoring required in subsection
(l)(1)(A) of this Section, the owner or operator shall inspect and
monitor the closed-vent system as follows:
i)
Closed-vent system joints, seams, or other connections
that are permanently or semi-permanently sealed (e.g., a
welded joint between two sections of hard piping or a
bolted and gasketed ducting flange) must be visually
inspected at least once per year to check for defects that
could result in air pollutant emissions. The owner or
operator shall monitor a component or connection using
the procedures specified in Section 724.934(b) to
demonstrate that it operates with no detectable emissions
following any time the component is repaired or replaced
(e.g., a section of damaged hard piping is replaced with
new hard piping) or the connection is unsealed (e.g., a
flange is unbolted).
ii)
Closed-vent system components or connections other than
those specified in subsection (l)(1)(B)(i) of this Section
must be monitored annually and at other times as
163
requested by the Regional Administrator, except as
provided for in subsection (o) of this Section, using the
procedures specified in Section 724.934(b) to demonstrate
that the components or connections operate with no
detectable emissions.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect or leak in accordance with the
requirements of subsection (l)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 724.935.
2)
Each closed-vent system that is used to comply with subsection (k)(2) of
this Section must be inspected and monitored in accordance with the
following requirements:
A)
The closed-vent system must be visually inspected by the owner
or operator to check for defects that could result in air pollutant
emissions. Defects include, but are not limited to, visible cracks,
holes, or gaps in ductwork or piping or loose connections.
B)
The owner or operator shall perform an initial inspection of the
closed-vent system on or before the date that the system becomes
subject to this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (l)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 724.935.
3)
The owner or operator shall repair all detected defects as follows:
A)
Detectable emissions, as indicated by visual inspection or by an
instrument reading greater than 500 ppmv above background,
must be controlled as soon as practicable, but not later than 15
calendar days after the emission is detected, except as provided
for in subsection (l)(3)(C) of this Section.
164
B)
A first attempt at repair must be made no later than five calendar
days after the emission is detected.
C)
Delay of repair of a closed-vent system for which leaks have been
detected is allowed if the repair is technically infeasible without a
process unit shutdown, or if the owner or operator determines
that emissions resulting from immediate repair would be greater
than the fugitive emissions likely to result from delay of repair.
Repair of such equipment must be completed by the end of the
next process unit shutdown.
D)
The owner or operator shall maintain a record of the defect repair
in accordance with the requirements specified in Section 724.935.
m)
A closed-vent system or control device used to comply with provisions of this
Subpart must be operated at all times when emissions may be vented to it.
n)
The owner or operator using a carbon adsorption system to control air pollutant
emissions shall document that all carbon removed that is a hazardous waste and
that is removed from the control device is managed in one of the following
manners, regardless of the volatile organic concentration of the carbon:
1)
It is regenerated or reactivated in a thermal treatment unit that meets one
of the following:
A)
The owner or operator of the unit has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 724.Subpart X; or
B)
The unit is equipped with and operating air emission controls in
accordance with the applicable requirements of 724.Subparts AA
and CC or 35 Ill. Adm. Code 725.Subparts AA and CC; or
C)
The unit is equipped with and operating air emission controls in
accordance with a national emission standard for hazardous air
pollutants under 40 CFR 61 or 40 CFR 63.
2)
It is incinerated in a hazardous waste incinerator for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 724.Subpart O,; or
165
B)
The owner or operator has certified compliance in accordance
with the interim status requirements of 35 Ill. Adm. Code
725.Subpart O.
3)
It is burned in a boiler or industrial furnace for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 726.Subpart H,; or
B)
The owner or operator has designed and operates the boiler or
industrial furnace in accordance with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
o)
Any components of a closed-vent system that are designated, as described in
Section 724.935(c)(9), as unsafe to monitor are exempt from the requirements
of subsection (l)(1)(B)(ii) of this Section if both of the following conditions are
fulfilled:
1)
The owner or operator of the closed-vent system has determined that the
components of the closed-vent system are unsafe to monitor because
monitoring personnel would be exposed to an immediate danger as a
consequence of complying with subsection (l)(1)(B)(ii) of this Section;
and
2)
The owner or operator of the closed-vent system adheres to a written
plan that requires monitoring the closed-vent system components using
the procedure specified in subsection (l)(1)(B)(ii) as frequently as
practicable during safe-to-monitor times.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.934
Test methods Methods and procedures Procedures
a)
Each owner or operator subject to the provisions of this Subpart shall comply
with the test methods and procedures requirements provided in this Section
b)
When a closed-vent system is tested for compliance with no detectable
emissions, as required in Section 724.933(l), the test must comply with the
following requirements:
1)
Monitoring must comply with Reference Method 21 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111.
166
2)
The detection instrument must meet the performance criteria of
Reference Method 21.
3)
The instrument must be calibrated before use on each day of its use by
the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a concentration of
approximately, but less than, 10,000 ppm methane or n-hexane.
5)
The background level must be determined as set forth in Reference
Method 21.
6)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible as described in Reference
Method 21.
7)
The arithmetic difference between the maximum concentration indicated
by the instrument and the background level is compared with 500 ppm
for determining compliance.
c)
Performance tests to determine compliance with Section 724.932(a) and with the
total organic compound concentration limit of Section 724.933(c) must comply
with the following:
1)
Performance tests to determine total organic compound concentrations
and mass flow rates entering and exiting control devices must be
conducted and data reduced in accordance with the following reference
methods and calculation procedures:
A)
Method 2 in 40 CFR 60 for velocity and volumetric flow rate.
B)
Method 18 in 40 CFR 60 for organic content.
C)
Each performance test must consist of three separate runs, each
run conducted for at least 1 hour under the conditions that exist
when the hazardous waste management unit is operating at the
highest load or capacity level reasonably expected to occur. For
the purpose of determining total organic compound
concentrations and mass flow rates, the average of results of all
runs applies. The average must be computed on a time-weighed
basis.
167
D)
Total organic mass flow rates must be determined by the
following equation:
h
2sd
i
i
-6
E = Q
x(
n
i= 1
C xMW
)x0.0416x
10
∑
h
2sd
i
i
-6
E
= Q
x(
n
i = 1
C x MW )x0.0416x10
∑
Where:
E
h
=
The total organic mass flow rate, kg/h.
Q
2sd
= The volumetric flow rate of gases entering or
exiting control device, dscm/h, as determined by
Method 2 in 40 CFR 60, incorporated by reference
in 35 Ill. Adm. Code 720.111.
n =
The number of organic compounds in the vent gas.
C
i
=
The organic concentration in ppm, dry basis, of
compound i in the vent gas, as determined by
Method 18 in 40 CFR 60.
MW
i
=
The molecular weight of organic compound
i in the vent gas, kg/kg-mol.
0.0416 = The conversion factor for molar volume, kg-
mol/m
3
, at 293 K and 760 mm Hg.
10
-6
= The conversion factor from ppm.
E)
The annual total organic emission rate must be determined by the
following equation:
A = F
×
H
Where:
A is total organic emission rate, kg/y.
168
F is the total organic mass flow rate, kg/h, as calculated
in subsection (c)(1)(D) of this Section.
H is the total annual hours of operation for the affected
unit.
F)
Total organic emissions from all affected process vents at the
facility must be determined by summing the hourly total organic
mass emissions rates (F as determined in subsection (c)(1)(D) of
this Section) and by summing the annual total organic mass
emission rates (A as determined in subsection (c)(1)(E) of this
Section) for all affected process vents at the facility.
2)
The owner or operator shall record such process information as is
necessary to determine the conditions of the performance tests.
Operations during periods of startup, shutdown and malfunction do not
constitute representative conditions for the purpose of a performance
test.
3)
The owner or operator of an affected facility shall provide, or cause to
be provided, performance testing facilities as follows:
A)
Sampling ports adequate for the test methods specified in
subsection (c)(1) of this Section.
B)
Safe sampling platform(s).
C)
Safe access to sampling platform(s).
D)
Utilities for sampling and testing equipment.
4)
For the purpose of making compliance determinations, the time-weighted
average of the results of the three runs must apply. In the event that a
sample is accidentally lost or conditions occur in which one of the three
runs must be discontinued because of forced shutdown, failure of an
irreplaceable portion of the sample train, extreme meteorological
conditions or other circumstances beyond the owner or operator’s
control, compliance may, upon the Agency’s approval, be determined
using the average of the results of the two other runs.
d)
To show that a process vent associated with a hazardous waste distillation,
fractionation, thin-film evaporation, solvent extraction, or air or steam stripping
operation is not subject to the requirements of this Subpart, the owner or
operator shall make an initial determination that the time-weighted, annual
169
average total organic concentration of the waste managed by the waste
management unit is less than 10 ppmw using one of the following two methods:
1)
Direct measurement of the organic concentration of the waste using the
following procedures:
A)
The owner or operator shall take a minimum of four grab
samples of waste for each wastestream managed in the affected
unit under process conditions expected to cause the maximum
waste organic concentration.
B)
For waste generated onsite, the grab samples must be collected at
a point before the waste is exposed to the atmosphere such as in
an enclosed pipe or other closed system that is used to transfer
the waste after generation to the first affected distillation,
fractionation, thin-film evaporation, solvent extraction, or air or
steam stripping operation. For waste generated offsite, the grab
samples must be collected at the inlet to the first waste
management unit that receives the waste provided the waste has
been transferred to the facility in a closed system such as a tank
truck and the waste is not diluted or mixed with other waste.
C)
Each sample must be analyzed and the total organic concentration
of the sample must be computed using Method 9060 or 8240
8260 of SW-846, incorporated by reference under 35 Ill. Adm.
Code 720.111.
D)
The arithmetic mean of the results of the analyses of the four
samples apply for each wastestream managed in the unit in
determining the time-weighted, annual average total organic
concentration of the waste. The time-weighted average is to be
calculated using the annual quantity of each waste stream
processed and the mean organic concentration of each
wastestream managed in the unit.
2)
Using knowledge of the waste to determine that its total organic
concentration is less than 10 ppmw. Documentation of the waste
determination is required. Examples of documentation that must be used
to support a determination under this subsection (d)(2) include:
A)
Production process information documenting that no organic
compounds are used;
B)
Information that the waste is generated by a process that is
identical to a process at the same or another facility that has
170
previously been demonstrated by direct measurement to generate
a wastestream having a total organic content less than 10 ppmw;
or
C)
Prior speciation analysis results on the same wastestream where it
is also documented that no process changes have occurred since
that analysis that could affect the waste total organic
concentration.
e)
The determination that a distillation, fractionation, thin-film evaporation,
solvent extraction, or air or steam stripping operation that manages hazardous
wastes that have time-weighted, annual average total organic concentrations less
than 10 ppmw must be made as follows:
1)
By the effective date that the facility becomes subject to the provisions of
this Subpart or by the date when the waste is first managed in a waste
management unit, whichever is later; and
2)
For continuously generated waste, annually; or
3)
Whenever there is a change in the waste being managed or a change in
the process that generates or treats the waste.
f)
When an owner or operator and the Agency do not agree on whether a
distillation, fractionation, thin-film evaporation, solvent extraction, or air or
steam stripping operation manages a hazardous waste with organic
concentrations of at least 10 ppmw based on knowledge of the waste, the
procedures in Method 8240 8260 in SW-846, incorporated by reference in 35
Ill. Adm. Code 720.111, must may be used to resolve the dispute.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 724.950
Applicability
a)
The regulations in this Subpart apply to owners and operators of facilities that
treat, store, or dispose of hazardous wastes (except as provided in Section
724.101).
b)
Except as provided in Section 724.964(k), this Subpart applies to equipment that
contains or contacts hazardous wastes with organic concentrations of at least
10% percent by weight that are managed in one of the following:
171
1)
A unit that is subject to the RCRA permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705,
2)
A unit (including a hazardous waste recycling unit) that is not exempt
from permitting under the provisions of 35 Ill. Adm. Code 722.134(a)
(i.e., a hazardous waste recycling unit that is not a “90-day” tank or
container) and that is located at a hazardous waste management facility
otherwise subject to the permitting requirements of 35 Ill. Adm. Code
702, 703, and 705, or
3)
A unit that is exempt from permitting under the provisions of 35 Ill.
Adm. Code 722.134(a) (i.e., a “90-day” tank or container).
c)
If the owner or operator of equipment subject to the requirements of Sections
724.952 through 724.965 has received a RCRA permit prior to December 21,
1990, the requirements of Sections 724.952 through 724.965 must be
incorporated when the permit is reissued under 35 Ill. Adm. Code 705.201 or
reviewed under 35 Ill. Adm. Code 702.161.
d)
Each piece of equipment to which this Subpart applies must be marked in such a
manner that it can be distinguished readily from other pieces of equipment.
e)
Equipment that is in vacuum service is excluded from the requirements of
Sections 724.952 to 724.960, if it is identified as required in Section
724.964(g)(5).
f)
Equipment that contains or contacts hazardous waste with an organic
concentration of at least 10% percent by weight for a period of less than 300
hours per calendar year is excluded from the requirements of Sections 264.952
724.952 through 264.960 724.960 if it is identified as required in Section
724.964(g)(6).
BOARD NOTE: The requirements of Sections 724.952 through 724.965 apply
to equipment associated with hazardous waste recycling units previously exempt
under 35 Ill. Adm. Code 721.106(c)(1). Other exemptions under 35 Ill. Adm.
Code 721.104 and 724.101(g) are not affected by these requirements.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.963
Test Methods and Procedures
a)
Each owner or operator subject to the provisions of this Subpart shall comply
with the test methods and procedures requirements provided in this Section.
172
b)
Leak detection monitoring, as required in Sections 724.952 through 724.962,
must comply with the following requirements:
1)
Monitoring must comply with Reference Method 21 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The detection instrument must meet the performance criteria of
Reference Method 21.
3)
The instrument must be calibrated before use on each day of its use by
the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a concentration of
approximately, but less than 10,000 ppm methane or n-hexane.
5)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible as described in Reference
Method 21.
c)
When equipment is tested for compliance with no detectable emissions, as
required in Sections 724.952(e), 724.953(i), 724.954, and 724.957(f), the test
must comply with the following requirements:
1)
The requirements of subsections (b)(1) through (b)(4) above of this
Section apply.
2)
The background level must be determined as set forth in Reference
Method 21.
3)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible as described in Reference
Method 21.
4)
This arithmetic difference between the maximum concentration indicated
by the instrument and the background level is compared with 500 ppm
for determining compliance.
d)
In accordance with the waste analysis plan required by Section 724.113(b), an
owner or operator of a facility shall determine, for each piece of equipment,
whether the equipment contains or contacts a hazardous waste with organic
concentration that equals or exceeds 10 percent by weight using the following:
173
1)
Methods described in ASTM Methods D 2267-88, E 168-88, E 169-87,
and E 260-85, incorporated by reference in 35 Ill. Adm. Code 720.111;
2)
Method 9060 or 8240 8260 of SW-846, incorporated by reference in 35
Ill. Adm. Code 720.111; or
3)
Application of the knowledge of the nature of the hazardous wastestream
or the process by which it was produced. Documentation of a waste
determination by knowledge is required. Examples of documentation
that must be used to support a determination under this provision include
production process information documenting that no organic compounds
are used, information that the waste is generated by a process that is
identical to a process at the same or another facility that has previously
been demonstrated by direct measurement to have a total organic content
less than 10 percent, or prior speciation analysis results on the same
wastestream where it is also documented that no process changes have
occurred since that analysis that could affect the waste total organic
concentration.
e)
If an owner or operator determines that a piece of equipment contains or
contacts a hazardous waste with organic concentrations at least 10 percent by
weight, the determination can be revised only after following the procedures in
subsection (d)(1) or (d)(2) above of this Section.
f)
When an owner or operator and the Agency do not agree on whether a piece of
equipment contains or contacts a hazardous waste with organic concentrations at
least 10 percent by weight, the procedures in subsection (d)(1) or (d)(2) above
of this Section must be used to resolve the dispute.
g)
Samples used in determining the percent organic content must be representative
of the highest total organic content hazardous waste that is expected to be
contained in or contact the equipment.
h)
To determine if pumps or valves are in light liquid service, the vapor pressures
of constituents must either be obtained from standard reference texts or be
determined by ASTM D 2879-8692, incorporated by reference in 35 Ill. Adm.
Code 720.111.
i)
Performance tests to determine if a control device achieves 95 weight percent
organic emission reduction must comply with the procedures of Section
724.934(c)(1) through (c)(4).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
174
Section 724.964
Recordkeeping Requirements
a)
Lumping Units
1)
Each owner or operator subject to the provisions of this Subpart shall
comply with the recordkeeping requirements of this Section.
2)
An owner or operator of more than one hazardous waste management
unit subject to the provisions of this Subpart may comply with the
recordkeeping requirements for these hazardous waste management units
in one recordkeeping system if the system identifies each record by each
hazardous waste management unit.
b)
Owners and operators shall record the following information in the facility
operating record:
1)
For each piece of equipment to which this Subpart applies:
A)
Equipment identification number and hazardous waste
management unit identification.
B)
Approximate locations within the facility (e.g., identify the
hazardous waste management unit on a facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total organics in the hazardous wastestream at
the equipment.
E)
Hazardous waste state at the equipment (e.g., gas-vapor or
liquid).
F)
Method of compliance with the standard (e.g., “monthly leak
detection and repair” or “equipped with dual mechanical seals”).
2)
For facilities than that comply with the provisions of Section
724.933(a)(2), an implementation schedule as specified in that Section.
3)
Where an owner or operator chooses to use test data to demonstrate the
organic removal efficiency or total organic compound concentration
achieved by the control device, a performance test plan as specified in
Section 724.935(b)(3).
175
4)
Documentation of compliance with Section 724.960, including the
detailed design documentation or performance test results specified in
Section 724.935(b)(4).
c)
When each leak is detected as specified in Sections 724.952, 724.953, 724.957
or 724.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked with the
equipment identification number, the date evidence of a potential leak
was found in accordance with Section 724.958(a), and the date the leak
was detected, must be attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be removed after
it has been repaired.
3)
The identification on a valve may be removed after it has been
monitored for 2 successive months as specified in Section 724.957(c)
and no leak has been detected during those 2 months.
d)
When each leak is detected as specified in Sections 724.952, 724.953, 724.957
or 724.958, the following information must be recorded in an inspection log and
must be kept in the facility operating record:
1)
The instrument and operator identification numbers and the equipment
identification number.
2)
The date evidence of a potential leak was found in accordance with
Section 724.958(a).
3)
The date the leak was detected and the dates of each attempt to repair the
leak.
4)
Repair methods applied in each attempt to repair the leak.
5)
“Above 10,000”, if the maximum instrument reading measured by the
methods specified in Section 724.963(b) after each repair attempt is
equal to or greater than 10,000 ppm.
6)
“Repair delayed” and the reason for the delay if a leak is not repaired
within 15 calendar days after discovery of the leak.
7)
Documentation supporting the delay of repair of a valve in compliance
with Section 724.959(c).
176
8)
The signature of the owner or operator (or designate) whose decision it
was that repair could not be effected without a hazardous waste
management unit shutdown.
9)
The expected date of successful repair of the leak if a leak is not repaired
within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection information for
each closed-vent system and control device required to comply with the
provisions of Section 724.960 must be recorded and kept up-to-date in the
facility operating record as specified in Section 724.935(c)(1) and (c)(2), and
monitoring, operating and inspection information in Section 724.935(c)(3)
through (c)(8).
f)
For a control device other than a thermal vapor incinerator, catalytic vapor
incinerator, flare, boiler, process heater, condenser, or carbon adsorption
system, the Agency shall specify the appropriate recordkeeping requirements,
indicating proper operation and maintenance of the control device, in the RCRA
permit.
g)
The following information pertaining to all equipment subject to the
requirements in Sections 724.952 through 724.960 must be recorded in a log
that is kept in the facility operating record:
1)
A list of identification numbers for equipment (except welded fittings)
subject to the requirements of this Subpart.
2)
List of Equipment
A)
A list of identification numbers for equipment that the owner or
operator elects to designate for no detectable emissions, as
indicated by an instrument reading of less than 500 ppm above
background, under the provisions of Sections 724.952(e),
724.953(i) and 724.957(f).
B)
The designation of this equipment as subject to the requirements
of Section 724.952(e), 724.953(i) or 724.957(f) must be signed
by the owner or operator.
3)
A list of equipment identification numbers for pressure relief devices
required to comply with Section 724.954(a).
4)
Compliance tests.
177
A)
The dates of each compliance test required in Sections
724.952(e), 724.953(i), 724.954 and 724.957(f).
B)
The background level measured during each compliance test.
C)
The maximum instrument reading measured at the equipment
during each compliance test.
5)
A list of identification numbers for equipment in vacuum service.
6)
Identification, either by list or location (area or group), of equipment
that contains or contacts hazardous waste with an organic concentration
of at least 10% percent by weight for a period of less than 300 hours per
year.
h)
The following information pertaining to all valves subject to the requirements of
Section 724.957(g) and (h) must be recorded in a log that is kept in the facility
operating record:
1)
A list of identification numbers for valves that are designated as unsafe
to monitor, an explanation for each valve stating why the valve is unsafe
to monitor, and the plan for monitoring each valve.
2)
A list of identification numbers for valves that are designated as difficult
to monitor, an explanation for each valve stating why the valve is
difficult to monitor, and the planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility operating record for
valves complying with Section 724.962:
1)
A schedule of monitoring.
2)
The percent of valves found leaking during each monitoring period.
j)
The following information must be recorded in a log that is kept in the facility
operating record:
1)
Criteria required in Sections 724.952(d)(5)(B) and 724.953(e)(2) and an
explanation of the design criteria.
2)
Any changes to these criteria and the reasons for the changes.
178
k)
The following information must be recorded in a log that is kept in the facility
operating record for use in determining exemptions as provided in Section
724.950 and other specific Subparts:
1)
An analysis determining the design capacity of the hazardous waste
management unit.
2)
A statement listing the hazardous waste influent to and effluent from
each hazardous waste management unit subject to the requirements in
Section 724.960 and an analysis determining whether these hazardous
wastes are heavy liquids.
3)
An up-to-date analysis and the supporting information and data used to
determine whether or not equipment is subject to the requirements in
Sections 724.952 through 724.960. The record must include supporting
documentation as required by Section 724.963(d)(3) when application of
the knowledge of the nature of the hazardous wastestream or the process
by which it was produced is used. If the owner or operator takes any
action (e.g., changing the process that produced the waste) that could
result in an increase in the total organic content of the waste contained in
or contacted by equipment determined not to be subject to the
requirements in Sections 724.952 through 724.960, then a new
determination is required.
l)
Records of the equipment leak information required by subsection (d) of this
Section and the operating information required by subsection (e) of this Section
need be kept only 3 years.
m)
The owner or operator of any facility that is subject to this Subpart and to
regulations at 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart V, incorporated
by reference in 35 Ill. Adm. Code 720.111, may elect to determine compliance
with this Subpart by documentation either pursuant to Section 724.964, or
pursuant to those provisions of 40 CFR 60 or 61, to the extent that the
documentation under the regulation at 40 CFR 60 or 61 duplicates the
documentation required under this Subpart. The documentation under the
regulation at 40 CFR 60 or 61 must be kept with or made readily available with
the facility operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
179
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section 724.980
Applicability
a)
The requirements of this Subpart apply, effective October 6, 1996, to owners
and operators of all facilities that treat, store, or dispose of hazardous waste in
tanks, surface impoundments, or containers subject to 724.Subparts I, J, or K,
except as Section 724.101 and subsection (b) of this Section provide otherwise.
BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
(Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828 (May 19,
1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed. Reg. 28508 (June 5,
1996), USEPA delayed the effective date until October 6, 1996. If action by
USEPA or a decision of a federal court changes the effectiveness of these
regulations, the Board does not intend that the 724.Subpart CC rules be
enforceable to the extent that they become more stringent that than the federal
regulations upon which they are based.
b)
The requirements of this Subpart do not apply to the following waste
management units at the facility:
1)
A waste management unit that holds hazardous waste placed in the unit
before October 6, 1996, and in which no hazardous waste is added to the
unit on or after this date.
2)
A container that has a design capacity less than or equal to 0.1 m
3
(3.5
ft
3
or 26.4 gal).
3)
A tank in which an owner or operator has stopped adding hazardous
waste and the owner or operator has begun implementing or completed
closure pursuant to an approved closure plan.
4)
A surface impoundment in which an owner or operator has stopped
adding hazardous waste (except to implement an approved closure plan)
and the owner or operator has begun implementing or completed closure
pursuant to an approved closure plan.
5)
A waste management unit that is used solely for on-site treatment or
storage of hazardous waste that is generated as the result of
implementing remedial activities required pursuant to the Act or Board
regulations or under the corrective action authorities of RCRA section
3004(u), 3004(v) or 3008(h); CERCLA authorities; or similar federal or
state State authorities.
180
6)
A waste management unit that is used solely for the management of
radioactive mixed waste in accordance with all applicable regulations
under the authority of the Atomic Energy Act (42 U.S.C. 2011 et seq.)
and the Nuclear Waste Policy Act.
7)
A hazardous waste management unit that the owner or operator certifies
is equipped with and operating air emission controls in accordance with
the requirements of an applicable federal Clean Air Act regulation
codified under 40 CFR 60, 61, or 63. For the purpose of complying
with this subsection (b)(7), a tank for which the air emission control
includes an enclosure, as opposed to a cover, must be in compliance
with the enclosure and control device requirements of Section
724.984(i), except as provided in Section 724.982(c)(5).
8)
A tank that has a process vent, as defined in 35 Ill. Adm. Code 724.931.
c)
For the owner and operator of a facility subject to this Subpart and that received
a final RCRA permit prior to October 6, 1996, the requirements of this Subpart
shall be incorporated into the permit when the permit is reissued, renewed, or
modified in accordance with the requirements of 35 Ill. Adm. Code 703 and
705. Until such date when the owner and operator receives a final permit
incorporating the requirements of this Subpart, the owner and operator is subject
to the requirements of 35 Ill. Adm. Code 725.Subpart CC.
d)
The requirements of this Subpart, except for the recordkeeping requirements
specified in Section 724.989(i), are stayed for a tank or container used for the
management of hazardous waste generated by organic peroxide manufacturing
and its associated laboratory operations, when the owner or operator of the unit
meets all of the following conditions:
1)
The owner or operator identifies that the tank or container receives
hazardous waste generated by an organic peroxide manufacturing process
producing more than one functional family of organic peroxides or
multiple organic peroxides within one functional family, that one or
more of these organic peroxides could potentially undergo self-
accelerating thermal decomposition at or below ambient temperatures,
and that organic peroxides are the predominant products manufactured
by the process. For the purposes of this subsection, “organic peroxide”
means an organic compound that contains the bivalent -O-O- structure
and which may be considered to be a structural derivative of hydrogen
peroxide where one or both of the hydrogen atoms has been replaced by
an organic radical.
2)
The owner or operator prepares documentation, in accordance with
Section 724.989(i), explaining why an undue safety hazard would be
181
created if air emission controls specified in Sections 724.984 through
724.987 are installed and operated on the tanks and containers used at
the facility to manage the hazardous waste generated by the organic
peroxide manufacturing process or processes meeting the conditions of
subsection (d)(1) of this Section.
3)
The owner or operator notifies the Agency in writing that hazardous
waste generated by an organic peroxide manufacturing process or
processes meeting the conditions of subsection (d)(1) of this Section are
managed at the facility in tanks or containers meeting the conditions of
subsection (d)(2) of this Section. The notification must state the name
and address of the facility and be signed and dated by an authorized
representative of the facility owner or operator.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.984
Standards: Tanks
a)
The provisions of this Section apply to the control of air pollutant emissions
from tanks for which Section 724.982(b) references the use of this Section for
such air emission control.
b)
The owner or operator shall control air pollutant emissions from each tank
subject to this Section in accordance with the following requirements, as
applicable:
1)
For a tank that manages hazardous waste that meets all of the conditions
specified in subsections (b)(1)(A) through (b)(1)(C) of this Section, the
owner or operator shall control air pollutant emissions from the tank in
accordance with the Tank Level 1 controls specified in subsection (c) of
this Section or the Tank Level 2 controls specified in subsection (d) of
this Section.
A)
The hazardous waste in the tank has a maximum organic vapor
pressure that is less than the maximum organic vapor pressure
limit for the tank’s design capacity category as follows:
i)
For a tank design capacity equal to or greater than 151 m
3
(39,900 gal), the maximum organic vapor pressure limit
for the tank is 5.2 kPa (0.75 psig).
ii)
For a tank design capacity equal to or greater than 75 m
3
(19,800 gal) but less than 151 m
3
(39,900 gal), the
maximum organic vapor pressure limit for the tank is 27.6
kPa (4.00 psig).
182
iii)
For a tank design capacity less than 75 m
3
(19,800 gal),
the maximum organic vapor pressure limit for the tank is
76.6 kPa (11.1 psig).
B)
The hazardous waste in the tank is not heated by the owner or
operator to a temperature that is greater than the temperature at
which the maximum organic vapor pressure of the hazardous
waste is determined for the purpose of complying with subsection
(b)(1)(A) of this Section.
C)
The hazardous waste in the tank is not treated by the owner or
operator using a waste stabilization process, as defined in 35 Ill.
Adm. Code 725.981.
2)
For a tank that manages hazardous waste that does not meet all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank by using Tank Level 2 controls in accordance with the
requirements of subsection (d) of this Section. Examples of tanks
required to use Tank Level 2 controls include a tank used for a waste
stabilization process and a tank for which the hazardous waste in the tank
has a maximum organic vapor pressure that is equal to or greater than
the maximum organic vapor pressure limit for the tank’s design capacity
category as specified in subsection (b)(1)(A) of this Section.
c)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 1 controls must meet the requirements specified in subsections (c)(1)
through (c)(4) of this Section:
1)
The owner or operator shall determine the maximum organic vapor
pressure for a hazardous waste to be managed in the tank using Tank
Level 1 controls before the first time the hazardous waste is placed in the
tank. The maximum organic vapor pressure must be determined using
the procedures specified in Section 724.983(c). Thereafter, the owner or
operator shall perform a new determination whenever changes to the
hazardous waste managed in the tank could potentially cause the
maximum organic vapor pressure to increase to a level that is equal to or
greater than the maximum organic vapor pressure limit for the tank
design capacity category specified in subsection (b)(1)(A) of this
Section, as applicable to the tank.
2)
The tank must be equipped with a fixed roof designed to meet the
following specifications:
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A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the hazardous
waste in the tank. The fixed roof may be a separate cover
installed on the tank (e.g., a removable cover mounted on an
open-top tank) or may be an integral part of the tank structural
design (e.g., a horizontal cylindrical tank equipped with a hatch).
B)
The fixed roof must be installed in a manner such that there are
no visible cracks, holes, gaps, or other open spaces between roof
Section section joints or between the interface of the roof edge
and the tank wall.
C)
Each opening in the fixed roof must be either:
i)
Equipped with a closure device designed to operate such
that when the closure device is secured in the closed
position there are no visible cracks, holes, gaps, or other
open spaces in the closure device or between the perimeter
of the opening and the closure device; or
ii)
Connected by a closed-vent system that is vented to a
control device. The control device must remove or
destroy organics in the vent stream, and it must be
operating whenever hazardous waste is managed in the
tank.
D)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: the organic vapor permeability; the
effects of any contact with the hazardous waste or its vapors
managed in the tank; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices used for the
tank on which the fixed roof is installed.
3)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position, except
as follows:
A)
Opening of closure devices or removal of the fixed roof is
allowed at the following times:
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i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
the liquid in the tank, or when a worker needs to open a
hatch to maintain or repair equipment. Following
completion of the activity, the owner or operator shall
promptly secure the closure device in the closed position
or reinstall the cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of the tank.
B)
Opening of a spring-loaded pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the tank internal pressure in
accordance with the tank design specifications. The device must
be designed to operate with no detectable organic emissions when
the device is secured in the closed position. The settings at which
the device opens must be established such that the device remains
in the closed position whenever the tank internal pressure is
within the internal pressure operating range determined by the
owner or operator based on the tank manufacturer
recommendations, applicable regulations, fire protection and
prevention codes, standard engineering codes and practices, or
other requirements for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to open are
during those times when the tank internal pressure exceeds the
internal pressure operating range for the tank as a result of
loading operations or diurnal ambient temperature fluctuations.
C)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
4)
The owner or operator shall inspect the air emission control equipment
in accordance with the following requirements.
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof sections or between the
roof and the tank wall; broken, cracked, or otherwise damaged
185
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
fixed roof and its closure devices on or before the date that the
tank becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year
except under the special conditions provided for in subsection (l)
of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
d)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 2 controls must use one of the following tanks:
1)
A fixed-roof tank equipped with an internal floating roof in accordance
with the requirements specified in subsection (e) of this Section;
2)
A tank equipped with an external floating roof in accordance with the
requirements specified in subsection (f) of this Section;
3)
A tank vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (g) of this
Section;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) of this Section; or
5)
A tank located inside an enclosure that is vented through a closed-vent
system to an enclosed combustion control device in accordance with the
requirements specified in subsection (i) of this Section.
e)
The owner or operator that controls air pollutant emissions from a tank using a
fixed roof with an internal floating roof shall meet the requirements specified in
subsections (e)(1) through (e)(3) of this Section.
1)
The tank must be equipped with a fixed roof and an internal floating roof
in accordance with the following requirements:
186
A)
The internal floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The internal floating roof must be equipped with a continuous
seal between the wall of the tank and the floating roof edge that
meets either of the following requirements:
i)
A single continuous seal that is either a liquid-mounted
seal or a metallic shoe seal, as defined in 35 Ill. Adm.
Code 725.981; or
ii)
Two continuous seals mounted one of this Section above
the other. The lower seal may be a vapor-mounted seal.
C)
The internal floating roof must meet the following specifications:
i)
Each opening in a noncontact internal floating roof except
for automatic bleeder vents (vacuum breaker vents) and
the rim space vents is to provide a projection below the
liquid surface.
ii)
Each opening in the internal floating roof must be
equipped with a gasketed cover or a gasketed lid except
for leg sleeves, automatic bleeder vents, rim space vents,
column wells, ladder wells, sample wells, and stub drains.
iii)
Each penetration of the internal floating roof for the
purpose of sampling must have a slit fabric cover that
covers at least 90% percent of the opening.
iv)
Each automatic bleeder vent and rim space vent must be
gasketed.
v)
Each penetration of the internal floating roof that allows
for passage of a ladder must have a gasketed sliding
cover.
vi)
Each penetration of the internal floating roof that allows
for passage of a column supporting the fixed roof must
have a flexible fabric sleeve seal or a gasketed sliding
cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
187
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
C)
Prior to filling the tank, each cover, access hatch, gauge float
well or lid on any opening in the internal floating roof must be
bolted or fastened closed (i.e., no visible gaps). Rim space vents
must be set to open only when the internal floating roof is not
floating or when the pressure beneath the rim exceeds the
manufacturer’s recommended setting.
3)
The owner or operator shall inspect the internal floating roof in
accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects that could
result in air pollutant emissions. Defects include, but are not
limited to, any of the following: when the internal floating roof
is not floating on the surface of the liquid inside the tank; when
liquid has accumulated on top of the internal floating roof; when
any portion of the roof seals have detached from the roof rim;
when holes, tears, or other openings are visible in the seal fabric;
when the gaskets no longer close off the hazardous waste surface
from the atmosphere; or when the slotted membrane has more
than 10% percent open area.
B)
The owner or operator shall inspect the internal floating roof
components as follows, except as provided in subsection
(e)(3)(C) of this Section:
i)
Visually inspect the internal floating roof components
through openings on the fixed-roof (e.g., manholes and
roof hatches) at least once every 12 months after initial
fill, and
ii)
Visually inspect the internal floating roof, primary seal,
secondary seal (if one is in service), gaskets, slotted
membranes, and sleeve seals (if any) each time the tank is
emptied and degassed and at least once every 10 years.
188
C)
As an alternative to performing the inspections specified in
subsection (e)(3)(B) of this Section for an internal floating roof
equipped with two continuous seals mounted one above the other,
the owner or operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted membranes,
and sleeve seals (if any) each time the tank is emptied and
degassed and at least every five years.
D)
Prior to each inspection required by subsection (e)(3)(B) or
(e)(3)(C) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each visual inspection of an internal floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned, as provided for in subsection
(e)(3)(D)(ii) of this Section.
ii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Agency at least seven calendar days before refilling the
tank.
E)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
F)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
189
f)
The owner or operator that controls air pollutant emissions from a tank using an
external floating roof must meet the requirements specified in subsections (f)(1)
through (f)(3) of this Section.
1)
The owner or operator shall design the external floating roof in
accordance with the following requirements:
A)
The external floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The floating roof must be equipped with two continuous seals,
one above the other, between the wall of the tank and the roof
edge. The lower seal is referred to as the primary seal, and the
upper seal is referred to as the secondary seal.
i)
The primary seal must be a liquid-mounted seal or a
metallic shoe seal, as defined in 35 Ill. Adm. Code
725.981. The total area of the gaps between the tank wall
and the primary seal must not exceed 212 square
centimeters (cm
2
) per meter (10.0 square inches (in
2
) per
foot) of tank diameter, and the width of any portion of
these gaps must not exceed 3.8 centimeters (cm) (1.5 in).
If a metallic shoe seal is used for the primary seal, the
metallic shoe seal must be designed so that one end
extends into the liquid in the tank and the other end
extends a vertical distance of at least 61 cm (24 in) above
the liquid surface.
ii)
The secondary seal must be mounted above the primary
seal and cover the annular space between the floating roof
and the wall of the tank. The total area of the gaps
between the tank wall and the secondary seal must not
exceed 21.2 cm
2
per meter (1.00 in
2
per foot) of tank
diameter, and the width of any portion of these gaps must
not exceed 1.3 cm (0.51 in).
C)
The external floating roof must meet the following specifications:
i)
Except for automatic bleeder vents (vacuum breaker
vents) and rim space vents, each opening in a noncontact
external floating roof must provide a projection below the
liquid surface.
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ii)
Except for automatic bleeder vents, rim space vents, roof
drains, and leg sleeves, each opening in the roof must be
equipped with a gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must be
equipped with a cover designed to be bolted or fastened
when the cover is secured in the closed position.
iv)
Each automatic bleeder vent and each rim space vent must
be equipped with a gasket.
v)
Each roof drain that empties into the liquid managed in
the tank must be equipped with a slotted membrane fabric
cover that covers at least 90% percent of the area of the
opening.
vi)
Each unslotted and slotted guide pole well must be
equipped with a gasketed sliding cover or a flexible fabric
sleeve seal.
vii)
Each unslotted guide pole must be equipped with a
gasketed cap on the end of the pole.
viii)
Each slotted guide pole must be equipped with a gasketed
float or other device which closes off the liquid surface
from the atmosphere.
ix)
Each gauge hatch and each sample well must be equipped
with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents, roof drains,
and leg sleeves, each opening in the roof must be secured and
maintained in a closed position at all times except when the
closure device must be open for access.
C)
Covers on each access hatch and each gauge float well must be
bolted or fastened when secured in the closed position.
191
D)
Automatic bleeder vents must be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
E)
Rim space vents must be set to open only at those times that the
roof is being floated off the roof leg supports or when the
pressure beneath the rim seal exceeds the manufacturer’s
recommended setting.
F)
The cap on the end of each unslotted guide pole must be secured
in the closed position at all times except when measuring the
level or collecting samples of the liquid in the tank.
G)
The cover on each gauge hatch or sample well must be secured in
the closed position at all times except when the hatch or well
must be opened for access.
H)
Both the primary seal and the secondary seal must completely
cover the annular space between the external floating roof and the
wall of the tank in a continuous fashion except during
inspections.
3)
The owner or operator shall inspect the external floating roof in
accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external floating roof
seal gaps in accordance with the following requirements:
i)
The owner or operator shall perform measurements of
gaps between the tank wall and the primary seal within 60
calendar days after initial operation of the tank following
installation of the floating roof and, thereafter, at least
once every five years.
ii)
The owner or operator shall perform measurements of
gaps between the tank wall and the secondary seal within
60 calendar days after initial operation of the tank
following installation of the floating roof and, thereafter,
at least once every year.
iii)
If a tank ceases to hold hazardous waste for a period of
one year or more, subsequent introduction of hazardous
waste into the tank must be considered an initial operation
for the purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) of this Section.
192
iv)
The owner or operator shall determine the total surface
area of gaps in the primary seal and in the secondary seal
individually using the procedure of subsection (f)(3)(D) of
this Section.
v)
In the event that the seal gap measurements do not
conform to the specifications in subsection (f)(1)(B) of
this Section, the owner or operator shall repair the defect
in accordance with the requirements of subsection (k) of
this Section.
vi)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 724.989(b).
B)
The owner or operator shall visually inspect the external floating
roof in accordance with the following requirements:
i)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects
include, but are not limited to, any of the following
conditions: holes, tears, or other openings in the rim seal
or seal fabric of the floating roof; a rim seal detached
from the floating roof; all or a portion of the floating roof
deck being submerged below the surface of the liquid in
the tank; broken, cracked, or otherwise damaged seals or
gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
ii)
The owner or operator shall perform an initial inspection
of the external floating roof and its closure devices on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall perform
the inspections at least once every year except for the
special conditions provided for in subsection (l) of this
Section.
iii)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k) of this Section.
193
iv)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 724.989(b).
C)
Prior to each inspection required by subsection (f)(3)(A) or
(f)(3)(B), the owner or operator shall notify the Agency in
advance of each inspection to provide the Agency with the
opportunity to have an observer present during the inspection.
The owner or operator shall notify the Agency of the date and
location of the inspection as follows:
i)
Prior to each inspection to measure external floating roof
seal gaps as required under subsection (f)(3)(A) of this
Section, written notification must be prepared and sent by
the owner or operator so that it is received by the Agency
at least 30 calendar days before the date the measurements
are scheduled to be performed.
ii)
Prior to each visual inspection of an external floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned as provided for in subsection
(f)(3)(C)(iii) of this Section.
iii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Agency at least seven calendar days before refilling the
tank.
D)
Procedure for determining the total surface area of gaps in the
primary seal and the secondary seal:
i)
The seal gap measurements must be performed at one or
more floating roof levels when the roof is floating off the
roof supports.
194
ii)
Seal gaps, if any, must be measured around the entire
perimeter of the floating roof in each place where a 0.32
cm (0.125 in) diameter uniform probe passes freely
(without forcing or binding against the seal) between the
seal and the wall of the tank and measure the
circumferential distance of each such location.
iii)
For a seal gap measured under subsection (f)(3) of this
Section, the gap surface area must be determined by using
probes of various widths to measure accurately the actual
distance from the tank wall to the seal and multiplying
each such width by its respective circumferential distance.
iv)
The total gap area must be calculated by adding the gap
surface areas determined for each identified gap location
for the primary seal and the secondary seal individually,
and then dividing the sum for each seal type by the
nominal perimeter of the tank. These total gap areas for
the primary seal and secondary seal are then compared to
the respective standards for the seal type, as specified in
subsection (f)(1)(B) of this Section.
BOARD NOTE: Subsections (f)(3)(D)(i) through
(f)(3)(D)(iv) correspond with 40 CFR
264.1084(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4), which the
Board has codified here to comport with Illinois
Administrative Code format requirements.
g)
The owner or operator that controls air pollutant emissions from a tank by
venting the tank to a control device shall meet the requirements specified in
subsections (g)(1) through (g)(3) of this Section.
1)
The tank must be covered by a fixed roof and vented directly through a
closed-vent system to a control device in accordance with the following
requirements:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
tank.
B)
Each opening in the fixed roof not vented to the control device
must be equipped with a closure device. If the pressure in the
vapor headspace underneath the fixed roof is less than
atmospheric pressure when the control device is operating, the
195
closure devices must be designed to operate such that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device. If the pressure in the vapor headspace underneath
the fixed roof is equal to or greater than atmospheric pressure
when the control device is operating, the closure device must be
designed to operate with no detectable organic emissions.
C)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: organic vapor permeability; the
effects of any contact with the liquid and its vapor managed in
the tank; the effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the tank on which
the fixed roof is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 724.987.
2)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position and the
vapor headspace underneath the fixed roof vented to the control device
except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the fixed roof is allowed at the
following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to open a hatch
to maintain or repair equipment. Following completion of
the activity, the owner or operator shall promptly secure
the closure device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of a tank.
196
B)
Opening of a safety device, as defined in 35 Ill. Adm. Code
725.981, is allowed at any time conditions require doing so to
avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to,
any of the following: visible cracks, holes, or gaps in the roof
sections or between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure devices; and
broken or missing hatches, access covers, caps, or other closure
devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 724.987.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the tank
becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year
except for the special conditions provided for in subsection (l) of
this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
724.989(b).
h)
The owner or operator that controls air pollutant emissions by using a pressure
tank must meet the following requirements:
1)
The tank must be designed not to vent to the atmosphere as a result of
compression of the vapor headspace in the tank during filling of the tank
to its design capacity.
197
2)
All tank openings must be equipped with closure devices designed to
operate with no detectable organic emissions as determined using the
procedure specified in Section 724.983(d).
3)
Whenever a hazardous waste is in the tank, the tank must be operated as
a closed system that does not vent to the atmosphere except in the event
that a safety device, as defined in 35 Ill. Adm. Code 725.981, is
required to open to avoid an unsafe condition.
i)
The owner or operator that controls air pollutant emissions by using an
enclosure vented through a closed-vent system to an enclosed combustion
control device must meet the requirements specified in subsections (i)(1)
through (i)(4) of this Section.
1)
The tank must be located inside an enclosure. The enclosure must be
designed and operated in accordance with the criteria for a permanent
total enclosure, as specified in “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure” under 40
CFR 52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the verification
procedure for the enclosure, as specified in Section 5.0 to “Procedure T-
-Criteria for and Verification of a Permanent or Temporary Total
Enclosure”, initially when the enclosure is first installed and, thereafter,
annually.
2)
The enclosure must be vented through a closed-vent system to an
enclosed combustion control device that is designed and operated in
accordance with the standards for either a vapor incinerator, boiler, or
process heater specified in Section 724.987.
3)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may be
installed and operated as necessary on any enclosure, closed-vent system,
or control device used to comply with the requirements of subsections
(i)(1) and (i)(2) of this Section.
4)
The owner or operator shall inspect and monitor the closed-vent system
and control device as specified in Section 724.987.
j)
The owner or operator shall transfer hazardous waste to a tank subject to this
Section in accordance with the following requirements:
198
1)
Transfer of hazardous waste, except as provided in subsection (j)(2) of
this Section, to the tank from another tank subject to this Section or from
a surface impoundment subject to Section 724.985 must be conducted
using continuous hard-piping or another closed system that does not
allow exposure of the hazardous waste to the atmosphere. For the
purpose of complying with this provision, an individual drain system is
considered to be a closed system when it meets the requirements of 40
CFR 63, subpart RR, “National Emission Standards for Individual Drain
Systems”, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) of this Section do not apply when
transferring a hazardous waste to the tank under any of the following
conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 724.982(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
724.982(c)(2).
k)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(4), (e)(3),
(f)(3), or (g)(3) of this Section, as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair must be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (k)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the tank and no alternative tank
capacity is available at the site to accept the hazardous waste normally
managed in the tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating the hazardous
waste managed in the tank stops operation. Repair of the defect must be
completed before the process or unit resumes operation.
l)
Following the initial inspection and monitoring of the cover, as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year under the following special
conditions:
199
1)
In the case when inspecting or monitoring the cover would expose a
worker to dangerous, hazardous, or other unsafe conditions, then the
owner or operator may designate a cover as an “unsafe to inspect and
monitor cover” and comply with all of the following requirements:
A)
Prepare a written explanation for the cover stating the reasons
why the cover is unsafe to visually inspect or to monitor, if
required.
B)
Develop and implement a written plan and schedule to inspect
and monitor the cover, using the procedures specified in the
applicable Section of this Subpart, as frequently as practicable
during those times when a worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely underground, an
owner or operator is required to inspect and monitor, as required by the
applicable provisions of this Section, only those portions of the tank
cover and those connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground surface.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 724.990
Reporting Requirements
a)
Each owner or operator managing hazardous waste in a tank, surface
impoundment, or container exempted from using air emission controls under the
provisions of Section 724.982(c) shall report to the Agency each occurrence
when hazardous waste is placed in the waste management unit in noncompliance
with the conditions specified in Section 724.982(c)(1) or (c)(2), as applicable.
Examples of such occurrences include placing in the waste management unit a
hazardous waste having an average VO concentration equal to or greater than
500 ppmw at the point of waste origination or placing in the waste management
unit a treated hazardous waste that fails to meet the applicable conditions
specified in Section 724.982(c)(2)(A) through (c)(2)(F). The owner or operator
shall submit a written report within 15 calendar days of the time that the owner
or operator becomes aware of the occurrence. The written report shall contain
the USEPA identification number, the facility name and address, a description
of the noncompliance event and the cause, the dates of the noncompliance, and
the actions taken to correct the noncompliance and prevent recurrence of the
noncompliance. The report shall be signed and dated by an authorized
representative of the owner or operator.
b)
Each owner or operator using air emission controls on a tank in accordance with
the requirements of Section 724.984(c) shall report to the Agency each
occurrence when hazardous waste is managed in the tank in noncompliance with
200
the conditions specified in Section 724.984(b). The owner or operator shall
submit a written report within 15 calendar days of the time that the owner or
operator becomes aware of the occurrence. The written report shall contain the
USEPA identification number, the facility name and address, a description of
the noncompliance event and the cause, the dates of the noncompliance, and the
actions taken to correct the noncompliance and prevent recurrence of the
noncompliance. The report shall be signed and dated by an authorized
representative of the owner or operator.
c)
Each owner or operator using a control device in accordance with the
requirements of Section 724.987 shall submit a semiannual written report to the
Agency, excepted except as provided for in subsection (d) of this Section. The
report shall describe each occurrence during the previous 6-month period when
either of the two following events occurs: a control device is operated
continuously for 24 hours or longer in noncompliance with the applicable
operating values defined in Section 724.935(c)(4) or a flare is operated with
visible emissions for five minutes or longer in a two-hour period, as defined in
Section 724.933(d). The written report shall include the USEPA identification
number, the facility name and address, and an explanation why the control
device could not be returned to compliance within 24 hours, and actions taken
to correct the noncompliance. The report shall be signed and dated by an
authorized representative of the owner or operator.
d)
A report to the Agency in accordance with the requirements of subsection (c) of
this Section is not required for a 6-month period during which all control
devices subject to this Subpart are operated by the owner or operator so that
both of the following conditions result: during no period of 24 hours or longer
did a control device operate continuously in noncompliance with the applicable
operating values defined in Section 724.935(c)(4) and no flare was operated
with visible emissions for five minutes or longer in a two-hour period, as
defined in Section 724.933(d).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section 724.1200 Applicability
The requirements of this Subpart EE apply to owners or operators who store munitions and
explosive hazardous wastes, except as Section 724.101 provides otherwise.
BOARD NOTE: Depending on explosive hazards, hazardous waste munitions and explosives
may also be managed in other types of storage units, including containment buildings (Subpart
201
DD of this Part), tanks (Subpart J of this Part), or containers (Subpart I of this Part); see 35
Ill. Adm. Code 726.305 for storage of waste military munitions.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 724.1201 Design and Operating Standards
a) An owner or operator of a hazardous waste munitions and explosives storage
unit shall design and operate the unit with containment systems, controls, and
monitoring that fulfill each of the following requirements:
1) The owner or operator minimizes the potential for detonation or other
means of release of hazardous waste, hazardous constituents, hazardous
decomposition products, or contaminated run-off to the soil, ground
water, surface water, and atmosphere;
2) The owner or operator provides a primary barrier, which may be a
container (including a shell) or tank, designed to contain the hazardous
waste;
3) For wastes stored outdoors, the owner or operator provides that the
waste and containers will not be in standing precipitation;
4) For liquid wastes, the owner or operator provides a secondary
containment system that assures that any released liquids are contained
and promptly detected and removed from the waste area or a vapor
detection system that assures that any released liquids or vapors are
promptly detected and an appropriate response taken (e.g., additional
containment, such as overpacking or removal from the waste area); and
5) The owner or operator provides monitoring and inspection procedures
that assure the controls and containment systems are working as designed
and that releases that may adversely impact human health or the
environment are not escaping from the unit.
b) Hazardous waste munitions and explosives stored under this Subpart EE may be
stored in one of the following:
1) Earth-covered magazines. The owner or operator of an earth-covered
magazine shall fulfill each of the following requirements:
A) The magazine is constructed of waterproofed, reinforced concrete
or structural steel arches, with steel doors that are kept closed
when not being accessed;
202
B) The magazine is so designed and constructed that it fulfills each
of the following requirements:
i) The magazine is of sufficient strength and thickness to
support the weight of any explosives or munitions stored
and any equipment used in the unit;
ii) The magazine provides working space for personnel and
equipment in the unit; and
iii) The magazine can withstand movement activities that
occur in the unit; and
C) The magazine is located and designed, with walls and earthen
covers that direct an explosion in the unit in a safe direction, so
as to minimize the propagation of an explosion to adjacent units
and to minimize other effects of any explosion.
2) Above-ground magazines. Above-ground magazines must be located
and designed so as to minimize the propagation of an explosion to
adjacent units and to minimize other effects of any explosion.
3) Outdoor or open storage areas. Outdoor or open storage areas must be
located and designed so as to minimize the propagation of an explosion
to adjacent units and to minimize other effects of any explosion.
c) An owner or operator shall store hazardous waste munitions and explosives in
accordance with a standard operating procedure that specifies procedures which
ensure safety, security, and environmental protection. If these procedures serve
the same purpose as the security and inspection requirements of Section
724.114, the preparedness and prevention procedures of Subpart C of this Part,
and the contingency plan and emergency procedures requirements of Subpart D
of this Part, then the standard operating procedure may be used to fulfill those
requirements.
d) An owner or operator shall package hazardous waste munitions and explosives
to ensure safety in handling and storage.
e) An owner or operator shall inventory hazardous waste munitions and explosives
at least annually.
f) An owner or operator shall inspect and monitor hazardous waste munitions and
explosives and their storage units as necessary to ensure explosives safety and to
ensure that there is no migration of contaminants out of the unit.
203
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 724.1202 Closure and Post-Closure Care
a) At closure of a magazine or unit which stored hazardous waste under this
Subpart, the owner or operator shall remove or decontaminate all waste
residues, contaminated containment system components, contaminated subsoils,
and structures and equipment contaminated with waste and manage them as
hazardous waste unless 35 Ill. Adm. Code 721.103(d) applies. The closure
plan, closure activities, cost estimates for closure, and financial responsibility
for magazines or units must meet all of the requirements specified in Subparts G
and H of this Part, except that the owner or operator may defer closure of the
unit as long as it remains in service as a munitions or explosives magazine or
storage unit.
b) If, after removing or decontaminating all residues and making all reasonable
efforts to effect removal or decontamination of contaminated components,
subsoils, structures, and equipment as required in subsection (a) of this Section,
the owner or operator finds that not all contaminated subsoils can be practicably
removed or decontaminated, the owner or operator shall close the facility and
perform post-closure care in accordance with the closure and post-closure
requirements that apply to landfills (see Section 724.410).
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 724.Appendix I
Groundwater Monitoring List
a)
The regulatory requirements pertain only to the list of substances; the right hand
columns (Methods and PQL) are given for informational purposes only. See
also subsections (e) and (f) of this Section.
b)
Common names are those widely used in government regulations, scientific
publications and commerce; synonyms exist for many chemicals.
c)
“CAS RN” means “Chemical Abstracts Service Registry Number”. Where
“total” is entered, all species in the groundwater that contain this element are
included.
d)
CAS index names are those used in the 9th Cumulative index.
e)
“Suggested Methods” refer to analytical procedure numbers used in “Test
Methods for Solid Waste,” SW-846, incorporated by reference in 35 Ill. Adm.
Code 720.111. Analytical details can be found in “Test Methods”, and in
documentation on file with USEPA. Caution: The methods listed are
204
representative procedures and may not always be the most suitable methods for
monitoring an analyte under the regulations. The packed column gas
chromatography methods 8010, 8020, 8030, 8040, 8060, 8080, 8090, 8110,
8120, 8140, 8150, 8240, and 8250 were in Update IIB of SW-846. However,
in Update III, USEPA replaced these methods with “capillary column gas
chromatography (GC) methods”, as the suggested methods.
f)
Practical Quantitation Limits (“PQLs”) are the lowest concentrations of analytes
in groundwater that can be reliably determined within specified limits of
precision and accuracy by the indicated methods under routine laboratory
operating conditions. The POLs listed are generally stated to one significant
figure. Caution: The PQL values in many cases are based only on a general
estimate for the method and not on a determination for individual compounds;
PQLs are not a part of the regulation.
g)
PCBs (CAS RN 1336-36-3). This category contains congener chemicals,
including constituents Aroclor-1016 (CAS RN 12674-11-2), Aroclor-1221 (CAS
RN 11104-28-2), Aroclor-1232 (CAS RN 11141-16-5), Aroclor-1242 (CAS RN
53469-21-9), Aroclor-1248 (CAS RN 12672-29-6), Aroclor-1254 (CAS RN
11097-69-1) and Aroclor-1260 (CAS RN 11096-82-5). The PQL shown is an
average value for PCB congeners.
h)
PCDDs. This category includes congener chemicals, including tetrachloro-
dibenzo-p-dioxins (see also 2,3,7,8-TCDD), pentachlorodibenzo-p-dioxins and
hexachlorodibenzo-p-dioxins. The PQL shown is an average value for PCDD
congeners.
i)
PCDFs. This category contains congener chemicals, including tetrachloro-
dibenzofurans, pentachlorodibenzofurans and hexachlorodibenzofurans. The
PQL shown is an average for all PCDF congeners.
Common Name
CAS RN
Chemical Abstracts Service
Index Name
Suggested
methods
PQL
(ug/L)
Acenaphthene
83-32-9
Acenaphthylene, 1,2-di-
hydro-
8100
8270
200.
10.
Acenaphthylene
208-96-8
Acenaphthylene
8100
8270
200.
10.
Acetone
67-64-1
2-Propanone
8240
100.
Acetophenone
98-86-2
Ethanone, 1-phenyl-
8270
10.
205
Acetonitrile; Methyl
cyanide
75-05-8
Acetonitrile
8015
100.
2-Acetylaminofluorene; 2-
AAF
53-96-3
Acetamide, N-9H-fluoren-
2-yl-
8270
10.
Acrolein
107-02-8
2-Propenal
8030
8240
5.
5.
Acrylonitrile
107-13-1
2-Propenenitrile
8030
8240
5.
5.
Aldrin
309-00-2
1,4:5,8-Dimethano-
naphthalene,
1,2,3,4,10,10-hexachloro-
1,4,4a,5,8,8a-hexahydro-
(1alpha
α
,4alpha
α
,4abeta
β
,
5alpha
α
,8alpha
α
,8abeta
β
)-
8080
8270
0.05
10.
Allyl chloride
107-05-1
1-Propene, 3-chloro-
8010
8240
5.
100.
4-Aminobiphenyl
92-67-1
[1,1'-Biphenyl]-4-amine
8270
10.
Aniline
62-53-3
Benzenamine
8270
10.
Anthracene
120-12-7
Anthracene
8100
8270
200.
10.
Antimony
(Total)
Antimony
6010
7040
7041
300.
2000.
30.
Aramite
140-57-8
Sulfurous acid, 2-chloro-
ethyl 2-[4-(1,1-dimethyl-
ethyl)phenoxy]-1-methyl-
ethyl ester
8270
10.
Arsenic
(Total)
Arsenic
6010
7060
7061
500.
10.
20.
Barium
(Total)
Barium
6010
7080
20.
1000.
206
Benzene
71-43-2
Benzene
8020
8240
2.
5.
Benzo[a]anthracene; Benz-
anthracene
56-55-3
Benz[a]anthracene
8100
8270
200.
10.
Benzo[b]fluoranthene
205-99-2
Benz[e]acephenanthrylene
8100
8270
200.
10.
Benzo[k]fluoranthene
207-08-9
Benzo[k]fluoranthene
8100
8270
200.
10.
Benzo[ghi]perylene
191-24-2
Benzo[ghi]perylene
8100
8270
200.
10.
Benzo[a]pyrene
50-32-8
Benzo[a]pyrene
8100
8270
200.
10.
Benzyl alcohol
100-51-6
Benzenemethanol
8270
20.
Beryllium
(Total)
Beryllium
6010
7090
7091
3.
50.
2.
alpha
α
-BHC
319-84-6
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
(1alpha
α
,2alpha
α
,3beta
β
,4
alpha
α
,5beta
β
,6beta
β
)-
8080
8250
0.05
10.
beta
β
-BHC
319-85-7
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
(1alpha
α
,2beta
β
,3alpha
α
,4
beta
β
,5alpha
α
,6beta
β
)-
8080
8250
0.05
40.
delta
δ
-BHC
319-86-8
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
(1alpha
α
,2alpha
α
,3alpha
α
,
4beta
β
,5alpha
α
,6beta
β
)-
8080
8250
0.1
30.
gamma
χ
-BHC; Lindane
58-89-9
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
(1alpha
α
,2alpha
α
,3beta
β
,4
alpha
α
,5alpha
α
,6beta
β
)-
8080
8250
0.05
10.
207
Bis(2-chloroethoxy)-
methane
111-91-1
Ethane, 1,1'-[methylene-
bis(oxy)]bis[2-chloro-
8270
10.
Bis(2-chloroethyl)ether
111-44-4
Ethane, 1,1'-oxybis[2-
chloro-
8270
10.
Bis(2-chloro-1-methylethyl)
ether; 2,2'-Dichlorodiiso-
propyl ether
108-60-1
Propane, 2,2'-oxybis[1-
chloro-
8010
8270
100.
10.
Bis(2-ethylhexyl) phthalate
117-81-7
1,2-Benzenedicarboxylic
acid, bis(2-ethylhexyl) ester
8060
8270
20.
10.
Bromodichloromethane
75-27-4
Methane, bromodichloro-
8010
8240
1.
5.
Bromoform; Tribromo-
methane
75-25-2
Methane, tribromo-
8010
8240
2.
5.
4-Bromophenyl phenyl
ether
101-55-3
Benzene, 1-bromo-4-
phenoxy-
8270
10.
Butyl benzyl phthalate;
Benzyl butyl phthalate
85-68-7
1,2-Benzenedicarboxylic
acid, butyl phenylmethyl
ester
8060
8270
5.
10.
Cadmium
Total
Cadmium
6010
7130
7131
40.
50.
1.
Carbon disulfide
75-15-0
Carbon disulfide
8240
5.
Carbon tetrachloride
56-23-5
Methane, tetrachloro-
8010
8240
1.
5.
Chlordane
57-74-9
4,7-Methano-1H-
indene,1,2,4,5,6,7,8,8-
octachloro-2,3,3a,4,7,7a-
hexahydro-
8080
8250
0.1
10.
p-Chloroaniline
106-47-8
Benzeneamine, 4-chloro-
8270
20.
208
Chlorobenzene
108-90-7
Benzene, chloro-
8010
8020
8240
2.
2.
5.
Chlorobenzilate
510-15-6
Benzeneacetic acid, 4-
chloro-alpha
α
-(4-chloro-
phenyl)-alpha
α
-hydroxy-,
ethylf ester
8270
10.
p-Chloro-m-cresol
59-50-7
Phenol, 4-chloro-3-methyl-
8040
8270
5.
20.
Chloroethane; Ethyl
chloride
75-00-3
Ethane, chloro-
8010
8240
5.
10.
Chloroform
67-66-3
Methane, trichloro-
8010
8240
0.5
5.
2-Chloronapthalene
91-58-7
Naphthalene, 2-chloro-
8120
8270
10.
10.
2-Chlorophenol
95-57-8
Phenol, 2-chloro-
8040
8270
5.
10.
4-Chlorophenyl phenyl
ether
7005-72-3
Benzene, 1-chloro-4-
phenoxy-
8270
10.
Chloroprene
126-99-8
1,3-Butadiene, 2-chloro-
8010
8240
50.
5.
Chromium
(Total)
Chromium
6010
7190
7191
70.
500.
10.
Chrysene
218-01-9
Chrysene
8100
8270
200.
10.
Cobalt
(Total)
Cobalt
6010
7200
7201
70.
500.
10.
Copper
(Total)
Copper
6010
7210
60.
200.
209
m-Cresol
108-39-4
Phenol, 3-methyl-
8270
10.
o-Cresol
95-48-7
Phenol, 2-methyl-
8270
10.
p-Cresol
106-44-5
Phenol, 4-methyl-
8270
10.
Cyanide
57-12-5
Cyanide
9010
40.
2,4-D; 2,4-Dichloro-
phenoxyacetic acid
94-75-7
Acetic acid, (2,4-dichloro-
phenoxy)-
8150
10.
4,4'-DDD
72-54-8
Benzene, 1,1'-(2,2-di-
chloroethylidene)bis[4-
chloro-
8080
8270
0.1
10.
4,4'-DDE
72-55-9
Benzene, 1,1'-(dichloro-
ethylidene)bis[4-chloro-
8080
8270
0.05
10.
4,4'-DDT
50-29-3
Benzene, 1,1'-(2,2,2-tri-
chloroethylidene)bis[4-
chloro-
8080
8270
0.1
10.
Diallate
2303-16-4
Carbamothioic acid, bis(1-
methylethyl)-, S-(2,3-di-
chloro--2-propenyl) ester
8270
10.
Dibenz[a,h]anthracene
53-70-3
Dibenz[a,h]anthracene
8100
8270
200.
10.
Dibenzofuran
132-64-9
Dibenzofuran
8270
10.
Dibromochloromethane;
Chlorodibromomethane
124-48-1
Methane, dibromochloro-
8010
8240
1.
5.
1,2-Dibromo-3-chloro-
propane; DBCP
96-12-8
Propane, 1,2-dibromo-3-
chloro-
8010
8240
8270
100.
5.
10.
1,2-Dibromoethane;
Ethylene dibromide
106-93-4
Ethane, 1,2-dibromo-
8010
8240
10.
5.
Di-n-butyl phthalate
84-74-2
1,2-Benzenedicarboxylic
acid, dibutyl ester
8060
8270
5.
10.
210
o-Dichlorobenzene
95-50-1
Benzene, 1,2-dichloro-
8010
8020
8120
8270
2.
5.
10.
10.
m-Dichlorobenzene
541-73-1
Benzene, 1,3-dichloro-
8010
8020
8120
8270
5.
5.
10.
10.
p-Dichlorobenzene
106-46-7
Benzene, 1,4-dichloro-
8010
8020
8120
8270
2.
5.
15.
10.
3,3'-Dichlorobenzidine
91-94-1
[1,1'-Biphenyl]-4,4'-di-
amine, 3,3'-dichloro-
8270
20.
trans-1,4-Dichloro-2-
butene
110-57-6
2-Butene, 1,4-dichloro-,
(E)-
8240
5.
Dichlorodifluoromethane
75-71-8
Methane, dichlorodifluoro-
8010
8240
10.
5.
1,1-Dichloroethane
75-34-3
Ethane, 1,1-dichloro-
8010
8240
1.
5.
1,2-Dichloroethane;
Ethylene dichloride
107-06-2
Ethane, 1,2-dichloro-
8010
8240
0.5
5.
1,1-Dichloroethylene;
Vinylidene chloride
75-35-4
Ethene, 1,1-dichloro-
8010
8240
1.
5.
trans-1,2-Dichloroethylene
156-60-5
Ethene, 1,2-dichloro-, (E)-
8010
8240
1.
5.
2,4-Dichlorophenol
120-83-2
Phenol, 2,4-dichloro-
8040
8270
5.
10.
2,6-Dichlorophenol
87-65-0
Phenol, 2,6-dichloro-
8270
10.
1,2-Dichloropropane
78-87-5
Propane, 1,2-dichloro-
8010
8240
0.5
5.
211
cis-1,3-Dichloropropene
10061-01-5
1-Propene, 1,3-dichloro-,
(Z)-
8010
8240
20.
5.
trans-1,3-Dichloropropene
10061-02-6
1-Propene, 1,3-dichloro-,
(E)-
8010
8240
5.
5.
