)
ILLINOIS ENVIRONMENTAL PROTECTION AGENCY
2009 MALL STREET, COLLINSVILLE, ILLINOIS 62234
THOMAS V. SKINNER, DIRECTOR
618/346-5120
FAX:
618/346-5155
CERTIFIED MAIL #7099 3400 0002
6815
3463
November 2, 2000
RETURN RECEIPT REQUESTED
Prior Oil Company
Attn: John Prior
140 Gompers Street
Wamac, Illinois 62801
Re:
Violation Notice, L-2000-01302
#1894925001
--
Washington County
Prior Oil Company
Compliance File
Dear Mr. Prior:
This constitutes a Violation Notice pursuant to Section 31 (a)(1) ofthe Illinois Environmental
Protection Act, 415 ILCS 5/31 (a)( 1), and is based upon an inspection completed on August 22,
2000 by a representative ofthe Illinois Environmental Protection Agency (“Illinois EPA”).
The Illinois EPA hereby provides notice ofviolations ofenvironmental statutes, regulations, or
permits as set forth in Attachment A to this letter. Attachment A includes an explanation ofthe
activities that the Illinois EPA believes may resolve the specified violations, including an estimate
ofa reasonable time period to complete the necessary activities. Due to the nature and
seriousness ofthe violations cited, please be advised that resolution ofthe violations may require
the involvement of a prosecutorial authority for purposes that may include, among others, the
imposition ofstatutory penalties.
A written response, which may include a request for a meeting with representatives ofthe Illinois
EPA, must be submitted via certified mail to the Illinois EPA within 45 days ofreceipt ofthis
letter. The response must address each violation specified in Attachment A and include for each
an explanation ofthe activities that will be implemented and the time schedule for the completion
ofthat activity. The written response will constitute a proposed Compliance Commitment
Agreement (“CCA”) pursuant to Section 31 ofthe Act. The Illinois EPA will review the proposed
CCA and will accept or reject it within 30 days ofreceipt.
Ifa timely written response to this Violation Notice is not provided, it shall be considered to be a
waiver of the opportunity to respond and to meet and the Illinois EPA may proceed with a referral
to the prosecutorial authority.
PEOPLE’S
EXHIBIT
3
‘~.
cc )r’.
21-’. ,-~
I
p.
#1894925001-- Washington County
Prior Oil Company
Page 2
Written communications should be directed to:
Illinois EPA
Attn: Kenneth Mensing
2009 Mall Street
Collinsville, Illinois 62234
All communications must include reference to this
VIOLATION NOTICE NUMBER, L-2000-
01302.
Questions regarding this matter should be directed to
CHRIS CAHNOVSKY at 618/346-5120.
Sincerely,
Kenneth G. Mensing
Regional Manager
Bureau of Land
KGM:CNC:cas
Attachment
bcc: BOL
-
Records Unit
bcc: DLC
-
Chris Perzan
bcc: DLC
-
Todd Retting
bce: BOL
-
Collinsville
1894925001
--
Washington County
Prior Oil Company
ATTACHMENT A
Pursuant
to Section 21(a) ofthe Illinois Environmental Protection Act (415 ILCS
5/21(a)), no person shall cause or allowthe open dumping ofany waste.
A violation of Section 2 1(a) ofthe Illinois Environmental Protection Act (415 ILCS
5/21(a)) is alleged for the following
reason: Evidence of open dumping ofwaste was
observed during the inspections.
2.
Pursuant to Section 21(d) ofthe Illinois Environmental Protection Act (415 ILCS
5/21(d)), no person shall conduct any waste-storage, waste-treatment, or waste-disposal
operation:
1.
Without a permit granted by the Agency or in violation of any conditions imposed
by such permit, including periodic reports and full access to adequate records and
the inspection of facilities, as may be necessary to assure compliance with this Act
and with regulations and standards adopted thereunder...
2.
In violation ofany regulations or standards adopted by the Board under this Act.
This subsection (d) shall not apply to hazardous waste.
A violation of Section 21(d) ofthe Illinois Environmental Protection Act (415 ILCS
5/21(d)) is alleged forthe following reason: Waste was disposed
without a permit
granted
by
the Illinois EPA.
3.
Pursuant to Section 21(e) ofthe Illinois Environmental Protection Act (415 ILCS
5/21(e)), no person shall dispose, treat, store or abandon any waste, or transport any waste
into this State for disposal, treatment, storage or abandonment, except at a site or facility
which meets the requirements of this Act and of regulations and standards thereunder.
A violation of Section 2 1(e) of the Illinois Environmental Protection Act (415 ILCS
5/21(e)) is alleged forthe following reason: Waste was disposed at this site
which
does
not meet the requirements of the Act and regulations thereunder.
1894925001 --Washington County
Prior Oil Company
Page 2 of 4
4.
Pursuant to Section 21QD)(1) &
(6)
ofthe Illinois Environmental Protection Act (415
ILCS 5/21(p)), no person shall, in violation ofsubdivision (a) ofthis Section21, cause
or allow the open dumping ofany waste in a manner which results in litter and standing
or flowing liquid discharge from the dump site.
The prohibitions specified in this subsection (p) shall be enforceable by the Agency either
by administrative citation under Section 31.1 ofthis Act or as otherwise provided by this
Act. The specific prohibitions in this subsection do not limit the power ofthe Board to
establish regulations or standards applicable to open dumping.
A violation of Section 2l(~)(l)&
(6)
ofthe Illinois Environmental Protection Act (415
ILCS 5/21QD)(l) & (6) is alleged forthe following reason: Evidence of
open dumping
ofwaste was observed during the inspections. Liquid crude oil was observed in a
pit on Prior Oil Company’s property.
5.
Pursuant to 35 Ill. Adm. Code 722.111, a person who generates a solid waste, as defined
in Section 721.102, must determine if that waste is a hazardous waste using the following
method:
a)
The person should first determine if the waste is excluded from regulation under
35
Ill. Adm. Code 721.104.
b)
The person should then determine if the waste is listed as a hazardous waste in 35
Ill. Adm. Code 72l.SubpartD.
Board Note: Even if a waste is listed, the generator still has an opportunity under 35 Ill.
Adm. Code 720.122 to demonstrate that the waste from the generator’s particular facility
or operation is not a hazardous waste.
c)
For purposes ofcompliance with 35 Ill. Adm. Code 728, or if the waste is not
listed as a hazardous waste in 35 Ill. Adm. Code 721 .Subpart D the generator shall
then determine whether the waste is identified in 35 Ill. Adm. Code 721 .Subpart C
by either:
1894925001
--
Washington County
-
Prior Oil Company
-
Page3of4
1)
Testing the waste according to the methods set forth in 35 Ill. Adm. Code
721.Subpart C, or according to an equivalent method approved by the
Board under 35 Ill. Adm. Code 720.121; or
2)
Applying knowledge ofthe hazard characteristic ofthe waste in light of
the materials or the processes used.
d)
Ifthe generator determines that the waste is hazardous, the generator shall refer to
35 Ill. Adm. Code 724, 725 and 728 for possible exclusions or restrictions
pertaining to the management ofthe specific waste.
