ILLINOIS POLLUTION CONTROL BOARD
    July 24, 1997
    IN THE MATTER OF:
    )
    )
    R96-10
    RCRA UPDATE, USEPA REGULATIONS
    )
    (Identical in Substance Rules)
    (July 1 through December 31, 1995)
    )
    ______________________________________
    IN THE MATTER OF:
    )
    )
    R97-3
    UIC UPDATE, USEPA REGULATIONS
    )
    (Identical-in-Substance Rules)
    (January 1 through June 30, 1996)
    )
    ______________________________________
    IN THE MATTER OF:
    )
    )
    R97-5
    RCRA UPDATE, USEPA REGULATIONS
    )
    (Identical in Substance Rules)
    (January 1 through June 30, 1996)
    )
    Proposed Rule. Proposal for Public Comment.
    ORDER OF THE BOARD (by K.M. Hennessey):
    Pursuant to Section 13(c) and 22.4(a) of the Environmental Protection Act (Act) [415
    ILCS 5/13(c) & 22.4(a) (1996)], the Board proposes amendments to the Resource
    Conservation and Recovery Act of 1976 (RCRA Subtitle C) hazardous waste regulations.
    Section 22.4(a) provides for quick adoption of regulations that are "identical in
    substance" to federal regulations adopted by USEPA to implement Sections 3001 through 3005
    of RCRA, 42 U.S.C. ยงยง 6921-6925 (1996)) and that Title VII of the Act and Section 5 of the
    Administrative Procedure Act (APA) [5 ILCS 100/5-35 & 5-40 (1996)] shall not apply.
    Because this rulemaking is not subject to Section 5 of the APA, it is not subject to first notice
    or to second notice review by the Joint Committee on Administrative Rules (JCAR). The
    federal RCRA Subtitle C regulations are found at 40 CFR 260 through 268, 270 through 271,
    279, and, more recently, 273.
    This order is supported by a proposed opinion adopted on the same day. The Board
    will submit Notices of Proposed Amendments for publication in the Illinois Register. The
    complete text of the proposed rules follows.
    IT IS SO ORDERED.
    2
    I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control Board, certify that the
    above order was adopted on the 24th day of July 1997, by a vote of 4-0.
    Dorothy M. Gunn, Clerk
    Illinois Pollution Control Board
    3
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER b: PERMITS
    PART 702
    RCRA AND UIC PERMIT PROGRAMS
    SUBPART A: GENERAL PROVISIONS
    Section
    702.101
    Purpose, Scope, and Applicability
    702.102
    Purpose and Scope (Repealed)
    702.103
    Confidentiality of Informa
    tion Submitted to the Agency or Board
    702.104
    References
    702.105
    Rulemaking
    702.106
    Adoption of Agency Criteria
    702.107
    Permit Appeals and Review of Agency Determinations
    702.108
    Variances and Adjusted Standards
    702.109
    Enforcement Actions
    702.110
    Definitions
    SUBPART B: PERMIT APPLICATIONS
    Section
    702.120
    Permit Application
    702.121
    Who Applies
    702.122
    Completeness
    702.123
    Information Requirements
    702.124
    Recordkeeping
    702.125
    Continuation of Expiring Permits
    702.126
    Signatories to Permit Applications and
    Reports
    SUBPART C: PERMIT CONDITIONS
    Section
    702.140
    Conditions Applicable to all Permits
    702.141
    Duty to Comply
    702.142
    Duty to Reapply
    702.143
    Need to Halt or Reduce Activity Not a Defense
    702.144
    Duty to Mitigate
    702.145
    Proper Operation and Maintenance
    702.146
    Permit Actions
    702.147
    Property Rights
    702.148
    Duty to Provide Information
    702.149
    Inspection and Entry
    702.150
    Monitoring and Records
    702.151
    Signature Requirements
    702.152
    Reporting Requirements
    702.160
    Establishing Permit Conditions
    702.161
    Duration of Permits
    702.162
    Schedules of Compliance
    702.163
    Alternative Schedules of Compliance
    702.164
    Recording and Reporting
    SUBPART D: ISSUED PERMITS
    Section
    702.181
    Effect of a Permit
    702.182
    Transfer
    702.183
    Modification
    702.184
    Causes for Modification
    702.185
    Facility Siting
    702.186
    Revocation
    702.187
    Minor Modifications
    4
    AUTHORITY: Implementing Section 13 and 22.4 and authorized by Section 27 of
    the Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
    SOURCE: Adopted in R81-32, 47 PCB 93, at 6 Ill. Reg. 12479, effective May 17,
    1982; amended in R82-19, at 53 PCB 131, 7 Ill. Reg. 14352, effective May 17,
    1982; amended in R84-9 at 9 Ill. Reg. 11926, effective July 24, 1985; amended
    in R85-23 at 10 Ill. Reg. 13274, effective July 29, 1986; amended in R86-1 at
    10 Ill. Reg. 14083, effective August 12, 1986; amended in R86-28 at 11 Ill.
    Reg. 6131, effective March 24, 1987; amended in R87-5 at 11 Ill. Reg. 19376,
    effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2579, effective
    January 15, 1988; amended in R87-29 at 12 Ill. Reg. 6673, effective March 28,
    1988; amended in R87-39 at 12 Ill. Reg. 13083, effective July 29, 1988;
    amended in R89-1 at 13 Ill. Reg. 18452, effective November 13, 1989; amended
    in R89-2 at 14 Ill. Reg. 3089, effective February 20, 1990; amended in R89-9
    at 14 Ill. Reg. 6273, effective April 16, 1990; amended in R92-10 at 17 Ill.
    Reg. 5769, effective March 26, 1993; amended in R93-16 at 18 Ill. Reg. 6918,
    effective April 26, 1994; amended in R94-5 at 18 Ill. Reg. 18284, effective
    December 20, 1994; amended in R95-6 at 19 Ill. Reg. 9913, effective June 27,
    1995; amended in R95-20 at 20 Ill. Reg. 11210, effective August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    SUBPART A: GENERAL PROVISIONS
    Section 702.110
    Definitions
    The following definitions apply to 35 Ill. Adm. Code 702, 703, 704, and 705.
    Terms not defined in this Section have the meaning given by the appropriate
    Act. When a defined term appears in a definition, the defined term is
    sometimes placed within quotation marks as to an aid to readers. When a
    definition applies primarily to one or more programs, those programs appear in
    parentheses after the defined terms.
    "Act" or "Environmental Protection Act" means the Environmental
    Protection Act [415 ILCS 5].
    "Administrator" means the Administrator of the United States
    Environmental Protection Agency, or an authorized representative.
    "Agency" means the Illinois Environmental Protection Agency.
    "Application" means the Agency forms for applying for a permit.
    For RCRA, application also includes the information required by
    the Agency under 35 Ill. Adm. Code 703.182 through 703.212
    (contents of Part B of the RCRA application).
    "Appropriate act and regulations" means the Resource Conservation
    and Recovery Act (RCRA); Safe Drinking Water Act (SDWA); or the
    "Environmental Protection Act", whichever is applicable; and
    applicable regulations promulgated under those statutes.
    "Approved program or
    approved State" means a State or interstate
    program that has been approved or authorized by EPA under 40 CFR
    271 (19 9296) (RCRA) or Section 1422 of the SDWA (UIC).
    "Aquifer" (RCRA and UIC) means a geological "formation", group of
    formations, or part of a formation that is capable of yielding a
    significant amount of water to a well or spring.
    5
    "Area of review" (UIC) means the area surrounding an injection
    well described according to the criteria set forth in 35 Ill. Adm.
    Code 730.106, or in the case of an area permit, the project area
    plus a circumscribing area the width of that is either 402 meters
    (1/4 of a mile) or a number calculated according to the criteria
    set forth in 35 Ill. Adm. Code 730.106.
    "Board" means the Illinois Pollution Control Board.
    "Closure" (RCRA) means the act of securing a "Hazardous Waste
    Management Facility" pursuant to the requirements of 35 Ill. Adm.
    Code 724.
    "Component" (RCRA) means any constituent part of a unit or any
    group of constituent parts of a unit that are assembled to perform
    a specific function (e.g., a pump seal, pump, kiln liner, or kiln
    thermocouple).
    "Contaminant" (UIC) means any physical, chemical, biological, or
    radiological substance or matter in water.
    "Corrective action management unit" or "CAMU" means an area within
    a facility that is designated by the Agency under 35 Ill. Adm.
    Code 724.Subpart S for the purpose of implementing corrective
    action requirements under 35 Ill. Adm. Code 724.201 and RCRA
    section 3008(h). A CAMU shall only be used for the management of
    remediation wastes pursuant to implementing such corrective action
    requirements at the facility.
    BOARD NOTE: USEPA must also designate a CAMU until it grants this
    authority to the Agency. See the note following 35 Ill. Adm. Code
    724.652.
    "CWA" means the Clean Water Act (formerly referred to as the
    Federal Water Pollution Control Act or Federal Water Pollution
    Control Act Amendments of 1972), P.L. 92-500, as amended by P.L.
    95-217 and P.L. 95-576; 33 U.S.C. 1251 et seq. (19
    9296).
    "Date of approval by USEPA of the Illinois UIC program" means
    March 3, 1984.
    "Director" means the Director of the Illinois Environmental
    Protection Agency or the Director's designee.
    "Disposal" (RCRA) means the discharge, deposit, injection,
    dumping, spilling, leaking, or placing of any "hazardous waste"
    into or on any land or water so that such hazardous waste or any
    constituent of the waste may enter the environment or be emitted
    into the air or discharged into any waters, including groundwater.
    "Disposal Facility" (RCRA) means a facility or part of a facility
    at which "hazardous waste" is intentionally placed into or on the
    land or water, and at which hazardous waste will remain after
    closure. The term disposal facility does not include a corrective
    action management unit into which remediation wastes are placed.
    "Draft Permit" means a document prepared under 35 Ill. Adm. Code
    705.141 indicating the Agency's tentative decision to issue, deny,
    modify, terminate, or reissue a "permit". A notice of intent to
    deny a permit, as discussed in 35 Ill. Adm. Code 705.141, is a
    type of "draft permit". A denial of a request for modification,
    as discussed in 35 Ill. Adm. Code 705.128, is not a "draft
    6
    permit". A "proposed permit" is not a "draft permit".
    "Drilling Mud" (UIC) means a heavy suspension used in drilling an
    "injection well", introduced down the drill pipe and through the
    drill bit.
    "Elementary neutralization unit" means a device which:
    Is used for neutralizing wastes that are ha
    zardous wastes
    only because they exhibit the corrosivity characteristics
    defined in 35 Ill. Adm. Code 721.122, or are listed in 35
    Ill. Adm. Code 721.Subpart D only for this reason; and
    Meets the definition of tank, tank system, container,
    transport vehicle or vessel in 35 Ill. Adm. Code 720.110.
    "Emergency Permit" means a RCRA or UIC "permit" issued in
    accordance with 35 Ill. Adm. Code 703.221 or 704.163,
    respectively.
    "Environmental Protection Agency" ("EPA" or "USEPA") means the
    United States Environmental Protection Agency.
    "Exempted aquifer" (UIC) means an "aquifer" or its portion that
    meets the criteria in the definition of "underground source of
    drinking water" but which has been exempted according to the
    procedures in 35 Ill. Adm. Code 702.105, 704.104, and 704.123(b).
    "Existing hazardous waste management (HWM) facility" or "existing
    facility" means a facility that was in operation or for which
    construction commenced on or before November 19, 1980. A facility
    has commenced construction if:
    The owner or operator has obtained the Federal, State, and
    local approvals or permits necessary to begin physical
    construction; and
    Either:
    A continuous on-site, physical construction program
    has begun; or
    The owner or operator has entered into contractual
    obligations--that cannot be canceled or modified
    without substantial loss--for physical construction of
    the facility to be completed within a reasonable time.
    "Existing injection well" (UIC) means an "injection well" other
    than a "new injection well".
    "Facility mailing list" means the mailing list for a facility
    maintained by the Agency in accordance with 35 Ill. Adm. Code
    705.163(a).
    "Facility or activity" means any "HWM facility", UIC "injection
    well", or any other facility or activity (including land or
    appurtenances thereto) that is subject to regulations under the
    Illinois RCRA or UIC program.
    "Facility mailing list" (RCRA) means the mailing list for a
    facility maintained by the Agency in accordance with 35 Ill. Adm.
    7
    Code 705.163.
    "Federal, State, and local approvals or permits necessary to begin
    physical construction" means permits and approvals required under
    Federal, State, or local hazardous waste control statutes,
    regulations, or ordinances. (See 35 Ill. Adm. Code 700.102.)
    "Final authorization" (RCRA) means approval by EPA of the Illinois
    Hazardous Waste Management Program that has met the requirements
    of Section 3006(b) of RCRA and the applicable requirements of 40
    CFR 271, Subpart A (19
    9296). EPA granted initial final
    authorization on January 31, 1986.
    "Fluid" (UIC) means any material or substance that flows or moves
    whether in a semisolid, liquid, sludge, gas, or any other form or
    state.
    "Formation" (UIC) means a body of rock characterized by a degree
    of lithologic homogeneity that is prevailingly, but not
    necessarily, tabular and is mappable on the earth's surface or
    traceable in the subsurface.
    "Formation fluid" (UIC) means "fluid" present in a "formation"
    under natural conditions, as opposed to introduced fluids, such as
    "drilling mud".
    "Functionally equivalent component" (RCRA) means a component that
    performs the same function or measurement and which meets or
    exceeds the performance specifications of another component.
    "Generator" (RCRA) means any person, by site location, whose act
    or process produces "hazardous waste" identified or listed in 35
    Ill. Adm. Code 721.
    "Groundwater" (RCRA and UIC) means a water below the land surface
    in a zone of saturation.
    "Hazardous Waste" (RCRA a
    nd UIC) means a hazardous waste as
    defined in 35 Ill. Adm. Code 721.103.
    "Hazardous waste management facility" ("HWM facility") means all
    contiguous land and structures, other appurtenances, and
    improvements on the land, used for treating, storing, or disposing
    of "hazardous waste". A facility may consist of several
    "treatment", "storage", or "disposal" operational units (for
    example, one or more landfills, surface impoundments, or
    combinations of them).
    "HWM facility" (RCRA) means "Hazardous Waste M
    anagement facility".
    "Injection well" (RCRA and UIC) means a "well" into which "fluids"
    are being injected.
    "Injection zone" (UIC) means a geological "formation", group of
    formations, or part of a formation receiving fluids through a
    "well".
    "In operation" (RCRA) means a facility that is treating, storing,
    or disposing of "hazardous waste".
    "Interim authorization" (RCRA) means approval by EPA of the
    8
    Illinois Hazardous Waste Management program that has met the
    requirements of Section 3006(g)(2) of RCRA and applicable
    requirements of 40 CFR 271 (19
    9296). This happened on May 17,
    1982.
    "Interstate agency" means an agency of two or more states
    established by or under an agreement or compact approved by the
    Congress, or any other agency of two or more states having
    substantial powers or duties pertaining to the control of
    pollution as determined and approved by the Administrator under
    the "appropriate Act and regulations".
    "Major facility" means any RCRA or UIC "facility or activity"
    classified as such by the Regional Administrator or the Agency.
    "Manifest" (RCRA and UIC) means the shipping document originated
    and signed by the "generator" that contains the information
    required by 35 Ill. Adm. Code 722.Subpart B.
    "National Pollutant Discharge Elimination System" means the
    program for issuing, modifying, revoking and reissuing,
    terminating, monitoring, and enforcing permits and imposing and
    enforcing pretreatment requirements under Section 12(f) of the
    Environmental Protection Act and 35 Ill. Adm. Code 309.Subpart A
    and 310. The term includes an "approved program".
    "New HWM facility" (RCRA) means a "Hazardous Waste Management
    facility" that began operation or for which construction commenced
    after November 19, 1980.
    "New injection well" (UIC) means a "well" that began injection
    after the UIC program for the State of Illinois applicable to the
    well is approved.
    "Off-site" (RCRA) means any site that is not "on-site".
    "On-site" (RCRA) means on the same or geographically contiguous
    property that may be divided by public or private right(s)-of-way,
    provided the entrance and exit between the properties is at a
    cross-roads intersection, and access is by crossing as opposed to
    going along, the right(s)-of-way. Non-contiguous properties owned
    by the same person but connected by a right-of-way that the person
    controls and to which the public does not have access, is also
    considered on-site property.
    "Owner or operator" means the owner or operator of any "facility
    or activity" subject to regulation under the RCRA or UIC programs.
    "Permit" means an authorization, license, or equivalent control
    document issued to implement the requirements of this Part and 35
    Ill. Adm. Code 703, 704, and 705.
    "Permit" includes RCRA "permit by rule" (35 Ill. Adm. Code
    703.141), UIC area permit (35 Ill. Adm. Code 704.162), and RCRA or
    UIC "Emergency Permit" (35 Ill. Adm. Code 703.221 and 704.163).
    "Permit" does not include RCRA interim status (35 Ill. Adm. Code
    703.153 through 703.157), UIC authorization by rule (35 Ill. Adm.
    Code 704.Subpart C), or any permit that has not yet been the
    subject of final Agency action, such as a "Draft Permit" or a
    "Proposed Permit".
    9
    "Person" means any individual, partnership, co-partnership, firm,
    company, corporation, association, joint stock company, trust,
    estate, political subdivision, state agency, or any other legal
    entity, or their legal representative, agency, or assigns.
    "Physical construction" (RCRA) means excavation, movement of
    earth, erection of forms or structures or similar activity to
    prepare an "HWM facility" to accept "hazardous waste".
    "Plugging" (UIC) means the act or process of stopping the flow of
    water, oil, or gas into or out of a formation through a borehole
    or well penetrating that formation.
    "POTW" means "publicly owned treatment works".
    "Project" (UIC) means a group of wells in a single operation.
    "Publicly owned treatment works" ("POTW") is as defined in 35 Ill.
    Adm. Code 310.
    "Radioactive waste" (UIC) means any waste that conta
    ins
    radioactive material in concentrations that exceed those listed in
    10 CFR 20, Appendix B, Table II, Column 2, incorporated by
    reference in 35 Ill. Adm. Code 720.111.
    "RCRA" means the Solid Waste Disposal Act as amended by the
    Resource Conservation and Recovery Act of 1976 (P.L. 94-580, as
    amended by P.L. 95-609, P.L. 96-510, 42 U.S.C. 6901 et seq.
    (199296)). For the purposes of regulation under 35 Ill. Adm. Code
    700 through 705, 720 through 728, and 739, "RCRA" refers only to
    RCRA Subtitle C. This does not include the RCRA Subtitle D
    (municipal solid waste landfill) regulations, found in 35 Ill.
    Adm. Code 810 through 815, and the RCRA Subtitle I (underground
    storage tank) regulations found in 35 Ill. Adm. Code 731 and 732.
    "RCRA permit" means a permit required under Section 21(f) of the
    Environmental Protection Act.
    "Regional Administrator" means the Regional Administrator for the
    EPA Region in which the facility is located or the Regional
    Administrator's designee.
    "Schedule of compliance" m
    eans a schedule of remedial measures
    included in a "permit", including an enforceable sequence of
    interim requirements (for example, actions, operations, or
    milestone events) leading to compliance with the "appropriate Act
    and regulations".
    "SDWA" means the Safe Drinking Water Act (P.L. 93-523, as amended,
    42 U.S.C. 300f et seq. (19
    9296)).
    "Site" means the land or water area where any "facility or
    activity" is physically located or conducted, including adjacent
    land used in connection with the facility or activity.
    "SIC Code" means codes pursuant to the Standard Industrial
    Classification Manual incorporated by reference in 35 Ill. Adm.
    Code 720.111.
    "State" means the State of Illinois.
    10
    "State Director" means the Director of the Illinois Environmental
    Protection Agency.
    "State/EPA Agreement" means an agreement between the Regional
    Administrator and the State that coordinates EPA and State
    activities, responsibilities, and programs including those under
    the RCRA and SDWA.
    "Storage" (RCRA) m
    eans the holding of "hazardous waste" for a
    temporary period, at the end of which the hazardous waste is
    treated, disposed, or stored elsewhere.
    "Stratum (plural strata)" (UIC) means a single sedimentary bed or
    layer, regardless of thickness, that consists of generally the
    same kind of rock material.
    "Total dissolved solids" (UIC) means the total dissolved
    (filterable) solids as determined by use of the method specified
    in 40 CFR 136, incorporated by reference in 35 Ill. Adm. Code
    720.111.
    "Transfe r facility" means any transportation related facility
    including loading docks, parking areas, storage areas, and other
    similar areas where shipments of hazardous wastes are held during
    the normal course of transportation.
    "Transferee" (UIC) means the owner or operator receiving ownership
    or operational control of the well.
    "Transferor" (UIC) means the owner or operator transferring
    ownership or operational control of the well.
    "Transporter" (RCRA) means a person engaged in the off-site
    transportation of "hazardous waste" by air, rail, highway, or
    water.
    "Treatment" (RCRA) means any method, technique, process, including
    neutralization, designed to change the physical, chemical, or
    biological character or composition of any "hazardous waste" so as
    to neutralize such wastes, or so as to recover energy or material
    resources from the waste, or so as to render such wastes non-
    hazardous, or less hazardous; safer to transport, store, or
    dispose of; or amenable for recovery, amenable for storage, or
    reduced in volume.
    "UIC" means the Underground Injection Control program.
    "Underground Injection" (UIC) means a "well injection".
    "Underground source of drinking water" ("USDW") (RCRA and UIC)
    means an "aquifer" or its portion:
    Which:
    Supplies any public water system; or
    Contains a sufficient quantity of groundwater to
    supply a public water system; and
    Currently supplies drinking water for human
    consumption; or
    11
    Contains less than 10,000 mg/1 total dissolved solids;
    and
    That i s not an "exempted aquifer".
    "USDW" (RCRA and UIC) means an "underground source of drinking
    water".
    "Wastewater treatment unit" means a device which:
    Is part of a wastewater treatment facility that is subject
    to regulation under 35 Ill. Adm. Code 309.Subpart A or 310;
    and
    Receives and treats or stores an influent wastewater that is
    a hazardous waste as defined in 35 Ill. Adm. Code 721.103,
    or generates and accumulates a wastewater treatment sludge
    that is a hazardous waste as defined in 35 Ill. Adm. Code
    721.103, or treats or stores a wastewater treatment sludge
    that is a hazardous waste as defined in 35 Ill. Adm. Code
    721.103; and
    Meets the definition of tank or tank system in 35 Ill. Adm.
    Code 720.110.
    "Well" (UIC) means a bored, drilled, or driven shaft, or a dug
    hole, whose depth is greater than the largest surface dimension.
    "Well injection" (UIC) means the subsurface emplacement of
    "fluids" through a bored, drilled, or driven "well"; or through a
    dug well, where the depth of the dug well is greater than the
    largest surface dimension.
    BOARD NOTE: Derived from 40 CFR 144.3 (19
    9496) and 270.2
    (199496), as amended at 60 Fed. Reg. 33914 (June 29, 1995)
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER b: PERMITS
    PART 703
    RCRA PERMIT PROGRAM
    SUBPART A: GENERAL PROVISIONS
    Section
    703.100
    Scope and Relation to Other Parts
    703.101
    Purpose
    703.110
    References
    SUBPART B: PROHIBITIONS
    Section
    703.120
    Prohibitions in General
    703.121
    RCRA Permits
    703.122
    Specific Inclusions in Permit Program
    703.123
    Specific Exclusions from Permit Program
    703.124
    Discharges of Hazardous Waste
    12
    703.125
    Reapplications
    703.126
    Initial Applications
    703.127
    Federal Permits (Repealed)
    SUBPART C: AUTHORIZATION BY RULE AND INTERIM STATUS
    Section
    703.140
    Purpose and Scope
    703.141
    Permits by Rule
    703.150
    Application by Existing HWM Facilities and Interim Status
    Qualifications
    703.151
    Application by New HWM Facilities
    703.152
    Amended Part A Application
    703.153
    Qualifying for Interim Status
    703.154
    Prohibitions During Interim Status
    703.155
    Changes During Interim Status
    703.156
    Interim Status Standards
    703.157
    Grounds for Termination of Interim Status
    703.158
    Permits for Less Than an Entire Facility
    703.159
    Closure by Removal
    703.160
    Procedures for Closure Determination
    SUBPART D: APPLICATIONS
    Section
    703.180
    Applications in General
    703.181
    Contents of Part A
    703.182
    Contents of Part B
    703.183
    General Information
    703.184
    Facility Location Information
    703.185
    Groundwater Protection Information
    703.186
    Exposure Information
    703.187
    Solid Waste Management Units
    703.188
    Other Information
    703.191
    Public Participation: Pre-Application Public Notice and Meeting
    703.192
    Public Participation: Public Notice of Application
    703.193
    Public Participation: Information Repository
    703.200
    Specific Part B Application Information
    703.201
    Containers
    703.202
    Tank Systems
    703.203
    Surface Impoundme
    nts
    703.204
    Waste Piles
    703.205
    Incinerators that Burn Hazardous Waste
    703.206
    Land Treatment
    703.207
    Landfills
    703.208
    Boilers and Industrial Furnaces Burning Hazardous Waste
    703.209
    Miscellaneous Units
    703.210
    Process Vents
    703.211
    Equipment
    703.212
    Drip Pads
    703.213
    Air Emission Controls for Tanks, Surface Impoundments, and
    Containers
    SUBPART E: SHORT TERM AND PHASED PERMITS
    Section
    703.221
    Emergency Permits
    703.222
    Incinerator Conditions Prior to Trial Burn
    703.223
    Incinerator Conditions During Trial
    Burn
    703.224
    Incinerator Conditions After Trial Burn
    703.225
    Trial Burns for Existing Incinerators
    703.230
    Land Treatment Demonstration
    703.231
    Research, Development and Demonstration Permits
    703.232
    Permits for Boilers and Industrial Furnaces Burning Hazardous
    13
    Waste
    SUBPART F: PERMIT CONDITIONS OR DENIAL
    Section
    703.240
    Permit Denial
    703.241
    Establishing Permit Conditions
    703.242
    Noncompliance Pursuant to Emergency Permit
    703.243
    Monitoring
    703.244
    Notice of Planned Changes (Repealed)
    703.245
    Twenty-four Hour Reporting
    703.246
    Reporting Requirements
    703.247
    Anticipated Noncompliance
    703.248
    Information Repository
    SUBPART G: CHANGES TO PERMITS
    Section
    703.260
    Transfer
    703.270
    Modification
    703.271
    Causes for Modification
    703.272
    Causes for Modification or Reissuance
    703.273
    Facility Siting
    703.280
    Permit Modification at the Request of the Permittee
    703.281
    Class 1 Modifications
    703.282
    Class 2 Modifications
    703.283
    Class 3 Modifications
    703.Appendix A
    Classification of Permit Modifications
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14289, effective October
    12, 1983; amended in R83-24 at 8 Ill. Reg. 206, effective December 27, 1983;
    amended in R84-9 at 9 Ill. Reg. 11899, effective July 24, 1985; amended in
    R85-22 at 10 Ill. Reg. 1110, effective January 2, 1986; amended in R85-23 at
    10 Ill. Reg. 13284, effective July 28, 1986; amended in R86-1 at 10 Ill. Reg.
    14093, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20702,
    effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6121, effective
    March 24, 1987; amended in R86-46 at 11 Ill. Reg. 13543, effective August 4,
    1987; amended in R87-5 at 11 Ill. Reg. 19383, effective November 12, 1987;
    amended in R87-26 at 12 Ill. Reg. 2584, effective January 15, 1988; amended in
    R87-39 at 12 Ill. Reg. 13069, effective July 29, 1988; amended in R88-16 at 13
    Ill. Reg. 447, effective December 27, 1988; amended in R89-1 at 13 Ill. Reg.
    18477, effective November 13, 1989; amended in R89-9 at 14 Ill. Reg. 6278,
    effective April 16, 1990; amended in R90-2 at 14 Ill. Reg. 14492, effective
    August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9616, effective June 17,
    1991; amended in R91-1 at 15 Ill. Reg. 14554, effective September 30, 1991;
    amended in R91-13 at 16 Ill Reg. 9767, effective June 9, 1992; amended in R92-
    10 at 17 Ill. Reg. 5774, effective March 26, 1993; amended in R93-4 at 17 Ill.
    Reg. 20794, effective November 22, 1993; amended in R93-16 at 18 Ill. Reg.
    6898, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg. 12392,
    effective July 29, 1994; amended in R94-5 at 18 Ill. Reg. 18316, effective
    December 20, 1994; amended in R95-6 at 19 Ill. Reg. 9920, effective June 27,
    1995; amended in R95-20 at 20 Ill. Reg. 11225, effective August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    SUBPART D: APPLICATIONS
    Section 703.180
    Applications in General
    14
    a)
    This Subpart c ontains requirements for applications for RCRA
    permits. A "Part A" application is required of all facilities to
    obtain interim status. The "Part B" application is a prerequisite
    to an actual permit, and need be filed for an existing facility
    with interim status only when requested. New facilities must file
    Part A and Part B at the same time;
    b)
    Subpart E contains requirements for applications for emergency
    permits, trial burn permits and land treatment demonstration
    permits;
    c)
    The application packag
    e consists of the following:
    1)
    Information required by 35 Ill. Adm. Code 702.123;
    2)
    Part A (Section 703.181);
    3)
    Part B:
    A)
    General information (Section 703.183);
    B)
    Facility location information (Section 703.184);
    C)
    Groundwater protection information, if required
    (Section 703.185);
    D)
    Specific information for each type of TSD unit, i.e.
    tanks, surface impoundments, landfills, etc. (Sections
    703.200 et seq.);
    E)
    Additional information to demonstrate compliance with
    35 Ill. Adm. Code 724 (Section 703.183(t));
    F)
    Information for trial burn permits and land treatment
    demonstrations (Subpart E).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 703.183
    General Information
    The following information is required in the Part B application for all HWM
    facilities, except as 35 Ill. Adm. Code 724.101 provides otherwise:
    a)
    A general description of the facility;
    b)
    Chemical and physical analyses of the hazardous wastes and
    hazardous debris to be handled at the facility. At a minimum,
    these analyses must contain all the information which must be
    known to treat, store or dispose of the wastes properly in
    accordance with 35 Ill. Adm. Code 724;
    c)
    A copy of the waste analysis plan required by 35 Ill. Adm. Code
    724.113(b) and, if applicable, 35 Ill. Adm. Code 724.113(c);
    d)
    A description of the security procedures and equipment required by
    35 Ill. Adm. Code 724.114, or a justification demonstrating the
    reasons for requesting a waiver of this requirement;
    e)
    A copy of the general inspection schedule required by 35 Ill. Adm.
    Code 724.115(b). Include where applicable, as part of the
    15
    inspection schedule, specific requirements in 35 Ill. Adm. Code
    724.274, 724.293(i), 724.295, 724.326, 724.354, 724.373, 724.403,
    724.702, 724.933, 724.952, 724.953, 724.958,
    724.984, 724.985,
    724.986, and 724.988 , and 724.991 ;
    f)
    A justification of any request for a waiver of the preparedness
    and prevention requirements of 35 Ill. Adm. Code 724.Subpart C;
    g)
    A copy of the contingency plan required by 35 Ill. Adm. Code
    724.Subpart D;
    BOARD NOTE: Include, where applicable, as part of the contingency
    plan, specific requirements in 35 Ill. Adm. Code 724.327 and
    724.355. 35 Ill. Adm. Code 724.355 has not yet been adopted.
    h)
    A description of procedures, structures, or equipment used at the
    facility to:
    1)
    Prevent hazards in unloading operations (for example, ramps,
    or special forklifts);
    2)
    Prevent runoff from hazardous waste handling areas to other
    areas of the facility or environment, or to prevent flooding
    (for example, berms, dikes, or trenches);
    3)
    Prevent contamination of water supplies;
    4)
    Mitigate effects of equipment failure and power outages;
    5)
    Prevent undue exposure of personnel to hazardous waste (for
    example, protective clothing); and
    6)
    Prevent releases to the atmosphere.
    i)
    A description of precautions to prevent accidental ignition or
    reaction of ignitable, reactive, or incompatible wastes, as
    required to demonstrate compliance with 35 Ill. Adm. Code 724.117,
    including documentation demonstrating compliance with 35 Ill. Adm.
    Code 724.117(c);
    j)
    Traffic pattern, estimated volume (number and types of vehicles),
    and control (for example, show turns across traffic lanes and
    stacking lanes, if appropriate); describe access road surfacing
    and load bearing capacity; and show traffic control signals;
    k)
    Facility location information, as required by Section 703.184;
    l)
    An outline of both the introductory and continuing training
    programs by the owner or operator to prepare persons to operate or
    maintain the HWM facility in a safe manner, as required to
    demonstrate compliance with 35 Ill. Adm. Code 724.116. A brief
    description of how training will be designed to meet actual job
    tasks in accordance with requirements in 35 Ill. Adm. Code
    724.116(a)(3);
    m)
    A copy of the closure plan and, where applicable, the post-closure
    plan required by 35 Ill. Adm. Code 724.212, 724.218, and 724.297.