Dieldrin
60-57-1
2,7:3,6-Dimethanonaphth-
[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-
1a,2,2a,3,6,6a,7,7a-octa-
hydro-
,(1aalpha
α
,2beta
β
,2aalpha
α
,3beta
β
,6beta
β
,6aalpha
α
,
7beta
β
,7aalpha
α
)-
8080
8270
0.05
10.
Diethyl phthalate
84-66-2
1,2-Benzenedicarboxylic
acid, diethyl ester
8060
8270
5.
10.
O,O-Diethyl O-2-pyrazinyl
phosphorothioate;
Thionazin
297-97-2
Phosphorothioic acid, O,O-
diethyl O-pyrazinyl ester
8270
10.
Dimethoate
60-51-5
Phosphorodithioic acid,
O,O-dimethyl S-[2-
(methylamino)-2-oxoethyl]
ester
8270
10.
p-(Dimethylamino)-
azobenzene
60-11-7
Benzenamine, N,N-di-
methyl-4-(phenylazo)-
8270
10.
7,12-Dimethylbenz[a]-
anthracene
57-97-6
Benz[a]anthracene,7,12-di-
methyl-
8270
10.
3,3'-Dimethylbenzidine
119-93-7
[1,1'-Biphenyl]-4,4'-di-
amine, 3,3'-dimethyl-
8270
10.
alpha
α
,alpha
α
-Dimethyl-
phenethylamine
122-09-8
Benzeneethanamine,
alpha
α
,alpha
α
-dimethyl-
8270
10.
2,4-Dimethylphenol
105-67-9
Phenol, 2,4-dimethyl-
8040
8270
5.
10.
Dimethyl phthalate
131-11-3
1,2-Benzenedicarboxylic
acid, dimethyl ester
8060
8270
5.
10.
212
m-Dinitrobenzene
99-65-0
Benzene, 1,3-dinitro-
8270
10.
4,6-Dinitro-o-cresol
534-52-1
Phenol, 2-methyl-4,6-di-
nitro-
8040
8270
150.
50.
2,4-Dinitrophenol
51-28-5
Phenol, 2,4-dinitro-
8040
8270
150.
50.
2,4-Dinitrotoluene
121-14-2
Benzene, 1-methyl-2,4-di-
nitro-
8090
8270
0.2
10.
2,6-Dinitrotoluene
606-20-2
Benzene, 2-methyl-1,3-di-
nitro-
8090
8270
0.1
10.
Dinoseb; DNBP; 2-sec-
Butyl-4,6-dinitrophenol
88-85-7
Phenol, 2-(1-methyl-
propyl)-4,6-dinitro-
8150
8270
1.
10.
Di-n-octyl phthalate
117-84-0
1,2-Benzenedicarboxylic
acid, dioctyl ester
8060
8270
30.
10.
1,4-Dioxane
123-91-1
1,4-Dioxane
8015
150.
Diphenylamine
122-39-4
Benzeneamine, N-phenyl-
8270
10.
Disulfoton
298-04-4
Phosphorodithioic acid,
O,O-diethyl S-[2-(ethyl-
thio)ethyl] ester
8140
8270
2.
10.
Endosulfan I
959-98-8
6,9-Methano-2,4,3-
benzodi-
oxathiepin,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-oxide,
(3alpha
α
,5abeta
β
,6alpha
α
,
9alpha
α
,9abeta
β
)-
8080
8250
0.1
10.
Endosulfan II
33213-65-9
6,9-Methano-2,4,3-
benzodi-
oxathiepin,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-oxide,
(3alpha
α
,5aalpha
α
,6beta
β
,
9beta
β
,9aalpha
α
)-
8080
0.05
213
Endosulfan sulfate
1031-07-8
6,9-Methano-2,4,3-
benzodi-
oxathiepin,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-,3,3-dioxide
8080
8270
0.5
10.
Endrin
72-20-8
2,7:3,6-Dimethanonaphth-
[2,3-b]oxirene,
3,4,5,6,9,9-hexachloro-
1a,2,2a,3,6,6a,7,7a-octa-
hydro-,
(1aalpha
α
,2beta
β
,2abeta
β
,
3alpha
α
,6alpha
α
,6abeta
β
,7
beta
β
,7aalpha
α
)-
8080
8250
0.1
10.
Endrin aldehyde
7421-93-4
1,2,4-Methanocyclopenta-
[cd]pentalene-5-carbox-
aldehyde, 2,2a,3,3,4,7-
hexachlorodecahydro-,
(1alpha
α
,2beta
β
,2abeta
β
,4
beta
β
,4abeta
β
,5beta
β
,6abet
a
β
,6bbeta
β
,7R)-
8080
8270
0.2
10.
Ethylbenzene
100-41-4
Benzene, ethyl-
8020
8240
2.
5.
Ethyl methacrylate
97-63-2
2-Propenoic acid, 2-
methyl-, ethyl ester
8015
8240
8270
10.
5.
10.
Ethyl methanesulfonate
62-50-0
Methanesulfonic acid, ethyl
ester
8270
10.
Famphur
52-85-7
Phosphorothioic acid, O-
[4-[(dimethylamino)-
sulfonyl]phenyl]-O,O-di-
methyl ester
8270
10.
Fluoranthene
206-44-0
Fluoranthene
8100
8270
200.
10.
Fluorene
86-73-7
9H-Fluorene
8100
8270
200.
10.
214
Heptachlor
76-44-8
4,7-Methano-1H-indene,
1,4,5,6,7,8,8-heptachloro-
3a,4,7,7a-tetrahydro-
8080
8270
0.05
10.
Heptachlor epoxide
1024-57-3
2,5-Methano-2H-indeno-
[1,2-b]oxirene,
2,3,4,5,6,7,7-heptachloro-
1a,1b,5,5a,6,6a-hexa-
hydro-,
(1aalpha
α
,1bbeta
β
,2alpha
α
,5alpha
α
,5abeta
β
,6beta
β
,6
aalpha
α
)-
8080
8270
1.
10.
Hexachlorobenzene
118-74-1
Benzene, hexachloro-
8120
8270
0.5
10.
Hexachlorobutadiene
87-68-3
1,3-Butadiene, 1,1,2,3,4,4-
hexachloro-
8120
8270
5.
10.
Hexachlorocyclopentadiene
77-47-4
1,3-Cyclopentadiene,
1,2,3,4,5,5-hexachloro-
8120
8270
5.
10.
Hexachloroethane
67-72-1
Ethane, hexachloro-
8120
8270
0.5
10.
Hexachlorophene
70-30-4
Phenol, 2,2'-methylenebis-
[3,4,6-trichloro-
8270
10.
Hexachloropropene
1888-71-7
1-Propene, 1,1,2,3,3,3-
hexachloro-
8270
10.
2-Hexanone
591-78-6
2-Hexanone
8240
50.
Indeno(1,2,3-cd)pyrene
193-39-5
Indeno[1,2,3-cd]pyrene
8100
8270
200.
10.
Isobutyl alcohol
78-83-1
1-Propanol, 2-methyl-
8015
50.
Isodrin
465-73-6
1,4,5,8-Dimethano-
naphthalene,
1,2,3,4,10,10-hexachloro-
1,4,4a,5,8,8a-hexahydro-
(1alpha
α
,4alpha
α
,4abeta
β
,
5beta
β
,8beta
β
,8abeta
β
)-
8270
10.
215
Isophorone
78-59-1
2-Cyclohexen-1-one, 3,5,5-
trimethyl-
8090
8270
60.
10.
Isosafrole
120-58-1
1,3-Benzodioxole, 5-(1-
propenyl)-
8270
10.
Kepone
143-50-0
1,3,4-Metheno-2H-cyclo-
buta-[c,d]pentalen-2-one,
1,1a,3,3a,4,5,5,5a,5b,6-
decachlorooctahydro-
8270
10.
Lead
(Total)
Lead
6010
7420
7421
40.
1000.
10.
Mercury
(Total)
Mercury
7470
2.
Methacrylonitrile
126-96-7
2-Propenenitrile, 2-methyl-
8015
8240
5.
5.
Methapyrilene
91-80-5
1,2-Ethanediamine, N,N-
dimethyl-N’-2-pyridinyl-
N’-(2-thienylmethyl)-
8270
10.
Methoxychlor
72-43-5
Benzene, 1,1'-(2,2,2-tri-
chloroethylidene)bis[4-
methoxy-
8080
8270
2.
10.
Methyl bromide; Bromo-
methane
74-83-9
Methane, bromo-
8010
8240
20.
10.
Methyl chloride; Chloro-
methane
74-87-3
Methane, chloro-
8010
8240
1.
10.
3-Methylcholanthrene
56-49-5
Benz[j]aceanthrylene, 1,2-
dihydro-3-methyl-
8270
10.
Methylene bromide; Di-
bromomethane
74-95-3
Methane, dibromo-
8010
8240
15.
5.
Methylene chloride; Di-
chloromethane
75-09-2
Methane, dichloro-
8010
8240
5.
5.
216
Methyl ethyl ketone; MEK
78-93-3
2-Butanone
8015
8240
10.
100.
Methyl iodide;
Iodomethane
74-88-4
Methane, iodo-
8010
8240
40.
5.
Methyl methacrylate
80-62-6
2-Propenoic acid, 2-
methyl-, methyl ester
8015
8240
2.
5.
Methyl methanesulfonate
66-27-3
Methanesulfonic acid,
methyl ester
8270
10.
2-Methylnaphthalene
91-57-6
Naphthylene, 2-methyl-
8270
10.
Methyl parathion;
Parathion methyl
298-00-0
Phosphorothioic acid, O,O-
dimethyl O-(4-nitrophenyl)
ester
8140
8270
0.5
10.
4-Methyl-2-pentanone;
Methyl isobutyl ketone
108-10-1
2-Pentanone, 4-methyl-
8015
8240
5.
50.
Naphthalene
91-20-3
Naphthalene
8100
8270
200.
10.
1,4-Naphthoquinone
130-15-4
1,4-Naphthalenedione
8270
10.
1-Naphthylamine
134-32-7
1-Naphthalenamine
8270
10.
2-Naphthylamine
91-59-8
2-Naphthalenamine
8270
10.
Nickel
(Total)
Nickel
6010
7520
50.
400.
o-Nitroaniline
88-74-4
Benzenamine, 2-nitro-
8270
50.
m-Nitroaniline
99-09-2
Benzenamine, 3-nitro-
8270
50.
p-Nitroaniline
100-01-6
Benzenamine, 4-nitro-
8270
50.
Nitrobenzene
98-95-3
Benzene, nitro-
8090
8270
40.
10.
o-Nitrophenol
88-75-5
Phenol, 2-nitro-
8040
8270
5.
10.
217
p-Nitrophenol
100-02-7
Phenol, 4-nitro-
8040
8270
10.
50.
4-Nitroquinoline 1-oxide
56-57-5
Quinoline, 4-nitro-, 1-
oxide
8270
10.
N-Nitrosodi-n-butylamine
924-16-3
1-Butanamine, N-butyl-N-
nitroso-
8270
10.
N-Nitrosodiethylamine
55-18-5
Ethanamine, N-ethyl-N-
nitroso-
8270
10.
N-Nitrosodimethylamine
62-75-9
Methanamine, N-methyl-
N-nitroso-
8270
10.
N-Nitrosodiphenylamine
86-30-6
Benzenamine, N-nitroso-N-
phenyl-
8270
10.
N-Nitrosodipropylamine;
Di-n-propylnitrosamine
621-64-7
1-Propanamine, N-nitroso-
N-propyl-
8270
10.
N-Nitrosomethylethylamine
10595-95-6
Ethanamine, N-methyl-N-
nitroso-
8270
10.
N-Nitrosomorpholine
59-89-2
Morpholine, 4-nitroso-
8270
10.
N-Nitrosopiperidene
100-75-4
Piperidene, 1-nitroso-
8270
10.
N-Nitrosopyrrolidine
930-55-2
Pyrrolidine, 1-nitroso-
8270
10.
5-Nitro-o-toluidine
99-55-8
Benzenamine, 2-methyl-5-
nitro-
8270
10.
Parathion
56-38-2
Phosphorothioic acid, O,O-
diethyl-O-(4-nitrophenyl)
ester
8270
10.
Polychlorinated biphenyls;
PCBs
See (g)
1,1'-Biphenyl, chloro
derivatives
8080
8250
50.
100.
Polychlorinated dibenzo-p-
dioxins; PCDDs
See (h)
Dibenzo[b,e][1,4]dioxin,
chloro derivatives
8280
0.01
218
Polychlorinated di-
benzofurans; PCDFs
See (i)
Bibenzofuran, chloro
derivatives
8280
0.01
Pentachlorobenzene
608-93-5
Benzene, pentachloro-
8270
10.
Pentachloroethane
76-01-7
Ethane, pentachloro-
8240
8270
5.
10.
Pentachloronitrobenzene
82-68-8
Benzene, pentachloronitro-
8270
10.
Pentachlorophenol
87-86-5
Phenol, pentachloro-
8040
8270
5.
50.
Phenacetin
62-44-2
Acetamide, N-(4-ethoxy-
phenyl)
8270
10.
Phenanthrene
85-01-8
Phenanthrene
8100
8270
200.
10.
Phenol
108-95-2
Phenol
8040
8270
1.
10.
p-Phenylenediamine
106-50-3
1,4-Benzenediamine
8270
10.
Phorate
298-02-2
Phosphorodithioic acid,
O,O-diethyl S-[(ethylthio)-
methyl] ester
8140
8270
2.
10.
2-Picoline
109-06-8
Pyridine, 2-methyl-
8240
8270
5.
10.
Pronamide
23950-58-5
Benzamide, 3,5-dichloro-
N-(1,1-dimethyl-2-
propenyl)-
8270
10.
Propionitrile; Ethyl cyanide
107-12-0
Propanenitrile
8015
8240
60.
5.
Pyrene
129-00-0
Pyrene
8100
8270
200.
10.
Pyridine
110-86-1
Pyridine
8240
8270
5.
10.
219
Safrole
94-59-7
1,3-Benzodioxole, 5-(2-
propenyl)-
8270
10.
Selenium
(Total)
Selenium
6010
7740
7741
750.
20.
20.
Silver
(Total)
Silver
6010
7760
70.
100.
Silvex; 2,4,5-TP
93-72-1
Propanoic acid, 2-(2,4,5-
trichlorophenoxy)-
8150
2.
Styrene
100-42-5
Benzene, ethenyl-
8020
8240
1.
5.
Sulfide
18496-25-8
Sulfide
9030
10000.
2,4,5-T; 2,4,5-Trichloro-
phenoxyacetic acid
93-76-5
Acetic acid, (2,4,5-tri-
chlorophenoxy)-
8150
2.
2,3,7,8-TCDD; 2,3,7,8-
Tetrachlorodibenzo-p-
dioxin
1746-01-8
Dibenzo[b,e][1,4]dioxin,
2,3,7,8-tetrachloro-
8280
0.005
1,2,4,5-Tetrachlorobenzene
95-94-3
Benzene, 1,2,4,5-tetra-
chloro-
8270
10.
1,1,1,2-Tetrachloroethane
630-20-6
Ethane, 1,1,1,2-tetra-
chloro-
8010
8240
5.
5.
1,1,2,2,-Tetrachloroethane
79-34-5
Ethane, 1,1,2,2-tetra-
chloro-
8010
8240
0.5
5.
Tetrachloroethylene;
Perchloroethylene; Tetra-
chloroethene
127-18-4
Ethene, tetrachloro-
8010
8240
0.5
5.
2,3,4,6-Tetrachlorophenol
58-90-2
Phenol, 2,3,4,6-tetra-
chloro-
8270
10.
Tetraethyl dithiopyro-
phosphate; Sulfotepp
3689-24-5
Thiodiphosphoric acid
([(HO)2P(S)]2O), tetra-
ethyl ester
8270
10.
220
Thallium
(Total)
Thallium
6010
7840
7841
400.
1000.
10.
Tin
(Total)
Tin
7870
8000.
Toluene
108-88-3
Benzene, methyl-
8020
8240
2.
5.
o-Toluidine
95-53-4
Benzenamine, 2-methyl-
8270
10.
Toxaphene
8001-35-2
Toxaphene
8080
8250
2.
10.
1,2,4-Trichlorobenzene
120-82-1
Benzene, 1,2,4-trichloro-
8270
10.
1,1,1-Trichloroethane;
Methyl chloroform
71-55-6
Ethane, 1,1,1-trichloro-
8240
5.
1,1,2-Trichloroethane
79-00-5
Ethane, 1,1,2-trichloro-
8010
8240
0.2
5.
Trichloroethylene; Tri-
chloroethene
79-01-6
Ethene, trichloro-
8010
8240
1.
5.
Trichlorofluoromethane
75-69-4
Methane, trichlorofluoro-
8010
8240
10.
5.
2,4,5-Trichlorophenol
95-96-4
Phenol, 2,4,5-trichloro-
8270
10.
2,4,6-Trichlorophenol
88-06-2
Phenol, 2,4,6-trichloro-
8040
8270
5.
10.
1,2,3-Trichloropropane
96-18-4
Propane, 1,2,3-trichloro-
8010
8240
10.
5.
O,O,O-Triethyl
phosphorothioate
126-68-1
Phosphorothioic acid,
O,O,O-triethyl ester
8270
10.
sym-Trinitrobenzene
99-35-4
Benzene, 1,3,5-trinitro-
8270
10.
Vanadium
(Total)
Vanadium
6010
7910
7911
80.
2000.
40.
221
Vinyl acetate
108-05-4
Acetic acid, ethenyl ester
8240
5.
Vinyl chloride
75-01-4
Ethene, chloro-
8010
8240
2.
10.
Xylene (total)
1330-20-7
Benzene, dimethyl-
8020
8240
5.
5.
Zinc
(Total)
Zinc
6010
7950
20.
50.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 725
INTERIM STATUS STANDARDS FOR OWNERS AND OPERATORS OF
HAZARDOUS WASTE TREATMENT, STORAGE, AND DISPOSAL
FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
725.101
Purpose, Scope and Applicability
725.104
Imminent Hazard Action
SUBPART B: GENERAL FACILITY STANDARDS
Section
725.110
Applicability
725.111
USEPA Identification Number
725.112
Required Notices
725.113
General Waste Analysis
725.114
Security
725.115
General Inspection Requirements
725.116
Personnel Training
725.117
General Requirements for Ignitable, Reactive, or Incompatible Wastes
725.118
Location Standards
725.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
725.130
Applicability
222
725.131
Maintenance and Operation of Facility
725.132
Required Equipment
725.133
Testing and Maintenance of Equipment
725.134
Access to Communications or Alarm System
725.135
Required Aisle Space
725.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
725.150
Applicability
725.151
Purpose and Implementation of Contingency Plan
725.152
Content of Contingency Plan
725.153
Copies of Contingency Plan
725.154
Amendment of Contingency Plan
725.155
Emergency Coordinator
725.156
Emergency Procedures
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND
REPORTING
Section
725.170
Applicability
725.171
Use of Manifest System
725.172
Manifest Discrepancies
725.173
Operating Record
725.174
Availability, Retention and Disposition of Records
725.175
Annual Report
725.176
Unmanifested Waste Report
725.177
Additional Reports
SUBPART F: GROUNDWATER MONITORING
Section
725.190
Applicability
725.191
Groundwater Monitoring System
725.192
Sampling and Analysis
725.193
Preparation, Evaluation and Response
725.194
Recordkeeping and Reporting
SUBPART G: CLOSURE AND POST-CLOSURE
Section
725.210
Applicability
725.211
Closure Performance Standard
725.212
Closure Plan; Amendment of Plan
725.213
Closure; Time Allowed for Closure
725.214
Disposal or Decontamination of Equipment, Structures and Soils
725.215
Certification of Closure
223
725.216
Survey Plat
725.217
Post-closure Care and Use of Property
725.218
Post-closure Plan; Amendment of Plan
725.219
Post-Closure Notices
725.220
Certification of Completion of Post-Closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
725.240
Applicability
725.241
Definitions of Terms as Used in this Subpart
725.242
Cost Estimate for Closure
725.243
Financial Assurance for Closure
725.244
Cost Estimate for Post-closure Care
725.245
Financial Assurance for Post-closure Monitoring and Maintenance
725.246
Use of a Mechanism for Financial Assurance of Both Closure and Post-closure
Care
725.247
Liability Requirements
725.248
Incapacity of Owners or Operators, Guarantors or Financial Institutions
725.251
Promulgation of Forms (Repealed)
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
725.270
Applicability
725.271
Condition of Containers
725.272
Compatibility of Waste with Container
725.273
Management of Containers
725.274
Inspections
725.276
Special Requirements for Ignitable or Reactive Waste
725.277
Special Requirements for Incompatible Wastes
725.278
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
725.290
Applicability
725.291
Assessment of Existing Tank System’s Integrity
725.292
Design and Installation of New Tank Systems or Components
725.293
Containment and Detection of Releases
725.294
General Operating Requirements
725.295
Inspections
725.296
Response to leaks or spills and disposition of Tank Systems
725.297
Closure and Post-Closure Care
725.298
Special Requirements for Ignitable or Reactive Waste
725.299
Special Requirements for Incompatible Wastes
725.300
Waste Analysis and Trial Tests
725.301
Generators of 100 to 1000 kg/mo Kilograms of Hazardous Waste Per Month
224
725.302
Air Emission Standards
SUBPART K: SURFACE IMPOUNDMENTS
Section
725.320
Applicability
725.321
Design and Operating Requirements
725.322
Action Leakage Rate
725.323
Response Actions
725.324
Containment System
725.325
Waste Analysis and Trial Tests
725.326
Monitoring and Inspections
725.328
Closure and Post-closure Care
725.329
Special Requirements for Ignitable or Reactive Waste
725.330
Special Requirements for Incompatible Wastes
725.331
Air Emission Standards
SUBPART L: WASTE PILES
Section
725.350
Applicability
725.351
Protection from Wind
725.352
Waste Analysis
725.353
Containment
725.354
Design and Operating Requirements
725.355
Action Leakage Rates
725.356
Special Requirements for Ignitable or Reactive Waste
725.357
Special Requirements for Incompatible Wastes
725.358
Closure and Post-closure Care
725.359
Response Actions
725.360
Monitoring and Inspection
SUBPART M: LAND TREATMENT
Section
725.370
Applicability
725.372
General Operating Requirements
725.373
Waste Analysis
725.376
Food Chain Crops
725.378
Unsaturated Zone (Zone of Aeration) Monitoring
725.379
Recordkeeping
725.380
Closure and Post-closure
725.381
Special Requirements for Ignitable or Reactive Waste
725.382
Special Requirements for Incompatible Wastes
SUBPART N: LANDFILLS
Section
725.400
Applicability
225
725.401
Design Requirements
725.402
Action Leakage Rate
725.403
Response Actions
725.404
Monitoring and Inspection
725.409
Surveying and Recordkeeping
725.410
Closure and Post-closure
725.412
Special Requirements for Ignitable or Reactive Waste
725.413
Special Requirements for Incompatible Wastes
725.414
Special Requirements for Liquid Wastes
725.415
Special Requirements for Containers
725.416
Disposal of Small Containers of Hazardous Waste in Overpacked Drums (Lab
Packs)
SUBPART O: INCINERATORS
Section
725.440
Applicability
725.441
Waste Analysis
725.445
General Operating Requirements
725.447
Monitoring and Inspection
725.451
Closure
725.452
Interim Status Incinerators Burning Particular Hazardous Wastes
SUBPART P: THERMAL TREATMENT
Section
725.470
Other Thermal Treatment
725.473
General Operating Requirements
725.475
Waste Analysis
725.477
Monitoring and Inspections
725.481
Closure
725.482
Open Burning; Waste Explosives
725.483
Interim Status Thermal Treatment Devices Burning Particular Hazardous Waste
SUBPART Q: CHEMICAL, PHYSICAL AND BIOLOGICAL TREATMENT
Section
725.500
Applicability
725.501
General Operating Requirements
725.502
Waste Analysis and Trial Tests
725.503
Inspections
725.504
Closure
725.505
Special Requirements for Ignitable or Reactive Waste
725.506
Special Requirements for Incompatible Wastes
SUBPART R: UNDERGROUND INJECTION
Section
725.530
Applicability
226
SUBPART W: DRIP PADS
Section
725.540
Applicability
725.541
Assessment of existing drip pad integrity
725.542
Design and installation of new drip pads
725.543
Design and operating requirements
725.544
Inspections
725.545
Closure
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
725.930
Applicability
725.931
Definitions
725.932
Standards: Process Vents
725.933
Standards: Closed-ventVent Systems and Control Devices
725.934
Test methods and procedures
725.935
Recordkeeping Requirements
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
725.950
Applicability
725.951
Definitions
725.952
Standards: Pumps in Light Liquid Service
725.953
Standards: Compressors
725.954
Standards: Pressure Relief Devices in Gas/Vapor Service
725.955
Standards: Sampling Connecting Systems
725.956
Standards: Open-ended Valves or Lines
725.957
Standards: Valves in Gas/Vapor or Light Liquid Service
725.958
Standards: Pumps, Valves, Pressure Relief Devices, Flanges and other
Connectors
725.959
Standards: Delay of Repair
725.960
Standards: Closed-vent Systems and Control Devices
725.961
Percent Leakage Alternative for Valves
725.962
Skip Period Alternative for Valves
725.963
Test Methods and Procedures
725.964
Recordkeeping Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section
725.980
Applicability
725.981
Definitions
725.982
Schedule for Implementation of Air Emission Standards
725.983
Standards: General
227
725.984
Waste Determination Procedures
725.985
Standards: Tanks
725.986
Standards: Surface Impoundments
725.987
Standards: Containers
725.988
Standards: Closed-ventVent Systems and Control Devices
725.989
Inspection and Monitoring Requirements
725.990
Recordkeeping Requirements
725.991
Alternative Tank Emission Control Requirements (Repealed)
SUBPART DD: CONTAINMENT BUILDINGS
Section
725.1100
Applicability
725.1101
Design and operating standards
725.1102
Closure and Post Closure-Care
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section
725.1200 Applicability
725.1201 Design and Operating Standards
725.1202 Closure and Post-Closure Care
725.Appendix A
Recordkeeping Instructions
725.Appendix B
EPA Report Form and Instructions (Repealed)
725.Appendix C
EPA Interim Primary Drinking Water Standards
725.Appendix D
Tests for Significance
725.Appendix E
Examples of Potentially Incompatible Waste
725.Appendix F
Compounds With Henry’s Law Constant Less Than 0.1 Y/X (at 25°C)
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17, 1982; amended and codified
in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828, effective May 17, 1982; amended in R82-18, 51 PCB 831, at 7 Ill.
Reg. 2518, effective February 22, 1983; amended in R82-19, 53 PCB 131, at 7 Ill. Reg. 14034, effective October
12, 1983; amended in R84-9, at 9 Ill. Reg. 11869, effective July 24, 1985; amended in R85-22 at 10 Ill. Reg.
1085, effective January 2, 1986; amended in R86-1 at 10 Ill. Reg. 14069, effective August 12, 1986; amended in
R86-28 at 11 Ill. Reg. 6044, effective March 24, 1987; amended in R86-46 at 11 Ill. Reg. 13489, effective
August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19338, effective November 10, 1987; amended in R87-26 at 12
Ill. Reg. 2485, effective January 15, 1988; amended in R87-39 at 12 Ill. Reg. 13027, effective July 29, 1988;
amended in R88-16 at 13 Ill. Reg. 437, effective December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18354,
effective November 13, 1989; amended in R90-2 at 14 Ill. Reg. 14447, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16498, effective September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9398, effective
June 17, 1991; amended in R91-1 at 15 Ill. Reg. 14534, effective October 1, 1991; amended in R91-13 at 16 Ill.
Reg. 9578, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17672, effective November 6, 1992; amended
in R92-10 at 17 Ill. Reg. 5681, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20620, effective
November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6771, effective April 26, 1994; amended in R94-7 at 18
228
Ill. Reg. 12190, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17548, effective November 23, 1994;
amended in R95-6 at 19 Ill. Reg. 9566, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11078,
effective August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 369, effective December 16, 1997;
amended in R98-12 at 22 Ill. Reg. 7620, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill.
Reg. ________, effective ______________________.
SUBPART A: GENERAL PROVISIONS
Section 725.101
Purpose, Scope and Applicability
a)
The purpose of this Part is to establish minimum standards that define the
acceptable management of hazardous waste during the period of interim status
and until certification of final closure or, if the facility is subject to post-closure
requirements, until post-closure responsibilities are fulfilled.
b)
Except as provided in Section 725.980(b), the standards in this Part and 35 Ill.
Adm. Code 724.652 and 724.653 apply to owners and operators of facilities
that treat, store, or dispose of hazardous waste that have fully complied with the
requirements for interim status under Section 3005(e) of the Resource
Conservation and Recovery Act (RCRA) (42 U.S.C. 6901 et seq.) and 35 Ill.
Adm. Code 703, until either a permit is issued under Section 3005 of the
Resource Conservation and Recovery Act or Section 21(f) of the Environmental
Protection Act, or until applicable closure and post-closure responsibilities
under this Part are fulfilled, and to those owners and operators of facilities in
existence on November 19, 1980, that have failed to provide timely notification
as required by Section 3010(a) of RCRA or that have failed to file Part A of the
Permit Application, as required by 40 CFR 270.10(e) and (g) or 35 Ill. Adm.
Code 703.150 and 703.152. These standards apply to all treatment, storage, or
disposal of hazardous waste at these facilities after November 19, 1980, except
as specifically provided otherwise in this Part or 35 Ill. Adm. Code 721.
BOARD NOTE: As stated in Section 3005(a) of RCRA, after the effective date
of regulations under that Section (i.e., 40 CFR 270 and 124) the treatment,
storage, or disposal of hazardous waste is prohibited except in accordance with
a permit. Section 3005(e) of RCRA provides for the continued operation of an
existing facility that meets certain conditions until final administrative
disposition of the owner’s and operator’s permit application is made. 35 Ill.
Adm. Code 703.140 et seq. provide that a permit is deemed issued under
Section 21(f)(1) of the Environmental Protection Act under conditions similar to
federal interim status.
c)
The requirements of this Part do not apply to:
229
1)
A person disposing of hazardous waste by means of ocean disposal
subject to a permit issued under the Marine Protection, Research and
Sanctuaries Act (16 U.S.C. 1431-1434; 33 U.S.C. 1401);
BOARD NOTE: This Part applies to the treatment or storage of
hazardous waste before it is loaded into an ocean vessel for incineration
or disposal at sea, as provided in subsection (b) above of this Section.
2) This subsection corresponds with 40 CFR 265.1(c)(2), marked
“reserved” by USEPA. This statement maintains structural consistency
with USEPA rules;
3)
The owner or operator of a POTW (publicly owned treatment works)
that treats, stores or disposes of hazardous waste;
BOARD NOTE: The owner or operator of a facility under subsections
(c)(1) throughand (c)(3) is subject to the requirements of 35 Ill. Adm.
Code 724 to the extent they are included in a permit by rule granted to
such a person under 35 Ill. Adm. Code 702 and 703 or are required by
35 Ill. Adm. Code 704.Subpart F.
4) This subsection corresponds with 40 CFR 265.1(c)(4), which pertains
exclusively to the applicability of the federal regulations in authorized
states. There is no need for a parallel provision in the Illinois
regulations. This statement maintains structural consistency with
USEPA rules;
5)
The owner or operator of a facility permitted, licensed, or registered by
Illinois to manage municipal or industrial solid waste, if the only
hazardous waste the facility treats, stores, or disposes of is excluded
from regulation under this Part by 35 Ill. Adm. Code 721.105;
6)
The owner or operator of a facility managing recyclable materials
described in 35 Ill. Adm. Code 721.106(a)(2) through (a)(4), except to
the extent that requirements of this Part are referred to in 35 Ill. Adm.
Code 726.Subparts C, F, G, or H or 35 Ill. Adm. Code 739;
7)
A generator accumulating waste on-site in compliance with 35 Ill. Adm.
Code 722.134, except to the extent the requirements are included in 35
Ill. Adm. Code 722.134;
8)
A farmer disposing of waste pesticides from the farmer’s own use in
compliance with 35 Ill. Adm. Code 722.170;
230
9)
The owner or operator of a totally enclosed treatment facility, as defined
in 35 Ill. Adm. Code 720.110;
10)
The owner or operator of an elementary neutralization unit or a
wastewater treatment unit as defined in 35 Ill. Adm. Code 720.110,
provided that if the owner or operator is diluting hazardous ignitable
(D001) wastes (other than the D001 High TOC Subcategory defined in
35 Ill. Adm. Code 728.Table T) or reactive (D003) waste in order to
remove the characteristic before land disposal, the owner or operator
must comply with the requirements set out in Section 725.117(b);
11)
Immediate response:
A)
Except as provided in subsection (c)(11)(B) below of this Section,
a person engaged in treatment or containment activities during
immediate response to any of the following situations:
i)
A discharge of a hazardous waste;
ii)
An imminent and substantial threat of a discharge of a
hazardous waste;
iii)
A discharge of a material that becomes a hazardous waste
when discharged.; or
iv) An immediate threat to human health, public safety,
property, or the environment from the known or suspected
presence of military munitions, other explosive material,
or an explosive device, as determined by an explosives or
munitions emergency response specialist as defined in 35
Ill. Adm. Code 720.110.
B)
An owner or operator of a facility otherwise regulated by this
Part must comply with all applicable requirements of
725.Subparts C and D.
C)
Any person that is covered by subsection (c)(11)(A) above of this
Section that continues or initiates hazardous waste treatment or
containment activities after the immediate response is over is
subject to all applicable requirements of this Part and 35 Ill.
Adm. Code 702, 703, and 705 for those activities;
D) In the case of an explosives or munitions emergency response, if
a federal, state, or local official acting within the scope of his or
her official responsibilities or an explosives or munitions
231
emergency response specialist determines that immediate removal
of the material or waste is necessary to protect human health or
the environment, that official or specialist may authorize the
removal of the material or waste by transporters who do not have
USEPA identification numbers and without the preparation of a
manifest. In the case of emergencies involving military
munitions, the responding military emergency response
specialist's organizational unit shall retain records for three years
identifying the dates of the response, the responsible persons
responding, the type and description of material addressed, and
its disposition;
12)
A transporter storing manifested shipments of hazardous waste in
containers meeting the requirements of 35 Ill. Adm. Code 722.130 at a
transfer facility for a period of ten days or less;
13)
The addition of absorbent material to waste in a container (as defined in
35 Ill. Adm. Code 720.110) or the addition of waste to the absorbent
material in a container, provided that these actions occur at the time that
the waste is first placed in the containers and Sections 725.117(b),
725.271, and 725.272 are complied with;
14)
A universal waste handler or universal waste transporter (as defined in
35 Ill. Adm. Code 720.110) that handles any of the wastes listed below
is subject to regulation under 35 Ill. Adm. Code 733 when handling the
following universal wastes:
A)
Batteries, as described in 35 Ill. Adm. Code 733.102;
B)
Pesticides, as described in 35 Ill. Adm. Code 733.103;
C)
Thermostats, as described in 35 Ill. Adm. Code 733.104 and; and
D)
Mercury-containing lamps, as described in 35 Ill. Adm. Code
733.107.
BOARD NOTE: Subsection (c)(14)(D) of this Section was added
pursuant to Section 22.23a of the Act [415 ILCS 5/22.23a] (see
P.A. 90-502, effective August 19, 1997).
d)
The following hazardous wastes must not be managed at facilities subject to
regulation under this Part: hazardous waste numbers F020, F021, F022, F023,
F026, or F027 unless:
1)
The wastewater treatment sludge is generated in a surface impoundment
as part of the plant’s wastewater treatment system;
232
2)
The waste is stored in tanks or containers;
3)
The waste is stored or treated in waste piles that meet the requirements
of 35 Ill. Adm. Code 724.350(c) and all other applicable requirements
of 725.Subpart L;
4)
The waste is burned in incinerators that are certified pursuant to the
standards and procedures in Section 725.452; or
5)
The waste is burned in facilities that thermally treat the waste in a device
other than an incinerator and that are certified pursuant to the standards
and procedures in Section 725.483.
e)
This Part applies to owners and operators of facilities that treat, store, or
dispose of hazardous wastes referred to in 35 Ill. Adm. Code 728, and the 35
Ill. Adm. Code 728 standards are considered material conditions or
requirements of the interim status standards of this Part.
f) 35 Ill. Adm. Code 726.505 identifies when the requirements of this Part apply
to the storage of military munitions classified as solid waste under 35 Ill. Adm.
Code 726.302. The treatment and disposal of hazardous waste military
munitions are subject to the applicable permitting, procedural, and technical
standards in 35 Ill. Adm. Code 702, 703, 705, 720 through 726, and 728.
fg)
Other bodies of regulations may apply a person, facility, or activity, such as 35
Ill. Adm. Code 809 (special waste hauling), 35 Ill. Adm. Code 807 or 810
through 817 (solid waste landfills), 35 Ill. Adm. Code 848 or 849 (used and
scrap tires), or 35 Ill. Adm. Code 1420 through 1422 (potentially infectious
medical waste), depending on the provisions of those other regulations.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART B: GENERAL FACILITY STANDARDS
Section 725.112
Required Notices
a)
Receipt from a foreign source.
1)
The owner or operator of a facility that has arranged to receive
hazardous waste from a foreign source must notify the Regional
Administrator in writing at least four weeks in advance of the date the
waste is expected to arrive at the facility. Notice of subsequent
233
shipments of the same waste from the same foreign source is not
required.
2)
The owner or operator of a recovery facility that has arranged to receive
hazardous waste subject to 35 Ill. Adm. Code 722.Subpart H must
provide a copy of the tracking document bearing all required signatures
to the notifier, to the Office of Enforcement and Compliance Assurance,
Office of Compliance, Enforcement Planning, Targeting and Data
Division (2222A), Environmental Protection Agency, 401 M St., SW,
Washington, DC 20460; to the Bureau of Land, Division of Land
Pollution Control, Illinois Environmental Protection Agency, P.O. Box
19276, Springfield, IL 62794-9276; and to the competent authorities of
all other concerned countries within three working days of receipt of the
shipment. The original of the signed tracking document must be
maintained at the facility for at least three years.
b)
Before transferring ownership or operation of a facility during its operating life,
or of a disposal facility during the post-closure care period, the owner or
operator must notify the new owner or operator in writing of the requirements
of this Part and 35 Ill. Adm. Code 702 and 703 (Aalso see 40 35 Ill. Adm.
Code 703.155).
BOARD NOTE: An owner’s or operator’s failure to notify the new owner or
operator of the requirements of this Part in no way relieves the new owner or
operator of his obligation to comply with all applicable requirements.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.113
General Waste Analysis
a)
Waste analysis:
1)
Before an owner or operator treats, stores, or disposes of any hazardous
wastes, or non-hazardous wastes if applicable under Section 725.213(d),
the owner or operator shall obtain a detailed chemical and physical
analysis of a representative sample of the wastes. At a minimum, the
analysis must contain all the information that must be known to treat,
store, or dispose of the waste in accordance with this Part and 35 Ill.
Adm. Code 728.
2)
The analysis may include data developed under 35 Ill. Adm. Code 721
and existing published or documented data on the hazardous waste or on
waste generated from similar processes.
234
BOARD NOTE: For example, the facility’s record of analyses
performed on the waste before the effective date of these regulations or
studies conducted on hazardous waste generated from processes similar
to that which generated the waste to be managed at the facility may be
included in the data base required to comply with subsection (a)(1) of
this Section, except as otherwise specified in 35 Ill. Adm. Code
728.107(b) and (c). The owner or operator of an off-site facility may
arrange for the generator of the hazardous waste to supply part or all of
the information required by subsection (a)(1) of this Section. If the
generator does not supply the information and the owner or operator
chooses to accept a hazardous waste, the owner or operator is
responsible for obtaining the information required to comply with this
Section.
3)
The analysis must be repeated as necessary to ensure that it is accurate
and up to date. At a minimum, the analysis must be repeated:
A)
When the owner or operator is notified or has reason to believe
that the process or operation generating the hazardous waste, or
non-hazardous waste if applicable under Section 725.213(d), has
changed; and
B)
For off-site facilities, when the results of the inspection required
in subsection (a)(4) of this Section indicate that the hazardous
waste received at the facility does not match the waste designated
on the accompanying manifest or shipping paper.
4)
The owner or operator of an off-site facility shall inspect and, if
necessary, analyze each hazardous waste movement received at the
facility to determine whether it matches the identity of the waste
specified on the accompanying manifest or shipping paper.
b)
The owner or operator shall develop and follow a written waste analysis plan
that describes the procedures that the owner or operator will carry out to comply
with subsection (a) of this Section. The owner or operator shall keep this plan
at the facility. At a minimum, the plan must specify:
1)
The parameters for which each hazardous waste, or non-hazardous waste
if applicable under Section 725.213(d), will be analyzed and the
rationale for the selection of these parameters (i.e., how analysis for
these parameters will provide sufficient information on the waste’s
properties to comply with subsection (a) of this Section.
2)
The test methods that will be used to test for these parameters.
235
3)
The sampling method that will be used to obtain a representative sample
of the waste to be analyzed. A representative sample may be obtained
using either:
A)
One of the sampling methods described in 35 Ill. Adm. Code
721.Appendix A, or
B)
An equivalent sampling method.
BOARD NOTE: See 35 Ill. Adm. Code 720.120(c) for related
discussion.
4)
The frequency with which the initial analysis of the waste will be
reviewed or repeated to ensure that the analysis is accurate and up-to-
date.
5)
For off-site facilities, the waste analyses that hazardous waste generators
have agreed to supply.
6)
Where applicable, the methods that will be used to meet the additional
waste analysis requirements for specific waste management methods, as
specified in Sections 725.300, 725.325, 725.352, 725.373, 725.414,
725.441, 725.475, 725.502, 725.934(d), 725.963(d), and 725.984, and
35 Ill. Adm. Code 728.107.
7)
For surface impoundments exempted from land disposal restrictions
under 35 Ill. Adm. Code 728.104(a), the procedures and schedules for:
A)
The sampling of impoundment contents;
B)
The analysis of test data; and
C)
The annual removal of residues that are not delisted under 35 Ill.
Adm. Code 720.122 or that exhibit a characteristic of hazardous
waste and either:
i)
Do not meet the applicable treatment standards of 35 Ill.
Adm. Code 728.Subpart D, or
ii)
Where no treatment standards have been established:
Such residues are prohibited from land disposal under 35
Ill. Adm. Code 728.132 or 728.139.
8)
For owners and operators seeking an exemption to the air emission
standards of 724.Subpart CC in accordance with Section 725.983:
236
A)
If direct measurement is used for the waste determination, the
procedures and schedules for waste sampling and analysis, and
the analysis of test data to verify the exemption.
B)
If knowledge of the waste is used for the waste determination,
any information prepared by the facility owner or operator, or by
the generator of the waste if the waste is received form from off-
site, that is used as the basis for knowledge of the waste.
c)
For off-site facilities, the waste analysis plan required in subsection (b) of this
Section must also specify the procedures that will be used to inspect and, if
necessary, analyze each movement of hazardous waste received at the facility to
ensure that it matches the identity of the waste designated on the accompanying
manifest or shipping paper. At a minimum, the plan must describe:
1)
The procedures that will be used to determine the identity of each
movement of waste managed at the facility; and
2)
The sampling method that will be used to obtain a representative sample
of the waste to be identified if the identification method includes
sampling.; and
3)
The procedures that the owner or operator of an off-site landfill
receiving containerized hazardous waste will use to determine whether a
hazardous waste generator or treater has added a biodegradable sorbent
to the waste in the container.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 725.170
Applicability
The regulations in this subpart apply to owners and operators of both on-site and off-site
facilities, except as Section 725.101 provides otherwise. Sections 725.171, 725.172 and
725.176 do not apply to owners and operators of on-site facilities that do not receive any
hazardous waste from off-site sources, nor do they apply to owners and operators of off-site
facilities with respect to waste military munitions exempted from manifest requirements under
35 Ill. Adm. Code 726.303(a).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
237
Section 725.171
Use of Manifest System
a)
If a facility receives hazardous waste accompanied by a manifest, the owner or
operator or his agent must:
1)
Sign and date each copy of the manifest to certify that the hazardous
waste covered by the manifest was received;
2)
Note any significant discrepancies in the manifest, as defined in Section
725.172(a), on each copy of the manifest;
BOARD NOTE: An owner or operator of a facility whose procedures
under Section 725.113(c) include waste analysis need not perform that
analysis before signing the manifest and giving it to the transporter.
Section 725.172(b), however, requires the owner or operator to report
any unreconciled discrepancy discovered during later analysis.
3)
Immediately give the transporter at least one copy of the signed
manifest;
4)
Send a copy of the manifest to each of the generator and the Agency
within 30 days of the date of delivery; and
5)
Retain at the facility a copy of each manifest for at least three years from
the date of delivery.
b)
If a facility receives from a rail or water (bulk shipment) transporter hazardous
waste that is accompanied by a shipping paper containing all the information
required on the manifest (excluding the USEPA identification numbers,
generator’s certification and signatures), the owner or operator or its agent
must:
1)
Sign and date each copy of the manifest or shipping paper (if the
manifest has not been received) to certify that the hazardous waste
covered by the manifest or shipping paper was received;
2)
Note any significant discrepancies, as defined in Section 725.172(a), in
the manifest or shipping paper (if the manifest has not been received) on
each copy of the manifest or shipping paper;
BOARD NOTE: The owner or operator of a facility whose procedures
under Section 725.113(c) include waste analysis need not perform that
analysis before signing the shipping paper and giving it to the
transporter. Section 725.172(b), however, requires reporting an
unreconciled discrepancy discovered during later analysis.
238
3)
Immediately give the rail or water (bulk shipment) transporter at least
one copy of the manifest or shipping paper (if the manifest has not been
received);
4)
Send a copy of the signed and dated manifest to the generator and to the
Agency within 30 days after the delivery; however, if the manifest has
not been received within 30 days after delivery, the owner or operator,
or his agent, must send a copy of the shipping paper signed and dated to
the generator; and
BOARD NOTE: 35 Ill. Adm. Code 722.123(c) requires the generator
to send three copies of the manifest to the facility when hazardous waste
is sent by rail or water (bulk shipment).
5)
Retain at the facility a copy of the manifest and shipping paper (if signed
in lieu of the manifest at the time of delivery) for at least three years
from the date of delivery.
c)
Whenever a shipment of hazardous waste is initiated from a facility, the owner
or operator of that facility must comply with the requirements of 35 Ill. Adm.
Code 722.
BOARD NOTE: The provisions of 35 Ill. Adm. Code 722.134 are applicable
to the on-site accumulation of hazardous wastes by generators. Therefore, the
provisions of 35 Ill. Adm. Code 722.134 apply only to owners or operators that
are shipping hazardous waste that they generated at that facility.
d)
Within three working days of the receipt of a shipment subject to 35 Ill. Adm.
Code 722.Subpart H, the owner or operator of the facility must provide a copy
of the tracking document bearing all required signatures to the notifier; to the
Office of Enforcement and Compliance Assurance, Office of Compliance,
Enforcement Planning, Targeting and Data Division (2222A), Environmental
Protection Agency, 401 M St., SW, Washington, DC 20460; to the Bureau of
Land, Division of Land Pollution Control, Illinois Environmental Protection
Agency, P.O. Box 19276, Springfield, IL 62794-9276; and to competent
authorities of all other concerned countries. The original copy of the tracking
document must be maintained at the facility for at least three years from the date
of signature.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
239
SUBPART J: TANK SYSTEMS
Section 725.298
Special Requirements for Ignitable or Reactive Waste
a)
Ignitable or reactive waste must not be placed in a tank system, unless:
1)
The waste is treated, rendered or mixed before or immediately after
placement in the tank system so that
A)
The resulting waste, mixture or dissolved material no longer
meets the definition of ignitable or reactive waste under 35 Ill.
Adm. Code 721.121 or 721.123 and
B)
Section 725.117(b) is complied with; or
2)
The waste is stored or treated in such a way that it is protected from any
material or conditions which may cause the waste to ignite or react; or
3)
The tank system is used solely for emergencies.
b)
The owner or operator of a facility where ignitable or reactive waste is stored or
tested in tanks shall comply with the requirements for the maintenance of
protective distances between the waste management area and any public ways,
streets, alleys or an adjoining property line that can be built upon as required in
Tables 2-1 through 2-6 of the National Fire Protection Association’s
“Flammable and Combustible Liquids Code,” NFPA 30, incorporated by
reference in 35 Ill. Adm. Code 720.111.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.301
Generators of 100 to 1000 kg/mo Kilograms of Hazardous Waste Per
Month
a)
The requirements of this Section apply to small quantity generators that generate
more than 100 kg but less than 1000 kg of hazardous waste in a calendar month,
that accumulate hazardous waste in tanks for less than 180 days (or 270 days if
the generator must ship the waste greater than 200 miles), and that do not
accumulate over 6,000 kg on-site at any time.
b)
A generator of between 100 and 1000 kg/mo hazardous waste shall comply with
the following general operating requirements:
1)
Treatment or storage of hazardous waste in tanks must comply with
Section 725.117(b);
240
2)
Hazardous wastes or treatment reagents must not be placed in a tank if
they could cause the tank or its inner liner to rupture, leak, corrode, or
otherwise fail before the end of its intended life;
3)
Uncovered tanks must be operated to ensure at least 60 centimeters (2
feet) of freeboard unless the tank is equipped with a containment
structure (e.g., dike or trench), a drainage control system, or a diversion
structure (e.g., standby tank) with a capacity that equals or exceeds the
volume of the top 60 centimeters (2 feet) of the tank; and
4)
Where hazardous waste is continuously fed into a tank, the tank must be
equipped with a means to stop this inflow (e.g., waste feed cutoff system
or by-pass system to a stand-by tank).
BOARD NOTE: These systems are intended to be used in the event of a
leak or overflow from the tank due to a system failure (e.g., a
malfunction in the treatment process, a crack in the tank, etc.).
c)
A generator of between 100 and 1000 kg/mo accumulating hazardous waste in
tanks shall inspect, where present:
1)
Discharge control equipment (e.g., waste feed cutoff systems, by-pass
systems, and drainage systems) at least once each operating day, to
ensure that it is in good working order;
2)
Data gathered from monitoring equipment (e.g., pressure and
temperature gauges) at least once each operating day to ensure that the
tank is being operated according to its design;
3)
The level of waste in the tank at least once each operating day to ensure
compliance with subsection (b)(3) above of this Section;
4)
The construction materials of the tank at least weekly to detect corrosion
or leaking of fixtures or seams; and
5)
The construction materials of and the area immediately surrounding
discharge confinement structures (e.g., dikes) at least weekly to detect
erosion or obvious signs of leakage (e.g., wet spots or dead vegetation).
BOARD NOTE: As required by Section 725.115(c), the owner or
operator must remedy any deterioration or malfunction the owner or
operator finds.
241
d)
A generator of between 100 and 1000 kg/mo accumulating hazardous waste in
tanks shall, upon closure of the facility, remove all hazardous waste from tanks,
discharge control equipment and discharge confinement structures.
BOARD NOTE: At closure, as throughout the operating period, unless the
owner or operator demonstrates, in accordance with 35 Ill. Adm. Code
721.103(d) or (e), that any solid waste removed from the tank is not a
hazardous waste, the owner or operator becomes a generator of hazardous waste
and must manage it in accordance with all applicable requirements of 35 Ill.
Adm. Code 722, 723, and 725.
e)
A generator of between 100 and 1000 kg/mo shall comply with the following
special requirements for ignitable or reactive waste:
1)
Ignitable or reactive waste must not be placed in a tank unless:
A)
The waste is treated, rendered, or mixed before or immediately
after placement in a tank so that; the following is true of the
waste:
i)
The resulting waste, mixture, or dissolution of material no
longer meets the definition of ignitable or reactive waste
under 35 Ill. Adm. Code 721.121 or 721.123, and
ii)
Section 725.117(b) is complied with;
B)
The waste is stored or treated in such a way that it is protected
from any material or conditions that may cause the waste to ignite
or react; or
C)
The tank is used solely for emergencies.
2)
The owner or operator of a facility that treats or stores ignitable or
reactive waste in covered tanks shall comply with the buffer zone
requirements for tanks contained in Tables 2-1 through 2-6 of the
National Fire Protection Association’s “Flammable and Combustible
Liquids Code,” NFPA 30, incorporated by reference in 35 Ill. Adm.
Code 720.111.
f)
A generator of between 100 and 1000 kg/mo shall comply with the following
special requirements for incompatible wastes:
1)
Incompatible wastes or incompatible wastes and materials (see Appendix
E for examples) must not be placed in the same tank unless Section
725.117(b) is complied with.
242
2)
Hazardous waste must not be placed in an unwashed tank that previously
held an incompatible waste or material unless Section 725.117(b) is
complied with.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART N: LANDFILLS
Section 725.414
Special Requirements for Liquid Wastes
a)
This subsection corresponds with 40 CFR 265.314(a), which pertains to the
placement of bulk or non-containerized liquid waste or waste containing free
liquids in a landfill prior to May 8, 1985. This statement maintains structural
consistency with USEPA rules.
b)
The placement of bulk or non-containerized liquid hazardous waste or hazardous
waste containing free liquids (whether or not sorbents have been added) in any
landfill is prohibited.
c)
Containers holding free liquids must not be placed in a landfill unless:
1)
All free-standing liquid:
A)
has been removed by decanting or other methods;
B)
has been mixed with sorbent or solidified so that free-standing
liquid is no longer observed; or
C)
has been otherwise eliminated; or
2)
The container is very small, such as an ampule; or
3)
The container is designed to hold free liquids for use other than storage,
such as a battery or capacitor; or
4)
The container is a lab pack as defined in Section 724.416 and is disposed
of in accordance with Section 724.416.
d)
To demonstrate the absence or presence of free liquids in either a containerized
or a bulk waste, the following test must be used: Method 9095 (Paint Filter
Liquids Test), as described in “Test Methods for Evaluating Solid Wastes,
Physical/Chemical Methods”, USEPA Publication No. SW-846, incorporated
by reference in 35 Ill. Adm. Code 720.111.
243
e)
The placement of any liquids that is not a hazardous waste in a landfill is
prohibited (35 Ill. Adm. Code 729.311).
f)
Sorbents used to treat free liquids to be disposed of in landfills must be
nonbiodegradable. Nonbiodegradable sorbents are: materials listed or
described in subsection (f)(1) of this Section; materials that pass one of the tests
in subsection (f)(2) of this Section; or materials that are determined by the
Board to be nonbiodegradable through the 35 Ill. Adm. Code 106 adjusted
standard process.
1)
Nonbiodegradable sorbents are:
A)
Inorganic minerals, other inorganic materials, and elemental
carbon (e.g., aluminosilicates, clays, smectites, Fuller’s earth,
bentonite, calcium bentonite, montmorillonite, calcined
montmorillonite, kaolinite, micas (illite), vermiculites, zeolites;
calcium carbonate (organic free limestone); oxides/hydroxides,
alumina, lime, silica (sand), diatomaceous earth; perlite (volcanic
glass); expanded volcanic rock; volcanic ash; cement kiln dust;
fly ash; rice hull ash; activated charcoal/activated carbon); or
B)
High molecular weight synthetic polymers (e.g., polyethylene,
high density polyethylene (HDPE), polypropylene, polystyrene,
polyurethane, polyacrylate, polynorborene, polyisobutylene,
ground synthetic rubber, cross-linked allylstyrene and tertiary
butyl copolymers). This does not include polymers derived from
biological material or polymers specifically designed to be
degradable; or
C)
Mixtures of these nonbiodegradable materials.
2)
Tests for nonbiodegradable sorbents.
A)
The sorbent material is determined to be nonbiodegradable under
ASTM Method G21-70 (1984a)--”Standard Practice for
Determining Resistance of Synthetic Polymer Materials to
Fungi”, incorporated by reference in 35 Ill. Adm. Code 720.111;
B)
The sorbent material is determined to be nonbiodegradable under
ASTM Method G22-76 (1984b)--”Standard Practice for
Determining Resistance of Plastics to Bacteria”, incorporated by
reference in 35 Ill. Adm. Code 720.111; or
244
C)
The sorbent material is determined to be non-biodegradable under
OECD test 301B (CO
2
Evolution (Modified Sturm Test)),
incorporated by reference in 35 Ill. Adm. Code 720.111.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 725.933
Standards: Closed-ventVent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control devices used to
comply with provisions of this Part shall comply with the provisions of
this Section.
2)
The owner or operator of an existing facility that cannot install a closed-
vent system and control device to comply with the provisions of this
Subpart on the effective date that the facility becomes subject to the
provisions of this Subpart shall prepare an implementation schedule that
includes dates by which the closed-vent system and control device will
be installed and in operation. The controls must be installed as soon as
possible, but the implementation schedule may allow up to 30 months
after the effective date that the facility becomes subject to this Subpart
for installation and startup. All units that begin operation after
December 21, 1990, must comply with the rules immediately (i.e., must
have control devices installed and operating on startup of the affected
unit); the 2-year implementation schedule does not apply to these units.
b)
A control device involving vapor recovery (e.g., a condenser or adsorber) must
be designed and operated to recover the organic vapors vented to it with an
efficiency of 95 weight percent or greater unless the total organic emission
limits of Section 725.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler, or process
heater) must be designed and operated to reduce the organic emissions vented to
it by 95 weight percent or greater; to achieve a total organic compound
concentration of 20 ppmv, expressed as the sum of the actual compounds, not
carbon equivalents, on a dry basis corrected to three percent oxygen; or to
provide a minimum residence time of 0.50 seconds at a minimum temperature
of 760° C. If a boiler or process heater is used as the control device, then the
vent stream must be introduced into the flame combustion zone of the boiler or
process heater.
245
d)
Flares.
1)
A flare must be designed for and operated with no visible emissions as
determined by the methods specified in subsection (e)(1) of this Section
except for periods not to exceed a total of 5 minutes during any 2
consecutive hours.
2)
A flare must be operated with a flame present at all times, as determined
by the methods specified in subsection (f)(2)(c) of this Section.
3)
A flare must be used only if the net heating value of the gas being
combusted is 11.2 MJ/scm (300 Btu/scf) or greater if the flare is steam-
assisted or air-assisted, or if the net heating value of the gas being
combusted is 7.45 MJ/scm (200 Btu/scf) or greater if the flare is
nonassisted. The net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2) of this Section.
4)
Exit Velocity.
A)
A steam-assisted or nonassisted flare must be designed for and
operated with an exit velocity, as determined by the methods
specified in subsection (e)(3) of this Section, less than 18.3 m/s
(60 ft/s), except as provided in subsections (d)(4)(B) and
(d)(4)(C) of this Section.
B)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, equal to or greater than 18.3
m/s (60 ft/s) but less than 122 m/s (400 ft/s) is allowed if the net
heating value of the gas being combusted is greater than 37.3
MJ/scm (1000 Btu/scf).
C)
A steam-assisted or nonassisted flare designed for and operated
with an exit velocity, as determined by the methods specified in
subsection (e)(3) of this Section, less than the velocity, V as
determined by the method specified in subsection (e)(4) and less
than 122 m/s (400 ft/s) is allowed.
5)
An air-assisted flare must be designed and operated with an exit velocity
less than the velocity, V as determined by the method specified in
subsection (e)(5) of this Section.
6)
A flare used to comply with this Section must be steam-assisted, air-
assisted, or nonassisted.
246
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111, must be used to determine the compliance of a
flare with the visible emission provisions of this Subpart. The
observation period is 2 hours and must be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare must be
calculated using the following equation:
T
i
i
H
= K
i
n
C
H
×
=
∑
×
1
T
i
i
i
1
n
H
= K
C
H
×
×
=
∑
Where:
H
T
is the net heating value of the sample in MJ/scm; where the
net enthalpy per mole of offgas is based on combustion at 25° C
and 760 mm Hg, but the standard temperature for determining
the volume corrersponding to 1 mole is 20° C.
K = 1.74
×
10
-7
(1/ppm)(g mol/scm)(MJ/kcal) where the standard
temperature for (g mol/scm) is 20° C.
S
Σ
X
i
means the sum of the values of X for each component i,
from i=1 to n.
C
i
is the concentration of sample component i in ppm on a wet
basis, as measured for organics by Reference Method 18 in 40
CFR 60, and for carbon monoxide, by ASTM D 1946-90,
incorporated by reference in 35 Ill. Adm. Code 720.111.
H
i
is the net heat of combustion of sample component i,
kcal/gmol at 25° C and 760 mm Hg. The heats of combustion
must be determined using ASTM D 2382-88, incorporated by
reference in 35 Ill. Adm. Code 720.111, if published values are
not available or cannot be calculated.
3)
The actual exit velocity of a flare must be determined by dividing the
volumetric flow rate (in units of standard temperature and pressure), as
247
determined by Reference Methods 2, 2A, 2C, or 2D in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111, as appropriate,
by the unobstructed (free) cross-sectional area of the flare tip.
4)
The maximum allowed velocity in m/s, V for a flare complying with
subsection (d)(4)(C) of this Section must be determined by the following
equation:
(
)
log
.
.
max
10
28 8
317
V
H
T
=
+
(
)
log
V
H
28.8
31.7
10
max
T
=
+
Where:
Log
10
log
10
means logarithm to the base 10
H
T
is the net heating value as determined in subsection (e)(2) of
this Section.
5)
The maximum allowed velocity in m/s, V for an air-assisted flare must
be determined by the following equation:
V = 8.706+0.7084H
T
V = 8.706 + 0.7084H
T
Where:
H
T
is the net heating value as determined in subsection (e)(2) of
this Section.
f)
The owner or operator shall monitor and inspect each control device required to
comply with this Section to ensure proper operation and maintenance of the
control device by implementing the following requirements:
1)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a flow indicator that provides a record of vent stream flow
from each affected process vent to the control device at least once every
hour. The flow indicator sensor must be installed in the vent stream at
the nearest feasible point to the control device inlet but before being
combined with other vent streams.
248
2)
Install, calibrate, maintain, and operate according to the manufacturer’s
specifications a device to continuously monitor control device operation
as specified below:
A)
For a thermal vapor incinerator, a temperature monitoring device
equipped with a continuous recorder. The device must have
accuracy of ±1% percent of the temperature being monitored in
° C or ± 0.5° C, whichever is greater. The temperature sensor
must be installed at a location in the combustion chamber
downstream of the combustion zone.
B)
For a catalytic vapor incinerator, a temperature monitoring
device equipped with a continuous recorder. The device must be
capable of monitoring temperature at two locations and have an
accuracy of ±1% percent of the temperature being monitored in
° C or ± 0.5° C, whichever is greater. One temperature sensor
must be installed in the vent stream at the nearest feasible point to
the catalyst bed inlet and a second temperature sensor must be
installed in the vent stream at the nearest feasible point to the
catalyst bed outlet.
C)
For a flare, a heat sensing monitoring device equipped with a
continuous recorder that indicates the continuous ignition of the
pilot flame.
D)
For a boiler or process heater having a design heat input capacity
less than 44 MW, a temperature monitoring device equipped with
a continuous recorder. The device must have an accuracy of
±1% percent of the temperature being monitored in ° C or ±
0.5° C, whichever is greater. The temperature sensor must be
installed at a location in the furnace downstream of the
combustion zone.
E)
For a boiler or process heater having a design heat input capacity
greater than or equal to 44 MW, a monitoring device equipped
with a continuous recorder to measure parameters that indicate
good combustion operating practices are being used.
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the
condenser; or
249
ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable of
monitoring temperature with an accuracy of ±1% percent
of the temperature being monitored in degrees Celsius (°
C) or ±0.5° C, whichever is greater. The temperature
sensor must be installed at a location in the exhaust vent
stream from the condenser exit (i.e., product side).
G)
For a carbon adsorption system such as a fixed-bed carbon
adsorber that regenerates the carbon bed directly in the control
device, either:
i)
A monitoring device equipped with a continuous recorder
to measure the concentration level of the organic
compounds in the exhaust vent stream from the carbon
bed; or
ii)
A monitoring device equipped with a continuous recorder
to measure a parameter that indicates the carbon bed is
regenerated on a regular, predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsections (f)(1) and (f)(2) of this Section at least once each operating
day to check control device operation and, if necessary, immediately
implement the corrective measures necessary to ensure the control device
operates in compliance with the requirements of this Section.
g)
An owner or operator using a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
at a regular, predetermined time interval that is no longer than the carbon
service life established as a requirement of Section 725.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system, such as a carbon
canister, that does not regenerate the carbon bed directly onsite in the control
device shall replace the existing carbon in the control device with fresh carbon
on a regular basis by using one of the following procedures:
1)
Monitor the concentration level of the organic compounds in the exhaust
vent stream from the carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon immediately when
carbon breakthrough is indicated. The monitoring frequency must be
daily or at an interval no greater than 20% percent of the time required
250
to consume the total carbon working capacity established as a
requirement of Section 725.935(b)(4)(C)(vii), whichever is longer.
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design carbon
replacement interval established as a requirement of Section
725.935(b)(4)(C)(vii).
i)
An owner or operator of an affected facility seeking to comply with the
provisions of this Part by using a control device other than a thermal vapor
incinerator, catalytic vapor incinerator, flare, boiler, process heater, condenser,
or carbon adsorption system is required to develop documentation including
sufficient information to describe the control device operation and identify the
process parameter or parameters that indicate proper operation and maintenance
of the control device.
j)
A closed vent closed-vent system must meet either of the following design
requirements:
1)
A closed-vent system must be designed to operate with no detectable
emissions, as indicated by an instrument reading of less than 500 ppmv
above background, as determined by the methods specified at Section
725.934(b), and by visual inspections; or
2)
A closed-vent system must be designed to operate at a pressure below
atmospheric pressure. The system must be equipped with at least one
pressure gauge or other pressure measurement device that can be read
from a readily accessible location to verify that negative pressure is
being maintained in the closed-vent system when the control device is
operating.
k)
The owner or operator shall monitor and inspect each closed-vent system
required to comply with this Section to ensure proper operation and maintenance
of the closed-vent system by implementing the following requirements:
1)
Each closed-vent system that is used to comply with subsection (j)(1) of
this Section shall be inspected and monitored in accordance with the
following requirements:
A)
An initial leak detection monitoring of the closed-vent system
shall be conducted by the owner or operator on or before the date
that the system becomes subject to this Section. The owner or
operator shall monitor the closed-vent system components and
connections using the procedures specified in Section 725.934(b)
to demonstrate that the closed-vent system operates with no
251
detectable emissions, as indicated by an instrument reading of
less than 500 ppmv above background.
B)
After initial leak detection monitoring required in subsection
(k)(1)(A) of this Section, the owner or operator shall inspect and
monitor the closed-vent system as follows:
i)
Closed-vent system joints, seams, or other connections
that are permanently or semi-permanently sealed (e.g., a
welded joint between two sections of hard piping or a
bolted and gasketed ducting flange) must be visually
inspected at least once per year to check for defects that
could result in air pollutant emissions. The owner or
operator shall monitor a component or connection using
the procedures specified in Section 725.934(b) to
demonstrate that it operates with no detectable emissions
following any time the component is repaired or replaced
(e.g., a section of damaged hard piping is replaced with
new hard piping) or the connection is unsealed (e.g., a
flange is unbolted).
ii)
Closed-vent system components or connections other than
those specified in subsection (k)(1)(B)(i) of this Section
must be monitored annually and at other times as
requested by the Regional Administrator, except as
provided for in subsection (n) of this Section, using the
procedures specified in Section 725.934(b) to demonstrate
that the components or connections operate with no
detectable emissions.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect or leak in accordance with the
requirements of subsection (k)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 725.935.
2)
Each closed-vent system that is used to comply with subsection (j)(2) of
this Section must be inspected and monitored in accordance with the
following requirements:
A)
The closed-vent system must be visually inspected by the owner
or operator to check for defects that could result in air pollutant
252
emissions. Defects include, but are not limited to, visible cracks,
holes, or gaps in ductwork or piping or loose connections.
B)
The owner or operator shall perform an initial inspection of the
closed-vent system on or before the date that the system becomes
subject to this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year.
C)
In the event that a defect or leak is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k)(3) of this Section.
D)
The owner or operator shall maintain a record of the inspection
and monitoring in accordance with the requirements specified in
Section 725.935.
3)
The owner or operator shall repair all detected defects as follows:
A)
Detectable emissions, as indicated by visual inspection or by an
instrument reading greater than 500 ppmv above background,
must be controlled as soon as practicable, but not later than 15
calendar days after the emission is detected, except as provided
for in subsection (k)(3)(C) of this Section.