A violation of35 Ill. Adm. Code 722.111 is alleged forthe following reason:
Prior Oil
Company failed to make a hazardous waste determination ofthe
two
drums ofused
oil on the side of the southwest side of the shop.
6.
Pursuant to 35 Ill. Adm. Code 739.122(c), containers and aboveground tanks used to
store used oil at generator facilities must, be labeled with the words “Used Oil”.
A viOlation of 35 Ill. Adm. Code 739.122(c) is alleged for the following reason:
Prior
Oil Company failed to label the
two
drums of
used oil
on the southwest
side of the
shop with the words “Used Oil”.
7.
Pursuant to 35 Ill. Adm. Code 739.122(d), upon detection ofa release ofused oil to the
environment, a generator shall perform the following cleanup steps:
1)
Stop the release;
2)
Contain the released used oil;
3.)
Clean up and properly manage the released used oil and other material; and
4)
Ifnecessary, prevent further releases, repair or replace any leaking used oil
storage containers or tanks prior returning them to service.
A violation of35 Ill. Adm. Code 739.122(d) is alleged for the following reason: Oil was
observed
on the ground around the two drums ofused oil on the southwest side of
the Shop.
8.
Pursuant to 35 Ill. Adm. Code 808.12 1(a), Each person who generates waste shall
determine whether the waste is a special waste.
A violation of 35 Ill. Adm. Code 808.12 1(a) is alleged for the following reason: Prior
Oil Company failed to make
a special waste determination of
the
two
drums of
used
oil on the side ofthe southwest side ofthe shop.
1894925001 --Washington County
Prior Oil Company
Page 4 of 4
SUGGESTED RESOLUTIONS
1.
IMMEDIATELY cease all open dumping.
2.
IMMEDIATELY label all containers of used oil with the words “Used Oil.”
3.
IMMEDIATELY begin cleaning up the released oil from the
two
drums of used oil
on the southwest side of the shop. The oil contaminated soil must be taken to a
permitted landfill. A special waste manifest must be used to accompany the load to
the landfill.
4.
By December 14, 2000 submit what steps Prior Oil Company has taken to clean up
the crude oil in the pit. Once this waste is no longer a liquid, it may be disposed of
as a special waste in a permitted landfill. A special waste manifest must be used to
accompany the load to the landfill.
5.
By December 14, 2000 conduct a hazardous waste determination ofthe
two
drums
of used oil on the southwest side ofthe shop. This determination must at a
minimum consist of an analysis for flash point (SW846 Method 1010).
6.
All waste must be removed from the site by December 14, 2000.
The written response to this Violation Notice must include information in rebuttal,
explanation, or justification of each alleged violation. The written response must also
include a proposed Compliance Commitment Agreement that commits to specific remedial
actions, includes specified times for achieving each commitment, and may include a
statement that compliance has been achieved.
ILLINOIS
ENVIRONMENTAL PROTECTION AGENCY
Open- Dump Inspection Checklist
County: - Washington
-
Location/Site Name:
Prior Oil Company
Date:
August 22,
2000
Inspector(s):
Chris Cahnovsky
No. of Photos
Taken: #
13
Interviewed:
John Prior
To
13:00
Weather:
Region:
Collinsville
Previous Inspection Date:
82°Fhot
20
yds3
Samples Taken:
Yes#
X
Complaint #:
- Responsible Party
- “Mailing Address(es)
and Phone Number(s):
Prior Oil Company
John Prior
140 Gompers Street
Wamac, Illinois 62801
SECTION
DESCRIPTION
VIOL.
I
ILLINOIS ENVIRONMENTAL PROTECTION ACT REQUIREMENTS
I
1.
9(a)
CAUSE, THREATEN OR ALLOW AIR POLLUTION IN ILLINOIS
2.
9(c)
CAUSE OR ALLOW OPEN BURNING
3.
12(a)
CAUSE, THREATEN OR ALLOW WATER POLLUTION IN ILLINOIS
4.
12(d)
CREATE A WATER POLLUTION HAZARD
5.
21(a)
CAUSE OR ALLOW OPEN DUMPING
21(d)
CONDUCT
ANY WASTE-STORAGE, WASTE-TREATMENT,
OR WASTE- DISPOSAL
OPERATION:
(1)
Without a Permit
(2)
In Violation of Any Regulations or Standards Adopted by the Board
. -
7.
21(e)
DISPOSE, TREAT, STORE, OR ABANDON ANY WASTE, OR TRANSPORT ANY
WASTE INTO THE STATE AT/TO SITES NOT MEETING REQUIREMENTS OF
ACT AND REGULATIONS
21(p)
CAUSE OR ALLOW THE OPEN DUMPING OF ANY WASTE IN A MANNER WHICH RESULTS
IN
ANY OF THE FOLLOWING OCCURRENCES AT THE DUMP SITE:
‘
(1)
(2)
(3)
(4)
(5)
Litter
Scavenging
Open Burning
.
NUII
Deposition of Waste in Standing or Flowing Waters
6200,9
Proliferation of Disease Vectors
x
‘
(6)
(7)
Standing or Flowing Liguid Discharge from the Dump Site
DemolitionDeposition Debrisof
General Construction or Demolition Debris; or Clean
R1E~~~A
y
(Open Dump - 1)
BLE1
NO\’ 2 2 2000
REV~EWER
MD
LPC#:
1894925001
Time:
From
12:00
Est.
Amt. of Waste:
No
6.
8.
•PC#: 1894925001 --WASHINGTON COUNTY
Inspection Date: 08/22/2000
9.
55(a)
NO PERSON SHALL:
(1)
Cause or Allow Open Dumping of Any Used or Waste Tire
~2)
Cause or Allow Open Burning of Any Used or Waste Tire
35 ILLINOIS ADMINISTRATIVE CODE REQUIREMENTS
SUBTITLE G
II
10.
812.101(a)
FAILURE TO SUBMIT
AN APPLICATION
FOR
A PERMIT
TO DEVELOP AND
OPERATE
A
LANDFILL
11.
722.111
HAZARDOUS WASTE DETERMINATION
12.
808.121
SPECIAL
WASTE
DETERMINATION
13.
809.302(a)
ACCEPTANCE OF SPECIAL WASTE FROM A WASTE TRANSPORTER
WITHOUT A WASTE HAULING PERMIT, UNIFORM WASTE PROGRAM
I
I REGISTRATION AND PERMIT AND/OR MANIFEST
I
I
OTHER REQUIREMENTS
14.
APPARENT VIOLATION OF:
( )
PCB;
( )
CIRCUIT COURT
CASE NUMBER:
-
ORDER ENTERED ON:
15.
739.122(c)
-
CONTAINERS
USED TO STORE USED OIL MUST BE LABELED WITH THE
WORDS “USED OIL”
739.122(d)
UPON DETECTION OF A
GENERATOR SHALL PE
SUBSECTION
RELEASE OF USED OIL TO THE ENVIRONMENT, A
RFORM CLEANUP STEP PROVIDED IN THIS’
‘
p1~f~atureof Inspector(s)
Informational Notes
V
1.
Illinois Environmental Protection Act:’415 ILCS 5/4.
2.
Illinois Pollution Control Board: 35 III. Adm. Code, Subtitle G.
3.