    Include where applicable, as part of the plans, specific
    requirements in 35 Ill. Adm. Code 724.278, 724.297, 724.328,
    724.358, 724.380, 724.410, 724.451, 724.701, and 724.703;
    16
    n)
    For hazardous waste disposal units that have been closed,
    documentation that notices required under 35 Ill. Adm Code 724.219
    have been filed;
    o)
    The most recent closure cost estimate for the facility, prepared
    in accordance with 35 Ill. Adm. Code 724.242, and a copy of the
    documentation required to demonstrate financial assurance under 35
    Ill. Adm. Code 724.243. For a new facility, a copy of the
    required documentation may be submitted 60 days prior to the
    initial receipt of hazardous wastes, if it is later than the
    submission of the Part B permit application;
    p)
    Where applicable, the most recent post-closure cost estimate for
    the facility, prepared in accordance with 35 Ill. Adm. Code
    724.244, plus a copy of the documentation required to demonstrate
    financial assurance under 35 Ill. Adm. Code 724.245. For a new
    facility, a copy of the required documentation may be submitted 60
    days prior to the initial receipt of hazardous wastes, if it is
    later than the submission of the Part B permit application;
    q)
    Where applicable, a copy of the insurance policy or other
    documentation which comprises compliance with the requirements of
    35 Ill. Adm. Code 724.247. For a new facility, documentation
    showing the amount of insurance meeting the specification of 35
    Ill. Adm. Code 724.247(a) and, if applicable, 35 Ill. Adm. Code
    724.247(b) that the owner or operator plans to have in effect
    before initial receipt of hazardous waste for treatment, storage,
    or disposal. A request for an alternative level of required
    coverage for a new or existing facility may be submitted as
    specified in 35 Ill. Adm. Code 724.247(c);
    r)
    A topographic map showing a distance of 1000 feet around the
    facility at a scale of 2.5 centimeters (1 inch) equal to not more
    than 61.0 meters (200 feet). Contours must be shown on the map.
    The contour interval must be sufficient to clearly show the
    pattern of surface water flow in the vicinity of and from each
    operational unit of the facility. For example, contours with an
    interval of 1.5 meters (5 feet), if relief is greater than 6.1
    meters (20 feet), or an interval of 0.6 meters (2 feet), if relief
    is less than 6.1 meters (20 feet). Owners and operators of HWM
    facilities located in mountainous areas shall use larger contour
    intervals to adequately show topographic profiles of facilities.
    The map must clearly show the following:
    1)
    Map scale and date;
    2)
    100-year floodp lain area;
    3)
    Surface waters including intermittent streams;
    4)
    Surrounding land uses (e.g., residential, commercial,
    agricultural, recreational, etc.);
    5)
    A wind rose (i.e., prevailing windspeed and direction);
    6)
    Orientation of the map (north arrow);
    7)
    Legal boundaries of the HWM facility site;
    8)
    Access control (e.g., fences, gates, etc.);
    17
    9)
    Injection and withdrawal wells both on-site and off-site;
    10)
    Buildings; treatment, storage, or disposal operations; or
    other structures (e.g., recreation areas, runoff control
    systems, access and internal roads, storm, sanitary and
    process sewage systems, loading and unloading areas, fire
    control facilities, etc.);
    11)
    Barriers for drainage or flood control;
    12)
    Location of operational units within the HWM facility site,
    where hazardous waste is (or will be) treated, stored, or
    disposed (include equipment cleanup areas);
    BOARD NOTE: For large HWM facilities, the Agency shall
    allow the use of other scales on a case by case basis.
    s)
    Applicants shall submit such information as the Agency determines
    is necessary for it to determine whether to issue a permit and
    what conditions to impose in any permit issued; and
    t)
    For land disposal facilities, if a case-by-case extension has been
    approved under 35 Ill. Adm. Code 728.105 or if a petition has been
    approved under 35 Ill. Adm. Code 728.106, a copy of the notice of
    approval of the extension or of approval of the petition is
    required.
    u)
    A summary of the pre
    -application meeting, along
    with a list of
    attendees and their addresses, and copies of any written comments
    or materials submitted at the meeting, as required under 35 Ill.
    Adm. Code 703.191(c).
    BOARD NOTE: Derived from 40 CFR 270.14(b) (199
    46), as amended at
    5961 Fed. Reg. 6295259996 (Dec. 6, 1994 Nov. 25, 1996 ).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 703.191
    Public Participation: Pre-Application Public Notice and
    Meeting
    a)
    Applicability. The requirements of this Section shall apply to
    any RCRA Part B application seeking an initial permit for a
    hazardous waste management unit. The requirements of this Section
    shall also apply to any RCRA Part B application seeking renewal of
    a permit for such a unit, where the renewal application is
    proposing a significant change in facility operations. For the
    purposes of this Section, a "significant change" is any change
    that would qualify as a class 3 permit modification under Sections
    703.283 and 703.Appendix A. The requirements of this Section do
    not apply to permit modifications under Sections 703.280 through
    703.283 or to applications that are submitted for the sole purpose
    of conducting post
    -closure activities or post
    -closure activities
    and corrective action at a facility.
    b)
    Prior to the submission of a RCRA Part B permit application for a
    facility, the applicant must hold at least one meeting with the
    public in order to solicit questions from the community and inform
    the community of its proposed hazardous waste management
    activities. The applicant shall post a sign
    -in sheet or otherwise
    provide a voluntary opportunity for attendees to provide their
    names and addresses.
    18
    c)
    The applicant shall submit to the Agency, as part of its RCRA Part
    B permit application, a summary of the meeting, along with the
    list of attendees and their addresses developed under subsection
    (b) above and copies of any written comments or materials
    submitted at the meeting, in accordance with Section 703.183.
    d)
    The applicant must provide public notice of the pre
    -application
    meeting at least 30 days prior to the meeting. The applicant must
    maintain documentation of the notice, and provide that
    documentation to the permitting agency upon request.
    1)
    The applicant shall provide public notice in each of the
    following forms:
    A)
    A newspaper advertisement. The applicant shall
    publish a notice in a newspaper of general circulation
    in the county that hosts the proposed location of the
    facility. The notice must fulfill the requirements
    set forth in subsection (d)(2) below. In addition,
    the Agency shall instruct the applicant to publish the
    notice in newspapers of general circulation in
    adjacent counties, where the Agency determines that
    such publication is necessary to inform the affected
    public. The notice must be published as a display
    advertisement.
    B)
    A visible and accessible sign. The applicant shall
    post a notice on a clearly marked sign at or near the
    facility. The notice must fulfill the requirements
    set forth in subsection (d)(2) below. If the
    applicant places the sign on the facility property,
    then the sign must be large enough to be readable from
    the nearest point where the public would pass by the
    site.
    C)
    A broadcast media announcement. The applicant shall
    broadcast a notice at least once on at least one local
    radio station or television station. The notice must
    fulfill the requirements set forth in subsection
    (d)(2) below. The applicant may employ another medium
    with prior approval of the Agency.
    D)
    A notice to the Agency. The applicant shall send a
    copy of the newspaper notice to the permitting agency
    and to the appropriate units of State and local
    government, in accordance with Section 705.163(a).
    2)
    The notices required under subsection (d)(1) above must
    include:
    A)
    The date, time, and location of the meeting;
    B)
    A brief description of the purpose of the meeting;
    C)
    A brief description of the facility and proposed
    operations, including the address or a map (e.g., a
    sketched or copied street map) of the facility
    location;
    D)
    A statement encouraging people to contact the facility
    19
    at least 72 hours before the meeting if they need
    special access to participate in the meeting; and
    E)
    The name, address, and telephone number of a contact
    person for the applicant.
    BOARD NOTE: Derived from 40 CFR 124.31 (1996).
    Source: Added at 21 Ill. Reg. ________, effective ____________________)
    Section 703.192
    Public Participation: Public Notice of Application
    a)
    Applicability. The requirements of this Section shall apply to
    any RCRA Part B application seeking an initial permit for a
    hazardous waste management unit. The requirements of this Section
    shall also apply to any RCRA Part B application seeking renewal of
    a permit for such a unit under 35 Ill. Adm. Code 702.125. The
    requirements of this Section do not apply to permit modifications
    under Sections 703.280 through 703.283 or a permit application
    submitted for the sole purpose of conducting post
    -closure
    activities or post
    -closure activities and corrective acti
    on at a
    facility.
    b)
    Notification at application submittal.
    1)
    The Agency shall provide public notice as set forth in
    Section 35 Ill. Adm. Code 705.161, and notice to appropriate
    units of State and local government as set forth in that
    Section, that a Part B permit application has been submitted
    to the Agency and is available for review.
    2)
    The notice shall be published within 10 calendar days after
    the application is received by the Agency. The notice must
    include:
    A)
    The name and telephone number of the applicant's
    contact person;
    B)
    The name and telephone number of the appropriate
    Agency regional office, as directed by the Agency, and
    a mailing address to which information, opinions, and
    inquiries may be directed throughout the permit review
    process;
    C)
    An address to which people can write in order to be
    put on the facility mailing list;
    D)
    The location where copies of the permit application
    and any supporting documents can be viewed and copied;
    E)
    A brief description of the facility and proposed
    operations, including the address or a map (e.g., a
    sketched or copied street map) of the facility
    location on the front page of the notice; and
    F)
    The date that the application was submitted.
    c)
    Concurrent with the notice required under subsection (b) above,
    the Agency shall place the permit application and any supporting
    documents in a location accessible to the public in the vicinity
    of the facility or at the Agency regional office appropriate for
    20
    the facility.
    BOARD NOTE: Derived from 40 CFR 124.32 (1996).
    Source: Added at 21 Ill. Reg. ________, effective ____________________)
    Section 703.193
    Public Participation: Information Repository
    a)
    Applicability. The requirements of this Section shall apply to
    any application seeking a RCRA permit for a hazardous waste
    management unit.
    b)
    The Agency shall assess the need for an information repository on
    a case -by-case basis. When assessing the need for an information
    repository, the Agency shall consider a variety of factors,
    including the following: the level of public interest; the type
    of facility; the presence of an existing repository; and the
    proximity to the nearest copy of the administrative record. If
    the Agency determines, at any time after submittal of a permit
    application, that there is a need for a repository, then the
    Agency shall notify the facility that it must establish and
    maintain an information repository. (See Section 703.248 for
    similar provisions relating to the information repository during
    the life of a permit).
    c)
    The information repository must contain all documents, reports,
    data, and information deemed necessary by the Agency to fulfill
    the purposes for which the repository is established. The Agency
    will have the discretion to limit the contents of the repository.
    d)
    The information repository must be located and maintained at a
    site chosen by the facility. If the Agency determines that the
    chosen site unsuitable for the purposes and persons for which it
    was established, due to problems with the location, hours of
    availability, access, or other relevant considerations, then the
    Agency shall specify a more appropriate site.
    e)
    The Agency shall specify requirements for the applicant for
    informing the public about the information repository. At a
    minimum, the Agency shall require the facility to provide a
    written notice about the information repository to all individuals
    on the facility mailing list.
    f)
    The facility owner or operator shall be responsible for
    maintaining and updating the repository with appropriate
    information throughout a time period specified by the Agency. The
    Agency may close the repository if it determines that the
    repository is no longer needed based on its consideration of the
    factors in subsection (b) above.
    BOARD NOTE: Derived from 40 CFR 124.33 (1996).
    Source: Added at 21 Ill. Reg. ________, effective ____________________)
    Section 703.213
    Air Emission Controls for Tanks, Surface Impoundments, and
    Containers
    Except as otherwise provided in 35 Ill. Adm. Code 724.101, owners and
    operators of tanks, surface impoundments, or containers that use air emission
    controls in accordance with the requirements of 35 Ill. Adm. Code 724.Subpart
    CC shall provide the following additional information:
    21
    a)
    Documentation for each
    floating roof cover installed on a tank
    subject to 35 Ill. Adm. Code 724.984
    (b)(2) or 724.984(b)(3)
    (d)(1)
    or (d)(2) that includes information prepared by the owner or
    operator or provided by the cover manufacturer or vendor
    describing the cover design, and certification by the owner or
    operator that the cover meets the applicable design
    specifications , as listed in 35 Ill. Adm. Code 725.991
    (c)(e)(1) or
    (f)(1) .
    b)
    Identification of each container area subject to the requirements
    of 35 Ill. Adm. Code 724.Subpart CC and certification by the owner
    or operator that the requirements of this Subpart are met.
    c)
    Documentation for each enclosure used to control air
    pollutant
    emissions from containers in accordance with the requirements of
    35 Ill. Adm. Code
    724.984(d)(5) or
    724.986 (b)(2)(A) (e)(1)(ii) that
    includes information prepared by the owner or operator or provided
    by the manufacturer or vendor describing the enclosure design, and
    certification by the owner or operator that the enclosure meets
    the specifications listed in 35 Ill. Adm. Code
    725.987(b)(2)(B) records for the most recent set of calculations
    and measurements performed by the owner or operator to verify that
    the enclosure meets the criteria of a permanent total enclosure,
    as specified in "Procedure T
    --Criteria for and Verification of a
    Permanent or Temporary Total Enclosure" under 40 CFR 52.741,
    appendix B, incorporated by reference in 35 Ill. Adm. Code
    720.111 .
    d)
    Documentation for each floating membrane cover installed on a
    surface impoundment in accordance with the requirements of 35 Ill.
    Adm. Code 724.985(c) that includes information prepared by the
    owner or operator or provided by the cover manufacturer or vendor
    describing the cover design, and certification by the owner or
    operator that the cover meets the specifications listed in 35 Ill.
    Adm. Code 725.986(e) 264.985(c)(1) .
    e)
    Documentation for each closed-vent system and control device
    installed in accordance with the requirements of 35 Ill. Adm. Code
    724.987 that includes design and performance information
    , as
    specified in Section 703.124(c) and (d).
    f)
    An emission monitoring plan for both Method 21
    in 40 CFR 60,
    appendix A, incorporated by reference in 35 Ill. Adm. Code
    720.111, and control device monitoring methods. This plan must
    include the following information: monitoring points, monitoring
    methods for control devices, monitoring frequency, procedures for
    documenting exceedances, and procedures for mitigating
    noncompliances.
    g)
    When an owner or operator of a facility subject to 35 Ill. Adm.
    Code 725.Subpart CC cannot comply with 35 Ill. Adm. Code
    724.Subpart CC by the date of permit issuance, the schedule of
    implementation required under 35 Ill. Adm. Code 725.982.
    BOARD NOTE: Derived from 40 CFR 270.27
    (a), added at 59 Fed. Reg.
    62952 (Dec. 6, 1994)
    (1996), as amended at 61 Fed. Reg. 59996
    (Nov. 25, 1996) .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    22
    SUBPART E: SHORT TERM AND PHASED PERMITS
    Section 703.221
    Emergency Permits
    a)
    Notwithstanding any other provision of this Part or 35 Ill. Adm.
    Code 702 or 705, in the event that the Agency finds an imminent
    and substantial endangerment to human health or the environment
    the Agency may issue a temporary emergency permit:
    1)
    To a non -permitted facility to allow treatment, storage or
    disposal of hazardous waste; or
    2)
    To a permitted facility to allow treatment, storage or
    disposal of a hazardous waste not covered by an effective
    permit.
    b)
    This emergency permit:
    1)
    May be oral or written. If oral, it must be followed in
    five days by a written emergency permit;
    2)
    Shall not exceed 90 days in duration;
    3)
    Shall clearly specify the hazardous wastes to be received
    and the manner and location of their treatment, storage or
    disposal;
    4)
    May be terminated by the Agency at any time without process
    if it determines that termination is appropriate to protect
    human health and the environment;
    5)
    Shall be accompanied by a public notice published under 35
    Ill. Adm. Code 705.162 including:
    A)
    Name and address of the office granting the emergency
    authorization;
    B)
    Name and location of the permitted HWM facility;
    C)
    A brief description of the wastes involved;
    D)
    A brief description of the action authorized and
    reasons for authorizing it; and
    E)
    Duration of the emergency permit; and
    6)
    Shall incorporate, to the extent possible and not
    inconsistent with the emergency situation, all applicable
    requirements of this Part and 35 Ill. Adm. Code 724.
    7)
    Emergency permits which would authorize actions not in
    compliance with Board rules, other than procedural
    requirements, require a variance or provisional variance
    pursuant to Title IX of the Environmental Protection Act and
    35 Ill. Adm. Code 104.
    (Board Note BOARD NOTE : SeeDerived from 40 CFR 270.61
    (1996) .)
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    23
    Section 703.223 Incinerator Conditions During Trial Burn
    For the purposes of determining feasibility of compliance with the performance
    standards of 35 Ill. Adm. Code 724.443 and of determining adequate operating
    conditions under 35 Ill. Adm. Code 724.445, the Agency shall establish
    conditions in the permit to a new hazardous waste incinerator to be effective
    during the trial burn.
    a)
    Applica nts shall propose a trial burn plan, prepared under
    subsection (b) below with Part B of the permit application;
    b)
    The trial burn plan must include the following information:
    1)
    An analysis of each waste or mixture of wastes to be burned
    that includes:
    A)
    Heat value of the waste in the form and composition in
    which it will be burned;
    B)
    Viscosity (if applicable), or description of physical
    form of the waste;
    C)
    An identification of any hazardous organic
    constituents listed in 35 Ill. Adm. Code 721.Appendix
    H, that are present in the waste to be burned, except
    that the applicant need not analyze for constituents
    listed in 35 Ill. Adm. Code 721.Appendix H that would
    reasonably not be expected to be found in the waste.
    The constituents excluded from analysis must be
    identified, and the basis for their exclusion stated.
    The waste analysis must rely on analytical techniques
    specified in "Test Methods for the Evaluation of Solid
    Waste, Physical/Chemical Methods", U
    .S. EPA
    Publication SW-846, as incorporated by reference at 35
    Ill. Adm. Code 720.111 and Section 703.110, or their
    equivalent;
    D)
    An approximate quantification of the hazardous
    constituents identified in the waste, within the
    precision produced by the analytical methods specified
    in "Test Methods for the Evaluation of Solid Waste,
    Physical/Chemical Methods", U
    .S. EPA Publication SW-
    846, as incorporated by reference at 35 Ill. Adm. Code
    720.111 and Section 703.110, or their equivalent;
    2)
    A detailed engineering description of the i
    ncinerator for
    which the permit is sought including:
    A)
    Manufacturer's name and model number of incinerator
    (if available);
    B)
    Type of incinerator;
    C)
    Linear dimensions of the incinerator unit including
    the cross sectional area of combustion chamber;
    D)
    Description of the auxiliary fuel system (type/feed);
    E)
    Capacity of prime mover;
    24
    F)
    Description of automatic waste feed cut
    -off system(s);
    G)
    Stack gas monitoring and pollution control equipment;
    H)
    Nozzle and burner design;
    I)
    Construction materials;
    J)
    Location and description of temperature, pressure and
    flow indicating and control devices;
    3)
    A detailed description of sampling and monitoring
    procedures, including sampling and monitoring locations in
    the system, the equipment to be used, sampling and
    monitoring frequency and planned analytical procedures for
    sample analysis;
    4)
    A detailed test schedule for each waste for which the trial
    burn is planned including date(s), duration, quantity of
    waste to be burned and other factors relevant to the
    Agency's decision under subsection (e) below;
    5)
    A detailed test protocol, including, for each waste
    identified, the ranges of temperature, waste feed rate,
    combustion gas velocity, use of auxiliary fuel and any other
    relevant parameters that will be varied to affect the
    destruction and removal efficiency of the incinerator;
    6)
    A description of, and planned operating conditions for, any
    emission control equipment that will be used;
    7)
    Procedures for rapidly stoppi
    ng waste feed, shutting down
    the incinerator and controlling emissions in the event of an
    equipment malfunction;
    8)
    Such other information as the Agency reasonably finds
    necessary to determine whether to approve the trial burn
    plan in light of the purposes of this subsection and the
    criteria in subsection (e) below. Such information must be
    requested by the Agency pursuant to 35 Ill. Adm. Code
    705.123.
    c)
    The Agency, in reviewing the trial burn plan, shall evaluate the
    sufficiency of the information provided and shall require the
    applicant, pursuant to 35 Ill. Adm. Code 705.123, to supplement
    this information, if necessary, to achieve the purposes of this
    subsection;
    d)
    Based on the waste analysis data in the trial burn plan, the
    Agency shall specify as trial Principal Organic Hazardous
    Constituents (POHCs), those constituents for which destruction and
    removal efficiencies must be calculated during the trial burn.
    These trial POHCs must be specified by the Agency based on its
    estimate of the difficulty of incineration of the constituents
    identified in the waste analysis, their concentration or mass in
    the waste feed, and, for wastes listed in 35 Ill. Adm. Code
    721.Subpart D, the hazardous waste organic constituent of
    constituents identified in 35 Ill. Adm. Code 721.Appendix G or H
    as the basis for listing;
    e)
    The Agency shall approve a trial burn plan if it finds that:
    25
    1)
    The trial burn is likely to determine whether the
    incinerator performance standard required by 35 Ill. Adm.
    Code 724.443 can be met;
    2)
    The trial burn itself will not present an imminent hazard to
    human health or the environment;
    3)
    The trial burn will help the Agency to determine operating
    requirements to be specified under 35 Ill. Adm. Code
    724.445; and
    4)
    The information sought in subsections (e)(1) and (e)(3)
    above cannot reasonably be developed through other means;
    f)
    The Agency shall send a notice to all persons on the facility
    mailing list, as set forth in 35 Ill. Adm. Code 705.161(a), and to
    the appropriate units of State and local government, as set forth
    in that Section, announcing the scheduled commencement and
    completion dates for the trial burn. The applicant may not
    commence the trial burn until after the Agency has issued such
    notice.
    1)
    This notice must be mailed within a reasonable time period
    before the scheduled trial burn. An additional notice is
    not required if the trial burn is delayed due to
    circumstances beyond the control of the facility or the
    Agency.
    2)
    This notice must contain:
    A)
    The name and telephone number of the applicant's
    contact person;
    B)
    The name and telephone number of the Agency regional
    office appropriate for the facility;
    C)
    The location where the approved trial burn plan and
    any supporting documents can be reviewed and copied;
    and
    D)
    An expected time period for commencement and
    completion of the trial burn.
    fg)
    During each approved trial burn (or as soon after the burn as is
    practicable), the applicant shall make the following
    determinations:
    1)
    A quanti tative analysis of the trial POHCs, in the waste
    feed to the incinerator;
    2)
    A quantitative analysis of the exhaust gas for the
    concentration and mass emissions of the trial POHC's,
    molecular oxygen and hydrogen chloride (HCl);
    3)
    A quantitative analysis of the scrubber water (if any), ash
    residues and other residues, for the purpose of estimating
    the fate of the trial POHCs;
    4)
    A computation of destruction and removal efficiency (DRE),
    in accordance with the DRE formula specified in 35 Ill. Adm.
    26
    Code 724.443(a);
    5)
    If the HCl (hydrogen chloride) emission rate exceeds 1.8
    kilograms of HCl per hour (4 pounds per hour), a computation
    of HCl removal efficiency in accordance with 35 Ill. Adm.
    Code 724.443(b);
    6)
    A computation of particulate emissions, in accordance with
    35 Ill. Adm. Code 724.443(c);
    7)
    An identification of sources of fugitive emissions and their
    means of control;
    8)
    A measurement of average, maximum and minimum temperatures
    and combustion gas velocity;
    9)
    A continuous meas
    urement of carbon monoxide (CO) in the
    exhaust gas;
    10)
    Such other information as the Agency specifies as necessary
    to ensure that the trial burn will determine compliance with
    the performance standards in 35 Ill. Adm. Code 724.443 and
    to establish the operating conditions required by 35 Ill.
    Adm. Code 724.445 as necessary to meet that performance
    standard.
    gh)
    The applicant shall submit to the Agency a certification that the
    trial burn has been carried out in accordance with the approved
    trial burn plan, and shall submit the results of all the
    determinations required in subsection (f) above. This submission
    must be made within 90 days of completion of the trial burn, or
    later if approved by the Agency;
    hi)
    All data collected during any trial burn must be submitted to the
    Agency following the completion of the trial burn;
    ij)
    All submissions required by this subsection must be certified on
    behalf of the applicant by the signature of a person authorized to
    sign a permit application or a report under 35 Ill. Adm. Code
    702.126;
    jk)
    Based on the results of the trial burn, the Agency shall set the
    operating requirements in the final permit according to 35 Ill.
    Adm. Code 724.445. The permit modification must proceed as a
    minor modification according to Section 703.280.
    BOARD NOTE: Derived from 40 CFR 270.62(
    ab)(19), as amended at 58
    Fed. Reg. 46051 (Aug. 31, 1993)
    (1996) .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 703.225
    Trial Burns for Existing Incinerator
    s
    For the purpose of determining feasibility of compliance with the performance
    standards of 35 Ill. Adm. code 724.443 and of determining adequate operating
    conditions under 35 Ill. Adm. Code 724.445, the applicant for a permit for an
    existing hazardous waste incinerator shall prepare and submit a trial burn
    plan and perform a trial burn in accordance with Sections 703.205(b) and
    703.223(b) through (
    ie) and (g) through (j)
    , or, instead, submit other
    information as specified in Section 703.205(c).
    The Agency shall announce its
    intention to approve the trial burn plan in accordance with the timing and
    27
    distribution requirements of Section 703.223(f). The contents of the notice
    must include: the name and telephone number of a contact person at the
    facility; the name and telephone number of a contact office at the Agency; the
    location where the trial burn plan and any supporting documents can be
    reviewed and copied; and a schedule of the activities that are required prior
    to permit issuance, including the anticipated time schedule for Agency
    approval of the plan and the time period during which the trial burn would be
    conducted. Applicants submitting information under Section 703.205(a) are
    exempt from compliance with 35 Ill. Adm. Code 724.443 and 724.445 and,
    therefore, are exempt from the requirement to conduct a trail burn.
    Applicants whothat submit trial burn plans and receive approval before
    submission of a permit application shall complete the trial burn and submit
    the results, specified in Section 703.223(
    fg), with Part B of the permit
    application. If completion of this process conflicts with the date set for
    submission of the Part B application, the applicant shall contact the Agency
    to establish a later date for submission of the Part B application or the
    trial burn results. Trial burn results must be submitted prior to issuance of
    the permit. When the applicant submits a trail burn plan with Part B of the
    permit application, the Agency shall specify a time period prior to permit
    application, the Agency shall specify a time period prior to permit issuance
    in which the trial burn must be conducted and the results submitted.
    (Board Note BOARD NOTE : Derived from 40 CFR 270.62(d) (19
    8896), as amended at
    54 Fed. Reg. 4288, January 30, 1989
    .)
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 703.232
    Permits for Boilers and Industrial Furnaces Burning
    Hazardous Waste
    a)
    General. Owners and operators of new boilers and industrial
    furnaces (those not operating under the interim status standards
    of 35 Ill. Adm. Code 726.203) are subject to subsection (b)
    through (f) below. Boilers and industrial furnaces operating
    under the interim status standards of 35 Ill. Adm. Code 726.203
    are subject to subsection (g) below.
    b)
    Permit operating periods for new boilers and industrial furnaces.
    A permit for a new boiler or industrial furnace must specify
    appropriate conditions for the following operating periods:
    1)
    Pretrial burn period. For the period beginning with initial
    introduction of hazardous waste and ending with initiation
    of the trial burn, and only for the minimum time required to
    bring the boiler or industrial furnace to a point of
    operation readiness to conduct a trial burn, not to exceed
    720 hours operating time when burning hazardous waste, the
    Agency shall establish in the Pretrial Burn Period of the
    permit conditions, including but not limited to allowable
    hazardous waste feed rates and operating conditions. The
    Agency shall extend the duration of this operational period
    once, for up to 720 additional hours, at the request of the
    applicant when good cause is shown. The permit most be
    modified to reflect the extension according to Section
    703.280 et seq.
    A)
    Applicants must submit a statement, with part B of the
    permit application, that suggests the conditions
    necessary to operate in compliance with the standards
    of 35 Ill. Adm. Code 726.204 through 726.207 during
    28
    this period. This statement should include, at a
    minimum, restrictions on the applicable operating
    requirements identified in 35 Ill. Adm. Code 726.202
    (e).
    B)
    The Agency shall review this statement and any other
    relevant information submitted with part B of the
    permit application and specify requirements for this
    period sufficient to meet the performance standards of
    35 Ill. Adm. Code 726.204 through 726.207 based on the
    Agency's engineering judgment.
    2)
    Trial burn period. For the duration of the trial burn, the
    Agency shall establish conditions in the permit for the
    purposes of determining feasibility of compliance with the
    performance standards of 35 Ill. Adm. Code 726.204 through
    726.207 and determining adequate operating conditions under
    35 Ill. Adm. Code 726.202(e). Applicants shall propose a
    trial burn plan, prepared under subsection (c) below, to be
    submitted with part B of the permit application.
    3)
    Post-trial burn period.
    A)
    For the period immediately following completion of the
    trial burn, and only for the minimum period sufficient
    to allow sample analysis, data computation and
    submission of the trial burn results by the applicant,
    and review of the trial burn results and modification
    of the facility permit by the Agency to reflect the
    trial burn results, the Agency shall establish the
    operating requirements most likely to ensure
    compliance with the performance standards of 35 Ill.
    Adm. Code 726.204 through 726.207 based on the
    Agency's engineering judgment.
    B)
    Applicants shall submit a statement, with part B of
    the application, that identifies the conditions
    necessary to operate during this period in compliance
    with the performance standards of 35 Ill. Adm. Code
    726.204 through 726.207. This statement should
    include, at a minimum, restrictions on the operating
    requirements provided by 35 Ill. Adm. Code 726.202
    (e).
    C)
    The Agency shall review this statement and any other
    relevant information submitted with part B of the
    permit application and specify requirements of this
    period sufficient to meet the performance standards of
    35 Ill. Adm. Code 726.204 through 726.207 based on the
    Agency's engineering judgment.
    4)
    Final permit period. For the final period of operation the
    Agency shall develop operating requirements in conformance
    with 35 Ill. Adm. Code 726.202(e) that reflect conditions in
    the trial burn plan and are likely to ensure compliance with
    the performance standards of 35 Ill. Adm. Code 726.204
    through 726.207. Based on the trial burn results, the
    Agency shall make any necessary modifications to the
    operating requirements to ensure compliance with the
    performance standards. The permit modification must proceed
    according to Section 703.280 et seq.
    29
    c)
    Requirements for trial burn plans. The trial burn plan must
    include the following information. The Agency, in reviewing the
    trial burn plan, shall evaluate the sufficiency of the information
    provided and may require the applicant to supplement this
    information, if necessary, to achieve the purposes of this
    subsection.
    1)
    An analysis of each feed stream, including hazardous waste,
    other fuels, and industrial furnace feed stocks, as fired,
    that includes:
    A)
    Heating value, levels of antimony, arsenic, barium,
    beryllium, cadmium, chromium, lead, mercury, silver,
    thallium, total chlorine/chloride
    , and ash;
    B)
    Viscosity or description of the physical form of the
    feed stream;
    2)
    An analysis of each hazardous waste, as fired, including:
    A)
    An identification of any hazardous organic
    constituents listed in 35 Ill. Adm. Code 721.Appendix
    H that are present in the feed stream, except that
    the applicant need not analyze for constituents listed
    in 35 Ill. Adm. Code 721.Appendix H that would
    reasonably not be expected to be found in the
    hazardous waste. The constituents excluded from
    analysis must be identified as the basis for this
    exclusion explained. The analysis must be conducted
    in accordance with analytical techniques specified in
    "Test Methods for the Evaluation of Solid Waste,
    Physical/Chemical Methods", U
    .S. EPA Publication SW-
    846, as incorporated by reference at 35 Ill. Adm. Code
    720.111 and Section 703.110, or their equivalent.
    B)
    An approximate quantification of the hazardous
    constituents identified in the hazardous waste, within
    the precision produced by the analytical methods
    specified in "Test Methods for the Evaluation of Solid
    Waste, Physical/Chemical Methods", U
    .S. EPA
    Publication SW-846, as incorporated by reference at 35
    Ill. Adm. Code 720.111 and Section 703.110, or other
    equivalent.
    C)
    A description of blending procedures, if applicable,
    prior to firing the hazardous waste, including a
    detailed analysis of the hazardous waste prior to
    blending, an analysis of the material with which the
    hazardous waste prior to blending, an analysis of the
    material with which the hazardous waste is blended,
    and blending ratios.
    3)
    A detailed engineering description of the boiler or
    industrial furnace, including:
    A)
    Manufacturer's name and model number of the boiler or
    industrial furnace;
    B)
    Type of boiler or industrial furnace;
    30
    C)
    Maximum design capacity in appropriate units;
    D)
    Descript ion of the Feed system for the hazardous
    waste, and, as appropriate, other fuels and industrial
    furnace feedstocks;
    E)
    Capacity of hazardous waste feed system;
    F)
    Description of automatic hazardous waste feed cutoff
    system(s); and
    G)
    Description of any pollution control system; and
    H)
    Description of stack gas monitoring and any pollution
    control monitoring systems.
    4)
    A detailed description of sampling and monitoring procedures
    including sampling and monitoring locations in the system,
    the equipment to be used, sampling and monitoring frequency
    ,
    and sample analysis.
    5)
    A detailed test schedule for each hazardous waste for which
    the trial burn is planned, including date(s), duration,
    quantity of hazardous waste to be burned, and other factors
    relevant to the Agency's decision under subsection (b)(2)
    above.
    6)
    A detailed test protocol, including, for each hazardous
    waste identified, the ranges of hazardous waste feed rate,
    and, as appropriate, the feed rates of other fuels and
    industrial furnace feedstocks, and any other relevant
    parameters that may affect the ability of the boiler or
    industrial furnace to meet the performance standards in 35
    Ill. Adm. Code 726.204 through 726.207.
    7)
    A description of and planned operating conditions for any
    emission control equipment that will be used.
    8)
    Procedures for rapidly stopping the hazardous waste feed and
    controlling emissions in the event of an equipment
    malfunction.