B)
A first attempt at repair must be made no later than five calendar
days after the emission is detected.
C)
Delay of repair of a closed-vent system for which leaks have been
detected is allowed if the repair is technically infeasible without a
process unit shutdown, or if the owner or operator determines
that emissions resulting from immediate repair would be greater
than the fugitive emissions likely to result from delay of repair.
Repair of such equipment must be completed by the end of the
next process unit shutdown.
D)
The owner or operator shall maintain a record of the defect repair
in accordance with the requirements specified in Section 725.935.
l)
A closed-vent system or control device used to comply with provisions of this
Subpart must be operated at all times when emissions may be vented to it.
m)
The owner or operator using a carbon adsorption system to control air pollutant
emissions shall document that all carbon removed that is a hazardous waste and
that is removed from the control device is managed in one of the following
manners, regardless of the volatile organic concentration of the carbon:
253
1)
It is regenerated or reactivated in a thermal treatment unit that meets one
of the following:
A)
The owner or operator of the unit has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 724.Subpart X; or
B)
The unit is equipped with and operating air emission controls in
accordance with the applicable requirements of 725.Subparts AA
and CC or 35 Ill. Adm. Code 724; or
C)
The unit is equipped with and operating air emission controls in
accordance with a national emission standard for hazardous air
pollutants under 40 CFR 61 or 40 CFR 63.
2)
It is incinerated in a hazardous waste incinerator for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 724.Subpart O, or
B)
The owner or operator has designed and operates the incinerator
in accordance with the interim status requirements of 725.Subpart
O.
3)
It is burned in a boiler or industrial furnace for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 that implements the
requirements of 35 Ill. Adm. Code 726.Subpart H, or
B)
The owner or operator has designed and operates the boiler or
industrial furnace in accordance with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
n)
Any components of a closed-vent system that are designated, as described in
Section 725.935(c)(9), as unsafe to monitor are exempt from the requirements
of subsection (k)(1)(B)(ii) of this Section if both of the following conditions are
fulfilled:
1)
The owner or operator of the closed-vent system has determined that the
components of the closed-vent system are unsafe to monitor because
254
monitoring personnel would be exposed to an immediate danger as a
consequence of complying with subsection (k)(1)(B)(ii) of this Section;
and
2)
The owner or operator of the closed-vent system adheres to a written
plan that requires monitoring the closed-vent system components using
the procedure specified in subsection (k)(1)(B)(ii) of this Section as
frequently as practicable during safe-to-monitor times.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.934
Test Methods and Procedures
a)
Each owner or operator subject to the provisions of this Subpart shall comply
with the test methods and procedures requirements provided in this Section.
b)
When a closed-vent system is tested for compliance with no detectable
emissions, as required in Section 725.933(k), the test must comply with the
following requirements:
1)
Monitoring must comply with Reference Method 21 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The detection instrument must meet the performance criteria of
Reference Method 21.
3)
The instrument must be calibrated before use on each day of its use by
the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a concentration of
approximately, but less than, 10,000 ppm methane or n-hexane.
5)
The background level must be determined as set forth in Reference
Method 21.
6)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible, as described in Reference
Method 21.
255
7)
The arithmetic difference between the maximum concentration indicated
by the instrument and the background level is compared with 500 ppm
for determining compliance.
c)
Performance tests to determine compliance with Section 725.932(a) and with the
total organic compound concentration limit of Section 725.933(c) must comply
with the following:
1)
Performance tests to determine total organic compound concentrations
and mass flow rates entering and exiting control devices must be
conducted and data reduced in accordance with the following reference
methods and calculation procedures:
A)
Method 2 in 40 CFR 60 for velocity and volumetric flow rate.
B)
Method 18 in 40 CFR 60 for organic content.
C)
Each performance test must consist of three separate runs, each
run conducted for at least 1 hour under the conditions that exist
when the hazardous waste management unit is operating at the
highest load or capacity level reasonably expected to occur. For
the purpose of determining total organic compound
concentrations and mass flow rates, the average of results of all
runs applies. The average must be computed on a time-weighed
basis.
D)
Total organic mass flow rates must be determined by the
following equation:
h
2sd
i
i
-6
E = Q
x(
n
i= 1
C xMW
)x0.0416x
10
∑
h
2sd
i
i
-6
E
= Q
x(
n
i = 1
C x MW )x0.0416x10
∑
Where:
E
h
= The total organic mass flow rate, kg/h.
Q
2sd
= The volumetric flow rate of gases entering or
exiting control device, dscm/h, as determined by Method
256
2 in 40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111.
n = The number of organic compounds in the vent gas.
C
i
= The organic concentration in ppm, dry basis, of
compound i in the vent gas, as determined by Method 18
in 40 CFR 60.
MW
i
= The molecular weight of organic compound i in
the vent gas, kg/kg-mol.
0.0416 = The conversion factor for molar volume, kg-
mol/m
3
, at 293 K and 760 mm Hg.
10
6
10
-6
= The conversion factor from ppm.
E)
The annual total organic emission rate must be determined by the
following equation:
A = F
×
H
Where:
A is total organic emission rate, kg/y.
F is the total organic mass flow rate, kg/h, as calculated
in subsection (c)(1)(D) of this Section.
H is the total annual hours of operation for the affected
unit.
F)
Total organic emissions from all affected process vents at the
facility must be determined by summing the hourly total organic
mass emissions rates (F as determined in subsection (c)(1)(D) of
this Section) and by summing the annual total organic mass
emission rates (A as determined in subsection (c)(1)(E) of this
Section) for all affected process vents at the facility.
2)
The owner or operator shall record such process information as is
necessary to determine the conditions of the performance tests.
Operations during periods of startup, shutdown and malfunction do not
constitute representative conditions for the purpose of a performance
test.
257
3)
The owner or operator of an affected facility shall provide, or cause to
be provided, performance testing facilities as follows:
A)
Sampling ports adequate for the test methods specified in
subsection (c)(1) of this Section.
B)
Safe sampling platform(s).
C)
Safe access to sampling platform(s).
D)
Utilities for sampling and testing equipment.
4)
For the purpose of making compliance determinations, the time-weighted
average of the results of the three runs must apply. In the event that a
sample is accidentally lost or conditions occur in which one of the three
runs must be discontinued because of forced shutdown, failure of an
irreplaceable portion of the sample train, extreme meteorological
conditions or other circumstances beyond the owner or operator’s
control, compliance may, upon the Agency’s approval, be determined
using the average of the results of the two other runs.
d)
To show that a process vent associated with a hazardous waste distillation,
fractionation, thin-film evaporation, solvent extraction, or air or steam stripping
operation is not subject to the requirements of this Subpart, the owner or
operator shall make an initial determination that the time-weighted, annual
average total organic concentration of the waste managed by the waste
management unit is less than 10 ppmw using one of the following two methods:
1)
Direct measurement of the organic concentration of the waste using the
following procedures:
A)
The owner or operator shall take a minimum of four grab
samples of waste for each wastestream managed in the affected
unit under process conditions expected to cause the maximum
waste organic concentration.
B)
For waste generated onsite, the grab samples must be collected at
a point before the waste is exposed to the atmosphere such as in
an enclosed pipe or other closed system that is used to transfer
the waste after generation to the first affected distillation,
fractionation, thin-film evaporation, solvent extraction, or air or
steam stripping operation. For waste generated offsite, the grab
samples must be collected at the inlet to the first waste
management unit that receives the waste provided the waste has
258
been transferred to the facility in a closed system such as a tank
truck and the waste is not diluted or mixed with other waste.
C)
Each sample must be analyzed and the total organic concentration
of the sample must be computed using Method 9060 or 8240
8260 of SW-846, incorporated by reference under 35 Ill. Adm.
Code 720.111.
D)
The arithmetic mean of the results of the analyses of the four
samples apply for each wastestream managed in the unit in
determining the time-weighted, annual average total organic
concentration of the waste. The time-weighted average is to be
calculated using the annual quantity of each waste stream
processed and the mean organic concentration of each
wastestream managed in the unit.
2)
Using knowledge of the waste to determine that its total organic
concentration is less than 10 ppmw. Documentation of the waste
determination is required. Examples of documentation that must be used
to support a determination under this subsection (d)(2) include:
A)
Production process information documenting that no organic
compounds are used;
B)
Information that the waste is generated by a process that is
identical to a process at the same or another facility that has
previously been demonstrated by direct measurement to generate
a wastestream having a total organic content less than 10 ppmw;
or
C)
Prior speciation analysis results on the same wastestream where it
is documented that no process changes have occurred since that
analysis that could affect the waste total organic concentration.
e)
The determination that distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operations which manage hazardous wastes
with time-weighted, annual average total organic concentrations less than 10
ppmw must be made as follows:
1)
By the effective date that the facility becomes subject to the provisions of
this Subpart or by the date when the waste is first managed in a waste
management unit, whichever is later; and
2)
For continuously generated waste, annually; or
259
3)
Whenever there is a change in the waste being managed or a change in
the process that generates or treats the waste.
f)
When an owner or operator and the Agency do not agree on whether a
distillation, fractionation, thin-film evaporation, solvent extraction, or air or
steam stripping operation manages a hazardous waste with organic
concentrations of at least 10 ppmw based on knowledge of the waste, the
procedures in Method 8240 8260 in SW-846, incorporated by reference in 35
Ill. Adm. Code 720.111, must be used to resolve the dispute.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 725.963
Test Methods and Procedures
a)
Each owner or operator subject to the provisions of this Subpart shall comply
with the test methods and procedures requirements provided in this Section.
b)
Leak detection monitoring, as required in Sections 725.952 through 725.962,
must comply with the following requirements:
1)
Monitoring must comply with Reference Method 21 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The detection instrument must meet the performance criteria of
Reference Method 21.
3)
The instrument must be calibrated before use on each day of its use by
the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a concentration of
approximately, but less than, 10,000 ppm methane or n-hexane.
5)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible as described in Reference
Method 21.
260
c)
When equipment is tested for compliance with no detectable emissions, as
required in Sections 725.952(e), 725.953(i), 725.954, and 725.957(f), the test
must comply with the following requirements:
1)
The requirements of subsections (b)(1) through (b)(4) above of this
Section apply.
2)
The background level must be determined as set forth in Reference
Method 21.
3)
The instrument probe must be traversed around all potential leak
interfaces as close to the interface as possible as described in Reference
Method 21.
4)
This arithmetic difference between the maximum concentration indicated
by the instrument and the background level is compared with 500 ppm
for determining compliance.
d)
In accordance with the waste analysis plan required by Section 725.113(b), an
owner or operator of a facility shall determine, for each piece of equipment,
whether the equipment contains or contacts a hazardous waste with organic
concentration that equals or exceeds 10 percent by weight using the following:
1)
Methods described in ASTM Methods D 2267-88, E 168-88, E 169-87,
or E 260-85, incorporated by reference in 35 Ill. Adm. Code 720.111;
2)
Method 9060 or 8240 8260 of SW-846, incorporated by reference in 35
Ill. Adm. Code 720.111; or
3)
Application of the knowledge of the nature of the hazardous wastestream
or the process by which it was produced. Documentation of a waste
determination by knowledge is required. Examples of documentation
that must be used to support a determination under this provision include
production process information documenting that no organic compounds
are used, information that the waste is generated by a process that is
identical to a process at the same or another facility that has previously
been demonstrated by direct measurement to have a total organic content
less than 10 percent, or prior speciation analysis results on the same
wastestream where it is also documented that no process changes have
occurred since that analysis that could affect the waste total organic
concentration.
e)
If an owner or operator determines that a piece of equipment contains or
contacts a hazardous waste with organic concentrations at least 10 percent by
261
weight, the determination can be revised only after following the procedures in
subsection (d)(1) or (d)(2) above of this Section.
f)
When an owner or operator and the Agency do not agree on whether a piece of
equipment contains or contacts a hazardous waste with organic concentrations at
least 10 percent by weight, the procedures in subsection (d)(1) or (d)(2) above
of this Section must be used to resolve the dispute.
g)
Samples used in determining the percent organic content must be representative
of the highest total organic content hazardous waste that is expected to be
contained in or contact the equipment.
h)
To determine if pumps or valves are in light liquid service, the vapor pressures
of constituents must either be obtained from standard reference texts or be
determined by ASTM D 2879-8692, incorporated by reference in 35 Ill. Adm.
Code 720.111.
i)
Performance tests to determine if a control device achieves 95 weight percent
organic emission reduction must comply with the procedures of Section
725.934(c)(1) through (c)(4).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.964
Recordkeeping Requirements
a)
Lumping Units.
1)
Each owner or operator subject to the provisions of this Subpart shall
comply with the recordkeeping requirements of this Section.
2)
An owner or operator of more than one hazardous waste management
unit subject to the provisions of this Subpart may comply with the
recordkeeping requirements for these hazardous waste management units
in one recordkeeping system if the system identifies each record by each
hazardous waste management unit.
b)
Owners and operators shall record the following information in the facility
operating record:
1)
For each piece of equipment to which this Subpart applies:
A)
Equipment identification number and hazardous waste
management unit identification.
262
B)
Approximate locations within the facility (e.g., identify the
hazardous waste management unit on a facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total organics in the hazardous wastestream at
the equipment.
E)
Hazardous waste state at the equipment (e.g., gas/vapor or
liquid).
F)
Method of compliance with the standard (e.g., “monthly leak
detection and repair” or “equipped with dual mechanical seals”).
2)
For facilities than that comply with the provisions of Section
725.933(a)(2), an implementation schedule as specified in that Section.
3)
Where an owner or operator chooses to use test data to demonstrate the
organic removal efficiency or total organic compound concentration
achieved by the control device, a performance test plan as specified in
Section 725.935(b)(3).
4)
Documentation of compliance with Section 725.960, including the
detailed design documentation or performance test results specified in
Section 725.935(b)(4).
c)
When each leak is detected as specified in Sections Section 725.952, 725.953,
725.957, or 725.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked with the
equipment identification number, the date evidence of a potential leak
was found in accordance with Section 725.958(a), and the date the leak
was detected, must be attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be removed after
it has been repaired.
3)
The identification on a valve may be removed after it has been
monitored for 2 successive months as specified in Section 725.957(c)
and no leak has been detected during those 2 months.
d)
When each leak is detected as specified in Sections 725.952, 725.953, 725.957
or 725.958, the following information must be recorded in an inspection log and
must be kept in the facility operating record:
263
1)
The instrument and operator identification numbers and the equipment
identification number.
2)
The date evidence of a potential leak was found in accordance with
Section 725.958(a).
3)
The date the leak was detected and the dates of each attempt to repair the
leak.
4)
Repair methods applied in each attempt to repair the leak.
5)
“Above 10,000”, if the maximum instrument reading measured by the
methods specified in Section 725.963(b) after each repair attempt is
equal to or greater than 10,000 ppm.
6)
“Repair delayed” and the reason for the delay if a leak is not repaired
within 15 calendar days after discovery of the leak.
7)
Documentation supporting the delay of repair of a valve in compliance
with Section 725.959(c).
8)
The signature of the owner or operator (or designate) whose decision it
was that repair could not be effected without a hazardous waste
management unit shutdown.
9)
The expected date of successful repair of the leak if a leak is not repaired
within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection information for
each closed-vent system and control device required to comply with the
provisions of Section 725.960 must be recorded and kept up-to-date in the
facility operating record as specified in Section 725.935(c)(1) and (c)(2), and
monitoring, operating and inspection information in Section 725.935(c)(3)
through (c)(8).
f)
For a control device other than a thermal vapor incinerator, catalytic vapor
incinerator, flare, boiler, process heater, condenser, or carbon adsorption
system, monitoring and inspection information indicating proper operation and
maintenance of the control device must be recorded in the facility operating
record.
264
g)
The following information pertaining to all equipment subject to the
requirements in Sections 725.952 through 725.960 must be recorded in a log
that is kept in the facility operating record:
1)
A list of identification numbers for equipment (except welded fittings)
subject to the requirements of this Subpart.
2)
List of Equipment.
A)
A list of identification numbers for equipment that the owner or
operator elects to designate for no detectable emissions, as
indicated by an instrument reading of less than 500 ppm above
background, under the provisions of Sections 725.952(e),
725.953(i) and 725.957(f).
B)
The designation of this equipment as subject to the requirements
of Section 725.952(e), 725.953(i) or 725.957(f) must be signed
by the owner or operator.
3)
A list of equipment identification numbers for pressure relief devices
required to comply with Section 725.954(a).
4)
Compliance tests.
A)
The dates of each compliance test required in Sections
725.952(e), 725.953(i), 725.954, and 725.957(f).
B)
The background level measured during each compliance test.
C)
The maximum instrument reading measured at the equipment
during each compliance test.
5)
A list of identification numbers for equipment in vacuum service.
6)
Identification, either by list or location (area or group) of equipment that
contains or contacts hazardous waste with an organic concentration of at
least 10% percent by weight for a period of less than 300 hours per year.
h)
The following information pertaining to all valves subject to the requirements of
Section 725.957(g) and (h) must be recorded in a log that is kept in the facility
operating record:
1)
A list of identification numbers for valves that are designated as unsafe
to monitor, an explanation for each valve stating why the valve is unsafe
to monitor, and the plan for monitoring each valve.
265
2)
A list of identification numbers for valves that are designated as difficult
to monitor, an explanation for each valve stating why the valve is
difficult to monitor, and the planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility operating record for
valves complying with Section 725.962:
1)
A schedule of monitoring.
2)
The percent of valves found leaking during each monitoring period.
j)
The following information must be recorded in a log that is kept in the facility
operating record:
1)
Criteria required in Section Sections 725.952(d)(5)(B) and 725.953(e)(2)
and an explanation of the criteria.
2)
Any changes to these criteria and the reasons for the changes.
k)
The following information must be recorded in a log that is kept in the facility
operating record for use in determining exemptions as provided in Section
725.950 and other specific Subparts:
1)
An analysis determining the design capacity of the hazardous waste
management unit.
2)
A statement listing the hazardous waste influent to and effluent from
each hazardous waste management unit subject to the requirements in
Sections Section 725.960 and an analysis determining whether these
hazardous wastes are heavy liquids.
3)
An up-to-date analysis and the supporting information and data used to
determine whether or not equipment is subject to the requirements in
Sections 725.952 through 725.960. The record must include supporting
documentation as required by Section 725.963(d)(3) when application of
the knowledge of the nature of the hazardous wastestream or the process
by which it was produced is used. If the owner or operator takes any
action (e.g., changing the process that produced the waste) that could
result in an increase in the total organic content of the waste contained in
or contacted by equipment determined not to be subject to the
requirements in Sections 725.952 through 725.960, then a new
determination is required.
266
l)
Records of the equipment leak information required by subsection (d) of this
Section and the operating information required by subsection (e) of this Section
need be kept only three years.
m)
The owner or operator of any facility that is subject to this Subpart and to
regulations at 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart V, incorporated
by reference in 35 Ill. Adm. Code 720.111, may elect to determine compliance
with this Subpart by documentation either pursuant to Section 725.964, or
pursuant to those provisions of 40 CFR 60 or 61, to the extent that the
documentation under the regulation at 40 CFR 60 or 61 duplicates the
documentation required under this Subpart. The documentation under the
regulation at 40 CFR 60 or 61 must be kept with or made readily available with
the facility operating record.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS, SURFACE
IMPOUNDMENTS, AND CONTAINERS
Section 725.981
Definitions
As used in this Subpart and in 35 Ill. Adm. Code 724, all terms not defined herein shall have
the meanings given to them in the Act and 35 Ill. Adm. Code 720 through 726.
“Average volatile organic concentration” or “average VO concentration” means
the mass-weighted average volatile organic concentration of a hazardous waste,
as determined in accordance with the requirements of Section 725.984.
“Closure device” means a cap, hatch, lid, plug, seal, valve, or other type of
fitting that blocks an opening in a cover so that when the device is secured in
the closed position it prevents or reduces air pollutant emissions to the
atmosphere. Closure devices include devices that are detachable from the cover
(e.g., a sampling port cap), manually operated (e.g., a hinged access lid or
hatch), or automatically operated (e.g., a spring-loaded pressure relief valve).
“Continuous seal” means a seal that forms a continuous closure that completely
covers the space between the edge of the floating roof and the wall of a tank. A
continuous seal may be a vapor-mounted seal, liquid-mounted seal, or metallic
shoe seal. A continuous seal may be constructed of fastened segments so as to
form a continuous seal.
“Cover” means a device that provides a continuous barrier over the hazardous
waste managed in a unit to prevent or reduce air emissions to the atmosphere.
A cover may have openings (such as access hatches, sampling ports, and gauge
267
wells) that are necessary for operation, inspection, maintenance, or repair of the
unit on which the cover is used. A cover may be a separate piece of equipment
which can be detached and removed from the unit or a cover may be formed by
structural features permanently integrated into the design of the unit.
“Enclosure” means a structure that surrounds a tank or container, captures
organic vapors emitted from the tank or container, and vents the captured
vapors through a closed-vent system to a control device.
“External floating roof” means a pontoon-type or double-deck type cover that
rests on the surface of a hazardous waste being managed in a tank with no fixed
roof.
“Fixed roof” means a cover that is mounted on a unit in a stationary position
and does not move with fluctuations in the level of the material managed in the
unit.
“Floating membrane cover” means a cover consisting of a synthetic flexible
membrane material that rests upon and is supported by the hazardous waste
being managed in a surface impoundment.
“Floating roof” means a cover consisting of a double-deck, pontoon single-
deck, or internal floating cover that rests upon and is supported by the material
being contained, and is equipped with a continuous seal.
“Hard-piping” means pipe or tubing that is manufactured and properly installed
in accordance with relevant standards and good engineering practices.
“In light material service” means the container is used to manage a material for
which both of the following conditions apply: the vapor pressure of one or
more of the organic constituents in the material is greater than 0.3 kilopascals
(kPa) at 20°C (1.2 inches H
2
O at 68°F); and the total concentration of the pure
organic constituents having a vapor pressure greater than 0.3 kPa at 20°C (1.2
inches H
2
O at 68°F) is equal to or greater than 20% percent by weight.
“Internal floating roof” means a cover that rests or floats on the material surface
(but not necessarily in complete contact with it) inside a tank that has a fixed
roof.
“Liquid-mounted seal” means a foam or liquid-filled primary seal mounted in
contact with the hazardous waste between the tank wall and the floating roof,
continuously around the circumference of the tank.
“Malfunction” means any sudden, infrequent, and not reasonably preventable
failure of air pollution control equipment, process equipment, or a process to
268
operate in a normal or usual manner. A failure that is caused in part by poor
maintenance or careless operation is not a malfunction.
“Maximum organic vapor pressure” means the sum of the individual organic
constituent partial pressures exerted by the material contained in a tank at the
maximum vapor pressure-causing conditions (i.e., temperature, agitation, pH
effects of combining wastes, etc.) reasonably expected to occur in the tank. For
the purpose of this Subpart, maximum organic vapor pressure is determined
using the procedures specified in Section 725.984(c).
“Metallic shoe seal” means a continuous seal that is constructed of metal sheets
that are held vertically against the wall of the tank by springs, weighted levers,
or other mechanisms and which is connected to the floating roof by braces or
other means. A flexible coated fabric (envelope) spans the annular space
between the metal sheet and the floating roof.
“No detectable organic emissions” means no escape of organics to the
atmosphere, as determined using the procedure specified in Section 725.984(d).
“Point of waste origination” means as follows:
When the facility owner or operator is the generator of the hazardous
waste, the “point of waste origination” means the point where a solid
waste produced by a system, process, or waste management unit is
determined to be a hazardous waste, as defined in 35 Ill. Adm. Code
721.
BOARD NOTE: In this case, this term is being used in a manner
similar to the use of the term “point of generation” in air standards
established for waste management operations under authority of the
federal Clean Air Act in 40 CFR 60, 61, and 63.
When the facility owner and operator are not the generator of the
hazardous waste, “point of waste origination” means the point where the
owner or operator accepts delivery or takes possession of the hazardous
waste.
“Point of waste treatment” means the point where a hazardous waste to be
treated in accordance with Section 725.983(c)(2) exits the treatment process.
Any waste determination must be made before the waste is conveyed, handled,
or otherwise managed in a manner that allows the waste to volatilize to the
atmosphere.
“Safety device” means a closure device, such as a pressure relief valve,
frangible disc, fusible plug, or any other type of device, which functions
269
exclusively to prevent physical damage or permanent deformation to a unit or its
air emission control equipment by venting gases or vapors directly to the
atmosphere during unsafe conditions resulting from an unplanned, accidental, or
emergency event. For the purpose of this Subpart, a safety device is not used
for routine venting of gases or vapors from the vapor headspace underneath a
cover such as during filling of the unit or to adjust the pressure in this vapor
headspace in response to normal daily diurnal ambient temperature fluctuations.
A safety device is designed to remain in a closed position during normal
operations and open only when the internal pressure, or another relevant
parameter, exceeds the device threshold setting applicable to the air emission
control equipment as determined by the owner or operator based on
manufacturer recommendations, applicable regulations, fire protection and
prevention codes, standard engineering codes and practices, or other
requirements for the safe handling of flammable, ignitable, explosive, reactive,
or hazardous materials.
“Single-seal system” means a floating roof having one continuous seal. This
seal may be vapor-mounted, liquid-mounted, or a metallic shoe seal.
“Vapor-mounted seal” means a continuous seal that is mounted so that there is a
vapor space between the hazardous waste in the unit and the bottom of the seal.
“Volatile organic concentration” or “VO concentration” means the fraction by
weight of organic compounds contained in a hazardous waste expressed in terms
of parts per million (ppmw), as determined by direct measurement or by
knowledge of the waste, in accordance with the requirements of Section
725.984. For the purpose of determining the VO concentration of a hazardous
waste, organic compounds with a Henry’s law constant value of at least 0.1
mole-fraction-in-the-gas-phase/mole-fraction-in the liquid-phase mole-fraction-
in-the-gas-phase/mole-fraction-in-the-liquid-phase (0.1 Y/X) (which can also be
expressed as 1.8
×
10
-6
atmospheres/gram-mole/m
3
) at 25° C (77° F) must be
included. Section 725.Appendix F presents a list of compounds known to have
a Henry’s law constant value less than the cutoff level.
“Waste determination” means performing all applicable procedures in
accordance with the requirements of Section 725.984 to determine whether a
hazardous waste meets standards specified in this Subpart. Examples of a waste
determination include performing the procedures in accordance with the
requirements of Section 725.984 to determine the average VO concentration of
a hazardous waste at the point of waste origination, determining the average VO
concentration of a hazardous waste at the point of waste treatment and
comparing the results to the exit concentration limit specified for the process
used to treat the hazardous waste, the organic reduction efficiency and the
organic biodegradation efficiency for a biological process used to treat a
hazardous waste and comparing the results to the applicable standards, or
270
determining the maximum volatile organic vapor pressure for a hazardous waste
in a tank and comparing the results to the applicable standards.
“Waste stabilization process” means any physical or chemical process used to
either reduce the mobility of hazardous constituents in a hazardous waste or
eliminate free liquids as determined by Test Method 9095 (Paint Filter Liquids
Test) in “Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods”, incorporated by reference in Section 720.111. A waste stabilization
process includes mixing the hazardous waste with binders or other materials and
curing the resulting hazardous waste and binder mixture. Other synonymous
terms used to refer to this process are “waste fixation” or “waste
solidification”. This does not include the addition of absorbent materials to the
surface of a waste to absorb free liquid without mixing, agitation, or subsequent
curing.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.985
Standards: Tanks
a)
The provisions of this Section apply to the control of air pollutant emissions
from tanks for which Section 725.983(b) references the use of this Section for
such air emission control.
b)
The owner or operator shall control air pollutant emissions from each tank
subject to this Section in accordance with the following requirements, as
applicable:
1)
For a tank that manages hazardous waste which meets all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank in accordance with the Tank Level 1 controls specified in
subsection (c) of this Section or the Tank Level 2 controls specified in
subsection (d) of this Section.
A)
The hazardous waste in the tank has a maximum organic vapor
pressure that is less than the maximum organic vapor pressure
limit for the tank’s design capacity category, as follows:
i)
For a tank design capacity equal to or greater than 151 m
3
(5333 ft
3
or 39,887 gal), the maximum organic vapor
pressure limit for the tank is 5.2 kPa (0.75 psia or 39 mm
Hg);
ii)
For a tank design capacity equal to or greater than 75 m
3
(2649 ft
3
or 19,810 gal) but less than 151 m
3
(5333 ft
3
or
271
39,887 gal), the maximum organic vapor pressure limit
for the tank is 27.6 kPa (4.0 psia or 207 mm Hg); or
iii)
For a tank design capacity is less than 75 m
3
(2649 ft
3
or
19,810 gal), the maximum organic vapor pressure limit
for the tank is 76.6 kPa (11.1 psia or 574 mm Hg).
B)
The hazardous waste in the tank is not heated by the owner or
operator to a temperature that is greater than the temperature at
which the maximum organic vapor pressure of the hazardous
waste is determined for the purpose of complying with subsection
(b)(1)(A) of this Section.
C)
The hazardous waste in the tank is not treated by the owner or
operator using a waste stabilization process, as defined in Section
725.981.
2)
For a tank that manages hazardous waste that does not meet all of the
conditions specified in subsections (b)(1)(A) through (b)(1)(C) of this
Section, the owner or operator shall control air pollutant emissions from
the tank by using Tank Level 2 controls in accordance with the
requirements of subsection (d) of this Section. Examples of tanks
required to use Tank Level 2 controls include the following: a tank used
for a waste stabilization process and a tank for which the hazardous
waste in the tank has a maximum organic vapor pressure that is equal to
or greater than the maximum organic vapor pressure limit for the tank’s
design capacity category, as specified in subsection (b)(1)(A) of this
Section.
c)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 1 controls shall meet the requirements specified in subsections (c)(1)
through (c)(4) of this Section:
1)
The owner or operator shall determine the maximum organic vapor
pressure for a hazardous waste to be managed in the tank using Tank
Level 1 controls before the first time the hazardous waste is placed in the
tank. The maximum organic vapor pressure must be determined using
the procedures specified in Section 725.984(c). Thereafter, the owner or
operator shall perform a new determination whenever changes to the
hazardous waste managed in the tank could potentially cause the
maximum organic vapor pressure to increase to a level that is equal to or
greater than the maximum organic vapor pressure limit for the tank
design capacity category specified in subsection (b)(1)(A) of this
Section, as applicable to the tank.
272
2)
The tank must be equipped with a fixed roof designed to meet the
following specifications:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the hazardous
waste in the tank. The fixed roof may be a separate cover
installed on the tank (e.g., a removable cover mounted on an
open-top tank) or may be an integral part of the tank structural
design (e.g., a horizontal cylindrical tank equipped with a hatch).
B)
The fixed roof must be installed in a manner such that there are
no visible cracks, holes, gaps, or other open spaces between roof
Section section joints or between the interface of the roof edge
and the tank wall.
C)
Each opening in the fixed roof must be either:
i)
Equipped with a closure device designed to operate such
that when the closure device is secured in the closed
position there are no visible cracks, holes, gaps, or other
open spaces in the closure device or between the perimeter
of the opening and the closure device; or
ii)
Connected by a closed-vent system that is vented to a
control device. The control device must remove or
destroy organics in the vent stream, and it must be
operating whenever hazardous waste is managed in the
tank.
D)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and which will maintain
the integrity of the fixed roof and closure devices throughout
their intended service life. Factors to be considered when
selecting the materials for and designing the fixed roof and
closure devices must include the following: organic vapor
permeability; the effects of any contact with the hazardous waste
or its vapors managed in the tank; the effects of outdoor exposure
to wind, moisture, and sunlight; and the operating practices used
for the tank on which the fixed roof is installed.
3)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position, except
as follows:
273
A)
Opening of closure devices or removal of the fixed roof is
allowed at the following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
the liquid in the tank, or when a worker needs to open a
hatch to maintain or repair equipment. Following
completion of the activity, the owner or operator shall
promptly secure the closure device in the closed position
or reinstall the cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of tank.
B)
Opening of a spring-loaded pressure-vacuum relief valve,
conservation vent, or similar type of pressure relief device which
vents to the atmosphere is allowed during normal operations for
the purpose of maintaining the tank internal pressure in
accordance with the tank design specifications. The device must
be designed to operate with no detectable organic emissions when
the device is secured in the closed position. The settings at which
the device opens must be established such that the device remains
in the closed position whenever the tank internal pressure is
within the internal pressure operating range determined by the
owner or operator based on the tank manufacturer
recommendations; applicable regulations; fire protection and
prevention codes; standard engineering codes and practices; or
other requirements for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to open are
during those times when the tank internal pressure exceeds the
internal pressure operating range for the tank as a result of
loading operations or diurnal ambient temperature fluctuations.
C)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
4)
The owner or operator shall inspect the air emission control equipment
in accordance with the following requirements.
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
274
air pollutant emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof Sections sections or
between the roof and the tank wall; broken, cracked, or
otherwise damaged seals or gaskets on closure devices; and
broken or missing hatches, access covers, caps, or other closure
devices.
B)
The owner or operator shall perform an initial inspection of the
fixed roof and its closure devices on or before the date that the
tank becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year,
except under the special conditions provided for in subsection (l)
of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
d)
Owners and operators controlling air pollutant emissions from a tank using Tank
Level 2 controls shall use one of the following tanks:
1)
A fixed-roof tank equipped with an internal floating roof in accordance
with the requirements specified in subsection (e) of this Section;
2)
A tank equipped with an external floating roof in accordance with the
requirements specified in subsection (f) of this Section;
3)
A tank vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (g) of this
Section;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) of this Section; or
5)
A tank located inside an enclosure that is vented through a closed-vent
system to an enclosed combustion control device in accordance with the
requirements specified in subsection (i) of this Section.
e)
The owner or operator that controls air pollutant emissions from a tank using a
fixed-roof fixed roof with an internal floating roof shall meet the requirements
specified in subsections (e)(1) through (e)(3) of this Section.
275
1)
The tank must be equipped with a fixed roof and an internal floating roof
in accordance with the following requirements:
A)
The internal floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The internal floating roof must be equipped with a continuous
seal between the wall of the tank and the floating roof edge that
meets either of the following requirements:
i)
A single continuous seal that is either a liquid-mounted
seal or a metallic shoe seal, as defined in Section
725.981; or
ii)
Two continuous seals mounted one of this Section above
the other. The lower seal may be a vapor-mounted seal.
C)
The internal floating roof must meet the following specifications:
i)
Each opening in a noncontact internal floating roof except
for automatic bleeder vents (vacuum breaker vents) and
the rim space vents is to provide a projection below the
liquid surface.
ii)
Each opening in the internal floating roof must be
equipped with a gasketed cover or a gasketed lid except
for leg sleeves, automatic bleeder vents, rim space vents,
column wells, ladder wells, sample wells, and stub drains.
iii)
Each penetration of the internal floating roof for the
purpose of sampling must have a slit fabric cover that
covers at least 90% percent of the opening.
iv)
Each automatic bleeder vent and rim space vent must be
gasketed.
v)
Each penetration of the internal floating roof that allows
for passage of a ladder must have a gasketed sliding
cover.
vi)
Each penetration of the internal floating roof that allows
for passage of a column supporting the fixed roof must
276
have a flexible fabric sleeve seal or a gasketed sliding
cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
C)
Prior to filling the tank, each cover, access hatch, gauge float
well or lid on any opening in the internal floating roof must be
bolted or fastened closed (i.e., no visible gaps). Rim space vents
are to be set to open only when the internal floating roof is not
floating or when the pressure beneath the rim exceeds the
manufacturer’s recommended setting.
3)
The owner or operator shall inspect the internal floating roof in
accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects that could
result in air pollutant emissions. Defects include, but are not
limited to, the following: when the internal floating roof is not
floating on the surface of the liquid inside the tank; when liquid
has accumulated on top of the internal floating roof; when any
portion of the roof seals have detached from the roof rim; when
holes, tears, or other openings are visible in the seal fabric; when
the gaskets no longer close off the hazardous waste surface from
the atmosphere; or when the slotted membrane has more than
10% percent open area.
B)
The owner or operator shall inspect the internal floating roof
components as follows, except as provided in subsection
(e)(3)(C) of this Section:
i)
Visually inspect the internal floating roof components
through openings on the fixed-roof fixed roof (e.g.,
manholes and roof hatches) at least once every 12 months
after initial fill, and
277
ii)
Visually inspect the internal floating roof, primary seal,
secondary seal (if one is in service), gaskets, slotted
membranes, and sleeve seals (if any) each time the tank is
emptied and degassed and at least once every 10 years.
C)
As an alternative to performing the inspections specified in
subsection (e)(3)(B) of this Section for an internal floating roof
equipped with two continuous seals mounted one above the other,
the owner or operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted membranes,
and sleeve seals (if any) each time the tank is emptied and
degassed and at least every five years.
D)
Prior to each inspection required by subsection (e)(3)(B) or
(e)(3)(C) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each visual inspection of an internal floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank, except when an
inspection is not planned, as provided for in subsection
(e)(3)(D)(ii) of this Section.
ii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Regional Administrator at least seven calendar days before
refilling the tank.
E)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
278
F)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
f)
The owner or operator that controls air pollutant emissions from a tank using an
external floating roof shall meet the requirements specified in subsections (f)(1)
through (f)(3) of this Section.
1)
The owner or operator shall design the external floating roof in
accordance with the following requirements:
A)
The external floating roof must be designed to float on the liquid
surface except when the floating roof must be supported by the
leg supports.
B)
The floating roof must be equipped with two continuous seals,
one above the other, between the wall of the tank and the roof
edge. The lower seal is referred to as the primary seal, and the
upper seal is referred to as the secondary seal.
i)
The primary seal must be a liquid-mounted seal or a
metallic shoe seal, as defined in Section 725.981. The
total area of the gaps between the tank wall and the
primary seal must not exceed 212 square centimeters
(cm
2
) per meter (10.0 in
2
per foot) of tank diameter, and
the width of any portion of these gaps must not exceed
3.8 centimeters (cm) (1.5 inches). If a metallic shoe seal
is used for the primary seal, the metallic shoe seal must be
designed so that one end extends into the liquid in the tank
and the other end extends a vertical distance of at least 61
centimeters above the liquid surface.
ii)
The secondary seal must be mounted above the primary
seal and cover the annular space between the floating roof
and the wall of the tank. The total area of the gaps
between the tank wall and the secondary seal must not
exceed 21.2 cm
2
per meter (1.0 in
2
per foot) of tank
diameter, and the width of any portion of these gaps must
not exceed 1.3 cm (0.5 inch).
C)
The external floating roof must meet the following specifications:
i)
Except for automatic bleeder vents (vacuum breaker
vents) and rim space vents, each opening in a noncontact
279
external floating roof must provide a projection below the
liquid surface.
ii)
Except for automatic bleeder vents, rim space vents, roof
drains, and leg sleeves, each opening in the roof must be
equipped with a gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must be
equipped with a cover designed to be bolted or fastened
when the cover is secured in the closed position.
iv)
Each automatic bleeder vent and each rim space vent must
be equipped with a gasket.
v)
Each roof drain that empties into the liquid managed in
the tank must be equipped with a slotted membrane fabric
cover that covers at least 90% percent of the area of the
opening.
vi)
Each unslotted and slotted guide pole well must be
equipped with a gasketed sliding cover or a flexible fabric
sleeve seal.
vii)
Each unslotted guide pole must be equipped with a
gasketed cap on the end of the pole.
viii)
Each slotted guide pole must be equipped with a gasketed
float or other device which closes off the liquid surface
from the atmosphere.
ix)
Each gauge hatch and each sample well must be equipped
with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance with the
following requirements:
A)
When the floating roof is resting on the leg supports, the process
of filling, emptying, or refilling must be continuous and must be
completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents, roof drains,
and leg sleeves, each opening in the roof must be secured and
maintained in a closed position at all times except when the
closure device must be open for access.
280
C)
Covers on each access hatch and each gauge float well must be
bolted or fastened when secured in the closed position.
D)
Automatic bleeder vents must be set closed at all times when the
roof is floating, except when the roof is being floated off or is
being landed on the leg supports.
E)
Rim space vents must be set to open only at those times that the
roof is being floated off the roof leg supports or when the
pressure beneath the rim seal exceeds the manufacturer’s
recommended setting.
F)
The cap on the end of each unslotted guide pole must be secured
in the closed position at all times except when measuring the
level or collecting samples of the liquid in the tank.
G)
The cover on each gauge hatch or sample well must be secured in
the closed position at all times except when the hatch or well
must be opened for access.
H)
Both the primary seal and the secondary seal must completely
cover the annular space between the external floating roof and the
wall of the tank in a continuous fashion except during
inspections.
3)
The owner or operator shall inspect the external floating roof in
accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external floating roof
seal gaps in accordance with the following requirements:
i)
The owner or operator shall perform measurements of
gaps between the tank wall and the primary seal within 60
calendar days after initial operation of the tank following
installation of the floating roof and, thereafter, at least
once every five years.
ii)
The owner or operator shall perform measurements of
gaps between the tank wall and the secondary seal within
60 calendar days after initial operation of the tank
following installation of the floating roof and, thereafter,
at least once every year.
iii)
If a tank ceases to hold hazardous waste for a period of
one year or more, subsequent introduction of hazardous
281
waste into the tank must be considered an initial operation
for the purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) of this Section.
iv)
The owner or operator shall determine the total surface
area of gaps in the primary seal and in the secondary seal
individually using the procedure set forth in subsection
(f)(4)(D) of this Section.
v)
In the event that the seal gap measurements do not
conform to the specifications in subsection (f)(1)(B) of
this Section, the owner or operator must repair the defect
in accordance with the requirements of subsection (k) of
this Section.
vi)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 725.990(b).
B)
The owner or operator shall visually inspect the external floating
roof in accordance with the following requirements:
i)
The floating roof and its closure devices must be visually
inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects
include, but are not limited to any of the following:
holes, tears, or other openings in the rim seal or seal
fabric of the floating roof; a rim seal detached from the
floating roof; all or a portion of the floating roof deck
being submerged of this Section below the surface of the
liquid in the tank; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
ii)
The owner or operator shall perform an initial inspection
of the external floating roof and its closure devices on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall perform
the inspections at least once every year except for the
special conditions provided for in subsection (l) of this
Section.
iii)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with the
requirements of subsection (k) of this Section.
282
iv)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements specified
in Section 725.990(b).
C)
Prior to each inspection required by subsection (f)(3)(A) or
(f)(3)(B) of this Section, the owner or operator shall notify the
Agency in advance of each inspection to provide the Agency with
the opportunity to have an observer present during the
inspection. The owner or operator shall notify the Agency of the
date and location of the inspection as follows:
i)
Prior to each inspection to measure external floating roof
seal gaps as required under subsection (f)(3)(A) of this
Section, written notification must be prepared and sent by
the owner or operator so that it is received by the Agency
at least 30 calendar days before the date the measurements
are scheduled to be performed.
ii)
Prior to each visual inspection of an external floating roof
in a tank that has been emptied and degassed, written
notification must be prepared and sent by the owner or
operator so that it is received by the Agency at least 30
calendar days before refilling the tank except when an
inspection is not planned, as provided for in subsection
(f)(3)(C)(iii) of this Section.
iii)
When a visual inspection is not planned and the owner or
operator could not have known about the inspection 30
calendar days before refilling the tank, the owner or
operator shall notify the Agency as soon as possible, but
no later than seven calendar days before refilling of the
tank. This notification may be made by telephone and
immediately followed by a written explanation for why
the inspection is unplanned. Alternatively, written
notification, including the explanation for the unplanned
inspection, may be sent so that it is received by the
Regional Administrator at least seven calendar days before
refilling the tank.
D)
Procedure for determining gaps in the primary seal and in the
secondary seal for the purposes of subsection (f)(3)(A)(iv) of this
Section:
283
i)
The seal gap measurements must be performed at one or
more floating roof levels when the roof is floating off the
roof supports.
ii)
Seal gaps, if any, must be measured around the entire
perimeter of the floating roof in each place where a 0.32-
cm (_-inch) diameter uniform probe passes freely (without
forcing or binding against the seal) between the seal and
the wall of the tank and measure the circumferential
distance of each such location.
iii)
For a seal gap measured under this subsection (f)(3), the
gap surface area must be determined by using probes of
various widths to measure accurately the actual distance
from the tank wall to the seal and multiplying each such
width by its respective circumferential distance.
iv)
The total gap area must be calculated by adding the gap
surface areas determined for each identified gap location
for the primary seal and the secondary seal individually,
and then dividing the sum for each seal type by the
nominal perimeter of the tank. These total gap areas for
the primary seal and secondary seal are then are compared
to the respective standards for the seal type, as specified
in subsection (f)(1)(B) of this Section.
BOARD NOTE: Subsections (f)(3)(D)(i) through
(f)(3)(D)(iv) correspond with 40 CFR
265.1085(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4), which the
Board has codified here to comport with Illinois
Administrative Code format requirements.
g)
The owner or operator that controls air pollutant emissions from a tank by
venting the tank to a control device shall meet the requirements specified in
subsections (g)(1) through (g)(3) of this Section.
1)
The tank must be covered by a fixed roof and vented directly through a
closed-vent system to a control device in accordance with the following
requirements:
A)
The fixed roof and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
tank.
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B)
Each opening in the fixed roof not vented to the control device
must be equipped with a closure device. If the pressure in the
vapor headspace underneath the fixed roof is less than
atmospheric pressure when the control device is operating, the
closure devices must be designed to operate such that when the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device. If the pressure in the vapor headspace underneath
the fixed roof is equal to or greater than atmospheric pressure
when the control device is operating, the closure device must be
designed to operate with no detectable organic emissions.
C)
The fixed roof and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the fixed roof and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the fixed roof and closure devices
must include the following: organic vapor permeability; the
effects of any contact with the liquid and its vapor managed in
the tank; the effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the tank on which
the fixed roof is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 725.988.
2)
Whenever a hazardous waste is in the tank, the fixed roof must be
installed with each closure device secured in the closed position and the
vapor headspace underneath the fixed roof vented to the control device
except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the fixed roof is allowed at the
following times:
i)
To provide access to the tank for performing routine
inspection, maintenance, or other activities needed for
normal operations. Examples of such activities include
those times when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to open a hatch
to maintain or repair equipment. Following completion of
the activity, the owner or operator shall promptly secure
285
the closure device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues from the
bottom of a tank.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
A)
The fixed roof and its closure devices must be visually inspected
by the owner or operator to check for defects that could result in
air pollutant emissions. Defects include, but are not limited to
any of the following: visible cracks, holes, or gaps in the roof
sections or between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure devices; and
broken or missing hatches, access covers, caps, or other closure
devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 725.988.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the tank
becomes subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once every year
except for the special conditions provided for in subsection (l) of
this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (k) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(b).
h)
The owner or operator that controls air pollutant emissions by using a pressure
tank must meet the following requirements.
286
1)
The tank shall be designed not to vent to the atmosphere as a result of
compression of the vapor headspace in the tank during filling of the tank
to its design capacity.
2)
All tank openings must be equipped with closure devices designed to
operate with no detectable organic emissions as determined using the
procedure specified in Section 725.984(d).
3)
Whenever a hazardous waste is in the tank, the tank must be operated as
a closed system that does not vent to the atmosphere except in the event
that a safety device, as defined in Section 725.981, is required to open to
avoid an unsafe condition.
i)
The owner or operator that controls air pollutant emissions by using an
enclosure vented through a closed-vent system to an enclosed combustion
control device shall meet the requirements specified in subsections (i)(1) through
(i)(4) of this Section.
1)
The tank must be located inside an enclosure. The enclosure must be
designed and operated in accordance with the criteria for a permanent
total enclosure, as specified in “Procedure T--Criteria for and
Verification of a Permanent or Temporary Total Enclosure” under 40
CFR 52.741, appendix B, incorporated by reference in 35 Ill. Adm.
Code 720.111. The enclosure may have permanent or temporary
openings to allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means; entry of
permanent mechanical or electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the verification
procedure for the enclosure as specified in Section 5.0 to “Procedure T--
Criteria for and Verification of a Permanent or Temporary Total
Enclosure” initially when the enclosure is first installed and, thereafter,
annually.
2)
The enclosure must be vented through a closed-vent system to an
enclosed combustion control device that is designed and operated in
accordance with the standards for either a vapor incinerator, boiler, or
process heater specified in Section 725.988.
3)
Safety devices, as defined in Section 725.981, may be installed and
operated as necessary on any enclosure, closed-vent system, or control
device used to comply with the requirements of subsections (i)(1) and
(i)(2) of this Section.
4)
The owner or operator shall inspect and monitor the closed-vent system
and control device, as specified in Section 725.988.
287
j)
The owner or operator shall transfer hazardous waste to a tank subject to this
Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (j)(2) of
this Section, to the tank from another tank subject to this Section or from
a surface impoundment subject to Section 725.986 must be conducted
using continuous hard-piping or another closed system that does not
allow exposure of the hazardous waste to the atmosphere. For the
purpose of complying with this provision, an individual drain system is
considered to be a closed system when it meets the requirements of 40
CFR 63, subpart RR, “National Emission Standards for Individual Drain
Systems”, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) of this Section do not apply when
transferring a hazardous waste to the tank under any of the following
conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
725.983(c)(2).
k)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsections subsection (c)(4),
(e)(3), (f)(3), or (g)(3) of this Section as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair shall be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (k)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the tank and no alternative tank
capacity is available at the site to accept the hazardous waste normally
managed in the tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating the hazardous
waste managed in the tank stops operation. Repair of the defect must be
completed before the process or unit resumes operation.
288
l)
Following the initial inspection and monitoring of the cover as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year under the following special
conditions:
1)
Where inspecting or monitoring the cover would expose a worker to
dangerous, hazardous, or other unsafe conditions, then the owner or
operator may designate a cover as an “unsafe to inspect and monitor
cover” and comply with all of the following requirements:
A)
Prepare a written explanation for the cover stating the reasons
why the cover is unsafe to visually inspect or to monitor, if
required.
B)
Develop and implement a written plan and schedule to inspect
and monitor the cover, using the procedures specified in the
applicable Section of this Subpart, as frequently as practicable
during those times when a worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely underground, an
owner or operator is required to inspect and monitor, as required by the
applicable provisions of this Section, only those portions of the tank
cover and those connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground surface.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.986
Standards: Surface Impoundments
a)
The provisions of this Section apply to the control of air pollutant emissions
from surface impoundments for which Section 725.983(b) of this Subpart
references the use of this Section for such air emission control.
b)
The owner or operator shall control air pollutant emissions from the surface
impoundment by installing and operating either of the following:
1)
A floating membrane cover in accordance with the provisions specified
in subsection (c) of this Section; or
2)
A cover that is vented through a closed-vent system to a control device
in accordance with the provisions specified in subsection (d) of this
Section.
289
c)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a floating membrane cover must meet the requirements
specified in subsections (c)(1) through (c)(3) of this Section.
1)
The surface impoundment must be equipped with a floating membrane
cover designed to meet the following specifications:
A)
The floating membrane cover must be designed to float on the
liquid surface during normal operations and form a continuous
barrier over the entire surface area of the liquid.
B)
The cover must be fabricated from a synthetic membrane material
that is either:
i)
High density polyethylene (HDPE) with a thickness no
less than 2.5 millimeters (mm) (0.10 inch); or
ii)
A material or a composite of different materials
determined to have both organic permeability properties
that are equivalent to those of the material listed in
subsection (c)(1)(B)(i) of this Section and chemical and
physical properties that maintain the material integrity for
the intended service life of the material.
C)
The cover must be installed in a manner such that there are no
visible cracks, holes, gaps, or other open spaces between cover
section seams or between the interface of the cover edge and its
foundation mountings.
D)
Except as provided for in subsection (c)(1)(E) of this Section,
each opening in the floating membrane cover must be equipped
with a closure device so designed as to operate that when that the
closure device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in the closure
device or between the perimeter of the cover opening and the
closure device.
E)
The floating membrane cover may be equipped with one or more
emergency cover drains for removal of stormwater. Each
emergency cover drain must be equipped with a slotted
membrane fabric cover that covers at least 90% percent of the
area of the opening or a flexible fabric sleeve seal.
F)
The closure devices must be made of suitable materials that will
minimize exposure of the hazardous waste to the atmosphere, to
290
the extent practical, and will maintain the integrity of the closure
devices throughout their intended service life. Factors to be
considered when selecting the materials of construction and
designing the cover and closure devices must include the
following: the organic vapor permeability; the effects of any
contact with the liquid and its vapor managed in the surface
impoundment; the effects of outdoor exposure to wind, moisture,
and sunlight; and the operating practices used for the surface
impoundment on which the floating membrane cover is installed.
2)
Whenever a hazardous waste is in the surface impoundment, the floating
membrane cover must float on the liquid and each closure device must
be secured in the closed position except as follows:
A)
Opening of closure devices or removal of the cover is allowed at
the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample the liquid in the surface impoundment, or
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly replace the cover and
secure the closure device in the closed position, as
applicable.
ii)
To remove accumulated sludge or other residues from the
bottom of surface impoundment.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect the floating membrane cover in
accordance with the following procedures:
A)
The floating membrane cover and its closure devices must be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
291
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The owner or operator shall perform an initial inspection of the
floating membrane cover and its closure devices on or before the
date that the surface impoundment becomes subject to this
Section. Thereafter, the owner or operator shall perform the
inspections at least once every year except for the special
conditions provided for in subsection (g) of this Section.
C)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
D)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(c).
d)
The owner or operator that controls air pollutant emissions from a surface
impoundment using a cover vented to a control device shall meet the
requirements specified in subsections (d)(1) through (d)(3) of this Section.
1)
The surface impoundment must be covered by a cover and vented
directly through a closed-vent system to a control device in accordance
with the following requirements:
A)
The cover and its closure devices must be designed to form a
continuous barrier over the entire surface area of the liquid in the
surface impoundment.
B)
Each opening in the cover not vented to the control device must
be equipped with a closure device. If the pressure in the vapor
headspace underneath the cover is less than atmospheric pressure
when the control device is operating, the closure devices must be
designed to operate such that when the closure device is secured
in the closed position there are no visible cracks, holes, gaps, or
other open spaces in the closure device or between the perimeter
of the cover opening and the closure device. If the pressure in
the vapor headspace underneath the cover is equal to or greater
than atmospheric pressure when the control device is operating,
the closure device must be designed to operate with no detectable
organic emissions using the procedure specified in Section
725.984(d).
292
C)
The cover and its closure devices must be made of suitable
materials that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will maintain the
integrity of the cover and closure devices throughout their
intended service life. Factors to be considered when selecting the
materials for and designing the cover and closure devices must
include the following: the organic vapor permeability; the effects
of any contact with the liquid or its vapors managed in the
surface impoundment; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices used for the
surface impoundment on which the cover is installed.
D)
The closed-vent system and control device must be designed and
operated in accordance with the requirements of Section 725.988.
2)
Whenever a hazardous waste is in the surface impoundment, the cover
must be installed with each closure device secured in the closed position
and the vapor headspace underneath the cover vented to the control
device except as follows:
A)
Venting to the control device is not required, and opening of
closure devices or removal of the cover is allowed at the
following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or other
activities needed for normal operations. Examples of such
activities include those times when a worker needs to open
a port to sample liquid in the surface impoundment, or
when a worker needs to open a hatch to maintain or repair
equipment. Following completion of the activity, the
owner or operator shall promptly secure the closure
device in the closed position or reinstall the cover, as
applicable, to the surface impoundment.
ii)
To remove accumulated sludge or other residues from the
bottom of surface impoundment.
B)
Opening of a safety device, as defined in Section 725.981, is
allowed at any time conditions require doing so to avoid an
unsafe condition.
3)
The owner or operator shall inspect and monitor the air emission control
equipment in accordance with the following procedures:
293
A)
The surface impoundment cover and its closure devices must be
visually inspected by the owner or operator to check for defects
that could result in air pollutant emissions. Defects include, but
are not limited to, visible cracks, holes, or gaps in the cover
section seams or between the interface of the cover edge and its
foundation mountings; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure devices.
B)
The closed-vent system and control device must be inspected and
monitored by the owner or operator in accordance with the
procedures specified in Section 725.988.
C)
The owner or operator shall perform an initial inspection of the
air emission control equipment on or before the date that the
surface impoundment becomes subject to this Section.
Thereafter, the owner or operator shall perform the inspections at
least once every year except for the special conditions provided
for in subsection (g) of this Section.
D)
In the event that a defect is detected, the owner or operator shall
repair the defect in accordance with the requirements of
subsection (f) of this Section.
E)
The owner or operator shall maintain a record of the inspection in
accordance with the requirements specified in Section
725.990(c).
e)
The owner or operator shall transfer hazardous waste to a surface impoundment
subject to this Section in accordance with the following requirements:
1)
Transfer of hazardous waste, except as provided in subsection (e)(2) of
this Section, to the surface impoundment from another surface
impoundment subject to this Section or from a tank subject to Section
725.985 must be conducted using continuous hard-piping or another
closed system that does not allow exposure of the waste to the
atmosphere. For the purpose of complying with this provision, an
individual drain system is considered to be a closed system when it meets
the requirements of 40 CFR 63, Subpart RR, “National Emission
Standards for Individual Drain Systems”, incorporated by reference in
35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (e)(1) of this Section do not apply when
transferring a hazardous waste to the surface impoundment under either
of the following conditions:
294
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the point of waste
origination.
B)
The hazardous waste has been treated by an organic destruction
or removal process to meet the requirements in Section
725.983(c)(2).
f)
The owner or operator shall repair each defect detected during an inspection
performed in accordance with the requirements of subsection (c)(3) or (d)(3) of
this Section as follows:
1)
The owner or operator shall make first efforts at repair of the defect no
later than five calendar days after detection, and repair must be
completed as soon as possible but no later than 45 calendar days after
detection except as provided in subsection (f)(2) of this Section.
2)
Repair of a defect may be delayed beyond 45 calendar days if the owner
or operator determines that repair of the defect requires emptying or
temporary removal from service of the surface impoundment and no
alternative capacity is available at the site to accept the hazardous waste
normally managed in the surface impoundment. In this case, the owner
or operator shall repair the defect the next time the process or unit that is
generating the hazardous waste managed in the tank stops operation.
Repair of the defect must be completed before the process or unit
resumes operation.
g)
Following the initial inspection and monitoring of the cover as required by the
applicable provisions of this Subpart, subsequent inspection and monitoring may
be performed at intervals longer than one year in the case when inspecting or
monitoring the cover would expose a worker to dangerous, hazardous, or other
unsafe conditions. In this case, the owner or operator may designate the cover
as an “unsafe to inspect and monitor cover” and comply with all of the
following requirements:
1)
Prepare a written explanation for the cover stating the reasons why the
cover is unsafe to visually inspect or to monitor, if required.
2)
Develop and implement a written plan and schedule to inspect and
monitor the cover using the procedures specified in the applicable
Section of this Subpart as frequently as practicable during those times
when a worker can safely access the cover.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
295
Section 725.988
Standards: Closed-ventVent Systems and Control Devices
a)
This Section applies to each closed-vent system and control device installed and
operated by the owner or operator to control air emissions in accordance with
standards of this Subpart.
b)
The closed-vent system must meet the following requirements:
1)
The closed-vent system must route the gases, vapors, and fumes emitted
from the hazardous waste in the waste management unit to a control
device that meets the requirements specified in subsection (c) of this
Section.
2)
The closed-vent system must be designed and operated in accordance
with the requirements specified in Section 725.933(j).
3)
When the closed-vent system includes bypass devices that could be used
to divert the gas or vapor stream to the atmosphere before entering the
control device, each bypass device must be equipped with either a flow
indicator as specified in subsection (b)(3)(A) of this Section or a seal or
locking device as specified in subsection (b)(3)(B) of this Section. For
the purpose of complying with this subsection, low leg drains, high point
bleeds, analyzer vents, open-ended valves or lines, spring-loaded
pressure relief valves, and other fittings used for safety purposes are not
considered to be bypass devices.
A)
If a flow indicator is used to comply with this subsection (b)(3),
the indicator must be installed at the inlet to the bypass line used
to divert gases and vapors from the closed-vent system to the
atmosphere at a point upstream of the control device inlet. For
the purposes of this subsection, a flow indicator means a device
which indicates the presence of either gas or vapor flow in the
bypass line.
B)
If a seal or locking device is used to comply with this subsection
(b)(3), the device must be placed on the mechanism by which the
bypass device position is controlled (e.g., valve handle or damper
lever) when the bypass device is in the closed position such that
the bypass device cannot be opened without breaking the seal or
removing the lock. Examples of such devices include, but are
not limited to, a car-seal or a lock-and-key configuration valve.
The owner or operator shall visually inspect the seal or closure
mechanism at least once every month to verify that the bypass
mechanism is maintained in the closed position.
296
4)
The closed-vent system must be inspected and monitored by the owner
or operator in accordance with the procedure specified in Section
725.933(k).
c)
The control device must meet the following requirements:
1)
The control device must be one of the following devices:
A)
A control device designed and operated to reduce the total
organic content of the inlet vapor stream vented to the control
device by at least 95% percent by weight;
B)
An enclosed combustion device designed and operated in
accordance with the requirements of Section 725.933(c); or
C)
A flare designed and operated in accordance with the
requirements of Section 725.933(d).
2)
The owner or operator that elects to use a closed-vent system and control
device to comply with the requirements of this Section shall comply with
the requirements specified in subsections (c)(2)(A) through (c)(2)(G) of
this Section.
A)
Periods of planned routine maintenance of the control device,
during which the control device does not meet the specifications
of subsections (c)(1)(A), (c)(1)(B), or (c)(1)(C) of this Section,
as applicable, must not exceed 240 hours per year.
B)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during periods of planned routine maintenance.
C)
The specifications and requirements in subsections (c)(1)(A),
(c)(1)(B), and (c)(1)(C) of this Section for control devices do not
apply during a control device system malfunction.
D)
The owner or operator shall demonstrate compliance with the
requirements of subsection (c)(2)(A) of this Section (i.e., planned
routine maintenance of a control device, during which the control
device does not meet the specifications of subsections (c)(1)(A),
(c)(1)(B), or (c)(1)(C) of this Section, as applicable, must not
exceed 240 hours per year) by recording the information
specified in Section 725.990(e)(1)(E).
297
E)
The owner or operator shall correct control device system
malfunctions as soon as practicable after their occurrence in order
to minimize excess emissions of air pollutants.
F)
The owner or operator shall operate the closed-vent system so
that gases, vapors, or fumes are not actively vented to the control
device during periods of planned maintenance or control device
system malfunction (i.e., periods when the control device is not
operating or not operating normally), except in cases when it is
necessary to vent the gases, vapors, or fumes to avoid an unsafe
condition or to implement malfunction corrective actions or
planned maintenance actions.
3)
The owner or operator using a carbon adsorption system to comply with
subsection (c)(1) of this Section shall operate and maintain the control
device in accordance with the following requirements:
A)
Following the initial startup of the control device, all activated
carbon in the control device must be replaced with fresh carbon
on a regular basis in accordance with the requirements of Section
725.933(g) or 725.933(h).
B)
All carbon removed from the control device must be managed in
accordance with the requirements of Section 725.933(m).
4)
An owner or operator using a control device other than a thermal vapor
incinerator, flare, boiler, process heater, condenser, or carbon
adsorption system to comply with subsection (c)(1) of this Section shall
operate and maintain the control device in accordance with the
requirements of Section 725.933(i).
5)
The owner or operator shall demonstrate that a control device achieves
the performance requirements of subsection (c)(1) of this Section as
follows:
A)
An owner or operator shall demonstrate using either a
performance test, as specified in subsection (c)(5)(C) of this
Section, or a design analysis, as specified in subsection (c)(5)(D)
of this Section, the performance of each control device except for
the following:
i)
A flare;
ii)
A boiler or process heater with a design heat input
capacity of 44 megawatts or greater;
298
iii)
A boiler or process heater into which the vent stream is
introduced with the primary fuel;
iv)
A boiler or industrial furnace burning hazardous waste for
which the owner or operator has been issued a final
permit under 35 Ill. Adm. Code 702, 703, and 705 and
has designed and operates in accordance with the
requirements of 35 Ill. Adm. Code 726.Subpart H; or
v)
A boiler or industrial furnace burning hazardous waste for
which the owner or operator has designed and operates in
accordance with the interim status requirements of 35 Ill.
Adm. Code 726.Subpart H.
B)
An owner or operator shall demonstrate the performance of each
flare in accordance with the requirements specified in Section
725.933(e).
C)
For a performance test conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the owner or operator shall
use the test methods and procedures specified in Section
725.934(c)(1) through (c)(4).
D)
For a design analysis conducted to meet the requirements of
subsection (c)(5)(A) of this Section, the design analysis must
meet the requirements specified in Section 725.935(b)(4)(C).
E)
The owner or operator shall demonstrate that a carbon adsorption
system achieves the performance requirements of subsection
(c)(1) of this Section based on the total quantity of organics
vented to the atmosphere from all carbon adsorption system
equipment that is used for organic adsorption, organic desorption
or carbon regeneration, organic recovery, and carbon disposal.
6)
If the owner or operator and the Agency do not agree on a demonstration
of control device performance using a design analysis, then the
disagreement must be resolved using the results of a performance test
performed by the owner or operator in accordance with the requirements
of subsection (c)(5)(C) of this Section. The Agency may choose to have
an authorized representative observe the performance test.
7)
The control device must be inspected and monitored by the owner or
operator in accordance with the procedures specified in Section
725.1033725.933(f)(2) and (k). The readings from each monitoring
299
device required by Section 725.1033725.933(f)(2) must be inspected at
least once each operating day to check control device operation. Any
necessary corrective measures must be immediately implemented to
ensure the control device is operated in compliance with the
requirements of this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.989
Inspection and Monitoring Requirements
a)
The owner or operator shall inspect and monitor air emission control equipment
used to comply with this Subpart in accordance with the requirements specified
in Sections 725.985 through 725.988.
b)
The owner or operator shall develop and implement a written plan and schedule
to perform the inspections and monitoring required by subsection (a) of this
Section. The owner or operator shall incorporate this plan and schedule into the
facility inspection plan required under Section 265.115725.115.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 725.990
Recordkeeping Requirements
a)
Each owner or operator of a facility subject to requirements in this Subpart shall
record and maintain the information specified in subsections (b) through (i) of
this Section, as applicable to the facility. Except for air emission control
equipment design documentation and information required by subsection (i) of
this Section, records required by this Section must be maintained in the
operating record for a minimum of three years. Air emission control equipment
design documentation must be maintained in the operating record until the air
emission control equipment is replaced or is otherwise no longer in service.
Information required by subsection (i) of this Section must be maintained in the
operating record for as long as the tank or container is not using air emission
controls specified in Sections 264.984724.984 through 264.987724.987, in
accordance with the conditions specified in Section 724.984(d).
b)
The owner or operator of a tank using air emission controls in accordance with
the requirements of Section 725.985 shall prepare and maintain records for the
tank that include the following information:
1)
For each tank using air emission controls in accordance with the
requirements of Section 725.985 of this Subpart, the owner or operator
shall record:
300
A)
A tank identification number (or other unique identification
description as selected by the owner or operator).
B)
A record for each inspection required by Section 725.985 that
includes the following information:
i)
Date inspection was conducted.
ii)
For each defect detected during the inspection, the
following information: the location of the defect, a
description of the defect, the date of detection, and
corrective action taken to repair the defect. In the event
that repair of the defect is delayed in accordance with the
provisions of Section 725.985, the owner or operator shall
also record the reason for the delay and the date that
completion of repair of the defect is expected.
2)
In addition to the information required by subsection (b)(1) of this
Section, the owner or operator shall record the following information, as
applicable to the tank:
A)
The owner or operator using a fixed roof to comply with the
Tank Level 1 control requirements specified in Section
725.985(c) shall prepare and maintain records for each
determination for the maximum organic vapor pressure of the
hazardous waste in the tank performed in accordance with the
requirements of Section 725.985(c). The records must include
the date and time the samples were collected, the analysis method
used, and the analysis results.
B)
The owner or operator using an internal floating roof to comply
with the Tank Level 2 control requirements specified in Section
725.985(e) shall prepare and maintain documentation describing
the floating roof design.