Statutory and regulatory references herein are provided forconvenience only and should not be construed as legal
conclusions
ofthe Agency or as limiting the Agency’s statutory or regulatory powers. Requirements of some statutes
and regulations cited are in summary format. Full text of requirements can be found in references listed in 1. and 2.
above:
4. The provisions of subsection (p) of Section 21 of the Illinois Environmental Protection Act shall be enforceable either
by administrative citation under Section 31.1 of the Act or by complaint under Section 31 of the Act.
5. This inspection was conducted in accordance with Sections 4(c) and 4(d) of the Illinois Environmental Protection Act:
415
ILCS
514(c)and(d).
6.
Items marked with an “NE” were not evaluated at the time of this inspection.
7.
Statutory effective date: through 7/9/99.
8. Regulatory effective date: through 5/20/99.
(Open Dump -2)
1~94925001
--
Washington County
Prior
Oil Company
Date of Inspection: August 22, 29 and 31, 2000
Prepared by: Chris Cahnovsky
NARRATIVE
On August 22, 2000, while investigating an unrelated complaint in Wamac, Illinois, I entered
• property owned by John Prior, .Pri~rOil Company. This property is at 140 Gompers Street and is
the location ofPrior Oil Company’s office, shop and equipment storage. I entered the property
from a field to the north. I observed a large pit containing waste and an oily liquid. This pit was
25 feet long by 10 feetwide by about seven feet deep. The pit contained an old BBQ grill, car
-
parts, plastic containers, paint cans, cloths, used oil absorbent pads and landscape waste. In the
pit I observed a large amount ofoil. I observed oil pooled on the bottom ofthe pit and oil
‘coating the side walls ofthe pit. There was a large concentration ofoil in the deepest part ofthe
pit covering an area about seven feetby ten feet.
I proceeded to the office and met Mr. John Prior. Mr. Prior and I walked back to the pit. I asked
Mr. Prior what he knows about the pit and the oil in the pit. He stated he had no idea, none. He
went on to say the he does not know who put the waste in the pit. He stated he did not know the
pit was there. I asked if this was crude oil. Mr. Prior stated that he does not think it is crude
oil
because it is too black. Mr. Prior claimed that one ofthe neighbors orHarold Alexander dumped
the oil on his property.
-
Mr. Prior said he would immediately begin cleaning
up
the pit. I stated that the waste must be
dug out and taken
to a
landfill. Mr. Prior wanted to begin the removal the next day. I stated that
he may want to wait until I have a chance to sample the oil in the pit. He claimed that he is about
to sell his tractor and will not have access to it anymore so he wanted to begin right away. I told
him I wanted to be present for the removal. We arranged to meet at the site at 9:00 a.m. on
August 24, 2000.
Tom Miller and I returned to this site on August 23, 2000 to obtain a sample ofthe oil in the pit.
-
No one representing Prior Oil Company was present during this sampling inspection. The
sample was labeled X201. I observed that the pool of oil in the pit was about eight to ten inches
deep and had a kerosine like odor.
-
Sample X201 was taken using a 32-ounce glass jar. The sample was placed into two 2-ounce,
one 32-ounce and one 9-ounce glass jar. The sample was placed in a cooler of “blue ice” and
transported to the Collinsville Regional Office. In Collinsville, the samples were sealed with
evidence tape and repacked for shipment to the JEPA’s Springfield Organics laboratory. The
requested analysis were flash point, PCB, TCLP volatile organics and TCLP semi-volatile
organics. A request was also made to compare the sample against crude oil standards to
determine ifthe oil was crude oil or used motor oil.
A/ri
0~fl~
iv~4’jj
FZ:~
6
200ü
1894925001
--
Washington County
Prior Oil Company
Page2of2
On August 24, 2000, Mr. Prior called to inform me that he would not be able to remove the
waste because the area had received an inch ofrain overnight. He said he would call me when he
would begin excavation. John Senjan and Ireturned to the site on August 29, 2000. The pit has
remained unchanged since my August 22, 2000, inspection. I spoke with Mr. Prior during this
inspection and he told me he would begin excavation on August 31, 2000. He also told me that
he had the pit dug over one month ago to bury concrete. I did not observe any concrete in the
ditch.
Mr. Prior called me on August 30, 2000 and told me that he had dug out the ditch yesterday and
today. He stated that he had the equipment and the manpower on hand and did the work. I asked
ifthe waste was still on-site. Mr. Prior stated that it was still on-site in a lined roll-offbox. I
told Mr. Prior that I had received some preliminary lab results and that the material in the box
may be a hazardous waste. I explained that he should not move the box until I received all ofthe
analysis back from the lab. He agreed not to move the box until I had the lab results.
On August 31, 2000, I conducted an inspection at this site. No one was present. I observed that
the waste had been removed from the pit. I observed a 20-yd3 roll off-box ofoily contaminated
dirt. The box was on the back ofa truck. The name on the side ofthe truck was H&H Ship
Service Co. San Francisco, CA USDOT 193737.
On the southwest side ofthe shop, I observed two 30-gallon drums ofused oil. Neither drum
was labeled used oil. Also, a large amount of oil was observed on the top ofthe drums and on
the ground around the drums. I went in the office and informed Prior Oil employee, Jenni
Dining, that the oil drums were leaking and the released oil must be cleaned up. I told her that
the oil contaminated soil could probably go into the roll-offbox ofoil contaminated soil. She
stated she would tell the guys in the shop.
The Collinsville Office received the laboratory ‘results of October 27, 2000. The laboratory
report for the oil in the pit shows that the oil appears to match the pattern ofcrude oil and not
usedmotor oil. Pursuant to 35 Ill. Adm. Code 721.104(b)(5) drilling fluids, produced water and
other waste associated with the exploration, development or production ofcrude oil are solid
wastes. This oily waste in the pit would also meet the definition of special waste.
SUMMARY OF APPARENT VIOLATIONS
1.
21(a)
-
causing or allowing the open dumping ofwaste.
2.
21(d)
-
disposing of waste with out a permit
3.
2 1(e)
-
disposing of waste at a site that is not in compliance
4.
21 (p)(1)(6)
-
open dumping and standing liquid discharge from a dump site.
5.
722.111
-
Haz determination of used oil by the shop
6.
808.12 1(a)
-
Special waste determination of the used oil by the shop
7.
739.122(c)
-
no label on drums of used oil
8.
739.122(d)
-
used oil on ground
‘S
THE ENVIRONMENTAL PROTECTION AGENCY
DIVISION OF LAND POLLUTION
RECEIPT FOR SAMPLES
Site Enventory #:
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Facility Name:
Federal I.D. #:
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County:
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Indicated #
Sample #:
of Bottles
Date Collected
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Duplicate Samples requested: /~ / Yes
No
-
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Date
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Date
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Rece~ t for s pies listed ove is reby acknowledged.’
~~
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Title
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Agency resentative
Title
COMMENTS:
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NOTE:
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Division File
Yellow Copy
-
Regions
Pink Copy
-
Owner/Operator/Agent
GS : TH: lhh : AC-XI
IL 532—1752
LPC 3fl9 12/88
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(Analysis Request and Receipt for Samples)
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ID#
Page
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Proj~ctManager’s Name/Address/Phone #:
(~/ti-~c
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2125 S. 1st Street
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Champaign, IL 61820, 217/278-5858
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Receipt
for
Samples: Collection of the above-listed samplets) at the indicated
site
is hereby ackn~e~~d.