    9)
    Such other information as the Agency finds necessary to
    determine whether to approve the trial burn plan in light of
    the purposes of this subsection and the criteria in
    subsection (b)(2) above.
    d)
    Trial burn procedures.
    1)
    A trial burn must be conducted to demonstrate conformance
    with the standards of 35 Ill. Adm. Code 726.104 through
    726.107.
    2)
    The Agency shall approve a trial burn plan if the Agency
    finds that:
    A)
    The trial burn is likely to determine whether the
    boiler or industrial furnace can meet the performance
    standards of 35 Ill. Adm. Code 726.104 through
    726.107.
    31
    B)
    The trial burn itself will not present an imminent
    hazard to human health and the environment;
    C)
    The trial burn will help the Agency to determine
    operating requirements to be specified under 35 Ill.
    Adm. Code 726.102(e); and
    D)
    The information sought in the trial burn cannot
    reasonably be developed through other means.
    3)
    The Agency shall send a notice to all persons on the
    facility mailing list, as set forth in 35 Ill. Adm. Code
    705.161(a), and to the appropriate units of State and local
    government, as set forth in that Section, announcing the
    scheduled commencement and completion dates for the trial
    burn. The applicant may not commence the trial burn until
    after the Agency has issued such notice.
    A)
    This notice must be mailed within a reasonable time
    period before the trial burn. An additional notice is
    not required if the trial burn is delayed due to
    circumstances beyond the control of the facility or
    the Agency.
    B)
    This notice must contain:
    i)
    The name and telephone number of applicant's
    contact person;
    ii)
    The name and telephone number of the Agency
    regional office appropriate for the facility;
    iii)
    The location where the approved trial burn plan
    and any supporting documents can be reviewed and
    copied; and
    iv)
    An expected time period for commencement and
    completion of the trial burn.
    34)
    The applicant shall submit to the Agency a certification
    that the trial burn has been carried out in accordance with
    the approved trial burn plan, and submit the results of all
    the determinations required in subsection (c) above. The
    Agency shall, in the trial burn plan, require that the
    submission be made within 90 days after completion of the
    trial burn, or later if the Agency determines that a later
    date is acceptable.
    45)
    All data collected during any trial burn must be submitted
    to the Agency following completion of the trial burn.
    56)
    All submissions required by this subsection must be
    certified on behalf of the applicant by the signature of a
    person authorized to sign a permit application or a report
    under 35 Ill. Adm. Code 702.126.
    e)
    Special procedures for DRE trial burns. When a DRE trial burn is
    required under 35 Ill. Adm. Code 726.104, the Agency shall specify
    (based on the hazardous waste analysis data and other information
    in the trial burn plan) as trial Principal Organic Hazardous
    Constituents (POHCs) those compounds for which destruction and
    32
    removal efficiencies must be calculated during the trial burn.
    These trial POHCs will be specified by the Agency based on
    information including the Agency's estimate of the difficulty of
    destroying the constituents identified in the hazardous waste
    analysis, their concentrations or mass in the hazardous waste
    feed, and, for hazardous waste containing or derived from wastes
    listed in 35 Ill. Adm. Code 721.Subpart D, the hazardous waste
    organic constituent(s) identified in 35 Ill. Adm. Code
    721.Appendix G as the basis for listing.
    f)
    Determinations based on trial burn. During each approved trial
    burn (or as soon after the burn as is practicable), the applicant
    shall make the following determinations:
    1)
    A quantitative analysis of the levels of antimony, arsenic,
    barium, beryllium, cadmium, chromium, lead, mercury,
    thallium, silver, and chlorine/chloride
    , in the feed streams
    (hazardous waste, other fuels, and industrial furnace
    feedstocks);
    2)
    When a DRE trial burn is required under 35 Ill. Adm. Code
    726.204(a):
    A)
    A quantitative analysis of the trial POHCs in the
    hazardous waste feed;
    B)
    A quantitative analysis of the stack gas for the
    concentration and mass emissions of the trial POHCs;
    and
    C)
    A computation of (DRE), in accordance with the DRE
    formula specified in 35 Ill. Adm. Code 726.204(a).
    3)
    When a trial burn for chlorinated dioxins and furans is
    required under 35 Ill. Adm. Code 726.204(e), a quantitative
    analysis of the stack gas for the concentration and mass
    emission rate of the 2,3,7,8-chlorinated tetra-octa
    congeners of chlorinated dibenzo-p-dioxins and furans, and a
    computation showing conformance with the emission standard.
    4)
    When a trial burn for PM, metals, or HCl/Chlorine gas is
    required under 35 Ill. Adm. Code 726.205, 726.206(c) or (d)
    or 726.207(b)(2) or (c), a quantitative analysis of the
    stack gas for the concentrations and mass emissions of PM,
    metals, or HCl and chlorine gas and computations showing
    conformance with the applicable emission performance
    standards;
    5)
    When a trial burn for DRE, metals, and HCl/Chlorine gas is
    required under 35 Ill. Adm. Code 726.204(a), 726.206(c) or
    (d), or 726.207(b)(2) or (c), a quantitative analysis of the
    scrubber water (if any), ash residues, other residues, and
    products for the purpose of estimating the fate of the trial
    POHCs, metals, and chlorine/chloride;
    6)
    An identification of sources of fugitive emissions and their
    means of control;
    7)
    A continuous measurement of carbon monoxide (CO), oxygen,
    and, where required, hydrocarbons (HC), in the stack gas;
    and
    33
    8)
    Such other information as the Agency specifies
    as necessary
    to ensure that the trial burn will determine compliance with
    the performance standards 35 Ill. Adm. Code 726.204 through
    726.207 and to establish the operating conditions required
    by 35 Ill. Adm. Code 726.204 through 726.207 and of
    determining adequate operating conditions under 35 Ill. Adm.
    Code 726.203, and to establish the operating conditions
    required by 35 Ill. Adm. Code 726.202(e) as necessary to
    meet those performance standards.
    g)
    Interim status boilers and industrial furnaces. for
    the purpose
    of determining feasibility of compliance with the performance
    standards of 35 Ill. Adm. Code 726.204 through 726.207 and of
    determining adequate operating conditions under 35 Ill. Adm. Code
    726.203, applicants owning or operating existing boilers or
    industrial furnaces operated under the interim status standards of
    35 Ill. Adm. Code 726.203 shall either prepare and submit a trial
    burn plan and perform a trial burn in accordance with the
    requirements of the Section or submit other information as
    specified in Section 703.208(a)(6).
    The Agency shall announce its
    intention to approve of the trial burn plan in accordance with the
    timing and distribution requirements of subsection (d)(3) above.
    The contents of the notice must include: the name and telephone
    number of a contact person at the facility; the name and telephone
    number of Agency regional office appropriate for the facility; the
    location where the trial burn plan and any supporting documents
    can be reviewed and copied; and a schedule of the activities that
    are required prior to permit issuance, including the anticipated
    time schedule for agency approval of the plan and the time periods
    during which the trial burn would be conducted.
    Applicants that
    submit a trial burn plan and receive approval before submission of
    the part B permit application shall complete the trial burn and
    submit the results specified in subsection (f) above with the part
    B permit application. If completion of this process conflicts
    with the date set for submission of the part B application, the
    applicant shall contact the Agency to establish a later date for
    submission of the part B application or the trial burn results.
    If the applicant submits a trial burn plan with part B of the
    permit application, the trial burn must be conducted and the
    results submitted within a time period prior to permit issuance to
    be specified by the Agency.
    BOARD NOTE: Derived from 40 CFR 270.66 (199
    26), as amended at 58
    Fed. Reg. 46051 (Aug. 31, 1993)
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART F: PERMIT CONDITIONS OR DENIAL
    Section 703.240
    Permit Denial
    The Agency may, pursuant to the procedures of 35 Ill. Adm. Code 705, deny the
    permit application either in its entirety or
    only as to the active life of a
    HWM facility or unit
    only.
    (Board Note BOARD NOTE : Derived from 40 CFR 270.29
    (1996) , as adopted at 54
    Fed. Reg. 9607, March 7, 1989.)
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    34
    Section 703.248
    Information Repository
    The Agency may require the permittee to establish and maintain an information
    repository at any time, based on the factors set forth in Section 703.193(b).
    The information repository shall be governed by the provisions in Section
    703.193(c) through (f).
    BOARD NOTE: Derived from 40 CFR 270.30(m) (1996).
    (Source: Added at 21 Ill. Reg. ________, effective ____________________)
    SUBPART G: CHANGES TO PERMITS
    Section 703.260
    Transfer
    a)
    A permit may be transferred by the permittee to a ne
    w owner or
    operator only if the permit has been modified or reissued (under
    subsection (b) or Section 703.272) to identify the new permittee
    and incorporate such other requirements as are necessary under the
    appropriate Act. The new owner or operator to whom the permit is
    transferred shall comply with all the terms and conditions
    specified in such permit.
    b)
    Changes in the ownership or operational control of a facility must
    be made as a Class 1 modification with the prior written approval
    of the Agency in accordance with Section 703.281. The new owner
    or operator shall submit a revised permit application no later
    than 90 days prior to the scheduled change. A written agreement
    containing a specific date for transfer of permit responsibility
    between the current and new permittees must also be submitted to
    the Agency. When a transfer of ownership or operational control
    occurs, the old owner or operator shall comply with the
    requirements of 35 Ill. Adm. Code 724.Subpart H (Financial
    Requirements), until the new owner or operator has demonstrated
    compliance with that Subpart. The new owner or operator shall
    demonstrate compliance with that Subpart within six months after
    the date of change of operational control of the facility. Upon
    demonstration to the Agency by the new owner or operator of
    compliance with that Subpart, the Agency shall notify the old
    owner or operator that the old owner or operator no longer needs
    to comply with that Subpart as of the date of demonstration.
    (Board Note: Derived from 4
    0 CFR 270.40, as amended at 53 Fed.
    Reg. 37934, September 28, 1988.)
    (Board Note: The new operator may be required to employ a chief
    operator whothat is certified pursuant to 35 Ill. Adm. Code 745.)
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 720
    HAZARDOUS WASTE MANAGEMENT SYSTEM: GENERAL
    35
    SUBPART A: GE NERAL PROVISIONS
    Section
    720.101
    Purpose, Scope and Applicability
    720.102
    Availability of Information; Confidentiality of Information
    720.103
    Use of Number and Gender
    SUBPART B: DEFINITIONS
    Section
    720.110
    Definitions
    720.111
    References
    SUBPART C: RULEMAKING PETITIONS AND OTHER PROCEDURES
    Section
    720.120
    Rulemaking
    720.121
    Alternative Equivalent Testing Methods
    720.122
    Waste Delisting
    720.123
    Petitions for Regulation as Universal Waste
    720.130
    Procedures for Solid Waste Determinations
    720.131
    Solid W aste Determinations
    720.132
    Boiler Determinations
    720.133
    Procedures for Determinations
    720.140
    Additional regulation of certain hazardous waste Recycling
    Activities on a case-by-case Basis
    720.141
    Procedures for case-by-case regulation of hazardous waste
    Recycling Activities
    720.Appendix A
    Overview of 40 CFR, Subtitle C Regulations
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
    1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
    effective May 17, 1982; amended in R82-19 at 7 Ill. Reg. 14015, effective
    October 12, 1983; amended in R84-9, 53 PCB 131 at 9 Ill. Reg. 11819, effective
    July 24, 1985; amended in R85-22 at 10 Ill. Reg. 968, effective January 2,
    1986; amended in R86-1 at 10 Ill. Reg. 13998, effective August 12, 1986;
    amended in R86-19 at 10 Ill. Reg. 20630, effective December 2, 1986; amended
    in R86-28 at 11 Ill. Reg. 6017, effective March 24, 1987; amended in R86-46 at
    11 Ill. Reg. 13435, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg.
    19280, effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2450,
    effective January 15, 1988; amended in R87-39 at 12 Ill. Reg. 12999, effective
    July 29, 1988; amended in R88-16 at 13 Ill. Reg. 362, effective December 27,
    1988; amended in R89-1 at 13 Ill. Reg. 18278, effective November 13, 1989;
    amended in R89-2 at 14 Ill. Reg. 3075, effective February 20, 1990; amended in
    R89-9 at 14 Ill. Reg. 6225, effective April 16, 1990; amended in R90-10 at 14
    Ill. Reg. 16450, effective September 25, 1990; amended in R90-17 at 15 Ill.
    Reg. 7934, effective May 9, 1991; amended in R90-11 at 15 Ill. Reg. 9323,
    effective June 17, 1991; amended in R91-1 at 15 Ill. Reg. 14446, effective
    September 30, 1991; amended in R91-13 at 16 Ill. Reg. 9489, effective June 9,
    1992; amended in R92-1 at 16 Ill. Reg. 17636, effective November 6, 1992;
    amended in R92-10 at 17 Ill. Reg. 5625, effective March 26, 1993; amended in
    R93-4 at 17 Ill. Reg. 20545, effective November 22, 1993; amended in R93-16 at
    18 Ill. Reg. 6720, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
    12160, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17480,
    effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9508, effective
    June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10929, August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    36
    SUBPART A: GENERA
    L
    Section 720.102
    Availability of Information; Confidentiality of Information
    a)
    Availability and confidentiality of information is governed by
    Illinois law, including Sections 7 and 7.1 of the Environmental
    Protection Act (Ill. Rev. Stat. 1983, ch. 111 1/2, pars. 1007 and
    1007.1) and 35 Ill. Adm. Code 101.107 and 120.
    b)
    Information required under 35 Ill. Adm. Code 722.153(a) and
    722.183 that is submitted in a notification of intent to export a
    hazardous waste will be provided to the U.S. Department of State
    and the appropriate authorities in the transit and receiving or
    importing countries regardless of any claims of confidentiality or
    trade secret.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART B: DEFINITIONS
    Section 720.111
    References
    a)
    The following publications are incorporated by reference:
    ANSI. Available from the American National Standards
    Institute, 1430 Broadway, New York, New York 10018, 212-
    354-3300:
    ANSI B31.3 and B31.4. See ASME/AN
    SI B31.3 and B31.4
    ACI. Available from the American Concrete Institute, Box
    19150, Redford Station, Detroit, Michigan 48219:
    ACI 318-83: "Building Code Requirements for
    Reinforced Concrete", adopted September, 1983.
    API. Available from the American Petroleum Institute, 1220
    L Street, N.W., Washington, D.C. 20005, 202-682-8000:
    "Cathodic Protection of Underground Petroleum Storage
    Tanks and Piping Systems", API Recommended Practice
    1632, Second Edition, December, 1987.
    "Evaporativ e Loss from External Floating-Roof Tanks",
    API Publication 2517, Third Edition, February, 1989.
    "Guide for Inspection of Refinery Equipment, Chapter
    XIII, Atmospheric and Low Pressure Storage Tanks", 4th
    Edition, 1981, reaffirmed December, 1987.
    "Installation of Underground Petroleum Storage
    Systems", API Recommended Practice 1615, Fourth
    Edition, November, 1987.
    APTI. Available from the Air and Waste Management
    Association, Box 2861, Pittsburgh, PA 15230, 412-232-3444:
    APTI Course 415: Control of Gaseous Emissions, USEPA
    Publication EPA-450/2-81-005, December, 1981.
    37
    ASME. Available from the American Society of Mechanical
    Engineers, 345 East 47th Street, New York, NY 10017, 212-
    705-7722:
    "Chemical Plant and Petroleum Refinery Piping",
    ASME/ANSI B31.3-1987, as supplemented by B31.3a-1988
    and B31.3b-1988. Also available from ANSI.
    "Liquid Transportation Systems for Hydrocarbons,
    Liquid Petroleum Gas, Anhydrous Ammonia, and
    Alcohols", ASME/ANSI B31.4-1986, as supplemented by
    B31.4a-1987. Also available from ANSI.
    ASTM. Available from American Society for Testing and
    Materials, 1916 Race Street, Philadelphia, PA 19103, 215-
    299-5400:
    ASTM C 94-90, Standard Specification for Ready-Mixed
    Concrete, approved March 30, 1990.
    ASTM D 88-87, Standard Test Method for Saybolt
    Viscosity, April 24, 1981, reapproved January, 1987.
    ASTM D 93-85, Standard Test Methods for Flash Point by
    Pensky-Martens Closed Tester, approved October 25,
    1985.
    ASTM D 1946-90, Standard
    Practice for Analysis of
    Reformed Gas by Gas Chromatography, Approved March 30,
    1990.
    ASTM D 2161-87, Standard Practice for Conversion of
    Kinematic Viscosity to Saybolt Universal or to Saybolt
    Furol Viscosity, March 27, 1987.
    ASTM D 2267-88, Standard Test Method for Aromatics in
    Light Naphthas and Aviation Gasolines by Gas
    Chromatography, approved November 17, 1988.
    ASTM D 2382-88, Standard Test Method for Heat of
    Combustion of Hydrocarbon Fuels by Bomb Calorimeter
    (High Precision Method), approved October 31, 1988.
    ASTM D 2879-86, Standard Test Method for Vapor
    Pressure-Temperature Relationship and Initial
    Decomposition Temperature of Liquids by Isoteniscope,
    approved October 31, 1986.
    ASTM D 2879-92, Standard Test Method for Vapor
    Pressure-Temperature Relationship and Initial
    Decomposition Temperature of Liquids by Isoteniscope,
    approved 1992.
    ASTM D 3828-87, Standard Test Methods for Flash Point
    of Liquids by Setaflash Closed Tester, approved
    December 14, 1988.
    ASTM E 16 8-88, Standard Practices for General
    Techniques of Infrared Quantitative Analysis, approved
    May 27, 1988.
    38
    ASTM E 169-87, Standard Practices for General
    Techniques of Ultraviolet-Visible Quantitative
    Analysis, approved February 1, 1987.
    ASTM E 260-85, Standard Practice for Packed Column Gas
    Chromatography, approved June 28, 1985.
    ASTM E 926-88 C, Standard Test Methods for Preparing
    Refuse-Derived Fuel (RDF) Samples for Analysis of
    Metals, Bomb-Acid Digestion Method, approved March 25,
    1988.
    ASTM Method G 21-70 (1984a) -- Standard Practice for
    Determining Resistance of Synthetic Polymer Materials
    to Fungi
    ASTM Method G 22-76 (1984b) -- Standard Practice for
    Determining Resistance of Plastics to Bacteria.
    GPO. Available from the Superintendent of Documents, U.S.
    Government Printing Office, Washington, D.C. 20402, 202-
    783-3238:
    Standard Industrial Classification Manual (1972), and
    1977 Supplement, republished in 1983
    "Test Methods for Evaluating Solid Waste,
    Physical/Chemical Methods", USEPA Publication number
    SW-846 (Third Edition, November, 1986), as amended by
    Updates I (July, 1992), II (September, 1994), IIA
    (August, 1993), and IIB (January, 1995) (Document
    Number 955-001-00000-1).
    NACE. Available from the National Association of Corrosion
    Engineers, 1400 South Creek Dr., Houston, TX 77084, 713-
    492-0535:
    "Control of External Corrosion on Metallic Buried,
    Partially Buried, or Submerged Liquid Storage
    Systems", NACE Recommended Practice RP0285-85,
    approved March, 1985.
    NFPA. Available from the National Fire Protection
    Association, Batterymarch Park, Boston, MA 02269, 617-770-
    3000 or 800-344-3555:
    "Flammable and Combustible Liquids Code" NFPA 30,
    issued July 17, 1987. Also available from ANSI.
    NTIS. Available from the U.S. Department of Commerce,
    National Technical Information Service, 5285 Port Royal
    Road, Springfield, VA 22161, 703-487-4600:
    "Generic Quality Assurance Project Plan for Land
    Disposal Restrictions Program", EPA/530-SW-87-011,
    March 15, 1987. (Document number PB 88-170766.)
    "Guidance on Air Quality Models", Revised 1986.
    (Document number PB86-245-248 (Guideline) and PB88-
    150-958 (Supplement)).
    39
    "Methods for Chemical Analysis of Water and Wastes",
    Third Edition, March, 1983. (Document number PB 84-
    128677).
    "Methods Manual for Compliance with BIF Regulations",
    December, 1990. (Document number PB91-120-006).
    "Petitions to Delist Hazardous Wastes -- A Guidance
    Manual", EPA/530-SW-85-003, April, 1985. (Document
    Number PB 85-194488).
    "Procedures Manual for Ground Water Monitoring at
    Solid Waste Disposal Facilities", EPA-530/SW-611,
    1977. (Document number PB 84-174820).
    "Screening Procedures for Estimating the Air Quality
    Impact of Stationary Sources", October, 1992,
    Publication Number EPA-450/R-92-019.
    OECD. Organisation for Economic Co
    -operation and
    Development, Environment Direcorate, 2 rue Andre Pascal,
    75775 Paris Cedex 16, France):
    OECD Guideline for Testing of Chemicals, Method 301B:
    "CO
    2
    Evolution (Modified Sturm Test)", adopted 17
    July 1992.
    Table 2.B of the Annex of OECD Council Decision
    C(88)90(Final) of 27 May 1988.
    STI. Available from the Steel Tank Institute, 728 Anthony
    Trail, Northbrook, IL 60062, 708-498-1980:
    "Standard for Dual Wall Underground Steel Storage
    Tanks" (1986).
    USEPA. Available from United States Environmental
    Protection Agency, Office of Drinking Water, State Programs
    Division, WH 550 E, Washington, D.C. 20460:
    "Technical Assistance Docum
    ent: Corrosion, Its
    Detection and Control in Injection Wells", EPA 570/9-
    87-002, August, 1987.
    USEPA. Available from Receptor Analysis Branch, USEPA (MD-
    14), Research Triangle Park, NC 27711:
    "Screening Procedures for Estimating the Air Quality
    Impact of Stationary Sources, Revised", October, 1992,
    Publication Number EPA-450/R-92-019.
    USEPA. Available from RCRA Information Center (RIC), 1235
    Jefferson -Davis Highway, first floor, Arlington, VA 22203
    (Docket # F -94-IEHF-FFFFF):
    OECD Green List of Wastes, Appendix 3 to the OECD
    Council Decision C(92)39/FINAL (Concerning the Control
    of Transfrontier Movements of Wastes Destined for
    Recovery Operations) (May 1994).
    OECD Red List of Wastes, Appendix 5 to the OECD
    40
    Council Decision C(92)39/FINAL (Concerning the COntrol
    of Transfrontier Movements of Wastes Destined for
    Recovery Operations) (May 1993).
    OECD Yellow List of Wastes, Appendix 4 to the OECD
    Council Decision C(92)39/FINAL (Concerning the COntrol
    of Transfrontier Movements of Wastes Destined for
    Recovery Operations) (May 1993).
    Table 2.B of the Annex of OECD Council Decision
    C(88)90(Final) (May 27, 1988).
    b)
    Code of Federal Regulations. Available from the Superintendent of
    Documents, U.S. Government Printing Office, Washington, D.C.
    20401, 202-783-3238:
    10 CFR 20, Appendix B (199
    46)
    40 CFR 51.100(ii) (199
    46)
    40 CFR 51, Subpart W (199
    46)
    40 CFR 52.741, Appendix B (1996)
    40 CFR 60 (199 46), as amended at 59 Fed. Reg. 62924 (Dec. 6,
    1994)
    40 CFR 61, S ubpart V (199 46)
    40 CFR 136 (199 46), as amended at 60 Fed. Reg. 17160 (Apr.
    4, 1995)
    40 CFR 142 (199 46)
    40 CFR 220 (199 46)
    40 CFR 260.20 (199
    46)
    40 CFR 264 (199 46)
    40 CFR 268.Appendix IX (199
    46)
    40 CFR 302.4, 302.5 and 302.6 (199
    46)
    40 CFR 761 (199 46)
    49 CFR 171 (199 56)
    49 CFR 173 (199 56)
    49 CFR 178 (199 46)
    c)
    Federal Statutes
    Section 3004 of the Resource Conservation and Recovery Act (42
    U.S.C. 6901 et seq.), as amended through December 31, 1987.
    Sections 201(v), 201(w), and 360b(j) of the Federal Food, Drug,
    and Cosmetic Act (FFDCA; 21 U.S.C. ยงยง
    321(v), 321(w) & 512(j)), as
    amended through October 25, 1994.
    41
    d)
    This Section incorporates no later editions or amendments.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 721
    IDENTIFICATION AND LISTING OF HAZARDOUS WA
    STE
    SUBPART A: GENERAL PROVISIONS
    Section
    721.101
    Purpose and Scope
    721.102
    Definition of Solid Waste
    721.103
    Definition of Hazardous Waste
    721.104
    Exclusions
    721.105
    Special Requirements for Hazardous Waste Generated by Small
    Quantity Generators
    721.106
    Requirements for Recyclable Materials
    721.107
    Residues of Hazardous Waste in Empty Containers
    721.108
    PCB Wastes Regulated under TSCA
    721.109
    Requirements for Universal Waste
    SUBPART B: CRITERIA FOR IDENTIFYING THE CHARACTERISTICS
    OF HAZARDOUS WASTE
    AND FOR LISTING HAZARDOUS WASTES
    Section
    721.110
    Criteria for Identifying the Characteristics of Hazardous Waste
    721.111
    Criteria for Listing Hazardous Waste
    SUBPART C: CHARACTERISTICS OF HAZARDOUS WASTE
    Section
    721.120
    General
    721.121
    Characteristic of Ignitability
    721.122
    Characteristic of Corrosivity
    721.123
    Characteristic of Reactivity
    721.124
    Toxicity Characteristic
    SUBPART D: LISTS OF HAZARDOUS WASTE
    Section
    721.130
    General
    721.131
    Hazardous Wastes From Nonspecific Sources
    721.132
    Hazardous Was te from Specific Sources
    721.133
    Discarded Commercial Chemical Products, Off-Specification Species,
    Container Residues, and Spill Residues Thereof
    721.135
    Wood Preserving Wastes
    721.Appendix A
    Representative Sampling Methods
    721.Appendix B
    Method 1311 Toxicity Characteristic Leaching Procedure
    (TCLP)
    721.Appendix C
    Chemical Analysis Test Methods
    Table A
    Analytical Characteristics of Organic Chemicals (Repealed)
    Table B
    Analytical Characteristics of Inorganic Species (Repealed)
    Table C
    Sample Preparation
    /Sample Introduction Techniques (Repealed)
    721.Appendix G
    Basis for Listing Hazardous Wastes
    721.Appendix H
    Hazardous Constituents
    721.Appendix I
    Wastes Excluded by Administrative Action
    Table A
    Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22
    from Non-Specific Sources
    42
    Table B
    Wastes Excluded by USEPA under 40 CFR 260.20 and 260.22 from
    Specific Sources
    Table C
    Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22
    from Commercial Chemical Products, Off-Specification
    Species, Container Residues, and Soil Residues Thereof
    Table D
    Wastes Excluded by the Board by Adjusted Standard
    721.Appendix J
    Method of Analysis for Chlorinated Dibenzo-p-Dioxins and
    Dibenzofurans (Repealed)
    721.Appendix Z
    Table to Section 721.102
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
    1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
    effective as noted in 35 Ill. Adm. Code May 17, 1982; amended in R82-18, 51
    PCB 31, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in R82-19,
    53 PCB 131, at 7 Ill. Reg. 13999, effective October 12, 1983; amended in R84-
    34, 61 PCB 247, at 8 Ill. Reg. 24562, effective December 11, 1984; amended in
    R84-9, at 9 Ill. Reg. 11834, effective July 24, 1985; amended in R85-22 at 10
    Ill. Reg. 998, effective January 2, 1986; amended in R85-2 at 10 Ill. Reg.
    8112, effective May 2, 1986; amended in R86-1 at 10 Ill. Reg. 14002, effective
    August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20647, effective December
    2, 1986; amended in R86-28 at 11 Ill. Reg. 6035, effective March 24, 1987;
    amended in R86-46 at 11 Ill. Reg. 13466, effective August 4, 1987; amended in
    R87-32 at 11 Ill. Reg. 16698, effective September 30, 1987; amended in R87-5
    at 11 Ill. Reg. 19303, effective November 12, 1987; amended in R87-26 at 12
    Ill. Reg. 2456, effective January 15, 1988; amended in R87-30 at 12 Ill. Reg.
    12070, effective July 12, 1988; amended in R87-39 at 12 Ill. Reg. 13006,
    effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 382, effective
    December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18300, effective November
    13, 1989; amended in R90-2 at 14 Ill. Reg. 14401, effective August 22, 1990;
    amended in R90-10 at 14 Ill. Reg. 16472, effective September 25, 1990; amended
    in R90-17 at 15 Ill. Reg. 7950, effective May 9, 1991; amended in R90-11 at 15
    Ill. Reg. 9332, effective June 17, 1991; amended in R91-1 at 15 Ill. Reg.
    14473, effective September 30, 1991; amended in R91-12 at 16 Ill. Reg. 2155,
    effective January 27, 1992; amended in R91-26 at 16 Ill. Reg. 2600, effective
    February 3, 1992; amended in R91-13 at 16 Ill. Reg. 9519, effective June 9,
    1992; amended in R92-1 at 16 Ill. Reg. 17666, effective November 6, 1992;
    amended in R92-10 at 17 Ill. Reg. 5650, effective March 26, 1993; amended in
    R93-4 at 17 Ill. Reg. 20568, effective November 22, 1993; amended in R93-16 at
    18 Ill. Reg. 6741, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
    12175, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17490,
    effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9522, effective
    June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10963, August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    SUBPART A: GENERAL PROVISIONS
    Section 721.104
    Exclusions
    a)
    Materials that are not solid wastes. The following materials are
    not solid wastes for the purpose of this Part:
    1)
    Sewage:
    A)
    Domestic sewage; and
    B)
    Any mixture of domestic sewage and other waste that
    43
    passes through a sewer system to publicly-owned
    treatment works for treatment.
    C)
    "Domestic sewage" means untreated sanitary wastes that
    pass through a sewer system.
    2)
    Industrial wastewater discharges that are point source
    discharges with NPDES permits issued by the Agency pursuant
    to Section 12(f) of the Environmental Protection Act and 35
    Ill. Adm. Code 309.
    BOARD NOTE: This exclusion applies
    only to the actual point
    source discharge. It does not exclude industrial
    wastewaters while they are being collected, stored, or
    treated before discharge, nor does it exclude sludges that
    are generated by industrial wastewater treatment.
    3)
    Irrigation return flows.
    4)
    Source, special nuclear, or by-product material as defined
    by the Atomic Energy Act of 1954, as amended (42 U.S.C. 2011
    et seq.)
    5)
    Materials subjected to in-situ mining techniques that are
    not removed from the ground as part of the extraction
    process.
    6)
    Pulping liquors (i.e., black liquor) that are reclaimed in a
    pulping liquor recovery furnace and then reused in the
    pulping process, unless accumulated speculatively, as
    defined in Section 721.101(c).
    7)
    Spent sulfuric acid used to produce virgin sulfuric acid
    unless it is accumulated speculatively, as defined in
    Section 721.101(c).
    8)
    Secondary materials that are reclaimed and returned to the
    original process or processes in which they were generated
    where they are reused in the production process, provided:
    A)
    Only tank storage is involved, and the entire process
    through completion of reclamation is closed by being
    entirely connected with pipes or other comparable
    enclosed means of conveyance;
    B)
    Reclamation does not involve controlled flame
    combustion (such as occurs in boilers, industrial
    furnaces or incinerators);
    C)
    The secondary materials are never accumulated in such
    tanks for over twelve months without being reclaimed;
    and
    D)
    The reclaimed material is
    not used to produce a fuel
    or used to produce products that are used in a manner
    constituting disposal.
    9)
    Wood preserving wastes.
    A)
    Spent wood preserving solutions that have been used
    and which are reclaimed and reused for their original
    44
    intended purpose; and
    B)
    Wastewaters from the wood preserving process that have
    been reclaimed and which are reused to treat wood.
    10)
    Hazardous waste numbers K060, K087, K141, K142, K143, K144,
    K145, K147, and K148, and any wastes from the coke by-
    products processes that are hazardous only because they
    exhibit the toxicity characteristic specified in Section
    721.124, when subsequent to generation these materials are
    recycled to coke ovens, to the tar recovery process as a
    feedstock to produce coal tar, or are mixed with coal tar
    prior to the tar's sale or refining. This exclusion is
    conditioned on there being no land disposal of the waste
    from the point it is generated to the point it is recycled
    to coke ovens, to tar recovery, to the tar refining
    processes, or prior to when it is mixed with coal.
    11)
    Nonwastewater splash condenser dross residue from the
    treatment of hazardous waste number K061 in high temperature
    metals recovery units, provided it is shipped in drums (if
    shipped) and not land disposed before recovery.
    12)
    Recovered oil from petroleum refining, exploration, and
    production and from transportation incident thereto that is
    to be inserted into the petroleum refining process (SIC Code
    2911) along with normal process streams prior to crude
    distillation or catalytic cracking
    at or before a point
    (other than direct insertion into a coker) where
    contaminants are removed
    . This exclusion applies to
    recovered oil stored or transported prior to insertion,
    except that the oil must not be stored in a manner involving
    placement on the land and the oil must not be accumulated
    speculatively before being recycled. Recovered oil is oil
    that has been reclaimed from secondary materials (such as
    wastewater) generated from normal petroleum refining,
    exploration , and production, and
    from transportation
    practices. Recovered oil includes oil that is recovered
    from refinery wastewater collection and treatment systems,
    oil recovered from oil and gas drilling operations, and oil
    recovered from wastes removed from crude oil storage tanks.
    Recovered oil does not include (among other things) oil-
    bearing hazardous wastes listed in 721.Subpart D (e.g., K048
    through K052, F037, and F038). However, oil recovered from
    such wastes may be considered recovered oil. Recovered oil
    also does not include used oil as defined in 35 Ill. Adm.