C)
Owners and operators using an external floating roof to comply
with the Tank Level 2 control requirements specified in Section
725.985(f) shall prepare and maintain the following records:
i)
Documentation describing the floating roof design and the
dimensions of the tank.
ii)
Records for each seal gap inspection required by Section
725.985(f)(3) describing the results of the seal gap
measurements. The records must include the date that the
301
measurements were performed, the raw data obtained for
the measurements, and the calculations of the total gap
surface area. In the event that the seal gap measurements
do not conform to the specifications in Section
725.985(f)(1), the records must include a description of
the repairs that were made, the date the repairs were
made, and the date the tank was emptied, if necessary.
D)
Each owner or operator using an enclosure to comply with the
Tank Level 2 control requirements specified in Section
725.985(i) shall prepare and maintain the following records:
i)
Records for the most recent set of calculations and
measurements performed by the owner or operator to
verify that the enclosure meets the criteria of a permanent
total enclosure as specified in “Procedure T--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure” under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code 720.111.
ii)
Records required for the closed-vent system and control
device in accordance with the requirements of subsection
(e) of this Section.
c)
The owner or operator of a surface impoundment using air emission controls in
accordance with the requirements of Section 725.986 shall prepare and maintain
records for the surface impoundment that include the following information:
1)
A surface impoundment identification number (or other unique
identification description as selected by the owner or operator).
2)
Documentation describing the floating membrane cover or cover design,
as applicable to the surface impoundment, that includes information
prepared by the owner or operator or provided by the cover
manufacturer or vendor describing the cover design, and certification by
the owner or operator that the cover meets the specifications listed in
Section 725.986(c).
3)
A record for each inspection required by Section 725.986 that includes
the following information:
A)
Date inspection was conducted.
B)
For each defect detected during the inspection the following
information: the location of the defect, a description of the
302
defect, the date of detection, and corrective action taken to repair
the defect. In the event that repair of the defect is delayed in
accordance with the provisions of Section 725.986(f), the owner
or operator shall also record the reason for the delay and the date
that completion of repair of the defect is expected.
4)
For a surface impoundment equipped with a cover and vented through a
closed-vent system to a control device, the owner or operator shall
prepare and maintain the records specified in subsection (e) of this
Section.
d)
The owner or operator of containers using Container Level 3 air emission
controls in accordance with the requirements of Section 725.987 shall prepare
and maintain records that include the following information:
1)
Records for the most recent set of calculations and measurements
performed by the owner or operator to verify that the enclosure meets
the criteria of a permanent total enclosure as specified in “Procedure T--
Criteria for and Verification of a Permanent or Temporary Total
Enclosure” under 40 CFR 52.741, appendix B, incorporated by
reference in 35 Ill. Adm. Code 720.111.
2)
Records required for the closed-vent system and control device in
accordance with the requirements of subsection (e) of this Section.
e)
The owner or operator using a closed-vent system and control device in
accordance with the requirements of Section 725.988 shall prepare and maintain
records that include the following information:
1)
Documentation for the closed-vent system and control device that
includes:
A)
Certification that is signed and dated by the owner or operator
stating that the control device is designed to operate at the
performance level documented by a design analysis as specified
in subsection (e)(1)(B) of this Section or by performance tests as
specified in subsection (e)(1)(C) of this Section when the tank,
surface impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to occur.
B)
If a design analysis is used, then design documentation, as
specified in Section 725.1035725.935(b)(4). The documentation
must include information prepared by the owner or operator or
provided by the control device manufacturer or vendor that
describes the control device design in accordance with Section
303
725.1035725.935(b)(4)(C) and certification by the owner or
operator that the control equipment meets the applicable
specifications.
C)
If performance tests are used, then a performance test plan as
specified in Section 265.935725.935(b)(3) and all test results.
D)
Information as required by 40 CFR 265.1035(c)(1)Section
725.935(c)(1) and Section 725.935(c)(2), as applicable.
E)
An owner or operator shall record, on a semiannual basis, the
information specified in subsections (e)(1)(E)(i) and (e)(1)(E)(ii)
of this Section for those planned routine maintenance operations
that would require the control device not to meet the
requirements of Section 725.988(c)(1)(A), (c)(1)(B), or
(c)(1)(C), as applicable.
i)
A description of the planned routine maintenance that is
anticipated to be performed for the control device during
the next six-month period. This description must include
the type of maintenance necessary, planned frequency of
maintenance, and lengths of maintenance periods.
ii)
A description of the planned routine maintenance that was
performed for the control device during the previous six-
month period. This description must include the type of
maintenance performed and the total number of hours
during those six months that the control device did not
meet the requirements of Section 725.988(c)(1)(A),
(c)(1)(B), or (c)(1)(C), as applicable, due to planned
routine maintenance.
F)
An owner or operator shall record the information specified in
subsections (e)(1)(F)(i) through (e)(1)(F)(iii) of this Section for
those unexpected control device system malfunctions that would
require the control device not to meet the requirements of Section
725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as applicable.
i)
The occurrence and duration of each malfunction of the
control device system.
ii)
The duration of each period during a malfunction when
gases, vapors, or fumes are vented from the waste
management unit through the closed-vent system to the
304
control device while the control device is not properly
functioning.
iii)
Actions taken during periods of malfunction to restore a
malfunctioning control device to its normal or usual
manner of operation.
G)
Records of the management of carbon removed from a carbon
adsorption system conducted in accordance with Section
725.988(c)(3)(B).
f)
The owner or operator of a tank, surface impoundment, or container exempted
from standards in accordance with the provisions of Section 725.983(c) of this
Subpart shall prepare and maintain the following records, as applicable:
1)
For tanks, surface impoundments, or containers exempted under the
hazardous waste organic concentration conditions specified in Section
725.983 (c)(1) or (c)(2) of this Subpart, the owner or operator shall
record the information used for each waste determination (e.g., test
results, measurements, calculations, and other documentation) in the
facility operating log. If analysis results for waste samples are used for
the waste determination, then the owner or operator shall record the
date, time, and location that each waste sample is collected in
accordance with applicable requirements of Section 725.984 of this
Subpart.
2)
For tanks, surface impoundments, or containers exempted under the
provisions of Section 725.983(c)(2)(vii)(G) or Section
725.983(c)(2)(viii)(H) of this Subpart, the owner or operator shall record
the identification number for the incinerator, boiler, or industrial furnace
in which the hazardous waste is treated.
g)
An owner or operator designating a cover as “unsafe to inspect and monitor”
pursuant to Section 725.985(l) shall record in a log that is kept in the facility
operating record the following information: the identification numbers for
waste management units with covers that are designated as “unsafe to inspect
and monitor”, the explanation for each cover stating why the cover is unsafe to
inspect and monitor, and the plan and schedule for inspecting and monitoring
each cover.
h)
The owner or operator of a facility that is subject to this Subpart and to the
control device standards in 40 CFR 60, Subpart VV, or 40 CFR 61, Subpart V,
incorporated by reference in 35 Ill. Adm. Code 270.111, may elect to
demonstrate compliance with the applicable Sections of this Subpart by
documentation either pursuant to this Subpart, or pursuant to the provisions of
305
40 CFR 60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
documentation required by 40 CFR 60 or 61 duplicates the documentation
required by this Section.
i)
For each tank or container not using air emission controls specified in Sections
725.985 through 725.988 in accordance with the conditions specified in Section
725.980(d), the owner or operator shall record and maintain the following
information:
1)
A list of the individual organic peroxide compounds manufactured at the
facility that meet the conditions specified in Section 725.980(d)(1).
2)
A description of how the hazardous waste containing the organic
peroxide compounds identified pursuant to subsection (i)(1) are managed
at the facility in tanks and containers. This description must include the
following information:
A)
For the tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to describe each tank: a
facility identification number for the tank, the purpose and
placement of this tank in the management train of this hazardous
waste, and the procedures used to ultimately dispose of the
hazardous waste managed in the tanks.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to describe the
following for each container: a facility identification number for
the container or group of containers; the purpose and placement
of this container or group of containers in the management train
of this hazardous waste; and the procedures used to ultimately
dispose of the hazardous waste handled in the containers.
3)
An explanation of why managing the hazardous waste containing the
organic peroxide compounds identified pursuant to subsection (i)(1) of
this Section in the tanks or containers identified pursuant to subsection
(i)(2) of this Section would create an undue safety hazard if the air
emission controls specified in Sections 725.985 through 725.988 were
installed and operated on these waste management units. This
explanation must include the following information:
A)
For tanks used at the facility to manage this hazardous waste,
sufficient information must be provided to explain: how use of
the required air emission controls on the tanks would affect the
tank design features and facility operating procedures currently
used to prevent an undue safety hazard during the management of
306
this hazardous waste in the tanks; and why installation of safety
devices on the required air emission controls, as allowed under
this Subpart, would not address those situations in which
evacuation of tanks equipped with these air emission controls is
necessary and consistent with good engineering and safety
practices for handling organic peroxides.
B)
For containers used at the facility to manage this hazardous
waste, sufficient information must be provided to explain: how
use of the required air emission controls on the containers would
affect the container design features and handling procedures
currently used to prevent an undue safety hazard during
management of this hazardous waste in the containers; and why
installation of safety devices on the required air emission
controls, as allowed under this Subpart, would not address those
situations in which evacuation of containers equipped with these
air emission controls is necessary and consistent with good
engineering and safety practices for handling organic peroxides.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART EE: HAZARDOUS WASTE MUNITIONS AND EXPLOSIVES
STORAGE
Section 725.1200 Applicability
The requirements of this Subpart EE apply to owners or operators who store munitions and
explosive hazardous wastes, except as Section 725.101 provides otherwise.
BOARD NOTE: Depending on explosive hazards, hazardous waste munitions and explosives
may also be managed in other types of storage units, including containment buildings (Subpart
DD of this Part), tanks (Subpart J of this Part), or containers (Subpart I of this Part); see 35
Ill. Adm. Code 726.305 for storage of waste military munitions.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 725.1201 Design and Operating Standards
a) An owner or operator of a hazardous waste munitions and explosives storage
unit shall design and operate the unit with containment systems, controls, and
monitoring that fulfill each of the following requirements:
1) The owner or operator minimizes the potential for detonation or other
means of release of hazardous waste, hazardous constituents, hazardous
307
decomposition products, or contaminated run-off to the soil, ground
water, surface water, and atmosphere;
2) The owner or operator provides a primary barrier, which may be a
container (including a shell) or tank, designed to contain the hazardous
waste;
3) For wastes stored outdoors, the owner or operator provides that the
waste and containers will not be in standing precipitation;
4) For liquid wastes, the owner or operator provides a secondary
containment system that assures that any released liquids are contained
and promptly detected and removed from the waste area or a vapor
detection system that assures that any released liquids or vapors are
promptly detected and an appropriate response taken (e.g., additional
containment, such as overpacking or removal from the waste area); and
5) The owner or operator provides monitoring and inspection procedures
that assure the controls and containment systems are working as designed
and that releases that may adversely impact human health or the
environment are not escaping from the unit.
b) Hazardous waste munitions and explosives stored under this Subpart EE may be
stored in one of the following:
1) Earth-covered magazines. The owner or operator of an earth-covered
magazine shall fulfill each of the following requirements:
A) The magazine is constructed of waterproofed, reinforced concrete
or structural steel arches, with steel doors that are kept closed
when not being accessed;
B) The magazine is so designed and constructed that it fulfills each
of the following requirements:
i) The magazine is of sufficient strength and thickness to
support the weight of any explosives or munitions stored
and any equipment used in the unit;
ii) The magazine provides working space for personnel and
equipment in the unit; and
iii) The magazine can withstand movement activities that
occur in the unit; and
308
C) The magazine is located and designed, with walls and earthen
covers that direct an explosion in the unit in a safe direction, so
as to minimize the propagation of an explosion to adjacent units
and to minimize other effects of any explosion.
2) Above-ground magazines. Above-ground magazines must be located
and designed so as to minimize the propagation of an explosion to
adjacent units and to minimize other effects of any explosion.
3) Outdoor or open storage areas. Outdoor or open storage areas must be
located and designed so as to minimize the propagation of an explosion
to adjacent units and to minimize other effects of any explosion.
c) An owner or operator shall store hazardous waste munitions and explosives in
accordance with a Standard Operating Procedure that specifies procedures which
ensure safety, security, and environmental protection. If these procedures serve
the same purpose as the security and inspection requirements of Section
725.114, the preparedness and prevention procedures of Subpart C of this Part,
and the contingency plan and emergency procedures requirements of Subpart of
this Part, then the Standard Operating Procedure may be used to fulfill those
requirements.
d) An owner or operator shall package hazardous waste munitions and explosives
to ensure safety in handling and storage.
e) An owner or operator shall inventory hazardous waste munitions and explosives
at least annually.
f) An owner or operator shall inspect and monitor hazardous waste munitions and
explosives and their storage units as necessary to ensure explosives safety and to
ensure that there is no migration of contaminants out of the unit.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 725.1202 Closure and Post-Closure Care
a) At closure of a magazine or unit that stored hazardous waste under this Subpart,
the owner or operator shall remove or decontaminate all waste residues,
contaminated containment system components, contaminated subsoils, and
structures and equipment contaminated with waste and manage them as
hazardous waste unless 35 Ill. Adm. Code 721.103(d) applies. The closure
plan, closure activities, cost estimates for closure, and financial responsibility
for magazines or units must meet all of the requirements specified in Subparts G
and H of this Part, except that the owner or operator may defer closure of the
309
unit as long as it remains in service as a munitions or explosives magazine or
storage unit.
b) If, after removing or decontaminating all residues and making all reasonable
efforts to effect removal or decontamination of contaminated components,
subsoils, structures, and equipment as required in subsection (a) of this Section,
the owner or operator finds that not all contaminated subsoils can be practicably
removed or decontaminated, the owner or operator shall close the facility and
perform post-closure care in accordance with the closure and post-closure
requirements that apply to landfills (see 35 Ill. Adm. Code 724.410).
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 725.Appendix F
Compounds With Henry’s Law Constant Less Than 0.1 Y/X (at
25
°
C)
Compound name
CAS No.
Acetaldol
107-89-1
Acetamide
60-35-5
2-Acetylaminofluorene
53-96-3
3-Acetyl-5-hydroxypiperidine
3-Acetylpiperidine
618-42-8
1-Acetyl-2-thiourea
591-08-2
Acrylamide
79-06-1
Acrylic acid
79-10-7
Adenine
73-24-5
Adipic acid
124-04-9
Adiponitrile
111-69-3
Alachlor
15972-60-8
Aldicarb
116-06-3
Ametryn
834-12-8
4-Aminobiphenyl
92-67-1
4-Aminopyridine
504-24-5
Aniline
62-53-3
o-Anisidine
90-04-0
Anthraquinone
84-65-1
Atrazine
1912-24-9
Benzenearsonic acid
98-05-5
Benzenesulfonic acid
98-11-3
Benzidine
92-87-5
Benzo(a)anthracene
56-55-3
Benzo(k)fluoranthene
207-08-9
Benzoic acid
65-85-0
310
Benzo(g,h,i)perylene
191-24-2
Benzo(a)pyrene
50-32-8
Benzyl alcohol
100-51-6
gamma
γ
-BHC
58-89-9
Bis(2-ethylhexyl)phthalate
117-81-7
Bromochloromethyl acetate
Bromoxynil
1689-84-5
Butyric acid
107-92-6
Caprolactam (hexahydro-2H-azepin-2-one)
105-60-2
Catechol (o-dihydroxybenzene)
120-80-9
Cellulose
9004-34-6
Cell wall
Chlorhydrin (3-Chloro-1,2-propanediol)
96-24-2
Chloroacetic acid
79-11-8
2-Chloroacetophenone
93-76-5
p-Chloroaniline
106-47-8
p-Chlorobenzophenone
134-85-0
Chlorobenzylate
510-15-6
p-Chloro-m-cresol (6-chloro-m-cresol)
59-50-7
3-Chloro-2,5-diketopyrrolidine
Chloro-1,2-ethane diol
4-Chlorophenol
106-48-9
Chlorophenol polymers (2-chlorophenol & 4-chlorophenol)
95-57-8 &
106-48-9
1-(o-Chlorophenyl)thiourea
5344-82-1
Chrysene
218-01-9
Citric acid
77-92-9
Creosote
8001-58-9
m-Cresol
108-39-4
o-Cresol
95-48-7
p-Cresol
106-44-5
Cresol (mixed isomers)
1319-77-3
4-Cumylphenol
27576-86
Cyanide
57-12-5
4-Cyanomethyl benzoate
Diazinon
333-41-5
Dibenzo(a,h)anthracene
53-70-3
3,5-Dibromo-4-hydroxybenzonitrile
1689-84-5
Dibutylphthalate
84-74-2
2,5-Dichloroaniline (N,N'-dichloroaniline)
95-82-9
2,6-Dichlorobenzonitrile
1194-65-6
2,6-Dichloro-4-nitroaniline
99-30-9
2,5-Dichlorophenol
3,4-Dichlorotetrahydrofuran
3511-19
Dichlorvos
106-47-8
311
Diethanolamine
111-42-2
N,N-Diethylaniline
91-66-7
Diethylene glycol
111-46-6
Diethylene glycol dimethyl ether (dimethyl Carbitol)
111-96-6
Diethylene glycol monobutyl ether (butyl Carbitol)
112-34-5
Diethylene glycol monoethyl ether acetate (Carbitol acetate)
112-15-2
Diethylene glycol monoethyl ether (Carbitol Cellosolve)
111-90-0
Diethylene glycol monomethyl ether (methyl Carbitol)
111-77-3
N,N'-Diethylhydrazine
1615-80-1
Diethyl(4-methylumbelliferyl)thionophosphate
299-45-6
Diethylphosphorothioate
126-75-0
N,N'-Diethylpropionamide
15299-99-7
Dimethoate
60-51-5
4-Dimethylaminoazobenzene
60-11-7
7,12-Dimethylbenz(a)anthracene
57-97-6
3,3-Dimethylbenzidine
119-93-7
Dimethylcarbamoyl chloride
79-44-7
Dimethyldisulfide
624-92-0
Dimethylformamide
68-12-2
1,1-Dimethylhydrazine
57-14-7
Dimethylphthalate
131-11-3
Dimethylsulfone
67-71-0
Dimethylsulfoxide
67-68-5
2,3-Dimethoxystrychnidin-10-one
357-57-3
4,6-Dinitro-o-cresol
534-52-1
1,2-Diphenylhydrazine
122-66-7
Dipropylene glycol (1,1'-oxydi-2-propanol)
110-98-5
Endrin
72-20-8
Epinephrine
51-43-4
Ethyl carbamate (urethane)
51-79-6
Ethylene glycol
107-21-1
Ethylene glycol monobutyl ether (butyl Cellosolve)
111-76-2
Ethylene glycol monoethyl ether (Cellosolve)
110-80-5
Ethylene glycol monoethyl ether acetate (Cellosolve acetate)
111-15-9
Ethylene glycol monomethyl ether (methyl Cellosolve)
109-86-4
Ethylene glycol monophenyl ether (phenyl Cellosolve)
122-99-6
Ethylene glycol monopropyl ether (propyl Cellosolve)
2807-30-9
Ethylene thiourea (2-imidazolidinethione)
9-64-57
4-Ethylmorpholine
100-74-3
3-Ethylphenol
620-17-7
Fluoroacetic acid, sodium salt
62-74-8
Formaldehyde
50-00-0
Formamide
75-12-7
Formic acid
64-18-6
Fumaric acid
110-17-8
312
Glutaric acid
110-94-1
Glycerin (Glycerol)
56-81-5
Glycidol
556-52-5
Glycinamide
598-41-4
Glyphosate
1071-83-6
Guthion
86-50-0
Hexamethylene-1,6-diisocyanate (1,6-diisocyanatohexane)
822-06-0
Hexamethyl phosphoramide
680-31-9
Hexanoic acid
142-62-1
Hydrazine
302-01-2
Hydrocyanic acid
74-90-8
Hydroquinone
123-31-9
Hydroxy-2-propionitrile (hydracrylonitrile)
109-78-4
Indeno(1,2,3-cd)pyrene
193-39-5
Lead acetate
301-04-2
Lead subacetate (lead acetate, monobasic)
1335-32-6
Leucine
61-90-5
Malathion
121-75-5
Maleic acid
110-16-7
Maleic anhydride
108-31-6
Mesityl oxide
141-79-7
Methane sulfonic acid
75-75-2
Methomyl
16752-77-5
p-Methoxyphenol
150-76-5
Methylacrylate
96-33-3
4,4'-Methylene-bis-(2-chloroaniline)
101-14-4
4,4'-Methylenediphenyl diisocyanate (diphenyl methane diisocyanate)
101-68-8
4,4'-Methylenedianiline
101-77-9
Methylene diphenylamine (MDA)
5-Methylfurfural
620-02-0
Methylhydrazine
60-34-4
Methyliminoacetic acid
Methyl methane sulfonate
66-27-3
1-Methyl-2-methoxyaziridine
Methylparathion
298-00-0
Methyl sulfuric acid (sulfuric acid, dimethyl ester)
77-78-1
4-Methylthiophenol
106-45-6
Monoethanolamine
141-43-5
Monomethylformamide (N-methylformamide)
123-39-7
Nabam
142-59-6
alpha
α
-Naphthol
90-15-3
beta
β
-Naphthol
135-19-3
alpha
α
-Naphthylamine
134-32-7
beta
β
-Naphthylamine
91-59-8
Neopentyl glycol
126-30-7
313
Niacinamide
98-92-0
o-Nitroaniline
88-74-4
Nitroglycerin
55-63-0
2-Nitrophenol
88-75-5
4-Nitrophenol
100-02-7
N-Nitrosodimethylamine
62-75-9
Nitrosoguanidine
674-81-7
N-Nitroso-n-methylurea
684-93-5
N-Nitrosomorpholine (4-nitrosomorpholine)
59-89-2
Oxalic acid
144-62-7
Parathion
56-38-2
Pentaerythritol
115-77-5
Phenacetin
62-44-2
Phenol
108-95-2
Phenylacetic acid
103-82-2
m-Phenylene diamine
108-45-2
o-Phenylene diamine
95-54-5
p-Phenylene diamine
106-50-3
Phenyl mercuric acetate
62-38-4
Phorate
298-02-2
Phthalic anhydride
85-44-9
alpha
α
-Picoline (2-methyl pyridine)
109-06-8
1,3-Propane sulfone
1120-71-4
beta
β
-Propiolactone
57-57-8
Proporur (Baygon)
Propylene glycol
57-55-6
Pyrene
129-00-0
Pyridinium bromide
39416-48-3
Quinoline
91-22-5
Quinone (p-benzoquinone)
106-51-4
Resorcinol
108-46-3
Simazine
122-34-9
Sodium acetate
127-09-3
Sodium formate
141-53-7
Strychnine
57-24-9
Succinic acid
110-15-6
Succinimide
123-56-8
Sulfanilic acid
121-47-1
Terephthalic acid
100-21-0
Tetraethyldithiopyrophosphate
3689-24-5
Tetraethylenepentamine
112-57-2
Thiofanox
39196-18-4
Thiosemicarbazide
79-19-6
2,4-Toluenediamine
95-80-7
2,6-Toluenediamine
823-40-5
314
3,4-Toluenediamine
496-72-0
2,4-Toluene diisocyanate
584-84-9
p-Toluic acid
99-94-5
m-Toluidine
108-44-1
1,1,2-Trichloro-1,2,2-trifluoroethane
76-13-1
Triethanolamine
102-71-6
Triethylene glycol dimethyl ether
Tripropylene glycol
24800-44-0
Warfarin
81-81-2
3,4-Xylenol (3,4-dimethylphenol)
95-65-8
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 726
STANDARDS FOR THE MANAGEMENT OF SPECIFIC HAZARDOUS
WASTE AND SPECIFIC TYPES OF HAZARDOUS WASTE
MANAGEMENT FACILITIES
SUBPART C: RECYCLABLE MATERIALS USED IN A MANNER
CONSTITUTING DISPOSAL
Section
726.120
Applicability
726.121
Standards applicable to generators and transporters of materials used in a
manner that constitutes disposal
726.122
Standards applicable to storers, who are not the ultimate users, of materials that
are to be used in a manner that constitutes disposal
726.123
Standards Applicable to Users of Materials that are Used in a Manner that
Constitutes Disposal
SUBPART D: HAZARDOUS WASTE BURNED FOR ENERGY
RECOVERY
Section
726.130
Applicability (Repealed)
726.131
Prohibitions (Repealed)
726.132
Standards applicable to generators of hazardous waste fuel (Repealed)
726.133
Standards applicable to transporters of hazardous waste fuel (Repealed)
726.134
Standards applicable to marketers of hazardous waste fuel (Repealed)
726.135
Standards applicable to burners of hazardous waste fuel (Repealed)
315
726.136
Conditional exemption for spent materials and by-products exhibiting a
characteristic of hazardous waste (Repealed)
SUBPART E: USED OIL BURNED FOR ENERGY RECOVERY (Repealed)
Section
726.140
Applicability (Repealed)
726.141
Prohibitions (Repealed)
726.142
Standards applicable to generators of used oil burned for energy recovery
(Repealed)
726.143
Standards applicable to marketers of used oil burned for energy recovery
(Repealed)
726.144
Standards applicable to burners of used oil burned for energy recovery
(Repealed)
SUBPART F: RECYCLABLE MATERIALS UTILIZED FOR PRECIOUS
METAL RECOVERY
Section
726.170
Applicability and requirements
SUBPART G: SPENT LEAD-ACID BATTERIES BEING RECLAIMED
Section
726.180
Applicability and requirements
SUBPART H: HAZARDOUS WASTE BURNED IN BOILERS AND
INDUSTRIAL FURNACES
Section
726.200
Applicability
726.201
Management prior to Burning
726.202
Permit standards for Burners
726.203
Interim Status Standards for Burners
726.204
Standards to Control Organic Emissions
726.205
Standards to control PM
726.206
Standards to Control Metals Emissions
726.207
Standards to control HCl and Chlorine Gas Emissions
726.208
Small quantity On-site Burner Exemption
726.209
Low risk waste Exemption
726.210
Waiver of DRE trial burn for Boilers
726.211
Standards for direct Transfer
726.212
Regulation of Residues
726.219
Extensions of Time
SUBPART M: MILITARY MUNITIONS
Section
726.300 Applicability
726.301 Definitions
316
726.302 Definition of Solid Waste
726.303 Standards Applicable to the Transportation of Solid Waste Military Munitions
726.304 Standards Applicable to Emergency Responses
726.305 Standards Applicable to the Storage of Solid Waste Military Munitions
726.306 Standards Applicable to the Treatment and Disposal of Waste Military
Munitions
726.Appendix A
Tier I and Tier II Feed Rate and Emissions Screening Limits for Metals
726.Appendix B
Tier I Feed Rate Screening Limits for Total Chlorine
726.Appendix C
Tier II Emission Rate Screening Limits for Free Chlorine and Hydrogen
Chloride
726.Appendix D
Reference Air Concentrations
726.Appendix E
Risk Specific Doses
726.Appendix F
Stack Plume Rise
726.Appendix G
Health-Based Limits for Exclusion of Waste-Derived Residues
726.Appendix H
Potential PICs for Determination of Exclusion of Waste-Derived
Residues
726.Appendix I
Methods Manual for Compliance with BIF Regulations
726.Appendix J
Guideline on Air Quality Models
726.Appendix K
Lead-Bearing Materials That May be Processed in Exempt Lead
Smelters
726.Appendix L
Nickel or Chromium-Bearing Materials that may be Processed in Exempt
Nickel-Chromium Recovery Furnaces
726.Appendix M
Mercury-Bearing Wastes That May Be Processed in Exempt Mercury
Recovery Units
726.Table A
Exempt Quantities for Small Quantity Burner Exemption
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R85-22 at 10 Ill. Reg. 1162, effective January 2, 1986; amended in R86-1 at 10 Ill. Reg
.
14156, effective August 12, 1986; amended in R87-26 at 12 Ill. Reg. 2900, effective January 15, 1988; amended
in R89-1 at 13 Ill. Reg. 18606, effective November 13, 1989; amended in R90-2 at 14 Ill. Reg. 14533, effective
August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9727, effective June 17, 1991; amended in R91-13 at 16 Ill.
Reg. 9858, effective June 9, 1992; amended in R92-10 at 17 Ill. Reg. 5865, effective March 26, 1993; amended in
R93-4 at 17 Ill. Reg. 20904, effective November 22, 1993; amended in R94-7 at 18 Ill. Reg. 12500, effective July
29, 1994; amended in R95-6 at 19 Ill. Reg. 10006, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg.
11263, effective August 1, 1996; amended in R96-10/R97-3/R97-5 at 22 Ill. Reg. 754, effective December 16,
1997; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg. ________, effective ______________________.
SUBPART H: HAZARDOUS WASTE BURNED IN BOILERS AND
INDUSTRIAL FURNACES
Section 726.204
Standards to Control Organic Emissions
a)
DRE standard.
317
1)
General. Except as provided in subsection (a)(3) above of this Section, a
BIF burning hazardous waste must achieve a DRE of 99.99% percent for
all organic hazardous constituents in the waste feed. To demonstrate
conformance with this requirement, 99.99% percent DRE must be
demonstrated during a trial burn for each principal organic hazardous
constituent (POHC) designated (under subsection (a)(2) above of this
Section) in its permit for each waste feed. DRE is determined for each
POHC from the following equation:
DRE = 100(I - O)/I
DRE = 100
(I - O)
I
where:
I =
Mass feed rate of one POHC in the hazardous
waste fired to the BIF; and
O =
Mass emission rate of the same POHC present in
stack gas prior to release to the atmosphere.
2)
Designation of POHCs. POHCs are those compounds for which
compliance with the DRE requirements of this Section must be
demonstrated in a trial burn in conformance with procedures prescribed
in 35 Ill. Adm. Code 703.232. One or more POHCs must be designated
by the Agency for each waste feed to be burned. POHCs must be
designated based on the degree of difficulty of destruction of the organic
constituents in the waste and on their concentrations or mass in the waste
feed considering the results of waste analyses submitted with Part B of
the permit application. POHCs are most likely to be selected from
among those compounds listed in 35 Ill. Adm. Code 721.Appendix H
that are also present in the normal waste feed. However, if the applicant
demonstrates to the Agency that a compound not listed in 35 Ill. Adm.
Code 721.Appendix H or not present in the normal waste feed is a
suitable indicator of compliance with the DRE requirements of this
Section, that compound must be designated as a POHC. Such POHCs
need not be toxic or organic compounds.
3)
Dioxin-listed waste. A BIF burning hazardous waste containing (or
derived from) USEPA Hazardous Wastes Nos. F020, F021, F022,
F023, F026 or F027 must achieve a destruction and removal efficiency
(DRE) of 99.9999% percent for each POHC designated (under
subsection (a)(2) above of this Section) in its permit. This performance
318
must be demonstrated on POHCs that are more difficult to burn than
tetra-, penta- and hexachlorodibenzo-p-dioxins and dibenzofurans. DRE
is determined for each POHC from the equation in subsection (a)(1)
above of this Section. In addition, the owner or operator of the BIF
shall notify the Agency of intent to burn USEPA Hazardous Waste Nos.
F020, F021, F022, F023, F026 or F027.
4)
Automatic waiver of DRE trial burn. Owners and operators of boilers
operated under the special operating requirements provided by Section
726.210 are considered to be in compliance with the DRE standard of
subsection (a)(1) above of this Section and are exempt from the DRE
trial burn.
5)
Low risk waste. Owners and operators of BIFs that burn hazardous
waste in compliance with the requirements of Section 726.209(a) are
considered to be in compliance with the DRE standard of subsection
(a)(1) above of this Section and are exempt from the DRE trial burn.
b)
CO standard.
1)
Except as provided in subsection (c) below of this Section, the stack gas
concentration of CO from a BIF burning hazardous waste cannot exceed
100 ppmv on an hourly rolling average basis (i.e., over any 60 minute
period), continuously corrected to 7 percent oxygen, dry gas basis.
2)
CO and oxygen must be continuously monitored in conformance with
“Performance Specifications for Continuous Emission Monitoring of
Carbon Monoxide and Oxygen for Incinerators, Boilers, and Industrial
Furnaces Burning Hazardous Waste” in Section 726.Appendix I.
3)
Compliance with the 100 ppmv CO limit must be demonstrated during
the trial burn (for new facilities or an interim status facility applying for
a permit) or the compliance test (for interim status facilities). To
demonstrate compliance, the highest hourly rolling average CO level
during any valid run of the trial burn or compliance test must not exceed
100 ppmv.
c)
Alternative CO standard.
1)
The stack gas concentration of CO from a BIF burning hazardous waste
may exceed the 100 ppmv limit provided that stack gas concentrations of
HCs do not exceed 20 ppmv, except as provided by subsection (f) below
of this Section for certain industrial furnaces.
319
2)
HC limits must be established under this Section on an hourly rolling
average basis (i.e., over any 60 minute period), reported as propane, and
continuously corrected to 7 percent oxygen, dry gas basis.
3)
HC must be continuously monitored in conformance with “Performance
Specifications for Continuous Emission Monitoring of Hydrocarbons for
Incinerators, Boilers, and Industrial Furnaces Burning Hazardous Waste”
in Section 726.Appendix I. CO and oxygen must be continuously
monitored in conformance with subsection (b)(2) above of this Section.
4)
The alternative CO standard is established based on CO data during the
trial burn (for a new facility) and the compliance test (for an interim
status facility). The alternative CO standard is the average over all valid
runs of the highest hourly average CO level for each run. The CO limit
is implemented on an hourly rolling average basis, and continuously
corrected to 7 percent oxygen, dry gas basis.
d)
Special requirements for furnaces. Owners and operators of industrial furnaces
(e.g., kilns, cupolas) that feed hazardous waste for a purpose other than solely
as an ingredient (see Section 726.203(a)(5)(B)) at any location other than the
end where products are normally discharged and where fuels are normally fired
must comply with the HC limits provided by subsections subsection (c) above or
(f) below of this Section irrespective of whether stack gas CO concentrations
meet the 100 ppmv limit of subsection (b) above of this Section.
e)
Controls for dioxins and furans. Owners and operators of BIFs that are
equipped with a dry PM control device that operates within the temperature
range of 450 through 750° F, and industrial furnaces operating under an
alternative HC limit established under subsection (f) below of this Section shall
conduct a site-specific risk assessment as follows to demonstrate that emissions
of chlorinated dibenzo-p-dioxins and dibenzofurans do not result in an increased
lifetime cancer risk to the hypothetical maximum exposed individual (MEI)
exceeding 1
×
10
-5
(1 in 100,000):
1)
During the trial burn (for new facilities or an interim status facility
applying for a permit) or compliance test (for interim status facilities),
determine emission rates of the tetra-octa congeners of chlorinated
dibenzo-p-dioxins (PCDDs) and dibenzofurans (CDDs/CDFs) using
Method 0023A, “Determination of Polychlorinated Dibenzo-p-Dioxins
and Polychlorinated Dibenzofurans (PCDFs) from Stationary Sources”,
in Section 726.Appendix I “Sampling Method for Polychlorinated
Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans Emissions from
Stationary Sources,” USEPA Publication SW-846, incorporated by
reference in 35 Ill. Adm. Code 720.111;
320
2)
Estimate the 2,3,7,8-TCDD toxicity equivalence of the tetra-octa
CDDs/CDFs congeners using “Procedures for Estimating the Toxicity
Equivalence of Chlorinated Dibenzo-p-Dioxin and Dibenzofuran
Congeners” in Section 726.Appendix I. Multiply the emission rates of
CDD/CDF congeners with a toxicity equivalence greater than zero (see
the procedure) by the calculated toxicity equivalence factor to estimate
the equivalent emission rate of 2,3,7,8-TCDD;
3)
Conduct dispersion modeling using methods recommended in 40 CFR
51, Appendix W, as incorporated by reference at 35 Ill. Adm. Code
720.111 (“Guideline on Air Quality Models (Revised)” (1986) and its
supplements), the “Hazardous Waste Combustion Air Quality Screening
Procedure”, provided in Appendix I, or in “Screening Procedures for
Estimating Air Quality Impact of Stationary Sources, Revised”
(incorporated by reference in 35 Ill. Adm. Code 720.111) to predict the
maximum annual average off-site ground level concentration of 2,3,7,8-
TCDD equivalents determined under subsection (e)(2) above of this
Section. The maximum annual average on-site concentration must be
used when a person resides on-site; and
4)
The ratio of the predicted maximum annual average ground level
concentration of 2,3,7,8-TCDD equivalents to the risk-specific dose
(RSD) for 2,3,7,8-TCDD provided in Section 726.Appendix E (2.2´10
-
7
) must not exceed 1.0.
f)
Monitoring CO and HC in the by-pass duct of a cement kiln. Cement kilns may
comply with the CO and HC limits provided by subsections (b), (c) and (d)
above of this Section by monitoring in the by-pass duct provided that:
1)
Hazardous waste is fired only into the kiln and not at any location
downstream from the kiln exit relative to the direction of gas flow; and
2)
The by-pass duct diverts a minimum of 10% percent of kiln off-gas into
the duct.
g)
Use of emissions test data to demonstrate compliance and establish operating
limits. Compliance with the requirements of this Section must be demonstrated
simultaneously by emissions testing or during separate runs under identical
operating conditions. Further, data to demonstrate compliance with the CO and
HC limits of this Section or to establish alternative CO or HC limits under this
Section must be obtained during the time that DRE testing, and where
applicable, CDD/CDF testing under subsection (e) above of this Section and
comprehensive organic emissions testing under subsection (f) above of this
Section is conducted.
321
h)
Enforcement. For the purposes of permit enforcement, compliance with the
operating requirements specified in the permit (under Section 726.202) will be
regarded as compliance with this Section. However, evidence that compliance
with those permit conditions is insufficient to ensure compliance with the
requirements of this Section is “information” justifying modification or
revocation and re-issuance of a permit under 35 Ill. Adm. Code 703.270 et seq.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 726.206
Standards to Control Metals Emissions
a)
General. The owner or operator shall comply with the metals standards
provided by subsections (b), (c), (d), (e) or (f) below of this Section for each
metal listed in subsection (b) below of this Section that is present in the
hazardous waste at detectable levels using analytical procedures specified in Test
Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW-846,
incorporated by reference in 35 Ill. Adm. Code 720.111.
b)
Tier I feed rate screening limits. Feed rate screening limits for metals are
specified in Section 726.Appendix A as a function of terrain-adjusted effective
stack height (TESH) and terrain and land use in the vicinity of the facility.
Criteria for facilities that are not eligible to comply with the screening limits are
provided in subsection (b)(7) below of this Section.
1)
Noncarcinogenic metals. The feed rates of the noncarcinogenic metals
in all feed streams, including hazardous waste, fuels and industrial
furnace feed stocks must not exceed the screening limits specified in
Section 726.Appendix A.
A)
The feed rate screening limits for antimony, barium, mercury,
thallium and silver are based on either:
i)
An hourly rolling average as defined in Sections
726.200(g) and 726.202(e)(6)(A)(ii); or
ii)
An instantaneous limit not to be exceeded at any time.
B)
The feed rate screening limit for lead is based on one of the
following:
i)
An hourly rolling average as defined in Sections
726.200(g) and 726.202(e)(6)(A)(ii);
ii)
An averaging period of 2 to 24 hours as defined in Section
726.202(e)(6)(B) with an instantaneous feed rate limit not
322
to exceed 10 times the feed rate that would be allowed on
an hourly rolling average basis; or
iii)
An instantaneous limit not to be exceeded at any time.
2)
Carcinogenic metals.
A)
The feed rates of carcinogenic metals in all feed streams,
including hazardous waste, fuels and industrial furnace feed
stocks must not exceed values derived from the screening limits
specified in Section 726.Appendix A. The feed rate of each of
these metals is limited to a level such that the sum of the ratios of
the actual feed rate to the feed rate screening limit specified in
Section 726.Appendix A must not exceed 1.0, as provided by the
following equation:
i=1
n
i
i
A
F
1.0
∑
≤
i =1
n
i
i
A
F
1.0
∑
≤
where:
Σ
A
i
/F
i
means the sum of the values of A/F for
each metal “i”, from i = 1 to n.
n =
number of carcinogenic metals.
A
i
=
the actual feed rate to the device for metal
“i”.
F
i
=
the feed rate screening limit provided by
Section 726.Appendix A for metal “i”.
B)
The feed rate screening limits for the carcinogenic metals are
based on either:
i)
An hourly rolling average; or
ii)
An averaging period of 2 to 24 hours, as defined in
Section 726.202(e)(6)(B), with an instantaneous feed rate
limit not to exceed 10 times the feed rate that would be
allowed on an hourly rolling average basis.
323
3)
TESH (terrain adjusted effective stack height).
A)
The TESH is determined according to the following equation:
TESH = H + P - T
where:
H =
Actual physical stack height (m).
P =
Plume rise (in m) as determined from
Section 726.Appendix F as a function of
stack flow rate and stack gas exhaust
temperature.
T =
Terrain rise (in m) within five kilometers of
the stack.
B)
The stack height (H) must not exceed good engineering practice
stack height, as defined in Section 726.200(g).
C)
If the TESH calculated pursuant to subsection (b)(3)(A) above of
this Section is not listed in Sections 726.Appendix A through
726.Appendix C, the values for the nearest lower TESH listed in
the table must be used. If the TESH is four meters or less, a
value based on four meters must be used.
4)
Terrain type. The screening limits are a function of whether the facility
is located in noncomplex or complex terrain. A device located where
any part of the surrounding terrain within 5 five kilometers of the stack
equals or exceeds the elevation of the physical stack height (H) is
considered to be in complex terrain and the screening limits for complex
terrain apply. Terrain measurements are to be made from U.S.
Geological Survey 7.5-minute topographic maps of the area surrounding
the facility.
5)
Land use. The screening limits are a function of whether the facility is
located in an area where the land use is urban or rural. To determine
whether land use in the vicinity of the facility is urban or rural,
procedures provided in Section 726.Appendix I or Section 726.Appendix
J shall be used.
6)
Multiple stacks. Owers and operators of facilities with more than one
on-site stack from a BIF, incinerator or other thermal treatment unit
324
subject to controls of metals emissions under a RCRA permit or interim
status controls shall comply with the screening limits for all such units
assuming all hazardous waste is fed into the device with the worst-case
stack based on dispersion characteristics. The stack with the lowest
value of K is the worst-case stack. K is determined from the following
equation as applied to each stack:
K = H
×
V
×
T
Where:
K =
a parameter accounting for relative influence of
stack height and plume rise;
H =
physical stack height (meters);
V =
stack gas flow rate (m3/sec (cubic meters per
second); and
T =
exhaust temperature (degrees K).
7)
Criteria for facilities not eligible for screening limits. If any criteria
below are met, the Tier I (and Tier II) screening limits do not apply.
Owners and operators of such facilities shall comply with either the Tier
III standards provided by subsection (d) below of this Section or with the
adjusted Tier I feed rate screening limits provided by subsection (e)
below of this Section.
A)
The device is located in a narrow valley less than one kilometer
wide;
B)
The device has a stack taller than 20 meters and is located such
that the terrain rises to the physical height within one kilometer
of the facility;
C)
The device has a stack taller than 20 meters and is located within
five kilometers of a shoreline of a large body of water such as an
ocean or large lake; or
D)
The physical stack height of any stack is less than 2.5 times the
height of any building within five building heights or five
projected building widths of the stack and the distance from the
stack to the closest boundary is within five building heights or
five projected building widths of the associated building; or.
325
E) The Agency determines that standards based on site-specific
dispersion modeling are required.
8)
Implementation. The feed rate of metals in each feedstream must be
monitored to ensure that the feed rate screening limits are not exceeded.
c)
Tier II emission rate screening limits. Emission rate screening limits are
specified in Section 726.Appendix A as a function of TESH and terrain and land
use in the vicinity of the facility. Criteria for facilities that are not eligible to
comply with the screening limits are provided in subsection (b)(7) above of this
Section.
1)
Noncarcinogenic metals. The emission rates of noncarcinogenic metals
must not exceed the screening limits specified in Section 726.Appendix
A.
2)
Carcinogenic metals. The emission rates of carcinogenic metals must
not exceed values derived from the screening limits specified in Section
726.Appendix A. The emission rate of each of these metals is limited to
a level such that the sum of the ratios of the actual emission rate to the
emission rate screening limit specified in Section 726.Appendix A must
not exceed 1.0, as provided by the following equation:
i=1
n
i
i
A
E
1.0
∑
≤
i =1
n
i
i
A
E
1.0
∑
≤
where:
Σ
A
i
/E
i
means the sum of the values of A/E for each
metal “i”, from i = 1 to n.
n =
number of carcinogenic metals.
A
i
=
the actual emission rate to the device for metal “i”.
E
i
=
the emission rate screening limit provided by
Section 726.Appendix A for metal “i”.
3)
Implementation. The emission rate limits must be implemented by
limiting feed rates of the individual metals to levels during the trial burn
(for new facilities or an interim status facility applying for a permit) or
326
the compliance test (for interim status facilities). The feed rate
averaging periods are the same as provided by subsections (b)(1)(A),
(b)(1)(B), and (b)(2)(B) above of this Section. The feed rate of metals in
each feedstream must be monitored to ensure that the feed rate limits for
the feedstreams specified under Sections 726.202 or 726.203 are not
exceeded.
4)
Definitions and limitations. The definitions and limitations provided by
subsection (b) above of this Section and 726.200(g) for the following
terms also apply to the Tier II emission rate screening limits provided by
this subsection (c): TESH, good engineering practice stack height,
terrain type, land use and criteria for facilities not eligible to use the
screening limits.
5)
Multiple stacks.
A)
Owners and operators of facilities with more than one on-site
stack from a BIF, incinerator or other thermal treatment unit
subject to controls on metals emissions under a RCRA permit or
interim status controls shall comply with the emissions screening
limits for any such stacks assuming all hazardous waste is fed
into the device with the worst-case stack based on dispersion
characteristics.
B)
The worst-case stack is determined by procedures provided in
subsection (b)(6) above of this Section.
C)
For each metal, the total emissions of the metal from those stacks
must not exceed the screening limit for the worst-case stack.
d)
Tier III site-specific risk assessment. The requirements of this subsection apply
to facilities complying with either the Tier III or Adjusted Tier I except where
specified otherwise.
1)
General. Conformance with the Tier III metals controls must be
demonstrated by emissions testing to determine the emission rate for
each metal. In addition, conformance with either Tier III or Adjusted
Tier I metals controls must be demonstrated by air dispersion modeling
to predict the maximum annual average off-site ground level
concentration for each metal and a demonstration that acceptable ambient
levels are not exceeded.
2)
Acceptable ambient levels. Sections 726.Appendix D and 726.Appendix
E list the acceptable ambient levels for purposes of this Subpart.
Reference air concentrations (RACs) are listed for the noncarcinogenic
327
metals and 1
×
10
-5
RSDs are listed for the carcinogenic metals. The RSD
for a metal is the acceptable ambient level for that metal provided that
only one of the four carcinogenic metals is emitted. If more than one
carcinogenic metal is emitted, the acceptable ambient level for the
carcinogenic metals is a fraction of the RSD as described in subsection
(d)(3) below of this Section.
3)
Carcinogenic metals. For the carcinogenic metals the sum of the ratios
of the predicted maximum annual average off-site ground level
concentrations (except that on-site concentrations must be considered if a
person resides on site) to the RSD for all carcinogenic metals emitted
must not exceed 1.0 as determined by the following equation:
i=1
n
i
i
P
R
1.0
∑
≤
i=1
n
i
i
P
R
1.0
∑
≤
SUM(Pi/Ri)
≤
1.0
where:
S
Σ
P
i
/R
i
means the sum of the values of P/R for each
metal “i”, from i = 1 to n.
n =
number of carcinogenic metals.
P
i
=
the predicted ambient concentration for metal i.
R
i
=
the RSD for metal i.
4)
Noncarcinogenic metals. For the noncarcinogenic metals, the predicted
maximum annual average off-site ground level concentration for each
metal must not exceed the RAC.
5)
Multiple stacks. Owners and operators of facilities with more than one
on-site stack from a BIF, incinerator or other thermal treatment unit
subject to controls on metals emissions under a RCRA permit or interim
status controls shall conduct emissions testing (except that facilities
complying with Adjusted Tier I controls need not conduct emissions
testing) and dispersion modeling to demonstrate that the aggregate
emissions from all such on-site stacks do not result in an exceedance of
the acceptable ambient levels.
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6)
Implementation. Under Tier III, the metals controls must be
implemented by limiting feed rates of the individual metals to levels
during the trial burn (for new facilities or an interim status facility
applying for a permit) or the compliance test (for interim status
facilities). The feed rate averaging periods are the same as provided by
subsections (b)(1)(A), (b)(1)(B), and (b)(2)(B) above of this Section.
The feed rate of metals in each feedstream must be monitored to ensure
that the feed rate limits for the feedstreams specified under Sections
726.202 or 726.203 are not exceeded.
e)
Adjusted Tier I feed rate screening limits. The owner or operator may adjust
the feed rate screening limits provided by Section 726.Appendix A to account
for site-specific dispersion modeling. Under this approach, the adjusted feed
rate screening limit for a metal is determined by back-calculating from the
acceptable ambient levels provided by Sections 726.Appendix D and
726.Appendix E using dispersion modeling to determine the maximum
allowable emission rate. This emission rate becomes the adjusted Tier I feed
rate screening limit. The feed rate screening limits for carcinogenic metals are
implemented as prescribed in subsection (b)(2) above of this Section.
f)
Alternative implementation approaches.
1)
Pursuant to subsection (f)(2) below of this Section the Agency shall
approve on a case-by-case basis approaches to implement the Tier II or
Tier III metals emission limits provided by subsection (c) or (d) above of
this Section alternative to monitoring the feed rate of metals in each
feedstream.
2)
The emission limits provided by subsection (d) above of this Section
must be determined as follows:
A)
For each noncarcinogenic metal, by back-calculating from the
RAC provided in Section 726.Appendix D to determine the
allowable emission rate for each metal using the dilution factor
for the maximum annual average ground level concentration
predicted by dispersion modeling in conformance with subsection
(h) below of this Section; and
B)
For each carcinogenic metal by:
i)
Back-calculating from the RSD provided in Section
726.Appendix E to determine the allowable emission rate
for each metal if that metal were the only carcinogenic
metal emitted using the dilution factor for the maximum
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annual average ground level concentration predicted by
dispersion modeling in conformance with subsection (h)
below of this Section; and
ii)
If more than one carcinogenic metal is emitted, selecting
an emission limit for each carcinogenic metal not to
exceed the emission rate determined by subsection
(f)(2)(B)(i) above of this Section, such that the sum for all
carcinogenic metals of the ratios of the selected emission
limit to the emission rate determined by that subsection
does not exceed 1.0.
g)
Emission testing.
1)
General. Emission testing for metals must be conducted using the
Multiple Metals Train as described in Section 726.Appendix I Method
0060, “Determinations of Metals in Stack Emissions,” USEPA
Publication SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111.
2)
Hexavalent chromium. Emissions of chromium are assumed to be
hexavalent chromium unless the owner or operator conducts emissions
testing to determine hexavalent chromium emissions using procedures
prescribed in Section 726.Appendix I Method 0061, “Determination of
Hexavalent Chromium Emissions from Stationary Sources,” USEPA
Publication SW-846, incorporated by reference in 35 Ill. Adm. Code
720.111.
h)
Dispersion modeling. Dispersion modeling required under this Section must be
conducted according to methods recommended in 40 CFR 51, appendix W
(“Guideline on Air Quality Models (Revised)” (1986) and its supplements), the
“Hazardous Waste Combustion Air Quality Screening Procedure” described in
Section 726.Appendix I, or in “Screening Procedures for Estimating the Air
Quality Impact of Stationary Sources, Revised” (incorporated by reference in 35
Ill. Adm. Code 720.111) to predict the maximum annual average off-site
ground level concentration. However, on-site concentrations must be
considered when a person resides on-site.
i)
Enforcement. For the purposes of permit enforcement, compliance with the
operating requirements specified in the permit (under Section 726.202) will be
regarded as compliance with this Section. However, evidence that compliance
with those permit conditions is insufficient to ensure compliance with the
requirements of this Section is “information” justifying modification or
revocation and re-issuance of a permit under 35 Ill. Adm. Code 703.270 et seq.
330
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 726.207
Standards to Control HCl and Chlorine Gas Emissions
a)
General. The owner or operator shall comply with the HCl and chlorine gas
controls provided by subsections (b), (c) or (e), below.
b)
Screening limits.
1)
Tier I feed rate screening limits. Feed rate screening limits are specified for
total chlorine in Section 726.Appendix B as a function of TESH and terrain
and land use in the vicinity of the facility. The feed rate of total chlorine
and chloride, both organic and inorganic, in all feed streams, including
hazardous waste, fuels and industrial furnace feed stocks must not exceed
the levels specified.
2)
Tier II emission rate screening limits. Emission rate screening limits for
HCl and chlorine gas are specified in Section 726.Appendix C as a function
of TESH and terrain and land use in the vicinity of the facility. The stack
emission rates of HCl and chlorine gas must not exceed the levels specified.
3)
Definitions and limitations. The definitions and limitations provided by
Section 726.200(g) and 726.206(b) for the following terms also apply to the
screening limits provided by this subsection: TESH, good engineering
practice stack height, terrain type, land use and criteria for facilities not
eligible to use the screening limits.
4)
Multiple stacks. Owners and operators of facilities with more than one on-
site stack from a BIF, incinerator or other thermal treatment unit subject to
controls on HCl or chlorine gas emissions under a RCRA permit or interim
status controls shall comply with the Tier I and Tier II screening limits for
those stacks assuming all hazardous waste is fed into the device with the
worst-case stack based on dispersion characteristics.
A)
The worst-case stack is determined by procedures provided in
Section 726.206(b)(6).
B)
Under Tier I, the total feed rate of chlorine and chloride to all
subject devices must not exceed the screening limit for the worst-
case stack.
C)
Under Tier II, the total emissions of HCl and chlorine gas from all
subject stacks must not exceed the screening limit for the worst-case
stack.
331
c)
Tier III site-specific risk assessments.
1)
General. Conformance with the Tier III controls must be demonstrated by
emissions testing to determine the emission rate for HCl and chlorine gas,
air dispersion modeling to predict the maximum annual average off-site
ground level concentration for each compound, and a demonstration that
acceptable ambient levels are not exceeded.
2)
Acceptable ambient levels. Section 726.Appendix D lists the RACs for HCl
(7 ug/cu m) and chlorine gas (0.4 ug/cu m).
3)
Multiple stacks. Owners and operators of facilities with more than one on-
site stack from a BIF, incinerator or other thermal treatment unit subject to
controls on HCl or chlorine gas emissions under a RCRA permit or interim
status controls shall conduct emissions testing and dispersion modeling to
demonstrate that the aggregate emissions from all such on-site stacks do not
result in an exceedance of the acceptable ambient levels for HCl and
chlorine gas.
d)
Averaging periods. The HCl and chlorine gas controls are implemented by limiting
the feed rate of total chlorine and chloride in all feedstreams, including hazardous
waste, fuels and industrial furnace feed stocks. Under Tier I, the feed rate of total
chlorine and chloride is limited to the Tier I Screening Limits. Under Tier II and
Tier III, the feed rate of total chlorine and chloride is limited to the feed rates during
the trial burn (for new facilities or an interim status facility applying for a permit) or
the compliance test (for interim status facilities). The feed rate limits are based on
either:
1)
An hourly rolling average as defined in Section 726.200(g) and
726.202(e)(6); or
2)
An instantaneous basis not to be exceeded at any time.
e)
Adjusted Tier I feed rate screening limits. The owner or operator may adjust the
feed rate screening limit provided by Section 726.Appendix B to account for site-
specific dispersion modeling. Under this approach, the adjusted feed rate screening
limit is determined by back-calculating from the acceptable ambient level for
chlorine gas provided by Section 726.Appendix D using dispersion modeling to
determine the maximum allowable emission rate. This emission rate becomes the
adjusted Tier I feed rate screening limit.
f)
Emissions testing. Emissions testing for HCl and chlorine gas (Cl
2
) must be
conducted using the procedures described in Section 726.Appendix I (“eye”)
Method 0050 or 0051, USEPA Publication SW-846, incorporated by reference
in 35 Ill. Adm. Code 720.111.
332
g)
Dispersion modeling. Dispersion modeling must be conducted according to the
provisions of Section 726.206(h).
h)
Enforcement. For the purposes of permit enforcement, compliance with the
operating requirements specified in the permit (under Section 726.202) will be
regarded as compliance with this Section. However, evidence that compliance with
those permit conditions is insufficient to ensure compliance with the requirements of
this Section is “information” justifying modification or revocation and re-issuance of
a permit under 35 Ill. Adm. Code 703.270 et seq.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART M: MILITARY MUNITIONS
Section 726.300 Applicability
a) The regulations in this Subpart identify when military munitions become a solid
waste, and, if these wastes are also hazardous under this Subpart M or 35 Ill.
Adm. Code 721, the management standards that apply to these wastes.
b) Unless otherwise specified in this Subpart M, all applicable requirements in 35
Ill. Adm. Code 702, 703, 705, 720 through 726, and 728 apply to waste
military munitions.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.301 Definitions
In addition to the definitions in 35 Ill. Adm. Code 720.110, the following definitions apply to
this Subpart M:
“Active range” means a military range that is currently in service and is being
regularly used for range activities.
“Chemical agents” and “chemical munitions” are defined as in the Department
of Defense Authorization Act of 1986, 50 U.S.C. 1521(j)(1) (1997),
incorporated by reference in 35 Ill. Adm. Code 720.111.
“Director” is as defined in 35 Ill. Adm. Code 702.110.
“Explosives or munitions emergency response specialist” is as defined in 35 Ill.
Adm. Code 720.110.
333
“Explosives or munitions emergency” is as defined in 35 Ill. Adm. Code
720.110.
“Explosives or munitions emergency response” is as defined in 35 Ill. Adm.
Code 720.110.
“Inactive range” means a military range that is not currently being used but
which is still under military control and considered by the military to be a
potential range area and which has not been put to a new use that is
incompatible with range activities.
“Military” means the United States (U.S.) Department of Defense (DOD), the
Armed Services, Coast Guard, National Guard, Department of Energy (DOE)
or other parties under contract or acting as an agent for the foregoing who
handle military munitions.
“Military munitions” is as defined in 35 Ill. Adm. Code 720.110.
“Military range” means designated land and water areas that are set aside;
managed; and used to conduct research on, develop, test, and evaluate military
munitions and explosives, other ordnance, or weapon systems or areas that are
set aside, managed, and used to train military personnel in their use and
handling. Ranges include firing lines and positions, maneuver areas, firing
lanes, test pads, detonation pads, impact areas, and buffer zones with restricted
access and exclusionary areas.
“Unexploded ordnance” or “UXO” means military munitions that have been
primed, fused, armed, or otherwise prepared for action and that have been
fired, dropped, launched, projected, or placed in such a manner as to constitute
a hazard to operations, installation, personnel, or material and remain
unexploded either by malfunction, design, or any other cause.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.302 Definition of Solid Waste
a) A military munition is not a solid waste when any of the following situations
describes the munition:
1) It is used for its intended purpose, including any of the following uses:
A) Use in training military personnel or explosives and munitions
emergency response specialists (including training in proper
destruction of unused propellant or other munitions);
334
B) Use in research, development, testing, and evaluation of military
munitions, weapons, or weapon systems; or
C) Recovery, collection, and on-range destruction of unexploded
ordnance and munitions fragments during range clearance
activities at active or inactive ranges. However, “use for
intended purpose” does not include the on-range disposal or
burial of unexploded ordnance and contaminants when the burial
is not a result of product use.
2) It is an unused munition, or component thereof, it is being repaired,
reused, recycled, reclaimed, disassembled, reconfigured, or otherwise
subjected to materials recovery activities, unless such activities involve
use constituting disposal, as defined in 35 Ill. Adm. Code 721.102(c)(1),
or it is burned for energy recovery, as defined in 35 Ill. Adm. Code
721.102(c)(2).
b) An unused military munition is a solid waste when any of the following occurs:
1) The munition is abandoned by being disposed of, burned, detonated
(except during intended use as specified in subsection (a) of this
Section), incinerated, or treated prior to disposal;
2) The munition is removed from storage in a military magazine or other
storage area for the purpose of being disposed of, burned, incinerated, or
treated prior to disposal;
3) The munition is deteriorated or damaged (e.g., the integrity of the
munition is compromised by cracks, leaks, or other damage) to the point
that it cannot be put into serviceable condition, and cannot reasonably be
recycled or used for other purposes; or
4) The munition has been declared a solid waste by an authorized military
official.
c) A used or fired military munition is a solid waste when either of the following
activites occurs with regard to the munition:
1) The munition is transported off-range or from the site of use (where the
site of use is not a range) for the purpose of storage, reclamation,
treatment, disposal, or treatment prior to disposal; or
2) The munition is recovered, collected, and then disposed of by burial or
landfilling either on or off a range.
335
d) For purposes of RCRA section 1004(27) (42 U.S.C. 6903(27) (1996)), a used
or fired military munition is a solid waste, and, therefore, is potentially subject
to RCRA corrective action authorities under sections 3004(u) and (v) (42
U.S.C. 6924(u) and (v) (1996)), and 3008(h) (42 U.S.C. 6928(h) (1996)) or to
imminent and substantial endangerment authorities under section 7003 (42
U.S.C. 6963 (1996)) if the munition lands off-range and is not promptly
rendered safe or retrieved. Any imminent and substantial threats associated
with any remaining material must be addressed. If remedial action is infeasible,
the operator of the range shall maintain a record of the event for as long as any
threat remains. The record shall include the type of munition and its location
(to the extent the location is known).
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.303 Standards Applicable to the Transportation of Solid Waste Military
Munitions
a) Criteria for hazardous waste regulation of waste non-chemical military
munitions in transportation.
1) Waste military munitions that are being transported and which exhibit a
hazardous waste characteristic or which are listed as hazardous waste
under 35 Ill. Adm. Code 721 are subject to regulation under 35 Ill.
Adm. Code 702, 703, 705, 720 through 726, and 728, unless the
munitions meet all the following conditions:
A) The waste military munitions are not chemical agents or chemical
munitions;
B) The waste military munitions are transported in accordance with
the Department of Defense shipping controls applicable to the
transport of military munitions;
C) The waste military munitions are transported from a military-
owned or -operated installation to a military-owned or -operated
treatment, storage, or disposal facility; and
D) The transporter of the waste shall provide oral notice to the
Agency within 24 hours from the time when either the transporter
becomes aware of any loss or theft of the waste military
munitions or when any failure to meet a condition of subsection
(a)(1) of this Section occurs that may endanger human health or
the environment. In addition, a written submission describing the
circumstances shall be provided within five days from the time
when the transporter becomes aware of any loss or theft of the
336
waste military munitions or when any failure to meet a condition
of subsection (a)(1) of this Section occurs.
2) If any waste military munitions shipped under subsection (a)(1) of this
Section are not received by the receiving facility within 45 days of the
day the waste was shipped, the owner or operator of the receiving
facility shall report this non-receipt to the Agency within five days.
3) The conditional exemption from regulation as hazardous waste in
subsection (a)(1) of this Section shall apply only to the transportation of
non-chemical waste military munitions. It does not affect the regulatory
status of waste military munitions as hazardous wastes with regard to
storage, treatment, or disposal.
4) The conditional exemption in subsection (a)(1) of this Section applies
only so long as all of the conditions in subsection (a)(1) of this Section
are met.
b) Reinstatement of exemption. If any waste military munition loses its exemption
under subsection (a)(1) of this Section, the transporter may file an application
for reinstatement of the exemption from hazardous waste transportation
regulation with respect to such munition as soon as the munition is returned to
compliance with the conditions of subsection (a)(1) of this Section. If the
Agency finds that reinstatement of the exemption is appropriate based on factors
such as the transporter’s provision of a satisfactory explanation of the
circumstances of the violation, or a demonstration that the violations are not
likely to recur, the Agency may reinstate the exemption under subsection (a)(1)
of this Section. If the Agency does not take action on the reinstatement
application within 60 days after receipt of the application, then reinstatement
shall be deemed granted, retroactive to the date of the application. However,
the Agency may terminate a conditional exemption reinstated by default under
the preceding sentence if the Agency finds that reinstatement is inappropriate
based on factors such as the transporter’s failure to provide a satisfactory
explanation of the circumstances of the violation, or failure to demonstrate that
the violations are not likely to recur. In reinstating the exemption under
subsection (a)(1) of this Section, the Agency may specify additional conditions
as are necessary to ensure and document proper transportation to protect human
health and the environment.
b) Reinstatement of conditional exemption.
1) If any waste military munition loses its conditional exemption under
subsection (a)(1) of this Section, the transporter may file with the
Agency an application for reinstatement of the conditional exemption
from hazardous waste transportation regulation with respect to such
337
munition as soon as the munition is returned to compliance with the
conditions of subsection (a)(1) of this Section.
2) If the Agency finds that reinstatement of the conditional exemption is
appropriate, it shall reinstate the conditional exemption of subsection
(a)(1) of this Section in writing. The Agency’s decision to reinstate or
not to reinstate the conditional exemption shall be based on the nature of
the risks to human health and the environment posed by the waste and
either the transporter's provision of a satisfactory explanation of the
circumstances of the violation or any demonstration that the violations
are not likely to recur. If the Agency denies an application, it shall
transmit to the applicant specific, detailed statements in writing as to the
reasons it denied the application. In reinstating the conditional
exemption under subsection (a)(1) of this Section, the Agency may
specify additional conditions as are necessary to ensure and document
proper transportation to protect human health and the environment. If
the Agency does not take action on the reinstatement application within
60 days after receipt of the application, then reinstatement shall be
deemed granted, retroactive to the date of the application.
3) The Agency may terminate a conditional exemption reinstated by default
under the preceding sentence in writing if it finds that reinstatement is
inappropriate based on its consideration of the factors set forth in
subsection (b)(2) of this Section. If the Agency terminates a reinstated
exemption, it shall transmit to the applicant specific, detailed statements
in writing as to the reasons it terminated the reinstated exemption.
4) The applicant under this subsection (b) may appeal the Ageny’s
determination to deny the reinstatement, to grant the reinstatement with
conditions, or to terminate a reinstatement before the Board pursuant to
Section 40 of the Act [415 ILCS 5/40].
c) Amendments to DOD shipping controls. The Department of Defense shipping
controls applicable to the transport of military munitions referenced in
subsection (a)(1)(B) of this Section are Government Bill of Lading (GBL) (GSA
Standard Form 1109), Requisition Tracking Form (DD Form 1348), the
Signature and Talley Record (DD Form 1907), Special Instructions for Motor
Vehicle Drivers (DD Form 836), and the Motor Vehicle Inspection Report (DD
Form 626) in effect on November 8, 1995, incorporated by reference in 35 Ill.
Adm. Code 720.111.
BOARD NOTE: 40 CFR 266.203(c), as added at 62 Fed. Reg. 6655 (Feb. 12,
1997), further provides as follows: “Any amendments to the Department of
Defense shipping controls shall become effective for purposes of paragraph
(a)(1) of this section on the date the Department of Defense publishes notice in
338
the Federal Register that the shipping controls referenced in paragraph (a)(1)(ii)
of this section have been amended.” (40 CFR 266.203(a)(1)(ii) corresponds
with 35 Ill. Adm. Code 726.303(a)(1)(B).) Section 5-75 of the Illinois
Administrative Procedure Act [5 ILCS 100/5-75] prohibits the incorporation of
later amendments and editions by reference. For this reason, interested
members of the regulated community will need to notify the Board of any
amendments of these references before those amendments can become effective
under Illinois law.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.304 Standards Applicable to Emergency Responses
Explosives and munitions emergencies involving military munitions or explosives are subject
to 35 Ill. Adm. Code 722.110(i), 723.110(e), 724.101(g)(8), 725.101(c)(11), and
703.121(c)(3), or alternatively to 35 Ill. Adm. Code 703.221.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.305 Standards Applicable to the Storage of Solid Waste Military Munitions
a) Criteria for hazardous waste regulation of waste non-chemical military
munitions in storage.