Signature/Title
of Facility Representative. Date
IL
532-2311
LPC 525
Rev. ‘5/2000
Wfir6i~i
PL~L0~
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825 N. Rutledge Stre
Springfield,
IL 62702, 21
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Date
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-_______________________________
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ORGANIC BOilERS
CONSTITUENT
Alhaliolty
315.2’
At,aoinrrm
200.7’
Ammonia-Nit.
300.1
Antimony
Arsenic
Barium
200.7’
Beryllium
200.7’
Boron
200.7’
Carlmium
200.7’
Calcium
200.7’
Chloride
525.2’
Chenmiuer
2507r
Cobalt
2007’
Copper
200.7’
Cyaeide
335.4’
Fluoride
432705’
l-la,doesu
200.72
line
200.7’
Lead
0
Magnesium
200.7’
Macgoode
200.7’
Mercury
245.1’
Nickel
200.7’
NitriteiNitrate
305.2’
pH
150.1’
Flreools .
420.4’
Phouphomu
365.1’
Pnladium
200.7’
Selenium
$
Silver
200.7’
Sodioer
200.7’
Op.
Coud.
—
Struetinni
200.7’
Sulfate
375.2’
Sulfide
—
Thallium
~o5/go5
160.1’
TOO
—
TOC
—
Vauadiuur
200.7’
11cc
200.7’
$200.8’ foe cleaner
-
saesples; 200.9’ Se’
more concentrated
oues.
56020 fur cleaner
samples;
indicated
method for mule
coecentrared ones.
‘EPA 600/4-79.020
‘EPA 6001R-94/t
lt~
‘USGS
310.2’
601
GA
300.1’
57041
57060
601 GA
hOtGA
uGtOA
6OIOA
601 GA
9251
hOtGA
6GtGA
hOtOA
901 GA
432705’
601 GA
07421
601 CA
601 GA
747GA
601 GA
305.2’
0040A
9066
365.1’
64-IDA
57740
hOtGA
6OtGA
0050
6O1OA
$036
G7e4t
160.1’
601 GA
605GA
310.2’
601 GA
350.1’
0704t
07060
603 GA
6OSGA
601 GA
60 ISA
GOlDA
$253
603 GA
602 SA
601 GA
432705’
6GtGA
07421
6010A
601 GA
7470A
6GtGA
353.2’
365.t’
6GIGA
07740
6GSOA
6GtOA
601 GA
0036
3704t
6G30A
6010A
310.2’
200.7’
350.1’
200.7’
200.7’
250.7’
200.7’
200.7’
325.2’
200.7’
200.7’
200.7’
335.4’
432705’
200.7’
200.7’
200.7’
200.7’
245.1’
200.7’
303.2’
I
50•.i’
420.4’
360.1’
20.7’
200.7’
200.71
120.3’
200.7’
3/5.2’
376.1’
160.1’
160.2’
410.5’
200.7’
250.7’
TOTL1
TOTI2
-
10T13
TOTL4
6G1GA
1,2,3,4
57043
3, 2, 3, 4
$7060
t,2,3,4
6G1GA
1,2,3,4
6SIGA
1,2,3,4
6OtGA
1,2,3,4
6$IGA
1,2,5,4
6O1GA
1,2,3,4
6G1GA
1,2,3,4
GOlDA
1,2,3,4
6OtOA
1, 2, 3. 4
$0i$A
3,4
GOlDA
1,2,3,4
07421
1,2,3,4
6G1GA
1,2,3,4
6G1GA
1,2,3,4
7470-lA
1,2,3,4
6GIGA
1,2,3,4
$040A
3,4
0066
5.
4
6OIGA -
1.2,3,4
07740
1,2,3,4
6O1GA
1,2,3-4
6G3GA
1,2,3,4
6OtOA
1,2,3,4
9531
3,4
07841
1,2,3,4
9060
5,4
6G1GA
1,2,3,4
SGIOA
1,2,3,4
N,ru,heos
0—4
correupned to grolrps
7011.1 through
70114.
For enample,
1011.0 cuolaint all
c000tituerso 1653 hone
a 1 tilled ahee them,
70712 containsall
c000titueetsmirh a 2
listed after thom. etc.
TCLPI
TCLP2
07041
5756$
601 GA
6510A
601
GA
601 GA
37423
7,70.ru•
6035,’,
OG4OA
*7740
601 GA
37841
GO1GA
sour
60
lanOod
,Srr,
rim,
“ale”
by
4
Jediuaud
nethnd
‘Meex~y
is 7470A
for
aqueous,
7473 A
foroxo-
aqlre000.
VOC
Vohule, by CC/ND
FoPosueed tub,,,
Medrod 8260
(sole, 0035)
00d,hi,0 Water subset by
CC
Method 0Ô2..2’
l,l.DietrloroethAoe
PD
t,t,2,2-T,snohloroetbA,e
D
t,l,2-Trichlorueth.Aee
D
l.l,l.Trfuhtoroed,Aee
PD
I,I,l,2-Teoruclslure,d,ueo 0 oely
I,2-Diohtorobemeee
-~
D oo$y
l,2-OichlueoprupAoe
D
I.2.3-TriuhlmmpropAoe
.0
L1,4.Teiehlorubeeue,r,
0 ecly
l.9-DiuhloropropAoe
0
t,3-Diohlorobeeoene
0 cob’
1,1 -DiuhtoroprupEne
0
l,2.Diohloreert,Aoe
PD
t,l-Diohleromhploee
0
I,4.Oiohlorobeocerse
0 oety
2,2-OichloropropAoe
0
2’ChloroethpMeyl Ether
2-Neuaeoee (P18K)
4-Nethyl-S’peomoeue (P118K)
Ao,tuoo
Ben,,,,
F
Rremob,nuen,
0
Bremochturomedraee
bromofurm
0
Bromomethu,e
0
Garbo, Tecruohloride
PD
Corhoe Ohu$ide
Chlorobeooe,e
0
Chlerodibromume,fraoe
0
Chloroedraee
0
Chtoruloem
FO
Chteromethuoe
0
Cis.l,2-Diohloeeodq4ee,
FO
Ch-l.3’Diohloropropeee
0
Dlheomo,eesho,,
0
Dichlorohromame,frae,
0
Bthp7oeraeee
PD
toopropplbeeoeet
Methyl Ethyl Ke,oee
Nethpteee Chloride
PD
lo1re,e
-
FO
Tetraclstoroethytdro
PD
Iota,,,
PD
True,-
l,2-Diohloroethyt,e,
0
Trues.I,3.Didsloropropeoe
0
Triohloroethylese
FO
Triutrlorofuurome,haee
Vieyf Chloride
PD
Visyl
Acetate
Xyleso
FO