    Code 739.100.
    b)
    Solid wastes that are not hazardous wastes. The following solid
    wastes are not hazardous wastes:
    1)
    Household waste, including household waste that has been
    collected, transported, stored, treated, disposed, recovered
    (e.g., refuse-derived fuel), or reused. "Household waste"
    means any waste material (including garbage, trash, and
    sanitary wastes in septic tanks) derived from households
    (including single and multiple residences, hotels, and
    motels, bunkhouses, ranger stations, crew quarters,
    campgrounds, picnic grounds, and day-use recreation areas).
    A resource recovery facility managing municipal solid waste
    shall not be deemed to be treating, storing, disposing of,
    45
    or otherwise managing hazardous wastes for the purposes of
    regulation under this Part, if such facility:
    A)
    Receives and burns only:
    i)
    Household waste (from single and multiple
    dwellings, hotels, motels, and other residential
    sources); and
    ii)
    Solid waste from commercial or industrial
    sources that does not contain hazardous waste,
    and
    B)
    Such facility does not accept hazardous waste and the
    owner or operator of such facility has established
    contractual requirements or other appropriate
    notification or inspection procedures to assure that
    hazardous wastes are not received at or burned in such
    facility.
    BOARD NOTE: The U.S. Supreme Court determined, in
    City of Chicago v. Environmental Defense Fund, Inc.,
    -- U.S. --, 114 S. Ct. 1588 (1994), th
    at this
    exclusion and RCRA section 3001(i) (42 U.S.C.
    ยง 6921(i)) do not exclude the ash from facilities
    covered by this subsection from regulation as a
    hazardous waste. At 59 Fed. Reg. 29372 (June 7,
    1994), USEPA granted facilities managing ash from such
    facilities that is determined a hazardous waste under
    721.Subpart C until December 7, 1994 to file a Part A
    permit application pursuant to 35 Ill. Adm. Code
    703.181. At 60 Fed. Reg. 6666 (Feb. 3, 1995), USEPA
    stated that it interpreted that the point at which ash
    becomes subject to RCRA Subtitle C regulation is when
    that material leaves the combustion building
    (including connected air pollution control equipment).
    2)
    Solid wastes generated by any of the following that are
    returned to the soil as fertilizers:
    A)
    The growing and harvesting of agricultural crops, or
    B)
    The raising of animals, including animal manures.
    3)
    Mining overburden returned to the mine site.
    4)
    Fly ash waste, bottom ash waste, slag waste, and flue gas
    emission control waste generated primarily from the
    combustion of coal or other fossil fuels, except as provided
    in 35 Ill. Adm. Code 726.212 for facilities that burn or
    process hazardous waste.
    5)
    Drilling fluids, produced waters, and other wastes
    associated with the exploration, development, or production
    of crude oil, natural gas, or geothermal energy.
    6)
    Chromium wastes:
    A)
    Wastes that fail the test for the toxicity
    characteristic (Sections 721.124 and 721.Appendix B)
    because chromium is present or which are listed in
    46
    721.Subpart D due to the presence of chromium, that do
    not fail the test for the toxicity characteristic for
    any other constituent or which are not listed due to
    the presence of any other constituent, and that do not
    fail the test for any other characteristic, if it is
    shown by a waste generator or by waste generators
    that:
    i)
    The chromium in the waste is exclusively (or
    nearly exclusively) trivalent chromium;
    ii)
    The waste is generated from an industrial
    process that uses trivalent chromium exclusively
    (or nearly exclusively) and the process does not
    generate hexavalent chromium; and
    iii)
    The waste is typically and frequently managed in
    non-oxidizing environments.
    B)
    Specific wastes that meet the standard in subsection
    (b)(6)(A) above (so long as they do not fail the test
    for the toxicity characteristic for any other
    constituent and do not exhibit any other
    characteristic) are:
    i)
    Chrome (blue) trimmings generated by the
    following subcategories of the leather tanning
    and finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, retan/wet finish, no
    beamhouse, through-the-blue, and shearling;
    ii)
    Chrome (blue) shavings generated by the
    following subcategories of the leather tanning
    and finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, retan/wet finish, no
    beamhouse, through-the-blue, and shearling;
    iii)
    Buffing dust generated by the following
    subcategories of the leather tanning and
    finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, retan/wet finish, no
    beamhouse, through-the-blue;
    iv)
    Sewer screenings generated by the following
    subcategories of the leather tanning and
    finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, retan/wet finish, no
    beamhouse, through-the-blue, and shearling;
    v)
    Wastewater treatment sludges generated by the
    following subcategories of the leather tanning
    and finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, retan/wet finish, no
    beamhouse, through-the-blue, and shearling;
    vi)
    Wastewater treatment sludges generated by the
    47
    following subcategories of the leather tanning
    and finishing industry: hair pulp/chrome
    tan/retan/wet finish, hair save/chrome
    tan/retan/wet finish, and through-the-blue;
    vii)
    Waste scrap leather from the leather tanning
    industry, the shoe manufacturing industry, and
    other leather product manufacturing industries;
    and
    viii)
    Wastewater treatment sludges from the production
    of titanium dioxide pigment using chromium-
    bearing ores by the chloride process.
    7)
    Solid waste from the extraction, beneficiation, and
    processing of ores and minerals (including coal, phosphate
    rock, and overburden from the mining of uranium ore), except
    as provided by 35 Ill. Adm. Code 726.212 for facilities that
    burn or process hazardous waste. For purposes of this
    subsection, beneficiation of ores and minerals is restricted
    to the following activities: crushing, grinding, washing,
    dissolution, crystallization, filtration, sorting, sizing,
    drying, sintering, pelletizing, briquetting, calcining to
    remove water or carbon dioxide, roasting, autoclaving or
    chlorination in preparation for leaching (except where the
    roasting or autoclaving or chlorination and leaching
    sequence produces a final or intermediate product that does
    not undergo further beneficiation or processing), gravity
    concentration, magnetic separation, electrostatic
    separation, floatation, ion exchange, solvent extraction,
    electrowinning, precipitation, amalgamation, and heap, dump,
    vat tank, and in situ leaching. For the purposes of this
    subsection, solid waste from the processing of ores and
    minerals includes only the following wastes:
    A)
    Slag from primary copper processing,
    B)
    Slag from primary lead processing,
    C)
    Red and brown muds from bauxite refining,
    D)
    Phosphogypsum from phosphoric acid production,
    E)
    Slag from elementa
    l phosphorus production,
    F)
    Gasifier ash from coal gasification,
    G)
    Process wastewater from coal gasification,
    H)
    Calcium sulfate wastewater treatment plant sludge from
    primary copper processing,
    I)
    Slag tailings from primary copper processing,
    J)
    Fluorogypsum from hydrofluoric acid production,
    K)
    Process wastewater from hydrofluoric acid production,
    L)
    Air pollution control dust or sludge from iron blast
    furnaces,
    48
    M)
    Iron blast furnace slag,
    N)
    Treated residue from roast
    ing and leaching of chrome
    ore,
    O)
    Process wastewater from primary magnesium processing
    by the anhydrous process,
    P)
    Process wastewater from phosphoric acid production,
    Q)
    Basic oxygen furnace and open hearth furnace air
    pollution control dust or sludge from carbon steel
    production,
    R)
    Basic oxygen furnace and open hearth furnace slag from
    carbon steel production,
    S)
    Chloride processing waste solids from titanium
    tetrachloride production, and
    T)
    Slag from primary zinc smelting.
    8)
    Cement kiln dust waste, except as provided by 35 Ill. Adm.
    Code 726.212 for facilities that burn or process hazardous
    waste.
    9)
    Solid waste that consists of discarded arsenical-treated
    wood or wood products that fails the test for the toxicity
    characteristic for hazardous waste codes D004 through D017
    and which is not a hazardous waste for any other reason if
    the waste is generated by persons that utilize the
    arsenical-treated wood and wood products for these
    materials' intended end use.
    10)
    Petroleu m-contaminated media and debris that fail the test
    for the toxicity characteristic of Section 721.124
    (hazardous waste codes D018 through D043 only) and which are
    subject to corrective action regulations under 35 Ill. Adm.
    Code 731.
    11)
    This subsection corresponds with 40 CFR 261.4(b)(11), which
    expired by its own terms on January 25, 1993. This
    statement maintains structural parity with USEPA
    regulations.
    12)
    Used chloro fluoro carbon refrigerants from totally enclosed
    heat transfer equipment, including mobile air conditioning
    systems, mobile refrigeration, and commercial and industrial
    air conditioning and refrigeration systems, that uses
    chloro fluoro carbons as the heat transfer fluid in a
    refrigeration cycle, provided the refrigerant is reclaimed
    for further use.
    13)
    Non-terne plated used oil filters that are not mixed with
    wastes listed in 721.Subpart D, if these oil filters have
    been gravity hot-drained using one of the following methods:
    A)
    Puncturing the filter anti-drain back valve or
    the
    filter dome end and hot-draining;
    B)
    Hot-draining and crushing;
    49
    C)
    Dismantling and hot-draining; or
    D)
    Any other equivalent hot-draining method that will
    remove used oil.
    14)
    Used oil re-refining distillation bottoms that are used as
    feedstock to manufacture asphalt products.
    c)
    Hazardous wastes that are exempted from certain regulations. A
    hazardous waste that is generated in a product or raw material
    storage tank, a product or raw material transport vehicle or
    vessel, a product or raw material pipeline, or in a manufacturing
    process unit, or an associated non-waste-treatment manufacturing
    unit, is not subject to regulation under 35 Ill. Adm. Code 702,
    703, 705, and 722 through 725, and 728 or to the notification
    requirements of Section 3010 of RCRA until it exits the unit in
    which it was generated, unless the unit is a surface impoundment,
    or unless the hazardous waste remains in the unit more than 90
    days after the unit ceases to be operated for manufacturing or for
    storage or transportation of product or raw materials.
    d)
    Samples
    1)
    Except as provided in subsection (d)(2) below, a sample of
    solid waste or a sample of water, soil, or air that is
    collected for the sole purpose of testing to determine its
    characteristics or composition is not subject to any
    requirements of this Part or 35 Ill. Adm. Code 702, 703,
    705, and 722 through 728. The sample qualifies when:
    A)
    The sample is being transported to a laboratory for
    the purpose of testing;
    B)
    The sample is being transport
    ed back to the sample
    collector after testing;
    C)
    The sample is being stored by the sample collector
    before transport to a laboratory for testing;
    D)
    The sample is being stored in a laboratory before
    testing;
    E)
    The sample is being stored in a laboratory for testing
    but before it is returned to the sample collector; or
    F)
    The sample is being stored temporarily in the
    laboratory after testing for a specific purpose (for
    example, until conclusion of a court case or
    enforcement action where further testing of the sample
    may be necessary).
    2)
    In order to qualify for the exemption in subsection
    (d)(1)(A) or (d)(1)(B) above, a sample collector shipping
    samples to a laboratory and a laboratory returning samples
    to a sample collector shall:
    A)
    Comply with U.S. Department of Transportation (DOT),
    U.S. Postal Service (USPS), or any other applicable
    shipping requirements; or
    50
    B)
    Comply with the following requirements if the sample
    collector determines that DOT, USPS, or other shipping
    requirements do not apply to the shipment of the
    sample:
    i)
    Assure that the following information
    accompanies the sample: The sample collector's
    name, mailing address, and telephone number; the
    laboratory's name, mailing address, and
    telephone number; the quantity of the sample;
    the date of the shipment; and a description of
    the sample.
    ii)
    Package the sample so that it does not leak,
    spill, or vaporize from its packaging.
    3)
    This exemption does not apply if the laboratory determines
    that the waste is hazardous but the laboratory is no longer
    meeting any of the conditions stated in subsection (d)(1)
    above.
    e)
    Treatability study samples.
    1)
    Except as is provided in subsection (e)(2) below, a person
    that generates or collects samples for the purpose of
    conducting treatability studies, as defined in 35 Ill. Adm.
    Code 720.110, are not subject to any requirement of 35 Ill.
    Adm. Code 721 through 723 or to the notification
    requirements of Section 3010 of the Resource Conservation
    and Recovery Act. Nor are such samples included in the
    quantity determinations of Section 721.105 and 35 Ill. Adm.
    Code 722.134(d) when:
    A)
    The sample is being collected and prepared for
    transportation by the generator or sample collector;
    B)
    The sample is being accumulated or stored by the
    generator or sample collector prior to transportation
    to a laboratory or testing facility; or
    C)
    The sample is being transported to the laboratory or
    testing facility for the purpose of conducting a
    treatability study.
    2)
    The exem ption in subsection (e)(1) above is applicable to
    samples of hazardous waste being collected and shipped for
    the purpose of conducting treatability studies provided
    that:
    A)
    The generator or sample collector uses (in
    "treatability studies") no more than 10,000 kg of
    media contaminated with non-acute hazardous waste,
    1000 kg of non-acute hazardous waste other than
    contaminated media, 1 kg of acute hazardous waste, or
    2500 kg of media contaminated with acute hazardous
    waste for each process being evaluated for each
    generated wastestream;
    B)
    The mass of each shipment does not exceed 10,000 kg;
    the 10,000 kg quantity may be all media contaminated
    with non-acute hazardous waste, or may include 2500 kg
    51
    of media contaminated with acute hazardous waste, 1000
    kg of hazardous waste, and 1 kg of acute hazardous
    waste;
    C)
    The sample must be packaged so that it does not leak,
    spill, or vaporize from its packaging during shipment
    and the requirements of subsections (e)(2)(C)(i) or
    (e)(2)(C)(ii) , below , are met.
    i)
    The transportation of each sample shipment
    complies with U.S. Department of Transportation
    (DOT), U.S. Postal Service (USPS), or any other
    applicable shipping requirements; or
    ii)
    If the DOT, USPS, or other shipping requirements
    do not apply to the shipment of the sample, the
    following information must accompany the sample:
    The name, mailing address, and telephone number
    of the originator of the sample; the name,
    address, and telephone number of the facility
    that will perform the treatability study; the
    quantity of the sample; the date of the
    shipment; and, a description of the sample,
    including its USEPA hazardous waste number;
    D)
    The sample is shipped to a laboratory or testing
    facility that is exempt under subsection (f) below, or
    has an appropriate RCRA permit or interim status;
    E)
    The generator or sample collector maintains the
    following records for a period ending three years
    after completion of the treatability study:
    i)
    Copies of the shipping documents;
    ii)
    A copy of t he contract with the facility
    conducting the treatability study;
    iii)
    Documentation showing: The amount of waste
    shipped under this exemption; the name, address,
    and USEPA identification number of the
    laboratory or testing facility that received the
    waste; the date the shipment was made; and
    whether or not unused samples and residues were
    returned to the generator; and
    F)
    The generator reports the information required in
    subsection (e)(2)(E)(iii) above in its report under 35
    Ill. Adm. Code 722.141.
    3)
    The Agency may grant requests on a case-by-case basis for up
    to an additional two years for treatability studies
    involving bioremediation. The Agency may grant requests, on
    a case-by-case basis, for quantity limits in excess of those
    specified in subsection (e)(2)(A) and (e)(2)(B) above and
    (f)(4) below, for up to an additional 5000 kg of media
    contaminated with non-acute hazardous waste, 500 kg of non-
    acute hazardous waste, 2500 kg of media contaminated with
    acute hazardous waste, and 1 kg of acute hazardous waste:
    A)
    In response to requests for authorization to ship,
    52
    store, and conduct further treatability studies on
    additional quantities in advance of commencing
    treatability studies. Factors to be considered in
    reviewing such requests include the nature of the
    technology, the type of process (e.g., batch versus
    continuous), the size of the unit undergoing testing
    (particularly in relation to scale-up considerations),
    the time or quantity of material required to reach
    steady-state operating conditions, or test design
    considerations, such as mass balance calculations.
    B)
    In response to requests for authorization to ship,
    store, and conduct treatability studies on additional
    quantities after initiation or completion of initial
    treatability studies when: There has been an
    equipment or mechanical failure during the conduct of
    the treatability study, there is need to verify the
    results of a previously-conducted treatability study,
    there is a need to study and analyze alternative
    techniques within a previously-evaluated treatment
    process, or there is a need to do further evaluation
    of an ongoing treatability study to determine final
    specifications for treatment.
    C)
    The additional quantities allowed and timeframes
    allowed in subsections (e)(3)(A) and (e)(3)(B) above
    are subject to all the provisions in subsections
    (e)(1) and (e)(2)(B) through (e)(2)(F) above. The
    generator or sample collector shall apply to the
    Agency and provide in writing the following
    information:
    i)
    The reason why the
    generator or sample collector
    requires additional time or quantity of sample
    for the treatability study evaluation and the
    additional time or quantity needed;
    ii)
    Documentation accounting for all samples of
    hazardous waste from the wastestream that have
    been sent for or undergone treatability studies,
    including the date each previous sample from the
    waste stream was shipped, the quantity of each
    previous shipment, the laboratory or testing
    facility to which it was shipped, what
    treatability study processes were conducted on
    each sample shipped, and the available results
    of each treatability study;
    iii)
    A description of the technical modifications or
    change in specifications that will be evaluated
    and the expected results;
    iv)
    If such further study is being required due to
    equipment or mechanical failure, the applicant
    shall include information regarding the reason
    for the failure or breakdown and also include
    what procedures or equipment improvements have
    been made to protect against further breakdowns;
    and
    v)
    Such other information as the Agency determines
    53
    is necessary.
    4)
    Final Agency determinations pursuant to this subsection may
    be appealed to the Board.
    f)
    Samples undergoing treatability studies at laboratories or testing
    facilities. Samples undergoing treatability studies and the
    laboratory or testing facility conducting such treatability
    studies (to the extent such facilities are not otherwise subject
    to RCRA requirements) are not subject to any requirement of this
    Part, or of 35 Ill. Adm. Code 702, 703, 705, 722 through 726, and
    728 or to the notification requirements of Section 3010 of the
    Resource Conservation and Recovery Act, provided that the
    requirements of subsections (f)(1) through (f)(11) below are met.
    A mobile treatment unit may qualify as a testing facility subject
    to subsections (f)(1) through (f)(11) below. Where a group of
    mobile treatment units are located at the same site, the
    limitations specified in subsections (f)(1) through (f)(11) below
    apply to the entire group of mobile treatment units collectively
    as if the group were one mobile treatment unit.
    1)
    No less than 45 days before conducting treatability studies,
    the facility notifies the Agency in writing that it intends
    to conduct treatability studies under this subsection.
    2)
    The laboratory or testing facility conducting the
    treatability study has a USEPA identification number.
    3)
    No more than a total of 10,000 kg of "as received" media
    contaminated with non-acute hazardous waste, 2500 kg of
    media contaminated with acute hazardous waste, or 250 kg of
    other "as received" hazardous waste is subject to initiation
    of treatment in all treatability studies in any single day.
    "As received" waste refers to the waste as received in the
    shipment from the generator or sample collector.
    4)
    The quantity of "as received" hazardous waste stored at the
    facility for the purpose of evaluation in treatability
    studies does not exceed 10,000 kg, the total of which can
    include 10,000 kg of media contaminated with non-acute
    hazardous waste, 2500 kg of media contaminated with acute
    hazardous waste, 1000 kg of non-acute hazardous wastes other
    than contaminated media, and 1 kg of acute hazardous waste.
    This quantity limitation does not include treatment
    materials (including nonhazardous solid waste) added to "as
    received" hazardous waste.
    5)
    No more than 90 days have elapsed since the treatability
    study for the sample was completed, or no more than one year
    (two years for treatability studies involving
    bioremediation) has elapsed since the generator or sample
    collector shipped the sample to the laboratory or testing
    facility, whichever date first occurs. Up to 500 kg of
    treated material from a particular waste stream from
    treatability studies may be archived for future evaluation
    up to five years from the date of initial receipt.
    Quantities of materials archived are counted against the
    total storage limit for the facility.
    6)
    The treatability study does not involve the placement of
    hazardous waste on the land or open burning of hazardous
    54
    waste.
    7)
    The facility maintains records for three years following
    completion of each study that show compliance with the
    treatment rate limits and the storage time and quantity
    limits. The following specific information must be included
    for each treatability study conducted:
    A)
    The name, address, and USEPA identification number of
    the generator or sample collector of each waste
    sample;
    B)
    The date the shipment was received;
    C)
    The quantity of waste accepted;
    D)
    The quantity of "as received" waste in storage each
    day;
    E)
    The date the treatment study was initiated and the
    amount of "as received" waste introduced to treatment
    each day;
    F)
    The date the treatability study was concluded;
    G)
    The date any unused sample or residues generated from
    the treatability study were returned to the generator
    or sample collector or, if sent to a designated
    facility, the name of the facility and the USEPA
    identification number.
    8)
    The facility keeps, on-site, a copy of the
    treatability
    study contract and all shipping papers associated with the
    transport of treatability study samples to and from the
    facility for a period ending three years from the completion
    date of each treatability study.
    9)
    The facility prepares and submits a report to the Agency by
    March 15 of each year that estimates the number of studies
    and the amount of waste expected to be used in treatability
    studies during the current year, and includes the following
    information for the previous calendar year:
    A)
    The name, address, and USEPA identification number of
    the facility conducting the treatability studies;
    B)
    The types (by process) of treatability studies
    conducted;
    C)
    The names and addresses of persons for whom studies
    have been conducted (including their USEPA
    identification numbers);
    D)
    The total quantity of waste in storage each day;
    E)
    The quantity and types of waste subjected to
    treatability studies;
    F)
    When each treatability study was conducted; and
    G)
    The final disposi
    tion of residues and unused sample
    55
    from each treatability study.
    10)
    The facility determines whether any unused sample or
    residues generated by the treatability study are hazardous
    waste under Section 721.103 and, if so, are subject to 35
    Ill. Adm. Code 702, 703, and 721 through 728, unless the
    residues and unused samples are returned to the sample
    originator under the subsection (e) exemption above.
    11)
    The facility notifies the Agency by letter when the facility
    is no longer planning to conduct any treatability studies at
    the site.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 721.105
    Special Requirements for Hazardous Waste Generated by Small
    Quantity Generators
    a)
    A generator is a conditionally exempt small quantity generator in
    a calendar month if it generates no more than 100 kilograms of
    hazardous waste in that month. 35 Ill. Adm. Code 700 explains the
    relation of this to the 100 kg/mo exception of 35 Ill. Adm. Code
    809.
    b)
    Except for those wastes iden
    tified in subsections (e), (f), (g)
    and (j) below, a conditionally exempt small quantity generator's
    hazardous wastes are not subject to regulation under 35 Ill. Adm.
    Code 702, 703, 705 and 722 through 726 and 728, and the
    notification requirements of Section 3010 of Resource Conservation
    and Recovery Act, provided the generator complies with the
    requirements of subsections (f), (g) and (j) below.
    c)
    When making the quantity determinations of this Part and 35 Ill.
    Adm. Code 722, the generator must include all hazardous waste that
    it generates, except the following hazardous waste:
    1)
    Hazardous waste that is exempt from regulation under Section
    721.104(c) through (f), 721.106(a)(3), 721.107(a)(1), or
    721.108;
    2)
    Hazardous waste that is managed immediately upon generation
    only in on -site elementary neutralization units, wastewater
    treatment units, or totally enclosed treatment facilities,
    as defined in 35 Ill. Adm. Code 720.110;
    3)
    Hazardous waste that is recycled, without prior storage or
    accumulation, only in an on
    -site process subject to
    regulation under Section 721.106(c)(2);
    4)
    Hazardous waste that is used oil managed under the
    requirements of Section 721.106(a)(4) and 35 Ill. Adm. Code
    739;
    5)
    Hazardous waste that is spent lead
    -acid batteries managed
    under the requirements of 35 Ill. Adm. Code 726.Subpart G;
    and
    6)
    Hazardous waste that is universal waste managed under
    Section 721.109 and 35 Ill. Adm. Code 733.
    d)
    In determining the quantity of hazardous waste it generates, a
    56
    generator need not include:
    1)
    Hazardous waste when it is removed from on-site storage; or
    2)
    Hazardous waste produced by on-site treatment (including
    reclamation) of its hazardous waste so long as the hazardous
    waste that is treated was counted once; or
    3)
    Spent materials that are generated, reclaimed and
    subsequently reused on-site, so long as such spent materials
    have been counted once.
    e)
    If a generator generates acute hazardous waste in a calendar month
    in quantities greater than set forth below, all quantities of that
    acute hazardous waste are subject to full regulation under 35 Ill.
    Adm. Code 702, 703, 705 and 722 through 726 and 728, and the
    notification requirements of Section 3010 of the Resource
    Conservation and Recovery Act:
    1)
    A total of one kilogram of one or more of the acute
    hazardous wastes listed in Section 721.131, 721.132, or
    721.133(e); or
    2)
    A total of 100 kilograms of any residue or contaminated
    soil, waste or other debris resulting from the clean-up of a
    spill, into or on any land or water, of any one or more of
    the acute hazardous wastes listed in Section 721.131,
    721.132, or 721.133(e).
    BOARD NOTE: "Full regulation" means those regulations
    applicable to generators of greater than 1000 kg of non-
    acute hazardous waste in a calendar month.
    f)
    In order for acute hazardous wastes generated by a generator of
    acute hazardous wastes in quantities equal to or less than those
    set forth in subsection (e)(1) or (e)(2) above to be excluded from
    full regulation under this Section, the generator must comply with
    the following requirements:
    1)
    35 Ill. Adm. Code 722.111.
    2)
    The generator may accumulate acute hazardous waste on-site.
    If the generator accumulates at any time acute hazardous
    wastes in quantities greater than set forth in subsection
    (e)(1) or (e)(2) above, all of those accumulated wastes are
    subject to regulation under 35 Ill. Adm. Code 702, 703, 705
    and 722 through 726 and 728, and the applicable notification
    requirements of Section 3010 of the Resource Conservation
    and Recovery Act. The time period of 35 Ill. Adm. Code
    722.134(a), for accumulation of wastes on-site, begins when
    the accumulated wastes exceed the applicable exclusion
    limit.
    3)
    A conditionally exempt shall quantity generator may either
    treat or dispose of its acute hazardous waste in an on-site
    facility or ensure delivery to an off-site
    storage,
    treatment, storage, or disposal facility, provided that if
    the on-site or off-site facility is located in the United
    States, it fulfills either of which, if located in the United
    States, meets any of the following conditions:
    57
    A)
    The facility is permitted under 35 Ill. Adm. Code
    702
    and 703;
    B)
    The facility has interim status under 35 Ill. Adm.
    Code 702, 703 and 725;
    C)
    The facility is authorized to manage hazardous waste
    by a state with a hazardous waste management program
    approved by USEPA pursuant to 40 CFR 271;
    D)
    The facility is permitted, licensed
    , or registered by
    a state to manage municipal or industrial solid waste
    and, if managed in a municipal solid waste landfill
    facility, the landfill is subject to 35 Ill. Adm. Code
    810 through 817 or 40 CFR 258
    ;
    E)
    The facility is permitted, licensed, or registered by
    a state to manage non-municipal non-hazardous waste
    and, if managed in a non-municipal non-hazardous waste
    disposal unit after January 1, 1998, the unit is
    subject to the requirements of 40 CFR 257.5 through
    257.30;
    EF)
    The facility is a facility that:
    i)
    Beneficially uses or reuses or legitimately
    recycles or reclaims its waste; or
    ii)
    Treats its waste prior to beneficial use or
    reuse, or legitimate recycling or reclamation;
    or
    FG)
    For universal waste managed under 35 Ill. Adm. Code
    733 or 40 CFR 273 , the facility is a universal waste
    handler or destination facility subject to the
    requirements of 35 Ill. Adm. Code 733
    or 40 CFR 273 .
    g)
    In order for hazardous waste generated by a conditionally exempt
    small quantity generator in quantities of less than 100 kilograms
    of hazardous waste during a calendar month to be excluded from
    full regulation under this Section, the generator must comply with
    the following requirements:
    1)
    35 Ill. Adm. Code 722.111;
    2)
    The conditionally exempt small quantity generator may
    accumulate hazardous waste on-site. If it accumulates at
    any time more than a total of 1000 kilograms of the
    generator's hazardous waste, all of those accumulated wastes
    are subject to regulation under the special provisions of 35
    Ill. Adm. Code 722 applicable to generators of between 100
    kg and 1000 kg of hazardous waste in a calendar month as
    well as the requirements of 35 Ill. Adm. Code 702, 703, 705
    and 723 through 726 and 728, and the applicable notification
    requirements of Section 3010 of the Resource Conservation
    and Recovery Act. The time period of 35 Ill. Adm. Code
    722.134(d) for accumulation of wastes on-site begins for a
    small quantity generator when the accumulated wastes exceed
    1000 kilograms;
    3)
    A conditionally exempt small quantity generator may either
    58
    treat or dispose of its hazardous waste in an on-site
    facility or ensure delivery to an off-site
    storage,
    treatment, storage, or disposal facility,
    provided that if
    the on-site or off-site facility is located in
    either of
    which, if located in
    the United States,
    it fulfills meets any
    of the following conditions:
    A)
    The facility is permitted under 35 Ill. Adm. Code 702
    and 702 and 703;
    B)
    The facility has interim status under 35 Ill. Adm.
    Code 702, 703 and 725;
    C)
    The facility is authorized to manage hazardous waste
    by a state with a hazardous waste management program
    approved by USEPA under 40 CFR 271 (1986);
    D)
    The facility is permitted, licensed
    , or registered by
    a state to manage municipal
    or industrial solid waste
    and, if managed in a municipal solid waste landfill
    facility, the landfill is subject to 35 Ill. Adm. Code
    810 through 817 or 40 CFR 258
    ;
    E)
    The facility is permitted, licensed, or registered by
    a state to manage non-municipal non-hazardous waste
    and, if managed in a non-municipal non-hazardous waste
    disposal unit after January 1, 1998, the unit is
    subject to the requirements of 40 CFR 257.5 through
    257.30;
    EF)
    The facility is a facility that:
    i)
    Beneficially uses or re-uses, or legitimately
    recycles or reclaims the small quantity
    generator's waste; or
    ii)
    Treats its waste prior to beneficial use or re-
    use, or legitimate recycling or reclamation; or
    FG)
    For universal waste managed under 35 Ill. Adm. Code
    733 or 40 CFR 273 , the facility is a universal waste
    handler or destination facility subject to the
    requirements of 35 Ill. Adm. Code 733
    or 40 CFR 273 .
    h)
    Hazardous waste subject to the reduced requirements of this
    Section may be mixed with non-hazardous waste and remain subject
    to these reduced requirements even though the resultant mixture
    exceeds the quantity limitations identified in this Section,
    unless the mixture meets any of the characteristics of hazardous
    wastes identified in Subpart C.
    i)
    If a small quantity generator mixes a solid waste with a hazardous
    waste that exceeds a quantity exclusion level of this Section, the
    mixture is subject to full regulation.
    j)
    If a conditionally exempt small quantity generator's hazardous
    wastes are mixed with used oil, the mixture is subject to 35 Ill.
    Adm. Code 739, if it is destined to be burned for energy recovery.
    Any material produced from such a mixture by processing,
    blending, or other treatment is also so regulated if it is
    destined to be burned for energy recovery.
    59
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 721.106
    Requirements for Recyclable Materials
    a)
    Recyclable materials:
    1)
    Hazardous wastes that are recycled are subject to the
    requirements for generators, transporters, and storage
    facilities of subsections (b) and (c) below, except for the
    materials listed in subsections (a)(2) and (a)(3) below.
    Hazardous wastes that are recycled will be known as
    "recyclable materials".
    2)
    The following recyclable materials are not subject to the
    requirements of this Section but are regulated under 35 Ill.
    Adm. Code 726.Subparts C through H and all applicable
    provisions in 35 Ill. Adm. Code 702, 703, and 705.
    A)
    Recyclable materials used in a manner constituting
    disposal (35 Ill. Adm. Code 726.Subpart C);
    B)
    Hazardous wastes burned for energy recovery in boilers
    and industrial furnaces that are not regulated under
    35 Ill. Adm. Code 724.Subpart O or 725.Subpart O (35
    Ill. Adm. Code 726.Subpart H);
    C)
    Recyclable materials from which precious metals are
    reclaimed (35 Ill. Adm. Code 726.Subpart F);
    D)
    Spent lead-acid batteries that are being reclaimed (35
    Ill. Adm. Code 726.Subpart G).
    3)
    The following recyclable materials are not subject to
    regulation under 35 Ill. Adm. Code 722 through 726, 728, or
    702, 703, or 705 and are not subject to the notification
    requirements of Section 3010 of the Resource Conservation
    and Recovery Act:
    A)
    Industrial ethyl alcohol that is reclaimed except
    that, unless provided otherwise in an international
    agreement as specified in 35 Ill. Adm. Code 722.158:
    i)
    A person initiating a shipment for reclamation
    in a foreign country and any intermediary
    arranging for the shipment shall comply with the
    requirements applicable to a primary exporter in
    35 Ill. Adm. Code 722.153; 722.156(a)(1) through
    (a)(4), (a)(6), and (b); and 722.157; shall
    export such materials only upon consent of the
    receiving country and in conformance with the
    USEPA Acknowledgement of Consent, as defined in
    35 Ill. Adm. Code 722.Subpart E; and shall
    provide a copy of the USEPA Acknowledgement of
    Consent to the shipment to the transporter
    transporting the shipment for export;
    ii)
    Transporters transporting a shipment for export
    shall not accept a shipment if the transporter
    knows that the shipment does not conform to the
    60
    USEPA Acknowledgement of Consent, shall ensure
    that a copy of the USEPA Acknowledgement of
    Consent accompanies the shipment, and shall
    ensure that it is delivered to the facility
    designated by the person initiating the
    shipment;
    B)
    Scrap metal;
    C)
    Fuels produced from t
    he refining of oil-bearing
    hazardous wastes along with normal process streams at
    a petroleum refining facility if such wastes result
    from normal petroleum refining, production, and
    transportation practices (this exemption does not
    apply to fuels produced from oil recovered from oil-
    bearing hazardous waste where such recovered oil is
    already excluded under Section 721.104(a)(12));
    D)
    Petroleum refining wastes.
    i)
    Hazardous waste fuel produced from oil-bearing
    hazardous wastes from petroleum refining,
    production, or transportation practices or
    produced from oil reclaimed from such hazardous
    wastes, where such hazardous wastes are
    reintroduced into a process that does not use
    distillation or does not produce products from
    crude oil, so long as the resulting fuel meets
    the used oil specification under 35 Ill. Adm.