1) Waste military munitions in storage that exhibit a hazardous waste
characteristic or are listed as hazardous waste under 35 Ill. Adm. Code
721 are listed or identified as a hazardous waste (and thus are subject to
regulation under 35 Ill. Adm. Code 702, 703, 705, 720 through 726,
728, 733, and 739), unless all the following conditions are met:
A) The waste military munitions are not chemical agents or chemical
munitions;
B) The waste military munitions must be subject to the jurisdiction
of the Department of Defense Explosives Safety Board (DDESB);
C) The waste military munitions must be stored in accordance with
the DDESB storage standards applicable to waste military
munitions;
D) Within 90 days of when a storage unit is first used to store waste
military munitions, the owner or operator shall notify the Agency
of the location of any waste storage unit used to store waste
military munitions for which the conditional exemption in
subsection (a)(1) of this Section is claimed;
339
E) The owner or operator shall provide oral notice to the Agency
within 24 hours from the time the owner or operator becomes
aware of any loss or theft of the waste military munitions, or any
failure to meet a condition of subsection (a)(1) of this Section that
may endanger health or the environment. In addition, a written
submission describing the circumstances shall be provided within
five days from the time the owner or operator becomes aware of
any loss or theft of the waste military munitions or any failure to
meet a condition of subsection (a)(1) of this Section;
F) The owner or operator shall inventory the waste military
munitions at least annually, shall inspect the waste military
munitions at least quarterly for compliance with the conditions of
subsection (a)(1) of this Section, and shall maintain records of the
findings of these inventories and inspections for at least three
years; and
G) Access to the stored waste military munitions must be limited to
appropriately trained and authorized personnel.
2) The conditional exemption in subsection (a)(1) of this Section from
regulation as hazardous waste shall apply only to the storage of non-
chemical waste military munitions. It does not affect the regulatory
status of waste military munitions as hazardous wastes with regard to
transportation, treatment or disposal.
3) The conditional exemption in subsection (a)(1) of this Section applies
only so long as all of the conditions in subsection (a)(1) of this Section
are met.
b) Notice of termination of waste storage. The owner or operator shall notify the
Agency when a storage unit identified in subsection (a)(1)(D) of this Section
will no longer be used to store waste military munitions.
c) Reinstatement of conditional exemption.
1) If any waste military munition loses its conditional exemption under
subsection (a)(1) of this Section, an application may be filed with the
Agency for reinstatement of the conditional exemption from hazardous
waste storage regulation with respect to such munition as soon as the
munition is returned to compliance with the conditions of subsection
(a)(1) of this Section.
340
2) If the Agency finds that reinstatement of the conditional exemption is
appropriate, it shall reinstate the conditional exemption of subsection
(a)(1) of this Section in writing. The Agency’s decision to reinstate or
not to reinstate the conditional exemption shall be based on the nature of
the risks to human health and the environment posed by the waste and
either the owner's or operator's provision of a satisfactory explanation of
the circumstances of the violation or any demonstration that the
violations are not likely to recur. If the Agency denies an application, it
shall transmit to the applicant specific, detailed statements in writing as
to the reasons it denied the application. In reinstating the conditional
exemption under subsection (a)(1) of this Section, the Agency may
specify additional conditions as are necessary to ensure and document
proper storage to protect human health and the environment.
3) The Agency may terminate a conditional exemption reinstated by default
under the preceding sentence in writing if it finds that reinstatement is
inappropriate based on its consideration of the factors set forth in
subsection (c)(2) of this Section. If the Agency terminates a reinstated
exemption, it shall transmit to the applicant specific, detailed statements
in writing as to the reasons it terminated the reinstated exemption.
4) The applicant under this subsection (c) may appeal the Ageny’s
determination to deny the reinstatement, to grant the reinstatement with
conditions, or to terminate a reinstatement before the Board pursuant to
Section 40 of the Act [415 ILCS 5/40].
d) Waste chemical munitions.
1) Waste military munitions that are chemical agents or chemical munitions
and that exhibit a hazardous waste characteristic or are listed as
hazardous waste under 35 Ill. Adm. Code 721, are listed or identified as
a hazardous waste and shall be subject to the applicable regulatory
requirements of RCRA subtitle C.
2) Waste military munitions that are chemical agents or chemical munitions
and that exhibit a hazardous waste characteristic or are listed as
hazardous waste under 35 Ill. Adm. Code 721, are not subject to the
storage prohibition in RCRA section 3004(j), codified at 35 Ill. Adm.
Code 728.150.
e) Amendments to DDESB storage standards. The DDESB storage standards
applicable to waste military munitions, referenced in subsection (a)(1)(C) of this
Section, are DOD 6055.9-STD (“DOD Ammunition and Explosive Safety
Standards”), in effect on November 8, 1995, incorporated by reference in 35
Ill. Adm. Code 720.111.
341
BOARD NOTE: 40 CFR 266.205(e), as added at 62 Fed. Reg. 6656 (Feb. 12,
1997), further provides as follows: “Any amendments to the DDESB storage
standards shall become effective for purposes of paragraph (a)(1) of this section
on the date the Department of Defense publishes notice in the Federal Register
that the DDESB standards referenced in paragraph (a)(1) of this section have
been amended.” Section 5-75 of the Illinois Administrative Procedure Act [5
ILCS 100/5-75] prohibits the incorporation of later amendments and editions by
reference. For this reason, interested members of the regulated community will
need to notify the Board of any amendments of these references before those
amendments can become effective under Illinois law.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.306 Standards Applicable to the Treatment and Disposal of Waste Military
Munitions
The treatment and disposal of hazardous waste military munitions are subject to the applicable
permitting, procedural, and technical standards in 35 Ill. Adm. Code 702, 703, 705, 720
through 726, and 728.
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 726.Appendix I
Methods Manual for Compliance with BIF Regulations
See “Methods Manual for Compliance with BIF Regulations”. This document is available
from two sources. It is available through NTIS, incorporated by reference in 35 Ill. Adm.
Code 720.111. It is also available as 40 CFR 266, Appendix IX (1997), adopted at 56 Fed.
Reg. 32688, July 17, 1991 and amended at 56 Fed. Reg. 42511, August 27, 1991, 57 Fed.
Reg. 38566, August 25, 1992, and 57 Fed. Reg. 45001, September 30, 1992, which is
incorporated by reference in 35 Ill. Adm. Code 720.111. This incorporation includes no
future editions or amendments.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 728
LAND DISPOSAL RESTRICTIONS
342
SUBPART A: GENERAL
Section
728.101
Purpose, Scope and Applicability
728.102
Definitions
728.103
Dilution Prohibited as a Substitute for Treatment
728.104
Treatment Surface Impoundment Exemption
728.105
Procedures for case-by-case Extensions to an Effective Date
728.106
Petitions to Allow Land Disposal of a Waste Prohibited under Subpart C
728.107
Waste Analysis Testing, Tracking, and Recordkeeping Requirements for
Generators, Treaters, and Disposal Facilities
728.108
Landfill and Surface Impoundment Disposal Restrictions (Repealed)
728.109
Special Rules for Characteristic Wastes
SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION AND
ESTABLISHMENT OF TREATMENT STANDARDS
Section
728.110
First Third (Repealed)
728.111
Second Third (Repealed)
728.112
Third Third (Repealed)
728.113
Newly Listed Wastes
728.114
Surface Impoundment exemptions
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section
728.130
Waste Specific Prohibitions -- Solvent Wood Preserving Wastes
728.131
Waste Specific Prohibitions -- Dioxin-Containing Wastes
728.132
Waste Specific Prohibitions -- California List Wastes (Repealed)
728.133
Waste Specific Prohibitions: -- First Third Wastes (Repealed)
728.134
Waste Specific Prohibitions -- Second Third Wastes (Repealed)
728.135
Waste Specific Prohibitions -- Third Third Wastes (Repealed)
728.136
Waste Specific Prohibitions -- Newly Listed Wastes (Repealed)
728.137
Waste Specific Prohibitions -- Ignitable and Corrosive Characteristic Wastes
Whose Treatment Standards Were Vacated
728.138
Waste-Specific Prohibitions: Newly-Identified Organic Toxicity Characteristic
Wastes and Newly-Listed Coke By-Product and Chlorotoluene Production
Wastes
728.139
Waste-Specific Prohibitions: End-of-pipe CWA, CWA-Equivalent, and Class I
Nonhazardous Waste Injection Well Treatment Standards; Spent Aluminum
Potliners; and Carbamate Wastes
SUBPART D: TREATMENT STANDARDS
Section
728.140
Applicability of Treatment Standards
728.141
Treatment Standards Expressed as Concentrations in Waste Extract
728.142
Treatment Standards Expressed as Specified Technologies
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728.143
Treatment Standards Expressed as Waste Concentrations
728.144
Adjustment of Treatment Standard
728.145
Treatment Standards for Hazardous Debris
728.146
Alternative Treatment Standards Based on HTMR
728.148
Universal Treatment Standards
SUBPART E: PROHIBITIONS ON STORAGE
Section
728.150
Prohibitions on Storage of Restricted Wastes
728.Appendix A
Toxicity Characteristic Leaching Procedure (TCLP) (Repealed)
728.Appendix B
Treatment Standards (As concentrations in the Treatment Residual
Extract) (Repealed)
728.Appendix C
List of Halogenated Organic Compounds (Repealed)
728.Appendix D
Wastes Excluded from Lab Packs
728.Appendix E
Organic Lab Packs (Repealed)
728.Appendix F
Technologies to Achieve Deactivation of Characteristics
728.Appendix G
Federal Effective Dates
728.Appendix H
National Capacity LDR Variances for UIC Wastes
728.Appendix I
EP Toxicity Test Method and Structural Integrity Test
728.Appendix J
Recordkeeping, Notification, and Certification Requirements (Repealed)
728.Appendix K
Metal Bearing Wastes Prohibited From Dilution in a Combustion Unit
According to Section 728.103(c)
728.Table A
Constituent Concentrations in Waste Extract (CCWE)
728.Table B
Constituent Concentrations in Wastes (CCW)
728.Table C
Technology Codes and Description of Technology-Based Standards
728.Table D
Technology-Based Standards by RCRA Waste Code
728.Table E
Standards for Radioactive Mixed Waste
728.Table F
Alternative Treatment Standards for Hazardous Debris
728.Table G
Alternative Treatment Standards Based on HMTR
728.Table H
Wastes Excluded from CCW Treatment Standards
728.Table I Generator Paperwork Requirements
728.Table T
Treatment Standards for Hazardous Wastes
728.Table U
Universal Treatment Standards (UTS)
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the Environmental
Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R87-5 at 11 Ill. Reg. 19354, effective November 12, 1987; amended
in R87-39 at 12 Ill. Reg. 13046, effective July 29, 1988; amended in R89-1 at 13 Ill. Reg.
18403, effective November 13, 1989; amended in R89-9 at 14 Ill. Reg. 6232, effective April
16, 1990; amended in R90-2 at 14 Ill. Reg. 14470, effective August 22, 1990; amended in
R90-10 at 14 Ill. Reg. 16508, effective September 25, 1990; amended in R90-11 at 15 Ill.
Reg. 9462, effective June 17, 1991; amendment withdrawn at 15 Ill. Reg. 14716, October 11,
344
1991; amended in R91-13 at 16 Ill. Reg. 9619, effective June 9, 1992; amended in R92-10 at
17 Ill. Reg. 5727, effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20692,
effective November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6799, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12203, effective July 29, 1994; amended in R94-17 at
18 Ill. Reg. 17563, effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9660,
effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11100, August 1, 1996; amended
in R96-10/R97-3/R97-5 at 22 Ill. Reg. 783, effective December 16, 1997; amended in R98-12
at 22 Ill. Reg. 7685, effective April 15, 1998; amended in R97-21/R98-3/R98-5 at 22 Ill.
Reg. ________, effective ______________________.
SUBPART A: GENERAL
Section 728.101
Purpose, Scope and Applicability
a)
This Part identifies hazardous wastes that are restricted from land disposal and
defines those limited circumstances under which an otherwise prohibited waste
may continue to be land disposed.
b)
Except as specifically provided otherwise in this Part or 35 Ill. Adm. Code 721,
the requirements of this Part apply to persons that generate or transport
hazardous waste and to owners and operators of hazardous waste treatment,
storage, and disposal facilities.
c)
Restricted wastes may continue to be land disposed as follows:
1)
Where persons have been granted an extension to the effective date of a
prohibition under Subpart C or pursuant to Section 728.105, with respect
to those wastes covered by the extension;
2)
Where persons have been granted an exemption from a prohibition
pursuant to a petition under Section 728.106, with respect to those
wastes and units covered by the petition;
3)
A waste that is hazardous only because it exhibits a characteristic of
hazardous waste and that is otherwise prohibited under this Part is not
prohibited if the waste:
A)
Is disposed into a nonhazardous or hazardous waste injection
well, as defined in 35 Ill. Adm. Code 704.106(a); and
B)
Does not exhibit any prohibited characteristic of hazardous waste
identified in 35 Ill. Adm. Code 721.Subpart C at the point of
injection.
345
4)
A waste that is hazardous only because it exhibits a characteristic of
hazardous waste and which is otherwise prohibited under this Part is not
prohibited if the waste meets any of the following criteria, unless the
waste is subject to a specified method of treatment other than DEACT in
Section 728.140 or is D003 reactive cyanide:
A) Any of the following is true of either treatment or management of
the waste:
Ai)
The waste is managed in a treatment system which
subsequently discharges to waters of the U.S. pursuant to
a permit issued under 35 Ill. Adm. Code 309; or
Bii)
The waste is treated for purposes of the pretreatment
requirements of 35 Ill. Adm. Code 307 and 310; or
Ciii)
The waste is managed in a zero discharge system engaged
in Clean Water Act (CWA)-equivalent treatment, as
defined in Section 728.137(a); and
DB)
The waste no longer exhibits a prohibited characteristic of
hazardous waste at the point of land disposal (i.e., placement in a
surface impoundment).
d)
This Part does not affect the availability of a waiver under Section 121(d)(4) of
the Comprehensive Environmental Response, Compensation, and Liability Act
of 1980 (CERCLA) (42 U.S.C. §§ 9601 et seq.).
e)
The following hazardous wastes are not subject to any provision of this Part:
1)
Wastes generated by small quantity generators of less than 100 kg of
non-acute hazardous waste or less than 1 kg of acute hazardous waste per
month, as defined in 35 Ill. Adm. Code 721.105;
2)
Waste pesticides that a farmer disposes of pursuant to 35 Ill. Adm. Code
722.170;
3)
Wastes identified or listed as hazardous after November 8, 1984, for
which USEPA has not promulgated a land disposal prohibitions or
treatment standards; or
4)
De minimis losses of waste that exhibits a characteristic of hazardous
waste to wastewaters are not considered to be prohibited waste and are
defined as follows:losses from normal material handling operations
(e.g., spills from the unloading or transfer of materials from bins or
346
other containers or leaks from pipes, valves, or other devices used to
transfer materials); minor leaks of process equipment, storage tanks, or
containers; leaks from well-maintained pump packings and seals; sample
purgings; relief device discharges; discharges from safety showers and
rinsing and cleaning of personal safety equipment; rinsate from empty
containers or from containers that are rendered empty by that rinsing;
and laboratory waste that does not exceed one percent of the total flow
of wastewater into the facility’s headworks on an annual basis, or with a
combined annualized average concentration not exceeding one part per
million (ppm) in the headworks of the facility’s wastewater treatment or
pretreatment facility.
A) Losses from normal material handling operations (e.g., spills
from the unloading or transfer of materials from bins or other
containers or leaks from pipes, valves, or other devices used to
transfer materials); minor leaks of process equipment, storage
tanks, or containers; leaks from well-maintained pump packings
and seals; sample purgings; relief device discharges; discharges
from safety showers and rinsing and cleaning of personal safety
equipment; rinsate from empty containers or from containers that
are rendered empty by that rinsing; and laboratory waste that
does not exceed one per cent of the total flow of wastewater into
the facility’s headworks on an annual basis, or with a combined
annualized average concentration not exceeding one part per
million (ppm) in the headworks of the facility’s wastewater
treatment or pretreatment facility; or
B) Decharacterized waste that is injected into Class I nonhazardous
wells in which the decharacterized waste’s combined volume is
less than one per cent of the total flow at the wellhead on an
annualized basis and no greater than 10,000 gallons per day, and
in which any underlying hazardous constituents in the
characteristic waste are present at the point of generation at levels
less than 10 times the treatment standards found at Section
728.148.
5)
Land disposal prohibitions for hazardous characteristic wastes do not
apply to laboratory wastes displaying the characteristic of ignitability
(D001), corrosivity (D002), or organic toxicity (D012 through D043)
that are mixed with other plant wastewaters at facilities whose ultimate
discharge is subject to regulation under the CWA (including wastewaters
at facilities that have eliminated the discharge of wastewater), provided
that the annualized flow of laboratory wastewater into the facility’s
headworks does not exceed one percent or that the laboratory wastes’
347
combined annualized average concentration does not exceed one part per
million in the facility’s headworks.
f)
A universal waste handler or universal waste transporter (as defined in 35 Ill.
Adm. Code 720.110) is exempt from Sections 728.107 and 728.150 for the
hazardous wastes listed below. Such a handler or transporter is subject to
regulation under 35 Ill. Adm. Code 733.
1)
Batteries, as described in 35 Ill. Adm. Code 733.102;
2)
Pesticides, as described in 35 Ill. Adm. Code 733.103;
3)
Thermostats, as described in 35 Ill. Adm. Code 733.104 and
4)
Mercury-containing lamps, as described in 35 Ill. Adm. Code 733.107.
BOARD NOTE: Subsection (f)(4) of this Section was added pursuant to
Section 22.23a of the Act [415 ILCS 5/22.23a] (see P.A. 90-502,
effective August 19, 1997).
g)
This Part is cumulative with the land disposal restrictions of 35 Ill. Adm. Code
729. The Environmental Protection Agency (Agency) shall not issue a
wastestream authorization pursuant to 35 Ill. Adm. Code 709 or Sections
Section 22.6 or 39(h) of the Environmental Protection Act [415 ILCS 5/22.6 or
39(h)] unless the waste meets the requirements of this Part as well as 35 Ill.
Adm. Code 729.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.104
Treatment Surface Impoundment Exemption
a)
Wastes which are otherwise prohibited from land disposal under this Part may
be treated in a surface impoundment or series of impoundments provided that all
of the following conditions are fulfilled:
1)
Treatment of such wastes occurs in the impoundments;
2)
The following conditions are met:
A)
Sampling and testing. For wastes with treatment standards in
Subpart D or prohibition levels in Subpart C, the residues from
treatment are analyzed, as specified in Section 728.107 or
728.132, to determine if they meet the applicable treatment
standards or, where no treatment standards have been established
for the waste, the applicable prohibition levels. The sampling
348
method, specified in the waste analysis plan under 35 Ill. Adm.
Code 724.113 or 725.113, must be designed such that
representative samples of the sludge and the supernatant are
tested separately rather than mixed to form homogeneous
samples.
B)
Removal. The following treatment residues (including any liquid
waste) must be removed at least annually: residues which do not
meet the treatment standards promulgated under Subpart D;
residues which do not meet the prohibition levels established
under Subpart C or Section 728.139 (where no treatment
standards have been established); residues which are from the
treatment of wastes prohibited from land disposal under Subpart
C (where no treatment standards have been established and no
prohibition levels apply); or residues from managing listed wastes
which are not delisted under 35 Ill. Adm. Code 720.122.
However, residues which are the subject of a valid certification
under Section 728.108 made no later than a year after placement
of the wastes in an impoundment are not required to be removed
annually. If the volume of liquid flowing through the
impoundment or series of impoundments annually is greater than
the volume of the impoundment or impoundments, this flow-
through constitutes removal of the supernatant for the purpose of
this requirement.
C)
Subsequent management. Treatment residues must not be placed
in any other surface impoundment for subsequent management
unless the residues are the subject of a valid certification under
Section 728.108 which allows disposal in surface impoundments
meeting the requirements of Section 728.108(a).
D)
Recordkeeping. The procedures and schedule for the sampling of
impoundment contents, the analysis of test data and the annual
removal of residues which do not meet the treatment standards,
or prohibition levels (where no treatment standards have been
established), or which are from the treatment of wastes prohibited
from land disposal under Subpart C (where no treatment
standards have been established and no prohibition levels apply),
must be specified in the facility’s waste analysis plan as required
under Sampling, testing, and recordkeeping provisions of 35 Ill.
Adm. Code 724.113 or 725.113 apply;.
3)
The impoundment meets the design requirements of 35 Ill. Adm. Code
724.321(c) or 725.321(a) even though the unit may not be new,
expanded or a replacement, and must be in compliance with applicable
349
groundwater monitoring requirements of 35 Ill. Adm. Code 724.Subpart
F or 725.Subpart F, unless any of the following conditions is fulfilled:
A)
It The impoundment is exempted pursuant to 35 Ill. Adm. Code
724.321(d) or (e), or to 35 Ill. Adm. Code 725.321(c) or (d); or
B)
Upon application by the owner or operator, the Agency has by
permit provided that the requirements of this Part do not apply on
the basis that the surface impoundment fulfills all of the
following conditions:
i)
Has The impoundment has at least one liner, for which
there is no evidence that such liner is leaking;
ii)
Is The impoundment is located more than one-quarter
mile from an underground source of drinking water; and
iii)
Is The impoundment is in compliance with generally
applicable groundwater monitoring requirements for
facilities with permits; or,
C)
Upon application by the owner or operator, the Board has,
pursuant to 35 Ill. Adm. Code 106, granted an adjusted standard
from the requirements of this Part. The justification for such an
adjusted standard shall be a demonstration that the surface
impoundment is located, designed and operated so as to assure
that there will be no migration of any hazardous constituent into
groundwater or surface water at any future time. And,; and
4)
The owner or operator submits to the Agency a written certification that
the requirements of Section 728.104subsection (a)(3)of this Section have
been met and submits a copy of the waste analysis plan required under
Section 728.104(a)(2). The following certification is required:
I certify under penalty of law that the requirements of 35 Ill.
Adm. Code 728.104(a)(3) have been met for all surface
impoundments being used to treat restricted wastes. I believe
that the submitted information is true, accurate and complete. I
am aware that there are significant penalties for submitting false
information, including the possibility of fine and imprisonment.
b)
Evaporation of hazardous constituents as the principal means of treatment is not
considered to be a treatment for purposes of an exemption under this Section.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
350
Section 728.107
Waste Analysis Testing, Tracking, and Recordkeeping Requirements for
Generators, Treaters, and Disposal Facilities
a) Except as specified in Section 728.132, where a generator’s waste is listed in 35
Ill. Adm. Code 721.Subpart D or if the waste exhibits one or more of the
characteristics set out at 35 Ill. Adm. Code 721.Subpart C, the generator shall
test its waste, or test an extract using the Toxicity Characteristic Leaching
Procedure, Method 1311, in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods”, USEPA Publication SW-846, as incorporated by
reference in 35 Ill. Adm. Code 720.111, or use knowledge of the waste to
determine if the waste is restricted from land disposal under this Part. If the
generator determines that its waste displays the characteristic of ignitability
(D001) (and is not in the High TOC Ignitable Liquids Subcategory or is not
treated by CMBST or RORGS of Section 728.Table C), or the waste displays
the characteristic of corrosivity (D002), reactivity (D003), or organic toxicity
(D012 through D043), and the waste is prohibited under Sections 728.137,
Section 728.138, and 728.139, the generator shall determine what underlying
hazardous constituents (as defined in Section 728.102), are reasonably expected
to be present in the D001, D002, D003, or D012 through D043 waste.
1) If a generator determines that it is managing a restricted waste under this
Part and the waste does not meet the applicable treatment standards set
forth in Subpart D of this Part or exceeds the applicable prohibition
levels set forth in Section 728.132 or 728.139, the generator shall send a
one-time written notice to each treatment or storage facility with the
initial shipment of waste. No further notification is necessary until such
time that the waste or facility change, in which case a new notification
must be sent and a copy placed in the generator’s file. The notice must
include the following information:
A) USEPA hazardous waste number;
B) The waste constituents that the treater will monitor, if monitoring
will not include all regulated constituents, for wastes F001
through F005, F039, D001, D002, D003, and D012 through
D043. The generator must also include whether the waste is a
nonwastewater or wastewater (as defined in Section 728.102 (d)
and (f)) and indicate the subcategory of the waste (such as “D003
reactive cyanide”) if applicable;
C) The manifest number associated with the shipment of waste;
D) For hazardous debris, the contaminants subject to treatment, as
provided by Section 728.145(b), and the following statement:
351
“This hazardous debris is subject to the alternative treatment
standards of 35 Ill. Adm. Code 728.145”; and
E) Waste analysis data, where available.
2) If a generator determines that it is managing a restricted waste under this
Part and determines that the waste can be land disposed without further
treatment, with the initial shipment of waste the generator shall submit a
one-time written notice and a certification to each treatment, storage, or
land disposal facility stating that the waste meets the applicable treatment
standards set forth in Subpart D of this Part and setting forth the
applicable prohibition levels set forth in Section 728.132 or RCRA
Section 3004(d), referenced in Section 728.139. A generator of
hazardous debris that is excluded from the definition of hazardous waste
under 35 Ill. Adm. Code 721.103(e)(2), 35 Ill. Adm. Code
728.103(f)(2), or 35 Ill. Adm. Code 720.122 (i.e. debris that is
delisted), however, is not subject to these notification and certification
requirements. If the waste changes, the generator shall send a new
notice and certification to the receiving facility, and place a copy in its
files.
A) The notice must include the following information:
i) USEPA hazardous waste number;
ii) The waste constituents that the treater will monitor, if
monitoring will not include all regulated constituents, for
wastes F001 through F005, F039, D001, D002, D003,
and D012 through D043. The generator must also include
whether the waste is a wastewater or nonwastewater (as
defined in Section 728.102 (d) and (f)) and indicate the
subcategory of the waste (such as “D003 reactive
cyanide”), if applicable;
iii) The manifest number associated with the shipment of
waste; and
iv) Waste analysis data, where available.
B) The certification must be signed by an authorized representative
and must state the following:
I certify under penalty of law that I personally have examined
and am familiar with the waste through analysis and testing or
through knowledge of the waste to support this certification that
352
the waste complies with the treatment standards specified in 35
Ill. Adm. Code Subpart D of this Part and all applicable
prohibitions set forth in 35 Ill. Adm. Code 728.132, 728.139, or
Section 3004(d) of the Resource Conservation and Recovery
Act. I believe that the information I submitted is true, accurate,
and complete. I am aware that there are significant penalties for
submitting a false certification, including the possibility of a fine
and imprisonment.
3) If a generator’s waste is subject to an exemption from a prohibition on
the type of land disposal method utilized for the waste (such as, but not
limited to, a case-by-case extension under Section 728.105, an
exemption under Section 728.106, an extension under Section
728.101(c)(3), or a nationwide capacity variance under 40 CFR
268.Subpart C (1996)), the generator shall submit a one-time written
notice with the initial shipment of the waste to each facility receiving the
generator’s waste stating that the waste is not prohibited from land
disposal. If the waste changes, the generator shall send a new notice and
certification to the receiving facility, and place a copy in its files. The
notice must include the following information:
A) USEPA hazardous waste number;
B) The waste constituents that the treater will monitor, if monitoring
will not include all regulated constituents, for wastes F001
through F005, F039, D001, D002, D003, and D012 through
D043. The generator must also include whether the waste is a
nonwastewater or wastewater (as defined in Section 728.102 (d)
and (f)) and indicate the subcategory of the waste (such as “D003
reactive cyanide”) if applicable;
C) The manifest number associated with the shipment of
waste;
D) Waste analysis data, where available;
E) For hazardous debris, when using the alternative treatment
technologies provided by Section 728.145:
i) The contaminants subject to treatment, as provided by
Section 728.145(b);
ii) An indication that these contaminants are being treated to
comply with Section 728.145;
353
F) For hazardous debris when using the treatment standards for the
contaminating waste(s) in Section 728.140: the requirements
described in subsections (a)(3)(A) through (a)(3)(D) and (a)(3)(G)
of this Section; and,
G) The date on which the waste is subject to the prohibitions.
4) If a generator is managing a prohibited waste in tanks, containers, or
containment buildings regulated under 35 Ill. Adm. Code 722.134 and is
treating such waste in tanks, containers, or containment buildings to
meet applicable treatment standards under Subpart D of this Part, the
generator shall develop and follow a written waste analysis plan that
describes the procedures the generator will carry out to comply with the
treatment standards. (A generator treating hazardous debris under the
alternative treatment standards of Section 728.Table F, however, is not
subject to these waste analysis requirements.) The plan must be kept on-
site in the generator’s records, and the following requirements must be
met:
A) The waste analysis plan must be based on a detailed chemical and
physical analysis of a representative sample of the prohibited
wastes being treated, and it must contain all information
necessary to treat the wastes in accordance with the requirements
of this Part, including the selected testing frequency.
B) Such plan must be filed with the Agency a minimum of 30 days
prior to the treatment activity, with delivery verified.
C) Wastes shipped off-site pursuant to this subsection must comply
with the notification requirements of Section 728.107(a)(2).
5) If a generator determines whether the waste is restricted based solely on
the generator’s knowledge of the waste, the generator shall retain all
supporting data used to make this determination on-site in the generator’s
files. If a generator determines whether the waste is restricted based on
testing the waste or an extract developed using the test method described
in Section 728.Appendix A, the generator shall retain all waste analysis
data on site in its files.
6) If a generator determines, subsequent to the time of generation, that it is
managing a restricted waste that is excluded from the definition of
hazardous or solid waste or exempt from regulation as a RCRA
hazardous waste under 35 Ill. Adm. Code 721.102 through 721.106, the
generator shall place, in the facility’s file, a one-time notice stating such
generation, the subsequent exclusion from the definition of hazardous or
354
solid waste or exemption from regulation as a RCRA hazardous waste,
and the disposition of the waste.
7) A generator shall retain on-site a copy of all notices, certifications,
demonstrations, waste analysis data, and other documentation produced
pursuant to this Section for at least five years from the date that the
waste that is the subject of such documentation was last sent to on-site or
off-site treatment, storage, or disposal. The five year record retention
period is automatically extended during the course of any unresolved
enforcement action regarding the regulated activity, or as requested by
the Agency. The requirements of this subsection apply to solid wastes
even when the hazardous characteristic is removed prior to disposal,
when the waste is excluded from the definition of hazardous or solid
waste under 35 Ill. Adm. Code 721.102 through 721.106, or when the
waste is exempted from regulation as a RCRA hazardous waste
subsequent to the point of generation.
8) If a generator is managing a lab pack that contains wastes identified in
Section 728.Appendix D and wishes to use the alternative treatment
standard under Section 728.142(c), with each shipment of waste the
generator shall submit a notice to the treatment facility in accordance
with subsection (a)(1) of this Section, except that underlying hazardous
constituents need not be determined. The generator shall also comply
with the requirements in subsections (a)(5) and (a)(6) of this Section and
shall submit the following certification, which must be signed by an
authorized representative:
I certify under penalty of law that I personally have examined
and am familiar with the waste and that the lab pack does not
contain any of the wastes identified in 35 Ill. Adm. Code
728.Appendix D. I am aware that there are significant penalties
for submitting a false certification, including the possibility of
fine or imprisonment.
9) This subsection corresponds with 40 CFR 268.7(a)(9), marked
“reserved” by USEPA at 59 Fed. Reg. 48045 (Sep. 19, 1994). This
statement maintains structural consistency with federal regulations.
10) Small quantity generators with tolling agreements pursuant to 35 Ill.
Adm. Code 722.120(e) shall comply with the applicable notification and
certification requirements of subsection (a) of this Section for the initial
shipment of the waste subject to the agreement. Such generators shall
retain on-site a copy of the notification and certification, together with
the tolling agreement, for at least three years after termination or
expiration of the agreement. The three-year record retention period is
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automatically extended following notification pursuant to Section 31(d)
of the Environmental Protection Act until either any subsequent
enforcement action is resolved or until the Agency notifies the generator
documents need not be retained.
a) Requirements for generators:
1) A generator of a hazardous waste shall determine if the waste has to be
treated before it can be land disposed. This is done by determining if
the hazardous waste meets the treatment standards in Section 728.140 or
Section 728.145. This determination can be made in either of two
ways: testing the waste or using knowledge of the waste. Testing
determines the total concentration of hazardous constituents, or the
concentration of hazardous constituents in an extract of the waste
obtained using SW-846 Method 1311 (the Toxicity Characteristic
Leaching Procedure), incorporated by reference in 35 Ill. Adm. Code
720.111, depending on whether the treatment standard for the waste is
expressed as a total concentration or concentration of hazardous
constituent in the waste’s extract. In addition, some hazardous wastes
must be treated by particular treatment methods before they can be land
disposed. These treatment standards are also found in Sections 728.140
and 728.Table T, and are described in detail in Section 728.Table C.
These wastes do not need to be tested (however, if they are in a waste
mixture, other wastes with concentration level treatment standards shall
be tested). If a generator determines that it is managing a waste that
displays a hazardous characteristic of ignitability, corrosivity, reactivity,
or toxicity, the generator shall comply with the special requirements of
Section 728.109 in addition to any applicable requirements in this
Section.
2) If the waste does not meet the treatment standard: With the initial
shipment of waste to each treatment or storage facility, the generator
shall send a one-time written notice to each treatment or storage facility
receiving the waste, and place a copy in the file. The notice must
include the information in column “728.107(a)(2)” of the Generator
Paperwork Requirements Table in Section 728.Table I. No further
notification is necessary until such time that the waste or facility
changes, in which case a new notification must be sent and a copy placed
in the generator’s file.
3) If the waste meets the treatment standard at the original point of
generation:
A) With the initial shipment of waste to each treatment, storage, or
disposal facility, the generator shall send a one-time written
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notice to each treatment, storage, or disposal facility receiving
the waste, and place a copy in its own file. The notice must
include the information indicated in column “728.107(a)(3)” of
the Generator Paperwork Requirements Table in Section
728.Table I and the following certification statement, signed by
an authorized representative:
I certify under penalty of law that I personally have
examined and am familiar with the waste through analysis
and testing or through knowledge of the waste to support
this certification that the waste complies with the
treatment standards specified in 35 Ill. Adm. Code
728.Subpart D. I believe that the information I submitted
is true, accurate, and complete. I am aware that there are
significant penalties for submitting a false certification,
including the possibility of a fine and imprisonment.
B) If the waste changes, the generator shall send a new notice and
certification to the receiving facility, and place a copy in its file.
Generators of hazardous debris excluded from the definition of
hazardous waste under 35 Ill. Adm. Code 721.103(f) are not
subject to these requirements.
4) For reporting, tracking and recordkeeping when exceptions allow certain
wastes that do not meet the treatment standards to be land disposed:
There are certain exemptions from the requirement that hazardous wastes
meet treatment standards before they can be land disposed. These
include, but are not limited to, case-by-case extensions under Section
728.105, disposal in a no-migration unit under Section 728.106, or a
national capacity variance or case-by-case capacity variance under
Subpart C of this Part. If a generator’s waste is so exempt, then with
the initial shipment of waste, the generator shall send a one-time written
notice to each land disposal facility receiving the waste. The notice must
include the information indicated in column “728.107(a)(4)” of the
Generator Paperwork Requirements Table in Section 728.Table I. If the
waste changes, the generator shall send a new notice to the receiving
facility, and place a copy in its file.
5) If a generator is managing and treating prohibited waste in tanks,
containers, or containment buildings regulated under 35 Ill. Adm. Code
722.134 to meet applicable LDR treatment standards found at Section
728.140, the generator shall develop and follow a written waste analysis
plan that describes the procedures it will carry out to comply with the
treatment standards. (Generators treating hazardous debris under the
alternative treatment standards of Section 728.Table F, however, are not
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subject to these waste analysis requirements.) The plan must be kept on
site in the generator’s records, and the following requirements must be
met:
A) The waste analysis plan must be based on a detailed chemical and
physical analysis of a representative sample of the prohibited
wastes being treated, and contain all information necessary to
treat the wastes in accordance with the requirements of this Part,
including the selected testing frequency;
B) Such plan must be kept in the facility’s on-site files and made
available to inspectors; and
C) Wastes shipped off-site pursuant to this subsection (a)(5) must
comply with the notification requirements of subsection (a)(3) of
this Section.
6) If a generator determines that the waste is restricted based solely on its
knowledge of the waste, all supporting data used to make this
determination must be retained on-site in the generator’s files. If a
generator determines that the waste is restricted based on testing this
waste or an extract developed using SW-846 Method 1311 (the Toxicity
Characteristic Leaching Procedure), incorporated by reference in 35 Ill.
Adm. Code 720.111, and all waste analysis data must be retained on-site
in the generator’s files.
7) If a generator determines that it is managing a restricted waste which is
excluded from the definition of hazardous or solid waste or which is
exempt from Subtitle C regulation under 35 Ill. Adm. Code 721.102
through 721.106 subsequent to the point of generation (including
deactivated characteristic hazardous wastes that are managed in
wastewater treatment systems subject to the CWA as specified at 35 Ill.
Adm. Code 721.104(a)(2), or which are CWA-equivalent), the generator
shall place a one-time notice stating such generation, subsequent
exclusion from the definition of hazardous or solid waste or exemption
from RCRA Subtitle C regulation, and the disposition of the waste in the
generating facility’s file.
8) A generator shall retain a copy of all notices, certifications, waste
analysis data, and other documentation produced pursuant to this Section
on-site for at least three years from the date that the waste that is the
subject of such documentation was last sent to on-site or off-site
treatment, storage, or disposal. The three year record retention period is
automatically extended during the course of any unresolved enforcement
action regarding the regulated activity or as requested by the Agency.
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The requirements of this subsection (a)(8) apply to solid wastes even
when the hazardous characteristic is removed prior to disposal, or when
the waste is excluded from the definition of hazardous or solid waste
under 35 Ill. Adm. Code 721.102 through 721.106, or exempted from
RCRA Subtitle C regulation, subsequent to the point of generation.
9) If a generator is managing a lab pack containing hazardous wastes and
wishes to use the alternative treatment standard for lab packs found at
Section 728.142(c), the generator shall fulfill the following conditions:
A) With the initial shipment of waste to a treatment facility, the
generator shall submit a notice that provides the information in
column “Section 728.107(a)(9)” in the Generator Paperwork
Requirements Table of Section 728.Table I and the following
certification. The certification, which must be signed by an
authorized representative and must be placed in the generator’s
files, must say the following:
I certify under penalty of law that I personally have
examined and am familiar with the waste and that the lab
pack contains only wastes that have not been excluded
under 35 Ill. Adm. Code 728.Appendix D and that this
lab pack will be sent to a combustion facility in
compliance with the alternative treatment standards for lab
packs at 35 Ill. Adm. Code 728.142(c). I am aware that
there are significant penalties for submitting a false
certification, including the possibility of fine or
imprisonment.
B) No further notification is necessary until such time as the wastes
in the lab pack change, or the receiving facility changes, in which
case a new notice and certification must be sent and a copy
placed in the generator’s file.
C) If the lab pack contains characteristic hazardous wastes (D001-
D043), underlying hazardous constituents (as defined in Section
728.102(i)) need not be determined.
D) The generator shall also comply with the requirements in
subsections (a)(6) and (a)(7) of this Section.
10) Small quantity generators with tolling agreements pursuant to 35 Ill.
Adm. Code 722.120(e) shall comply with the applicable notification and
certification requirements of subsection (a) of this Section for the initial
shipment of the waste subject to the agreement. Such generators shall
359
retain on-site a copy of the notification and certification, together with
the tolling agreement, for at least three years after termination or
expiration of the agreement. The three-year record retention period is
automatically extended during the course of any unresolved enforcement
action regarding the regulated activity or as requested by the Agency.
b)
Treatment facilities The owner or operator of a treatment facility shall test their
its wastes according to the frequency specified in their its waste analysis plans,
as required by 35 Ill. Adm. Code 724.113 (for permitted TSDs) or 725.113 (for
interim status facilities). Such testing must be performed as provided in
subsections (b)(1), (b)(2), and (b)(3) of this Section.
1)
For wastes with treatment standards expressed as concentrations in the
waste extract (Section 728.141TCLP), the owner or operator of the
treatment facility shall test an extract of the treatment residues or an
extract of such residues developed using the test method SW-846 Method
1311 (the Toxicity Characteristic Leaching Procedure), incorporated by
reference in 35 Ill. Adm. Code 720.111, to assure that the treatment
residues or extract meet meets the applicable treatment standards.
2) For wastes prohibited under Section 728.132 or 728.139 that are not
subject to any treatment standards under Subpart D of this Part, the
owner or operator of the treatment facility shall test the treatment
residues according to the generator testing requirements specified in
Section 728.132 to assure that the treatment residues comply with the
applicable prohibitions.
32)
For wastes with treatment standards expressed as concentrations in the
waste (Section 728.143), the owner or operator of the treatment facility
shall test the treatment residues (not an extract of such residues) to
assure that the treatment residues meet the applicable treatment
standards.
43)
A one-time notice must be sent with the initial waste shipment of waste
to each the land disposal facility that includes the following information,
except that debris excluded from the definition of the hazardous waste
under 35 Ill. Adm. Code 721.103(e) (i.e., debris treated by an extraction
or destruction technology provided by Section 728.Table F, and debris
that is delisted) is subject to the notification and certification
requirements of subsection (d) of this Section rather than these
notification requirements. No further notification is necessary until such
time that the waste or receiving facility change, in which case a new
notice must be sent and a A copy of the notice must be placed in the
treatment facility’s file.
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A)
USEPA hazardous waste number;No further notification is
necessary until such time that the waste or receiving facility
changes, in which case a new notice must be sent and a copy
placed in the treatment facility’s file.
B)
The waste constituents that the treater will monitor, if monitoring
will not include all regulated constituents, for wastes F001
through F005, F039, D001, D002, D003, and D012 through
D043. The generator must also include whether the waste is a
nonwastewater or wastewater (as defined in Section 728.102 (d)
and (f)) and indicate the subcategory of the waste (such as “D003
reactive cyanide”) if applicable;The one-time notice must include
the requirements indicated in the following table:
C) The manifest number associated with the shipment of waste; and
D) Waste analysis data, where available.
Treatment Facility Paperwork Requirements Table
Required information
Section
728.107(b)
1. USEPA Hazardous Waste and Manifest
numbers
ü
2. The waste is subject to the LDRs. The
constituents of concern for F001-F005 and
F039 and underlying hazardous constituents
(for wastes that are not managed in a Clean
Water Act (CWA) or CWA-equivalent
facility), unless the waste will be treated
and monitored for all constituents. If all
constituents will be treated and monitored,
there is no need to put them all on the LDR
notice
ü
3. The notice must include the applicable
wastewater/nonwastewater category (see
Section Section 728.102(d) and (f)) and
subdivisions made within a waste code
based on waste-specific criteria (such as
D003 reactive cyanide)
ü
4. Waste analysis data (when available)
ü
5. A certification statement is needed (see
applicable section for exact wording)
ü
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54)
The owner or operator of a treatment facility shall submit a certification
signed by an authorized representative with each the initial shipment of
waste or treatment residue of a restricted waste to the land disposal
facility stating that the waste or treatment residue has been treated in
compliance with the treatment standards specified in Subpart D of this
Part and the applicable prohibitions set forth in Section 728.132 or
728.139. Debris excluded from the definition of hazardous waste under
35 Ill. Adm. Code 721.103(e) (i.e., debris treated by an extraction or
destruction technology provided by Section 728.Table F, and debris that
is delisted), however, is subject to the notification and certification
requirements of subsection (d) of this Section rather than the certification
requirements of this subsection. The certification must state as follows:
I certify under penalty of law that I have personally examined
and am familiar with the treatment technology and operation of
the treatment process used to support this certification. Based on
my inquiry of those individuals immediately responsible for
obtaining this information, I believe that the treatment process
has been operated and maintained properly so as to comply with
the treatment standards specified in 35 Ill. Adm. Code 728.140
without impermissible dilution of the prohibited waste. I am
aware there are significant penalties for submitting a false
certification, including the possibility of fine and imprisonment.
A)
For wastes with treatment standards expressed as concentrations
in the waste extract or in the waste (Sections 728.141 or
728.143), or for wastes prohibited under Section 728.132 or
728.139 that are not subject to any treatment standards under
Subpart D of this Part, the certification must be signed by an
authorized representative and must state the following:A copy of
the certification must be placed in the treatment facility’s on-site
files. If the waste or treatment residue changes, or the receiving
facility changes, a new certification must be sent to the receiving
facility, and a copy placed in the treatment facility’s file.
I certify under penalty of law that I have personally
examined and am familiar with the treatment technology
and operation of the treatment process used to support this
certification and that, based on my inquiry of those
individuals immediately responsible for obtaining this
information, I believe that the treatment process has been
operated and maintained properly, so as to comply with
the performance levels specified in 35 Ill. Adm. Code
Subpart D of this Part and all applicable prohibitions set
forth in 35 Ill. Adm. Code 728.132 or 728.139 or Section
362
3004(d) of the Resource Conservation and Recovery Act
without impermissible dilution of the prohibited waste. I
am aware that there are significant penalties for
submitting a false certification, including the possibility of
fine and imprisonment.
B)
For wastes with treatment standards expressed as technologies
(Section 728.142), the certification must be signed by an
authorized representative and must state the following:Debris
excluded from the definition of hazardous waste under 35 Ill.
Adm. Code 721.103(e) (i.e., debris treated by an extraction or
destruction technology listed in Section 728.Table F and debris
that the Agency has determined does not contain hazardous
waste) is subject to the notification and certification requirements
of subsection (d) of this Section rather than the certification
requirements of this subsection (b)(4).
I certify under penalty of law that the waste has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.142. I am aware that there are
significant penalties for submitting a false certification,
including the possibility of fine and imprisonment.
C)
For wastes with organic constituents having treatment standards
expressed as concentrations levelsin the waste pursuant to Section
728.143, if compliance with the treatment standards in Subpart D
of this Part is based in part or in whole on the analytical detection
limit alternative specified in Section 728.143(c) 728.140(d), the
certification also must be signed by an authorized representative
and must state the following:
I certify under penalty of law that I have personally
examined and am familiar with the treatment technology
and operation of the treatment process used to support this
certification and that,. bBased on my inquiry of those
individuals immediately responsible for obtaining this
information, I believe that the nonwastewater organic
constituents have been treated by incineration in
combustion units operated as specified in accordance with
35 Ill. Adm. Code 724.Subpart O or 35 Ill. Adm. Code
725.Subpart O728.Table C, or by combustion in fuel
substitution units operating in accordance with applicable
technical requirements, and. I have been unable to detect
the nonwastewater organic constituents, despite having
used best good faith efforts to analyze for such
363
constituents. I am aware that there are significant
penalties for submitting a false certification, including the
possibility of fine and imprisonment.
D) For characteristic wastes D001, D002, D003, and D012 through
D043 that are subject to the treatment standards in Section
728.140 (other than those expressed as a required method of
treatment), that are reasonably expected to contain underlying
hazardous constituents (as defined in Section 728.102(i)), that are
treated on-site to remove the hazardous characteristic, and that
are then sent off-site for treatment of underlying hazardous
constituents, the certification must state the following:
I certify under penalty of law that the waste has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.140 to remove the hazardous
characteristic. This decharacterized waste contains
underlying hazardous constituents that require further
treatment to meet universal treatment standards. I am
aware that there are significant penalties for submitting a
false certification, including the possibility of fine and
imprisonment.
E) For characteristic wastes D001, D002, D003, and D012 through
D043 that contain underlying hazardous constituents, as defined
in Section 728.102(i), and which are treated on-site to remove the
hazardous characteristic and to treat underlying hazardous
constituents to levels set forth in the Sections 728.148 and
728.Table U Universal Treatment Standards, the certification
must state the following:
I certify under penalty of law that the waste has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.140 to remove the hazardous
characteristic, and that underlying hazardous constituents,
as defined in Section 728.102, have been treated on-site to
meet the Sections 728.148 and 728.Table U Universal
Treatment Standards. I am aware that there are
significant penalties for submitting a false certification,
including the possibility of fine and imprisonment.
65)
If the waste or treatment residue will be further managed at a different
treatment or storage facility, the treatment, storage, or disposal facility
sending the waste or treatment residue off-site must comply with the
364
notice and certification requirements applicable to generators under this
Section.
76)
Where the wastes are recyclable materials used in a manner constituting
disposal subject to the provisions of 35 Ill. Adm. Code 726.120(b),
regarding treatment standards and prohibition levels, the owner or
operator of a treatment facility (i.e., the recycler) is not required to
notify the receiving facility pursuant to subsection (b)(4) of this Section.
With each shipment of such wastes the owner or operator of the
recycling facility shall submit a certification described in subsection
(b)(5) of this Section and a notice that includes the information listed in
subsection (b)(4) of this Section (except the manifest number) to the
Agency. The recycling facility also shall keep records of the name and
location of each entity receiving the hazardous waste-derived product.
c)
Except where the owner or operator is disposing of any waste that is a
recyclable material used in a manner constituting disposal pursuant to 35 Ill.
Adm. Code 726.120(b), the owner or operator of any land disposal facility
disposing any waste subject to restrictions under this Part shall:
1)
Have Maintain in its files copies of the notice and certifications specified
in subsection (a) or (b) of this Section and the certification specified in
Section 728.108, if applicable.
2)
Test the waste or an extract of the waste or treatment residue developed
using the test method described in Section 728.Appendix A or using any
methods required by generators under Section 728.132 SW-846 Method
1311 (the Toxicity Characteristic Leaching Procedure), incorporated by
reference in 35 Ill. Adm. Code 720.111, to assure that the waste or
treatment residue is in compliance with the applicable treatment
standards set forth in Subpart D of this Part and all applicable
prohibitions set forth in Sections 728.132 or 728.139. Such testing must
be performed according to the frequency specified in the facility’s waste
analysis plan as required by 35 Ill. Adm. Code 724.113 or 725.113.
3)
Where the owner or operator is disposing of any waste that is subject to
the prohibitions under Section 728.133(f) but not subject to the
prohibitions set forth in Section 728.132, the owner or operator shall
ensure that such waste is the subject of a certification according to the
requirements of Section 728.108 prior to disposal in a landfill or surface
impoundment unit, and that such disposal is in accordance with the
requirements of Section 728.105(h)(2). The same requirement applies to
any waste that is subject to the prohibitions under Section 728.133(f) and
also is subject to the statutory prohibitions in the codified prohibitions in
Section 728.139 or Section 728.132.
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4)
Where the owner or operator is disposing of any waste that is a
recyclable material used in a manner constituting disposal subject to the
provisions of 35 Ill. Adm. Code 726.120(b), the owner or operator is
not subject to subsections (c)(1) through (c)(3) of this Section with
respect to such waste.
d)
A generator or treater that first claims that hazardous debris is excluded from
the definition of hazardous waste under 35 Ill. Adm. Code 721.103(e) (i.e.,
debris treated by an extraction or destruction technology provided by Section
728.Table F, and debris that has been delisted) is subject to the following
notification and certification requirements:
1)
A one-time notification must be submitted to the Agency including the
following information:
A)
The name and address of the RCRA Subtitle D (municipal solid
waste landfill) facility receiving the treated debris;
B)
A description of the hazardous debris as initially generated,
including the applicable USEPA hazardous waste numbers; and
C)
For debris excluded under 35 Ill. Adm. Code 721.103(e)(1), the
technology from Section 728.Table F used to treat the debris.
2)
The notification must be updated if the debris is shipped to a different
facility and, for debris excluded under 35 Ill. Adm. Code 721.2(d)(1)
721.102(e)(1), if a different type of debris is treated or if a different
technology is used to treat the debris.
3)
For debris excluded under 35 Ill. Adm. Code 721.103(e)(1), the owner
or operator of the treatment facility shall document and certify
compliance with the treatment standards of Section 728.Table F, as
follows:
A)
Records must be kept of all inspections, evaluations, and analyses
of treated debris that are made to determine compliance with the
treatment standards;
B)
Records must be kept of any data or information the treater
obtains during treatment of the debris that identifies key operating
parameters of the treatment unit; and
C)
For each shipment of treated debris, a certification of compliance
with the treatment standards must be signed by an authorized
366
representative and placed in the facility’s files. The certification
must state the following:
“I certify under penalty of law that the debris has been
treated in accordance with the requirements of 35 Ill.
Adm. Code 728.145. I am aware that there are
significant penalties for making a false certification,
including the possibility of fine and imprisonment.”
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.109
Special Rules for Characteristic Wastes
a)
The initial generator of a solid waste shall determine each USEPA hazardous
waste number (waste code) applicable to the waste in order to determine the
applicable treatment standards under Subpart D of this Part. For purposes of
this Part, the waste must carry the waste code for any applicable listing under
35 Ill. Adm. Code 721.Subpart D. In addition, the waste must carry one or
more of the waste codes under 35 Ill. Adm. Code 721.Subpart C where the
waste exhibits a characteristic, except in the case when the treatment standard
for the waste code listed waste in 35 Ill. Adm. Code 721.Subpart D operates in
lieu of the treatment standard for the characteristic waste code under 35 Ill.
Adm. Code 721.Subpart C, as specified in subsection (b) of this Section. If the
generator determines that its waste displays a characteristic of hazardous waste
(and the waste is not a D004 through D011 waste, a High TOC D001 waste
nonwastewaters treated by CMBST, RORGS, or POLYM of Section 728.Table
C, and is not treated by CMBST or RORGS, as described in Section 728.Table
C), the generator shall determine what underlying hazardous constituents (as
defined in Section 728.102) are reasonably expected to be present above the
universal treatment standards set forth in Sections 728.148 and 728.Table U, the
generator shall determine the underlying hazardous constituents (as defined at
Section 728.102(i)) in the characteristic waste.
b)
Where a prohibited waste is both listed under 35 Ill. Adm. Code 721.Subpart D
and exhibits a characteristic under 35 Ill. Adm. Code 721.Subpart C, the
treatment standard for the waste code listed in 35 Ill. Adm. Code 721.Subpart D
will operate in lieu of the standard for the waste code under 35 Ill. Adm. Code
721.Subpart C, provided that the treatment standard for the listed waste includes
a treatment standard for the constituent that causes the waste to exhibit the
characteristic. Otherwise, the waste must meet the treatment standards for all
applicable listed and characteristic waste codes.
c)
In addition to any applicable standards determined from the initial point of
generation, no prohibited waste that exhibits a characteristic under 35 Ill. Adm.
367
Code 721.Subpart C shall be land disposed unless the waste complies with the
treatment standards under Subpart D of this Part.
d)
A waste that exhibits a characteristic is also subject to Section 728.107
requirements, except that once the waste is no longer hazardous, a one-time
notification and certification must be placed in the generator’s or treater’s files
and sent to the Agency, except for those facilities described in subsection (f)
below of this Section. The notification and certification that is placed in the
generator’s or treater’s files must be updated if the process or operation
generating the waste changes or if the subtitle RCRA Subtitle D (municipal solid
waste landfill) facility receiving the waste changes. However, the generator or
treater need only notify the Agency on an annual basis if such changes occur.
Such notification and certification should be sent to the Agency by the end of
the year, but no later than December 31.
1)
The notification must include the following information:
A)
For a characteristic waste other than one managed on site in a
wastewater treatment system subject to the federal Clean Water
Act (CWA), a zero-discharger engaged in CWA-equivalent
treatment, or a Class I nonhazardous waste injection well, tThe
name and address of the RCRA Subtitle D (municipal solid waste
landfill) facility receiving the waste shipment; and
B)
For a waste that exhibits a characteristic of hazardous waste, a A
description of the waste as initially generated, including the
applicable USEPA hazardous waste numbers, the treatability
group(s), and the underlying hazardous constituents (as defined in
Section 728.102(i)), unless the waste will be treated and
monitored for all underlying hazardous constituents. If all
underlying hazardous constituents will be treated and monitored,
there is no requirement to list any of the underlying hazardous
constituents on the notice.
2)
The certification must be signed by an authorized representative and
must state the language found in Section 728.107(b)(54)(A). If
treatment removes the characteristic but does not treat underlying
hazardous constituents, then the certification found in Section
728.107(b)(5)(D) applies.
3)
For a characteristic waste whose ultimate disposal will be into a Class I
nonhazardous waste injection well, and for which compliance with the
treatment standards set forth in Sections 728.148 and 728.Table U for
underlying hazardous constituents is achieved through pollution
368
prevention that meets the criteria set forth at 35 Ill. Adm. Code
738.101(d), the following information must also be included:
A)
A description of the pollution prevention mechanism and when it
was implemented if already complete;
B)
The mass of each underlying hazardous constituent before
pollution prevention;
C)
The mass of each underlying hazardous constituent that must be
removed, adjusted to reflect variations in mass due to normal
operating conditions; and
D)
The mass reduction of each underlying hazardous constituent that
is achieved.
e)
For a decharacterized waste managed on-site in a wastewater treatment system
subject to the federal Clean Water Act (CWA) or zero-dischargers engaged in
CWA-equivalent treatment, compliance with the treatment standards set forth in
Sections 728.148 and 728.Table D must be monitored quarterly, unless the
treatment is aggressive biological treatment, in which case compliance must be
monitored annually. Monitoring results must be kept in on-site files for 5
years.
f)
For a decharacterized waste managed on-site in a wastewater treatment system
subject to the federal Clean Water Act (CWA) for which all underlying
hazardous constituents (as defined in Section 728.102) are addressed by a CWA
permit, this compliance must be documented and this documentation must be
kept in on-site files.
g)
For a characteristic waste whose ultimate disposal will be into a Class I
nonhazardous waste injection well that qualifies for the de minimis exclusion
described in Section 728.101, information supporting that qualification must be
kept in on-site files.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section 728.130
Waste Specific Prohibitions -- Solvent Wood Preserving Wastes
a) The spent solvent wastes specified in 35 Ill. Adm. Code 721.131 as U.S. EPA
Hazardous Waste Numbers F001, F002, F003, F004, and F005 are prohibited
under this Part from land disposal (except in an injection well) unless one or
more of the following conditions apply:
369
1) The generator of the solvent waste is a small quantity generator of 100 to
1000 kilograms of hazardous waste per month;
2) The solvent waste is generated from any response action taken under
CERCLA or from RCRA corrective action except where the waste is
contaminated soil or debris;
3) The initial generator’s solvent waste is a solvent-water mixture, solvent-
containing sludge or solid, or solvent-contaminated soil (non-CERCLA
or non-RCRA corrective action) containing less than 1 percent total F001
through F005 solvent constituents listed in Table T; or
4) The solvent waste is a residue from treating a waste described in
subsection (a)(1), (a)(2), or (a)(3) above, or the solvent waste is a
residue from treating a waste not described in subsection (a)(1), (a)(2),
or (a)(3), provided such residue belongs to a different treatability group
than the waste as initially generated and wastes belonging to such
treatability group are described in subsection (a)(3).
b) The F001 through F005 solvent wastes listed in subsections (a)(1), (a)(2),
(a)(3), or (a)(4) above are prohibited from land disposal.
c) The F001 through F005 solvent wastes that are contaminated soil and debris
resulting from a CERCLA response or RCRA corrective action or the residue
from treatment of these wastes are prohibited from land disposal.
d) The requirements of subsections (a), (b), and (c) above do not apply if:
1) The wastes meet the standards of 728.Subpart D; or
2) An exemption (adjusted standard) was granted from a prohibition
pursuant to a petition under Section 728.106 with respect to those wastes
and units and the activity is covered by the petition; or
3) Persons have been granted an extension to the effective date of a
prohibition by U.S. EPA pursuant to Section 728.105 with respect to
those wastes and units and the activity is covered by the extension.
a) The following wastes are prohibited from land disposal: the wastes specified in
35 Ill. Adm. Code 721 as USEPA hazardous waste numbers F032, F034, and
F035.
b) Effective May 12, 1999, the following wastes are prohibited from land
disposal: soil and debris contaminated with the wastes specified in 35 Ill. Adm.
370
Code 721 as F032, F034, F035; and radioactive wastes mixed with USEPA
hazardous waste numbers F032, F034, and F035.
c) Until May 12, 1999, soil and debris contaminated with the wastes specified in
35 Ill. Adm. Code 721 as USEPA hazardous waste numbers F032, F034, F035;
and radioactive waste mixed with USEPA hazardous waste numbers F032,
F034, and F035 may be disposed of in a landfill or surface impoundment only if
such unit is in compliance with the requirements specified in Section
728.105(h)(2).
d) The requirements of subsections (a) and (b) of this Section do not apply if:
1) The wastes meet the applicable treatment standards specified in Subpart
D of this Part;
2) Persons have been granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to those wastes and units
covered by the petition;
3) The wastes meet the applicable alternate treatment standards established
pursuant to a petition granted under Section 728.144; or
4) Persons have been granted an extension to the effective date of a
prohibition pursuant to 40 CFR 268.5 (see Section 728.105), with
respect to those wastes covered by the extension.
e) To determine whether a hazardous waste identified in this Section exceeds the
applicable treatment standards specified in Sections 728.140 and 728.Table T,
the initial generator shall test a sample of the waste extract or the entire waste,
depending on whether the treatment standards are expressed as concentrations in
the waste extract or the waste, or the generator may use knowledge of the
waste. If the waste contains constituents in excess of the applicable universal
treatment standard levels of Sections 728.148 and 728.Table U, the waste is
prohibited from land disposal and all requirements of Part 728 are applicable,
except as otherwise specified.
(Source: Repealed and New Section Added at 22 Ill. Reg. ________, effective
______________________)
Section 728.132
Waste Specific Prohibitions -- California List Wastes (Repealed)
a) The following hazardous wastes are prohibited from land disposal (except in
injection wells):
1) Liquid hazardous wastes having a pH less than or equal to two (2.0);
371
2) Liquid hazardous wastes containing PCBs at concentrations greater than or
equal to 50 ppm;
3) Liquid hazardous wastes that are primarily water and contain halogenated
organic compounds (HOCs) in total concentration greater than or equal to
1000 mg/1 and less than 10,000 mg/1 HOCs.
d) The requirements of subsection (a) and (e) do not apply until:
1) November 8, 1989 where the wastes are contaminated soil or debris not
resulting from a CERCLA response action or from RCRA corrective action,
as defined in Section 728.102. Until July 8, 1989, the wastes may be
disposed of in a landfill or surface impoundment only if such disposal is in
compliance with the requirements in 40 CFR 268.5(h)(2), incorporated by
reference in Section 728.105.
2) November 8, 1990, where the wastes are contaminated soil or debris
resulting from a CERCLA response action or RCRA corrective action.
Until November 8, 1990, the wastes may be disposed in a landfill or surface
impoundment only if such unit is in compliance with the requirements
specified in 40 CFR 268.5(h)(2), incorporated by reference in Section
728.105.
e) The following hazardous wastes are prohibited from land disposal (subject to any
regulation that may be promulgated with respect to disposal in injection wells):
1) Liquid hazardous wastes that contain HOCs in total concentration greater
than or equal to 1000 mg/1 and are not prohibited under subsection (a)(3);
and
2) Nonliquid hazardous wastes containing HOCs in total concentration greater
than or equal to 1000 mg/kg and which are not wastes described in
subsection (d).
f) The wastes described in subsections (e)(1) and (e)(2) may be disposed of in a
landfill or surface impoundment only if such unit is in compliance with the
requirements specified in 40 CFR 268.5(h)(2), incorporated by reference in Section
728.105.
g) The requirements of subsections (a) (d) and (e) do not apply if:
1) Persons have been granted an adjusted standard from a prohibition pursuant
to a petition under Section 728.106, with respect to those wastes and units
covered by the petition (except for liquid hazardous wastes containing PCBs
372
at concentrations greater than or equal to 500 ppm which are not eligible for
exemptions); or,
2) Persons have been granted an extension to the effective date of a prohibition
pursuant to Section 728.105, with respect to those wastes covered by the
extension; or
3) The wastes meet the applicable standards specified in Subpart D or, where
treatment standards are not specified, the wastes are in compliance with the
applicable prohibitions set forth in this Section or Section 728.139.
h) The prohibitions and effective dates specified in subsections (a)(3), (d) and (e) do
not apply where the waste is subject to a Subpart C prohibition and effective date for
a specified HOC (such as a hazardous waste chlorinated solvent, see e.g. Section
728.130(a)).
i) To determine whether or not a waste is a liquid under subsections (a) or (e) or under
Section 728.139, the following test must be used:
Method 9095 (Paint Filter Liquids Test), as described in “Test Methods for
Evaluating Solid Wastes”, incorporated by reference in 35 Ill. Adm. Code
720.111.
j) Except as otherwise provided in this subsection, the waste analysis and
recordkeeping requirements of Section 728.107 are applicable to wastes prohibited
under this Part or Section 728.139:
1) The initial generator of a liquid hazardous waste shall test the waste (not an
extract or filtrate) in accordance with the procedures specified in 35 Ill.
Adm. Code 721.122(a)(1), or use knowledge of the waste, to determine if
the waste has a pH less than or equal to two (2.0). If the liquid waste has a
pH less than or equal to two (2.0), it is restricted from land disposal and all
requirements of this Part are applicable, except as otherwise specified in this
Section.
2) The intitial generator of either a liquid hazardous waste containing PCBs or
a liquid or nonliquid hazardous waste containing HOCs shall test the waste
(not an extract or filtrate), or use knowledge of the waste, to determine
whether the concentration levels in the waste equal or exceed the prohibition
levels specified in this Section. If the concentration of PCBs or HOCs in the
waste is greater than or equal to the prohibition levels specified in this
Section, the waste is restricted from land disposal and all requirements of
this Part are applicable, except as otherwise specified in this Section.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
373
Section 728.133
Waste Specific Prohibitions: -- First Third Wastes (Repealed)
a) The wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA hazardous wastes
numbers listed below are prohibited from land disposal (except in an injection well).
F006 (nonwastewater)
K001
K004 wastes specified in Sections 728.140 and 728.Table T
K008 wastes specified in Sections 728.140 and 728.Table T
K015
K016
K018
K019
K020
K021 wastes specified in Section Sections 728.140 and 728.Table T
K022 (nonwastewater)
K024
K025 nonwastewaters specified in Sections 728.140 and 728.Table T
K030
K036 (nonwastewater)
K037
K044
K045 (nonexplosive)
K046 (nonwastewater)
K047
K060 (nonwastewater)
K06l (nonwastewaters containing less than 15% zinc)
K062 (non CaSO
4
)
K069 (nonwastewater)
K086 (solvent washes),
K087
K099
K100 nonwastewaters specified in Sections 728.140 and 728.Table T
K101 (wastewater)
K101 (nonwastewater, low arsenic subcategory--less than 1% total arsenic)
K102 (wastewater)
K102 (nonwastewater, low arsenic subcategory--less than 1% total arsenic)
K103
K104
b) The waste specified in 35 Ill. Adm. Code 721.132 as U.S. EPA Hazardous Waste
No. K071 is prohibited from land disposal.
374
c) The wastes specified in Section 728.110 having a treatment standard in 728.Subpart
D based on incineration and which are contaminated soil and debris are prohibited
from land disposal.
e) The requirements of subsection (a), (b), and (c) above do not apply if:
1) The waste meets the applicable standards specified in 728.Subpart D;
2) An adjusted standard was granted pursuant to Section 728.106 with respect
to those wastes and units, and the activity is covered by the adjusted
standard; or
3) Persons have been granted an extension to the effective date of a prohibition
by U.S. EPA pursuant to Section 728.105 with respect to those wastes and
units and the activity is covered by the extension.
f) This subsection corresponds with 40 CFR 268.33(f), a provision whose
effectiveness has expired. This statement maintains structural consistency with U.S.
EPA regulations.
g) To determine whether a hazardous waste listed in Section 728.110 exceeds the
applicable treatment standards specified in Sections 728.131, 728.140, and
728.Table T, the initial generator shall test a representative sample of the waste
extract or the entire waste depending on whether the treatment standards are
expressed as concentrations in the waste extract or the waste, or the generator may
use knowledge of the waste. If the waste contains constituents in excess of the
applicable 728.Subpart D levels, the waste is prohibited from land disposal and all
requirements of this Part are applicable except as otherwise specified.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.134
Waste Specific Prohibitions -- Second Third Wastes (Repealed)
a) The following wastes are prohibited from land disposal.