‘EPA 505-eerie,i
Methods forthe Derermioadoeof
Orgaoio Cumpooodt is Dfoldeg
Wuter, Supplemeos1,11,
and Ill
OVOC
Semioulsole, byGCJMS
PuPoua,ed subset
Method8270
l,2-Disisrohee,eee
Bersoo(b(fluoracctheee
P
l.2.4,$-Teteueldurobeooeee
E.eou(C$41)perylese
t.4-Dmitrubesoe,re
Beoao(b(fuerautheoe
P
t,3-Dieiwobemeue
Beecoic Add
L2’.Ouyhis-t.chlueuprspuse
Reouyt Alcohol
2.3.4,6-Teenchloropheool
Bis (2’ethylheu5l) Phthatate
F
4-Chlorophruq4pheoylethee
Si,
(l’obtorneobyl) Ether
4-Nhrohipheoy$
Si, (2.shloreethooy( Metfrioe
S-Ni,eo-e.solcddioe
Bisji.sNoroisopropyl( Ether
7,t2-Dimothylbenoo(o(sothraoese
Buoy$ Beooyl
Phthubte
F
t.2,4-Triohlorobee,e,e
Chryteee
F
t,4-Diohlorobeeoee,
F
Di.mbutylphthahte
l,3-Dichlorobee,eoe
F
Dus-uotylphthalate
I ,2-Diuhlorobeeaeoe
F
Dlheooo(AH(eethraeeee
2,4-Diekrntoleeee
Diheecofuro,
F
2.4.Oirhlurepheool
Disthytphthatete
P
2,4.Dieiorepheool
Dimethylphthalate
2,6-Dioitretuluece
Ethybesoruoosullurca,e
2.4-Dimethplpheoot
Floeraethene
P
2.4.6.Tr-icfrloeophmsot
Pluoeorm
-
F
2.4.l.Trirhtorophtool
Heoasbtorober,aeee
2-CNoeumphthuleoe
H,uuohtorohoradieee
2-Chloropheool
Neuuoldorooydopenmdieoe
2.Nethyleophthaleoe
F
Heuuchtoroethueo
2’N.thylpheool
P
Heuaohtoro~cro~erm
2.Niomaeliee
ledeeo(t,2,3.C0)Fyreee
2.Nitropheoel
Ituphorose
3,3’-Oiohlerober,xidiue
lsotuffrol,
3-Nhreuetiee
Ntthylmetlraoesuffooute
4.0-Oiohrn-2-methylpheoot
e-Nitrosu-di-e-propylamiee
4-Brnmophesytphteylsther
o-Nhrusupiperideeo
4-Chloro-3-methplpheonl
o-Aeiddiee
4.ChluroooGe,
o-Tulaidis,
4-Chluropheoyl Fheoyl
Ether
Naphthuleoe
F
4-Nedqlphooot
F
Niseohee,eoe
4-Nitroao3ioe
-
Feetashluropheoul
4-Nisroptreool
Feeruchlorosdorohemeee
Aceouphthpleoe
F
Fheoaoetiee
-
Aoeooptheoe
F
Fheosothreee
F
AoetuFheeoee
-
Fhdrul
-
F
Antheuoeoe
2’PiooGee
Ermo(e)aolhraoese
-
F
Fyreno
-
-
F
Seneu(o(Fyreoe
P
-
53CC
FCC 53CC
53CC/CC
553CC
FCC 553CC
PESTIECD’
FCC FESTIRCO’
PEST/NPC’
FCC FRSTINPO’
FCB’
HE6E/ECC
TCXAPHONE
TCLP53CC
TCLF *53CC
TCLF FEST
TCLF HOER
FUEL 10
NFLC FNA (TACO)
FLASH
FAIHTFILTEP,
pH
Esolssooes:
‘Per the
uleanem
sample. sullen,2
extra bottles for
QAJQC
BuGle Oescriptioot:
(All or-,gtuss enseps
EeCore’
I
‘4$ ml obl, poly-
peupyleoe sup mith
Tefno-hoed SOon,
Septum. S drops 55
HCI
‘80 no ~t
I gallon,
polypropylene tap
mhleftnn O’er
‘2cc, polypropylene
cap mile$uol’user
‘B eo. polypropylene
sap milefosliner
.16
no,pulyprupyleoo
sap ‘rdleflooO’er
‘02
us, putypropylsot
sap m/TeflmsGoer
‘Sg
tathms
polymer
GnCore
tube
Netrie Cunoertiem
40mb
1.30 ox
-
Test
Buotlet Required thyMatrisl
Waterj
e~a
).wr
(2(40
ml
vlul,’+hlanh
(3) EnCore’ tubes -
(t(200
(ur
(2)40mt
eiul,’-sbluoh
(3) EnCore’ tubes
(l(2tcefur
(2)40ml s$uls’+blurdu
MIA
NIA
(l)B0uobessler~
(l(Bou(urc
(l(Boz(ur
(1)05 on bomle”
(1)600
(or’
(1(5on pr
(t(800ehomle’-’
(l(Soofur’
(l(Rntfur
(l)BGunbotde”
(l(Ouefur’
(l)Boepr
(I)Bouohu,de’-’
(l(Bocfur’
(h(Boofur
(I(BSoohomle’-’
(l(800(ur’
(l)Buofsr
(l(Bsuehosde’-’
(l(Boc(urc
- (IfBoofur
(I) 0* uc beede”
(l)Boofur’
- (l(But(ur
(1)8500 botde’-’
(t( Boo (ur’
-
(1(8 uo pr
- (4(40 ml ehl,’+ bbob
(B)
EnCore’ tubes
(2)200 (or’ -
(l(BSoohettle’-’
(l)Ooo(ur’
(f)Bnt(ur-
(l(Boooheede”
(l)Boe(ar’
‘
(l)000far
(f)000ebeedeM
.(l)Oun(ur’
-
(l)600(or
(l)BGocbemle’
(t)Boo(or’
(t(Buefur
(t)B000hnrsk’
(l(Bon(or’
HIA
N/A
N/A
(l(Boe(or
-
t’fllA
(l)Oon(or
(I)Suo(sr
Any Coominer
Aey Coeruiner
Aey Ceotaiser
‘Nuuheum
of 2
‘Nauimum of
2 tents
‘PEST/EGO.
eutrunoines
from (I)
from (1(800 fuIc-
PESTINFD, &
-
BGoo hoed,
Collect eon-u (or or
sun be
rue
fro
-
use 16 oe
(or
fur
eusruueioo.
more
shoe2 tools.
-
-
Assigoleg Meld
Sorface Waler S
Numbers
I
—
Upslream
-
-
2
—
Mid-Site
-
G,oundmul,e C
S — Oomuotmam
-
0/I/Alpha
u Noeitor
4
— Rue-off
weo
S — tmpouoded
-
2
=
Priua,e Well
6 —
R,ut’ne
-
3
0 Spring
40 Lysimeter
Special S
5
=
Public Water
I
v
Suit
Supply
2
0
Wars,
GO
Eeroeerp
Well
3 u
Other
7
=
Io(estiue
Welt
0 0
Reconery Trreoh
Roamples:
TOT1OW,G
ClOluNo&Wef
Somple
leachule I.