    Code 726.140(e) and so long as no other
    hazardous wastes are used to produce the
    hazardous waste fuel;
    ii)
    Hazardous waste fuel produced from oil-bearing
    hazardous waste from petroleum refining
    production, and transportation practices, where
    such hazardous wastes are reintroduced into a
    refining process after a point at which
    contaminants are removed, so long as the fuel
    meets the used oil fuel specification under 35
    Ill. Adm. Code 726.140(e); and
    iii)
    Oil reclaimed from oil-bearing hazardous wastes
    from petroleum refining, production, and
    transportation practices, which reclaimed oil is
    burned as a fuel without reintroduction to a
    refining process, so long as the reclaimed oil
    meets the used oil fuel specification under 35
    Ill. Adm. Code 726.140(e); and
    E)
    Petroleum coke produced from petroleum refinery
    hazardous wastes containing oil by the same person
    that generated the wastes unless the resulting coke
    product exceeds one or more of the characteristics of
    hazardous waste in 721.Subpart C.
    4)
    Used oil that is recycled and is also a hazardous waste
    solely because it exhibits a hazardous characteristic is not
    subject to the requirements of 35 Ill. Adm. Code 720 through
    728, but it is regulated under 35 Ill. Adm. Code 739. Used
    oil that is recycled includes any used oil that is reused
    61
    for any purpose following its original use (including the
    purpose for which the oil was originally used). Such term
    includes, but is not limited to, oil that is re-refined,
    reclaimed, burned for energy recovery, or reprocessed.
    5)
    Hazardous waste that is exported to or imported from
    designated member countries of the Organization for Economic
    Cooperation and Development (OECD), as defined in Section
    722.158(a)(1), for the purpose of recovery is subject to the
    requirements of 35 Ill. Adm. Code 722.Subpart H if it is
    subject to either the hazardous waste manifesting
    requirements of 35 Ill. Adm. Code 722 or the universal waste
    management standards of 35 Ill. Adm. Code 733.
    b)
    Generators and transporters of recyclable materials are subject to
    the applicable requirements of 35 Ill. Adm. Code 722 and 723 and
    the notification requirements under Section 3010 of the Resource
    Conservation and Recovery Act, except as provided in subsection
    (a) above.
    c)
    Storage and recycling:
    1)
    Owners or operators of facilities that store recyclable
    materials before they are recycled are regulated under all
    applicable provisions of 35 Ill. Adm. Code 702, 703, and
    705; 724.Subparts A through L, AA,
    and BB, and CC ; and
    725.Subparts A through L, AA,
    and BB, and CC ; 726; 728; and
    the notification requirement under Section 3010 of the
    Resource Conservation and Recovery Act, except as provided
    in subsection (a) above. (The recycling process itself is
    exempt from regulation, except as provided in subsection (d)
    below.)
    2)
    Owners or operators of facilities that recycle recyclable
    materials without storing them before they are recycled are
    subject to the following requirements, except as provided in
    subsection (a) above:
    A)
    Notification requirements under Section 3010 of the
    Resource Conservation and Recovery Act,
    B)
    35 Ill. Adm. Code 725.171 and 725.172 (dealing with
    the use of the manifest and manifest discrepancies),
    and
    C)
    subsection (d) below.
    d)
    Owners or operators of facilities required to have a RCRA permit
    pursuant to 35 Ill. Adm. Code 703 with hazardous waste management
    units that recycle hazardous wastes are subject to 35 Ill. Adm.
    Code 724.Subparts AA and BB and 725.Subparts AA and BB.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART D: LISTS OF HAZARDOUS WASTE
    Section 721.132
    Hazardous Waste from Specific Sources
    The following solid wastes are listed hazardous wastes from specific sources
    unless they are excluded under 35 Ill. Adm. Code 720.120 and 720.122 and
    62
    listed in Section 721.Appendix I.
    EPA
    Hazardous
    Waste No.
    Industry and Hazardous Waste
    Hazard
    Code
    Wood Preservation:
    K001
    Bottom sediment sludge from the treatment of waste
    -
    waters from wood preserving processes that use
    creosote or penta
    chloro phenol.
    (T)
    Inorganic Pigments:
    K002
    Wastewater treatment sludge from the production of
    chrome yellow and orange pigments.
    (T)
    K003
    Wastewater treatment sludge from the production of
    molybdate orange pigments.
    (T)
    K004
    Wastewater treatment sludge from the production of
    zinc yellow pigments.
    (T)
    K005
    Wastewater treatment sludge from the production of
    chrome green pigments.
    (T)
    K006
    Wastewater treatment sludge from the production of
    chrome oxide green pigments (anhydrous and
    hydrated).
    (T)
    K007
    Wastewater treatment sludge from the production of
    iron blue pigments.
    (T)
    K008
    Oven residue from the production of chrome oxide
    green pigments.
    (T)
    Organic Chemicals:
    K009
    Distillation bottoms from the production of
    acetaldehyde from ethylene.
    (T)
    K010
    Distillation side cuts from the production of
    acetaldehyde from ethylene.
    (T)
    K011
    Bottom stream from the wastewater stripper in the
    production of acrylonitrile.
    (R,T)
    K013
    Bottom stream from the acetonitrile column in the
    production of acrylonitrile.
    (T)
    K014
    Bottoms from the acetonitrile purification column in
    the production of acrylonitrile.
    (T)
    K015
    Still bottoms from the distillation of benzyl
    chloride.
    (T)
    K016
    Heavy ends or distillation residues from the
    production of carbon tetra
    chloride.
    (T)
    K017
    Heavy ends (still bottoms) from the purification
    column in the production of epichloro
    hydrin.
    (T)
    63
    K018
    Heavy ends from the fractionation column in ethyl
    chloride production.
    (T)
    K019
    Heavy ends from the distillation of ethylene di
    -
    chloride in ethylene dichloride production.
    (T)
    K020
    Heavy ends from the distillation of vinyl chloride
    in vinyl chloride monomer production.
    (T)
    K021
    Aqueous spent antimony catalyst waste from
    fluoromethanes production.
    (T)
    K022
    Distillation bottom tars from the production of
    phenol/acetone from cumene.
    (T)
    K023
    Distillation light ends from the production of
    phthalic anhydride from naphthalene.
    (T)
    K024
    Distillation bottoms from the production of phthalic
    anhydride from naphthalene.
    (T)
    K093
    Distillation light ends from the production of
    phthalic anhydride from ortho-xylene.
    (T)
    K094
    Distillation bottoms from the production of phthalic
    anhydride from ortho-xylene.
    (T)
    K025
    Distillation bottoms from the production of
    nitrobenzene by the nitration of benzene.
    (T)
    K026
    Stripping still tails from the production of methyl
    ethyl pyridines.
    (T)
    K027
    Centrifuge and distillation residues from toluene
    diisocyanate production.
    (R,T)
    K028
    Spent catalyst from the hydrochlorinator reactor in
    the production of 1,1,1-tri
    chloro ethane.
    (T)
    K029
    Waste from the product stream stripper in the
    production of 1,1,1-tri
    chloro ethane.
    (T)
    K095
    Distillation bottoms from the production of 1,1,1-
    trichloro ethane.
    (T)
    K096
    Heavy ends from the heavy ends column from the
    production of 1,1,1-tri
    chloro ethane.
    (T)
    K030
    Column bottoms or heavy ends from the combined
    production of tri
    chloro ethylene and perchloro
    -
    ethylene.
    (T)
    K083
    Distillation bottoms from aniline production.
    (T)
    K103
    Process residues from aniline extraction from the
    production of aniline.
    (T)
    K104
    Combined wastewater streams generated from
    nitrobenzene/aniline production.
    (T)
    64
    K085
    Distillation or fractionation column bottoms
    from the production of chloro
    benzenes.
    (T)
    K105
    Separated aqueous stream from the reactor product
    washing step in the production of chloro
    benzenes.
    (T)
    K107
    Column bottoms from product separation from the
    production of 1,1-di
    methylhydrazine (UDMH) from
    carboxylic acid hydrazides.
    (C,T)
    K108
    Condensed column overheads from product separation
    and condensed reactor vent gases from the production
    of 1,1-di methylhydrazine (UDMH) from carboxylic acid
    hydrazides.
    (I,T)
    K109
    Spent filter cartridges from the product
    purification from the production of 1,1-di
    -
    methylhydrazine (UDMH) from carboxylic acid
    hydrazides.
    (T)
    K110
    Condensed column overheads from intermediate
    separation from the production of 1,1-di
    -
    methylhydrazine (UDMH) from carboxylic acid
    hydrazides.
    (T)
    K111
    Product wastewaters from the production of di
    -
    nitrotoluene via nitration of toluene.
    (C,T)
    K112
    Reaction by-product water from the drying column in
    the production of toluenedi
    amine via hydrogenati
    on
    of dinitrotoluene.
    (T)
    K113
    Condensed liquid light ends from the purification of
    toluenedi amine in the production of toluenedi
    amine
    via hydrogenation of dinitrotoluene.
    (T)
    K114
    Vicinals from the purification of toluene-di
    amine in
    the production of toluenedi
    amine via hydrogenation
    of dinitrotoluene.
    (T)
    K115
    Heavy ends from the purification of toluenedi
    amine
    in the production of toluenedi
    amine via
    hydrogenation of di
    nitrotoluene.
    (T)
    K116
    Organic condensate from the solvent recovery column
    in the production of toluene di
    isocyanate via
    phosgenation of toluenedi
    amine.
    (T)
    K117
    Wastewater from the reactor vent gas scrubber in the
    production of ethylene di
    bromide via bromination of
    ethene.
    (T)
    K118
    Spent adsorbent solids from purification of ethylene
    dibromide in the production of ethylene di
    bromide
    via bromination of ethene.
    (T)
    K136
    Still bottoms from the purification of ethylene di
    -
    bromide in the production of ethylene di
    bromide via
    bromination of ethene.
    (T)
    K156
    Organic waste (including heavy ends, still bottoms,
    (T)
    65
    light ends, spent solvents, filtrates, and
    decantates) from the production of carbamates and
    carbamoyl oximes.
    (This listing does not apply to
    wastes generated from the manufacture of 3-iodo-2-
    propynyl n -butylcarbamate.)
    K157
    Wastewaters (including scrubber waters, condenser
    waters, washwaters, and separation waters) from the
    production of carbamates and carbamoyl oximes.
      
    (This listing does not apply to wastes generated
    from the manufacture of 3-iodo-2-propynyl
    n-butylcarbamate.)
    (T)
    K158
    Bag house dusts and filter/separation solids from
    the production of carbamates and carbamoyl oximes.
      
    (This listing does not apply to wastes generated
    from the manufacture of 3-iodo-2-propynyl
    n-butylcarbamate.)
    (T)
    K159
    Organics from the treatment of thiocarbamate wastes.
    (T)
    K160
    Solids (including filter wastes, separation solids,
    and spent catalysts) from the production of
    thiocarbamates and solids from the treatment of
    thiocarbamate wastes.
    (T)
    K161
    Purification solids (including filtration,
    evaporation, and centrifugation solids), bag house
    dust and floor sweepings from the production of
    dithiocarbamate acids and their salts. (This listing
    does not include K125 or K126.)
    (R,T)
    Inorganic Chemicals:
    K071
    Brine purification muds from the mercury cell
    process in chlorine production, where separately
    prepurified brine is not used.
    (T)
    K073
    Chlorinated hydrocarbon waste from the purification
    step of the diaphragm cell process using graphite
    anodes in chlorine production.
    (T)
    K106
    Wastewater treatment sludge from the mercury cell
    process in chlorine production.
    (T)
    Pesticides:
    K031
    By-product salts generated in the production of MSMA
    and cacodylic acid.
    (T)
    K032
    Wastewater treatment sludge from the production of
    chlordane.
    (T)
    K033
    Wastewater and scrub water from the chlorination of
    cyclopenta diene in the production of chlordane.
    (T)
    K034
    Filter solids from the filtration of hexa
    chloro -
    cyclopenta diene in the production of chlordane.
    (T)
    K097
    Vacuum stripper discharge from the chlordane
    (T)
    66
    chlorinator in the production of chlordane.
    K035
    Wastewater treatment sludges generated in the
    production of creosote.
    (T)
    K036
    Still bottoms from toluene reclamation distillation
    in the production of di
    sulfoton.
    (T)
    K037
    Wastewater treatment sludges from the production of
    disulfoton.
    (T)
    K038
    Wastewater from the washing and stripping of phorate
    production.
    (T)
    K039
    Filter cake from the filtration of di
    ethylphosphoro -
    dithioic acid in the production of ph
    orate.
    (T)
    K040
    Wastewater treatment sludge from the production of
    phorate.
    (T)
    K041
    Wastewater treatment sludge from the production of
    toxaphene.
    (T)
    K098
    Untreated process wastewater from the production of
    toxaphene.
    (T)
    K042
    Heavy ends or distillation residues from the
    distillation of tetra
    chloro benzene in the production
    of 2,4,5-T.
    (T)
    K043
    2,6-Di chloro phenol waste from the production of 2,4-
    D.
    (T)
    K099
    Untreated wastewater from the production of 2,4-D.
    (T)
    K123
    Process wastewater (including supernates, filtrates
    and washwaters) from the production of ethylene
    bis-
    dithiocarbamic acid and its salts.
    (T)
    K124
    Reactor vent scrubber water from the production of
    ethylene bisdithiocarbamic acid and its salts.
    (C,T)
    K125
    Filtration, evaporation and centrifugation solids
    from the production of ethylene
    bisdithiocarbamic
    acid and its salts.
    (T)
    K126
    Baghouse dust and floor sweepings in milling and
    packaging operations from the production or
    formulation of ethylene
    bisdithiocarbamic a cid and
    its salts.
    (T)
    K131
    Wastewater from the reactor and spent sulfuric acid
    from the acid dryer from the production of methyl
    bromide.
    (C,T)
    K132
    Spent absorbent and wastewater separator solids from
    the production of methyl bromide.
    (T)
    Explosives:
    K044
    Wastewater treatment sludges from the manufacturing
    and processing of explosives.
    (R)
    67
    K045
    Spent carbon from the treatment of wastewater
    containing explosives.
    (R)
    K046
    Wastewater treatment sludges from the manufacturing,
    formulation and loading of lead-based initiating
    compounds.
    (T)
    K047
    Pink/red water from TNT operations.
    (R)
    Petroleum Refining:
    K048
    Dissolved air flotation (DAF) float from the
    petroleum refining industry.
    (T)
    K049
    Slop oil emulsion solids from the petroleum refining
    industry.
    (T)
    K050
    Heat exchanger bundle cleaning sludge from the
    petroleum refining industry.
    (T)
    K051
    API separator sludge from the petroleum refining
    industry.
    (T)
    K052
    Tank bottoms (leaded) from the petroleum refining
    industry.
    (T)
    Iron and Steel:
    K061
    Emission control dust/sludge from the primary
    production of steel in electric furnaces.
    (T)
    K062
    Spent pickle liquor generated by steel finishing
    operations of facilities within the iron and steel
    industry (SIC Codes 331 and 332) (as defined in 35
    Ill. Adm. Code 720.110).
    (C,T)
    Primary Copper:
    K064
    Acid plant blowdown slurry or sludge resulting from
    the thickening of blowdown slurry from primary
    copper production.
    (T)
    Primary Lead:
    K065
    Surface impoundment solids contained in and dredged
    from surface impoundments at primary lead smelting
    facilities.
    (T)
    Primary Zinc:
    K066
    Sludge from treatment of process wastewater or acid
    plant blowdown from primary zinc production.
    (T)
    BOARD NOTE: This waste listing is the subject of a
    judicial remand in American Mining Congress v. EPA,
    907 F.2d 1179 (D.D.C. 1990). The Board intends that
    this listing not become enforceable in Illinois
    until the first date upon which the Board RCRA
    program becomes "not equivalent to the Federal
    program", within the meaning of Section 3006(b) of
    68
    the RCRA Act, 42 U.S.C. 6926(b), the Board RCRA
    rules become "less stringent" than the USEPA rules,
    as this phrase is used in Section 3009, 42 U.S.C.
    6929, or the Board RCRA rules are not "identical in
    substance" with the federal rules as that term is
    intended by 415 ILCS 5/7.2 and 22.4 as a result of
    some action by USEPA with regard to this listing in
    response to the American Mining Congress remand.
    Primary Aluminum:
    K088
    Spent potliners from primary aluminum reduction.
    (T)
    Ferroalloys:
    K090
    Emission control dust or sludge from
    ferrochromiumsilicon production.
    (T)
    K091
    Emission control dust or sludge from ferrochromium
    production.
    (T)
    Secondary Lead:
    K069
    Emission control dust/sludge from secondary lead
    smelting.
    (T)
    BOARD NOTE: This listing is administratively stayed
    for sludge generated from secondary acid scrubber
    systems. The stay will remain in effect until this
    note is removed.
    K100
    Waste leaching solution from acid leaching of
    emission control dust/sludge from secondary lead
    smelting.
    (T)
    Veterinary Pharmaceuticals:
    K084
    Wastewater treatment sludges generated during the
    production of veterinary pharmaceuticals from
    arsenic or organo-arsenic compounds.
    (T)
    K101
    Distillation tar residues from the distillation of
    aniline-based compounds in the production of
    veterinary pharmaceuticals from arsenic or organo
    -
    arsenic compounds.
    (T)
    K102
    Residue from use of activated carbon for
    decolorization in the production of veterinary
    pharmaceuticals from arsenic or organo-arsenic
    compounds.
    (T)
    Ink Formulation:
    K086
    Solvent washes and sludges, caustic washes and
    sludges, or water washes and sludges from cleaning
    tubs and equipment used in the formulation of ink
    from pigments, dryers, soaps and stabilizers
    containing chromium and lead.
    (T)
    Coking:
    K060
    Ammonia still lime sludge from coking operations.
    (T)
    69
    K087
    Decanter tank tar sludge from coking operations.
    (T)
    K141
    Process residues from the recovery of coal tar,
    including, but not limited to, collecting sump
    residues from the production of coke from coal or
    the recovery of coke by-products produced from coal.
    This listing does not include K087 (decanter tank
    tar sludges from coking operations).
    (T)
    K142
    Tar storage tank residues from the production of
    coke from coal or from the recovery of coke by-
    products produced from coal.
    (T)
    K143
    Process residues from the recovery of light oil,
    including, but not limited to, those generated in
    stills, decanters, and wash oil recovery units from
    the recovery of coke by-products produced from coal.
    (T)
    K144
    Wastewater sump residues from light oil refining,
    including, but not limited to, intercepting or
    contamination sump sludges from the recovery of coke
    by-products produced from coal.
    (T)
    K145
    Residues from naphthalene collection and recovery
    operations from the recovery of coke by-products
    produced from coal.
    (T)
    K147
    Tar storage tank residues from coal tar refining.
    (T)
    K148
    Residues from coal tar distillation, including but
    not limited to, still bottoms.
    (T)
    K149
    Distillation bottoms from the production of alpha-
    (or methyl-) chlorinated toluenes, ring-chlorinated
    toluenes, benzoyl chlorides, and compounds with
    mixtures of these functional groups. (This waste
    does not include still bottoms from the distillation
    of benzyl chloride.)
    (T)
    K150
    Organic residuals, excluding spent carbon adsorbent,
    from the spent chlorine gas and hydrochloric acid
    recovery processes associated with the production of
    alpha- (or methyl-) chlorinated toluenes, ring-
    chlorinated toluenes, benzoyl chlorides, and
    compounds with mixtures of these functional groups.
    (T)
    K151
    Wastewater treatment sludges, excluding
    neutralization and biological sludges, generated
    during the treatment of wastewaters from the
    production of alpha- (or methyl-) chlorinated
    toluenes, ring-chlorinated toluenes, benzoyl
    chlorides, and compounds with mixtures of these
    functional groups.
    (T)
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 721.133
    Discarded Commer cial Chemical Products, Off-Specification
    Species, Container Residues, and Spill Residues Thereof
    The following materials or items are hazardous wastes if and when they are
    70
    discarded or intended to be discarded as described in Section
    721.102(a)(2)(A), when they are mixed with waste oil or used oil or other
    material and applied to the land for dust suppression or road treatment, when
    they are otherwise applied to the land in lieu of their original intended use
    or when they are contained in products that are applied to land in lieu of
    their original intended use, or when, in lieu of their original intended use,
    they are produced for use as (or as a component of) a fuel, distributed for
    use as a fuel, or burned as a fuel.
    a)
    Any commercial chemical product, or manufacturing chemical
    intermediate having the generic name listed in subsection (e) or
    (f) below.
    b)
    Any off-specification commercial chemical product or manufacturing
    chemical intermediate which, if it met specifications, would have
    the generic name listed in subsection (e) or (f) below.
    c)
    Any residue remaining in a container or inner liner removed from a
    container that has held any commercial chemical product or
    manufacturing chemical intermediate having the generic name listed
    in subsection (e) or (f) below, unless the container is empty as
    defined in Section 721.107(b)(3).
    BOARD NOTE: Unless the residue is being beneficially used or
    reused, or legitimately recycled or reclaimed, or being
    accumulated, stored, transported, or treated prior to such use,
    reuse, recycling, or reclamation, the Board considers the residue
    to be intended for discard, and thus a hazardous waste. An
    example of a legitimate reuse of the residue would be where the
    residue remains in the container and the container is used to hold
    the same commercial chemical product or manufacturing chemical
    intermediate it previously held. An example of the discard of the
    residue would be where the drum is sent to a drum reconditioner
    that reconditions the drum but discards the residue.
    d)
    Any residue or contaminated soil, water, or other debris resulting
    from the cleanup of a spill into or on any land or water of any
    commercial chemical product or manufacturing chemical intermediate
    having the generic name listed in subsection (e) or (f) below, or
    any residue or contaminated soil, water, or other debris resulting
    from the cleanup of a spill into or on any land or water, of any
    off-specification chemical product or manufacturing chemical
    intermediate which, if it met specifications, would have the
    generic name listed in subsection (e) or (f) below.
    BOARD NOTE: The phrase "commercial chemical product or
    manufacturing chemical intermediate having the generic name listed
    in ..." refers to a chemical substance that is manufactured or
    formulated for commercial or manufacturing use which consists of
    the commercially pure grade of the chemical, any technical grades
    of the chemical that are produced or marketed, and all
    formulations in which the chemical is the sole active ingredient.
    It does not refer to a material, such as a manufacturing process
    waste, that contains any of the substances listed in subsection
    (e) or (f) below. Where a manufacturing process waste is deemed
    to be a hazardous waste because it contains a substance listed in
    subsection (e) or (f) below, such waste will be listed in either
    Sections 721.131 or 721.132 or will be identified as a hazardous
    waste by the characteristics set forth in Subpart C.
    e)
    The commercial chemical products, manufacturing chemical
    71
    intermediates, or off-specification commercial chemical products
    or manufacturing chemical intermediates referred to in subsections
    (a) through (d) above, are identified as acute hazardous waste (H)
    and are subject to the small quantity exclusion defined in Section
    721.105(e). These wastes and their corresponding EPA Hazardous
    Waste Numbers are:
    BOARD NOTE: For the convenience of the regulated community the
    primary hazardous properties of these materials have been
    indicated by the letters T (Toxicity), and R (Reactivity). The
    absence of a letter indicates that the compound only is listed for
    acute toxicity.
    Hazardous
    Waste No.
    Chemical
    Abstracts
    No.