1) The wastes specified in 35 Ill. Adm. Code 721.131 as USEPA hazardous
waste numbers:
F010
F024
2) The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA hazardous
waste numbers:
K005
375
K007
K009 (nonwastewaters)
K010
K023
K027
K028
K029 (nonwastewaters)
K036 (wastewaters)
K038
K039
K040
K043
K093
K094
K095 (nonwastewaters)
K096 (nonwastewaters)
K113
K114
K115
K116
3) The wastes specified in 35 Ill. Adm. Code 721.133 as USEPA hazardous
waste numbers:
P013
P021
P029
P030
P039
P040
P041
P043
P044
P062
P063
P071
P074
P085
P089
P094
P097
P098
P099
P104
P106
376
P109
P111
P121
U028
U058
U069
U087
U088
U102
U107
U221
U223
U235
b) The following wastes are prohibited from land disposal, except when they are
injected into a UIC well pursuant to 35 Ill. Adm. Code 738.114(f) or 738.115(d)
USEPA hazardous waste numbers:
K009 (wastewaters)
K011 (nonwastewaters)
K013 (nonwastewaters)
K014 (nonwastewaters)
c) The following wastes are prohibited from land disposal: The wastes specified in 35
Ill. Adm. Code 721.131 as USEPA hazardous waste numbers:
F006--cyanide (nonwastewater)
F008
F009
F011 (wastewaters)
F012 (wastewaters)
1) The following waste is prohibited from land disposal except when it is
injected into a UIC well pursuant to 35 Ill. Adm. Code 738.114(f): The
waste specified in 35 Ill. Adm. Code 721.131 as USEPA hazardous waste
number F007.
2) The following wastes are prohibited from land disposal pursuant to the
treatment standards specified in Sections 728.141 or 728.143 applicable to
those wastes:
F011 (nonwastewaters)
F012 (nonwastewaters)
377
d) Effective June 8, 1991, the following wastes are prohibited from land disposal: The
wastes specified in this Section having a treatment standard in Subpart D based on
incineration, and which are contaminated contaminated soil and debris.
e) Until June 8, 1991, wastes included in subsections (c) and (d) may be disposed in a
landfill or surface impoundment, regardless whether such unit is a new, replacement
or lateral expansion unit, only if such unit is in compliance with the technical
requirements specified in 40 CFR 268.5(h)(2), incorporated by reference in Section
728.105.
f) The requirements of subsections (a), (b), (c) and (d) do not apply if:
1) The wastes meet the applicable standards specified in Subpart D; or
2) Persons have been granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to those wastes and units
covered by the petition.
g) The requirements of subsections (a), (b) and (c) do not apply if persons have been
granted an extension to the effective date of a prohibition pursuant to Section
728.105, with respect to those wastes covered by the extension.
h) Until May 8, 1990, the second third wastes specified in 40 CFR 268.11 (1989) for
which treatment standards under Subpart D are not applicable, including California
list wastes subject to the statutory prohibitions of Section 728.139 or codified
prohibitions under Section 728.132, are prohibited from disposal in a landfill or
surface impoundment unless the wastes are subject to a valid demonstration and
certification pursuant to Section 728.108.
i) To determine whether a hazardous wastes exceeds the applicable treatment standards
specified in Section 728.141 or 728.143, the initial generator shall test a
representative sample of the waste extract, or the entire waste, depending on
whether the treatment standards are expressed as concentrations in the waste extract
or the waste, or the generator may use knowledge of the waste. If the waste contain
constituents in excess of the applicable Subpart D levels, the wastes is prohibited
from land disposal and all the requirements of this Part are applicable, except as
otherwise specified.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.135
Waste Specific Prohibitions--Third Third Wastes (Repealed)
a) The following wastes are prohibited from land disposal.
378
1) The wastes specified in 35 Ill. Adm. Code 721.131 as U.S. EPA hazardous
waste numbers:
F002 (1,1,2-trichloroethane)
F005 (benzene)
F005 (2-ethoxyethanol)
F005 (2-nitropropane)
F006 (wastewaters),
F019
F025
F039 (wastewaters);
2) The wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA hazardous
waste numbers:
K002
K003
K004 (wastewaters)
K005 (wastewaters)
K006
K008 (wastewaters)
K011 (wastewaters)
K013 (wastewaters)
K014 (wastewaters)
K015 (nonwastewaters)
K017
K021 (wastewaters)
K022 (wastewaters)
K025 (wastewaters)
K026
K029 (wastewaters)
K031 (wastewaters)
K032
K033
K034
K035
K041
K042
K046 (wastewaters, reactive nonwastewaters)
K048 (wastewaters)
K049 (wastewaters)
K050 (wastewaters)
K051 (wastewaters)
K052 (wastewaters)
K060 (wastewaters)
379
K061 (wastewaters) and (high zinc subcategory > 15% zinc)
K069 (wastewaters, calcium sulfate nonwastewaters)
K073
K083
K084 (wastewaters)
K085
K095 (wastewaters)
K096 (wastewaters)
K097
K098
K100 (wastewaters)
K101 (wastewaters)
K102 (wastewaters)
K105
K106 (wastewaters)
3) The wastes specified in 35 Ill. Adm. Code 721.133(e) as U.S. EPA
hazardous waste numbers:
P001
P002
P003
P004
P005
P006
P007
P008
P009
P010 (wastewaters)
P011 (wastewaters)
P012 (wastewaters)
P014
P015
P016
P017
P018
P020
P022
P023
P024
P026
P027
P028
P031
P033
380
P034
P036 (wastewaters)
P037
P038 (wastewaters)
P042
P045
P046
P047
P048
P049
P050
P051
P054
P056
P057
P058
P059
P060
P064
P065 (wastewaters)
P066
P067
P068
P069
P070
P072
P073
P075
P076
P077
P078
P081
P082
P084
P088
P092 (wastewaters)
P093
P095
P096
P101
P102
P103
P105
P108
P110
381
P112
P113
P114
P115
P116
P118
P119
P120
P122
P123
4) The wastes specified in 35 Ill. Adm. Code 721.133(f) as U.S. EPA
hazardous waste numbers:
U001
U002
U003
U004
U005
U006
U007
U008
U009
U010
U011
U012
U014
U015
U016
U017
U018
U019
U020
U021
U022
U023
U024
U025
U026
U027
U029
U030
U031
U032
U033
382
U034
U035
U036
U037
U038
U039
U041
U042
U043
U044
U045
U046
U047
U048
U049
U050
U051
U052
U053
U055
U056
U057
U059
U060
U061
U062
U063
U064
U066
U067
U068
U070
U071
U072
U073
U074
U075
U076
U077
U078
U079
U080
U081
U082
U083
383
U084
U085
U086
U089
U090
U091
U092
U093
U094
U095
U096
U097
U098
U099
U101
U103
U105
U106
U108
U109
U110
U111
U112
U113
U114
U115
U116
U117
U118
U119
U120
U121
U122
U123
U124
U125
U126
U127
U128
U129
U130
U131
U132
U133
U134
384
U135
U136 (wastewaters)
U137
U138
U140
U141
U142
U143
U144
U145
U146
U147
U148
U149
U150
U151 (wastewaters)
U152
U153
U154
U155
U156
U157
U158
U159
U160
U161
U162
U163
U164
U165
U166
U167
U168
U169
U170
U171
U172
U173
U174
U176
U177
U178
U179
U180
U181
385
U182
U183
U184
U185
U186
U187
U188
U189
U191
U192
U193
U194
U196
U197
U200
U201
U202
U203
U204
U205
U206
U207
U208
U209
U210
U211
U213
U214
U215
U216
U217
U218
U219
U220
U222
U225
U226
U227
U228
U234
U236
U237
U238
U239
U240
386
U243
U244
U246
U247
U248
U249
5) The following wastes identified as hazardous based on a characteristic alone:
D001
D002
D003
D004 (wastewaters)
D005
D006
D007
D008 (except for lead materials stored before secondary smelting)
D009 (wastewaters)
D010
D011
D012
D013
D014
D015
D016
D017
b) The following wastes are prohibited from land disposal. The wastes specified in 35
Ill. Adm. Code 721.132 as U.S. EPA hazardous waste numbers:
K048 (nonwastewaters)
K049 (nonwastewaters)
K050 (nonwastewaters)
K051 (nonwastewaters)
K052 (nonwastewaters)
c) The following wastes are prohibited from land disposal:
1) The wastes specified in 35 Ill. Adm. Code 721.131 as U.S. EPA hazardous
waste numbers:
F039 (nonwastewaters)
2) The wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA hazardous
waste numbers:
387
K031 (nonwastewaters)
K084 (nonwastewaters)
K101 (nonwastewaters)
K102 (nonwastewaters)
K106 (nonwastewaters)
3) The wastes specified in 35 Ill. Adm. Code 721.133(e) as U.S. EPA
hazardous waste numbers:
P010 (nonwastewaters)
P011 (nonwastewaters)
P012 (nonwastewaters)
P036 (nonwastewaters)
P038 (nonwastewaters)
P065 (nonwastewaters)
P087
P092 (nonwastewaters)
4) The wastes specified in 35 Ill. Adm. Code 721.133(f) as U.S. EPA
hazardous waste numbers:
U136 (nonwastewaters)
U151 (nonwastewaters)
5) The following wastes identified as hazardous based on a characteristic alone:
D004 (nonwastewaters)
D009 (nonwastewaters);
6) RCRA hazardous wastes that contain naturally occurring radioactive
materials.
d) Hazardous wastes listed in Sections 728.110, 728.111 or 728.112 that are mixed
radioactive/hazardous wastes, and soil or debris contaminated with hazardous wastes
listed in Sections 728.110, 728.111 or 728.112 that are mixed radioactive/hazardous
wastes, are prohibited from land disposal, except as provided in subsection (e)
below.
e) Subject to the applicable prohibitions of Sections 728.130, 728.131, and 728.132,
contaminated soil and debris are prohibited from land disposal as follows:
388
1) Effective May 8, 1994, debris that is contaminated with wastes listed in
Section 728.112 and debris that is contaminated with any characteristic
waste for which treatment standards are established in Subpart D of this Part
are prohibited from land disposal.
2) Effective May 8, 1994, mixed radioactive hazardous debris that is
contaminated with hazardous wastes listed in Section 728.112 and mixed
radioactive hazardous debris that is contaminated with any characteristic
waste for which treatment standards are established in Subpart D of this Part
are prohibited from land disposal.
3) Subsections (e)(1) and (e)(2) of this Section shall not apply where the
generator has failed to make good-faith effort to locate treatment capacity
suitable for its waste, has not utilized such capacity as it has found to be
available, or has failed to file a report as required by Section 728.105(g) by
August 12, 1993 or within 90 days after the waste is generated (whichever is
later) describing the generator’s efforts to locate treatment capacity. Where
subsections (e)(1) and (e)(2) of this Section do not apply, all wastes
described in those two subsections are prohibited from land disposal.
BOARD NOTE: This subsection is derived from 40 CFR 268.35(e)(3), as
added at 58 Fed. Reg. 28510 (May 14, 1993). This was a HSWA-derived
amendment that went into effect as federal law in Illinois, effective May 8,
1993. The August 12, 1993 report was due on that date as a matter of
federal law.
4) Hazardous soil having treatment standards in 728.Subpart D based on
incineration, mercury retorting or vitrification, and soils contaminated with
hazardous wastes listed in Sections 728.110, 728.111 and 728.112 that are
mixed radioactive hazardous wastes, are prohibited from land disposal.
5) When used in subsections (e)(1) and (e)(2) of this Section, debris is defined
as follows:
A) Debris as defined in Section 728.102(g); or
B) Nonfriable inorganic solids that are incapable of passing through a
9.5 mm standard sieve that require cutting or crushing and grinding
in mechanical sizing equipment prior to stabilization, limited to the
following inorganic or metal materials:
i) Metal slag (either dross or scoria);
ii) Glassified slag;
389
iii) Glass;
iv) Concrete (excluding cementitious or pozzolanic stabilized
hazardous wastes);
v) Masonry and refractory bricks;
vi) Metal cans, containers, drums, or tanks;
vii) Metal nuts, bolts, pipes, pumps, valves, appliances, or
industrial equipment; or
viii) Scrap metal as defined in 35 Ill. Adm. Code 721.101(c)(6).
f) This subsection corresponds with 40 CFR 268.35(f), which pertains to an exemption
from a land disposal prohibition up until a date long since expired. This statement
maintains structural consistency with USEPA rules.
g) This subsection corresponds with 40 CFR 268.35(g), which pertains to an
exemption from a land disposal prohibition up until a date long since expired. This
statement maintains structural consistency with USEPA rules.
h) This subsection corresponds with 40 CFR 268.35(h), which pertains to landfill and
surface impoundment disposal of the wastes listed in subsections (c), (d) and (e)
above up until a date long since expired. This statement maintains structural
consistency with USEPA rules.
i) The requirements of subsections (a) through (e), above, do not apply if:
1) The wastes meet the applicable standards specified in Subpart D of this Part;
2) Persons have been granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to those wastes and units
covered by the petition;
3) The wastes meet the applicable alternate standards established pursuant to a
petition granted under Section 728.144;
4) Persons have been granted an extension to the effective date of a prohibition
pursuant to Section 728.105, with respect to these wastes covered by the
extension.
j) To determine whether a hazardous waste listed in Section 728.110, 728.111 or
728.112 exceeds the applicable treatment standards specified in Sections 728.141
and 728.143, the initial generator shall either test a representative sample of the
390
waste extract or the entire waste, depending on whether the treatment standards are
expressed as concentrations in the waste extract or the waste, or use knowledge of
the waste. If the waste contains constituents in excess of the applicable Subpart D
of this Part levels, the waste is prohibited from land disposal, and all requirements
of this Part are applicable, except as otherwise specified.
k) D008 lead materials stored before secondary smelting are prohibited from land
disposal. On or before March 1, 1993, the owner or operator of each secondary
lead smelting facility shall have submitted the following to the Agency: A binding
contractual commitment to construct or otherwise provide capacity for storing such
D008 wastes prior to smelting which complies with all applicable storage standards;
documentation that the capacity to be provided will be sufficient to manage the
entire quantity of such D008 wastes; and, a detailed schedule for providing such
capacity. Failure by a facility to have submitted such documentation will render
such D008 managed by that facility prohibited from land disposal. In addition, the
owner or operator of each facility shall place in the facility record documentation of
the manner and location in which such wastes will be managed pending completion
of such capacity, demonstrating that such management capacity will be adequate and
complies with all applicable requirements of 35 Ill. Adm. Code 720 through 728.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.136
Waste Specific Prohibitions -- Newly Listed Wastes (Repealed)
a) The wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA hazardous waste
numbers K107, K108, K109, K110, K111, K112, K117, K118, K123, K124,
K125, K126, K131, K132, and K136; and the wastes specified in 35 Ill. Adm.
Code 721.133(f) as U.S. EPA hazardous waste numbers U328, U353, and U359
are prohibited from land disposal.
b) The wastes specified in 35 Ill. Adm. Code 721.131 as U.S. EPA hazardous waste
numbers F037 and F038 that are not generated from surface impoundment cleanouts
or closures are prohibited from land disposal.
c) Effective June 30, 1994, the wastes specified in 35 Ill. Adm. Code 721.131 as U.S.
EPA hazardous waste numbers F037 and F038 that are generated from surface
impoundment cleanouts or closures are prohibited from land disposal.
d) Effective June 30, 1994, radioactive wastes that are mixed with hazardous wastes
specified in 35 Ill. Adm. Code 721.131 as U.S. EPA hazardous waste numbers
F037 and F038; the wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA
hazardous waste numbers K107, K108, K109, K110, K111, K112, K117, K118,
K123, K124, K125, K126 K131, K132, and K136; or the wastes specified in 35 Ill.
Adm. Code 721.133(f) as U.S. EPA hazardous waste numbers U328, U353, and
U359 are prohibited from land disposal.
391
e) Effective June 30, 1994, debris contaminated with hazardous wastes specified in 35
Ill. Adm. Code 721.131 as U.S. EPA hazardous waste numbers F037 and F038;
the wastes specified in 35 Ill. Adm. Code 721.132 as U.S. EPA hazardous waste
numbers K107, K108, K109, K110, K111, K112, K117, K118, K123, K124,
K125, K126 K131, K132, and K136; or the wastes specified in 35 Ill. Adm. Code
721.133(f) as U.S. EPA hazardous waste numbers U328, U353, and U359; and
which is not contaminated with any other waste already subject to a prohibition are
prohibited from land disposal.
f) This subsection corresponds with 40 CFR 268.36(f), which pertains to landfill
disposal of the wastes listed in subsection (b) above up until a date long since
expired. This statement maintains structural consistency with USEPA rules.
g) Between June 30, 1992 and June 30, 1994, the wastes included in subsections (d)
and (e) of this Section may be disposed of in a landfill only if such unit is in
compliance with the requirements specified in subsection 728.105(h)(2), and may be
generated in and disposed of in a surface impoundment only if such unit is in
compliance with either subsection 728.105(h)(2) or Section 728.114.
h) The requirements of subsections (a) through (e) above do not apply if:
1) The wastes meet the applicable standards specified in 728.Subpart D;
2) Persons have been granted an exemption from a prohibition pursuant to a
petition under Section 728.106, with respect to those wastes and units
covered by the petition;
3) The wastes meet the applicable alternate standards established pursuant to a
petition granted under Section 728.144;
4) Persons have been granted an extension to the effective date of a prohibition
pursuant to Section 728.105, with respect to the wastes covered by the
extension.
i) To determine whether a hazardous waste identified in this Section exceeds the
applicable treatment standards specified in Sections 728.141 and 728.143, the initial
generator shall test a representative sample of the waste extract or the entire waste,
depending on whether the treatment standards are expressed as concentrations in the
waste extract or the waste, or the generator may use knowledge of the waste. If the
waste contains constituents in excess of the applicable levels in 728.Subpart D, the
waste is prohibited from land disposal, and all requirements of Part 728 are
applicable, except as otherwise specified.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
392
SUBPART D: TREATMENT STANDARDS
Section 728.144
Adjustment of Treatment Standard
a)
Where the treatment standard is expressed as a concentration in a waste or waste
extract and a waste cannot be treated to the specified level, or where the
treatment technology is not appropriate to the waste, the generator or treatment
facility may petition to the Board for an adjusted treatment standard. As
justification, the petitioner shall demonstrate that, because the physical or
chemical properties of the waste differ significantly from wastes analyzed in
developing the treatment standard, the waste cannot be treated to specified
levels or by the specified methods.
BOARD NOTE: 40 CFR 268.44 refers to these as “treatability variances”.
The Board has not used this term in its rules to avoid confusion with the Board
variances under Title IX of the Environmental Protection Act. The equivalent
Board procedures are an “adjusted treatment standard” pursuant to subsections
(a) through (l) of this Section, or a “treatability exception” adopted pursuant to
subsections (m) et seq. While the latter is adopted by “identical in substance”
rulemaking following a USEPA action, the former is an original Board action
which will be the only mechanism following authorization to the State of this
component of the RCRA program.
b)
Each petition must be submitted in accordance with the procedures in 35 Ill.
Adm. Code 106.Subpart G.
c)
Each petition must include the following statement signed by the petitioner or an
authorized representative:
I certify under penalty of law that I have personally examined and am
familiar with the information submitted in this petition and all attached
documents, and that, based on my inquiry of those individuals
immediately responsible for obtaining the information, I believe that the
submitted information is true, accurate and complete. I am aware that
there are significant penalties for submitting false information, including
the possibility of fine and imprisonment.
d)
After receiving a petition for an adjusted treatment standard, the Board may
request any additional information or samples which are necessary to evaluate
the petition.
e)
The Board will give public notice and provide an opportunity for public
comment, as provided in 35 Ill. Adm. Code 106. In conjunction with any
393
updating of the RCRA regulations, the Board will maintain, in this Part, a
listing of all adjusted treatment standards granted by the Board pursuant to this
Section. A LISTING OF ALL ADJUSTED STANDARDS GRANTED
PURSUANT TO THIS SECTION WILL BE PUBLISHED IN THE ILLINOIS
REGISTER AND ENVIRONMENTAL REGISTER AT THE END OF EACH
FISCAL YEAR. (Section 28.1(d)(3) of the Environmental Protection Act [415
ILCS 5/28.1(d)(3)].)
f)
A generator, treatment facility or disposal facility that is managing a waste
covered by an adjusted treatment standard shall comply with the waste analysis
requirements for restricted wastes found under Section 728.107.
g)
During the petition review process, the applicant is required to comply with all
restrictions on land disposal under this Part once the effective date for the waste
has been reached.
h)
Where the treatment standard is expressed as a concentration in a waste or waste
extract and a waste generated under conditions specific to only one site cannot
be treated to the specified level, or where treatment technology is not
appropriate to the waste, the generator or treatment facility may petition the
Board for a site-specific adjusted treatment standard. The petitioner shall
demonstrate that, because the physical or chemical properties of the waste
differs significantly from the waste analyzed in developing the treatment
standard, the waste cannot be treated to specified levels or by the specified
methods.
i)
Each petition for a site-specific adjusted treatment standard must include the
information in 35 Ill. Adm. Code 720.120(b)(1) through (b)(4).
j)
After receiving a petition for a site-specific adjusted treatment standard, the
Board may request any additional information or samples which the Board
determines are necessary to evaluate the petition.
k)
A generator, treatment facility or disposal facility which is managing a waste
covered by a site-specific adjusted treatment standard shall comply with the
waste analysis requirements for restricted wastes in Section 728.107.
l)
During the petition review process, the petitioner for a site-specific adjusted
treatment standard shall comply with all restrictions on land disposal under this
Part once the effective date for the waste has been reached.
m)
If USEPA grants a treatability exception by regulatory action pursuant to 40
CFR 268.44 (1996) and a person demonstrates that the treatability exception
needs to be adopted as part of the Illinois RCRA program because the waste is
generated or managed in Illinois, the Board will adopt the treatability exception
394
by identical in substance rulemaking pursuant to Section 22.4(a) of the
Environmental Protection Act.
BOARD NOTE: The Board will adopt the treatability exception during a
RCRA update Docket if a timely demonstration is made. Otherwise, the Board
will assign the matter to a separate Docket. This subsection (m) is not derived
directly from a federal regulation. Corresponding 40 CFR 264.1030(m) is
marked “reserved” by USEPA.
n) This subsection (n) corresponds with 40 CFR 264.1030(n), marked “reserved”
by USEPA. This statement maintains structural consistency with USEPA rules.
o)
The facilities listed in Section 728.Table H are excluded from the treatment
standard standards under Sections 728.143(a) and 728.Table B, and are subject
to the constituent concentrations listed in Section 728.Table H.
p) This subsection (p) corresponds with 40 CFR 264.1030(p), which is a site-
specific regulation that applies to a facility outside Illinois. This statement
maintains structural consistency with USEPA rules.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix A
Toxicity Characteristic Leaching Procedure (TCLP)
(Repealed)
Note: The TCLP (Method 1311) is published in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods”, U.S. EPA Publication SW-846, as incorporated by reference in
35 Ill. Adm. Code 720.111.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix B
Treatment Standards (As concentrations in the Treatment Residual Extract)
(Repealed)
The Board incorporates by reference 40 CFR 268, Appendix II (1992), as amended at 57 Fed.
Reg. 37281 (Aug. 18, 1992). This incorporation includes no future editions or amendments.
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix C
List of Halogenated Organic Compounds (Repealed)
VOLATILES
Bromodichloromethane
Bromomethane
Carbon tetrachloride
Chlorobenzene
395
2-Chloro-1,3-butadiene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
3-Chloropropene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
Dibromomethane
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethylene
trans-1,2-Dichloroethene
1,2,-Dichloropropane
trans-1,3,-Dichloropropene
cis-1,3-Dichloropropene
Iodomethane
Methylene chloride
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tribromomethane
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichloromonofluoromethane
1,2,3-Trichloropropane
Vinyl chloride
SEMIVOLATILES
Bis(2-chloroethoxy)ethane
Bis(2-chloroethyl) ether
Bis(2-chloroisopropyl) ether
p-Chloroaniline
Chlorobenzilate
p-Chloro-m-cresol
2-Chloronaphthalene
2-Chlorophenol
3-Chloropropionitrile
m-Dichlorobenzene
o-Dichlorobenzene
396
p-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
2,6-Dichlorophenol
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Hexachlorophene
Hexachloropropene
4,4'-Methylenebis(2-chloroaniline)
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Pronamide
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Tris(2,3-dibromopropyl)phosphate
ORGANOCHLORINE PESTICIDES
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC
Chlordane
DDD
DDE
DDT
Dieldrin
Endosulfan I
Endosulfane II
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
Isodrin
Kepone
Methoxychlor
Toxaphene
397
PHENOXYACETIC ACID HERBICIDES
2,4-Dichlorophenoxyacetic acid
Silvex
2,4,5-T
PCBs
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
PCBs not otherwise specified
DIOXINS AND FURANS
Hexachlorodibenzo-p-dioxins
Hexachlorodibenzofuran
Pentachlorodibenzo-p-dioxins
Pentachlorodibenzofuran
Tetrachlorodibenzo-p-dioxins
Tetrachlorodibenzofuran
2,3,7,8,-Tetrachlorodibenzo-p-dioxin
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix F
Technologies to Achieve Deactivation of Characteri
stics
The treatment standard for many subcategories of D001, D002 and D003 wastes as well as for
K044, K045 and K047 wastes is listed in Section 728.142 simply as “Deactivation to remove
the characteristics of ignitability, corrosivity, and reactivity”. characteristic wastes is stated in
the Section 728.Table T, entitled “Treatment Standards for Hazardous Wastes,” as “DEACT
and meet Section 728.148 standards.” USEPA has determined that many technologies, when
used alone or in combination, can achieve this the deactivation portion of the treatment
standard. Characteristic wastes that are not managed in a facility regulated by the CWA or in
a CWA-equivalent facility, and that also contain underlying hazardous constituents (see Section
728.102(i)) must be treated not only by a “deactivating” technology to remove the
characteristic, but also to achieve the universal treatment standards (UTS) for underlying
hazardous constituents. The following This appendix presents a partial list of these
technologies, utilizing the five letter technology codes established in Table C, that may be
useful in meeting the treatment standard. Use of these specific technologies is not mandatory
398
and does not preclude direct reuse, recovery or the use of other pretreatment technologies,
provided deactivation is achieved and these alternative methods are not performed in units
designated as land disposal underlying hazardous constituents are treated to achieve the UTS.
Waste code/subcategory
Nonwastewaters
Wastewaters
D001 Ignitable Liquids based on 35 Ill. Adm. Code
721.121(a)(1)—Low TOC Nonwastewater
Subcategory (containing 1% one percent to <10%
percent TOC)
RORGS
WETOX
INCIN
CHOXD
BIODG
n.a.
D001 Ignitable Liquids based on 35 Ill. Adm. Code
721.121(a)(1)—Ignitable Wastewater Subcategory
(containing <1% percent TOC)
n.a.
WETOX
RORGS
INCIN
CHOXD
BIODG
D001 Compressed Gases based on 35 Ill. Adm. Code
721.121(a)(3)
RCGAS
FSUBS
INCIN
ADGAS fb.
INCIN
ADGAS fb.
(CHOXD; or
CHRED)
n.a.
D001 Ignitable Reactives based on 35 Ill. Adm. Code
721.121(a)(2)
WTRRX
CHOXD
CHRED
STABL
INCIN
n.a.
D001 Ignitable Oxidizers based on 35 Ill. Adm.
Code 721.121(a)(4)
CHRED
INCIN
CHRED
INCIN
D002 Acid Subcategory based on 35 Ill. Adm. Code
721.122(a)(1) with pH less than or equal to 2
RCORR
NEUTR
INCIN
NEUTR
INCIN
D002 Alkaline Subcategory based on 35 Ill. Adm.
Code 721.122(a)(1) with pH greater than or equal to
12.5
NEUTR
INCIN
NEUTR
INCIN
D002 Other Corrosives based on 35 Ill. Adm. Code
CHOXD
CHOXD
399
721.122(a)(2)
CHRED
INCIN
STABL
CHRED
INCIN
D003 Water Reactives based on 35 Ill. Adm. Code
721.123(a)(2), (3) and (4)
INCIN
WTRRX
CHOXD
CHRED
n.a.
D003 Reactive Sulfides based on 35 Ill. Adm. Code
721.123(a)(5)
CHOXD
CHRED
INCIN
STABL
CHOXD
CHRED
BIODG
INCIN
D003 Explosives based on 35 Ill. Adm. Code
721.123(a) (6), (7) and
INCIN
CHOXD
CHRED
INCIN
CHOXD
CHRED
BIODG
CARBN
D003 Other Reactives based on 35 Ill. Adm. Code
721.123(a)(1)
INCIN
CHOXD
CHRED
INCIN
CHOXD
CHRED
BIODG
CARBN
K044 Wastewater treatment sludges from the
manufacturing and processing of explosives
CHOXD
CHRED
INCIN
CHOXD
CHRED
BIODG
CARBN
INCIN
K045 Spent carbon from the treatment of wastewaters
containing explosives
CHOXD
CHRED
INCIN
CHOXD
CHRED
BIODG
CARBN
INCIN
K047 Pink/red water from TNT operations
CHOXD
CHRED
INCIN
CHOXD
CHRED
BIODG
CARBN
INCIN
Note: “n.a.” stands for “not applicable”.
400
“fb.” Stands for “followed by”.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix G
Federal Effective Dates
The following are the effective dates for the USEPA rules in 40 CFR 268. These generally became
effective as Illinois rules at a later date.
TABLE 1
EFFECTIVE DATES OF SURFACE DISPOSED WASTES (NON-SOIL AND
DEBRIS) REGULATED IN THE LDRS (A)
a
—COMPREHENSIVE LIST
Waste code
Waste category
Effective date
California list
Liquid hazardous wastes, including free liquids
associated with solid or sludge, containing free
cyanides at concentrations greater than or equal
to 1,000 mg/l or certain metals or compounds of
these metals greater than or equal to the
prohibition levels
July 8, 1987.
California list
Liquid (aqueous) hazardous wastes having a pH
less than or equal to 2
July 8, 1987.
California list
Dilute HOC wastewaters, defined as HOC-waste
mixtures that are primarily water and that contain
greater than or equal to 1,000 mg /l but less than
10,000 mg/l
July 8, 1987.
California list
Liquid hazardous waste containing PCBs greater
than or equal to 50 ppm
July 8, 1987.
California list
Other liquid and nonliquid hazardous wastes
containing HOCs in total concentration greater
than or equal to 1,000 mg
Nov. 8, 1988.
D001
c
All (except High TOC Ignitable Liquids)
Aug. 8, 1990
Aug. 9, 1993.
D001
High TOC Ignitable Liquids
Aug. 8, 1990.
D002
c
All
Aug. 8, 1990
Aug. 9, 1993.
D003
e
All
Aug. 8, 1990
July 8, 1996.
D004
Wastewater
Aug. 8, 1990.
D004
Nonwastewater
May 8, 1992.
D004
Wastewater
Aug. 8, 1992.
D005
All
Aug. 8, 1990.
D006
All
Aug. 8, 1990.
D007
All
Aug. 8, 1990.
401
D008
Lead materials before secondary smelting
May 8, 1992.
D008
All others
Aug. 8, 1990.
D009
Nonwastewater
May 8, 1992.
D009
All others
Aug. 8, 1990.
D010
All
Aug. 8, 1990.
D011
All
Aug. 8, 1990.
D012 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D013 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D014 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D015 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D016 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D017 (that exhibit the toxicity
characteristic based on the
TCLP)
d
All
Aug. 8, 1990
Dec. 14, 1994.
D018
Mixed with radioactive wastes
Sep. 19, 1996.
D018
All others
Dec. 19, 1994.
D019
Mixed with radioactive wastes
Sep. 19, 1996.
D019
All others
Dec. 19, 1994.
D020
Mixed with radioactive wastes
Sep. 19, 1996.
D020
All others
Dec. 19, 1994.
D021
Mixed with radioactive wastes
Sep. 19, 1996.
D021
All others
Dec. 19, 1994.
D022
Mixed with radioactive wastes
Sep. 19, 1996.
D022
All others
Dec. 19, 1994.
D023
Mixed with radioactive wastes
Sep. 19, 1996.
D023
All others
Dec. 19, 1994.
D024
Mixed with radioactive wastes
Sep. 19, 1996.
D024
All others
Dec. 19, 1994.
D025
Mixed with radioactive wastes
Sep. 19, 1996.
D025
All others
Dec. 19, 1994.
D026
Mixed with radioactive wastes
Sep. 19, 1996.
D026
All others
Dec. 19, 1994.
D027
Mixed with radioactive wastes
Sep. 19, 1996.
D027
All others
Dec. 19, 1994.
D028
Mixed with radioactive wastes
Sep. 19, 1996.
402
D028
All others
Dec. 19, 1994.
D029
Mixed with radioactive wastes
Sep. 19, 1996.
D029
All others
Dec. 19, 1994.
D030
Mixed with radioactive wastes
Sep. 19, 1996.
D030
All others
Dec. 19, 1994.
D031
Mixed with radioactive wastes
Sep. 19, 1996.
D031
All others
Dec. 19, 1994.
D032
Mixed with radioactive wastes
Sep. 19, 1996.
D032
All others
Dec. 19, 1994.
D033
Mixed with radioactive wastes
Sep. 19, 1996.
D033
All others
Dec. 19, 1994.
D034
Mixed with radioactive wastes
Sep. 19, 1996.
D034
All others
Dec. 19, 1994.
D035
Mixed with radioactive wastes
Sep. 19, 1996.
D035
All others
Dec. 19, 1994.
D036
Mixed with radioactive wastes
Sep. 19, 1996.
D036
All others
Dec. 19, 1994.
D037
Mixed with radioactive wastes
Sep. 19, 1996.
D037
All others
Dec. 19, 1994.
D038
Mixed with radioactive wastes
Sep. 19, 1996.
D038
All others
Dec. 19, 1994.
D039
Mixed with radioactive wastes
Sep. 19, 1996.
D039
All others
Dec. 19, 1994.
D040
Mixed with radioactive wastes
Sep. 19, 1996.
D040
All others
Dec. 19, 1994.
D041
Mixed with radioactive wastes
Sep. 19, 1996.
D041
All others
Dec. 19, 1994.
D042
Mixed with radioactive wastes
Sep. 19, 1996.
D042
All others
Dec. 19, 1994.
D043
Mixed with radioactive wastes
Sep. 19, 1996.
D043
All others
Dec. 19, 1994.
F001
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F001
All others
Nov. 8, 1986.
F002 (1,1,2- trichloroethane)
Wastewater and Nonwastewater
Aug. 8, 1990.
F002
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F002
All others
Nov. 8, 1986.
F003
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
Nov. 8, 1988.
403
containing sludges and solids
F003
All others
Nov. 8, 1986.
F004
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F004
All others
Nov. 8, 1986.
F005 (benzene, 2-ethoxy
ethanol, 2-nitropropane)
Wastewater and Nonwastewater
Aug. 8, 1990.
F005
Small quantity generators, CERCLA
response/RCRA corrective action, initial
generator’s solvent-water mixtures, solvent-
containing sludges and solids
Nov. 8, 1988.
F005
All others
Nov. 8, 1986.
F006
Wastewater
Aug. 8, 1990.
F006
Nonwastewater
Aug. 8, 1988.
F006 (cyanides)
Nonwastewater
July 8, 1989.
F007
All
July 8, 1989.
F008
All
July 8, 1989.
F009
All
July 8, 1989.
F010
All
June 8, 1989.
F011 (cyanides)
Nonwastewater
Dec. 8, 1989.
F011
All others
July 8, 1989.
F012 (cyanides)
Nonwastewater
Dec. 8, 1989.
F012
All others
July 8, 1989.
F019
All
Aug. 8, 1990.
F020
All
Nov. 8, 1988.
F021
All
Nov. 8, 1988.
F022
All
Nov. 8, 1988.
F023
All
Nov. 8, 1988.
F024 (metals)
Wastewater
June 8, 1989.
F024 (metals)
Nonwastewater
Aug. 8, 1990.
F024 B
All others
June 8, 1989.
F025
All
Aug. 8, 1990.
F026
All
Nov. 8, 1988.
F027
All
Nov. 8, 1988.
F028
All
Nov. 8, 1988.
F032
Mixed with radioactive wastes
May 12, 1999.
F032
All others
May 12, 1997.
F033
Mixed with radioactive wastes
May 12, 1999.
F033
All others
May 12, 1997.
F034
Mixed with radioactive wastes
May 12, 1999.
F034
All others
May 12, 1997.
F037
Not generated from surface impoundment
cleanouts or closures
June 30, 1993.
404
F037
Generated from surface impoundment
cleanouts or closures
June 30, 1994.
F037
Mixed with radioactive wastes
June 30, 1994.
F038
Not generated from surface impoundment
cleanouts or closures
June 30, 1993.
F038
Generated from surface impoundment
cleanouts or closures
June 30, 1994.
F038
Mixed with radioactive wastes
June 30, 1994.
F039
Wastewater
Aug. 8, 1990.
F039
Nonwastewater
May 8, 1992.
K001 (organics)
b
B
All
Aug. 8, 1988.
K001
All others
Aug. 8, 1988.
K002
All
Aug. 8, 1990.
K003
All
Aug. 8, 1990.
K004
Wastewater
Aug. 8, 1990.
K004 C
Nonwastewater
Aug. 8, 1988.
K005
Wastewater
Aug. 8, 1990.
K005 C
Nonwastewater
June 8, 1989.
K006
All
Aug. 8, 1990.
K007
Wastewater
Aug. 8, 1990.
K007 C
Nonwastewater
June 8, 1989.
K008
Wastewater
Aug. 8, 1990.
K008 C
Nonwastewater
Aug. 8, 1988.
K009
All
June 8, 1989.
K010
All
June 8, 1989.
K011
Wastewater
Aug. 8, 1990.
K011
Nonwastewater
June 8, 1989.
K013
Wastewater
Aug. 8, 1990.
K013
Nonwastewater
June 8, 1989.
K014
Wastewater
Aug. 8, 1990.
K014
Nonwastewater
June 8, 1989.
K015
Wastewater
Aug. 8, 1988.
K015
Nonwastewater
Aug. 8, 1990.
K016
All
Aug. 8, 1988.
K017
All
Aug. 8, 1990.
K018
All
Aug. 8, 1988.
K019
All
Aug. 8, 1988.
K020
All
Aug. 8, 1988.
K021
Wastewater
Aug. 8, 1990.
K021 C
Nonwastewater
Aug. 8, 1988.
K022
Wastewater
Aug. 8, 1990.
K022
Nonwastewater
Aug. 8, 1988.
K023
All
June 8, 1989.
K024
All
Aug. 8, 1988.
K025
Wastewater
Aug. 8, 1990.
405
K025 C
Nonwastewater
Aug. 8, 1988.
K026
All
Aug. 8, 1990.
K027
All
June 8, 1989.
K028 (metals)
Nonwastewater
Aug. 8, 1990.
K028
All others
June 8, 1989.
K029
Wastewater
Aug. 8, 1990.
K029
Nonwastewater
June 8, 1989.
K030
All
Aug. 8, 1988.
K031
Wastewater
Aug. 8, 1990.
K031
Nonwastewater
May 8, 1992.
K032
All
Aug. 8, 1990.
K033
All
Aug. 8, 1990.
K034
All
Aug. 8, 1990.
K035
All
Aug. 8, 1990.
K036
Wastewater
June 8, 1989.
K036 C
Nonwastewater
Aug. 8, 1988.
K037
b
B
Wastewater
Aug. 8, 1988.
K037
Nonwastewater
Aug. 8, 1988.
K038
All
June 8, 1989.
K039
All
June 8, 1989.
K040
All
June 8, 1989.
K041
All
Aug. 8, 1990.
K042
All
Aug. 8, 1990.
K043
All
June 8, 1989.
K044 C
All
Aug. 8, 1988.
K045 C
All
Aug. 8, 1988.
K046 (Nonreactive)
Nonwastewater
Aug. 8, 1988.
K046
All others
Aug. 8, 1990.
K047 C
All
Aug. 8, 1988.
K048
Wastewater
Aug. 8, 1990.
K048
Nonwastewater
Nov. 8, 1990.
K049
Wastewater
Aug. 8, 1990.
K049
Nonwastewater
Nov. 8, 1990.
K050
Wastewater
Aug. 8, 1990.
K050
Nonwastewater
Nov. 8, 1990.
K051
Wastewater
Aug. 8, 1990.
K051
Nonwastewater
Nov. 8, 1990.
K052
Wastewater
Aug. 8, 1990.
K052
Nonwastewater
Nov. 8, 1990.
K060
Wastewater
Aug. 8, 1990.
K060 C
Nonwastewater
Aug. 8, 1988.
K061
Wastewater
Aug. 8, 1990.
K061 (low zinc) (interim
standard for high zinc remains
in effect until August 7,
Nonwastewater
Aug. 8, 1988
June 30, 1992.
406
1991).
K062
All
Aug. 8, 1988.
K069 (Non-Calcium Sulfate)
C
Nonwastewater
Aug. 8, 1988.
K069
All others
Aug. 8, 1990.
K071
All
Aug. 8, 1990.
K073
All
Aug. 8, 1990.
K083
All
Aug. 8, 1990.
K084
Wastewater
Aug. 8, 1990.
K084
Nonwastewater
May 8, 1992.
K085
All
Aug. 8, 1990.
K086 (organics)
b
B
All
Aug. 8, 1988.
K086
All others
Aug. 8, 1988.
K087
All
Aug. 8, 1988.
K088
Mixed with radioactive wastes
Apr. 8, 1998.
K088
All others
Jan. 8, 1997.
K093
All
June 8, 1989.
K094
All
June 8, 1989.
K095
Wastewater
Aug. 8, 1990.
K095
Nonwastewater
June 8, 1989.
K096
Wastewater
Aug. 8, 1990.
K096
Nonwastewater
June 8, 1989.
K097
All
Aug. 8, 1990.
K098
All
Aug. 8, 1990.
K099
All
Aug. 8, 1988.
K100
Wastewater
Aug. 8, 1990.
K100 C
Nonwastewater
Aug. 8, 1988.
K101 (organics)
Wastewater
Aug. 8, 1988.
K101 (metals)
Wastewater
Aug. 8, 1990.
K101 (organics)
Nonwastewater
Aug. 8, 1988.
K101 (metals)
Nonwastewater
May 8, 1992.
K102 (organics)
Wastewater
Aug. 8, 1988.
K102 (metals)
Wastewater
Aug. 8, 1990.
K102 (organics)
Nonwastewater
Aug. 8, 1988.
K102 (metals)
Nonwastewater
May 8, 1992.
K103
All
Aug. 8, 1988.
K104
All
Aug. 8, 1988.
K105
All
Aug. 8, 1990.
K106
Wastewater
Aug. 8, 1990.
K106
Nonwastewater
May 8, 1992.
K107
Mixed with radioactive wastes
June 30, 1994.
K107
All others
Nov. 9, 1992.
K108
Mixed with radioactive wastes
June 30, 1994.
K108
All others
Nov. 9, 1992.
K109
Mixed with radioactive wastes
June 30, 1994.
407
K109
All others
Nov. 9, 1992.
K110
Mixed with radioactive wastes
June 30, 1994.
K110
All others
Nov. 9, 1992.
K111
Mixed with radioactive wastes
June 30, 1994.
K111
All others
Nov. 9, 1992.
K112
Mixed with radioactive wastes
June 30, 1994.
K112
All others
Nov. 9, 1992.
K113
All
June 8, 1989.
K114
All
June 8, 1989.
K115
All
June 8, 1989.
K116
All
June 8, 1989.
K117
Mixed with radioactive wastes
June 30, 1994.
K117
All others
Nov. 9, 1992.
K118
Mixed with radioactive wastes
June 30, 1994.
K118
All others
Nov. 9, 1992.
K123
Mixed with radioactive wastes
June 30, 1994.
K123
All others
Nov. 9, 1992.
K124
Mixed with radioactive wastes
June 30, 1994.
K124
All others
Nov. 9, 1992.
K125
Mixed with radioactive wastes
June 30, 1994.
K125
All others
Nov. 9, 1992.
K126
Mixed with radioactive wastes
June 30, 1994.
K126
All others
Nov. 9, 1992.
K131
Mixed with radioactive wastes
June 30, 1994.
K131
All others
Nov. 9, 1992.
K132
Mixed with radioactive wastes
June 30, 1994.
K132
All others
Nov. 9, 1992.
K136
Mixed with radioactive wastes
June 30, 1994.
K136
All others
Nov. 9, 1992.
K141
Mixed with radioactive wastes
Sep. 19, 1996.
K141
All others
Dec. 19, 1994.
K142
Mixed with radioactive wastes
Sep. 19, 1996.
K142
All others
Dec. 19, 1994.
K143
Mixed with radioactive wastes
Sep. 19, 1996.
K143
All others
Dec. 19, 1994.
K144
Mixed with radioactive wastes
Sep. 19, 1996.
K144
All others
Dec. 19, 1994.
K145
Mixed with radioactive wastes
Sep. 19, 1996.
K145
All others
Dec. 19, 1994.
K147
Mixed with radioactive wastes
Sep. 19, 1996.
K147
All others
Dec. 19, 1994.
K148
Mixed with radioactive wastes
Sep. 19, 1996.
K148
All others
Dec. 19, 1994.
K149
Mixed with radioactive wastes
Sep. 19, 1996.
K149
All others
Dec. 19, 1994.
408
K150
Mixed with radioactive wastes
Sep. 19, 1996.
K150
All others
Dec. 19, 1994.
K151
Mixed with radioactive wastes
Sep. 19, 1996.
K151
All others
Dec. 19, 1994.
K156
Mixed with radioactive wastes
Apr. 8, 1998.
K156
All others
July 8, 1996.
K157
Mixed with radioactive wastes
Apr. 8, 1998.
K157
All others
July 8, 1996.
K158
Mixed with radioactive wastes
Apr. 8, 1998.
K158
All others
July 8, 1996.
K159
Mixed with radioactive wastes
Apr. 8, 1998.
K159
All others
July 8, 1996.
K160
Mixed with radioactive wastes
Apr. 8, 1998.
K160
All others
July 8, 1996.
K161
Mixed with radioactive wastes
Apr. 8, 1998.
K161
All others
July 8, 1996.
P001
All
Aug. 8, 1990.
P002
All
Aug. 8, 1990.
P003
All
Aug. 8, 1990.
P004
All
Aug. 8, 1990.
P005
All
Aug. 8, 1990.
P006
All
Aug. 8, 1990.
P007
All
Aug. 8, 1990.
P008
All
Aug. 8, 1990.
P009
All
Aug. 8, 1990.
P010
Wastewater
Aug. 8, 1990.
P010
Nonwastewater
May 8, 1992.
P011
Wastewater
Aug. 8, 1990.
P011
Nonwastewater
May 8, 1992.
P012
Wastewater
Aug. 8, 1990.
P012
Nonwastewater
May 8, 1992.
P013 (barium)
Nonwastewater
Aug. 8, 1990.
P013
All others
June 8, 1989.
P014
All
Aug. 8, 1990.
P015
All
Aug. 8, 1990.
P016
All
Aug. 8, 1990.
P017
All
Aug. 8, 1990.
P018
All
Aug. 8, 1990.
P020
All
Aug. 8, 1990.
P021
All
June 8, 1989.
P022
All
Aug. 8, 1990.
P023
All
Aug. 8, 1990.
P024
All
Aug. 8, 1990.
P026
All
Aug. 8, 1990.
P027
All
Aug. 8, 1990.
409
P028
All
Aug. 8, 1990.
P029
All
June 8, 1989.
P030
All
June 8, 1989.
P031
All
Aug. 8, 1990.
P033
All
Aug. 8, 1990.
P034
All
Aug. 8, 1990.
P036
Wastewater
Aug. 8, 1990.
P036
Nonwastewater
May 8, 1992.
P037
All
Aug. 8, 1990.
P038
Wastewater
Aug. 8, 1990.
P038
Nonwastewater
May 8, 1992.
P039
All
June 8, 1989.
P040
All
June 8, 1989.
P041
All
June 8, 1989.
P042
All
Aug. 8, 1990.
P043
All
June 8, 1989.
P044
All
June 8, 1989.
P045
All
Aug. 8, 1990.
P046
All
Aug. 8, 1990.
P047
All
Aug. 8, 1990.
P048
All
Aug. 8, 1990.
P049
All
Aug. 8, 1990.
P050
All
Aug. 8, 1990.
P051
All
Aug. 8, 1990.
P054
All
Aug. 8, 1990.
P056
All
Aug. 8, 1990.
P057
All
Aug. 8, 1990.
P058
All
Aug. 8, 1990.
P059
All
Aug. 8, 1990.
P060
All
Aug. 8, 1990.
P062
All
June 8, 1989.
P063
All
June 8, 1989.
P064
All
Aug. 8, 1990.
P065
Wastewater
Aug. 8, 1990.
P065
Nonwastewater
May 8, 1992.
P066
All
Aug. 8, 1990.
P067
All
Aug. 8, 1990.
P068
All
Aug. 8, 1990.
P069
All
Aug. 8, 1990.
P070
All
Aug. 8, 1990.
P071
All
June 8, 1989.
P072
All
Aug. 8, 1990.
P073
All
Aug. 8, 1990.
P074
All
June 8, 1989.
P075
All
Aug. 8, 1990.
410
P076
All
Aug. 8, 1990.
P077
All
Aug. 8, 1990.
P078
All
Aug. 8, 1990.
P081
All
Aug. 8, 1990.
P082
All
Aug. 8, 1990.
P084
All
Aug. 8, 1990.
P085
All
June 8, 1989.
P087
All
May 8, 1992.
P088
All
Aug. 8, 1990.
P089
All
June 8, 1989.
P092
Wastewater
Aug. 8, 1990.
P092
Nonwastewater
May 8, 1992.
P093
All
Aug. 8, 1990.
P094
All
June 8, 1989.
P095
All
Aug. 8, 1990.
P096
All
Aug. 8, 1990.
P097
All
June 8, 1989.
P098
All
June 8, 1989.
P099 (silver)
Wastewater
Aug. 8, 1990.
P099
All others
June 8, 1989.
P101
All
Aug. 8, 1990.
P102
All
Aug. 8, 1990.
P103
All
Aug. 8, 1990.
P104 (silver)
Wastewater
Aug. 8, 1990.
P104
All others
June 8, 1989.
P105
All
Aug. 8, 1990.
P106
All
June 8, 1989.
P108
All
Aug. 8, 1990.
P109
All
June 8, 1989.
P110
All
Aug. 8, 1990.
P111
All
June 8, 1989.
P112
All
Aug. 8, 1990.
P113
All
Aug. 8, 1990.
P114
All
Aug. 8, 1990.
P115
All
Aug. 8, 1990.
P116
All
Aug. 8, 1990.
P118
All
Aug. 8, 1990.
P119
All
Aug. 8, 1990.
P120
All
Aug. 8, 1990.
P121
All
June 8, 1989.
P122
All
Aug. 8, 1990.
P123
All
Aug. 8, 1990.
P127
Mixed with radioactive wastes
Apr. 8, 1998.
P127
All others
July 8, 1996.
P128
Mixed with radioactive wastes
Apr. 8, 1998.
411
P128
All others
July 8, 1996.
P185
Mixed with radioactive wastes
Apr. 8, 1998.
P185
All others
July 8, 1996.
P188
Mixed with radioactive wastes
Apr. 8, 1998.
P188
All others
July 8, 1996.
P189
Mixed with radioactive wastes
Apr. 8, 1998.
P189
All others
July 8, 1996.
P190
Mixed with radioactive wastes
Apr. 8, 1998.
P190
All others
July 8, 1996.
P191
Mixed with radioactive wastes
Apr. 8, 1998.
P191
All others
July 8, 1996.
P192
Mixed with radioactive wastes
Apr. 8, 1998.
P192
All others
July 8, 1996.
P194
Mixed with radioactive wastes
Apr. 8, 1998.
P194
All others
July 8, 1996.
P196
Mixed with radioactive wastes
Apr. 8, 1998.
P196
All others
July 8, 1996.
P197
Mixed with radioactive wastes
Apr. 8, 1998.
P197
All others
July 8, 1996.
P198
Mixed with radioactive wastes
Apr. 8, 1998.
P198
All others
July 8, 1996.
P199
Mixed with radioactive wastes
Apr. 8, 1998.
P199
All others
July 8, 1996.
P201
Mixed with radioactive wastes
Apr. 8, 1998.
P201
All others
July 8, 1996.
P202
Mixed with radioactive wastes
Apr. 8, 1998.
P202
All others
July 8, 1996.
P203
Mixed with radioactive wastes
Apr. 8, 1998.
P203
All others
July 8, 1996.
P204
Mixed with radioactive wastes
Apr. 8, 1998.
P204
All others
July 8, 1996.
P205
Mixed with radioactive wastes
Apr. 8, 1998.
P205
All others
July 8, 1996.
U001
All
Aug. 8, 1990.
U002
All
Aug. 8, 1990.
U003
All
Aug. 8, 1990.
U004
All
Aug. 8, 1990.
U005
All
Aug. 8, 1990.
U006
All
Aug. 8, 1990.
U007
All
Aug. 8, 1990.
U008
All
Aug. 8, 1990.
U009
All
Aug. 8, 1990.
U010
All
Aug. 8, 1990.
U011
All
Aug. 8, 1990.
U012
All
Aug. 8, 1990.
412
U014
All
Aug. 8, 1990.
U015
All
Aug. 8, 1990.
U016
All
Aug. 8, 1990.
U017
All
Aug. 8, 1990.
U018
All
Aug. 8, 1990.
U019
All
Aug. 8, 1990.
U020
All
Aug. 8, 1990.
U021
All
Aug. 8, 1990.
U022
All
Aug. 8, 1990.
U023
All
Aug. 8, 1990.
U024
All
Aug. 8, 1990.
U025
All
Aug. 8, 1990.
U026
All
Aug. 8, 1990.
U027
All
Aug. 8, 1990.
U028
All
June 8, 1989.
U029
All
Aug. 8, 1990.
U030
All
Aug. 8, 1990.
U031
All
Aug. 8, 1990.
U032
All
Aug. 8, 1990.
U033
All
Aug. 8, 1990.
U034
All
Aug. 8, 1990.
U035
All
Aug. 8, 1990.
U036
All
Aug. 8, 1990.
U037
All
Aug. 8, 1990.
U038
All
Aug. 8, 1990.
U039
All
Aug. 8, 1990.
U041
All
Aug. 8, 1990.
U042
All
Aug. 8, 1990.
U043
All
Aug. 8, 1990.
U044
All
Aug. 8, 1990.
U045
All
Aug. 8, 1990.
U046
All
Aug. 8, 1990.
U047
All
Aug. 8, 1990.
U048
All
Aug. 8, 1990.
U049
All
Aug. 8, 1990.
U050
All
Aug. 8, 1990.
U051
All
Aug. 8, 1990.
U052
All
Aug. 8, 1990.
U053
All
Aug. 8, 1990.
U055
All
Aug. 8, 1990.
U056
All
Aug. 8, 1990.
U057
All
Aug. 8, 1990.
U058
All
June 8, 1989.
U059
All
Aug. 8, 1990.
U060
All
Aug. 8, 1990.
413
U061
All
Aug. 8, 1990.
U062
All
Aug. 8, 1990.
U063
All
Aug. 8, 1990.
U064
All
Aug. 8, 1990.
U066
All
Aug. 8, 1990.
U067
All
Aug. 8, 1990.
U068
All
Aug. 8, 1990.
U069
All
June 8, 1989
June 30, 1992.
U070
All
Aug. 8, 1990.
U071
All
Aug. 8, 1990.
U072
All
Aug. 8, 1990.
U073
All
Aug. 8, 1990.
U074
All
Aug. 8, 1990.
U075
All
Aug. 8, 1990.
U076
All
Aug. 8, 1990.
U077
All
Aug. 8, 1990.
U078
All
Aug. 8, 1990.
U079
All
Aug. 8, 1990.
U080
All
Aug. 8, 1990.
U081
All
Aug. 8, 1990.
U082
All
Aug. 8, 1990.
U083
All
Aug. 8, 1990.
U084
All
Aug. 8, 1990.
U085
All
Aug. 8, 1990.
U086
All
Aug. 8, 1990.
U087
All
June 8, 1989.
U088
All
June 8, 1989.
U089
All
Aug. 8, 1990.
U090
All
Aug. 8, 1990.
U091
All
Aug. 8, 1990.
U092
All
Aug. 8, 1990.
U093
All
Aug. 8, 1990.
U094
All
Aug. 8, 1990.
U095
All
Aug. 8, 1990.
U096
All
Aug. 8, 1990.
U097
All
Aug. 8, 1990.
U098
All
Aug. 8, 1990.
U099
All
Aug. 8, 1990.
U101
All
Aug. 8, 1990.
U102
All
June 8, 1989.
U103
All
Aug. 8, 1990.
U105
All
Aug. 8, 1990.
U106
All
Aug. 8, 1990.
U107
All
June 8, 1989.
414
U108
All
Aug. 8, 1990.
U109
All
Aug. 8, 1990.
U110
All
Aug. 8, 1990.
U111
All
Aug. 8, 1990.
U112
All
Aug. 8, 1990.
U113
All
Aug. 8, 1990.
U114
All
Aug. 8, 1990.
U115
All
Aug. 8, 1990.
U116
All
Aug. 8, 1990.
U117
All
Aug. 8, 1990.
U118
All
Aug. 8, 1990.
U119
All
Aug. 8, 1990.
U120
All
Aug. 8, 1990.
U121
All
Aug. 8, 1990.
U122
All
Aug. 8, 1990.
U123
All
Aug. 8, 1990.
U124
All
Aug. 8, 1990.
U125
All
Aug. 8, 1990.
U126
All
Aug. 8, 1990.
U127
All
Aug. 8, 1990.
U128
All
Aug. 8, 1990.
U129
All
Aug. 8, 1990.
U130
All
Aug. 8, 1990.
U131
All
Aug. 8, 1990.
U132
All
Aug. 8, 1990.
U133
All
Aug. 8, 1990.
U134
All
Aug. 8, 1990.
U135
All
Aug. 8, 1990.
U136
Wastewater
Aug. 8, 1990.
U136
Nonwastewater
May 8, 1992.
U137
All
Aug. 8, 1990.
U138
All
Aug. 8, 1990.
U140
All
Aug. 8, 1990.
U141
All
Aug. 8, 1990.
U142
All
Aug. 8, 1990.
U143
All
Aug. 8, 1990.
U144
All
Aug. 8, 1990.
U145
All
Aug. 8, 1990.
U146
All
Aug. 8, 1990.
U147
All
Aug. 8, 1990.
U148
All
Aug. 8, 1990.
U149
All
Aug. 8, 1990.
U150
All
Aug. 8, 1990.
U151
Wastewater
Aug. 8, 1990.
U151
Nonwastewater
May 8, 1992.
415
U152
All
Aug. 8, 1990.
U153
All
Aug. 8, 1990.
U154
All
Aug. 8, 1990.
U155
All
Aug. 8, 1990.
U156
All
Aug. 8, 1990.
U157
All
Aug. 8, 1990.
U158
All
Aug. 8, 1990.
U159
All
Aug. 8, 1990.
U160
All
Aug. 8, 1990.
U161
All
Aug. 8, 1990.
U162
All
Aug. 8, 1990.
U163
All
Aug. 8, 1990.
U164
All
Aug. 8, 1990.
U165
All
Aug. 8, 1990.
U166
All
Aug. 8, 1990.
U167
All
Aug. 8, 1990.
U168
All
Aug. 8, 1990.
U169
All
Aug. 8, 1990.
U170
All
Aug. 8, 1990.
U171
All
Aug. 8, 1990.
U172
All
Aug. 8, 1990.
U173
All
Aug. 8, 1990.
U174
All
Aug. 8, 1990.
U176
All
Aug. 8, 1990.
U177
All
Aug. 8, 1990.
U178
All
Aug. 8, 1990.
U179
All
Aug. 8, 1990.
U180
All
Aug. 8, 1990.
U181
All
Aug. 8, 1990.
U182
All
Aug. 8, 1990.
U183
All
Aug. 8, 1990.
U184
All
Aug. 8, 1990.
U185
All
Aug. 8, 1990.
U186
All
Aug. 8, 1990.
U187
All
Aug. 8, 1990.
U188
All
Aug. 8, 1990.
U189
All
Aug. 8, 1990.
U190
All
June 8, 1989.
U191
All
Aug. 8, 1990.
U192
All
Aug. 8, 1990.
U193
All
Aug. 8, 1990.
U194
All
Aug. 8, 1990
June 8, 1989.
U196
All
Aug. 8, 1990.
U197
All
Aug. 8, 1990.
416
U200
All
Aug. 8, 1990.
U201
All
Aug. 8, 1990.
U202
All
Aug. 8, 1990.
U203
All
Aug. 8, 1990.
U204
All
Aug. 8, 1990.
U205
All
Aug. 8, 1990.
U206
All
Aug. 8, 1990.
U207
All
Aug. 8, 1990.
U208
All
Aug. 8, 1990.
U209
All
Aug. 8, 1990.
U210
All
Aug. 8, 1990.
U211
All
Aug. 8, 1990.
U213
All
Aug. 8, 1990.
U214
All
Aug. 8, 1990.
U215
All
Aug. 8, 1990.
U216
All
Aug. 8, 1990.
U217
All
Aug. 8, 1990.
U218
All
Aug. 8, 1990.
U219
All
Aug. 8, 1990.
U220
All
Aug. 8, 1990.
U221
All
June 8, 1989.
U222
All
Aug. 8, 1990.
U223
All
June 8, 1989.
U225
All
Aug. 8, 1990.
U226
All
Aug. 8, 1990.
U227
All
Aug. 8, 1990.
U228
All
Aug. 8, 1990.
U234
All
Aug. 8, 1990.
U235
All
June 8, 1989.
U236
All
Aug. 8, 1990.
U237
All
Aug. 8, 1990.
U238
All
Aug. 8, 1990.
U239
All
Aug. 8, 1990.
U240
All
Aug. 8, 1990.
U243
All
Aug. 8, 1990.
U244
All
Aug. 8, 1990.
U246
All
Aug. 8, 1990.
U247
All
Aug. 8, 1990.
U248
All
Aug. 8, 1990.
U249
All
Aug. 8, 1990.
U271
Mixed with radioactive wastes
Apr. 8, 1998.
U271
All others
July 8, 1996.
U277
Mixed with radioactive wastes
Apr. 8, 1998.
U277
All others
July 8, 1996.
U278
Mixed with radioactive wastes
Apr. 8, 1998.
417
U278
All others
July 8, 1996.
U279
Mixed with radioactive wastes
Apr. 8, 1998.
U279
All others
July 8, 1996.
U280
Mixed with radioactive wastes
Apr. 8, 1998.
U280
All others
July 8, 1996.
U328
Mixed with radioactive wastes
June 30, 1994.
U328
All others
Nov. 9, 1992.
U353
Mixed with radioactive wastes
June 30, 1994.
U353
All others
Nov. 9, 1992.
U359
Mixed with radioactive wastes
June 30, 1994.
U359
All others
Nov. 9, 1992.
U364
Mixed with radioactive wastes
Apr. 8, 1998.
U364
All others
July 8, 1996.
U365
Mixed with radioactive wastes
Apr. 8, 1998.
U365
All others
July 8, 1996.
U366
Mixed with radioactive wastes
Apr. 8, 1998.
U366
All others
July 8, 1996.
U367
Mixed with radioactive wastes
Apr. 8, 1998.
U367
All others
July 8, 1996.
U372
Mixed with radioactive wastes
Apr. 8, 1998.
U372
All others
July 8, 1996.
U373
Mixed with radioactive wastes
Apr. 8, 1998.
U373
All others
July 8, 1996.
U375
Mixed with radioactive wastes
Apr. 8, 1998.
U375
All others
July 8, 1996.
U376
Mixed with radioactive wastes
Apr. 8, 1998.
U376
All others
July 8, 1996.
U377
Mixed with radioactive wastes
Apr. 8, 1998.
U377
All others
July 8, 1996.
U378
Mixed with radioactive wastes
Apr. 8, 1998.
U378
All others
July 8, 1996.
U379
Mixed with radioactive wastes
Apr. 8, 1998.
U379
All others
July 8, 1996.
U381
Mixed with radioactive wastes
Apr. 8, 1998.
U381
All others
July 8, 1996.
U382
Mixed with radioactive wastes
Apr. 8, 1998.
U382
All others
July 8, 1996.
U383
Mixed with radioactive wastes
Apr. 8, 1998.
U383
All others
July 8, 1996.
U384
Mixed with radioactive wastes
Apr. 8, 1998.
U384
All others
July 8, 1996.
U385
Mixed with radioactive wastes
Apr. 8, 1998.
U385
All others
July 8, 1996.
U386
Mixed with radioactive wastes
Apr. 8, 1998.
U386
All others
July 8, 1996.
418
U387
Mixed with radioactive wastes
Apr. 8, 1998.
U387
All others
July 8, 1996.
U389
Mixed with radioactive wastes
Apr. 8, 1998.
U389
All others
July 8, 1996.
U390
Mixed with radioactive wastes
Apr. 8, 1998.
U390
All others
July 8, 1996.
U391
Mixed with radioactive wastes
Apr. 8, 1998.
U391
All others
July 8, 1996.
U392
Mixed with radioactive wastes
Apr. 8, 1998.
U392
All others
July 8, 1996.
U393
Mixed with radioactive wastes
Apr. 8, 1998.
U393
All others
July 8, 1996.
U394
Mixed with radioactive wastes
Apr. 8, 1998.
U394
All others
July 8, 1996.
U395
Mixed with radioactive wastes
Apr. 8, 1998.
U395
All others
July 8, 1996.
U396
Mixed with radioactive wastes
Apr. 8, 1998.
U396
All others
July 8, 1996.
U400
Mixed with radioactive wastes
Apr. 8, 1998.
U400
All others
July 8, 1996.
U401
Mixed with radioactive wastes
Apr. 8, 1998.
U401
All others
July 8, 1996.
U402
Mixed with radioactive wastes
Apr. 8, 1998.
U402
All others
July 8, 1996.
U403
Mixed with radioactive wastes
Apr. 8, 1998.
U403
All others
July 8, 1996.
U404
Mixed with radioactive wastes
Apr. 8, 1998.
U404
All others
July 8, 1996.
U407
Mixed with radioactive wastes
Apr. 8, 1998.
U407
All others
July 8, 1996.
U409
Mixed with radioactive wastes
Apr. 8, 1998.
U409
All others
July 8, 1996.
U410
Mixed with radioactive wastes
Apr. 8, 1998.
U410
All others
July 8, 1996.
U411
Mixed with radioactive wastes
Apr. 8, 1998.
U411
All others
July 8, 1996.
A
a
This table does not include mixed radioactive wastes (from the First, Second, and Third
rules) which are receiving a national capacity variance until May 8, 1992, for all
applicable treatment technologies. This table also does not include contaminated soil
and debris wastes.
B
b
The standard has been was revised in the Third Third Final Rule (adopted by USEPA at
55 Fed. Reg. 22520 (June 1, 1990) and by the Board in docket R90-11 by orders dated
April 11, May 23, and August 8 and 22, 1991).
419
C
c
No land disposal USEPA amended the standard has been revised in the Third Third
Final Emergency Rule (at 58 Fed. Reg. 29860 (May 24, 1993), which the Board
adopted in docket R93-16 on March 17, 1994); the original effective date was August
8, 1990.
d
The standard was revised in the Phase II Final Rule (which USEPA adopted at 59 Fed.
Reg. 47982 (Sept. 19, 1994) and the Board adopted in docket R95-6 by orders dated
June 1 and 15, 1995); the original effective date was August 8, 1990.
e
The standards for selected reactive wastes was revised in the Phase III Final Rule
(which USEPA adopted at 61 Fed. Reg. 15566 (Apr. 8, 1996) and the Board adopted
in docket R96-10/R97-3/R97-5 (consolidated) by an order dated November 6, 1997);
the original effective date was August 8, 1990.
TABLE 2
SUMMARY OF EFFECTIVE DATES OF LAND DISPOSAL
RESTRICTIONS FOR CONTAMINATED SOIL AND DEBRIS (CSD)
Restricted hazardous waste in CSD
Effective date
1.
Solvent-(F001-F005) and dioxin-(F020-F023 and F026-F028)
containing soil and debris from CERCLA response of RCRA
corrective actions.
Nov. 8, 1990.
2.