)OSWWuson Sumplt
-
0 P1cm or leap
L201=Leastsaoe
Peed
2
=
Peed
Sample
3
0
Colleudoe Syttem
030 luoomettream
Sample
INORGANIC PARAMETER GROUP CEOCRIPTIONS
OTHER TROTS
INORGANIC EOTGLES
PESTIRCO
PESTINPO
OTHER TEOTO
-
Brief Inslructions for Ehe Choin of CusEody Docunser
-
Euudoe Pesdsides/ HerhMdea by
Roudee Pe,doid,slHerhisid,e by
PWELU Pdrale mellu, total hrrorgaidcs. BullIes, Cyaeide. Metals IS ool, Nrtdrett,
EOD (32 00) —400.1’
CYANIDR, Bo,
PR.
1.2$ ml
Eleosrun Capture Detector
Nitrogen Phosphorout Detersor
TarVDc—I3Il.eluo
1.Do cot mdte in any areau totally shaded
is
gray.
Theue are POE L
Phenol, Unprrsereed 116 GuI Total nolome,
44
ox.
TEJRBIOITI (00 ml(
—
SN MaCH
oxuted tubtes
PuPueused ,,,h,ec
~
USE ONLY. lAceas fur which (poe
of) theheadiog
is shaded hol the,
GWICT, Gruuedmalero,uuitudeg melt,, total iuorgauics, Eutlles, Cyanide,
Metals
180.1’
MBTAL$~32oo PG,20ml
Method BOBIA
MethodBI4IA
Tar
ext shaded ARE iate,rded for F CS lowdIe in; lbs
uhaded heading he
132 uzl,
Nutrieots, Pheeol, Unprrsgsved 116 xxi Tulal volume:
66oc.
pH (50
ml) — $G4GA’
SOS HNO,
Ahehlor
-
P
A,rocioe
I4Ee.R—ItrlsBIsIl,
esetelo aleOs the lab to iupu~dorahum this urea
GWDIO: Grosiodmater moiriloring mdl,, dissoloed ionrgaeics. Bottirt, Metals $32 oN.
OP. CONDLICTANCE
METALS: Bee FE
Aldrin
Ruuylate
P
PCB—ROB2
2. Complete form heading i,rfurosatieo, iodicate funding cede, conry
Nutrients, Unpretemed 116 oil. Total volume: S2oz.
-
-
(55 ml(
—9050’
NIJTRIBNTS,4 00 FE. 120 ml
Atraaine
P
Chlnrpyrdos
P
pH—9040A
file
heading, indicate pre(ecs manager
head
sunryler, who needs to
SURPW; Surface matew aod leachale Ilomu and seeps, lutal rnorgaorcs. BullIes,
SF. CMVIII (32 oo(
—
20 N5SC,
a.BHC
-
Diaorooo
P
PLASHPCINT—l0IO
receive the resuttsh bole, addre,,, and phuoe ounrher, circle or mdl’
Cyonide, Metals ISGel. Nurdrets, Phenol, Sulfide, Unpreuewed 164 oil. Total
0129667’
PHENOL:6 ouglust, 1.8 ml
‘y-EHC (Uoduon(
EPIC
-
PAIHTMLTER—9595
receideg laboratoryinlornralion, and indicale case number if Ibis is
volume, 122 00.
-
20 P1,00,
-
Cupmn
--
Peeufu,
-
FURL 10—1601
cdnli,ral innestigatioo.
bILl: Aqonuos
waules, mautemalrw & leachate culleOit,n system samples, total
Euo
frees
ospeesoreed PR
SULFIDE 32an P5,2 ml 2N
o’Chlorduee
P
Matathios
~
S. In ceturrrn heading areas ,rnder ‘Parameter Group and orher aeuly
metals. Eotlleu, Melalu 132 oul. 10101 volume, 32 ox.
-
boml,u; volume required
Zu(C,N,C,(1H,C
- y.Chlordae,
P
Methyl Paruthioo
P
Sperral Fetnu,des
-
lisr he p000reter grulrps or efher lesIs which mill he req,,esred.
30T12: Waste, sell, sedimei,l, sludge, and organic matrices,lural metals. Bottles,
listed after test
‘aloe
UNPRESERVED, 16.32, or 64
Cyaoaxioe
F
Phnru,e
-
(requett by peseoide
l’Pucoted’ Orgar~icuare furscreenieg purposru ouly, cot
Glass boltle 136 eel from Syeingfield Lahoratosy(. 10101 volume, lb uo.
os PE
Di,Idrio
P
Terbofus
name)
cuorpliance./e010tceole,lt.I LisI liul each sample, o,se percow, n,,der’
10113: Aqlieouu wastes, maltematels E leachate ~0llrO,oo syslem samples, lulal
‘OPA 600/4.79-020
Eedrln
(
Sanryle
n.’
Thee for each tanrpleIrumi, chech the required greop or
inurganics. Bollies, Cyaeide, Metals 132 ozl, Nurr,enls, Phenol. Sulfide,
Uopreserued
11W-fl-so
PRO Pulyethyleee herd,
HepsuohlorOpnuide
HERB
-
iediculo whelbee
Ike suosple mao split milh the facilil3 and whethes il
116 eel. Total vol,,o,e, 90 ox.
‘ANSIIASTM
gh,,
=
gbst bold,
fepracblnr
Plseonny Herbioidet by Eleosron
must
he retained after analysis fur evidentiary
purpose,,
isdicale rho
TOTL4: Wusle, loll, uedimeot, tludge, and orgasic nratriceu. total rnurgaelcs. BullIes:
sopso poly-peupylnnewlpulp&
Heuoshlorebeezeee
CaptureDesewor
-
-
nonrher
olbottles sshn,irled aud she volome in nunces for thelampl-
Glass bottle 116011 (Isom Springfield Lahoratery). Toral volume, lhoz.
Suruo fleer enoeprNusriets
Nnthoeyshlor
MethodBI S IA
Complele ‘Dare Collected a,rd Sealed’ thtough ‘Collector or Luhool
TCLFI, Aqoeens waltes, mastematew & Iruchatecobleclion systenl samples, TCLP
(uotined(
Nnoetuobtur
P
2.4.0
-
Comosenrs.’ ‘CoIleOor or Laboratory Comments’ maybe used by th
melulu. BullIes: Uoyreuemed 132 eel. Tubal volume, 32 ox.
Metrfbunin
-
2,4,S’IP
(Silueo)
or P05 for mi,cellaoeo,,u conroleot,. IIn,ore space is seeded, atlach
TCLP2: Waste, soil, sedimeel,sludge,
and
urgaeicmatrices, TCLP metals. BolIles,
PP-ODE
-
Dutupos
leparale shed of paper.
-
Glass boIlle 116 eel (from Springfield Laboratory). Total volume, 1600,
-
P.P’-DDD
Disuosh,
4. Par Ihe ‘Ifeceipl for Samples’seclion, circle ‘y’ or ‘n’IO lodicatg
AWAST foams us 10113 4- TCLPIE. BullIes, Cyauide, Meluls IS? oIl. NoIsleuls,
P.P.DDT
Dinoteb
wherhersplits more oeecod
aud/eraccepred, crese
hove tsr iusilu~.
Phenol, Sulfide, Uopres,rved 164 uzI. Total volume, 146 00.