    Substance
    P023
    107-20-0
    Acetaldehyde, chloro-
    P002
    591-08-2
    Acetamide, N-(amino
    thioxomethyl)
    P057
    640-19-7
    Acetamide, 2-fluoro-
    P058
    62-74-8
    Acetic acid, fluoro
    -, sodium salt
    P002
    591-08-2
    1-Acetyl-2-thiourea
    P003
    107-02-8
    Acrolein
    P070
    116-06-3
    Aldicarb
    P203
    1646-88-4
    Aldicarb sulfone
    P004
    309-00-2
    Aldrin
    P005
    107-18-6
    Allyl alcohol
    P006
    20859-73-8
    Aluminum phosphide (R,T)
    P007
    2763-96-4
    5-(Amino methyl)-3-isoxazolol
    P008
    504-24-5
    4-Amino pyridine
    P009
    131-74-8
    Ammonium picrate (R)
    P119
    7803-55-6
    Ammonium vanadate
    P099
    506-61-6
    Argentate(1-), bis
    (cyano-C) -, potassium
    P010
    7778-39-4
    Arsenic acid H
    3
    AsO
    4
    P012
    1327-53-3
    Arsenic oxide As
    2
    O
    3
    P011
    1303-28-2
    Arsenic oxide As
    2
    O
    5
    P011
    1303-28-2
    Arsenic pentoxide
    P012
    1327-53-3
    Arsenic tri oxide
    P038
    692-42-2
    Arsine, di ethyl-
    P036
    696-28-6
    Arsonous di chloride, phenyl-
    P054
    151-56-4
    Aziridine
    P067
    75-55-8
    Aziridine, 2-methyl
    P013
    542-62-1
    Barium cyanide
    P024
    106-47-8
    Benzenamine, 4-chloro-
    P077
    100-01-6
    Benzenamine, 4-nitro-
    P028
    100-44-7
    Benzene, (chloro methyl)-
    P042
    51-43-4
    1,2-Benzenediol, 4-[1-hydroxy-2-
    (methyl amino) ethyl] -, (R)-
    P046
    122-09-8
    Benzeneethanamine, alpha,alpha-di
    -
    methyl-
    P014
    108-98-5
    Benzenethiol
    P127
    1563-66-2
    7-Benzofuranol, 2,3-dihydro-2,2-
    dimethyl -, methylcarbamate
    P188
    57-64-7
    Benzoic acid, 2-hydroxy
    -, compound with
    (3aS-cis)-1,2,3,3a,8,8a-hexahydro-
    1,3a,8-tri methylpyrrolo [2,3-b] indol-5-
    yl methyl carbamate ester (1:1)
    P001
    81-81-2
    *
    2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-
    oxo-1-phenylbutyl)
    -, and salts, when
    present at concentrations greater than
    0.3%
    72
    P028
    100-44-7
    Benzyl chloride
    P015
    7440-41-7
    Beryllium powder
    P017
    598-31-2
    Bromoacetone
    P018
    357-57-3
    Brucine
    P045
    39196-18-6
    2-Butanone, 3,3-dimethyl-1-(methyl
    -
    thio)-, O-[methyl amino) carbonyl] oxime
    P021
    592-01-8
    Calcium cyanide
    P021
    592-01-8
    Calcium cyanide Ca(CN)
    2
    P189
    55285-14-8
    Carbamic acid, [(dibutyl
    amino)- thio] -
    methyl -, 2,3-dihydro-2,2-dimethyl-7-
    benzofuranyl ester
    P191
    644-64-4
    Carbamic acid, dimethyl
    -, 1-[(dimethyl-
    amino) carbonyl]-5-methyl-1H-pyrazol-3-
    yl ester
    P192
    119-38-0
    Carbamic acid, dimethyl
    -, 3-methyl-1-
    (1-methyl ethyl)-1H-pyrazol-5-yl ester
    P190
    1129-41-5
    Carbamic acid, methyl
    -, 3-methyl phenyl
    ester
    P127
    1563-66-2
    Carbofuran
    P022
    75-15-0
    Carbon di sulfide
    P095
    75-44-5
    Carbonic di chloride
    P189
    55285-14-8
    Carbosulfan
    P023
    107-20-0
    Chloro acetaldehyde
    P024
    106-47-8
    p-Chloroaniline
    P026
    5344-82-1
    1-(o-Chloro phenyl) thiourea
    P027
    542-76-7
    3-Chloropropionitrile
    P029
    544-92-3
    Copper cyanide
    P029
    544-92-3
    Copper cyanide CuCN
    P202
    64-00-6
    m-Cumenyl methylcarbamate
    P030
    Cyanides (soluble cyanide salts), not
    otherwise specified
    P031
    460-19-5
    Cyanogen
    P033
    506-77-4
    Cyanogen chloride
    P033
    506-77-4
    Cyanogen chloride CNCl
    P034
    131-89-5
    2-Cyclohexyl-4,6-di
    nitrophenol
    P016
    542-88-1
    Dichloro methyl ether
    P036
    696-28-6
    Dichloro phenylarsine
    P037
    60-57-1
    Dieldrin
    P038
    692-42-2
    Diethyl arsine
    P041
    311-45-5
    Diethyl-p-nitrophenyl phosphate
    P040
    297-97-2
    O,O-Di ethyl O-pyrazinyl
    phosphorothioate
    P043
    55-91-4
    Diisopropylfluorophosphate (DFP)
    P191
    644-64-4
    Dimetilan
    P004
    309-00-2
    1,4,5,8-Di methanonaphthalene,
    1,2,3,4,10,10-hexa
    chloro-1,4,4a,5,8,8a-
    hexahydro-,
    (1alpha,4alpha,4abeta,5alpha,8alpha,8ab
    eta)-
    P060
    465-73-6
    1,4,5,8-Di-methanonaphthalene,
    1,2,3,4,10,10-hexa
    chloro-1,4,4a,5,8,8a-
    hexahydro-,
    (1alpha,4alpha,4abeta,5beta,8beta,8abet
    a)-
    P037
    60-57-1
    2,7:3,6-Di methanona phth[2,3-b] oxirene,
    3,4,5,6,9,9-hexa chloro-
    1a,2,2a,3,6,6a,7,7a-octahydro
    -,
    (1aalpha,2beta,2aalpha,3beta,6beta,6aal
    pha,7beta,7aalpha)-
    P051
    72-20-8
    *
    2,7:3,6-Di methanonaphth[2,3-b]
    oxirene,
    3,4,5,6,9,9-hexa chloro-
    73
    1a,2,2a,3,6,6a,7,7a-octahydro
    -,
    (1aalpha,2beta,2abeta,3alpha,6alpha,6ab
    eta,7beta,7aalpha)
    -, and metabolites
    P044
    60-51-5
    Dimethoate
    P046
    122-09-8
    alpha,alpha-Di methyl phenethyl amine
    P047
    534-52-1
    *
    4,6-Di nitro-o-cresol and salts
    P048
    51-28-5
    2,4-Di nitrophenol
    P020
    88-85-7
    Dinoseb
    P085
    152-16-9
    Diphosphoramide, octamethyl-
    P111
    107-49-3
    Diphosphoric acid, tetra
    ethyl ester
    P039
    298-04-4
    Disulfoton
    P049
    541-53-7
    Dithiobiuret
    P185
    26419-73-8
    1,3-Dithiolane-2-carbox
    aldehyde, 2,4-
    dimethyl -, O-[(methyl amino)- carbonyl]
    -
    oxime
    P050
    115-29-7
    Endosulfan
    P088
    145-73-3
    Endothall
    P051
    72-20-8
    Endrin
    P051
    72-20-8
    Endrin, and metabolites
    P042
    51-43-4
    Epinephrine
    P031
    460-19-5
    Ethanedi nitrile
    P194
    23135-22-0
    Ethanimidothioc acid, 2-(di
    methyl -
    amino)-N-[[(methyl
    amino) carbonyl] oxy]-
    2-oxo-, methyl ester
    P066
    16752-77-5
    Ethanimidothioic acid, N-[[(methyl
    -
    amino) carbonyl] oxy]-, methyl ester
    P101
    107-12-0
    Ethyl cyanide
    P054
    151-56-4
    Ethylenimine
    P097
    52-85-7
    Famphur
    P056
    7782-41-4
    Fluorine
    P057
    640-19-7
    Fluoroacetamide
    P058
    62-74-8
    Fluoroacetic acid, sodium salt
    P198
    23422-53-9
    Formetanate hydro
    chloride
    P197
    17702-57-7
    Formparanate
    P065
    628-86-4
    Fulminic acid, mercury (2+) salt (R,T)
    P059
    76-44-8
    Heptachlor
    P062
    757-58-4
    Hexaethyl tetra phosphate
    P116
    79-19-6
    Hydrazinecarbothioamide
    P068
    60-34-4
    Hydrazine, methyl-
    P063
    74-90-8
    Hydrocyanic acid
    P063
    74-90-8
    Hydrogen cyanide
    P096
    7803-51-2
    Hydrogen phosphide
    P060
    465-73-6
    Isodrin
    P192
    119-38-0
    Isolan
    P202
    64-00-6
    3-Isopropyl phenyl-N-methyl carbamate
    P007
    2763-96-4
    3(2H)-Isoxazolone, 5-(amino
    methyl)-
    P196
    15339-36-3
    Manganese, bis(dimethyl
    carbamo -
    dithioato-S,S')-
    P196
    15339-36-3
    Manganese dimethyl
    dithio carbamate
    P092
    62-38-4
    Mercury, (acetato-O)
    phenyl-
    P065
    628-86-4
    Mercury fulminate (R,T)
    P082
    62-75-9
    Methanamine, N-methyl-N-nitroso-
    P064
    624-83-9
    Methane, isocyanato-
    P016
    542-88-1
    Methane, oxy bis[chloro-
    P112
    509-14-8
    Methane, tetra nitro- (R)
    P118
    75-70-7
    Methanethiol, tri
    chloro-
    P198
    23422-53-9
    Methanimidamide, N,N-dimethyl-N'-[3-
    [[(methyl amino)-carbonyl] oxy]phenyl] -,
    monohydro chloride
    P197
    17702-57-7
    Methanimidamide, N,N-dimethyl-N'-[2-
    methyl-4-[[(methyl
    amino) carbonyl] oxy]-
    74
    phenyl]-
    P199
    2032-65-7
    Methiocarb
    P050
    115-29-7
    6,9-Methano-2,4,3-benzodi
    oxathiepen,
    6,7,8,9,10,10-hexa
    chloro-1,5, 5a,6,9,9a-
    hexahydro-, 3-oxide
    P059
    76-44-8
    4,7-Methano-1H-indene, 1,4,5,6,7,8,8-
    heptachloro-3a,4,7,7a-tetra
    hydro-
    P066
    16752-77-5
    Methomyl
    P068
    60-34-4
    Methyl hydrazine
    P064
    624-83-9
    Methyl isocyanate
    P069
    75-86-5
    2-Methyllactonitrile
    P071
    298-00-0
    Methyl parathion
    P190
    1129-41-5
    Metolcarb
    P129
    315-8-4
    Mexacarbate
    P072
    86-88-4
    alpha-Naphthylthiourea
    P073
    13463-39-3
    Nickel carbonyl
    P073
    13463-39-3
    Nickel carbonyl Ni(CO)
    4
    , (T-4)-
    P074
    557-19-7
    Nickel cyanide
    P074
    557-19-7
    Nickel cyanide Ni(CN)
    2
    P075
    54-11-5
    *
    Nicotine, and salts
    P076
    10102-43-9
    Nitric oxide
    P077
    100-01-6
    p-Nitroaniline
    P078
    10102-44-0
    Nitrogen dioxide
    P076
    10102-43-9
    Nitrogen oxide NO
    P078
    10102-44-0
    Nitrogen oxide NO
    2
    P081
    55-63-0
    Nitroglycerine (R)
    P082
    62-75-9
    N-Nitrosodi methyl amine
    P084
    4549-40-0
    N-Nitrosomethyl vinylamine
    P085
    152-16-9
    Octamethyl pyrophosphoramide
    P087
    20816-12-0
    Osmium oxide OsO
    4
    , (T-4)-
    P087
    20816-12-0
    Osmium tetroxide
    P088
    145-73-3
    7-Oxabicyclo[2.2.1]
    heptane-2,3-di -
    carboxylic acid
    P194
    23135-22-0
    Oxamyl
    P089
    56-38-2
    Parathion
    P034
    131-89-5
    Phenol, 2-cyclohexyl-4,6-di
    nitro-
    P128
    315-18-4
    Phenol, 4-(dimethyl
    amino)-3,5-
    dimethyl -, methyl carbamate (ester)
    P199
    2032-65-7
    Phenol, (3,5-dimethyl-4-(methyl
    thio)-,
    methyl carbamate
    P048
    51-28-5
    Phenol, 2,4-di nitro-
    P047
    534-52-1
    *
    Phenol, 2-methyl-4,6-di
    nitro-, and
    salts
    P202
    64-00-6
    Phenol, 3-(1-methyl
    ethyl) -, methyl
    carbamate
    P201
    2631-37-0
    Phenol, 3-methyl-5-(1-methyl
    ethyl) -,
    methyl carbamate
    P020
    88-85-7
    Phenol, 2-(1-methylpropyl)-4,6-di
    nitro-
    P009
    131-74-8
    Phenol, 2,4,6-tri
    nitro-, ammonium salt
    (R)
    P092
    62-38-4
    Phenylmercury acetate
    P093
    103-85-5
    Phenylthiourea
    P094
    298-02-2
    Phorate
    P095
    75-44-5
    Phosgene
    P096
    7803-51-2
    Phosphine
    P041
    311-45-5
    Phosphoric acid, di
    ethyl 4-nitrophenyl
    ester
    P039
    298-04-4
    Phosphorodi thioic acid, O,O-di
    ethyl S-
    [2-(ethyl thio)ethyl] ester
    P094
    298-02-2
    Phosphorodi thioic acid, O,O-di
    ethyl S-
    [(ethyl thio)methyl] ester
    75
    P044
    60-51-5
    Phosphorodi thioic acid, O,O-di
    methyl S-
    [2-(methyl amino)-2 -oxoethyl] ester
    P043
    55-91-4
    Phosphorofluoridic acid, bis
    (1-methyl -
    ethyl) ester
    P089
    56-38-2
    Phosphorothioic acid, O,O-di
    ethyl O-(4-
    nitrophenyl) ester
    P040
    297-97-2
    Phosphorothioic acid, O,O-di
    ethyl O-
    pyrazinyl ester
    P097
    52-85-7
    Phosphorothioic acid, O-[4-[(di
    methyl -
    amino) sulfonyl)] phenyl] O,O-di methyl
    ester
    P071
    298-00-0
    Phosphorothioic acid, O,O-di
    methyl O-
    (4-nitrophenyl) ester
    P204
    57-47-6
    Physostigmine
    P188
    57-64-7
    Physostigmine salicylate
    P110
    78-00-2
    Plumbane, tetra ethyl-
    P098
    151-50-8
    Potassium cyanide
    P098
    151-50-8
    Potassium cyanide KCN
    P099
    506-61-6
    Potassium silver cyanide
    P201
    2631-37-0
    Promecarb
    P203
    1646-88-4
    Propanal, 2-methyl-2-(methyl-
    sulfonyl) -, O-[(methyl amino) carbonyl]
    oxime
    P070
    116-06-3
    Propanal, 2-methyl-2-(methyl
    thio)-, O-
    [(methyl amino) carbonyl] oxime
    P101
    107-12-0
    Propane nitrile
    P027
    542-76-7
    Propane nitrile, 3-chloro-
    P069
    75-86-5
    Propane nitrile, 2-hydroxy-2-methyl-
    P081
    55-63-0
    1,2,3-Propane triol, tri nitrate- (R)
    P017
    598-31-2
    2-Propanone, 1-bromo-
    P102
    107-19-7
    Propargyl alcohol
    P003
    107-02-8
    2-Propenal
    P005
    107-18-6
    2-Propen-1-ol
    P067
    75-55-8
    1,2-Propylenimine
    P102
    107-19-7
    2-Propyn-1-ol
    P008
    504-24-5
    4-Pyridinamine
    P075
    54-11-5
    *
    Pyridine, 3-(1-methyl-2-pyrrolidinyl)
    -,
    (S)- and salts
    P204
    57-47-6
    Pyrrolo [2,3-b] indol-5-ol,
    1,2,3,3a,8,8a-hexa
    hydro-1,3a,8-tri -
    methyl -, methyl carbamate (ester), (3aS-
    cis)-
    P114
    12039-52-0
    Selenious acid, di
    thallium (1+) salt
    P103
    630-10-4
    Selenourea
    P104
    506-64-9
    Silver cyanide
    P104
    506-64-9
    Silver cyanide AgCN
    P105
    26628-22-8
    Sodium azide
    P106
    143-33-9
    Sodium cyanide
    P106
    143-33-9
    Sodium cyanide NaCN
    P108
    57-24-9
    *
    Strychnidin-10-one, and salts
    P018
    357-57-3
    Strychnidin-10-one, 2,3-di
    methoxy-
    P108
    57-24-9
    *
    Strychnine and salts
    P115
    7446-18-6
    Sulfuric acid, di
    thallium (1+) salt
    P109
    3689-24-5
    Tetraethyldithiopyrophosphate
    P110
    78-00-2
    Tetraethyl lead
    P111
    107-49-3
    Tetraethylpyrophosphate
    P112
    509-14-8
    Tetranitromethane (R)
    P062
    757-58-4
    Tetraphosphoric acid, hexa
    ethyl ester
    P113
    1314-32-5
    Thallic oxide
    P113
    1314-32-5
    Thallium oxide Tl
    2
    O
    3
    P114
    12039-52-0
    Thallium (I) selenite
    76
    P115
    7446-18-6
    Thallium (I) sulfate
    P109
    3689-24-5
    Thiodiphosphoric acid, tetra
    ethyl ester
    P045
    39196-18-4
    Thiofanox
    P049
    541-53-7
    Thioimidodicarbonic di amide
    [(H
    2
    N)C(S)]
    2
    NH
    P014
    108-98-5
    Thiophenol
    P116
    79-19-6
    Thiosemicarbazide
    P026
    5344-82-1
    Thiourea, (2-chloro
    phenyl)-
    P072
    86-88-4
    Thiourea, 1-naphthalenyl-
    P093
    103-85-5
    Thiourea, phenyl-
    P123
    8001-35-2
    Toxaphene
    P185
    26419-73-8
    Tirpate
    P118
    75-70-7
    Trichloro methane thiol
    P119
    7803-55-6
    Vanadic acid, ammonium salt
    P120
    1314-62-1
    Vanadium oxide V
    2
    O
    5
    P120
    1314-62-1
    Vanadium pentoxide
    P084
    4549-40-0
    Vinylamine, N-methyl-N-nitroso-
    P001
    81-81-2
    *
    Warfarin, and salts, when present at
    concentrations greater than 0.3%
    P121
    557-21-1
    Zinc cyanide
    P121
    557-21-1
    Zinc cyanide Zn(CN)
    2
    P205
    137-30-4
    Zinc, bis (dimethyl carbamo dithioato-
    S,S')-
    P122
    1314-84-7
    Zinc phosphide Zn
    3
    P
    2
    , when present at
    concentrations greater than 10% (R,T)
    P205
    137-30-4
    Ziram
    BOARD NOTE: An asterisk (*) following the CAS number indicates
    that the CAS number is given for the parent compound only.
    f)
    The commercial chemical products, manufacturing chemical
    intermediates, or off-specification commercial chemical products
    referred to in subsections (a) through (d) above, are identified
    as toxic wastes (T) unless otherwise designated and are subject to
    the small quantity exclusion defined in Section 721.105(a) and
    (g). These wastes and their corresponding EPA Hazardous Waste
    Numbers are:
    BOARD NOTE: For the convenience of the regulated community, the
    primary hazardous properties of these materials have been
    indicated by the letters T (Toxicity), R (Reactivity), I
    (Ignitability), and C (Corrosivity). The absence of a letter
    indicates that the compound is only listed for toxicity.
    Hazardous
    Waste No.
    Chemical
    Abstracts
    No.
    Substance
    U394
    30558-43-1
    A2213
    U365
    2212-67-1
    H-Azepine-1-carbo
    thioic acid, hexa
    -
    hydro-, S-ethyl ester
    U001
    75-07-0
    Acetaldehyde (I)
    U034
    75-87-6
    Acetaldehyde, tri
    chloro -
    U187
    62-44-2
    Acetamide, N-(4-ethoxyphenyl)-
    U005
    53-96-3
    Acetamide, N-9H-fluoren-2-yl-
    U240
    P 94-75-7
    Acetic acid, (2,4-di
    chloro phenoxy) -,
    salts and esters
    U112
    141-78-6
    Acetic acid, ethyl ester (I)
    U144
    301-04-2
    Acetic acid, lead (2+) salt
    U214
    563-68-8
    Acetic acid, thallium (1+) salt
    See F027
    93-76-5
    Acetic acid, (2,4,5-tri
    chloro phenoxy)-
    77
    UOO2
    67-64-1
    Acetone (I)
    UOO3
    75-05-8
    Acetonitrile (I,T)
    U004
    98-86-2
    Acetophenone
    U005
    53-96-3
    2-Acetyl aminofluorene
    U006
    75-36-5
    Acetyl chloride (C,R,T)
    U007
    79-06-1
    Acrylamide
    U008
    79-10-7
    Acrylic acid (I)
    U009
    107-13-1
    Acrylonitrile
    U011
    61-82-5
    Amitrole
    U012
    62-53-3
    Aniline (I,T)
    U136
    75-60-5
    Arsinic acid, di methyl-
    U014
    492-80-8
    Auramine
    U015
    115-02-6
    Azaserine
    U010
    50-07-7
    Azirino [2',3':3,4] pyrrolo [1,2-a] indole-
    4,7-di one, 6-amino-8-[[(amino
    carbonyl) -
    oxy]methyl]-1,1a,2,8,8a,8b-hexa
    hydro-
    8a-methoxy-5-methyl
    -, [1a-S-
    (1aalpha,8beta,8aalpha,8balpha)]-
    U280
    101-27-9
    Barban
    U278
    22781-23-3
    Bendiocarb
    U364
    22961-82-6
    Bendiocarb phenol
    U271
    17804-35-2
    Benomyl
    U157
    56-49-5
    Benz[j]aceanthrylene, 1,2-di
    hydro-3-
    methyl-
    U016
    225-51-4
    Benz(c)acridine
    U017
    98-87-3
    Benzal chloride
    U192
    23950-58-5
    Benzamide, 3,5-di
    chloro -N-(1,1-di -
    methyl-2-propynyl)-
    U018
    56-55-3
    Benz[a]anthracene
    U094
    57-97-6
    Benz[a]anthracene, 7,12-di
    methyl-
    U012
    62-53-3
    Benzen amine (I,T)
    U014
    492-80-8
    Benzen amine, 4,4'-carbonimidoyl
    bis[N,N-
    dimethyl-
    U049
    3165-93-3
    Benzen amine, 4-chloro -2-methyl -,
    hydrochloride
    U093
    60-11-7
    Benzen amine, N,N-di methyl-4-(phenyl -
    azo)-
    U328
    95-53-4
    Benzen amine, 2-methyl-
    U353
    106-49-0
    Benzen amine, 4-methyl-
    U158
    101-14-4
    Benzen amine, 4,4'-methylene
    bis[2-
    chloro -
    U222
    636-21-5
    Benzen amine, 2-methyl -, hydrochloride
    U181
    99-55-8
    Benzen amine, 2-methyl-5-nitro-
    U019
    71-43-2
    Benzene (I,T)
    U038
    510-15-6
    Benzeneacetic acid, 4-chloro
    -alpha-(4-
    chloro phenyl)-alpha-hydroxy
    -, ethyl
    ester
    U030
    101-55-3
    Benzene, 1-bromo-4-phenoxy-
    U035
    305-03-3
    Benzenebutanoic acid, 4-[bis
    (2-chloro -
    ethyl) amino]-
    U037
    108-90-7
    Benzene, chloro -
    U221
    25376-45-8
    Benzenedi amine, ar-methyl-
    U028
    117-81-7
    1,2-Benzenedi carboxylic acid, bis
    (2-
    ethylhexyl) ester
    U069
    84-74-2
    1,2-Benzenedi carboxylic acid, di
    butyl
    ester
    U088
    84-66-2
    1,2-Benzenedi carboxylic acid, di
    ethyl
    ester
    U102
    131-11-3
    1,2-Benzenedi carboxylic acid, di
    methyl
    ester
    U107
    117-84-0
    1,2-Benzenedi carboxylic acid, di
    octyl
    78
    ester
    U070
    95-50-1
    Benzene, 1,2-di chloro -
    U071
    541-73-1
    Benzene, 1,3-di chloro -
    U072
    106-46-7
    Benzene, 1,4-di chloro -
    U060
    72-54-8
    Benzene, 1,1'-(2,2-di
    chloro ethylidene) -
    bis[4-chloro -
    U017
    98-87-3
    Benzene, (di chloro methyl)-
    U223
    26471-62-5
    Benzene, 1,3-di isocyanatomethyl- (R,T)
    U239
    1330-20-7
    Benzene, di methyl- (I,T)
    U201
    108-46-3
    1,3-Benzenedi ol
    U127
    118-74-1
    Benzene, hexa chloro -
    U056
    110-82-7
    Benzene, hexa hydro- (I)
    U220
    108-88-3
    Benzene, methyl-
    U105
    121-14-2
    Benzene, 1-methyl-2,4-di
    nitro-
    U106
    606-20-2
    Benzene, 2-methyl-1,3-di
    nitro-
    U055
    98-82-8
    Benzene, (1-methyl
    ethyl)- (I)
    U169
    98-95-3
    Benzene, nitro-
    U183
    608-93-5
    Benzene, penta chloro -
    U185
    82-68-8
    Benzene, penta chloro nitro-
    U020
    98-09-9
    Benzenesulfonic acid chloride (C,R)
    U020
    98-09-9
    Benzenesulfonyl chloride (C,R)
    U207
    95-94-3
    Benzene, 1,2,4,5-tetra
    chloro -
    U061
    50-29-3
    Benzene, 1,1'-(2,2,2-tri
    chloro ethyl-
    idene) bis[4-chloro -
    U247
    72-43-5
    Benzene, 1,1'-(2,2,2-tri
    chloro ethyl-
    idene) bis[4-methoxy-
    U023
    98-07-7
    Benzene, (tri chloro methyl)-
    U234
    99-35-4
    Benzene, 1,3,5-tri
    nitro-
    U021
    92-87-5
    Benzidene
    U202
    P 81-07-2
    1,2-Benzisothiazol-3(2H)-one, 1,1-di
    -
    oxide, and salts
    U203
    94-59-7
    1,3-Benzodi oxole, 5-(2-propenyl)-
    U141
    120-58-1
    1,3-Benzodi oxole, 5-(1-propenyl)-
    U090
    94-58-6
    1,3-Benzodi oxole, 5-propyl-
    U278
    22781-23-3
    1,3-Benzo dioxol-4-ol, 2,2-di
    methyl -,
    methyl carbamate
    U364
    22961-82-6
    1,3-Benzo dioxol-4-ol, 2,2-dimethyl-
    U367
    1563-38-8
    7-Benzo furanol, 2,3-di hydro-2,2-di -
    methyl-
    U064
    189-55-9
    Benzo[rst]pentaphene
    U248
    P 81-81-2
    2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-
    oxo-1-phenyl butyl) -, and salts, when
    present at concentrations of 0.3% or
    less
    U022
    50-32-8
    Benzo[a]pyrene
    U197
    106-51-4
    p-Benzoquinone
    U023
    98-07-7
    Benzotri chloride (C,R,T)
    U085
    1464-53-5
    2,2'-Bioxirane
    U021
    92-87-5
    [1,1'-Biphenyl]-4,4'-di
    amine
    U073
    91-94-1
    [1,1'-Biphenyl]-4,4'-di
    amine, 3,3'-di -
    chloro -
    U091
    119-90-4
    [1,1'-Biphenyl]-4,4'-di
    amine, 3,3'-di -
    methoxy-
    U095
    119-93-7
    [1,1'-Biphenyl]-4,4'-di
    amine, 3,3'-di -
    methyl-
    U401
    97-74-5
    Bis(dimethyl thiocarbamoyl) sulfide
    U400
    120-54-7
    Bis(penta methylene) thiuram tetra sulfide
    U225
    75-25-2
    Bromoform
    U030
    101-55-3
    4-Bromophenyl phenyl ether
    U128
    87-68-3
    1,3-Butadi ene, 1,1,2,3,4,4-hexa
    chloro -
    U172
    924-16-3
    1-Butan amine, N-butyl-N-nitroso-
    79
    U031
    71-36-3
    1-Butanol (I)
    U159
    78-93-3
    2-Butanone (I,T)
    U160
    1338-23-4
    2-Butanone, peroxide (R,T)
    U053
    4170-30-3
    2-Butenal
    U074
    764-41-0
    2-Butene, 1,4-di chloro - (I,T)
    U143
    303-34-4
    2-Butenoic acid, 2-methyl
    -, 7-[[2,3-di -
    hydroxy-2-(1-methoxy
    ethyl)-3-methyl-1-
    oxobutoxy] methyl]-2,3,5,7a-tetra
    hydro-
    1H-pyrrolizin-1-yl ester, [1S-
    [1alpha(Z), 7(2S*,3R*), 7aalpha]]-
    U031
    71-36-3
    n-Butyl alcohol (I)
    U392
    2008-41-5
    Butylate
    U136
    75-60-5
    Cacodylic acid
    U032
    13765-19-0
    Calcium chromate
    U372
    10605-21-7
    Carbamic acid, 1H-benz
    imidazol-2-yl,
    methyl ester
    U271
    17804-35-2
    Carbamic acid, [1-[(butyl
    amino) -
    carbonyl]-1H-benz
    imidazol-2-yl] -,
    methyl ester
    U375
    55406-53-6
    Carbamic acid, butyl
    -, 3-iodo-2-
    propynyl ester
    U280
    101-27-9
    Carbamic acid, (3-chloro
    phenyl) -, 4-
    chloro-2-butynyl ester
    U238
    51-79-6
    Carbamic acid, ethyl ester
    U178
    615-53-2
    Carbamic acid, methyl
    nitroso -, ethyl
    ester
    U373
    122-42-9
    Carbamic acid, phenyl
    -, 1-methyl ethyl
    ester
    U409
    23564-05-8
    Carbamic acid, [1,2-phenylenebis
    (imino -
    carbono thioyl)] bis-, dimethyl ester
    U097
    79-44-7
    Carbamic chloride, di
    methyl-
    U379
    136-30-1
    Carbamo dithioic acid, dibutyl, sodium
    salt
    U277
    95-06-7
    Carbamo dithioic acid, diethyl
    -, 2-
    chloro-2-propenyl ester
    U381
    148-18-5
    Carbamo dithioic acid, diethyl
    -, sodium
    salt
    U383
    128-03-0
    Carbamodithioic acid, dimethyl,
    potassium salt
    U382
    128-04-1
    Carbamo dithioic acid, dimethyl
    -, sodium
    salt
    U376
    144-34-3
    Carbamo dithioic acid, dimethyl
    -, tetra -
    anhydro sulfide with ortho
    thioselenious
    acid
    U114
    P 111-54-6
    Carbamodi thioic acid, 1,2-ethanedi
    yl-
    bis-, salts and esters
    U378
    51026-28-9
    Carbamo dithioic acid, (hydroxymethyl)
    -
    methyl -, mono potassium salt
    U384
    137-42-8
    Carbamo dithioic acid, methyl
    -, mono -
    sodium salt
    U377
    137-41-7
    Carbamo dithioic acid, methyl,- mono
    -
    potassium salt
    U062
    2303-16-4
    Carbamothioic acid, bis
    (1-methyl -
    ethyl) -, S-(2,3-di chloro -2-propenyl)
    ester
    U389
    2303-17-5
    Carbamo thioic acid, bis(1-methyl
    -
    ethyl) -, S-(2,3,3-tri chloro-2-propenyl)
    ester
    U392
    2008-41-5
    Carbamo thioic acid, bis(2-methyl
    -
    propyl) -, S-ethyl ester
    U391
    1114-71-2
    Carbamo thioic acid, butyl
    ethyl-, S-
    80
    propyl ester
    U386
    1134-23-2
    Carbamo thioic acid, cyclo
    hexylethyl-,
    S-ethyl ester
    U390
    759-94-4
    Carbamo thioic acid, dipropyl
    -, S-ethyl
    ester
    U387
    52888-80-9
    Carbamo thioic acid, dipropyl
    -, S-
    (phenyl methyl) ester
    U385
    1929-77-7
    Carbamo thioic acid, dipropyl
    -, S-propyl
    ester
    U279
    63-25-2
    Carbaryl
    U372
    10605-21-7
    Carbendazim
    U367
    1563-38-8
    Carbofuran phenol
    U215
    6533-73-9
    Carbonic acid, di
    thallium (1+) salt
    U033
    353-50-4
    Carbonic di fluoride
    U156
    79-22-1
    Carbonochloridic acid, methyl ester
    (I,T)
    U033
    353-50-4
    Carbon oxyfluoride (R,T)
    U211
    56-23-5
    Carbon tetra chloride
    U034
    75-87-6
    Chloral
    U035
    305-03-3
    Chlorambucil
    U036
    57-74-9
    Chlordanealpha and gamma isomers
    U026
    494-03-1
    Chlornaphazin
    U037
    108-90-7
    Chloro benzene
    U038
    510-15-6
    Chloro benzilate
    U039
    59-50-7
    p-Chloro -m-cresol
    U042
    110-75-8
    2-Chloro ethyl vinyl ether
    U044
    67-66-3
    Chloro form
    U046
    107-30-2
    Chloro methyl methyl ether
    U047
    91-58-7
    beta-Chloro naphthalene
    U048
    95-57-8
    o-Chloro phenol
    U049
    3165-93-3
    4-Chloro -o-toluidine, hydrochloride
    U032
    13765-19-0
    Chromic acid H
    2
    CrO
    4
    , calcium salt
    U050
    218-01-9
    Chrysene
    U393
    137-29-1
    Copper, bis(dimethyl
    carbamo dithioato-
    S,S')-
    U393
    137-29-1
    Copper dimethyl dithio carbamate
    U051
    Creosote
    U052
    1319-77-3
    Cresol (Cresylic acid)
    U053
    4170-30-3
    Crotonaldehyde
    U055
    98-82-8
    Cumeme (I)
    U246
    506-68-3
    Cyanogen bromide CNBr
    U386
    1134-23-2
    Cycloate
    U197
    106-51-4
    2,5-Cyclohexa diene-1,4-di one
    U056
    110-82-7
    Cyclohexane (I)
    U129
    58-89-9
    Cyclohexane, 1,2,3,4,5,6-hexa
    chloro -,
    (1alpha,2alpha,3beta,4alpha,5alpha,6bet
    a)-
    U057
    108-94-1
    Cyclohexanone (I)
    U130
    77-47-4
    1,3-Cyclopenta diene, 1,2,3,4,5,5-hexa
    -
    chloro -
    U058
    50-18-0
    Cyclophosphamide
    U240
    P 94-75-7
    2,4-D, salts and esters
    U059
    20830-81-3
    Daunomycin
    U366
    533-74-4
    Dazomet
    U060
    72-54-8
    DDD
    U061
    50-29-3
    DDT
    U062
    2303-16-4
    Diallate
    U063
    53-70-3
    Dibenz[a,h]anthracene
    U064
    189-55-9
    Dibenzo[a,i]pyrene
    U066
    96-12-8
    1,2-Di bromo-3-chloro propane
    U069
    84-74-2
    Dibutyl phthalate
    81
    U070
    95-50-1
    o-Dichloro benzene
    U071
    541-73-1
    m-Dichloro benzene
    U072
    106-46-7
    p-Dichloro benzene
    U073
    91-94-1
    3,3'-Di chloro benzidine
    U074
    764-41-0
    1,4-Di chloro -2-butene (I,T)
    U075
    75-71-8
    Dichloro difluoromethane
    U078
    75-35-4
    1,1-Di chloro ethylene
    U079
    156-60-5
    1,2-Di chloro ethylene
    U025
    111-44-4
    Dichloro ethyl ether
    U027
    108-60-1
    Dichloro isopropyl ether
    U024
    111-91-1
    Dichloro methoxy ethane
    U081
    120-83-2
    2,4-Di chloro phenol
    U082
    87-65-0
    2,6-Di chloro phenol
    U084
    542-75-6
    1,3-Di chloro propene
    U085
    1464-53-5
    1,2:3,4-Di epoxybutane (I,T)
    U395
    5952-26-1
    Diethylene glycol, dicarbamate
    U108
    123-91-1
    1,4-Di ethyleneoxide
    U028
    117-81-7
    Diethylhexyl phthalate
    U086
    1615-80-1
    N,N'-Di ethylhydrazine
    U087
    3288-58-2
    O,O-Di ethyl S-methyl di
    thiophosphate
    U088
    84-66-2
    Diethyl phthalate
    U089
    56-53-1
    Diethylstilbestrol
    U090
    94-58-6
    Dihydrosafrole
    U091
    119-90-4
    3,3'-Di methoxybenzidine
    U092
    124-40-3
    Dimethyl amine (I)
    U093
    60-11-7
    p-Dimethyl aminoazobenzene
    U094
    57-97-6
    7,12-Di methyl benz[a]anthracene
    U095
    119-93-7
    3,3'-Di methyl benzidine
    U096
    80-15-9
    alpha, alpha-Di methyl -
    benzylhydroperoxide (R)
    U097
    79-44-7
    Dimethyl carbamoyl chloride
    U098
    57-14-7
    1,1-Di methyl hydrazine
    U099
    540-73-8
    1,2-Di methyl hydrazine
    U101
    105-67-9
    2,4-Di methyl phenol
    U102
    131-11-3
    Dimethyl phthalate
    U103
    77-78-1
    Dimethyl sulfate
    U105
    121-14-2
    2,4-Di nitrotoluene
    U106
    606-20-2
    2,6-Di nitrotoluene
    U107
    117-84-0
    Di-n-octyl phthalate
    U108
    123-91-1
    1,4-Di oxane
    U109
    122-66-7
    1,2-Di phenyl hydrazine
    U110
    142-84-7
    Dipropyl amine (I)
    U111
    621-64-7
    Di-n-propyl nitros amine
    U403
    97-77-8
    Disulfiram
    U041
    106-89-8
    Epichloro hydrin
    U390
    759-94-4
    EPTC
    U001
    75-07-0
    Ethanal (I)
    U404
    121-44-8
    Ethanamine, N,N-diethyl-
    U174
    55-18-5
    Ethanamine, N- ethyl-N-nitroso-
    U155
    91-80-5
    1,2-Ethanedi amine, N,N-di methyl-N'-2-
    pyridinyl-N'-(2-thienyl
    methyl)-
    U067
    106-93-4
    Ethane, 1,2-di bromo-
    U076
    75-34-3
    Ethane, 1,1-di chloro -
    U077
    107-06-2
    Ethane, 1,2-di chloro -
    U131
    67-72-1
    Ethane, hexa chloro -
    U024
    111-91-1
    Ethane, 1,1'-[methyl
    enebis(oxy)] bis[2-
    chloro -
    U117
    60-29-7
    Ethane, 1,1'-oxy bis- (I)
    U025
    111-44-4
    Ethane, 1,1'-oxy bis[2-chloro -
    U184
    76-01-7
    Ethane, penta chloro -
    U208
    630-20-6
    Ethane, 1,1,1,2-tetra
    chloro -
    82
    U209
    79-34-5
    Ethane, 1,1,2,2-tetra
    chloro -
    U218
    62-55-5
    Ethanethioamide
    U226
    71-55-6
    Ethane, 1,1,1-tri
    chloro -
    U227
    79-00-5
    Ethane, 1,1,2-tri
    chloro -
    U410
    59669-26-0
    Ethanimidothioic acid, N,N'- [thiobis
    -