Soil and debris not from CERCLA response or RCRA corrective
actions contaminated with less than 1% one percent total
solvents (F001-F005) or dioxins (F020-F023 and F026-F028).
Nov. 8, 1988.
3. Soil and debris contaminated with California list HOCs from
CERCLA response or RCRA corrective actions.
Nov. 8, 1990.
4. Soil and debris contaminated with California list HOCs not from
CERCLA response or RCRA corrective actions.
July 8, 1989.
53. All soil and debris contaminated with First Third wastes for
which treatment standards are based on incineration.
Aug. 8, 1990.
64. All soil and debris contaminated with Second Third wastes for
which treatment standards are based on incineration.
June 8, 1991.
75. All soil and debris contaminated with Third Third wastes or,
First or Second Third “soft hammer” wastes which had
treatment standards promulgated in the Third Third rule, for
which treatment standards are based on incineration,
vitrification, or mercury retorting, acid leaching followed by
chemical precipitation, or thermal recovery of metals, as well as
all inorganic solids debris contaminated with D004-D011 wastes,
and all soil and debris contaminated with mixed
RCRA/radioactive wastes.
May 8, 1992.
6. Soil and debris contaminated with D012-D043, K141-K145,
and K147-151 wastes.
Dec. 19, 1994.
420
7. Debris (only) contaminated with F037, F038, K107-K112,
K117, K118, K123-K126, K131, K132, K136, U328, U353,
U359.
Dec. 19, 1994.
8.
Soil and debris contaminated with K156- K161, P127, P128,
P188-P192, P194, P196- P199, P201-P205, U271, U277-
U280, U364-U367, U372, U373, U375-U379, U381-U387,
U389-U396, U400-U404, U407, and U409-U411 wastes.
July 8, 1996.
9.
Soil and debris contaminated with K088 wastes.
Jan. 8, 1997.
10. Soil and debris contaminated with radioactive wastes mixed
with K088, K156-K161, P127, P128, P188-P192, P194,
P196-P199, P201-P205, U271, U277-U280, U364-
U367,U372, U373, U375-U379, U381-U387, U389-U396,
U400-U404, U407, and U409-U411 wastes.
April 8, 1998.
11. Soil and debris contaminated with F032, F034, and F035.
May 12, 1997.
BOARD NOTE: This table is provided for the convenience of the reader.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix H
National Capacity LDR Variances for UIC Wastes
See Note
a
Waste code
Waste category
Effective date
F001-F005
All spent F001-F005 solvent containing less than 1
percent total F001-F005 solvent constituents
Aug. 8, 1990.
California list
Liquid hazardous wastes, including free liquids
associated with any solid or sludge, containing free
cyanides at concentrations greater than or equal to
1,000 mg/l, or containing certain metals or
compounds of these metals greater than or equal to the
prohibition levels
Aug. 8, 1990.
California list
Liquid hazardous waste having a Ph less than or equal
to 2
Aug. 8, 1990.
California list
Hazardous wastes containing HOCs in total
concentrations less than 10,000 mg/l but greater than
or equal to 1,000 mg/l
Aug. 8, 1990.
D001 (except High
TOC Ignitable Liquids
Subcategory)
c
All
Feb. 10, 1994.
D001 (High TOC
Ignitable Characteristic
Liquids Subcategory)
Nonwastewater
Sep. 19, 1995.
D002
b
B
All
May 8, 1992.
D002
c
All
Feb. 10, 1994.
421
D003 (cyanides)
All
May 8, 1992.
D003 (sulfides)
All
May 8, 1992.
D003 (explosives,
reactives).
All
May 8, 1992.
D007
All
May 8, 1992.
D009
Nonwastewater
May 8, 1992.
D012
All
Sep. 19, 1995.
D013
All
Sep. 19, 1995.
D014
All
Sep. 19, 1995.
D015
All
Sep. 19, 1995.
D016
All
Sep. 19, 1995.
D017
All
Sep. 19, 1995.
D018
All, including mixed with radioactive wastes
Apr. 8, 1998.
D019
All, including mixed with radioactive wastes
Apr. 8, 1998.
D020
All, including mixed with radioactive wastes
Apr. 8, 1998.
D021
All, including mixed with radioactive wastes
Apr. 8, 1998.
D022
All, including mixed with radioactive wastes
Apr. 8, 1998.
D023
All, including mixed with radioactive wastes
Apr. 8, 1998.
D024
All, including mixed with radioactive wastes
Apr. 8, 1998.
D025
All, including mixed with radioactive wastes
Apr. 8, 1998.
D026
All, including mixed with radioactive wastes
Apr. 8, 1998.
D027
All, including mixed with radioactive wastes
Apr. 8, 1998.
D028
All, including mixed with radioactive wastes
Apr. 8, 1998.
D029
All, including mixed with radioactive wastes
Apr. 8, 1998.
D030
All, including mixed with radioactive wastes
Apr. 8, 1998.
D031
All, including mixed with radioactive wastes
Apr. 8, 1998.
D032
All, including mixed with radioactive wastes
Apr. 8, 1998.
D033
All, including mixed with radioactive wastes
Apr. 8, 1998.
D034
All, including mixed with radioactive wastes
Apr. 8, 1998.
D035
All, including mixed with radioactive wastes
Apr. 8, 1998.
D036
All, including mixed with radioactive wastes
Apr. 8, 1998.
D037
All, including mixed with radioactive wastes
Apr. 8, 1998.
D038
All, including mixed with radioactive wastes
Apr. 8, 1998.
D039
All, including mixed with radioactive wastes
Apr. 8, 1998.
D040
All, including mixed with radioactive wastes
Apr. 8, 1998.
D041
All, including mixed with radioactive wastes
Apr. 8, 1998.
D042
All, including mixed with radioactive wastes
Apr. 8, 1998.
D043
All, including mixed with radioactive wastes
Apr. 8, 1998.
F001-F005
All spent F001-F005 solvent containing less than 1
percent total F001-F005 solvent constituents
Aug. 8, 1990.
F007
All
June 8, 1991.
F032
All, including mixed with radioactive wastes
May 12, 1999.
F034
All, including mixed with radioactive wastes
May 12,1999.
F035
All, including mixed with radioactive wastes
May 12, 1999.
F037
All
Nov. 8, 1992.
422
F038
All
Nov. 8, 1992.
F039
Wastewater
May 8, 1992.
K009
Wastewater
June 8, 1991.
K011
Nonwastewater
June 8, 1991.
K011
Wastewater
May 8, 1992.
K013
Nonwastewater
June 8, 1991.
K013
Wastewater
May 8, 1992.
K014
All
May 8, 1992.
K016 (dilute)
All
June 8, 1991.
K049
All
Aug. 8, 1990.
K050
All
Aug. 8, 1990.
K051
All
Aug. 8, 1990.
K052
All
Aug. 8, 1990.
K062
All
Aug. 8, 1990.
K071
All
Aug. 8, 1990.
K088
All
Jan. 8, 1997.
K104
All
Aug. 8, 1990.
K107
All
Nov. 8, 1992.
K108
All
Nov. 9, 1992.
K109
All
Nov. 9, 1992.
K110
All
Nov. 9, 1992.
K111
All
Nov. 9, 1992.
K112
All
Nov. 9, 1992.
K117
All
June 30, 1995.
K118
All
June 30, 1995.
K123
All
Nov. 9, 1992.
K124
All
Nov. 9, 1992.
K125
All
Nov. 9, 1992.
K126
All
Nov. 9, 1992.
K131
All
June 30, 1995.
K132
All
June 30, 1995.
K136
All
Nov. 9, 1992.
K141
All
Dec. 19, 1994.
K142
All
Dec. 19, 1994.
K143
All
Dec. 19, 1994.
K144
All
Dec. 19, 1994.
K145
All
Dec. 19, 1994.
K147
All
Dec. 19, 1994.
K148
All
Dec. 19, 1994.
K149
All
Dec. 19, 1994.
K150
All
Dec. 19, 1994.
K151
All
Dec. 19, 1994.
K156
All
July 8, 1996.
K157
All
July 8, 1996.
K158
All
July 8, 1996.
423
K159
All
July 8, 1996.
K160
All
July 8, 1996.
K161
All
July 8, 1996.
P127
All
July 8, 1996.
P128
All
July 8, 1996.
P185
All
July 8, 1996.
P188
All
July 8, 1996.
P189
All
July 8, 1996.
P190
All
July 8, 1996.
P191
All
July 8, 1996.
P192
All
July 8, 1996.
P194
All
July 8, 1996.
P196
All
July 8, 1996.
P197
All
July 8, 1996.
P198
All
July 8, 1996.
P199
All
July 8, 1996.
P201
All
July 8, 1996.
P202
All
July 8, 1996.
P203
All
July 8, 1996.
P204
All
July 8, 1996.
P205
All
July 8, 1996.
U271
All
July 8, 1996.
U277
All
July 8, 1996.
U278
All
July 8, 1996.
U279
All
July 8, 1996.
U280
All
July 8, 1996.
U328
All
Nov. 9, 1992.
U353
All
Nov. 9, 1992.
U359
All
Nov. 9, 1992.
U364
All
July 8, 1996.
U365
All
July 8, 1996.
U366
All
July 8, 1996.
U367
All
July 8, 1996.
U372
All
July 8, 1996.
U373
All
July 8, 1996.
U375
All
July 8, 1996.
U376
All
July 8, 1996.
U377
All
July 8, 1996.
U378
All
July 8, 1996.
U379
All
July 8, 1996.
U381
All
July 8, 1996.
U382
All
July 8, 1996.
U383
All
July 8, 1996.
U384
All
July 8, 1996.
U385
All
July 8, 1996.
424
U386
All
July 8, 1996.
U387
All
July 8, 1996.
U389
All
July 8, 1996.
U390
All
July 8, 1996.
U391
All
July 8, 1996.
U392
All
July 8, 1996.
U395
All
July 8, 1996.
U396
All
July 8, 1996.
U400
All
July 8, 1996.
U401
All
July 8, 1996.
U402
All
July 8, 1996.
U403
All
July 8, 1996.
U404
All
July 8, 1996.
U407
All
July 8, 1996.
U409
All
July 8, 1996.
U410
All
July 8, 1996.
U411
All
July 8, 1996.
A
a
Wastes that are deep well disposed on-site receive a six-month variance, with
restrictions effective in November 1990.
B
b
Deep well injected D002 liquids with a pH less than 2 must meet the California List
treatment standards on August 8, 1990.
c
Managed in systems defined in 35 Ill. Adm. Code 730.105(e) as Class V injection
wells that do not engage in CWA-equivalent treatment before injection.
BOARD NOTE: This table is provided for the convenience of the reader.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Appendix J
Recordkeeping, Notification, and Certification Requirements
Repealed
Entity and Scenario
Frequency
Recipient of
Notification
Recordkeeping,
Notification, and
Certification Require-
ments
I. Generator
A. Waste does not
meet applicable treat-
ment standards or
exceeds applicable
prohibition levels (see
Each shipment
Treatment or
storage facility.
Notice must include:
•U.S. EPA hazardous
waste number.
425
Section
728.107(a)(1)).
•Constituents of
concern.
•Treatability group.
•Manifest number.
•Waste analysis data
(where available).
B. Waste can be dis-
posed of without
further treatment
(meets applicable
treatment standards or
does not exceed
prohibition levels upon
generation) (see
Section
728.107(a)(2)).
Each shipment
Land disposal
facility
Notice and certification
statement that waste
meets applicable treat-
ment standards or
applicable prohibition
levels.
Notice must include:
•U.S. EPA hazardous
waste number.
•Constituents of
concern.
•Treatability group.
•Manifest number.
•Waste analysis data
(where available).
Certification statement
required under Section
728.107(a)(2)(B) that
waste complies with
treatment standards and
prohibitions.
C. Waste is subject to
exemption from a
prohibition on the type
of land disposal
utilized for the waste,
such as a case-by-case
Each shipment
Receiving facility
Notice must include:
•Statement that waste is
not prohibited from land
disposal.
426
extension under
Section 728.105, an
exemption under Sec-
tion 728.106, or a
nationwide capacity
variance (see Section
728.107(a)(3)).
•U.S. EPA hazardous
waste number.
•Constituents of
concern.
•Treatability group.
•Manifest number.
•Waste analysis data
(where available).
•Date the waste is
subject to the prohibi-
tions.
D. Waste is being
accumulated in tanks
or containers regulated
under 35 Ill. Adm.
Code 722.134 and is
being treated in such
tanks or containers to
meet applicable treat-
ment standards (see
Section 728.107
(a)(4)).
Minimum of 30 days
prior to treatment
activity.
Agency. Delivery
must be verified.
Generator must
develop, keep on-site,
and follow a written
waste analysis plan
describing procedures
used to comply with the
treatment standards.
If waste is shipped off-
site, generator also must
comply with notification
requirement of Section
728.107(a)(2).
E. Generator is
managing a lab pack
containing certain
wastes and wishes to
use an alternative
treatment standard (see
Section
728.107(a)(8)).
Each shipment
Treatment facility
Notice in accordance
with Section
728.107(a)(1), (a)(5),
and (a)(6), where
applicable.
Certification in accor-
dance with Section
728.107(a)(8).
F. Small quantity
generators with tolling
agreements (pursuant
to 35 Ill. Adm. Code
Initial shipment
Treatment facility
Must comply with ap-
plicable notification and
certification require-
ments in Section
427
722.120(e)) (see
Section
728.107(a)(9)).
728.107(a).
Generator also must
retain copy of the notifi-
cation and certification
together with tolling
agreement on-site for at
least 3 years after termi-
nation or expiration of
agreement.
G. Generator has
determined waste is
restricted based solely
on his knowledge of
the waste (see Section
728.107(a)(5)).
N/A
Generator’s file
All supporting data must
be retained on-site in
generator’s files.
H. Generator has
determined waste is
restricted based on
testing waste or an ex-
tract (see Section
728.107(a)(5)).
N/A
Generator’s file
All waste analysis data
must be retained on-site
in generator’s files.
I. Generator has deter-
mined that waste is
excluded from the
definition of hazardous
or solid waste or
exempt from RCRA
Subtitle C (hazardous
waste) regulation (see
Section
728.107(a)(6)).
One-time
Generator’s file
Notice of generation
and subsequent
exclusion from the
definition of hazardous
or solid waste, or
exemption from RCRA
Subtitle C (hazardous
waste) regulation, and
information regarding
the disposition of the
waste.
J. Generator (or
treater) claims that
hazardous debris is
excluded from the
definition of hazardous
waste under 35 Ill.
Adm. Code
721.103(f)(1) (see
One-time
Agency.
Notification must
be updated as
necessary under
Section
728.107(d)(2).
Notice must include:
•Name and address of
RCRA Subtitle D
(municipal solid waste
landfill) facility
receiving treated debris.
428
Section 728.107(d)).
•U.S. EPA hazardous
waste number and
description of debris as
initially generated.
•Technology used to
treat the debris (Table 1
of Section 728.145).
Certification and
recordkeeping in
accordance with Section
728.107(d)(3).
K. Generator (or
treater) claims that
characteristic wastes
are no longer hazard-
ous (see Section
728.109 (d)).
One-time
Generator’s (or
treater’s) files and
Agency. Notifica-
tion must be
updated as
necessary under
Section 728.109(d).
Notice must include:
•Name and address of
RCRA Subtitle D
(municipal solid waste
landfill) facility
receiving the waste.
•U.S. EPA hazardous
waste number and
description of waste as
initially generated.
•Treatability group.
•Underlying hazardous
constituents.
Certification in
accordance with Section
728.109(d)(2).
L. Other
recordkeeping
requirements (see
Section
728.107(a)(7)).
N/A
Generator’s file
Generator must retain a
copy of all notices,
certifications,
demonstrations, waste
analysis data, and other
documentation produced
pursuant to Section
728.107 on-site for at
least 5 years from the
429
date that the waste was
last sent to on-site or
off-site treatment,
storage, or disposal.
This period is
automatically extended
during enforcement
actions or as requested
by the Agency.
II. Treatment Facility
A. Waste shipped
from treatment facility
to land disposal facility
(see Sections
728.107(b)(4) and
(b)(5)).
Each shipment
Land disposal
facility
Notice must include:
•U.S. EPA hazardous
waste number.
•Constituents of
concern.
•Treatability group.
•Manifest number.
•Waste analysis data
(where available).
Application
certification, in
accordance with Section
728.107(b)(5)(A),
(b)(5)(B) or (b)(5)(C),
stating that the waste or
treatment residue has
been treated in
compliance with
applicable treatment
standards and
prohibitions.
B. Waste treatment
residue from a
treatment or storage
facility will be further
managed at a different
Each shipment
Receiving facility
Treatment, storage, or
disposal facility must
comply with all notice
and certification
requirements applicable
430
treatment or storage
facility (see Section
728.107(b)(6)).
to generators.
C. Where wastes are
recyclable materials
used in a manner
constituting disposal
subject to Section
726.120(b) (see Sec-
tion 728.107(b)(7)).
Each shipment
Agency.
No notification to
receiving facility
required pursuant to
Section 728.107(b)(4).
Certification as
described in Section
728.107(b)(5) and
notice with information
listed in Section
728.107(b)(4), except
manifest number.
Recycling facility must
keep records of the
name and location of
each entity receiving
hazardous waste-derived
products.
III. Land Disposal Facility.
A. Wastes accepted by
land disposal facility
(see Section
728.107(c)).
N/A
N/A
Maintain copies of
notice and certifications
specified in Section
728.107(a) and (b).
Certification Statements
A. I certify under penalty of law that I personally have examined and am familiar with the
waste through analysis and testing or through knowledge of the waste to support this
certification that the waste complies with the treatment standards specified in 35 Ill. Adm.
Code 728.Subpart D and all applicable prohibitions set forth in 35 Ill. Adm. Code 728.132
or RCRA section 3004(d). I believe that the information I submitted is true, accurate and
complete. I am aware that there are significant penalties for submitting a false certification,
including the possibility of fine and imprisonment. (Section 728.107(a)(2)(B))
B. I certify under penalty of law that I personally have examined and am familiar with the
waste and that the lab pack does not contain any wastes identified at Section 728.Appendix
D. I am aware that there are significant penalties for submitting a false certification,
including possibility of fine or imprisonment. (Section 728.107(a)(8))
431
C. I certify under penalty of law that I have personally examined and am familiar with the
treatment technology and operation of the treatment process used to support this certification
and that, based on my inquiry of those individuals immediately responsible for obtaining
this information, I believe that the treatment process has been operated and maintained
properly so as to comply with the performance levels specified in 35 Ill. Adm. Code
728.Subpart D, and all applicable prohibitions set forth in 35 Ill. Adm. Code 728.132 or
RCRA section 3004(d) without impermissible dilution of the prohibited waste. I am aware
that there are significant penalties for submitting a false certification, including the
possibility of fine and imprisonment. (Section 728.107(b)(5)(A))
D. I certify under penalty of law that the waste has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.142. I am aware that there are significant penalties
for submitting a false certification, including the possibility of fine and imprisonment.
(Section 728.107(b)(5)(B))
E. I certify under penalty of law that I have personally examined and am familiar with the
treatment technology and operation of the treatment process used to support this certification
and that, based on my inquiry of those individuals immediately responsible for obtaining
this information, I believe that the nonwastewater organic constituents have been treated by
incineration in units operated in accordance with 35 Ill. Adm. Code 724.Subpart O or 35
Ill. Adm. Code 725.Subpart O or by combustion in fuel substitution units operating in
accordance with applicable technical requirements, and I have been unable to detect the
nonwastewater organic constituents, despite having used best good faith efforts to analyze
for such constituents. I am aware that there are significant penalties for submitting a false
certification, including the possibility of fine and imprisonment. (Section 728.107(b)(5)(C))
F. I certify under penalty of law that the waste has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.140 to remove the hazardous characteristic. This
decharacterized waste contains underlying hazardous constituents that require further
treatment to meet universal treatment standards. I am aware that there are significant
penalties for submitting a false certification, including the possibility of fine and
imprisonment. (Section 728.107(b)(5)(D))
G. I certify under penalty of law that the debris have been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.145. I am aware that there are significant penalties
for making a false certification, including the possibility of fine and imprisonment. (Section
728.107(d)(3)(C))
(Source: Repealed at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table C
Technology Codes and Description of Technology-Based Standards
Technology
432
code
Description of technology-based standard
ADGAS
Venting of compressed gases into an absorbing or reacting media (i.e., solid or
liquid)--venting can be accomplished through physical release utilizing valves or
piping; physical penetration of the container; or penetration through detonation.
AMLGM
Amalgamation of liquid, elemental mercury contaminated with radioactive
materials utilizing inorganic reagents such as copper, zinc, nickel, gold, and
sulfur that result in a nonliquid, semi-solid amalgam and thereby reducing
potential emissions of elemental mercury vapors to the air.
BIODG
Biodegradation of organics or non-metallic inorganics (i.e., degradable
inorganics that contain the elements of phosphorus, nitrogen, and sulfur) in
units operated under either aerobic or anaerobic conditions such that a surrogate
compound or indicator parameter has been substantially reduced in
concentration in the residuals (e.g., total organic carbon (TOC) can often be
used as an indicator parameter for the biodegradation of many organic
constituents that cannot be directly analyzed in wastewater residues).
CARBN
Carbon adsorption (granulated or powdered) of non-metallic inorganics, organo-
metallics, or organic constituents, operated so that a surrogate compound or
indicator parameter has not undergone breakthrough (e.g., total organic carbon
(TOC) can often be used as an indicator parameter for the adsorption of many
organic constituents that cannot be directly analyzed in wastewater residues).
Breakthrough occurs when the carbon has become saturated with the constituent
(or indicator parameter) and substantial change in adsorption rate associated
with that constituent occurs.
CHOXD
Chemical or electrolytic oxidation utilizing the following oxidation reagents (or
waste reagents) or combinations or reagents:
1)
hypochlorite (e.g., bleach);
2)
chlorine;
3)
chlorine dioxide;
4)
ozone or UV (ultraviolet light) assisted ozone;
5)
peroxides;
6)
persulfates;
7)
perchlorates;
433
8)
permanganates; or
9)
other oxidizing reagents of equivalent efficiency, performed in units operated so
that a surrogate compound or indicator parameter has been substantially reduced
in concentration in the residuals (e.g., total organic carbon (TOC) can often be
used as an indicator parameter for the oxidation of many organic constituents
that cannot be directly analyzed in wastewater residues). Chemical oxidation
specifically includes what is commonly referred to as alkaline chlorination.
CHRED
Chemical reduction utilizing the following reducing reagents (or waste reagents)
or combinations of reagents:
1)
sulfur dioxide;
2)
sodium, potassium, or alkali salts of sulfites, bisulfites, metabisulfites, and
polyethylene glycols (e.g., NaPEG and KPEG);
3)
sodium hydrosulfide;
4)
ferrous salts; or
5)
other reducing reagents of equivalent efficiency, performed in units operated
such that a surrogate compound or indicator parameter has been substantially
reduced in concentration in the residuals (e.g., total organic halogens (TOX)
can often be used as an indicator parameter for the reduction of many
halogenated organic constituents that cannot be directly analyzed in wastewater
residues). Chemical reduction is commonly used for the reduction of
hexavalent chromium to the trivalent state.
CMBST
Combustion High temperature organic destruction technologies, such as
combustion in incinerators, boilers, or industrial furnaces operated in
accordance with the applicable requirements of 35 Ill. Adm. Code 724.Subpart
O, 725.Subpart O, or 35 Ill. Adm. Code 726.Subpart H, and in other units
operated in accordance with applicable technical operating requirements; and
certain non-combustive technologies, such as the Catalytic Extraction Process.
DEACT
Deactivation to remove the hazardous characteristics of a waste due to its
ignitability, corrosivity, or reactivity.
FSUBS
Fuel substitution in units operated in accordance with applicable technical
operating requirements.
HLVIT
Vitrification of high level mixed radioactive wastes in units in compliance with
all applicable radioactive protection requirements under control of the federal
Nuclear Regulatory Commission.
434
IMERC
Incineration of wastes containing organics and mercury in units operated in
accordance with the technical operating requirements of 35 Ill. Adm. Code
724.Subpart O or 725.Subpart O. All wastewater and nonwastewater residues
derived from this process must then comply with the corresponding treatment
standards per waste code with consideration of any applicable subcategories
(e.g., high or low mercury subcategories).
INCIN
Incineration in units operated in accordance with the technical operating
requirements of 35 Ill. Adm. Code 724.Subpart O or 725.Subpart O.
LLEXT
Liquid-liquid extraction (often referred to as solvent extraction) of organics
from liquid wastes into an immiscible solvent for which the hazardous
constituents have a greater solvent affinity, resulting in an extract high in
organics that must undergo either incineration, reuse as a fuel, or other recovery
or reuse and a raffinate (extracted liquid waste) proportionately low in organics
that must undergo further treatment as specified in the standard.
MACRO
Macroencapsulation with surface coating materials such as polymeric organics
(e.g., resins and plastics) or with a jacket of inert inorganic materials to
substantially reduce surface exposure to potential leaching media.
Macroencapsulation specifically does not include any material that would be
classified as a tank or container according to 35 Ill. Adm. Code 720.110.
NEUTR
Neutralization with the following reagents (or waste reagents) or combinations
of reagents:
1)
acids;
2)
bases; or
3)
water (including wastewaters) resulting in a pH greater than 2 but less than 12.5
as measured in the aqueous residuals.
NLDBR
No land disposal based on recycling.
POLYM Formation of complex high-molecular weight solids through polymerization of
monomers in high-TOC D001 nonwastewaters that are chemical components in
the manufacture of plastics.
PRECP
Chemical precipitation of metals and other inorganics as insoluble precipitates of
oxides, hydroxides, carbonates, sulfides, sulfates, chlorides, fluorides, or
phosphates. The following reagents (or waste reagents) are typically used alone
or in combination:
435
1)
lime (i.e., containing oxides or hydroxides of calcium or magnesium);
2)
caustic (i.e., sodium or potassium hydroxides);
3)
soda ash (i.e., sodium carbonate);
4)
sodium sulfide;
5)
ferric sulfate or ferric chloride;
6)
alum; or
7)
sodium sulfate. Additional flocculating, coagulation, or similar reagents or
processes that enhance sludge dewatering characteristics are not precluded from
use.
RBERY
Thermal recovery of beryllium.
RCGAS
Recovery or reuse of compressed gases including techniques such as
reprocessing of the gases for reuse or resale; filtering or adsorption of
impurities; remixing for direct reuse or resale; and use of the gas as a fuel
source.
RCORR
Recovery of acids or bases utilizing one or more of the following recovery
technologies:
1)
distillation (i.e., thermal concentration);
2)
ion exchange;
3)
resin or solid adsorption;
4)
reverse osmosis; or
5)
incineration for the recovery of acid--
Note: this does not preclude the use of other physical phase separation or
concentration techniques such as decantation, filtration (including
ultrafiltration), and centrifugation, when used in conjunction with the above
listed recovery technologies.
RLEAD
Thermal recovery of lead in secondary lead smelters.
RMERC
Retorting or roasting in a thermal processing unit capable of volatilizing
mercury and subsequently condensing the volatilized mercury for recovery.
436
The retorting or roasting unit (or facility) must be subject to one or more of the
following:
a)
A national emissions standard for hazardous air pollutants (NESHAP) for
mercury (40 CFR 61, Subpart E);
b)
A best available control technology (BACT) or a lowest achievable emission
rate (LAER) standard for mercury imposed pursuant to a prevention of
significant deterioration (PSD) permit (including 35 Ill. Adm. Code 201
through 203); or
c)
A state permit that establishes emission limitations (within meaning of Section
302 of the Clean Air Act) for mercury, including a permit issued pursuant to 35
Ill. Adm. Code 201. All wastewater and nonwastewater residues derived from
this process must then comply with the corresponding treatment standards per
waste code with consideration of any applicable subcategories (e.g., high or low
mercury subcategories).
RMETL
Recovery of metals or inorganics utilizing one or more of the following direct
physical or removal technologies:
1)
ion exchange;
2)
resin or solid (i.e., zeolites) adsorption;
3)
reverse osmosis;
4)
chelation or solvent extraction;
5)
freeze crystallization;
6)
ultrafiltration; or
7)
simple precipitation (i.e., crystallization)
Note: this does not preclude the use of other physical phase separation or
concentration techniques such as decantation, filtration (including
ultrafiltration), and centrifugation, when used in conjunction with the above
listed recovery technologies.
RORGS
Recovery of organics utilizing one or more of the following technologies:
1)
Distillation;
2)
thin film evaporation;
437
3)
steam stripping;
4)
carbon adsorption;
5)
critical fluid extraction;
6)
liquid-liquid extraction;
7)
precipitation or crystallization (including freeze crystallization); or
8)
chemical phase separation techniques (i.e., addition of acids, bases,
demulsifiers, or similar chemicals).
Note: This does not preclude the use of other physical phase separation
techniques such as decantation, filtration (including ultrafiltration), and
centrifugation, when used in conjunction with the above listed recovery
technologies.
RTHRM
Thermal recovery of metals or inorganics from nonwastewaters in units defined
as cement kilns, blast furnaces, smelting, melting and refining furnaces,
combustion devices used to recover sulfur values from spent sulfuric acid and
“other devices” determined by the Agency pursuant to 35 Ill. Adm. Code
720.110, the definition of “industrial furnace”.
RZINC
Resmelting in high temperature metal recovery units for the purpose of recovery
of zinc.
STABL
Stabilization with the following reagents (or waste reagents) or combinations of
reagents:
1)
Portland cement; or
2)
lime or pozzolans (e.g., fly ash and cement kiln dust)--this does not preclude
the addition of reagents (e.g., iron salts, silicates, and clays) designed to
enhance the set or cure time or compressive strength, or to overall reduce the
leachability of the metal or inorganic.
SSTRP
Steam stripping of organics from liquid wastes utilizing direct application of
steam to the wastes operated such that liquid and vapor flow rates, as well as,
temperature and pressure ranges have been optimized, monitored, and
maintained. These operating parameters are dependent upon the design
parameters of the unit such as, the number of separation stages and the internal
column design. Thus, resulting in a condensed extract high in organics that
must undergo either incineration, reuse as a fuel, or other recovery or reuse and
438
an extracted wastewater that must undergo further treatment as specified in the
standard.
WETOX
Wet air oxidation performed in units operated such that a surrogate compound
or indicator parameter has been substantially reduced in concentration in the
residuals (e.g., total organic carbon (TOC) can often be used as an indicator
parameter for the oxidation of many organic constituents that cannot be directly
analyzed in wastewater residues).
WTRRX
Controlled reaction with water for highly reactive inorganic or organic
chemicals with precautionary controls for protection of workers from potential
violent reactions as well as precautionary controls for potential emissions of
toxic or ignitable levels of gases released during the reaction.
Note 1:
When a combination of these technologies (i.e., a treatment train) is specified as
a single treatment standard, the order of application is specified in Section
728.Table T by indicating the five letter technology code that must be applied
first, then the designation “fb.” (an abbreviation for “followed by”), then the
five letter technology code for the technology that must be applied next, and so
on.
Note 2:
When more than one technology (or treatment train) are specified as alternative
treatment standards, the five letter technology codes (or the treatment trains) are
separated by a semicolon (;) with the last technology preceded by the word
“OR”. This indicates that any one of these BDAT technologies or treatment
trains can be used for compliance with the standard.
BOARD NOTE: Derived from 40 CFR 268.42, Table 1 (1997).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table H
Wastes Excluded from CCW Treatment Standards
The following facilities are excluded from the treatment standard under Section 728.143(a) and
Table B, and are subject to the following constituent concentrations. These facilities have received
a treatability exception by regulatory action from USEPA pursuant to 40 CFR 268.44 (1991), and
have demonstrated that the Board needs to adopt the treatability exception as part of the Illinois
RCRA program. The Board may also grant an “adjusted treatment standard” pursuant to Section
728.144.
Facility name and
address
Waste
Code
See
Also
Regulated
hazardous
constituent
Wastewaters
Concentration
(mg/L)
Notes
Nonwaste-
waters
Concentration
(mg/L)
Notes
Craftsman Plating
F006
Table A
Cyanides
1.2
B
1800
D
439
and Tinning Corp.,
Chicago, IL
Section
728.140
(Total)
Cyanides
(amenable)
0.86
B and C
30
D
Cadmium
1.6
NA
Chromium
0.32
NA
Lead
0.40
NA
Nickel
0.44
NA
Northwestern Plat-
ing Works, Inc.,
Chicago, IL
F006
Table A
Section
728.140
Cyanides
(Total)
1.2
B
970
D
Cyanides
(amenable)
0.86
B and C
30
D
Cadmium
1.6
NA
Chromium
0.32
NA
Lead
0.40
NA
Nickel
0.44
NA
Notes:
A
An owner or operator may certify compliance with these treatment standards according to
the provisions of Section 728.107.
B
Cyanide wastewater standards for F006 are based on analysis of composite samples.
C
These owners and operators shall comply with 0.86 mg/L for amenable cyanides in the
wastewater exiting the alkaline chlorination system. These owners and operators shall also
comply with Section 728.107(a)(4) for appropriate monitoring frequency consistent with the
facilities’ waste analysis plan.
D
Cyanide nonwastewaters are analyzed using SW-846 Method 9010 or 9012, sample size 10
g, distillation time one hour and fifteen minutes. SW-846 is incorporated by reference in
35 Ill. Adm. Code 720.111.
NA
Not applicable.
BOARD NOTE: Derived from table to 40 CFR 268.44(o) (1997).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table I Generator Paperwork Requirements
Subsection of Section 728.107 under
which the Paperwork Is Required:
Required information
(a)(2)
(a)(3)
(a)(4)
(a)(9)
1. USEPA hazardous waste and manifest numbers
ü
ü
ü
ü
440
2. Statement: this waste is not prohibited from
land disposal
ü
3. The waste is subject to the LDRs. The
constituents of concern for F001 through F005
and F039, and underlying hazardous constituents
(for wastes that are not managed in a Clean Water
Act (CWA) or CWA-equivalent facility), unless
the waste will be treated and monitored for all
constituents. If all constituents will be treated
and monitored, there is no need to put them all on
the LDR notice
ü
ü
4. The notice must include the applicable
wastewater/ nonwastewater category (see Section
728.102(d) and (f)) and subdivisions made within
a waste code based on waste-specific criteria
(such as D003 reactive cyanide)
ü
ü
5. Waste analysis data (when available)
ü
ü
ü
6. Date the waste is subject to the prohibition
ü
7. For hazardous debris, when treating with the
alternative treatment technologies provided by
Section 728.145: the contaminants subject to
treatment, as described in Section 728.145(b);
and an indication that these contaminants are
being treated to comply with Section 728.145
ü
ü
8. A certification is needed (see applicable
subsection for exact wording)
ü
ü
BOARD NOTE: Derived from Table 1 to 40 CFR 268.7(a)(4) (1997).
(Source: Added at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table T
Treatment Standards for Hazardous Wastes
Note: The treatment standards that heretofore appeared in tables in Sections 728.141,
728.142, and 728.143 have been consolidated into this table.
Waste Code
Waste Description and Treatment or Regulatory Subcategory
1
441
Regulated Hazardous Constituent
Wastewaters
Nonwastewaters
Common Name
CAS
2
Number
Concentration in
mg/l
3
; or Tech-
nology Code
4
Concentration in
mg/kg
5
unless
noted as “mg/l
TCLP”; or
Technology
Code
4
D001
9
Ignitable Characteristic Wastes, except for the 35 Ill. Adm. Code 721.121(a)(1) High TOC
Subcategory.
NA
NA
DEACT and
meet Section
728.148
standards;
8
or
RORGS; or
CMBST
DEACT and
meet Section
728.148
standards;
8
or
RORGS; or
CMBST
D001
9
High TOC Ignitable Characteristic Liquids Subcategory based on 35 Ill. Adm. Code
721.121(a)(1) - Greater than or equal to 10% percent total organic carbon.
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
RORGS; or
CMBST; or
POLYM
D002
9
Corrosive Characteristic Wastes.
NA
NA
DEACT and
meet Section
728.148
standards
8
DEACT and
meet Section
728.148
standards
8
D002, D004, D005, D006, D007, D008, D009, D010, D011
Radioactive high level wastes generated during the reprocessing of fuel rods.
(Note: This subcategory consists of nonwastewaters only.)
Corrosivity (pH)
NA
NA
HLVIT
Arsenic
7440-38-2
NA
HLVIT
Barium
7440-39-3
NA
HLVIT
Cadmium
7440-43-9
NA
HLVIT
Chromium (Total)
7440-47-3
NA
HLVIT
Lead
7439-92-1
NA
HLVIT
Mercury
7439-97-6
NA
HLVIT
442
Selenium
7782-49-2
NA
HLVIT
Silver
7440-22-4
NA
HLVIT
D003
9
Reactive Sulfides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
NA
NA
DEACT
DEACT
D003
9
Explosive subcategory based on 35 Ill. Adm. Code 721.123(a)(6), (a)(7), and (a)(8).
NA
NA
DEACT and
meet Section
728.148
standards
8
DEACT and
meet Section
728.148
standards
8
D003
9
Unexploded ordnance and other explosive devices that have been the subject of an emergency
response.
NA
NA
DEACT
DEACT
D003
9
Other Reactives Subcategory based on 35 Ill. Adm. Code 721.123(a)(1).
NA
NA
DEACT and
meet Section
728.148
standards
8
DEACT and
meet Section
728.148
standards
8
D003
9
Water Reactive Subcategory based on 35 Ill. Adm. Code 721.123(a)(2), (a)(3), and (a)(4).
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
DEACT and
meet Section
728.148
standards
8
D003
9
Reactive Cyanides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
Cyanides (Total)
7
57-12-5
--
590
Cyanides (Amenable)
7
57-12-5
0.86
30
D004
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for arsenic based
on the extraction procedure (EP) in SW-846 Method 1310.
Arsenic
7440-38-2
5.0
5.0 mg/l EP
Arsenic; alternative
6
standard
for nonwastewaters only.
7440-38-2
NA
5.0 mg/l TCLP
443
D005
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for barium based
on the extraction procedure (EP) in SW-846 Method 1310.
Barium
7440-39-3
100
100 mg/l TCLP
D006
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for cadmium based
on the extraction procedure (EP) in SW-846 Method 1310.
Cadmium
7440-43-9
1.0
1.0 mg/l TCLP
D006
Cadmium-Containing Batteries Subcategory
(Note: This subcategory consists of nonwastewaters only.)
Cadmium
7440-43-9
NA
RTHRM
D007
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for chromium
based on the extraction procedure (EP) in SW-846 Method 1310.
Chromium (Total)
7440-47-3
5.0
5.0 mg/l TCLP
D008
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for lead based on
the extraction procedure (EP) in SW-846 Method 1310.
Lead
7439-92-1
5.0
5.0 mg/l EP
Lead; alternative
6
standard
for nonwastewaters only
7439-92-1
NA
5.0 mg/l TCLP
D008
Lead Acid Batteries Subcategory
(Note: This standard only applies to lead acid batteries that are identified as RCRA hazardous
wastes and that are not excluded elsewhere from regulation under the land disposal restrictions
of this Part or exempted under other regulations (see 35 Ill. Adm. Code 726.180). This
subcategory consists of nonwastewaters only.)
Lead
7439-92-1
NA
RLEAD
D008
Radioactive Lead Solids Subcategory
(Note: These lead solids include, but are not limited to, all forms of lead shielding and other
elemental forms of lead. These lead solids do not include treatment residuals such as
hydroxide sludges, other wastewater treatment residuals, or incinerator ashes that can undergo
conventional pozzolanic stabilization, nor do they include organo-lead materials that can be
incinerated and stabilized as ash. This subcategory consists of nonwastewaters only.)
Lead
7439-92-1
NA
MACRO
D009
444
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction procedure (EP) in SW-846 Method 1310; and contain greater
than or equal to 260 mg/kg total mercury that also contain organics and are not incinerator
residues. (High Mercury-Organic Subcategory)
Mercury
7439-97-6
NA
IMERC; or
RMERC
D009
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction procedure (EP) in SW-846 Method 1310; and contain greater
than or equal to 260 mg/kg total mercury that are inorganic, including incinerator residues and
residues from RMERC. (High Mercury-Inorganic Subcategory)
Mercury
7439-97-6
NA
RMERC
D009
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of toxicity for
mercury based on the extraction procedure (EP) in SW-846 Method 1310; and contain less
than 260 mg/kg total mercury. (Low Mercury Subcategory)
Mercury
7439-97-6
NA
0.20 mg/l TCLP
All D009 wastewaters.
Mercury
7439-97-6
0.20
NA
D009
Elemental mercury contaminated with radioactive materials.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
AMLGM
D009
Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
IMERC
D010
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for selenium based
on the extraction procedure (EP) in SW-846 Method 1310.
Selenium
7782-49-2
1.0
5.7 mg/l TCLP
D011
Wastes that exhibit, or are expected to exhibit, the characteristic of toxicity for silver based on
the extraction procedure (EP) in SW-846 Method 1310.
Silver
7440-22-4
5.0
5.0 mg/l TCLP
D012
9
445
Wastes that are TC for Endrin based on the TCLP in SW-846 Method 1311.
Endrin
72-20-8
BIODG; or
CMBST
0.13 and meet
Section 728.148
standards
8
Endrin aldehyde
7421-93-4
BIODG; or
CMBST
0.13 and meet
Section 728.148
standards
8
D013
9
Wastes that are TC for Lindane based on the TCLP in SW-846 Method 1311.
alpha
α
-BHC
319-84-6
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
beta
β
-BHC
319-85-7
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
delta
δ
-BHC
319-86-8
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
gamma
χ
-BHC (Lindane)
58-89-9
CARBN; or
CMBST
0.066 and meet
Section 728.148
standards
8
D014
9
Wastes that are TC for Methoxychlor based on the TCLP in SW-846 Method 1311.
Methoxychlor
72-43-5
WETOX or
CMBST
0.18 and meet
Section 728.148
standards
8
D015
9
Wastes that are TC for Toxaphene based on the TCLP in SW-846 Method 1311.
Toxaphene
8001-35-2
BIODG or
CMBST
2.6 and meet
Section 728.148
standards
8
D016
9
Wastes that are TC for 2,4-D (2,4-Dichlorophenoxyacetic acid) based on the TCLP in SW-846
Method 1311.
2,4-D (2,4-Dichloro-
phenoxyacetic acid)
94-75-7
CHOXD;
BIODG; or
CMBST
10 and meet
Section 728.148
standards
8
D017
9
Wastes that are TC for 2,4,5-TP (Silvex) based on the TCLP in SW-846 Method 1311.
2,4,5-TP (Silvex)
93-72-1
CHOXD or
7.9 and meet
446
CMBST
Section 728.148
standards
8
D018
9
Wastes that are TC for Benzene based on the TCLP in SW-846 Method 1311.
Benzene
71-43-2
0.14 and meet
Section 728.148
standards
8
10 and meet
Section 728.148
standards
8
D019
9
Wastes that are TC for Carbon tetrachloride based on the TCLP in SW-846 Method 1311.
Carbon tetrachloride
56-23-5
0.057 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D020
9
Wastes that are TC for Chlordane based on the TCLP in SW-846 Method 1311.
Chlordane (alpha
α
and
gamma
χ
isomers)
57-74-9
0.0033 and meet
Section 728.148
standards
8
0.26 and meet
Section 728.148
standards
8
D021
9
Wastes that are TC for Chlorobenzene based on the TCLP in SW-846 Method 1311.
Chlorobenzene
108-90-7
0.057 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D022
9
Wastes that are TC for Chloroform based on the TCLP in SW-846 Method 1311.
Chloroform
67-66-3
0.046 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D023
9
Wastes that are TC for o-Cresol based on the TCLP in SW-846 Method 1311.
o-Cresol
95-48-7
0.11 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D024
9
Wastes that are TC for m-Cresol based on the TCLP in SW-846 Method 1311.
m-Cresol
(difficult to distinguish from
p-cresol)
108-39-4
0.77 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
447
D025
9
Wastes that are TC for p-Cresol based on the TCLP in SW-846 Method 1311.
p-Cresol
(difficult to distinguish from
m-cresol)
106-44-5
0.77 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D026
9
Wastes that are TC for Cresols (Total) based on the TCLP in SW-846 Method 1311.
Cresol-mixed isomers
(Cresylic acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88 and meet
Section 728.148
standards
8
11.2 and meet
Section 728.148
standards
8
D027
9
Wastes that are TC for p-Dichlorobenzene based on the TCLP in SW-846 Method 1311.
p-Dichlorobenzene (1,4-
Dichlorobenzene)
106-46-7
0.090 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D028
9
Wastes that are TC for 1,2-Dichloroethane based on the TCLP in SW-846 Method 1311.
1,2-Dichloroethane
107-06-2
0.21 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D029
9
Wastes that are TC for 1,1-Dichloroethylene based on the TCLP in SW-846 Method 1311.
1,1-Dichloroethylene
75-35-4
0.025 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D030
9
Wastes that are TC for 2,4-Dinitrotoluene based on the TCLP in SW-846 Method 1311.
2,4-Dinitrotoluene
121-14-2
0.32 and meet
Section 728.148
standards
8
140 and meet
Section 728.148
standards
8
D031
9
Wastes that are TC for Heptachlor based on the TCLP in SW-846 Method 1311.
Heptachlor
76-44-8
0.0012 and meet
Section 728.148
standards
8
0.066 and meet
Section 728.148
standards
8
Heptachlor epoxide
1024-57-3
0.016 and meet
Section 728.148
standards
8
0.066 and meet
Section 728.148
standards
8
448
D032
9
Wastes that are TC for Hexachlorobenzene based on the TCLP in SW-846 Method 1311.
Hexachlorobenzene
118-74-1
0.055 and meet
Section 728.148
standards
8
10 and meet
Section 728.148
standards
8
D033
9
Wastes that are TC for Hexachlorobutadiene based on the TCLP in SW-846 Method 1311.
Hexachlorobutadiene
87-68-3
0.055 and meet
Section 728.148
standards
8
5.6 and meet
Section 728.148
standards
8
D034
9
Wastes that are TC for Hexachloroethane based on the TCLP in SW-846 Method 1311.
Hexachloroethane
67-72-1
0.055 and meet
Section 728.148
standards
8
30 and meet
Section 728.148
standards
8
D035
9
Wastes that are TC for Methyl ethyl ketone based on the TCLP in SW-846 Method 1311.
Methyl ethyl ketone
78-93-3
0.28 and meet
Section 728.148
standards
8
36 and meet
Section 728.148
standards
8
D036
9
Wastes that are TC for Nitrobenzene based on the TCLP in SW-846 Method 1311.
Nitrobenzene
98-95-3
0.068 and meet
Section 728.148
standards
8
14 and meet
Section 728.148
standards
8
D037
9
Wastes that are TC for Pentachlorophenol based on the TCLP in SW-846 Method 1311.
Pentachlorophenol
87-86-5
0.089 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
D038
9
Wastes that are TC for Pyridine based on the TCLP in SW-846 Method 1311.
Pyridine
110-86-1
0.014 and meet
Section 728.148
standards
8
16 and meet
Section 728.148
standards
8
D039
9
Wastes that are TC for Tetrachloroethylene based on the TCLP in SW-846 Method 1311.
449
Tetrachloroethylene
127-18-4
0.056 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D040
9
Wastes that are TC for Trichloroethylene based on the TCLP in SW-846 Method 1311.
Trichloroethylene
79-01-6
0.054 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
D041
9
Wastes that are TC for 2,4,5-Trichlorophenol based on the TCLP in SW-846 Method 1311.
2,4,5-Trichlorophenol
95-95-4
0.18 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
D042
9
Wastes that are TC for 2,4,6-Trichlorophenol based on the TCLP in SW-846 Method 1311.
2,4,6-Trichlorophenol
88-06-2
0.035 and meet
Section 728.148
standards
8
7.4 and meet
Section 728.148
standards
8
D043
9
Wastes that are TC for Vinyl chloride based on the TCLP in SW-846 Method 1311.
Vinyl chloride
75-01-4
0.27 and meet
Section 728.148
standards
8
6.0 and meet
Section 728.148
standards
8
F001, F002, F003, F004 & F005
F001, F002, F003, F004, or F005 solvent wastes that contain any combination of one or more
of the following spent solvents: acetone, benzene, n-butyl alcohol, carbon disulfide, carbon
tetrachloride, chlorinated fluorocarbons, chlorobenzene, o-cresol, m-cresol, p-cresol, cyclo-
hexanone, o-dichlorobenzene, 2-ethoxyethanol, ethyl acetate, ethyl benzene, ethyl ether,
isobutyl alcohol, methanol, methylene chloride, methyl ethyl ketone, methyl isobutyl ketone,
nitrobenzene, 2-nitropropane, pyridine, tetrachloroethylene, toluene, 1,1,1-trichloroethane,
1,1,2-trichloroethane, 1,1,2-trichloro-1,2,2-trifluoroethane, trichloroethylene, trichloromono-
fluoromethane, or xylenes (except as specifically noted in other subcategories). See further
details of these listings in 35 Ill. Adm. Code 721.131
Acetone
67-64-1
0.28
160
Benzene
71-43-2
0.14
10
n-Butyl alcohol
71-36-3
5.6
2.6
Carbon disulfide
75-15-0
3.8
NA
Carbon tetrachloride
56-23-5
0.057
6.0
Chlorobenzene
108-90-7
0.057
6.0
o-Cresol
95-48-7
0.11
5.6
450
m-Cresol
(difficult to distinguish from
p-cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from
m-cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers
(Cresylic acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88
11.2
Cyclohexanone
108-94-1
0.36
NA
o-Dichlorobenzene
95-50-1
0.088
6.0
Ethyl acetate
141-78-6
0.34
33
Ethyl benzene
100-41-4
0.057
10
Ethyl ether
60-29-7
0.12
160
Isobutyl alcohol
78-83-1
5.6
170
Methanol
67-56-1
5.6
NA
Methylene chloride
75-9-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Nitrobenzene
98-95-3
0.068
14
Pyridine
110-86-1
0.014
16
Tetrachloroethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
1,1,2-Trichloro-1,2,2-
trifluoroethane
76-13-1
0.057
30
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane
75-69-4
0.020
30
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
F001, F002, F003, F004 & F005
F003 and F005 solvent wastes that contain any combination of one or more of the following
three solvents as the only listed F001 through F005 solvents: carbon disulfide, cyclohexanone,
or methanol. (Formerly Section 728.141(c))
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
Methanol
67-56-1
5.6
0.75 mg/l TCLP
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Nitropropane as the only listed F001 through F005 solvent.
2-Nitropropane
79-46-9
(WETOX or
CMBST
451
CHOXD) fb
CARBN; or
CMBST
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Ethoxyethanol as the only listed F001 through F005 solvent.
2-Ethoxyethanol
110-80-5
BIODG; or
CMBST
CMBST
F006
Wastewater treatment sludges from electroplating operations except from the following
processes: (1) Sulfuric acid anodizing of aluminum; (2) tin plating on carbon steel; (3) zinc
plating (segregated basis) on carbon steel; (4) aluminum or zinc-aluminum plating on carbon
steel; (5) cleaning or stripping associated with tin, zinc, and aluminum plating on carbon steel;
and (6) chemical etching and milling of aluminum.
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F007
Spent cyanide plating bath solutions from electroplating operations.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F008
Plating bath residues from the bottom of plating baths from electroplating operations where
cyanides are used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F009
452
Spent stripping and cleaning bath solutions from electroplating operations where cyanides are
used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F010
Quenching bath residues from oil baths from metal heat treating operations where cyanides are
used in the process.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
NA
F011
Spent cyanide solutions from salt bath pot cleaning from metal heat treating operations.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F012
Quenching wastewater treatment sludges from metal heat treating operations where cyanides
are used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F019
Wastewater treatment sludges from the chemical conversion coating of aluminum except from
zirconium phosphating in aluminum can washing when such phosphating is an exclusive
conversion coating process.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
453
F020, F021, F022, F023, F026
Wastes (except wastewater and spent carbon from hydrogen chloride purification) from the
production or manufacturing use (as a reactant, chemical intermediate, or component in a
formulating process) of: (1) tri- or tetrachlorophenol, or of intermediates used to produce
their pesticide derivatives, excluding wastes from the production of Hexachlorophene from
highly purified 2,4,5-trichlorophenol (i.e., F020); (2) pentachlorophenol, or of intermediates
used to produce its derivatives (i.e., F021); (3) tetra-, penta-, or hexachlorobenzenes under
alkaline conditions (i.e., F022) and wastes (except wastewater and spent carbon from hydrogen
chloride purification) from the production of materials on equipment previously used for the
production or manufacturing use (as a reactant, chemical intermediate, or component in a
formulating process) of: (1) tri- or tetrachlorophenols, excluding wastes from equipment used
only for the production of Hexachlorophene from highly purified 2,4,5-trichlorophenol (F023)
or (2) tetra-, penta-, or hexachlorobenzenes under alkaline conditions (i.e., F026).
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F024
Process wastes, including but not limited to, distillation residues, heavy ends, tars, and reactor
clean-out wastes, from the production of certain chlorinated aliphatic hydrocarbons by free
radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon
chain lengths ranging from one to and including five, with varying amounts and positions of
chlorine substitution. (This listing does not include wastewaters, wastewater treatment
sludges, spent catalysts, and wastes listed in 35 Ill. Adm. Code 721.131 or 721.132.)
All F024 wastes
NA
CMBST
11
CMBST
11
2-Chloro-1,3-butadiene
126-99-8
0.057
0.28
3-Chloropropylene
107-05-1
0.036
30
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
454
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
bis(2-Ethylhexyl)phthalate
117-81-7
0.28
28
Hexachloroethane
67-72-1
0.055
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
F025
Condensed light ends from the production of certain chlorinated aliphatic hydrocarbons by free
radical catalyzed processes. These chlorinated aliphatic hydrocarbons are those having carbon
chain lengths ranging from one up to and including five, with varying amounts and positions
of chlorine substitution. F025--Light Ends Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F025
Spent filters and filter aids, and spent desiccant wastes from the production of certain
chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These chlorinated
aliphatic hydrocarbons are those having carbon chain lengths ranging from one to and
including five, with varying amounts and positions of chlorine substitution. F025--Spent
Filters/Aids and Desiccants Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F027
Discarded unused formulations contianing tri-, tetra-, or pentachlorophenol or discarded
unused formulations containing compounds derived from these chlorophenols. (This listing
does not include formulations containing hexachlorophene synthesized from prepurified 2,4,5-
trichlorophenol as the sole component.)
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
455
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F028
Residues resulting from the incineration or thermal treatment of soil contaminated with
USEPA hazardous waste numbers F020, F021, F023, F026, and F027.
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachlorophenol
87-86-5
0.089
7.4
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
F032
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes
generated at plants that currently use or have previously used chlorophenolic formulations
(except potentially cross-contaminated wastes that have had the F032 waste code deleted in
accordance with 35 Ill. Adm. Code 721.135 or potentially cross-contaminated wastes that are
otherwise currently regulated as hazardous wastes (i.e., F034 or F035), where the generator
does not resume or initiate use of chlorophenolic formulations). This listing does not include
K001 bottom sediment sludge from the treatment of wastewater from wood preserving
processes that use creosote and/or penta-chlorophenol.
Acenaphthene
83-32-9
0.059
3.4
456
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k) fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b) fluoranthene)
207-08-9
0.11
6.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
2-4-Dimethyl phenol
105-67-9
0.036
14
Fluorene
86-73-7
0.059
3.4
Hexachlorodibenzo-p-dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Hexachlorodibenzofurans
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Pentachlorodibenzo-p-
dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Pentachlorodibenzofurans
NA
0.000035 or
CMBST
11
0.001 or
CMBST
11
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Tetrachlorodibenzo-p-dioxins
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
Tetrachlorodibenzofurans
NA
0.000063 or
CMBST
11
0.001 or
CMBST
11
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
F034
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes
generated at plants that use creosote formulations. This listing does not include K001 bottom
sediment sludge from the treatment of wastewater from wood preserving processes that use
creosote or pentachlorophenol.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
457
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Fluorene
86-73-7
0.059
3.4
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
F035
Wastewaters (except those that have not come into contact with process contaminants), process
residuals, preservative drippage, and spent formulations from wood preserving processes that
are generated at plants that use inorganic preservatives containing arsenic or chromium. This
listing does not include K001 bottom sediment sludge from the treatment of wastewater from
wood preserving processes that use creosote or pentachlorophenol.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
F037
Petroleum refinery primary oil/water/solids separation sludge--Any sludge generated from the
gravitational separation of oil/water/solids during the storage or treatment of process
wastewaters and oily cooling wastewaters from petroleum refineries. Such sludges include,
but are not limited to, those generated in: oil/water/solids separators; tanks and
impoundments; ditches and other conveyances; sumps; and stormwater units receiving dry
weather flow. Sludge generated in stormwater units that do not receive dry weather flow,
sludges generated from non-contact once-through cooling waters segregated for treatment from
other process or oily cooling waters, sludges generated in agressive biological treatment units
as defined in 35 Ill. Adm. Code 721.131(b)(2) (including sludges generated in one or more
additional units after wastewaters have been treated in agressive biological treatment units) and
K051 wastes are not included in this listing.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
458
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
F038
Petroleum refinery secondary (emulsified) oil/water/solids separation sludge or float generated
from the physical or chemical separation of oil/water/solids in process wastewaters and oily
cooling wastewaters from petroleum refineries. Such wastes include, but are not limited to, all
sludges and floats generated in: induced air floatation (IAF) units, tanks and impoundments,
and all sludges generated in DAF units. Sludges generated in stormwater units that do not
receive dry weather flow, sludges generated from non-contact once-through cooling waters
segregated for treatment from other process or oily cooling waters, sludges and floats
generated in agressive biological treatment units as defined in 35 Ill. Adm. Code
721.131(b)(2) (including sludges and floats generated in one or more additional units after
wastewaters have been treated in agressive biological units) and F037, K048, and K051 are not
included in this listing.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
459
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
F039
Leachate (liquids that have percolated through land disposed wastes) resulting from the
disposal of more than one restricted waste classified as hazardous under Subpart D of this
Part. (Leachate resulting from the disposal of one or more of the following USEPA hazardous
wastes and no other hazardous wastes retains its USEPA hazardous waste numbers: F020,
F021, F022, F026, F027, or F028.).
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
NA
Acetophenone
96-86-2
0.010
9.7
2-Acetylaminofluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylonitrile
107-13-1
0.24
84
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
alpha
α
-BHC
319-84-6
0.00014
0.066
beta
β
-BHC
319-85-7
0.00014
0.066
delta
δ
-BHC
319-86-8
0.023
0.066
gamma
χ
-BHC
58-89-9
0.0017
0.066
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloromethane
75-27-4
0.35
15
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
4-Bromophenyl phenyl ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitro-
88-85-7
0.066
2.5
460
phenol (Dinoseb)
Carbon disulfide
75-15-0
3.8
NA
Carbon tetrachloride
56-23-5
0.057
6.0
Chlordane (alpha
α
and
gamma
χ
isomers)
57-74-9
0.0033
0.26
p-Chloroaniline
106-47-8
0.46
16
Chlorobenzene
108-90-7
0.057
6.0
Chlorobenzilate
510-15-6
0.10
NA
2-Chloro-1,3-butadiene
126-99-8
0.057
NA
Chlorodibromomethane
124-48-1
0.057
15
Chloroethane
75-00-3
0.27
6.0
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
Chloroform
67-66-3
0.046
6.0
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
2-Chloronaphthalene
91-58-7
0.055
5.6
2-Chlorophenol
95-57-8
0.044
5.7
3-Chloropropylene
107-05-1
0.036
30
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from
p-cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from
m-cresol)
106-44-5
0.77
5.6
Cyclohexanone
108-94-1
0.36
NA
1,2-Dibromo-3-chloro-
propane
96-12-8
0.11
15
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
Dibromomethane
74-95-3
0.11
15
2,4-D (2,4-Dichloro-
phenoxyacetic acid)
94-75-7
0.72
10
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
p,p’-DDE
72-55-9
0.031
0.087
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Dibenz(a,e)pyrene
192-65-4
0.061
NA
461
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Dichlorodifluoromethane
75-71-8
0.23
7.2
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
87-65-0
0.044
14
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethyl phthalate
84-66-2
0.20
28
2-4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
1,4-Dinitrobenzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitrophenol
51-28-5
0.12
160
2,4-Dinitrotoluene
121-14-2
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
Di-n-propylnitrosamine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
12.0
170
Diphenylamine (difficult to
distinguish from diphenyl-
nitrosamine)
122-39-4
0.92
NA
Diphenylnitrosamine
(difficult to distinguish from
diphenylamine)
86-30-6
0.92
NA
1,2-Diphenylhydrazine
122-66-7
0.087
NA
Disulfoton
298-04-4
0.017
6.2
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
Ethyl acetate
141-78-6
0.34
33
Ethyl cyanide (Propane-
nitrile)
107-12-0
0.24
360
Ethyl benzene
100-41-4
0.057
10
Ethyl ether
60-29-7
0.12
160
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
462
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-8
0.0011
0.13
Methacrylonitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
NA
Methapyrilene
91-80-5
0.081
1.5
Methoxychlor
72-43-5
0.25
0.18
3-Methylcholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methyl methacrylate
80-62-6
0.14
160
Methyl methansulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
p-Nitroaniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
p-Nitrophenol
100-02-7
0.12
29
N-Nitrosodiethylamine
55-18-5
0.40
28
N-Nitrosodimethylamine
62-75-9
0.40
NA
N-Nitroso-di-n-butylamine
924-16-3
0.40
17
N-Nitrosomethylethylamine
10595-95-6
0.40
2.3
463
N-Nitrosomorpholine
59-89-2
0.40
2.3
N-Nitrosopiperidine
100-75-4
0.013
35
N-Nitrosopyrrolidine
930-55-2
0.013
35
Parathion
56-38-2
0.014
4.6
Total PCBs
(sum of all PCB isomers, or
all Aroclors)
1336-36-3
0.10
10
Pentachlorobenzene
608-93-5
0.055
10
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachloronitrobenzene
82-68-8
0.055
4.8
Pentachlorophenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Phorate
298-02-2
0.021
4.6
Phthalic anhydride
85-44-9
0.055
NA
Pronamide
23950-58-5
0.093
1.5
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
2,4,5-T
93-76-5
0.72
7.9
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Bromoform (Tribromo-
methane)
75-25-2
0.63
15
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane
75-69-4
0.020
30
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
464
1,2,3-Trichloropropane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-
trifluoroethane
76-13-1
0.057
30
tris(2,3-Dibromopropyl)
phosphate
126-72-7
0.11
NA
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers
(sum or of o-, m-, and p-
xylene concentrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
NA
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
NA
Fluoride
16964-48-8
35
NA
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
0.15
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
Sulfide
8496-25-8
14
NA
Thallium
7440-28-0
1.4
NA
Vanadium
7440-62-2
4.3
NA
K001
Bottom sediment sludge from the treatment of wastewaters from wood preserving processes
that use creosote or pentachlorophenol.
Naphthalene
91-20-3
0.059
5.6
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K002
Wastewater treatment sludge from the production of chrome yellow and orange pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
465
K003
Wastewater treatment sludge from the production of molybdate orange pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K004
Wastewater treatment sludge from the production of zinc yellow pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K005
Wastewater treatment sludge from the production of chrome green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
K006
Wastewater treatment sludge from the production of chrome oxide green pigments
(anhydrous).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K006
Wastewater treatment sludge from the production of chrome oxide green pigments (hydrated).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
K007
Wastewater treatment sludge from the production of iron blue pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
K008
Oven residue from the production of chrome oxide green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K009
Distillation bottoms from the production of acetaldehyde from ethylene.
Chloroform
67-66-3
0.046
6.0
K010
Distillation side cuts from the production of acetaldehyde from ethylene.
466
Chloroform
67-66-3
0.046
6.0
K011
Bottom stream from the wastewater stripper in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K013
Bottom stream from the acetonitrile column in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K014
Bottoms from the acetonitrile purification column in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
38
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K015
Still bottoms from the distillation of benzyl chloride.
Anthracene
120-12-7
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K016
Heavy ends or distillation residues from the production of carbon tetrachloride.
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
467
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
Hexachloroethane
67-72-1
0.055
30
Tetrachloroethylene
127-18-4
0.056
6.0
K017
Heavy ends (still bottoms) from the purification column in the production of epichlorohydrin.
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
1,2-Dichloropropane
78-87-5
0.85
18
1,2,3-Trichloropropane
96-18-4
0.85
30
K018
Heavy ends from the fractionation column in ethyl chloride production.
Chloroethane
75-00-3
0.27
6.0
Chloromethane
74-87-3
0.19
NA
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
NA
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K019
Heavy ends from the distillation of ethylene dichloride in ethylene dichloride production.
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
p-Dichlorobenzene
106-46-7
0.090
NA
1,2-Dichloroethane
107-06-2
0.21
6.0
Fluorene
86-73-7
0.059
NA
Hexachloroethane
67-72-1
0.055
30
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
NA
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K020
Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer production.
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
K021
Aqueous spent antimony catalyst waste from fluoromethanes production.
468
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
K022
Distillation bottom tars from the production of phenol or acetone from cumene.
Toluene
108-88-3
0.080
10
Acetophenone
96-86-2
0.010
9.7
Diphenylamine (difficult to
distinguish from diphenyl-
nitrosamine)
122-39-4
0.92
13
Diphenylnitrosamine
(difficult to distinguish from
diphenylamine)
86-30-6
0.92
13
Phenol
108-95-2
0.039
6.2
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K023
Distillation light ends from the production of phthalic anhydride from naphthalene.
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
85-44-9
0.055
28
K024
Distillation bottoms from the production of phthalic anhydride from naphthalene.
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
85-44-9
0.055
28
K025
Distillation bottoms from the production of nitrobenzene by the nitration of benzene.
NA
NA
LLEXT fb
SSTRP fb
CARBN; or
CMBST
CMBST
K026
Stripping still tails from the production of methyl ethyl pyridines.
469
NA
NA
CMBST
CMBST
K027
Centrifuge and distillation residues from the toluene diisocyanate production.
NA
NA
CARBN; or
CMBST
CMBST
K028
Spent catalyst from the hydrochlorinator reactor in the production of 1,1,1-trichloroethane.
1,1-Dichloroethane
75-34-3
0.059
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
NA
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Cadmium
7440-43-9
0.69
NA
Chromium(Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K029
Waste from the product steam stripper in the production of 1,1,1-trichloroethane.
Chloroform
67-66-3
0.046
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
K030
Column bodies or heavy ends from the combined production of trichloroethylene and
perchloroethylene.
o-Dichlorobenzene
95-50-1
0.088
NA
p-Dichlorobenzene
106-46-7
0.090
NA
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
NA
30
Pentachlorobenzene
608-93-5
NA
10
Pentachloroethane
76-01-7
NA
6.0
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
470
K031
By-product salts generated in the production of MSMA and cacodylic acid.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K032
Wastewater treatment sludge from the production of chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
Chlordane (alpha
α
and
gamma
χ
isomers)
57-74-9
0.0033
0.26
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
K033
Wastewater and scrub water from the chlorination of cyclopentadiene in the production of
chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K034
Filter solids from the filtration of hexachlorocyclopentadiene in the production of chlordane.
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K035
Wastewater treatment sludges generated in the production of creosote.
Acenaphthene
83-32-9
NA
3.4
Anthracene
120-12-7
NA
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from
p-cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from
m-cresol)
106-44-5
0.77
5.6
Dibenz(a,h)anthracene
53-70-3
NA
8.2
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
NA
3.4
Indeno(1,2,3-cd)pyrene
193-39-5
NA
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
471
K036
Still bottoms from toluene reclamation distillaiton in the production of disulfoton.
Disulfoton
298-04-4
0.017
6.2
K037
Wastewater treatment sludges from the production of disulfoton.
Disulfoton
298-04-4
0.017
6.2
Toluene
108-88-3
0.080
10
K038
Wastewater from the washing and stripping of phorate production.
Phorate
298-02-2
0.021
4.6
K039
Filter cake from the filtration of diethylphosphorodithioic acid in the production of phorate.
NA
NA
CARBN; or
CMBST
CMBST
K040
Wastewater treatment sludge from the production of phorate.
Phorate
298-02-2
0.021
4.6
K041
Wastewater treatment sludge from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K042
Heavy ends or distillation residues from the distillation of tetrachlorobenzene in the production
of 2,4,5-T.