-
PeedimedruGe
-
P
Peewcirbererhseel
-
repeesenlarire tigu and par burnerlille and lhg
dole hI he lsthcaIefj
SWAST tsame asTCTL4 + TCI.P2y Bottles, Glassbottle 116 oil
Slsom
Spdngfield
Temorarm
Pislorum
-
gpSee
-
Laburarery).
Total volume, 1600,
-
5. Complele ‘Samplers. ‘Seater,’ and ‘Carriers’sections. 0thesompl
-
tohe th:pped, th’ lutr surcudiun ro:irqauhieg pdor to topping should oh
__________________________________________________________________
p_____________________
_________________________ ___________________________
__________________________
RIle‘To
containerfur
slripmeet”
bso.
-
SW-046 0 Tees Method, forEsuluadng Oohid Waste
EPA
6nerR.n4/I
II 0 M,chodt forthe Detennioutiooof Metal, in Rnuiromeeetal Samples
EPA
60014-7$.O20
=
Methods ‘or Chemivab
Aoulyses ofWar,rc,d Wn,seo
UOCS
=
Mrsbod,
Cur
Aoubrcis
of Inurganlu SuS,sunoes is Woterued Fluniul Oedimeero
EPA 000-twice
0
Methods forthe Oeo.rmirot
OrganisCumpeuuds I, Drh,bIeg Water. Supplemees 1.11, and IlL
All
inrormasueo outhit formic repeeseda, of27 Apnl
2000
forinfermudenul purpose, ooly and b tub)eet to shasgo
mith
eo Iiubiioy on the
porn
of the Agensy.
ILLINOIS ENVIRONMENTAL PROTECTION AGENCY
AMPLE NW~BER : D009949
~MPLING
POINT DESCU : X201/WASHINGTON/WAMAC/PRIOR OIL COMPANY
uBMITT1N~ SOURCE #
ATE COLL?CTED : .000823
TIME COLLECTED ~ 12.00
.LLECTED BY
C.C.
. DELIVERED BY :
UPS
OMIIENTS TCLP VOC~SVOCIFLASHPOINT/.PCB/LEGAL HOLD RUSI4 ON FLASWPOINT
~‘NDING CODE : LP41
AGENCY ROUTING :
——
UNIT CODE :
M TYPE CODE :
SAMPLE PURPOSE CODE : F REPORTING INDICATOR : B
..~TE RECEIVE.D 000824
TIME RECEIV.EP : 090.0
RECEIVED BY : MAR
.3 OBSERVATIONS : 1—160Z11—80Z/2—ZOZ
TRZP 3L SAM# :
~PERVISORS INITIALS CMC
.
NOTE
: K.
=
LESS THAN VALUE
8300 FLASH :POINT
DEG.F : 139
39519
TOTAL PCB$
‘4694
PHENOL
4273 B1S(2—CH•LOROEt•HYL)ETH.ER
..~4586.
2—CH.LOROPHENOL
00000 2—METHYLPHEN.OL.
~
•3Is(2—•CHLORO•ISO.PROPYL)ETHER
:0000 4METHYLPHENOL
~4428 N—NITROSO—DIN-~PR0PYLAMIN.E
4396 HEXACH.LO~OETHANE
4447 NITROBENZENE
34408 ISOPHORONE
4591
2—NITROPHENOL
34806 2,4—D.IMETHYLPHENOL
77247 BENIOIC ACID
~278 BIS(2—CHLOROETHOXY)METHANE
.~4601.2,4—DICHLOROPHENOL
~551. 1,2~4-TRICHLOROBENZENE
~696 ~4APHTHALENE
00000 4—C.HLOROANILINE
‘.~391 HEXACHLO.RO8:UTADIENE
UG.IG : 1.0K
:
130K
:
1.30K
:
130K
UG/G ~ 130K
U6/G :
UG/G :
.1.30K
UG/G : 130K
U61G
:
130K.
tJS/G :
130K
UG/G.:.130K
UG/G : 130K
UG/G
•:
130K
UGIG
:
UG/G : 130K
UGIG
:
130K
UG/G : 130K
UG/G : 130K
UGIG :
130K.
UG/G : 130K
34452 4—CHLORO’-3—METHYLPHENOL
77416 2—METHYLNAPHTHALENE
~.386 HEX.ACHLOROCYCLOPENTADIEi4E
.4621•
2,4~6—TRICHLOR0PHENOL
U.G/G : 130K
UG/G : 130K
UG/G : 430K#
UG/G
:
130K
RECEIVED
IEPA
OCT 2 7 2O~O
SITE ~
SAMPLING PROGRAM :
~4566
1,3—DICHLORO•BENZENE
..4571
1,4—DICHLOROBENZENE
77147 BENZYL ALCOHOL
4536 1,2—DICNLOROBEN.ZENE
UG/G
UG:/ G
UGIG
UG/G
U:G/
G
U
GIG
UG/t3
: 130K
: 130K
;
130K
COLL(NSV~LLEOFF~C~
~PL~ NUMBER : D009949
~7687 2,4~5TRICHLOROPHENOL
.
UG/G : 130K
4581 2—CHLORONAPHTHALENE
(JUG :
1.30•K#
u0000 2NITROANILINE
.
UG/G : 130K
34341 DI~ETHYLPHTHALATE
U6/G : 130K
4200 ACENAPHTHYLENE
UGIG : 130K
34626 2,6—DINITROTOLUENE
(JUG
130K
T8300
3NITROANILINE
.
~.
(JUG
130K
~:::4ZO5 ACENAP:HTHENE
.
U.GIG : 130K
~4616 2,4DINITROPHENOL
.
UG1G : 1300K#
4646 4—I’4.LTROPHENOL
(JUG : 130K
~1302 DI6ENZOFURAN
.
UG./G :
130K
34611 2,4—DINITROTOLUENE
U6/G : 130K
4336 DIETHYLPHTHALATE
(JUG : 130K
34641 4—CILOROPHENYL PHENYL ETHER
(JUG : 130K.
~•4381 FLUORENE
(JUG.
:•
130K
0000 4—NITROANILINE
.
UG.IG : 130K
00000 4,6—DINITRO2METKYLPHENOL
UGIG : 430K
4636 4—BROMOPHENYL PHENYL ETHER
UG/G : 130K
_9700 HEXACHLOROBENZENE
.
U.G/G. : 130K
39032 PENTA.CKLOROPHENOL
(JUG : 430K.#
4461 PHENANTHRENE
.
.
(JUG : 130K
34220 AN.THRACENE
UGIG
:
130K
‘Z.9110 .DI—M—BUTYLPHTHALATE
(JUG : 1.30K
:~.:4376 FLUORANTHENE
(JUG : .130K
34469 PYRENE
UG/G ~ 130K
:4292 BUTYL BENZYL PHTH.ALATE
UGi’G ~ 130K
_4631 3,3’—DICHLORO3ENZIDINE
(JUG : 130K
34526 BENZO(A)ANTHRACENE
.
(JUG
.Z
130K
4320 CHRYSENE
.
UG/G : 130K
39100 BIS(2ETHYL.H.EXYL)PHTHALATE
UG1G : 130K
~.4596 DI—N.0tTYLPHTHALATE
UG/G : 130K#
::h4230 8ENZO(B)FLUORANTHENE
(JUG 130K#
34242 BENZO(K)FLUORAMTHENE
(JUG : 130K
4247 3ENZO(A)PYRENE
.