    [(methyl imino) carbonyl oxy]]bis-,
    dimethyl ester
    U394
    30558-43-1
    Ethanimido thioic acid, 2-(dimethyl
    -
    amino)-N-hydroxy-2-oxo
    -, methyl ester
    U359
    110-80-5
    Ethanol, 2-ethoxy-
    U173
    1116-54-7
    Ethanol, 2,2'-(nitroso
    imino) bis-
    U395
    5952-26-1
    Ethanol, 2,2'-oxy
    bis-, dicarbamate
    U004
    98-86-2
    Ethanone, 1-phenyl-
    U043
    75-01-4
    Ethene, chloro -
    U042
    110-75-8
    Ethene, (2-chloro
    ethoxy)-
    U078
    75-35-4
    Ethene, 1,1-di chloro -
    U079
    156-60-5
    Ethene, 1,2-di chloro -, (E)-
    U210
    127-18-4
    Ethene, tetra chloro -
    U228
    79-01-6
    Ethene, tri chloro -
    U112
    141-78-6
    Ethyl acetate (I)
    U113
    140-88-5
    Ethyl acrylate (I)
    U238
    51-79-6
    Ethyl carbamate (urethane)
    U117
    60-29-7
    Ethyl ether
    U114
    P 111-54-6
    Ethylenebisdithiocarbamic acid, salts
    and esters
    U067
    106-93-4
    Ethylene di bromide
    U077
    107-06-2
    Ethylene di chloride
    U359
    110-80-5
    Ethylene glycol monoethyl ether
    U115
    75-21-8
    Ethylene oxide (I,T)
    U116
    96-45-7
    Ethylenethiourea
    U076
    75-34-3
    Ethylidene di chloride
    U118
    97-63-2
    Ethyl methacrylate
    U119
    62-50-0
    Ethyl methanesulfonate
    U407
    14324-55-1
    Ethyl Ziram
    U396
    14484-64-1
    Ferbam
    U120
    206-44-0
    Fluoranthene
    U122
    50-00-0
    Formaldehyde
    U123
    64-18-6
    Formic acid (C,T)
    U124
    110-00-9
    Furan (I)
    U125
    98-01-1
    2-Furancarboxaldehyde (I)
    U147
    108-31-6
    2,5-Furandi one
    U213
    109-99-9
    Furan, tetra hydro- (I)
    U125
    98-01-1
    Furfural (I)
    U124
    110-00-9
    Furfuran (I)
    U206
    18883-66-4
    Glucopyranose, 2-deoxy-2-(3-methyl-3-
    nitroso ureido) -, D-
    U206
    18883-66-4
    D-Glucose, 2-deoxy-2-[[(
    methyl nitroso -
    amino)-carbonyl] amino]-
    U126
    765-34-4
    Glycidylaldehyde
    U163
    70-25-7
    Guanidine, N-methyl-N'-nitro-N-nitroso-
    U127
    118-74-1
    Hexachloro benzene
    U128
    87-68-3
    Hexachloro butadi ene
    U130
    77-47-4
    Hexachloro cyclopenta diene
    U131
    67-72-1
    Hexachloro ethane
    U132
    70-30-4
    Hexachloro phene
    U243
    1888-71-7
    Hexachloro propene
    U133
    302-01-2
    Hydrazine (R,T)
    U086
    1615-80-1
    Hydrazine, 1,2-di
    ethyl-
    U098
    57-14-7
    Hydrazine, 1,1-di
    methyl-
    U099
    540-73-8
    Hydrazine, 1,2-di
    methyl-
    U109
    122-66-7
    Hydrazine, 1,2-di
    phenyl-
    83
    U134
    7664-39-3
    Hydrofluoric acid (C,T)
    U134
    7664-39-3
    Hydrogen fluoride (C,T)
    U135
    7783-06-4
    Hydrogen sulfide
    U135
    7783-06-4
    Hydrogen sulfide H
    2
    S
    U096
    80-15-9
    Hydroperoxide, 1-methyl-1-phenyl
    ethyl-
    (R)
    U116
    96-45-7
    2-Imidazolidinethione
    U137
    193-39-5
    Indeno [1,2,3-cd] pyrene
    U375
    55406-53-6
    3-Iodo-2-propynyl n-
    butylcarbamate
    U396
    14484-64-1
    Iron, tris(dimethyl carbamo dithioato -
    S,S')-
    U190
    85-44-9
    1,3-Isobenzofurandi
    one
    U140
    78-83-1
    Isobutyl alcohol (I,T)
    U141
    120-58-1
    Isosafrole
    U142
    143-50-0
    Kepone
    U143
    303-34-4
    Lasiocarpene
    U144
    301-04-2
    Lead acetate
    U146
    1335-32-6
    Lead, bis(acetato-O) tetrahydroxytri -
    U145
    7446-27-7
    Lead phosphate
    U146
    1335-32-6
    Lead subacetate
    U129
    58-89-9
    Lindane
    U163
    70-25-7
    MNNG
    U147
    108-31-6
    Maleic anhydride
    U148
    123-33-1
    Maleic hydrazide
    U149
    109-77-3
    Malononitrile
    U150
    148-82-3
    Melphalan
    U151
    7439-97-6
    Mercury
    U384
    137-42-8
    Metam Sodium
    U152
    126-98-7
    Methacrylonitrile (I,T)
    U092
    124-40-3
    Methan amine, N-methyl- (I)
    U029
    74-83-9
    Methane, bromo-
    U045
    74-87-3
    Methane, chloro- (I,T)
    U046
    107-30-2
    Methane, chloro methoxy -
    U068
    74-95-3
    Methane, dibromo-
    U080
    75-09-2
    Methane, dichloro -
    U075
    75-71-8
    Methane, dichloro difluoro -
    U138
    74-88-4
    Methane, iodo-
    U119
    62-50-0
    Methanesulfonic acid, ethyl ester
    U211
    56-23-5
    Methane, tetrachloro -
    U153
    74-93-1
    Methanethiol (I,T)
    U225
    75-25-2
    Methane, tribromo-
    U044
    67-66-3
    Methane, trichloro -
    U121
    75-69-4
    Methane, trichloro fluoro -
    U036
    57-74-9
    4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8-
    octachloro -2,3,3a,4,7,7a-hexa
    hydro-
    U154
    67-56-1
    Methanol (I)
    U155
    91-80-5
    Methapyrilene
    U142
    143-50-0
    1,3,4-Metheno-2H-cyclobuta
    [cd]pentalen-
    2-one, 1,1a,3,3a,4,5,5,5a,5b,6-
    decachloro octahydro-
    U247
    72-43-5
    Methoxychlor
    U154
    67-56-1
    Methyl alcohol (I)
    U029
    74-83-9
    Methyl bromide
    U186
    504-60-9
    1-Methyl butadiene (I)
    U045
    74-87-3
    Methyl chloride (I,T)
    U156
    79-22-1
    Methyl chloro carbonate (I,T)
    U226
    71-55-6
    Methyl chloro form
    U157
    56-49-5
    3-Methyl cholanthrene
    U158
    101-14-4
    4,4'-Methyl enebis(2-chloro aniline)
    U068
    74-95-3
    Methylene bromide
    U080
    75-09-2
    Methylene chloride
    84
    U159
    78-93-3
    Methyl ethyl ketone (MEK) (I,T)
    U160
    1338-23-4
    Methyl ethyl ketone peroxide (R,T)
    U138
    74-88-4
    Methyl iodide
    U161
    108-10-1
    Methyl isobutyl ketone (I)
    U162
    80-62-6
    Methyl methacrylate (I,T)
    U161
    108-10-1
    4-Methyl-2-pentanone (I)
    U164
    56-04-2
    Methyl thiouracil
    U010
    50-07-7
    Mitomycin C
    U365
    2212-67-1
    Molinate
    U059
    20830-81-3
    5,12-Naphthacenedi
    one, 8-acetyl-10-[(3-
    amino-2,3,6-tri deoxy)- alpha-L-lyxo-
    hexapyranosyl )oxyl]-7,8,9,10-tetra
    -
    hydro-6,8,11-tri hydroxy-1-methoxy
    -,
    (8S-cis)-
    U167
    134-32-7
    1-Naphthalen amine
    U168
    91-59-8
    2-Naphthalen amine
    U026
    494-03-1
    Naphthalene amine, N,N'- bis(2-chloro -
    ethyl)-
    U165
    91-20-3
    Naphthalene
    U047
    91-58-7
    Naphthalene, 2-chloro
    -
    U166
    130-15-4
    1,4-Naphthalenedi
    one
    U236
    72-57-1
    2,7-Naphthalenedi
    sulfonic acid, 3,3
    '-
    [(3,3'-di methyl-[1,1'-biphenyl]-4,4'-
    diyl)bis(azo)bis[5-amino-4-hydroxy]
    -,
    tetrasodium salt
    U279
    63-25-2
    1-Naphthalenol, methyl carbamate
    U166
    130-15-4
    1,4-Naphthoquinone
    U167
    134-32-7
    alpha- Naphthyl amine
    U168
    91-59-8
    beta-Naphthyl amine
    U217
    10102-45-1
    Nitric acid, thallium (1+) salt
    U169
    98-95-3
    Nitrobenzene (I,T)
    U170
    100-02-7
    p-Nitrophenol
    U171
    79-46-9
    2-Nitro propane (I,T)
    U172
    924-16-3
    N-Nitroso di-n-butyl amine
    U173
    1116-54-7
    N-Nitroso diethanol amine
    U174
    55-18-5
    N-Nitroso diethylamine
    U176
    759-73-9
    N-Nitroso-N-ethyl
    urea
    U177
    684-93-5
    N-Nitroso-N-methyl
    urea
    U178
    615-53-2
    N-Nitroso-N-methyl
    urethane
    U179
    100-75-4
    N-Nitroso piperidine
    U180
    930-55-2
    N-Nitroso pyrrolidine
    U181
    99-55-8
    5-Nitro-o-toluidine
    U193
    1120-71-4
    1,2-Oxathiolane, 2,2-di
    oxide
    U058
    50-18-0
    2H-1,3,2-Oxazaphosphorin-2-amine, N,N-
    bis(2-chloro ethyl) tetrahydro-, 2-oxide
    U115
    75-21-8
    Oxirane (I,T)
    U126
    765-34-4
    Oxiranecarboxyaldehyde
    U041
    106-89-8
    Oxirane, ( chloro methyl )-
    U182
    123-63-7
    Paraldehyde
    U391
    1114-71-2
    Pebulate
    U183
    608-93-5
    Pentachloro benzene
    U184
    76-01-7
    Pentachloro ethane
    U185
    82-68-8
    Pentachloro nitrobenzene (PCNB)
    See F027
    87-86-5
    Pentachloro phenol
    U161
    108-10-1
    Pentanol, 4-methyl-
    U186
    504-60-9
    1,3-Penta diene (I)
    U187
    62-44-2
    Phenacetin
    U188
    108-95-2
    Phenol
    U048
    95-57-8
    Phenol, 2-chloro -
    U039
    59-50-7
    Phenol, 4-chloro -3-methyl-
    U081
    120-83-2
    Phenol, 2,4-di chloro -
    85
    U082
    87-65-0
    Phenol, 2,6-di chloro -
    U089
    56-53-1
    Phenol, 4,4'-(1,2-di
    ethyl-1,2-ethenedi
    -
    yl)bis-, (E)-
    U101
    105-67-9
    Phenol, 2,4-di methyl-
    U052
    1319-77-3
    Phenol, methyl-
    U132
    70-30-4
    Phenol, 2,2'-methyl
    enebis[3,4,6-tri -
    chloro -
    U411
    114-26-1
    Phenol, 2-(1-methyl
    ethoxy) -, methyl -
    carbamate
    U170
    100-02-7
    Phenol, 4-nitro-
    See F027
    87-86-5
    Phenol, pentachloro -
    See F027
    58-90-2
    Phenol, 2,3,4,6-tetra
    chloro -
    See F027
    95-95-4
    Phenol, 2,4,5-tri
    chloro -
    See F027
    88-06-2
    Phenol, 2,4,6-tri
    chloro -
    U150
    148-82-3
    L-Phenyl alanine , 4-[bis(2-chloro ethyl) -
    amino]-
    U145
    7446-27-7
    Phosphoric acid, lead (2+) salt (2:3)
    U087
    3288-58-2
    Phosphorodi thioic acid, O,O-di ethyl S-
    methyl ester
    U189
    1314-80-3
    Phosphorus sulfide (R)
    U190
    85-44-9
    Phthalic anhydride
    U191
    109-06-8
    2-Picoline
    U179
    100-75-4
    Piperidine, 1-nitroso-
    U400
    120-54-7
    Piperidine, 1,1'-(
    tetrathiodicarbono -
    thioyl)- bis-
    U383
    128-03-0
    Potassium dimethyl dithio carbamate
    U378
    51026-28-9
    Potassium n-hydroxy methyl-n-methyl di-
    thiocarbamate
    U377
    137-41-7
    Potassium n- methyl dithio carbamate
    U192
    23950-58-5
    Pronamide
    U194
    107-10-8
    1-Propan amine (I,T)
    U111
    621-64-7
    1-Propan amine, N-nitroso-N-propyl-
    U110
    142-84-7
    1-Propan amine, N- propyl- (I)
    U066
    96-12-8
    Propane, 1,2-di bromo-3-chloro -
    U083
    78-87-5
    Propane, 1,2-di chloro -
    U149
    109-77-3
    Propanedi nitrile
    U171
    79-46-9
    Propane, 2-nitro- (I,T)
    U027
    108-60-1
    Propane, 2,2'-oxy
    bis[2-chloro -
    See F027
    93-72-1
    Propanoic acid, 2-(2,4,5-tri
    chloro -
    phenoxy)-
    U193
    1120-71-4
    1,3-Propane sultone
    U235
    126-72-7
    1-Propanol, 2,3-di
    bromo-, phosphate
    (3:1)
    U140
    78-83-1
    1-Propanol, 2-methyl- (I,T)
    U002
    67-64-1
    2-Propanone (I)
    U007
    79-06-1
    2-Propenamide
    U084
    542-75-6
    1-Propene, 1,3-di
    chloro -
    U243
    1888-71-7
    1-Propene, 1,1,2,3,3,3-hexa
    chloro -
    U009
    107-13-1
    2-Propenenitrile
    U152
    126-98-7
    2-Propenenitrile, 2-methyl- (I,T)
    U008
    79-10-7
    2-Propenoic acid (I)
    U113
    140-88-5
    2-Propenoic acid, ethyl ester (I)
    U118
    97-63-2
    2-Propenoic acid, 2-methyl
    -, ethyl
    ester
    U162
    80-62-6
    2-Propenoic acid, 2-methyl
    -, methyl
    ester (I,T)
    U373
    122-42-9
    Propham
    U411
    114-26-1
    Propoxur
    See F027
    93-72-1
    Propionic acid, 2-(2,4,5-tri
    chloro -
    phenoxy)-
    U194
    107-10-8
    n-Propyl amine (I,T)
    86
    U083
    78-87-5
    Propylene di chloride
    U387
    52888-80-9
    Prosulfocarb
    U148
    123-33-1
    3,6-Pyridazinedi one, 1,2-di hydro-
    U196
    110-86-1
    Pyridine
    U191
    109-06-8
    Pyridine, 2-methyl-
    U237
    66-75-1
    2,4-(1H,3H)- Pyrimidinedi one, 5-[bis(2-
    chloro ethyl) amino]-
    U164
    58-04-2
    4(1H)- Pyrimidinone, 2,3-di
    hydro-6-
    methyl-2-thioxo-
    U180
    930-55-2
    Pyrrolidine, 1-nitroso-
    U200
    50-55-5
    Reserpine
    U201
    108-46-3
    Resorcinol
    U202
    P 81-07-2
    Saccharin and salts
    U203
    94-59-7
    Safrole
    U204
    7783-00-8
    Selenious acid
    U204
    7783-00-8
    Selenium di oxide
    U205
    7488-56-4
    Selenium sulfide
    U205
    7488-56-4
    Selenium sulfide SeS
    2
    (R,T)
    U376
    144-34-3
    Selenium, tetrakis (dimethyl dithio -
    carbamate)
    U015
    115-02-6
    L-Serine, diazoacetate (ester)
    See F027
    93-72-1
    Silvex (2,4,5-TP)
    U379
    136-30-1
    Sodium dibutyl dithio carbamate
    U381
    148-18-5
    Sodium diethyl dithio carbamate
    U382
    128-04-1
    Sodium dimethyl dithio carbamate
    U206
    18883-66-4
    Streptozotocin
    U277
    95-06-7
    Sulfallate
    U103
    77-78-1
    Sulfuric acid, dimethyl ester
    U189
    1314-80-3
    Sulfur phosphide (R)
    See F027
    93-76-5
    2,4,5-T
    U402
    1634-02-2
    Tetrabutylthiuram disulfide
    U207
    95-94-3
    1,2,4,5-Tetra chloro benzene
    U208
    630-20-6
    1,1,1,2-Tetra chloro ethane
    U209
    79-34-5
    1,1,2,2-Tetra chloro ethane
    U210
    127-18-4
    Tetrachloro ethylene
    See F027
    58-90-2
    2,3,4,6-Tetra chloro phenol
    U213
    109-99-9
    Tetrahydrofuran (I)
    U401
    97-74-5
    Tetramethyl thiuram monosulfide
    U366
    533-74-4
    2H-1,3,5-Thia diazine- 2-thione, tetra
    -
    hydro-3,5-di methyl-
    U214
    563-68-8
    Thallium (I) acetate
    U215
    6533-73-9
    Thallium (I) carbonate
    U216
    7791-12-0
    Thallium (I) chloride
    U216
    7791-12-0
    Thallium chloride
    TlCl
    U217
    10102-45-1
    Thallium (I) nitrate
    U218
    62-55-5
    Thioacetamide
    U410
    59669-26-0
    Thiodicarb
    U153
    74-93-1
    Thiomethanol (I,T)
    U402
    1634-02-2
    Thioperoxy dicarbonic diamide, tetra-
    butyl
    U403
    97-77-8
    Thioperoxy dicarbonic diamide, tetra -
    ethyl
    U244
    137-26-8
    Thioperoxydi carbonic diamide
    [(H
    2
    N)C(S)]
    2
    S
    2
    , tetramethyl -
    U409
    23564-05-8
    Thiophanate -methyl
    U219
    62-56-6
    Thiourea
    U244
    137-26-8
    Thiram
    U220
    108-88-3
    Toluene
    U221
    25376-45-8
    Toluenedi amine
    U223
    26471-62-5
    Toluene di isocyanate (R,T)
    U328
    95-53-4
    o-Toluidine
    87
    U353
    106-49-0
    p-Toluidine
    U222
    636-21-5
    o-Toluidine hydrochloride
    U389
    2303-17-5
    Triallate
    U011
    61-82-5
    1H-1,2,4-Tri azol-3-amine
    U227
    79-00-5
    1,1,2-Tri chloro ethane
    U228
    79-01-6
    Trichloro ethylene
    U121
    75-69-4
    Trichloro monofluoromethane
    See F027
    95-95-4
    2,4,5-Tri chloro phenol
    See F027
    88-06-2
    2,4,6-Tri chlorophenol
    U404
    121-44-8
    Triethyl amine
    U234
    99-35-4
    1,3,5-Tri nitrobenzene (R,T)
    U182
    123-63-7
    1,3,5-Tri oxane, 2,4,6-tri methyl-
    U235
    126-72-7
    Tris(2,3-di bromopropyl) phosphate
    U236
    72-57-1
    Trypan blue
    U237
    66-75-1
    Uracil mustard
    U176
    759-73-9
    Urea, N-ethyl-N- nitroso-
    U177
    684-93-5
    Urea, N-methyl-N-
    nitroso-
    U385
    1929-77-7
    Vernolate
    U043
    75-01-4
    Vinyl chloride
    U248
    P 81-81-2
    Warfarin, and salts, when present at
    concentrations of 0.3% or less
    U239
    1330-20-7
    Xylene (I)
    U200
    50-55-5
    Yohimban-16-carboxylic acid, 11,17-di
    -
    methoxy-18-[(3,4,5-tri
    methoxybenzoyl)-
    oxy]-, methyl ester,
    (3beta,16beta,17alpha,18beta,20alpha)-
    U407
    14324-55-1
    Zinc, bis(diethyl carbamo dithioato -
    S,S')-
    U249
    1314-84-7
    Zinc phosphide Zn
    3
    P
    2
    , when present at
    concentrations of 10% or less
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 721.Appendix G
    Basis for Listing Hazardous Wastes
    EPA
    hazardous
    waste No.
    Hazardous constituents for which listed
    F001
    Tetrachloroethylene,
    methylene chloride,
    trichloroethylene, 1,1,1-
    trichloroethane, carbon tetrachloride, chlorinated fluorocarbons.
    F002
    Tetrachloroethylene,
    methylene chloride,
    trichloroethylene, 1,1,1-
    trichloroethane, 1,1,2-trichlorethane,
    chlorobenzene, 1,1,2-trichloro-
    1,2,2-trifluoroethane,
    ortho-dichlorobenzene,
    trichlorofluoromethane.
    F003
    N.A.
    F004
    Cresols and cresylic acid, nitrobenzene.
    F005
    Toluene, methyl ethyl
    ketone, carbon disulfide,
    isobutanol, pyridine, 2-
    ethoxyethanol, benzene, 2-nitropropane.
    F006
    Cadmium, hexavalen
    t chromium, nickel, cyanide (
    complexed).
    F007
    Cyanide (salts).
    F008
    Cyanide (salts).
    F009
    Cyanide (salts).
    F010
    Cyanide (salts).
    F011
    Cyanide (salts).
    F012
    Cyanide ( complexed).
    F019
    Hexavalent chromium, cyanide (
    complexed).
    F020
    Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
    pentachlorodibenzofurans;
    tri- and tetrachlorophenols and their
    clorophenoxy derivative acids, esters, ethers, amines and other salts.
    F021
    Penta- and hexachlorodibenzo-p-dioxins;
    penta- and
    88
    hexachlorodibenzofurans; pentachlorophenol and its derivatives.
    F022
    Tetra-, penta- and hexachlorodibenzo-p-dioxins; tetra
    -, penta- and
    hexachlorodibenzofurans.
    F023
    Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
    pentachlorodibenzofurans;
    tri- and tetra- chlorophenols and their
    chlorophenoxy derivative acids, esters, ethers, amines and other salts.
    F024
    Chloromethane, dichloromethane,
    trichloromethane, carbon tetrachloride,
    chloroethylene, 1,1-dichloroethane, 1,2-dichloroethane, trans-1,2-
    dichloroethylene, 1,1-dichloroethylene, 1,1,1-trichloroethane, 1,1,2-
    trichloroethane,
    trichloroethylene, 1,1,1,2-tetrachloroethane, 1,1,2,2-
    tetrachloroethane,
    tetrachloroethylene,
    pentachloroethane,
    hexachloroethane,
    allyl chloride (3-chloropropene),
    dichloropropane,
    dichloropropene, 2-chloro-1,3-butadiene, hexachloro-1,3-butadiene,
    hexachlorochylopentadiene,
    hexachlorocylohexane, benzene,
    chlorobenzene,
    dichlorobenzenes, 1,2,4-trichlorobenzene,
    tetrachlorobenzenes,
    pentachlorobenzene,
    hexachlorobenzene, toluene, naphthalene.
    F025
    Chloromethane, dicloromethane, trichloromethane; carbon tetrachloride;
    chloroethylene; 1,1-dichloroethane; 1,2-dichloroethane; trans-1,2-
    dichloroethylene; 1,1-dichloroethylene; 1,1,1-trichloroethane; 1,1,2-
    trichloroethane;
    trichloroethylene; 1,1,1,2-tetrachloroethane; 1,1,2,2-
    tetrachloroethane;
    tetrachloroethylene;
    pentachloroethane;
    hexachloroethane;
    allyl chloride (3-chloropropene);
    dichloropropane;
    dichloropropene; 2-chloro-1,3-butadiene; hexachloro-1,3-butadiene;
    hexachlorocyclopentadiene; benzene;
    chlorobenzene; dichlorobenzene;
    1,2,4-trichlorobenzene;
    tetrachlorobenzene;
    pentachlorobenzene;
    hexachlorobenzene; toluene; naphthalene.
    F026
    Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra
    -, penta-, and
    hexachlorodibenzofurans.
    F027
    Tetra-, penta, and hexachlorodibenzo-p-dioxins; tetra
    -, penta-, and
    hexachlorodibenzofurans;
    tri-, tetra -, and pentachlorophenols and their
    chlorophenoxy derivative acids, esters, ethers, amine and other salts.
    F028
    Tetra-, penta-, and hexachlorodibenzo-p-dixons;tetra
    -, penta-, and
    hexachlorodibenzofurans;
    tri-, tetra -, and pentachlorophenols and their
    chlorophenoxy derivative acids, esters, ethers, amine and other salts.
    F032
    Benz(a) anthracene, benzo(a) pyrene, dibenz( a,h)anthracene, indeno(1,2,3-
    cd)pyrene, pentachlorophenol, arsenic, chromium, tetra
    -, penta-, hexa-,
    heptachlorordibenzo-p-dioxins, tetra
    -, penta-, hexa-,
    heptachlorodibenzofurans.
    F034
    Benz(a) anthracene, benzo(k) fluoranthene, benzo(a) pyrene,
    dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene, naphthalene, arsenic
    chromium.
    F035
    Arsenic, chromiu m and lead.
    F037
    Benzene, benzo(a) pyrene, chrysene, lead, chromium.
    F038
    Benzene, benzo(a) pyrene, chrysene, lead, chromium.
    F039
    All constituents for which treatment standards are specified for
    multi-
    source leachate (wastewaters and non-wastewaters) under 35 Ill. Adm.
    Code 728.Table B (Constituent Concentrations in Waste).
    K001
    Pentachlorophenol, phenol, 2-chlorophenol, p-chloro-m-cresol, 2,4-
    dimethylphenol, 2,4-
    dinitrophenol, trichlorophenols,
    tetrachlorophenols, 2,4-
    dinitrophenol, cresosote, chrysene,
    naphthalene, fluoranthene, benzo(b) fluoranthene, benzo(a) pyrene,
    indeno(1,2,3-cd) pyrene, benz(a) anthracene, dibenz(a) anthracene,
    acenaphthalene.
    K002
    Hexavalent chromium, lead.
    K003
    Hexavalent chromium, lead.
    K004
    Hexavalent chromium.
    K005
    Hexavalent chromium, lead.
    K006
    Hexavalent chromium.
    K007
    Cyanide ( complexed), hexavalent chromium.
    K008
    Hexavalent chromium.
    K009
    Chloroform, formaldehyde,
    methylene chloride, methyl chloride,
    89
    paraldehyde, formic acid.
    K010
    Chloroform, formaldehyde,
    methylene chloride, methyl chloride,
    paraldehyde, formic acid,
    chloroacetaldehyde.
    K011
    Acrylonitrile, acetonitrile,
    hydrocyanic acid.
    K013
    Hydrocyanic acid, acrylonitrile, acetonitrile.
    K014
    Acetonitrile, acrylamide.
    K015
    Benzyl chloride,
    chlorobenzene, toluene,
    benzotrichloride.
    K016
    Hexachlorobenzene,
    hexachlorobutadiene, carbon tetrachloride,
    hexachloroethane,
    perchloroethylene.
    K017
    Epichlorohydrin,
    chloroethers [ bis(chloromethyl) ether and
    bis- (2-
    chloroethyl) ethers],
    trichloropropane,
    dichloropropanols.
    K018
    1,2-dichlor oethane, trichloroethylene,
    hexachlorobutadiene,
    hexachlorobenzene.
    K019
    Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
    tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
    tetrachloroethane),
    trichloroethylene,
    tetrachloroethylene, carbon
    tetrachloride, chloroform, vinyl chloride,
    vinylidene chloride.
    K020
    Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
    tetrachloro-ethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
    tetrachloroethane),
    trichloroethylene,
    tetrachloroethylene, carbon
    tetrachloride, chloroform, vinyl chloride,
    vinylidene chloride.
    K021
    Antimony, carbon tetrachloride, chloroform.
    K022
    Phenol, tars ( polycyclic aromatic hydrocarbons).
    K023
    Phthalic anhydride,
    maleic anhydride.
    K024
    Phthalic anhydride, 1,4-naphthoguinone.
    K025
    Meta-dinitrobenzene, 2,4-dinitrotoluene.
    K026
    Paraldehyde, pyridines, 2-picoline.
    K027
    Toluene diisocyanate, toluene-2,4-diamine.
    K028
    1,1,1-trichloroethane, vinyl chloride.
    K029
    1,2-dichloroethane, 1,1,1-trichloroethane, vinyl chloride,
    vinylidene
    chloride, chloroform.
    K030
    Hexachlorobenzene,
    hexachlorobutadiene,
    hexachloroethane, 1,1,1,2-
    tetrachloroethane, 1,1,2,2-tetrachloroethane, ethylene dichloride.
    K031
    Arsenic.
    K032
    Hexachlorocyclopentadiene.
    K033
    Hexachlorocyclopentadiene.
    K034
    Hexachlorocyclopentadiene.
    K035
    Creosote, chrysene, naphthalene,
    fluoranthene, benzo(b) fluoranthene,
    benzo(a)- pyrene, indeno(1,2,3-cd)
    pyrene, benzo(a) anthracene,
    dibenzo(a) anthracene, acenaphthalene.
    K036
    Toluene, phosphorodithioic and
    phosphorothioic acid esters.
    K037
    Toluene, phosphorodithioic and
    phosphorothioic acid esters.
    K038
    Phorate, formaldehyde,
    phosphorodithioic and
    phosphorothioic acid
    esters.
    K039
    Phosphorodithioic and
    phosphorothioic acid esters.
    K040
    Phorate, formaldehyde,
    phosphorodithioic and
    phosphorothioic acid
    esters.
    K041
    Toxaphene.
    K042
    Hexachlorobenzene,
    ortho-dichlorobenzene.
    K043
    2,4-dichlorophenol, 2,6-dichlorophenol, 2,4,6-trichlorophenol.
    K044
    N.A.
    K045
    N.A.
    K046
    Lead.
    K047
    N.A.
    K048
    Hexavalent chromium, lead.
    K049
    Hexavalent chr omium, lead.
    K050
    Hexavalent chromium.
    K051
    Hexavalent chromium, lead.
    K052
    Lead.
    K060
    Cyanide, naphthalene,
    phenolic compounds, arsenic.
    K061
    Hexavalent chromium, lead, cadmium.
    90
    K062
    Hexavalent chromium, lead.
    K064
    Lead, cadmium.
    K065
    Lead, cadmium.
    K066
    Lead, cadmium.
    K069
    Hexavalent chromium, lead, cadmium.
    K071
    Mercury.
    K073
    Chloroform, carbon tetrachloride,
    hexachloroethane,
    trichloroethane,
    tetrachloroethylene,
    dichloroethylene, 1,1,2,2-tetrachloroethane.
    K083
    Aniline, diphenylamine, nitrobenzene,
    phenylenediamine.
    K084
    Arsenic.
    K085
    Benzene, dichlorobenzenes,
    trichlorobenzenes,
    tetrachlorobenzenes,
    pentachlorobenzene,
    hexachlorobenzene, benzyl chloride.
    K086
    Lead, hexavalent chromium.
    K087
    Phenol, naphthalene.
    K088
    Cyanide (complexes).
    K090
    Chromium.
    K091
    Chromium.
    K093
    Phthalic anhydride,
    maleic anhydride.
    K094
    Phthalic anhydride.
    K095
    1,1,2-trichloroethane, 1,1,1,2-tetrachloroethane, 1,1,2,2-
    tetrachloroethane.
    K096
    1,2-dichloroethane, 1,1,1-trichloroethane, 1,1,2-trichloroethane.
    K097
    Chlordane, hept achlor.
    K098
    Toxaphene.
    K099
    2,4-dichlorophenol, 2,4,6-trichlorophenol.
    K100
    Hexavalent chromium, lead, cadmium.
    K101
    Arsenic.
    K102
    Arsenic.
    K103
    Aniline, nitrobenzene,
    phenylenediamine.
    K104
    Aniline, benzene,
    diphenylamine, nitrobenzene,
    phynylenediamine.
    K105
    Benzene, monochlorobenzene,
    dichlorobenzenes, 2,4,6-trichlorophenol.
    K106
    Mercury.
    K111
    2,4-Dinitrotoluene.
    K112
    2,4-Toluenediamine, o-
    toluidine, p- toluidine, aniline.
    K113
    2,4-Toluenediamine, o-
    toluidine, p- toluidine, aniline.
    K114
    2,4-Toluenediamin
    e, o-toluidine, p- toluidine.
    K115
    2,4-Toluenediamine.
    K116
    Carbon tetrachloride,
    tetrachloroethylene, chloroform, phosgene.
    K117
    Ethylene dibromide.
    K118
    Ethylene dibromide.
    K123
    Ethylene thiourea.
    K124
    Ethylene thiourea.
    K125
    Ethylene thiourea.
    K126
    Ethylene thiourea.
    K131
    Dimethyl sulfate, methyl bromide.
    K132
    Methyl bromide.
    K136
    Ethylene dibromide.
    K141
    Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
    benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
    K142
    Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
    benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
    K143
    Benzene, benz(a) anthracene, benzo(b) fluoranthene, benzo(k) fluoranthene.
    K144
    Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
    benzo(k) fluoranthene, dibenz( a,h)anthracene.
    K145
    Benzene, benz(a) anthracene, benzo(a) pyrene, dibenz( a,h)anthracene,
    naphthalene.
    K147
    Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
    benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
    K148
    Benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
    benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
    K149
    Benzotrichloride, benzyl chloride, chloroform,
    chloromethane,
    91
    chlorobenzene, 1,4-dichlorobenzene,
    hexachlorobenzene,
    pentachlorobenzene, 1,2,4,5-tetrachlorobenzene, toluene.
    K150
    Carbon tetrachloride, chloroform,
    chloromethane, 1,4-dichlorobenzene,
    hexachlorobenzene,
    pentachlorobenzene, 1,2,4,5-tetrachlorobenzene,
    1,1,2,2-tetrachloroethane,
    tetrachloroethylene, 1,2,4-trichlorobenzene.
    K151
    Benzene, carbon tetrachloride, chloroform,
    hexachlorobenzene,
    pentachlorobenzene, toluene, 1,2,4,5-tetrachlorobenzene,
    tetrachloroethylene.
    K156
    Benomyl, carbaryl, carbendazim, carbofuran, carbosulfan, formaldehyde,
    methylene chloride,
    triethylamine.
    K157
    Carbon tetrachloride, formaldehyde, methyl chloride,
    methylene chloride,
    pyridine, triethylamine.
    K158
    Benomyl, carbendazim, carbofuran, carbosulfan, chloroform,
    methylene
    chloride.
    K159
    Benzene, butylate, EPTC, molinate, pebulate, vernolate.
    K160 Benzene, butylate, EPTC, molinate, pebulate, vernolate.
    K161
    Antimony, arsenic,
    metam-sodium, ziram.
    N.A.--Waste is hazardous because it fails the test for the
    characteristic of
    ignitability, corrosivity or reactivity.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 721.Appendix H Hazardous Constituents
    Common Name
    Chemical Abstracts Name
    Chemical
    Abstracts
    Number
    Hazard
    ous
    Waste
    Number
    A2213
    Ethanimidothioic acid, 2 -
    (dimethyl amino)-N-hydroxy-
    2-oxo-, methyl ester
    30558-43-
    1
    U394
    Acetonitrile
    Same
    75-05-8
    U003
    Acetophenone
    Ethanone, 1-phenyl-
    98-86-2
    U004
    2-Acetylamino fluorene
    Acetamide, N-9H-fluoren-2-
    yl-
    53-96-3
    UOO5
    Acetyl chloride
    Same
    75-36-5
    U006
    1-Acetyl-2-thio urea
    Acetamide, N-
    (aminothioxomethyl)-
    591-08-2
    P002
    Acrolein
    2-Propenal
    107-02-8
    P003
    Acrylamide
    2-Propenamide
    79-06-1
    U007
    Acrylonitrile
    2-Propenenitrile
    107-13-1
    U009
    Aflatoxins
    Same
    1402-68-2
    Aldicarb
    Propanal, 2-methyl-2-
    (methylthio)-, O-
    [(methylamino)carbonyl]
    -
    oxime
    116-06-3
    P070
    Aldicarb sulfone
    Propanal, 2 -methyl-2-
    (methyl sulfonyl )-,
    O-[(methylamino) carbonyl] -
    oxime
    1646-88-4
    P203
    Aldrin
    1,4,5,8-Dimethano
    naph-
    thalene, 1,2,3,4,10,10-
    hexachloro-1,4,4a,5,8,8a-
    hexahydro-, (1-alpha,4-
    alpha,4a-beta,5-alpha,8-
    alpha,8a-beta)-
    309-00-2
    P004
    Allyl alcohol
    2-Propen-1-ol
    107-18-6
    P005
    Allyl chloride
    1-Propene, 3-chloro-
    107-18-6
    92
    Aluminum phosphide
    Same
    20859-73-
    8
    P006
    4-Aminobiphenyl
    [1,1'-Biphenyl]-4-amine
    92-67-1
    5-(Aminomethyl)-3-isoxazolol
    3(2H)- Isoxazolone, 5-
    (aminomethyl )-
    2763-96-4
    P007
    4-Aminopyridine
    4-Pyridinamine
    504-24-5
    P008
    Amitrole
    1H-1,2,4-Triazol-3-amine
    61-82-5
    U011
    Ammonium vanadate
    Vanadic acid, ammonium
    salt
    7803-55-6
    U119
    Aniline
    Benzenamine
    62-53-3
    U012
    Antimony
    Same
    7440-36-0
    Antimony compounds, N.O.S.