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K043
2,6-Dichlorophenol waste from the production of 2,4-D.
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
187-65-0
0.044
14
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Pentachlorophenol
87-86-5
0.089
7.4
Tetrachloroethylene
127-18-4
0.056
6.0
HxCDDs (All Hexachloro-
NA
0.000063
0.001
472
dibenzo-p-dioxins)
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
K044
Wastewater treatment sludges from the manufacturing and processing of explosives.
NA
NA
DEACT
DEACT
K045
Spent carbon from the treatment of wastewater containing explosives.
NA
NA
DEACT
DEACT
K046
Wastewater treatment sludges from the manufacturing, formulation and loading of lead-based
initiating compounds.
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K047
Pink or red water from TNT operations.
NA
NA
DEACT
DEACT
K048
Dissolved air flotation (DAF) float from the petroleum refining industry.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-33
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
1330-20-7
0.32
30
473
concentrations)
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K049
Slop oil emulsion solids from the petroleum refining industry.
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Carbon disulfide
75-15-0
3.8
NA
Chrysene
2218-01-9
0.059
3.4
2,4-Dimethylphenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K050
Heat exchanger bundle cleaning sludge from the petroleum refining industry.
Benzo(a)pyrene
50-32-8
0.061
3.4
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K051
API separator sludge from the petroleum refining industry.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
474
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Chrysene
2218-01-9
0.059
3.4
Di-n-butyl phthalate
105-67-9
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K052
Tank bottoms (leaded) from the petroleum refining industry.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to distinguish from
p-cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to distinguish from
m-cresol)
106-44-5
0.77
5.6
2,4-Dimethylphenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K060
Ammonia still lime sludge from coking operations.
475
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
Naphthalene
91-20-3
0.059
5.6
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K061
Emission control dust or sludge from the primary production of steel in electric furnaces.
Antimony
7440-36-0
NA
2.1 mg/l TCLP
Arsenic
7440-38-2
NA
5.0 mg/l TCLP
Barium
7440-39-3
NA
7.6 mg/l TCLP
Beryllium
7440-41-7
NA
0.014 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
NA
0.16 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
Thallium
7440-28-0
NA
0.078 mg/l
TCLP
Zinc
7440-66-6
NA
5.3 mg/l TCLP
K062
Spent pickle liquor generated by steel finishing operations of facilities within the iron and steel
industry (SIC Codes 331 and 332).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
NA
K069
Emission control dust or sludge from secondary lead smelting. - Calcium sulfate (Low Lead)
Subcategory
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K069
Emission control dust or sludge from secondary lead smelting. - Non-Calcium sulfate (High
Lead) Subcategory
NA
NA
NA
RLEAD
K071
476
K071 (Brine purification muds from the mercury cell process in chlorine production, where
separately prepurified brine is not used) nonwastewaters that are residues from RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
K071
K071 (Brine purification muds from the mercury cell process in chlorine production, where
separately prepurified brine is not used) nonwastewaters that are not residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
K071
All K071 wastewaters.
Mercury
7439-97-6
0.15
NA
K073
Chlorinated hydrocarbon waste from the purification step of the diaphragm cell process using
graphite anodes in chlorine production.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachloroethane
67-72-1
0.055
30
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,1-Trichloroethane
71-55-6
0.054
6.0
K083
Distillation bottoms from aniline production.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
Cyclohexanone
108-94-1
0.36
NA
Diphenylamine
(difficult to distinguish from
diphenylnitrosamine)
122-39-4
0.92
13
Diphenylnitrosamine
(difficult to distinguish from
diphenylamine)
86-30-6
0.92
13
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K084
Wastewater treatment sludges generated during the production of veterinary pharmaceuticals
from arsenic or organo-arsenic compounds.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K085
Distillation or fractionation column bottoms from the production of chlorobenzenes.
477
Benzene
71-43-2
0.14
10
Chlorobenzene
108-90-7
0.057
6.0
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Total PCBs
(sum of all PCB isomers, or
all Aroclors)
1336-36-3
0.10
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K086
Solvent wastes and sludges, caustic washes and sludges, or water washes and sludges from
cleaning tubs and equipment used in the formulation of ink from pigments, driers, soaps, and
stabilizers containing chromium and lead.
Acetone
67-64-1
0.28
160
Acetophenone
96-86-2
0.010
9.7
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
n-Butyl alcohol
71-36-3
5.6
2.6
Butylbenzyl phthalate
85-68-7
0.017
28
Cyclohexanone
108-94-1
0.36
NA
o-Dichlorobenzene
95-50-1
0.088
6.0
Diethyl phthalate
84-66-2
0.20
28
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
Di-n-octyl phthalate
117-84-0
0.017
28
Ethyl acetate
141-78-6
0.34
33
Ethylbenzene
100-41-4
0.057
10
Methanol
67-56-1
5.6
NA
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methylene chloride
75-09-2
0.089
30
Naphthalene
91-20-3
0.059
5.6
Nitrobenzene
98-95-3
0.068
14
Toluene
108-88-3
0.080
10
1,1,1-Trichloroethane
71-55-6
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
0.37 mg/l TCLP
478
K087
Decanter tank tar sludge from coking operations.
Acenaphthylene
208-96-8
0.059
3.4
Benzene
71-43-2
0.14
10
Chrysene
218-01-9
0.059
3.4
Fluoranthene
206-44-0
0.068
3.4
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K088
Spent potliners from primary aluminum reduction.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
205-99-2
0.11
6.8
Benzo(k)fluoranthene
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Fluoranthene
206-44-0
0.068
3.4
Indeno(1,2,3-c,d)pyrene
193-39-5
0.0055
3.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
0.014 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
0.15
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
Cyanide (Total)
7
57-12-5
1.2
590
479
Cyanide (Amenable)
7
57-12-5
0.86
30
Fluoride
16984-48-8
35
48 mg/l TCLP
K093
Distillation light ends from the production of phthalic anhydride from ortho-xylene.
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
85-44-9
0.055
28
K094
Distillation bottoms from the production of phthalic anhydride from ortho-xylene.
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
85-44-9
0.055
28
K095
Distillation bottoms from the production of 1,1,1-trichloroethane.
Hexachloroethane
67-72-1
0.055
30
Pentachloroethane
76-01-7
0.055
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
K096
Heavy ends from the heavy ends column from the production of 1,1,1-trichloroethane.
m-Dichlorobenzene
541-73-1
0.036
6.0
Pentachloroethane
76-01-7
0.055
6.0
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-6
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
K097
Vacuum stripper discharge from the chlordane chlorinator in the production of chlordane.
Chlordane (alpha
α
and
57-74-9
0.0033
0.26
480
gamma
χ
isomers)
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
K098
Untreated process wastewater from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K099
Untreated wastewater from the production of 2,4-D.
2,4-Dichlorophenoxyacetic
acid
94-75-7
0.72
10
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
K100
Waste leaching solution from acid leaching of emission control dust or sludge from secondary
lead smelting.
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K101
Distillation tar residues from the distillation of aniline-based compounds in the production of
veterinary pharmaceuticals from arsenic or organo-arsenic compounds.
o-Nitroaniline
88-74-4
0.27
14
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
K102
Residue from the use of activated carbon for decolorization in the production of veterinary
pharmaceuticals from arsenic or organo-arsenic compounds.
481
o-Nitrophenol
88-75-5
0.028
13
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
K103
Process residues from aniline extraction from the production of aniline.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
2,4-Dinitrophenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
K104
Combined wastewater streams generated from nitrobenzene or aniline production.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
2,4-Dinitrophenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K105
Separated aqueous stream from the reactor product washing step in the production of chloro-
benzenes.
Benzene
71-43-2
0.14
10
Chlorobenzene
108-90-7
0.057
6.0
2-Chlorophenol
95-57-8
0.044
5.7
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Phenol
108-95-2
0.039
6.2
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine production)
nonwastewaters that contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine production)
nonwastewaters that contain less than 260 mg/kg total mercury that are residues from
RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
482
K106
Other K106 nonwastewaters that contain less than 260 mg/kg total mercury and are not
residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
K106
All K106 wastewaters.
Mercury
7439-97-6
0.15
NA
K107
Column bottoms from product separation from the production of 1,1-dimethylhydrazine
(UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K108
Condensed column overheads from product separation and condensed reactor vent gases from
the production of 1,1-dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K109
Spent filter cartridges from product purification from the production of 1,1-dimethylhydrazine
(UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K110
Condensed column overheads from intermediate separation from the production of 1,1-
dimethylhydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CMBST
483
CARBN
K111
Product washwaters from the production of dinitrotoluene via nitration of toluene
2,4-Dinitrotoluene
121-1-1
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
K112
Reaction by-product water from the drying column in the production of toluenediamine via
hydrogenation of dinitrotoluene.
NA
NA
CMBST; or
CHOXD fb
CARBN; or
BIODG fb
CARBN
CMBST
K113
Condensed liquid light ends from the purification of toluenediamine in the production of
toluenediamine via hydrogenation of dinitrotoluene.
NA
NA
CARBN; or
CMBST
CMBST
K114
Vicinals from the purification of toluenediamine in the production of toluenediamine via
hydrogenation of dinitrotoluene.
NA
NA
CARBN; or
CMBST
CMBST
K115
Heavy ends from the purification of toluenediamine in the production of toluenediamine via
hydrogenation of dinitrotoluene.
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
NA
NA
CARBN; or
CMBST
CMBST
K116
Organic condensate from the solvent recovery column in the production of toluene diisocyanate
via phosgenation of toluenediamine.
NA
NA
CARBN; or
CMBST
CMBST
K117
Wastewater from the reactor vent gas scrubber in the production of ethylene dibromide via
bromination of ethene.
Methyl bromide (Bromo-
74-83-9
0.11
15
484
methane)
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K118
Spent absorbent solids from purification of ethylene dibromide in the production of ethylene
dibromide via bromination of ethene.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K123
Process wastewater (including supernates, filtrates, and washwaters) from the production of
ethylenebisdithiocarbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K124
Reactor vent scrubber water from the production of ethylenebisdithiocarbamic acid and its
salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K125
Filtration, evaporation, and centrifugation solids from the production of ethylenebisdithio-
carbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
K126
Baghouse dust and floor sweepings in milling and packaging operations from the production or
formulation of ethylenebisdithiocarbamic acid and its salts.
NA
NA
CMBST; or
CHOXD fb
(BIODG or
CARBN)
CMBST
485
K131
Wastewater from the reactor and spent sulfuric acid from the acid dryer from the production of
methyl bromide.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
K132
Spent absorbent and wastewater separator solids from the production of methyl bromide.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
K136
Still bottoms from the purification of ethylene dibromide in the production of ethylene
dibromide via bromination of ethene.
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
Chloroform
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
K141
Process residues from the recovery of coal tar, including, but not limited to, collecting sump
residues from the production of coke or the recovery of coke by-products produced from coal.
This listing does not include K087 (decanter tank tar sludge from coking operations).
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-2-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K142
Tar storage tank residues from the production of coke from coal or from the recovery of coke
by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
205-99-2
0.11
6.8
486
benzo(k)fluoranthene)
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Ideno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K143
Process residues from the recovery of light oil, including, but not limited to, those generated
in stills, decanters, and wash oil recovery units from the recovery of coke by-products
produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
K144
Wastewater sump residues from light oil refining, including, but not limited to, intercepting or
contamination sump sludges from the recovery of coke by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
K145
Residues from naphthalene collection and recovery operations from the recovery of coke by-
products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
487
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Naphthalene
91-20-3
0.059
5.6
K147
Tar storage tank residues from coal tar refining.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K148
Residues from coal tar distillation, including, but not limited to, still bottoms.
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Indeno(1,2,3-cd)pyrene
193-39-5
0.0055
3.4
K149
Distillation bottoms from the production of alpha
α
- (or methyl-) chlorinated toluenes, ring-
chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these functional
groups. (This waste does not include still bottoms from the distillations of benzyl chloride.)
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Toluene
108-88-3
0.080
10
488
K150
Organic residuals, excluding spent carbon adsorbent, from the spent chlorine gas and hydro-
chloric acid recovery processes associated with the production of alpha
α
- (or methyl-)
chlorinated toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with
mixtures of these functional groups.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
p-Dichlorobenzene
106-46-7
0.090
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
1,1,2,2- Tetrachloroethane
79-34-5
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
1,2,4-Trichlorobenzene
120-82-1
0.055
19
K151
Wastewater treatment sludges, excluding neutralization and biological sludges, generated
during the treatment of wastewaters from the production of alpha
α
- (or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with mixtures of these
functional groups.
Benzene
71-43-2
0.14
10
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Hexachlorobenzene
118-74-1
0.055
10
Pentachlorobenzene
608-93-5
0.055
10
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
Tetrachloroethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
K156
Organic waste (including heavy ends, still bottoms, light ends, spent solvents, filtrates, and
decantates) from the production of carbamates and carbamoyl oximes. (This listing does not
apply to wastes generated from the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Acetonitrile
75-05-8
5.6
38
Acetophenone
96-86-2
0.010
9.7
Aniline
62-53-3
0.81
14
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbaryl
63-25-21
0.006
0.14
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
489
o-Dichlorobenzene
95-50-1
0.088
6.0
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Naphthalene
91-20-3
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyridine
110-86-1
0.014
16
Toluene
108-88-3
0.080
10
Triethylamine
121-44-8
0.081
1.5
K157
Wastewaters (including scrubber waters, condenser waters, washwaters, and separation waters)
from the production of carbamates and carbamoyl oximes. (This listing does not apply to
wastes generated from the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
o-Phenylenediamine
95-54-5
0.056
5.6
Pyridine
110-86-1
0.014
16
Triethylamine
121-44-8
0.081
1.5
K158
Baghouse dusts and filter/separation solids from the production of carbamates and carbamoyl
oximes. (This listing does not apply to wastes generated from the manufacture of 3-iodo-2-
propyl-n-butylcarbamate.)
10
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chloroform
67-66-3
0.046
6.0
Methylene chloride
75-09-2
0.089
30
Phenol
108-95-2
0.039
6.2
K159
Organics from the treatment of thiocarbamate wastes.
10
Benzene
71-43-2
0.14
10
Butylate
2008-41-5
0.042
1.4
EPTC (Eptam)
759-94-4
0.042
1.4
Molinate
2212-67-1
0.042
1.4
Pebulate
1114-71-2
0.042
1.4
Vernolate
1929-77-7
0.042
1.4
490
K161
Purification solids (including filtration, evaporation, and centrifugation solids), baghouse dust
and floor sweepings from the production of dithiocarbamate acids and their salts.
10
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.9
5.0 mg/l TCLP
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Dithiocarbamates (total)
NA
0.028
28
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P001
Warfarin, & salts, when present at concentrations greater than 0.3% percent
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P002
1-Acetyl-2-thiourea
1-Acetyl-2-thiourea
591-08-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P003
Acrolein
Acrolein
107-02-8
0.29
CMBST
P004
Aldrin
Aldrin
309-00-2
0.021
0.066
P005
Allyl alcohol
Allyl alcohol
107-18-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P006
Aluminum phosphide
Aluminum phosphide
20859-73-8
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
491
P007
5-Aminomethyl-3-isoxazolol
5-Aminomethyl-3-isoxazolol
2763-96-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P008
4-Aminopyridine
4-Aminopyridine
504-24-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P009
Ammonium picrate
Ammonium picrate
131-74-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P010
Arsenic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P011
Arsenic pentoxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P012
Arsenic trioxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P013
Barium cyanide
Barium
7440-39-3
NA
7.6 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P014
Thiophenol (Benzene thiol)
Thiophenol (Benzene thiol)
108-98-5
(WETOX or
CHOXD) fb
CMBST
492
CARBN; or
CMBST
P015
Beryllium dust
Beryllium
7440-41-7
RMETL;or
RTHRM
RMETL; or
RTHRM
P016
Dichloromethyl ether (Bis(chloromethyl)ether)
Dichloromethyl ether
542-88-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P017
Bromoacetone
Bromoacetone
598-31-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P018
Brucine
Brucine
357-57-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P020
2-sec-Butyl-4,6-dinitrophenol (Dinoseb)
2-sec-Butyl-4,6-dinitro-
phenol (Dinoseb)
88-85-7
0.066
2.5
P021
Calcium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P022
Carbon disulfide
Carbon disulfide
75-15-0
3.8
CMBST
Carbon disulfide; alternate
6
standard for nonwastewaters
only
75-15-0
NA
4.8 mg/l TCLP
493
P023
Chloroacetaldehyde
Chloroacetaldehyde
107-20-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P024
p-Chloroaniline
p-Chloroaniline
106-47-8
0.46
16
P026
1-(o-Chlorophenyl)thiourea
1-(o-Chlorophenyl)thiourea
5344-82-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P027
3-Chloropropionitrile
3-Chloropropionitrile
542-76-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P028
Benzyl chloride
Benzyl chloride
100-44-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P029
Copper cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P030
Cyanides (soluble salts and complexes)
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P031
Cyanogen
494
Cyanogen
460-19-5
CHOXD;
WETOX; or
CMBST
CHOXD;
WETOX; or
CMBST
P033
Cyanogen chloride
Cyanogen chloride
506-77-4
CHOXD;
WETOX; or
CMBST
CHOXD;
WETOX; or
CMBST
P034
2-Cyclohexyl-4,6-dinitrophenol
2-Cyclohexyl-4,6-dinitro-
phenol
131-89-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P036
Dichlorophenylarsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P037
Dieldrin
Dieldrin
60-57-1
0.017
0.13
P038
Diethylarsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P039
Disulfoton
Disulfoton
298-04-4
0.017
6.2
P040
O,O-Diethyl-O-pyrazinyl-phosphorothioate
O,O-Diethyl-O-pyrazinyl-
phosphorothioate
297-97-2
CARBN; or
CMBST
CMBST
P041
Diethyl-p-nitrophenyl phosphate
Diethyl-p-nitrophenyl
phosphate
311-45-5
CARBN; or
CMBST
CMBST
P042
Epinephrine
495
Epinephrine
51-43-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P043
Diisopropylfluorophosphate (DFP)
Diisopropylfluorophosphate
(DFP)
55-91-4
CARBN; or
CMBST
CMBST
P044
Dimethoate
Dimethoate
60-51-5
CARBN; or
CMBST
CMBST
P045
Thiofanox
Thiofanox
39196-18-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P046
alpha
α
,alpha
α
-Dimethylphenethylamine
alpha
α
,alpha
α
-Dimethyl-
phenethylamine
122-09-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P047
4,6-Dinitro-o-cresol
4,6-Dinitro-o-cresol
543-52-1
0.28
160
P047
4,6-Dinitro-o-cresol salts
NA
NA
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P048
2,4-Dinitrophenol
2,4-Dinitrophenol
51-28-5
0.12
160
P049
496
Dithiobiuret
Dithiobiuret
541-53-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P050
Endosulfan
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
P051
Endrin
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
P054
Aziridine
Aziridine
151-56-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P056
Fluorine
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb
NEUTR
P057
Fluoroacetamide
Fluoroacetamide
640-19-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P058
Fluoroacetic acid, sodium salt
Fluoroacetic acid, sodium
salt
62-74-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P059
Heptachlor
497
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
P060
Isodrin
Isodrin
465-73-6
0.021
0.066
P062
Hexaethyl tetraphosphate
Hexaethyl tetraphosphate
757-58-4
CARBN; or
CMBST
CMBST
P063
Hydrogen cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P064
Isocyanic acid, ethyl ester
Isocyanic acid, ethyl ester
624-83-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P065
P065 (mercury fulminate) nonwastewaters, regardless of their total mercury content, that are
not incinerator residues or are not residues from RMERC.
Mercury
7439-97-6
NA
IMERC
P065
P065 (mercury fulminate) nonwastewaters that are either incinerator residues or are residues
from RMERC; and contain greater than or equal to 260 mg/kg total mercury.
Mercury
7339-97-6
NA
RMERC
P065
P065 (mercury fulminate) nonwastewaters that are residues from RMERC and contain less
than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
P065
P065 (mercury fulminate) nonwastewaters that are incinerator residues and contain less than
260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
498
P065
All P065 (mercury fulminate) wastewaters.
Mercury
7439-97-6
0.15
NA
P066
Methomyl
Methomyl
16752-77-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P067
2-Methyl-aziridine
2-Methyl-aziridine
75-55-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P068
Methyl hydrazine
Methyl hydrazine
60-34-4
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED, or
CMBST
P069
2-Methyllactonitrile
2-Methyllactonitrile
75-86-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P070
Aldicarb
Aldicarb
116-06-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P071
Methyl parathion
Methyl parathion
298-00-0
0.014
4.6
P072
499
1-Naphthyl-2-thiourea
1-Naphthyl-2-thiourea
86-88-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P073
Nickel carbonyl
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
P074
Nickel cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
P075
Nicotine and salts
Nicotine and salts
54-11-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P076
Nitric oxide
Nitric oxide
10102-43-9
ADGAS
ADGAS
P077
p-Nitroaniline
p-Nitroaniline
100-01-6
0.028
28
P078
Nitrogen dioxide
Nitrogen dioxide
10102-44-0
ADGAS
ADGAS
P081
Nitroglycerin
Nitroglycerin
55-63-0
CHOXD;
CHRED;
CARBN; BIODG
or CMBST
CHOXD;
CHRED; or
CMBST
P082
N-Nitrosodimethylamine
N-Nitrosodimethylamine
62-75-9
0.40
2.3
500
P084
N-Nitrosomethylvinylamine
N-Nitrosomethylvinylamine
4549-40-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P085
Octamethylpyrophosphoramide
Octamethylpyrophosphor-
amide
152-16-9
CARBN; or
CMBST
CMBST
P087
Osmium tetroxide
Osmium tetroxide
20816-12-0
RMETL; or
RTHRM
RMETL; or
RTHRM
P088
Endothall
Endothall
145-73-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P089
Parathion
Parathion
56-38-2
0.014
4.6
P092
P092 (phenyl mercuric acetate) nonwastewaters, regardless of their total mercury content, that
are not incinerator residues or are not residues from RMERC.
Mercury
7439-97-6
NA
IMERC; or
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are either incinerator residues or are
residues from RMERC; and still contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are residues from RMERC and contain
less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
501
P092
P092 (phenyl mercuric acetate) nonwastewaters that are incinerator residues and contain less
than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
P092
All P092 (phenyl mercuric acetate) wastewaters.
Mercury
7439-97-6
0.15
NA
P093
Phenylthiourea
Phenylthiourea
103-85-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P094
Phorate
Phorate
298-02-2
0.021
4.6
P095
Phosgene
Phosgene
75-44-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P096
Phosphine
Phosphine
7803-51-2
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
P097
Famphur
Famphur
52-85-7
0.017
15
P098
Potassium cyanide.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P099
Potassium silver cyanide
502
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 mg/l TCLP
P101
Ethyl cyanide (Propanenitrile)
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
P102
Propargyl alcohol
Propargyl alcohol
107-19-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P103
Selenourea
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P104
Silver cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 mg/l TCLP
P105
Sodium azide
Sodium azide
26628-22-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P106
Sodium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P108
Strychnine and salts
Strychnine and salts
57-24-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
503
P109
Tetraethyldithiopyrophosphate
Tetraethyldithiopyro-
phosphate
3689-24-5
CARBN; or
CMBST
CMBST
P110
Tetraethyl lead
Lead
7439-92-1
0.69
0.37 mg/l TCLP
P111
Tetraethylpyrophosphate
Tetraethylpyrophosphate
107-49-3
CARBN; or
CMBST
CMBST
P112
Tetranitromethane
Tetranitromethane
509-14-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
P113
Thallic oxide
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P114
Thallium selenite
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P115
Thallium (I) sulfate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P116
Thiosemicarbazide
Thiosemicarbazide
79-19-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P118
504
Trichloromethanethiol
Trichloromethanethiol
75-70-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
P119
Ammonium vanadate
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P120
Vanadium pentoxide
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P121
Zinc cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P122
Zinc phosphide Zn
3
P
2
, when present at concentrations greater than 10% percent
Zinc Phosphide
1314-84-7
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
P123
Toxaphene
Toxaphene
8001-35-2
0.0095
2.6
P127
Carbofuran
10
Carbofuran
1563-66-2
0.006
0.14
P128
Mexacarbate
10
Mexacarbate
315-18-4
0.056
1.4
P185
Tirpate
10
Tirpate
26419-73-8
0.056
0.28
P188
Physostigimine salicylate
10
505
Physostigmine salicylate
57-64-7
0.056
1.4
P189
Carbosulfan
10
Carbosulfan
55285-14-8
0.028
1.4
P190
Metolcarb
10
Metolcarb
1129-41-5
0.056
1.4
P191
Dimetilan
10
Dimetilan
644-64-4
0.056
1.4
P192
Isolan
10
Isolan
119-38-0
0.056
1.4
P194
Oxamyl
10
Oxamyl
23135-22-0
0.056
0.28
P196
Manganese dimethyldithiocarbamates (total)
10
Dithiocarbamates (total)
NA
0.028
28
P197
Formparanate
10
Formparanate
17702-57-7
0.056
1.4
P198
Formetanate hydrochloride
10
Formetanate hydrochloride
23422-53-9
0.056
1.4
P199
Methiocarb
10
Methiocarb
2032-65-7
0.056
1.4
P201
Promecarb
10
Promecarb
2631-37-0
0.056
1.4
P202
m-Cumenyl methylcarbamate
10
m-Cumenyl methylcarbamate
64-00-6
0.056
1.4
506
P203
Aldicarb sulfone
10
Aldicarb sulfone
1646-88-4
0.056
0.28
P204
Physostigmine
10
Physostigmine
57-47-6
0.056
1.4
P205
Ziram
10
Dithiocarbamates (total)
NA
0.028
28
U001
Acetaldehyde
Acetaldehyde
75-07-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U002
Acetone
Acetone
67-64-1
0.28
160
U003
Acetonitrile
Acetonitrile
75-05-8
5.6
CMBST
Acetonitrile; alternate
6
standard for nonwastewaters
only
75-05-8
NA
38
U004
Acetophenone
Acetophenone
98-86-2
0.010
9.7
U005
2-Acetylaminofluorene
2-Acetylaminofluorene
53-96-3
0.059
140
U006
Acetyl chloride
Acetyl chloride
75-36-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
507
U007
Acrylamide
Acrylamide
79-06-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U008
Acrylic acid
Acrylic acid
79-10-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U009
Acrylonitrile
Acrylonitrile
107-13-1
0.24
84
U010
Mitomycin C
Mitomycin C
50-07-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U011
Amitrole
Amitrole
61-82-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U012
Aniline
Aniline
62-53-3
0.81
14
U014
Auramine
Auramine
492-80-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U015
Azaserine
508
Azaserine
115-02-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U016
Benz(c)acridine
Benz(c)acridine
225-51-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U017
Benzal chloride
Benzal chloride
98-87-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U018
Benz(a)anthracene
Benz(a)anthracene
56-55-3
0.059
3.4
U019
Benzene
Benzene
71-43-2
0.14
10
U020
Benzenesulfonyl chloride
Benzenesulfonyl chloride
98-09-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U021
Benzidine
Benzidine
92-87-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U022
Benzo(a)pyrene
Benzo(a)pyrene
50-32-8
0.061
3.4
509
U023
Benzotrichloride
Benzotrichloride
98-07-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U024
bis(2-Chloroethoxy)methane
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
U025
bis(2-Chloroethyl)ether
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
U026
Chlornaphazine
Chlornaphazine
494-03-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U027
bis(2-Chloroisopropyl)ether
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
U028
bis(2-Ethylhexyl)phthalate
bis(2-Ethylhexyl)phthalate
117-81-7
0.28
28
U029
Methyl bromide (Bromomethane)
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
U030
4-Bromophenyl phenyl ether
4-Bromophenyl phenyl ether
101-55-3
0.055
15
U031
n-Butyl alcohol
n-Butyl alcohol
71-36-3
5.6
2.6
U032
510
Calcium chromate
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
U033
Carbon oxyfluoride
Carbon oxyfluoride
353-50-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U034
Trichloroacetaldehyde (Chloral)
Trichloroacetaldehyde
(Chloral)
75-87-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U035
Chlorambucil
Chlorambucil
305-03-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U036
Chlordane
Chlordane (alpha
α
and
gamma
χ
isomers)
57-74-9
0.0033
0.26
U037
Chlorobenzene
Chlorobenzene
108-90-7
0.057
6.0
U038
Chlorobenzilate
Chlorobenzilate
510-15-6
0.10
CMBST
U039
p-Chloro-m-cresol
p-Chloro-m-cresol
59-50-7
0.018
14
U041
Epichlorohydrin (1-Chloro-2,3-epoxypropane)
Epichlorohydrin (1-Chloro-
2,3-epoxypropane)
106-89-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
511
CMBST
U042
2-Chloroethyl vinyl ether
2-Chloroethyl vinyl ether
110-75-8
0.062
CMBST
U043
Vinyl chloride
Vinyl chloride
75-01-4
0.27
6.0
U044
Chloroform
Chloroform
67-66-3
0.046
6.0
U045
Chloromethane (Methyl chloride)
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
U046
Chloromethyl methyl ether
Chloromethyl methyl ether
107-30-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U047
2-Chloronaphthalene
2-Chloronaphthalene
91-58-7
0.055
5.6
U048
2-Chlorophenol
2-Chlorophenol
95-57-8
0.044
5.7
U049
4-Chloro-o-toluidine hydrochloride
4-Chloro-o-toluidine hydro-
chloride
3165-93-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U050
Chrysene
Chrysene
218-01-9
0.059
3.4
512
U051
Creosote
Naphthalene
91-20-3
0.059
5.6
Pentachlorophenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U052
Cresols (Cresylic acid)
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to
distinguish from p-cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to
distinguish from m-cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers
(Cresylic acid)
(sum of o-, m-, and p-cresol
concentrations)
1319-77-3
0.88
11.2
U053
Crotonaldehyde
Crotonaldehyde
4170-30-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U055
Cumene
Cumene
98-82-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U056
Cyclohexane
Cyclohexane
110-82-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
513
U057
Cyclohexanone
Cyclohexanone
108-94-1
0.36
CMBST
Cyclohexanone; alternate
6
standard for nonwastewaters
only
108-94-1
NA
0.75 mg/l TCLP
U058
Cyclophosphamide
Cyclophosphamide
50-18-0
CARBN; or
CMBST
CMBST
U059
Daunomycin
Daunomycin
20830-81-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U060
DDD
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
U061
DDT
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
p,p’-DDE
72-55-9
0.031
0.087
U062
Diallate
Diallate
2303-16-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U063
Dibenz(a,h)anthracene
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
U064
Dibenz(a,i)pyrene
514
Dibenz(a,i)pyrene
189-55-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U066
1,2-Dibromo-3-chloropropane
1,2-Dibromo-3-chloro-
propane
96-12-8
0.11
15
U067
Ethylene dibromide (1,2-Dibromoethane)
Ethylene dibromide (1,2-
Dibromoethane)
106-93-4
0.028
15
U068
Dibromomethane
Dibromomethane
74-95-3
0.11
15
U069
Di-n-butyl phthalate
Di-n-butyl phthalate
84-74-2
0.057
28
U070
o-Dichlorobenzene
o-Dichlorobenzene
95-50-1
0.088
6.0
U071
m-Dichlorobenzene
m-Dichlorobenzene
541-73-1
0.036
6.0
U072
p-Dichlorobenzene
p-Dichlorobenzene
106-46-7
0.090
6.0
U073
3,3'-Dichlorobenzidine
3,3'-Dichlorobenzidine
91-94-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U074
1,4-Dichloro-2-butene
cis-1,4-Dichloro-2-butene
1476-11-5
(WETOX or
CMBST
515
CHOXD) fb
CARBN; or
CMBST
trans-1,4-Dichloro-2-butene
764-41-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U075
Dichlorodifluoromethane
Dichlorodifluoromethane
75-71-8
0.23
7.2
U076
1,1-Dichloroethane
1,1-Dichloroethane
75-34-3
0.059
6.0
U077
1,2-Dichloroethane
1,2-Dichloroethane
107-06-2
0.21
6.0
U078
1,1-Dichloroethylene
1,1-Dichloroethylene
75-35-4
0.025
6.0
U079
1,2-Dichloroethylene
trans-1,2-Dichloroethylene
156-60-5
0.054
30
U080
Methylene chloride
Methylene chloride
75-09-2
0.089
30
U081
2,4-Dichlorophenol
2,4-Dichlorophenol
120-83-2
0.044
14
U082
2,6-Dichlorophenol
2,6-Dichlorophenol
87-65-0
0.044
14
U083
1,2-Dichloropropane
1,2-Dichloropropane
78-87-5
0.85
18
U084
1,3-Dichloropropylene
516
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
U085
1,2:3,4-Diepoxybutane
1,2:3,4-Diepoxybutane
1464-53-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U086
N,N’-Diethylhydrazine
N,N’-Diethylhydrazine
1615-80-1
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U087
O,O-Diethyl-S-methyldithiophosphate
O,O-Diethyl-S-methyldithio-
phosphate
3288-58-2
CARBN; or
CMBST
CMBST
U088
Diethyl phthalate
Diethyl phthalate
84-66-2
0.20
28
U089
Diethyl stilbestrol
Diethyl stilbestrol
56-53-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U090
Dihydrosafrole
Dihydrosafrole
94-58-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U091
3,3'-Dimethoxybenzidine
3,3'-Dimethoxybenzidine
119-90-4
(WETOX or
CHOXD) fb
CMBST
517
CARBN; or
CMBST
U092
Dimethylamine
Dimethylamine
124-40-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U093
p-Dimethylaminoazobenzene
p-Dimethylaminoazobenzene
60-11-7
0.13
CMBST
U094
7,12-Dimethylbenz(a)anthracene
7,12-Dimethylbenz(a)-
anthracene
57-97-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U095
3,3'-Dimethylbenzidine
3,3'-Dimethylbenzidine
119-93-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U096
alpha
α
, alpha
α
-Dimethyl benzyl hydroperoxide
alpha
α
, alpha
α
-Dimethyl
benzyl hydroperoxide
80-15-9
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U097
Dimethylcarbamoyl chloride
Dimethylcarbamoyl chloride
79-44-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U098
1,1-Dimethylhydrazine
518
1,1-Dimethylhydrazine
57-14-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U099
1,2-Dimethylhydrazine
1,2-Dimethylhydrazine
540-73-8
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U101
2,4-Dimethylphenol
2,4-Dimethylphenol
105-67-9
0.036
14
U102
Dimethyl phthalate
Dimethyl phthalate
131-11-3
0.047
28
U103
Dimethyl sulfate
Dimethyl sulfate
77-78-1
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U105
2,4-Dinitrotoluene
2,4-Dinitrotoluene
121-14-2
0.32
140
U106
2,6-Dinitrotoluene
2,6-Dinitrotoluene
606-20-2
0.55
28
U107
Di-n-octyl phthalate
Di-n-octyl phthalate
117-84-0
0.017
28
U108
1,4-Dioxane
1,4-Dioxane
123-91-1
(WETOX or
CMBST
519
CHOXD) fb
CARBN; or
CMBST
1,4-Dioxane; alternate
6
standard for nonwastewaters
only
123-91-1
NA
170
U109
1,2-Diphenylhydrazine
1,2-Diphenylhydrazine
122-66-7
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
1,2-Diphenylhydrazine;
alternate
6
standard for
wastewaters only
122-66-7
0.087
NA
U110
Dipropylamine
Dipropylamine
142-84-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U111
Di-n-propylnitrosamine
Di-n-propylnitrosamine
621-64-7
0.40
14
U112
Ethyl acetate
Ethyl acetate
141-78-6
0.34
33
U113
Ethyl acrylate
Ethyl acrylate
140-88-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U114
Ethylenebisdithiocarbamic acid salts and esters
Ethylenebisdithiocarbamic
acid
111-54-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
520
CMBST
U115
Ethylene oxide
Ethylene oxide
75-21-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CHOXD; or
CMBST
Ethylene oxide; alternate
6
standard for wastewaters
only
75-21-8
0.12
NA
U116
Ethylene thiourea
Ethylene thiourea
96-45-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U117
Ethyl ether
Ethyl ether
60-29-7
0.12
160
U118
Ethyl methacrylate
Ethyl methacrylate
97-63-2
0.14
160
U119
Ethyl methane sulfonate
Ethyl methane sulfonate
62-50-0
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U120
Fluoranthene
Fluoranthene
206-44-0
0.068
3.4
U121
Trichloromonofluoromethane
Trichloromonofluoromethane
75-69-4
0.020
30
U122
Formaldehyde
Formaldehyde
50-00-0
(WETOX or
CMBST
521
CHOXD) fb
CARBN; or
CMBST
U123
Formic acid
Formic acid
64-18-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U124
Furan
Furan
110-00-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U125
Furfural
Furfural
98-01-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U126
Glycidylaldehyde
Glycidylaldehyde
765-34-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U127
Hexachlorobenzene
Hexachlorobenzene
118-74-1
0.055
10
U128
Hexachlorobutadiene
Hexachlorobutadiene
87-68-3
0.055
5.6
U129
Lindane
alpha
α
-BHC
319-84-6
0.00014
0.066
beta
β
-BHC
319-85-7
0.00014
0.066
delta
δ
-BHC
319-86-8
0.023
0.066
522
gamma
χ
-BHC (Lindane)
58-89-9
0.0017
0.066
U130
Hexachlorocyclopentadiene
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
U131
Hexachloroethane
Hexachloroethane
67-72-1
0.055
30
U132
Hexachlorophene
Hexachlorophene
70-30-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U133
Hydrazine
Hydrazine
302-01-2
CHOXD;
CHRED;
CARBN;
BIODG; or
CMBST
CHOXD;
CHRED; or
CMBST
U134
Hydrogen fluoride
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb
NEUTR; or
NEUTR
U135
Hydrogen sulfide
Hydrogen sulfide
7783-06-4
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U136
Cacodylic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
U137
Indeno(1,2,3-c,d)pyrene
Indeno(1,2,3-c,d)pyrene
193-39-5
0.0055
3.4
523
U138
Iodomethane
Iodomethane
74-88-4
0.19
65
U140
Isobutyl alcohol
Isobutyl alcohol
78-83-1
5.6
170
U141
Isosafrole
Isosafrole
120-58-1
0.081
2.6
U142
Kepone
Kepone
143-50-8
0.0011
0.13
U143
Lasiocarpine
Lasiocarpine
303-34-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U144
Lead acetate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U145
Lead phosphate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U146
Lead subacetate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U147
Maleic anhydride
Maleic anhydride
108-31-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U148
Maleic hydrazide
Maleic hydrazide
123-33-1
(WETOX or
CMBST
524
CHOXD) fb
CARBN; or
CMBST
U149
Malononitrile
Malononitrile
109-77-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U150
Melphalan
Melphalan
148-82-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U151
U151 (mercury) nonwastewaters that contain greater than or equal to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury and that are
residues from RMERC only.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury and that are
not residues from RMERC only.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
U151
All U151 (mercury) wastewater.
Mercury
7439-97-6
0.15
NA
U151
Element Mercury Contaminated with Radioactive Materials
Mercury
7439-97-6
NA
AMLGM
U152
Methacrylonitrile
Methacrylonitrile
126-98-7
0.24
84
525
U153
Methanethiol
Methanethiol
74-93-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U154
Methanol
Methanol
67-56-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
Methanol; alternate
6
set of
standards for both
wastewaters and
nonwastewaters
67-56-1
5.6
0.75 mg/l TCLP
U155
Methapyrilene
Methapyrilene
91-80-5
0.081
1.5
U156
Methyl chlorocarbonate
Methyl chlorocarbonate
79-22-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U157
3-Methylcholanthrene
3-Methylcholanthrene
56-49-5
0.0055
15
U158
4,4'-Methylene bis(2-chloroaniline)
4,4'-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
U159
Methyl ethyl ketone
Methyl ethyl ketone
78-93-3
0.28
36
U160
Methyl ethyl ketone peroxide
Methyl ethyl ketone peroxide
1338-23-4
CHOXD;
CHOXD;
526
CHRED;
CARBN;
BIODG; or
CMBST
CHRED; or
CMBST
U161
Methyl isobutyl ketone
Methyl isobutyl ketone
108-10-1
0.14
33
U162
Methyl methacrylate
Methyl methacrylate
80-62-6
0.14
160
U163
N-Methyl-N’-nitro-N-nitrosoguanidine
N-Methyl-N’-nitro-N-
nitrosoguanidine
70-25-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U164
Methylthiouracil
Methylthiouracil
56-04-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U165
Naphthalene
Naphthalene
91-20-3
0.059
5.6
U166
1,4-Naphthoquinone
1,4-Naphthoquinone
130-15-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U167
1-Naphthylamine
1-Naphthylamine
134-32-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
527
U168
2-Naphthylamine
2-Naphthylamine
91-59-8
0.52
CMBST
U169
Nitrobenzene
Nitrobenzene
98-95-3
0.068
14
U170
p-Nitrophenol
p-Nitrophenol
100-02-7
0.12
29
U171
2-Nitropropane
2-Nitropropane
79-46-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U172
N-Nitrosodi-n-butylamine
N-Nitrosodi-n-butylamine
924-16-3
0.40
17
U173
N-Nitrosodiethanolamine
N-Nitrosodiethanolamine
1116-54-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U174
N-Nitrosodiethylamine
N-Nitrosodiethylamine
55-18-5
0.40
28
U176
N-Nitroso-N-ethylurea
N-Nitroso-N-ethylurea
759-73-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U177
N-Nitroso-N-methylurea
N-Nitroso-N-methylurea
684-93-5
(WETOX or
CHOXD) fb
CMBST
528
CARBN; or
CMBST
U178
N-Nitroso-N-methylurethane
N-Nitroso-N-methylurethane
615-53-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U179
N-Nitrosopiperidine
N-Nitrosopiperidine
100-75-4
0.013
35
U180
N-Nitrosopyrrolidine
N-Nitrosopyrrolidine
930-55-2
0.013
35
U181
5-Nitro-o-toluidine
5-Nitro-o-toluidine
99-55-8
0.32
28
U182
Paraldehyde
Paraldehyde
123-63-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U183
Pentachlorobenzene
Pentachlorobenzene
608-93-5
0.055
10
U184
Pentachloroethane
Pentachloroethane
76-01-7
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
Pentachloroethane; alternate
6
standards for both
wastewaters and
nonwastewaters
76-01-7
0.055
6.0
U185
529
Pentachloronitrobenzene
Pentachloronitrobenzene
82-68-8
0.055
4.8
U186
1,3-Pentadiene
1,3-Pentadiene
504-60-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U187
Phenacetin
Phenacetin
62-44-2
0.081
16
U188
Phenol
Phenol
108-95-2
0.039
6.2
U189
Phosphorus sulfide
Phosphorus sulfide
1314-80-3
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U190
Phthalic anhydride
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic acid
or Terephthalic acid)
85-44-9
0.055
28
U191
2-Picoline
2-Picoline
109-06-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U192
Pronamide
Pronamide
23950-58-5
0.093
1.5
U193
530
1,3-Propane sultone
1,3-Propane sultone
1120-71-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U194
n-Propylamine
n-Propylamine
107-10-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U196
Pyridine
Pyridine
110-86-1
0.014
16
U197
p-Benzoquinone
p-Benzoquinone
106-51-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U200
Reserpine
Reserpine
50-55-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U201
Resorcinol
Resorcinol
108-46-3
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U202
Saccharin and salts
Saccharin
81-07-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
531
U203
Safrole
Safrole
94-59-7
0.081
22
U204
Selenium dioxide
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
U205
Selenium sulfide
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
U206
Streptozotocin
Streptozotocin
18883-66-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U207
1,2,4,5-Tetrachlorobenzene
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
U208
1,1,1,2-Tetrachloroethane
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
U209
1,1,2,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
79-34-5
0.057
6.0
U210
Tetrachloroethylene
Tetrachloroethylene
127-18-4
0.056
6.0
U211
Carbon tetrachloride
Carbon tetrachloride
56-23-5
0.057
6.0
U213
Tetrahydrofuran
Tetrahydrofuran
109-99-9
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
532
U214
Thallium (I) acetate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U215
Thallium (I) carbonate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U216
Thallium (I) chloride
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U217
Thallium (I) nitrate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U218
Thioacetamide
Thioacetamide
62-55-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U219
Thiourea
Thiourea
62-56-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U220
Toluene
Toluene
108-88-3
0.080
10
U221
Toluenediamine
Toluenediamine
25376-45-8
CARBN; or
CMBST
CMBST
U222
533
o-Toluidine hydrochloride
o-Toluidine hydrochloride
636-21-5
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U223
Toluene diisocyanate
Toluene diisocyanate
26471-62-5
CARBN; or
CMBST
CMBST
U225
Bromoform (Tribromomethane)
Bromoform (Tribromo-
methane)
75-25-2
0.63
15
U226
1,1,1-Trichloroethane
1,1,1-Trichloroethane
71-55-6
0.054
6.0
U227
1,1,2-Trichloroethane
1,1,2-Trichloroethane
79-00-5
0.054
6.0
U228
Trichloroethylene
Trichloroethylene
79-01-6
0.054
6.0
U234
1,3,5-Trinitrobenzene
1,3,5-Trinitrobenzene
99-35-4
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U235
tris-(2,3-Dibromopropyl)-phosphate
tris-(2,3-Dibromopropyl)-
phosphate
126-72-7
0.11
0.10
U236
Trypan Blue
Trypan Blue
72-57-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
534
CMBST
U237
Uracil mustard
Uracil mustard
66-75-1
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U238
Urethane (Ethyl carbamate)
Urethane (Ethyl carbamate)
51-79-6
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U239
Xylenes
Xylenes-mixed isomers
(sum of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
U240
2,4-D (2,4-Dichlorophenoxyacetic acid)
2,4-D (2,4-Dichloro-
phenoxyacetic acid)
94-75-7
0.72
10
2,4-D (2,4-Dichloro-
phenoxyacetic acid) salts and
esters
NA
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U243
Hexachloropropylene
Hexachloropropylene
1888-71-7
0.035
30
U244
Thiram
Thiram
137-26-8
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U246
Cyanogen bromide
Cyanogen bromide
506-68-3
CHOXD;
CHOXD;
535
WETOX; or
CMBST
WETOX; or
CMBST
U247
Methoxychlor
Methoxychlor
72-43-5
0.25
0.18
U248
Warfarin, & salts, when present at concentrations of 0.3% percent or less
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
CMBST
CMBST
U249
Zinc phosphide, Zn
3
P
2
, when present at concentrations of 10% percent or less
Zinc Phosphide
1314-84-7
CHOXD;
CHRED; or
CMBST
CHOXD;
CHRED; or
CMBST
U271
Benomyl
10
Benomyl
17804-35-2
0.056
1.4
U278
Bendiocarb
10
Bendiocarb
22781-23-3
0.056
1.4
U279
Carbaryl
10
Carbaryl
63-25-2
0.006
0.14
U280
Barban
10
Barban
101-27-9
0.056
1.4
U328
o-Toluidine
o-Toluidine
95-53-4
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
536
U353
p-Toluidine
p-Toluidine
106-49-0
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
U359
2-Ethoxyethanol
2-Ethoxyethanol
110-80-5
CMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb
CARBN
CMBST
U364
Bendiocarb phenol
10
Bendiocarb phenol
22961-82-6
0.056
1.4
U367
Carbofuran phenol
10
Carbofuran phenol
1563-38-8
0.056
1.4
U372
Carbendazim
10
Carbendazim
10605-21-7
0.056
1.4
U373
Propham
10
Propham
122-42-9
0.056
1.4
U387
Prosulfocarb
10
Prosulfocarb
52888-80-9
0.042
1.4
U389
Triallate
10
Triallate
2303-17-5
0.042
1.4
U394
A2213
10
A2213
30558-43-1
0.042
1.4
537
U395
Diethylene glycol, dicarbamate
10
Diethylene glycol,
dicarbamate
5952-26-1
0.056
1.4
U404
Triethylamine
10
Triethylamine
101-44-8
0.081
1.5
U409
Thiophanate-methyl
10
Thiophanate-methyl
23564-05-8
0.056
1.4
U410
Thiodicarb
10
Thiodicarb
59669-26-0
0.019
1.4
U411
Propoxur
10
Propoxur
114-26-1
0.056
1.4
Notes:
1
The waste descriptions provided in this table do not replace waste descriptions in 35 Ill.
Adm. Code 721. Descriptions of Treatment or Regulatory Subcategories are provided,
as needed, to distinguish between applicability of different standards.
2
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts or esters, the
CAS number is given for the parent compound only.
3
Concentration standards for wastewaters are expressed in mg/l and are based on
analysis of composite samples.
4
All treatment standards expressed as a Technology Code or combination of Technology
Codes are explained in detail in 35 Ill. Adm. Code 728.Table C, “Technology Codes
and Descriptions of Technology-Based Standards”. “fb” inserted between waste codes
denotes “followed by”, so that the first-listed treatment is followed by the second-listed
treatment. “;” separates alternative treatement treatment schemes.
5
Except for Metals (EP or TCLP) and Cyanides (Total and Amenable) the
nonwastewater treatment standards expressed as a concentration were established, in
part, based upon incineration in units operated in accordance with the technical
requirements of 35 Ill. Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O
538
or based upon combustion in fuel substitution units operating in accordance with
applicable technical requirements. A facility may comply with these treatment
standards according to provisions in 35 Ill. Adm. Code 728.140(d). All concentration
standards for nonwastewaters are based on analysis of grab samples.
6
Where an alternate treatment standard or set of alternate standards has been indicated, a
facility may comply with this alternate standard, but only for the Treatment or
Regulatory Subcategory or physical form (i.e., wastewater or nonwastewater) specified
for that alternate standard.
7
Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to be analyzed
using Method 9010 or 9012, found in “Test Methods for Evaluating Solid Waste,
Physical or Chemical Methods”, USEPA Publication SW-846, as incorporated by
reference in 35 Ill. Adm. Code 720.111, with a sample size of 10 grams and a
distillation time of one hour and 15 minutes.
8
These wastes, when rendered nonhazardous and then subsequently managed in CWA or
CWA-equivalent systems, are not subject to treatment standards. (See Section
728.101(c)(3) and (c)(4).)
9
These wastes, when rendered nonhazardous and then subsequently injected in a Class I
SDWA well, are not subject to treatment standards. (See 35 Ill. Adm. Code
738.101(d).)
10
This footnote corresponds with note 10 to the table to 40 CFR 268.40, which has
already expired by its own terms. This statement maintains structural consistency with
the federal regulations.
11 For these wastes, the definition of CMBST is limited to any of the following that have
obtained a determination of equivalent treatment under Section 728.142(b): (1)
combustion units operating under 35 Ill. Adm. Code 726, (2) combustion units
permitted under 35 Ill. Adm. Code 724.Subpart O, or (3) combustion units operating
under 35 Ill. Adm. Code 725.Subpart O.
BOARD NOTE: Derived from table to 40 CFR 268.40 (1997).
NA
means not applicable.
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
Section 728.Table U
Universal Treatment Standards (UTS)
Nonwastewater
Standard
Concentration (in
539
Regulated Constituent-
Common Name
CAS
1
No.
Wastewater
Standard
Concentration (in
mg/l
2
)
mg/kg
3
unless
noted as “mg/l
TCLP”)
A2213
6
30558-43-1
0.042
1.4
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
38
Acetophenone
96-86-2
0.010
9.7
2-Acetylaminofluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylamide
79-06-1
19
23
Acrylonitrile
107-13-1
0.24
84
Aldicarb sulfone
6
1646-88-4
0.056
0.28
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
alpha
α
-BHC
319-84-6
0.00014
0.066
beta
β
-BHC
319-85-7
0.00014
0.066
delta
δ
-BHC
319-86-8
0.023
0.066
gamma
χ
-BHC
58-89-9
0.0017
0.066
Barban
6
101-27-9
0.056
1.4
Bendiocarb
6
22781-23-3
0.056
1.4
Bendiocarb phenol
6
22961-82-6
0.056
1.4
Benomyl
6
17804-35-2
0.056
1.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
Benzene
71-43-2
0.14
10
Benzo(b)fluoranthene
(difficult to distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloromethane
75-27-4
0.35
15
Methyl bromide (Bromo-
methane)
74-83-9
0.11
15
4-Bromophenyl phenyl ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butylate
6
2008-41-5
0.042
1.4
540
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitro-
phenol (Dinoseb)
88-85-7
0.066
2.5
Carbaryl
6
63-25-2
0.006
0.14
Carbenzadim
6
10605-21-7
0.056
1.4
Carbofuran
6
1563-66-2
0.006
0.14
Carbofuran phenol
6
1563-38-8
0.056
1.4
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Carbon tetrachloride
56-23-5
0.057
6.0
Carbosulfan
6
55285-14-8
0.028
1.4
Chlordane (alpha
α
and
gamma
χ
isomers)
57-74-9
0.0033
0.26
p-Chloroaniline
106-47-8
0.46
16
Chlorobenzene
108-90-7
0.057
6.0
Chlorobenzilate
510-15-6
0.10
NA
2-Chloro-1,3-butadiene
126-99-8
0.057
0.28
Chlorodibromomethane
124-48-1
0.057
15
Chloroethane
75-00-3
0.27
6.0
bis(2-Chloroethoxy)methane
111-91-1
0.036
7.2
bis(2-Chloroethyl)ether
111-44-4
0.033
6.0
2-Chloroethyl vinyl ether
110-75-8
0.062
NA
Chloroform
67-66-3
0.046
6.0
bis(2-Chloroisopropyl)ether
39638-32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
Chloromethane (Methyl
chloride)
74-87-3
0.19
30
2-Chloronaphthalene
91-58-7
0.055
5.6
2-Chlorophenol
95-57-8
0.044
5.7
3-Chloropropylene
107-05-1
0.036
30
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to
distinguish from p-cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to
distinguish from m-cresol)
106-44-5
0.77
5.6
m-Cumenyl methyl
-
carbamate
6
64-00-6
0.056
1.4
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
o,p’-DDD
53-19-0
0.023
0.087
p,p’-DDD
72-54-8
0.023
0.087
o,p’-DDE
3424-82-6
0.031
0.087
p,p’-DDE
72-55-9
0.031
0.087
o,p’-DDT
789-02-6
0.0039
0.087
p,p’-DDT
50-29-3
0.0039
0.087
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
541
Dibenz(a,e)pyrene
192-65-4
0.061
NA
1,2-Dibromo-3-chloro-
propane
96-12-8
0.11
15
1,2-Dibromoethane/Ethylene
dibromide
106-93-4
0.028
15
Dibromomethane
74-95-3
0.11
15
m-Dichlorobenzene
541-73-1
0.036
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
p-Dichlorobenzene
106-46-7
0.090
6.0
Dichlorodifluoromethane
75-71-8
0.23
7.2
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
trans-1,2-Dichloroethylene
156-60-5
0.054
30
2,4-Dichlorophenol
120-83-2
0.044
14
2,6-Dichlorophenol
87-65-0
0.044
14
2,4-Dichlorophenoxyacetic
acid/2,4-D
94-75-7
0.72
10
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylene
10061-01-5
0.036
18
trans-1,3-Dichloropropylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethylene glycol,
dicarbamate
6
5952-26-1
0.056
1.4
Diethyl phthalate
84-66-2
0.20
28
p-Dimethylaminoazobenzene
60-11-7
0.13
NA
2,4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Dimetilan
6
644-64-4
0.056
1.4
Di-n-butyl phthalate
84-74-2
0.057
28
1,4-Dinitrobenzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitrophenol
51-28-5
0.12
160
2,4-Dinitrotoluene
121-14-2
0.32
140
2,6-Dinitrotoluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
Di-n-propylnitrosamine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
12.0
170
Diphenylamine (difficult to
distinguish from
diphenylnitrosamine)
122-39-4
0.92
13
Diphenylnitrosamine
(difficult to distinguish from
diphenylamine)
86-30-6
0.92
13
1,2-Diphenylhydrazine
122-66-7
0.087
NA
542
Disulfoton
298-04-4
0.017
6.2
Dithiocarbamates (total)
6
137-30-4
0.028
28
Endosulfan I
959-98-8
0.023
0.066
Endosulfan II
33213-65-9
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
EPTC
6
759-94-4
0.042
1.4
Ethyl acetate
141-78-6
0.34
33
Ethyl benzene
100-41-4
0.057
10
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
Ethyl ether
60-29-7
0.12
160
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
bis(2-Ethylhexyl) phthalate
117-81-7
0.28
28
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Formetanate hydrochloride
6
23422-53-9
0.056
1.4
Formparanate
6
17702-57-7
0.056
1.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachlorocyclopentadiene
77-47-4
0.057
2.4
HxCDDs (All Hexachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro-
dibenzofurans)
NA
0.000063
0.001
Hexachloroethane
67-72-1
0.055
30
Hexachloropropylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d) pyrene
193-39-5
0.0055
3.4
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isolan
6
119-38-0
0.056
1.4
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-0
0.0011
0.13
Methacrylonitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
0.75 mg/l TCLP
Methapyrilene
91-80-5
0.081
1.5
Methiocarb
6
2032-65-7
0.056
1.4
Methomyl
6
16752-77-5
0.028
0.14
Methoxychlor
72-43-5
0.25
0.18
543
3-Methylcholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-chloro-
aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methyl methacrylate
80-62-6
0.14
160
Methyl methansulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Metolcarb
6
1129-41-5
0.056
1.4
Mexacarbate
6
315-18-4
0.056
1.4
Molinate
6
2212-67-1
0.042
1.4
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
o-Nitroaniline
88-74-4
0.27
14
p-Nitroaniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
o-Nitrophenol
88-75-5
0.028
13
p-Nitrophenol
100-02-7
0.12
29
N-Nitrosodiethylamine
55-18-5
0.40
28
N-Nitrosodimethylamine
62-75-9
0.40
2.3
N-Nitroso-di-n-butylamine
924-16-3
0.40
17
N-Nitrosomethylethylamine
10595-95-6
0.40
2.3
N-Nitrosomorpholine
59-89-2
0.40
2.3
N-Nitrosopiperidine
100-75-4
0.013
35
N-Nitrosopyrrolidine
930-55-2
0.013
35
Oxamyl
6
23135-22-0
0.056
0.28
Parathion
56-38-2
0.014
4.6
Total PCBs (sum of all PCB
isomers, or all Aroclors)
1336-36-3
0.10
10
Pebulate
6
1114-71-2
0.042
1.4
Pentachlorobenzene
608-93-5
0.055
10
PeCDDs (All Pentachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro-
dibenzofurans)
NA
0.000035
0.001
Pentachloroethane
76-01-7
0.055
6.0
Pentachloronitrobenzene
82-68-8
0.055
4.8
Pentachlorophenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
o-Phenylenediamine
6
95-54-5
0.056
5.6
Phorate
298-02-2
0.021
4.6
544
Phthalic acid
100-21-0
0.055
28
Phthalic anhydride
85-44-9
0.055
28
Physostigmine
6
57-47-6
0.056
1.4
Physostigmine salicylate
6
57-64-7
0.056
1.4
Promecarb
6
2631-37-0
0.056
1.4
Pronamide
23950-58-5
0.093
1.5
Propham
6
122-42-9
0.056
1.4
Propoxur
6
114-26-1
0.056
1.4
Prosulfocarb
6
52888-80-9
0.042
1.4
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
1,2,4,5-Tetrachlorobenzene
95-94-3
0.055
14
TCDDs (All Tetrachloro-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro-
dibenzofurans)
NA
0.000063
0.001
1,1,1,2-Tetrachloroethane
630-20-6
0.057
6.0
1,1,2,2-Tetrachloroethane
79-34-5
0.057
6.0
Tetrachloroethylene
127-18-4
0.056
6.0
2,3,4,6-Tetrachlorophenol
58-90-2
0.030
7.4
Thiodicarb
6
59669-26-0
0.019
1.4
Thiophanate-methyl
6
23564-05-8
0.056
1.4
Tirpate
6
26419-73-8
0.056
0.28
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Triallate
6
2303-17-5
0.042
1.4
Tribromomethane
(Bromoform)
75-25-2
0.63
15
1,2,4-Trichlorobenzene
120-82-1
0.055
19
1,1,1-Trichloroethane
71-55-6
0.054
6.0
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Trichloromonofluoromethane
75-69-4
0.020
30
2,4,5-Trichlorophenol
95-95-4
0.18
7.4
2,4,6-Trichlorophenol
88-06-2
0.035
7.4
2,4,5-Trichlorophenoxy-
acetic acid/2,4,5-T
93-76-5
0.72
7.9
1,2,3-Trichloropropane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-
trifluoroethane
76-13-1
0.057
30
Triethylamine
6
101-44-8
0.081
1.5
tris-(2,3-Dibromopropyl)
phosphate
126-72-7
0.11
0.10
545
Vernolate
6
1929-77-7
0.042
1.4
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers (sum
of o-, m-, and p-xylene
concentrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
0.014 mg/l TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
4
57-12-5
1.2
590
Cyanides (Amenable)
4
57-12-5
0.86
30
Fluoride
5
16984-48-8
35
NA
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury-Nonwastewater
from Retort
7439-97-6
NA
0.20 mg/l TCLP
Mercury-All Others
7439-97-6
0.15
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
Sulfide
18496-25-8
14
NA
Thallium
7440-28-0
1.4
0.078 mg/l TCLP
Vanadium
5
7440-62-2
4.3
0.23 mg/l TCLP
Zinc
5
7440-66-6
2.61
5.3 mg/l TCLP
1
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts or esters, the
CAS number is given for the parent compound only.
2
Concentration standards for wastewaters are expressed in mg/l are based on analysis of
composite samples.
3
Except for metals (EP or TCLP) and cyanides (total and amenable), the nonwastewater
treatment standards expressed as a concentration were established, in part, based on
incineration in units operated in accordance with the technical requirements of 35 Ill.
Adm. Code 724.Subpart O or 35 Ill. Adm. Code 725.Subpart O or on combustion in
fuel substitution units operating in accordance with applicable technical requirements.
A facility may comply with these treatment standards according to provisions in 40
CFR 268.40(d). All concentration standards for nonwastewaters are based on analysis
of grab samples.
4
Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to be analyzed
using Method 9010 or 9012, found in “Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods”, USEPA Publication SW-846, incorporated by reference
546
in 35 Ill. Adm. Code 720.111, with a sample size of 10 grams and a distillation time of
one hour and 15 minutes.
5
These constituents are not “underlying hazardous constituents” in characteristic wastes,
according to the definition at Section 728.102(i).
6
This footnote corresponds with note 6 to the table to 40 CFR 268.48(a), which has
already expired by its own terms. This statement maintains structural consistency with
the federal regulations.
Note: NA means not applicable.
BOARD NOTE: Derived from table to 40 CFR 268.48(a) (1997).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER d: UNDERGROUND INJECTION CONTROL AND
UNDERGROUND STORAGE TANK PROGRAMS
PART 738
HAZARDOUS WASTE INJECTION RESTRICTIONS
SUBPART A: GENERAL
Section
738.101
Purpose, Scope, and Applicability
738.102
Definitions
738.103
Dilution Prohibited as a Substitute for Treatment
738.104
Case-by-Case Extensions of an Effective Date
738.105
Waste Analysis
SUBPART B: PROHIBITIONS ON INJECTION
Section
738.110
Waste Specific Prohibitions - Solvent Wastes
738.111
Waste Specific Prohibitions - Dioxin-Containing Wastes
738.112
Waste Specific Prohibitions - California List Wastes
738.114
Waste Specific Prohibitions - First Third Wastes
738.115
Waste Specific Prohibitions - Second Third Wastes
738.116
Waste Specific Prohibitions - Third Third Wastes
738.117
Waste-Specific Prohibitions - Newly-Listed Wastes
738.118
Waste-Specific Prohibitions - Newly-Listed and Identified Wastes
547
SUBPART C: PETITION STANDARDS AND PROCEDURES
Section
738.120
Petitions to Allow Injection of a Prohibited Waste
738.121
Required Information to Support Petitions
738.122
Submission, Review and Approval or Denial of Petitions
738.123
Review of Adjusted Standards
738.124
Termination of Adjusted Standards
AUTHORITY: Implementing Sections 13 and 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
SOURCE: Adopted in R89-2 at 14 Ill. Reg. 3059, effective February 20, 1990; amended in R89-11 at 14
Ill.
Reg. 11948, effective July 9, 1990; amended in R90-14 at 15 Ill. Reg. 11425, effective July 24, 1991; amended in
R92-13 at 17 Ill. Reg. 6190, effective April 5, 1993; amended in R93-6 at 17 Ill. Reg. 15641, effective September
14, 1993; amended in R95-4 at 19 Ill. Reg. 9501, effective June 27, 1995; amended in R96-10/R97-3/R97-5 at
22 Ill. Reg. 238, effective December 16, 1997; amended in R97-21/R98-3/R98-5 at 22 Ill. Reg. ________,
effective ______________________.
SUBPART A: GENERAL
Section 738.101
Purpose, Scope, and Applicability
a)
This Part identifies hazardous wastes that are restricted from disposal into Class
I wells and defines those circumstances under which a waste, otherwise
prohibited from injection, may be injected.
b)
The requirements of this Part apply to owners or operators of the following
Class I wells:
1)
Hazardous waste injection wells that are used to inject hazardous waste;
and
2)
Injection wells that are used to inject wastes which once exhibited a
prohibited characteristic of hazardous waste identified in 35 Ill. Adm.
Code 721.Subpart C, at the point of generation, and which no longer
exhibit the characteristic at the point of injection.
c)
Wastes otherwise prohibited from injection may continue to be injected:
1)
If an extension from the effective date of a prohibition has been granted
pursuant to Section 738.104; or
2)
If an adjusted standard has been granted in response to a petition filed
under Section 738.120; or
548
3)
If the waste is generated by a conditionally exempt small quantity
generator, as defined in 35 Ill. Adm. Code 721.105.
d)
A waste that is hazardous only because it exhibits a characteristic of hazardous
waste and which is otherwise prohibited from injection under this Part or 35 Ill.
Adm. Code 728 is not prohibited from injection if the following is true of the
waste:
1)
It is disposed into a non-hazardous or hazardous waste injection well, as
defined under 35 Ill. Adm. Code 730.106(a); and
2)
It does not exhibit any prohibited characteristic of hazardous waste
identified in 35 Ill. Adm. Code 721.Subpart C at the point of injection.
BOARD NOTE: Derived from 40 CFR 148.1 (1996).
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
SUBPART B: PROHIBITIONS ON INJECTION
Section 738.118
Waste-Specific Prohibitions - Newly-Listed and Identified Wastes
a) Effective August 11, 1997, the wastes specified in 35 Ill. Adm. Code 721 as
USEPA hazardous waste numbers F032, F034, F035 are prohibited from
underground injection.
b) Effective May 12, 1999, the wastes specified in 35 Ill. Adm. Code 721 as
USEPA hazardous waste numbers F032, F034, F035 that are mixed with
radioactive wastes are prohibited from underground injection.
ac)
The wastes specified in 35 Ill. Adm. Code 721.132 as having the following
USEPA hazardous waste numbers are prohibited from underground injection:
K156
K157
K158
K159
K160
K161
P127
P128
P185
P188
P189
549
P190
P191
P192
P194
P196
P197
P198
P199
P201
P202
P203
P204
P205
U271
U277
U278
U279
U280
U364
U365
U366
U367
U372
U373
U375
U376
U377
U378
U379
U381
U382
U383
U384
U385
U386
U387
U389
U390
U391
U392
U393
U394
U395
U396
U400
550
U401
U402
U403
U404
U407
U409
U410
U411
bd)
The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA hazardous waste
number K088 is prohibited from underground injection.
ce)
On April 8, 1998, tThe wastes specified in 35 Ill. Adm. Code 721 as having the
following USEPA hazardous waste numbers and Mixed TC/Radioactive wastes
are prohibited from underground injection:
D018
D019
D020
D021
D022
D023
D024
D025
D026
D027
D028
D029
D030
D031
D032
D033
D034
D035
D036
D037
D038
D039
D040
D041
D042
D043
551
df)
On April 8, 1998, tThe wastes specified in 35 Ill. Adm. Code 721 as having the
following USEPA hazardous waste numbers are prohibited from underground
injection:
D001
D002
D003
(Source: Amended at 22 Ill. Reg. ________, effective ______________________)