(JUG : 130K
.4.403 IN.DENOCi,2~3—CD)PYRENE
(JUG
•~
i3OK~
34556 DIBENZO(AH)ANTHRACENE
UG/G 130.K#
4521 BENZO(GHI)PERYLENE
UG/G :
130K#
•a
#ACC.EPTABLE DUALITY CONTROL COULD
NOT
BE
OBTAINED FOR THIS ANALYTE.
~_
S
THIS SAMPLE WAS ANALYZED AFTER THE
30—DAY HOLDING PERIOD.
1PLE NUMBER : 0009949
.14418 CHLOROMETHANE
~J44i3
BROMOMETHANE
39175 VINYL CHLORIDE
CHLOROETHANE
4423 M.ETHYLENE CHLORIDE
•~4501
34.496
4546
7093
~2106
4531
.~1595
345 06
::~4704
~~91 80
~2i05
34511
~81 24
34699
.457o
:2104
.781
33
~71 03
~,4475
34516
~1551
XYLENE
ISOPROPYLBENZENE
UG/G 2.8
~ # QUANTITATION ~S APPROXIMATE.
UGI 6
US /6
(JUG
U6/G
U GIG
U
GIG
U.S/cS
(JUG
.UGI 6
1)6/6
U.G /S
(JUG
U6/G
116/6
116/6
UG /6
UG/G :
(JUG.:
UG/G :
U.G/G :
116/6
UG/C~
UGIG
(JUG
.:
2.2K
: 0.45K
: 0.45K
0.45K
: 01.45K
: 0.45K
: 0.45K
: 0.45K
0.45K
0.45K
0.45K
0.45K
0.45K
:
0.45K
:
0.45K
:
0.45K
:
0.45K
:
0.45K
.:
0.45K
.
0.45K
0.45K
0.45K
0.4 5K
0.45K
: 0.45K
2.2K#
: 0.45K
: 0.45K
US/S
UGIG
:
0.45K
U
GIG
US/cS
U.G/G
116/6
~i1552 ACETONE
~4488 TRICH.LOROFLUOROMETHANE
77277 BROMOCHLOR.OMETHANE
77041. CARBON DISULFIDE
:
0.45K
:
0.45K
:
0.45K
:
1.1K
1, 1—D ICJ4LOROETI4YtENE
I
,1—DICHLOROETHANE
TRANS—I, 2—.D.ICHLORGETHYL.ENE
CI S—I
~2—~ICHLOROETHYLENE
CHLOROFORM
1, 2—DICHLOROETHANE
2— BUTANON.E C MEK).
1,1~1—TRICHLORO.ETHA.NE
UG/tS :
U.G/G :
06/6 :
116/6
..2102 CARBON TETRACHLORIDE
46491 METHYL TE.RT BUTYL ETHER
T21 01 DICHLOROBROMOMETHANE
:4541 1,2—D.ICHLORGPROPANE
CIS~1~3DICHLOROPROP:ENE.
TRICHLOROETHYLENE
CH.LOROD IBROMOMETHANE
i,i~
a —
T RIC HLOR0ETHAN E
BENZENE
TRANS—i,3D.ICHLOROPROPENE
2—CHLOR.OET.HYLVINYL ETHER
BROMO FORM
4—METHYL—2—PENTA.NONE(MIBK)
2—HEX ANONE(M3K)
TETRA CHLOROETHYLENE
1,1 ,2,2—TETRACHLOROETHA.NE
~81.31 TOLUENE
1)5/6 : 0.64
34301 CHLOROBENZENE
UG/G : 0.45K
‘.811:3 ETHYLBENZENE
UG/G
1.4
7128
STYRENE
.
U6/G : 0.45K
NO TCLP COMPOUND ABOVE REGULATORY LIMITS
~PLE
NUt~3ER 0009949
DETECTED IN TOTAL SAMPLE ANALYSIS.
THE FOLLOWING QUANTITATIONS ARE APPROXIMATE
24,6TRI3ROMOPHENOL.#
116/6; 790.
MISC. PNAS
uv?;
4300
ALIPHATIC HYDROCARBONS
UG/G..42000
:.
OTHER ORGANIC COMPOUNDS
UGJG# 15000
#TENTATIVE IDENTIFICATION
: SAMPLE RE—RELEASED FOLLOWING INITIAL
COMPLETION DUE TO LATE ARIVAL OF CRUDE
OIL STANDARD
FRO~t CHEMICAL STANDARD SUPPLIER
—
SAI4PLE PATTERN APPEARS TO MATCH PATTERN OF
CRUDE OIL STANDARD.
.
STATE OF ILLINOIS
ENVIRONMENTAL PROTECTION AGENCY .
SITE SKETCH
Date of Inspection:
inspector: (7A,”,.r
~4Ano~ck~~
Site Code:lBfl
County:
,:
LM~ishaii~iLo~~
Site Hame:
Time:
/~~~‘/.‘O~
4..
_
‘•O
.1
~
.
.
..
•
.
•
OI’f~’IC?/
0
.
Mi’#c/veIJ Ln
IL
•
.
Printed on Recycted Paper
Lpe
zt~o10100
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date:
August 22, 2000
Time: 12:00-13:00
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1894925001-~O8222O0O-001
Date:
August 22, 2000
Time: 12:00-13:00
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1894925001~08222000-002
1894925001 —
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date:
August 22, 2000
Time:
12:00-13:00
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1 894925001—~08222000-003
Date: August 22, 2000
Time: 12:00-13:00
Direction: North
Photo by: Chris Cahnovsky
Photo Number:
1894925001—08222000-004
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date: August 22, 2000
Time: 12:00-13:00
Direction: East
Photo by: Chris Cahnovsky
Photo Number:
1894925001—08222000-005
STATE OF ILLINOIS
ENVIRONMENTAL PROTECTION AGENCY
Date of Inspection:
SITE SKETCH
08/3 I/~OO
~
Inspector:
~
Time:
~
‘IN
I~
•
I’4,‘#cJ,gII
Site Name:
Site Code:
I
21~
L
County: ~ .~
~
DPd~1~cie/
0
,‘l
I
IL
LPC 290 lO/B~
Pdnted on Recycted Paper
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date: August 31, 2000
Time: 10:20-10:40
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08312000-001
Date: August 31, 2000
Time: 10:20-10:40
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08312000-002
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date: August 31, 2000
Time: 10:20-10:40
Direction: West
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08312000-003
Date: August 31, 2000
Time; 10:20-10:40
Direction: Southwest
Photo by:
Chris Cahnovsky
Photo Number:
1894925001-08312000-004
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date: August 31, 2000
Time: 10:20-10:40
Direction: Northeast
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08222000-005
Date: August 31, 2000
Time: 10:20-10:40
Direction: Southwest
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08222000-006
1894925001
—
Washington County
Prior Oil Company
FOS
DIGITAL PHOTOGRAPH PHOTOCOPIES
Date: August31, 2000
Time: 10:20-10:40
Direction: Northeast
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08222000-007
Date: August 31, 2000
Time: 10:20-10:40
Direction: Northeast
Photo by: Chris Cahnovsky
Photo Number:
1894925001-08222000-008