    (not otherwise specified)
    Aramite
    Sulfurous acid, 2-
    chloroethyl-, 2-[4-(1,1-
    dimethyl ethyl) phenoxy]-1-
    methylethyl ester
    140-57-8
    Arsenic
    Arsenic
    7440-38-2
    Arsenic compounds, N.O.S.
    Arsenic acid
    Arsenic acid H
    3
    AsO
    4
    7778-39-4
    P010
    Arsenic pentoxide
    Arsenic oxide As
    2
    O
    5
    1303-28-2
    PO11
    Arsenic trioxide
    Arsenic oxide As
    2
    O
    3
    1327-53-3
    P012
    Auramine
    Benzenamine, 4,4'-carbon
    -
    imidoyl bis[N, N- dimethyl-
    492-80-8
    U014
    Azaserine
    L-Serine, diazoacetate
    (ester)
    115-02-6
    U015
    Barban
    Carbamic acid, (3
    -chloro -
    phenyl) -, 4-chloro-2-
    butynyl ester
    101-27-9
    U280
    Barium
    Same
    7440-39-3
    Barium compounds, N.O.S.
    Barium cyanide
    Same
    542-62-1
    P013
    Bendiocarb
    1,3-Benzo dioxol-4-ol-
    2,2-dimethyl -, methyl
    carbamate
    22781-23-
    3
    U278
    Bendiocarb phenol
    1,3-Benzo dioxol-4-ol-2,2-
    dimethyl -,
    22961-82-
    6
    U364
    Benomyl
    Carbamic acid, [1
    -
    [(butylamino)carbonyl]-1H-
    benzimidazol-2-yl] -,
    methyl ester
    17804-35-
    2
    U271
    Benz[c] acridine
    Same
    225-51-4
    U016
    Benz[a] anthra cene
    Same
    56-55-3
    U018
    Benzal chloride
    Benzene, ( dichloromethyl)-
    98-87-3
    U017
    Benzene
    Same
    71-43-2
    U018
    Benzenearsonic acid
    Arsonic acid, phenyl-
    98-05-5
    Benzidine
    [1,1'-Biphenyl]-4,4'-
    diamine
    92-87-5
    U021
    Benzo[b] fluoranthene
    Benz[e] acephenanthrylene
    205-99-2
    Benzo[j] fluoranthene
    Same
    205-82-3
    Benzo(k) fluoranthene
    Same
    207-08-9
    Benzo[a] pyrene
    Same
    50-32-8
    U022
    p-Benzoquinone
    2,5-Cyclohexadiene-1,4-
    dione
    106-51-4
    U197
    Benzotrichloride
    Benzene,
    (trichloromethyl)-
    98-07-7
    U023
    Benzyl chloride
    Benzene, ( chloromethyl)-
    100-44-7
    P028
    Beryllium powder
    Same
    7440-41-7
    P015
    Beryllium compounds, N.O.S.
    Bis(pentamethylene )thiuram
    tetrasulfide
    Piperidine, 1,1' -(tetra-
    thiodicarbono thioyl )-bis-
    120-54-7
    U400
    93
    Bromoacetone
    2-Propanone, 1-bromo-
    598-31-2
    P017
    Bromoform
    Methane, tribromo-
    75-25-2
    U225
    4-Bromophenyl phenyl ether
    Benzene, 1-bromo-4-
    phenoxy-
    101-55-3
    U030
    Brucine
    Strychnidin-10-one, 2,3-
    dimethoxy-
    357-57-3
    P018
    Butylate
    Carbamo thioic acid, bis-
    (2-methyl propyl) -, S-ethyl
    ester
    2008-41-5
    U392
    Butyl benzyl phthalate
    1,2-Benzenedicarboxylic
    acid, butyl phenylmethyl
    ester
    85-68-7
    Cacodylic acid
    Arsenic acid, dimethyl-
    75-60-5
    U136
    Cadmium
    Same
    7440-43-9
    Cadmium compounds, N.O.S.
    Calcium chromate
    Chromic acid H
    2
    CrO
    4
    ,
    calcium salt
    13765-19-
    0
    U032
    Calcium cyanide
    Calcium cyanide Ca(CN)
    2
    592-01-8
    P021
    Carbaryl
    1-Naphthalenol, methyl -
    carbamate
    63-25-2
    U279
    Carbendazim
    Carbamic acid, 1H
    -benz-
    imidazol-2-yl, methyl
    ester
    10605-21-
    7
    U372
    Carbofuran
    7-Benzofuranol, 2,3
    -di-
    hydro-2,2-dimethyl
    -,
    methyl carbamate
    1563-66-2
    P127
    Carbofuran phenol
    7-Benzo furanol, 2,3-
    dihydro-2,2-dimethyl
    -
    1563-38-8
    U367
    Carbosulfan
    Carbamic acid, [(
    dibutyl -
    amino) thio] methyl -,
    2,3-dihydro-2,2-dimethyl-
    7-benzo furanyl ester
    55285-14-
    8
    P189
    Carbon disulfide
    Same
    75-15-0
    P022
    Carbon oxyfluoride
    Carbonic difuoride
    353-50-4
    U033
    Carbon tetra chloride
    Methane, tetrachloro-
    56-23-5
    U211
    Chloral
    Acetaldehyde, trichloro-
    75-87-6
    U034
    Chlorambucil
    Benzenebutanoic acid,
    4[bis-(2-chloroethyl)
    -
    amino]-
    305-03-3
    U035
    Chlordane
    4,7-Methano-1H-indene,
    1,2,4,5,6,7,8,8-octa
    -
    chloro-2,3,3a,4,7,7a-hexa
    -
    hydro-
    57-74-9
    U036
    Chlordane, alpha and gamma
    isomers
    U036
    Chlorinated benzenes, N.O.S.
    Chlorinated ethane, N.O.S.
    Chlorinated fluorocarbons,
    N.O.S.
    Chlorinated naphthalene,
    N.O.S.
    Chlorinated phenol, N.O.S.
    Chlornaphazine
    Naphthalenamine, N,N'-
    bis(2-chloro ethyl)-
    494-03-1
    U026
    Chloroacet aldehyde
    Acetaldehyde, chloro-
    107-20-0
    P023
    Chloroalkyl ethers, N.O.S.
    p-Chloroaniline
    Benzenamine, 4-chloro-
    106-47-8
    P024
    Chlorobenzene
    Benzene, chloro-
    108-90-7
    U037
    Chlorobenzilate
    Benzeneacetic acid, 4-
    chloro-alpha-(4-
    chlorophenyl)-alpha-
    510-15-6
    U038
    94
    hydroxy-, ethyl ester
    p-Chloro-m-cresol
    Phenol, 4-chloro-3-methyl-
    59-50-7
    U039
    2-Chloroethyl vinyl ether
    Ethene, (2-chloroethoxy)-
    110-75-8
    U042
    Chloroform
    Methane, trichloro-
    67-66-3
    U044
    Chloromethyl methyl ether
    Methane, chloromethoxy-
    107-30-2
    U046
    beta-Chloro naphthalene
    Naphthalene, 2-chloro-
    91-58-7
    U047
    o-Chlorophenol
    Phenol, 2-chloro-
    95-57-8
    U048
    1-(o-Chloro phenyl )thiourea
    Thiourea, (2-chloro
    -
    phenyl)-
    5344-82-1
    P026
    Chloroprene
    1,3-Butadiene, 2-chloro-
    126-99-8
    3-Chloropropio nitrile
    Propanenitrile, 3-chloro-
    542-76-7
    P027
    Chromium
    Same
    7440-47-3
    Chromium compounds, N.O.S.
    Chrysene
    Same
    218-01-9
    U050
    Citrus red No. 2
    2-Naphthalenol, 1-[(2,5-
    dimethoxy phenyl) azo]-
    6358-53-8
    Coal tar creosote
    Same
    8007-45-2
    Copper cyanide
    Copper cyanide CuCN
    544-92-3
    P029
    Copper dimethyl dithio carbamate
    Copper, bis(dimethyl -
    carbamo dithioato -S,S') -,
    137-29-1
    U393
    Creosote
    Same
    U051
    Cresols ( Cresylic acid)
    Phenol, methyl-
    1319-77-3
    U052
    Crotonaldehyde
    2-Butenal
    4170-30-3
    U053
    m-Cumenyl methyl carbamate
    Phenol, 3 -(methyl ethyl)-,
    methyl carbamate
    64-00-6
    P202
    Cyanides (soluble salts and
    complexes), N.O.S.
    P030
    Cyanogen
    Ethanedinitrile
    460-19-5
    P031
    Cyanogen bromide
    Cyanogen bromide (CN)Br
    506-68-3
    U246
    Cyanogen chloride
    Cyanogen chloride (CN)
    Cl
    506-77-4
    P033
    Cycasin
    Beta-D- glucopyranoside,
    (methyl-ONN- azoxy)methyl-
    14901-08-
    7
    Cycloate
    Carbamo thioic acid, cyclo-
    hexylethyl-, S-ethyl ester
    1134-23-2
    U386
    2-Cyclohexyl-4,6-dinitro
    phenol
    Phenol, 2-cyclohexyl-4,6-
    dinitro-
    131-89-5
    P034
    Cyclophosphamide
    2H-1,3,2-Oxazaphosphorin-
    2-amine, N,N- bis(2-chloro -
    ethyl) tetrahydro-, 2-oxide
    50-18-0
    U058
    2,4-D
    Acetic acid, (2,4-
    dichloro phenoxy)-
    94-75-7
    U240
    2,4-D, salts and esters
    Acetic acid, (2,4-
    dichlorophenoxy)-, salts
    and esters
    U240
    Daunomycin
    5, 12-Naphthacenedione, 8-
    acetyl-10-[(3-amino-2,3,6-
    trideoxy-alpha-L-lyxo-
    hexopyranosyl) oxy]-
    7,8,9,10-tetrahydro-
    6,8,11-tri hydroxy-l-meth -
    oxy-, 8S-cis)-
    20830-81-
    3
    U059
    Dazomet
    2H-1,3,5-thia diazine-2-
    thione, tetra hydro-3,5-
    dimethyl
    533-74-4
    U366
    DDD
    Benzene, 1,1'-(2,2-
    dichloro ethylidene) bis[4-
    chloro-
    72-54-8
    U060
    DDE
    Benzene, 1,1'-( dichloro -
    ethenyl idene)bis[4-chloro-
    72-55-9
    DDT
    Benzene, 1,1'-(2,2,2-tri
    -
    chloro ethylidene) bis[4-
    50-29-3
    U061
    95
    chloro-
    Diallate
    Carbamothioic acid, bis(1-
    methyl ethyl)-, S-(2,3-
    dichloro-2-pro penyl) ester
    2303-16-4
    U062
    Dibenz[ a,h]acridine
    Same
    226-36-8
    Dibenz[ a,j]acridine
    Same
    224-42-0
    Dibenz[ a,h]anthracene
    Same
    53-70-3
    U063
    7H-Dibenzo [c,g]carbazole
    Same
    194-59-2
    Dibenzo[ a,e]pyrene
    Naphtho[1,2,3,4-def]
    -
    chrysene
    192-65-4
    Dibenzo[ a,h]pyrene
    Dibenzo[ b,def] chrysene
    189-64-0
    Dibenzo[ a,i]pyrene
    Benzo[ rst]pentaphene
    189-55-9
    U064
    1,2-Dibromo-3-chloropropane
    Propane, 1,2-dibromo-3-
    chloro-
    96-12-8
    U066
    Dibutyl phthalate
    1,2-Benzenedicarboxylic
    acid, dibutyl ester
    84-74-2
    U069
    o-Dichloro benzene
    Benzene, 1,2-dichloro-
    95-50-1
    U070
    m-Dichloro benzene
    Benzene, 1,3-dichloro-
    541-73-1
    U071
    p-Dichloro benzene
    Benzene, 1,4-dichloro-
    106-46-7
    U072
    Dichlorobenzene, N.O.S.
    Benzene, dichloro-
    25321-22-
    6
    3,3'-Dichloro benzidine
    [1,1'-Biphenyl]-4,4'-
    diamine, 3,3'-dichloro-
    91-94-1
    U073
    1,4-Dichloro-2-butene
    2-Butene, 1,4-dichloro-
    764-41-0
    U074
    Dichlorodifluoromethane
    Methane, dichlorodifluoro-
    75-71-8
    U075
    Dichloro ethylene , N.O.S.
    Dichloroethylene
    25323-30-
    2
    1,1-Dichloro ethylene
    Ethene, 1,1-dichloro-
    75-35-4
    U078
    1,2-Dichloro ethylene
    Ethene, 1,2-dichloro-,
    (E)-
    156-60-5
    U079
    Dichloroethyl ether
    Ethane, 1,1'-oxybis[2-
    chloro-
    111-44-4
    U025
    Dichloroiso propyl ether
    Propane, 2,2'-oxybis[2-
    chloro-
    108-60-1
    U027
    Dichloromethoxy ethane
    Ethane, 1,1'-[ methylene -
    bis(oxy)bis[2-chloro-
    111-91-1
    U024
    Dichloromethyl ether
    Methane, oxybis[chloro-
    542-88-1
    P016
    2,4-Dichloro phenol
    Phenol, 2,4-dichloro-
    120-83-2
    U081
    2,6-Dichloro phenol
    Phenol, 2,6-dichloro-
    87-65-0
    U082
    Dichlorophenyl arsine
    Arsonous dichloride,
    phenyl-
    696-28-6
    P036
    Dichloropropane, N.O.S.
    Propane, dichloro-
    26638-19-
    7
    Dichloro propanol , N.O.S.
    Propanol, dichloro-
    26545-73-
    3
    Dichloropropene, N.O.S.
    1-Propene, dichloro-
    26952-23-
    8
    1,3-Dichloro propene
    1-Propene, 1,3-dichloro-
    542-75-6
    U084
    Dieldrin
    2,7:3,6-Dimethanonaphth
    [2,
    3-b]oxirene,3,4,5,6,9,9-
    hexachloro-1a,2,2a,3,6,
    6a,7,7a-octahydro-,
    (1aalpha,2beta,2aalpha,3be
    ta,6beta,6aalpha,7beta,7aa
    lpha)-
    60-57-1
    P037
    1,2:3,4-Diepoxy butane
    2,2'-Bioxirane
    1464-53-5
    U085
    Diethylarsine
    Arsine, diethyl-
    692-42-2
    P038
    Diethylene glycol,
    dicarbamate
    Ethanol, 2,2' -oxybis -,
    dicarbamate
    5952-26-1
    U395
    1,4-Diethylene oxide
    1,4-Dioxane
    123-91-1
    U108
    Diethylhexyl phthalate
    1,2-Benzenedicarboxylic
    117-81-7
    U028
    96
    acid, bis(2-ethylhexyl)
    ester
    N,N'-Diethyl hydrazine
    Hydrazine, 1,2-diethyl-
    1615-80-1
    U086
    O,O-Diethyl-S-methyl
    dithio -
    phosphate
    Phosphorodithioic acid,
    O,O-diethyl S-methyl ester
    3288-58-2
    U087
    Diethyl-p- nitrophenyl
    phosphate
    Phosphoric acid, diethyl
    4-nitro phenyl ester
    311-45-5
    P041
    Diethyl phthalate
    1,2-Benzenedicarboxylic
    acid, diethyl ester
    84-66-2
    U088
    O,O-Diethyl O- pyrazinyl
    phosphoro thioate
    Phosphorothioic acid, O,O-
    diethyl O- pyrazinyl ester
    297-97-2
    P040
    Diethylstil bestrol
    Phenol, 4,4'-(1,2-diethyl-
    1,2-ethene diyl)bis-, (E)-
    56-53-1
    U089
    Dihydrosafrole
    1,3-Benzodioxole, 5-
    propyl-
    94-58-6
    U090
    Diisopropylfluorophosph
    ate
    (DFP)
    Phosphorofluoridic acid,
    bis(1-methylethyl) ester
    55-91-4
    P043
    Dimethoate
    Phosphorodithioic acid,
    O,O-dimethyl S-[2-( methyl -
    amino)-2-oxo ethyl] ester
    60-51-5
    P044
    Dimetilan
    Carbamic acid, dimethyl -,
    1- [(dimethyl amino)
    carbonyl]-5-methyl-1H-
    pyrazol-3-yl ester
    644-64-4
    P191
    3,3'-Dimethoxy benzidine
    [1,1'-Biphenyl]-4,4'-
    diamine, 3,3'-dimethoxy-
    119-90-4
    U091
    p-Dimethyl aminoazobenzene
    Benzenamine, N,N-dimethyl-
    4-(phenyl azo)-
    60-11-7
    U093
    7,12-Dimethyl benz[a] anthra cene
    Benz[a] anthracene, 7,12-
    dimethyl-
    57-97-6
    U094
    3,3'-Dimethyl benzidine
    [1,1'-Biphenyl]-4,4'-
    diamine, 3,3'-dimethyl-
    119-93-7
    U095
    Dimethylcarbam oyl chloride
    Carbamic chloride,
    dimethyl-
    79-44-7
    U097
    1,1-Dimethyl hydrazine
    Hydrazine, 1,1-dimethyl-
    57-14-7
    U098
    1,2-Dimethyl hydrazine
    Hydrazine, 1,2-dimethyl-
    540-73-8
    U099
    alpha,alpha-Dimethylphen
    -
    ethylamine
    Benzeneethanamine, alpha,
    alpha- dimethyl-
    122-09-8
    P046
    2,4-Dimethyl phenol
    Phenol, 2,4-dimethyl-
    105-67-9
    U101
    Dimethyl phthalate
    1,2-Benzenedicarboxylic
    acid, dimethyl ester
    131-11-3
    U102
    Dimethyl sulfate
    Sulfuric acid, dimethyl
    ester
    77-78-1
    U103
    Dinitrobenzene, N.O.S.
    Benzene, dinitro-
    25154-54-
    5
    4,6-Dinitro-o-cresol
    Phenol, 2-methyl-4,6-
    dinitro-
    534-52-1
    P047
    4,6-Dinitro-o-cresol salts
    P047
    2,4-Dinitro phenol
    Phenol, 2,4-dinitro-
    51-28-5
    P048
    2,4-Dinitro toluene
    Benzene, 1-methyl-2,4-
    dinitro-
    121-14-2
    U105
    2,6-Dinitro toluene
    Benzene, 2-methyl-1,3-
    dinitro-
    606-20-2
    U106
    Dinoseb
    Phenol, 2-(1-
    methylpropyl)-4,6-dinitro-
    88-85-7
    P020
    Di-n-octyl phthalate
    1,2-Benzenedicarboxylic
    acid, dioctyl ester
    117-84-0
    U107
    Diphenylamine
    Benzenamine, N-phenyl-
    122-39-4
    1,2-Diphenyl hydrazine
    Hydrazine, 1,2-diphenyl-
    122-66-7
    U109
    Di-n-propyl nitros amine
    1-Propanamine, N-nitroso-
    N-propyl-
    621-64-7
    U111
    97
    Disulfiram
    Thioperoxy dicarbonic
    diamide, tetraethyl
    97-77-8
    U403
    Disulfoton
    Phosphorodithioic acid,
    O,O-diethyl S-[2-(
    ethyl-
    thio)ethyl] ester
    298-04-4
    P039
    Dithiobiuret
    Thioimidodicarbonic
    diamide [(H
    2
    N)C(S)]
    2
    NH
    541-53-7
    P049
    Endosulfan
    6, 9-Methano-2,4,3-benzo
    -
    dioxathie-
    pen,6,7,8,9,10,10-
    hexachloro-1,5,5a,6,9,9a-
    hexahydro-, 3-oxide,
    115-29-7
    P050
    Endothal
    7-
    Oxabicyclo[2.2.1]heptane-
    2,3-di carboxylic acid
    145-73-3
    P088
    Endrin
    2,7:3,6-Dimethanonaphth
    -
    [2,3-b] oxirene,
    3,4,5,6,9,9-hexa chloro-
    1a,2,2a,3,6,6a,7,7a-
    octahydro-, (1a
    alpha,2beta,2abeta,3alpha,
    6alpha,6abeta,7beta,7aalph
    a)-,
    72-20-8
    P051
    Endrin metabolites
    P051
    Epichlorohydrin
    Oxirane, ( chloromethyl)-
    106-89-8
    U041
    Epinephrine
    1,2-Benzenediol, 4-[1-
    hydroxy-2-( methyl amino)-
    ethyl]-, (R)-
    51-43-4
    P042
    EPTC
    Carbamo thioic acid,
    dipropyl -, S-ethyl ester
    759-94-4
    U390
    Ethyl carbamate (urethane)
    Carbamic acid, ethyl ester
    51-79-6
    U238
    Ethyl cyanide
    Propanenitrile
    107-12-0
    P101
    Ethylenebisdithiocarbamic acid
    Carbamodithioic acid, 1,2-
    ethane diylbis-
    111-54-6
    U114
    Ethylenebisdithiocarbamic
    acid, salts and esters
    U114
    Ethylene dibromide
    Ethane, 1,2-dibromo-
    106-93-4
    U067
    Ethylene dichloride
    Ethane, 1,2-dichloro-
    107-06-2
    U077
    Ethylene glycol monoethyl
    ether
    Ethanol, 2-ethoxy-
    110-80-5
    U359
    Ethyleneimine
    Aziridine
    151-56-4
    P054
    Ethylene oxide
    Oxirane
    75-21-8
    U115
    Ethylenethiourea
    2-Imidazolidinethione
    96-45-7
    U116
    Ethylidine dichloride
    Ethane, 1,1-dichloro-
    75-34-3
    U076
    Ethyl methacrylate
    2-Propenoic acid, 2-
    methyl-, ethyl ester
    97-63-2
    U118
    Ethyl methanesulfonate
    Methanesulfonic acid,
    ethyl ester
    62-50-0
    U119
    Ethyl Ziram
    Zinc, bis(diethyl carbamo -
    dithioato -S,S') -
    14324-55-
    1
    U407
    Famphur
    Phosphorothioc acid, O-[4-
    [(dimethylamino) sulfonyl] -
    phenyl] O,O- dimethyl ester
    52-85-7
    P097
    Ferbam
    Iron, tris(dimethyl -
    carbamo dithioato -S,S') -,
    14484-64-
    1
    U396
    Fluoranthene
    Same
    206-44-0
    U120
    Fluorine
    Same
    7782-41-4
    P056
    Fluoroacetamide
    Acetamide, 2-fluoro-
    640-19-7
    P057
    Fluoroacetic acid, sodium salt
    Acetic acid, fluoro-,
    sodium salt
    62-74-8
    P058
    Formaldehyde
    Same
    50-00-0
    U122
    98
    Formetanate hydrochloride
    Methanimid amide,
    N,N-dimethyl-N'-[3-
    [[(methyl amino)carbonyl] -
    oxy]phenyl] -, monohydro-
    chloride
    23422-53-
    9
    P198
    Formic acid
    Same
    64-18-16
    U123
    Formparanate
    Methanimid amide,
    N,N-dimethyl-N'-[2-methyl-
    4-[[(methyl amino)-
    carbonyl] oxy]phenyl] -
    17702-57-
    7
    P197
    Glycidylaldehyde
    Oxiranecarboxaldehyde
    765-34-4
    U126
    Halomethanes, N.O.S.
    Heptachlor
    4,7-Methano-1H-
    indene,1,4,5,6,7,8,8-
    heptachloro-3a,4,7,7a-
    tetrahydro-
    76-44-8
    P059
    Heptachlor epoxide
    2,5-Methano-2H-indeno[1,
    2b]oxirene, 2,3,4,5,6,7,7-
    heptachloro-
    1a,1b,5,5a,6,6a-hexa
    hydro-
    ,
    (1aalpha,1bbeta,2alpha,5al
    pha,5abeta,6beta,6aalpha)-
    1024-57-3
    Heptachlor epoxide (alpha,
    beta, and gamma isomers)
    Heptachlorodibenzofurans
    Heptachlorodibenzo-p-dioxins
    Hexachloro benzene
    Benzene, hexachloro-
    118-74-1
    U127
    Hexachloro butadiene
    1,3-Butadiene,
    1,1,2,3,4,4-hexa chloro-
    87-68-3
    U128
    Hexachlorocyclo-pentadiene
    1,3-Cyclopentadiene,
    1,2,3,4,5,5-hexa chloro-
    77-47-4
    U130
    Hexachlorodi benzo-p-dioxins
    Hexachlorodi benzofurans
    Hexachloroethane
    Ethane, hexachloro-
    67-72-1
    U131
    Hexachlorophene
    Phenol, 2,2'-methylene
    -
    bis[3,4,6-tri chloro-
    70-30-4
    U132
    Hexachloropro pene
    1-Propene, 1,1,2,3,3,3-
    hexachloro-
    1888-71-7
    U243
    Hexaethyltetra phosphate
    Tetraphosphoric acid,
    hexaethyl ester
    757-58-4
    P062
    Hydrazine
    Same
    302-01-2
    U133
    Hydrogen cyanide
    Hydrocyanic acid
    74-90-8
    P063
    Hydrogen fluoride
    Hydrofluoric acid
    7664-39-3
    U134
    Hydrogen sulfide
    Hydrogen sulfide H2S
    7783-06-4
    U135
    Indeno[1,2,3-cd] pyrene
    Same
    193-39-5
    U137
    3-Iodo-2-propynyl-n-butyl
    -
    carbamate
    Carbamic acid, butyl
    -,
    3-iodo-2-propynyl ester
    55406-53-
    6
    U375
    Isobutyl alcohol
    1-Propanol, 2-methyl-
    78-83-1
    U140
    Isodrin
    1,4:5,8-Dimethano
    naph-
    thalene,1,2,3,4,10,10-
    hexachloro-1,4,4a,5,8,8a-
    hexahydro-,
    (1alpha,4alpha,4abeta,5bet
    a,8beta,8abeta)-,
    465-73-6
    P060
    Isolan
    Carbamic acid, dimethyl -,
    3-methyl-1-(1-methyl
    -
    ethyl)-1H-pyrazol-5-yl
    ester
    119-38-0
    P192
    Isosafrole
    1,3-Benzodioxole, 5-(1-
    propenyl)-
    120-58-1
    U141
    99
    Kepone
    1,3,4-Metheno-2H-cyclo
    -
    buta[cd]pentalen-2-one,
    1,1a,3,3a,4,5,5,5a,5b,6-
    decachlorooctahydro-,
    143-50-0
    U142
    Lasiocarpine
    2-Butenoic acid, 2-methyl-
    , 7-[[2,3-dihydroxy-2-(1-
    methoxyethyl)-3-methyl-1-
    oxobutoxy]methyl]-
    2,3,5,7a-tetrahydro-1H-
    pyrrol izin-l-yl ester,
    [1S-[1-
    alpha(Z),7(2S*,3R*),7aalph
    a]]-
    303-34-1
    U143
    Lead
    Same
    7439-92-1
    Lead and compounds, N.O.S.
    Lead acetate
    Acetic acid, lead (2+)
    salt
    301-04-2
    U144
    Lead phosphate
    Phosphoric acid, lead (2+)
    salt (2:3)
    7446-27-7
    U145
    Lead subacetate
    Lead, bis(acetato-O) tetra-
    hydroxy tri-
    1335-32-6
    U146
    Lindane
    Cyclohexane, 1,2,3,4,5,6-
    hexachloro-,
    1alpha,2alpha,3beta,4alpha
    ,5alpha,6beta)-
    58-89-9
    U129
    Maleic anhydride
    2,5-Furandione
    108-31-6
    U147
    Maleic hydrazide
    3,6-Pyridazinedione, 1,2-
    dihydro-
    123-33-1
    U148
    Malononitrile
    Propanedinitrile
    109-77-3
    U149
    Manganese dimethyl dithio -
    carbamate
    Manganese, bis(dimethyl -
    carbamo dithioato -S,S') -,
    15339-36-
    3
    P196
    Melphalan
    L-Phenylalanine, 4-[
    bis(2-
    chloro ethyl) amino]-
    148-82-3
    U150
    Mercury
    Same
    7439-97-6
    U151
    Mercury compounds, N.O.S.
    Mercury fulminate
    Fulminic acid, mercury
    (2+) salt
    628-86-4
    P065
    Metam Sodium
    Carbamo dithioic acid,
    methyl -, monosodium salt
    137-42-8
    U384
    Methacrylo nitrile
    2-Propenenitrile, 2-
    methyl-
    126-98-7
    U152
    Methapyrilene
    1,2-Ethanediamine, N,N-
    dimethyl-N'-2-pyridinyl-
    N'-(2-thienylmethyl)-
    91-80-5
    U155
    Methiocarb
    Phenol, (3,5 -dimethyl-4-
    (methylthio) -, methyl -
    carbamate
    2032-65-7
    P199
    Metholmyl
    Ethanimidothioic acid, N-
    [[(methyl -
    amino)carbonyl] oxy]-,
    methyl ester
    16752-77-
    5
    P066
    Methoxychlor
    Benzene, 1,1'-(2,2,2-
    trichloro ethylidene) bis[4-
    methoxy-
    72-43-5
    U247
    Methyl bromide
    Methane, bromo-
    74-83-9
    U029
    Methyl chloride
    Methane, chloro-
    74-87-3
    U045
    Methylchloro carbonate
    Carbonochloridic acid,
    methyl ester
    79-22-1
    U156
    Methyl chloroform
    Ethane, 1,1,1-trichloro-
    71-55-6
    U226
    3-Methylchol anthrene
    Benz[j] aceanthrylene, 1,2-
    dihydro-3-methyl-
    56-49-5
    U157
    100
    4,4'-Methylene bis(2-chloro -
    aniline)
    Benzenamine, 4,4'-
    methylene bis[2-chloro-
    101-14-4
    U158
    Methylene bromide
    Methane, dibromo-
    74-95-3
    U068
    Methylene chloride
    Methane, dichloro-
    75-09-2
    U080
    Methyl ethyl ketone (MEK)
    2-Butanone
    78-93-3
    U159
    Methyl ethyl ketone peroxide
    2-Butanone, peroxide
    1338-23-4
    U160
    Methyl hydrazine
    Hydrazine, methyl-
    60-34-4
    P068
    Methyl iodide
    Methane, iodo-
    74-88-4
    U138
    Methyl isocyanate
    Methane, isocyanato-
    624-83-9
    P064
    2-Methyl lactonitrile
    Propanenitrile, 2-hydroxy-
    2-methyl-
    75-86-5
    P069
    Methyl methacrylate
    2-Propenoic acid, 2-
    methyl-, methyl ester
    80-62-6
    U162
    Methyl methane sulfonate
    Methanesulfonic acid,
    methyl ester
    66-27-3
    Methyl parathion
    Phosphorothioic acid, O,O-
    dimethyl O-(4-nitrophenyl)
    ester
    298-00-0
    P071
    Methylthiour acil
    4-(1H)- Pyrimidinone, 2,3-
    dihydro-6-methyl-2-thioxo-
    56-04-2
    U164
    Metolcarb
    Carbamic acid, methyl
    -,
    3-methyl phenyl ester
    1129-41-5
    P190
    Mexacarbate
    Phenol, 4 -(dimethylamino)-
    3,5-dimethyl -, methyl -
    carbamate (ester)
    315-18-4
    P128
    Mitomycin C
    Azirino[2', 3':3,
    4]pyrrolo[1, 2-a]indole-4,
    7-dione, 6-amino-8-
    [[(aminocarbonyl )oxy]-
    methyl]-1,1a,2,8,8a,8b-
    hexahydro-8a-methoxy-5-
    methyl-, [1a-S-
    (1aalpha,8beta,8aalpha,8ba
    lpha)]-,
    50-07-7
    U010
    Molinate
    1H-Azepine-1-carbo thioic
    acid, hexahydro -, S-ethyl
    ester
    2212-67-1
    U365
    MNNG
    Guanidine, N-methyl-N'-
    nitro-N-nitroso-
    70-25-7
    U163
    Mustard gas
    Ethane, 1,1'-thiobis[2-
    chloro-
    505-60-2
    U165
    Naphthalene
    Same
    91-20-3
    U165
    1,4-Naphtho quinone
    1,4-Naphthalenedione
    130-15-4
    U166
    alpha- Naphthyl amine
    1-Naphthalenamine
    134-32-7
    U167
    beta-Naphthyl amine
    2-Naphthalenamine
    91-59-8
    U168
    alpha- Naphthyl thiourea
    Thiourea, 1-naphthalenyl-
    86-88-4
    P072
    Nickel
    Same
    7440-02-0
    Nickel compounds, N.O.S.
    Nickel carbonyl
    Nickel carbonyl Ni(CO)
    4
    ,
    (T-4)-
    13463-39-
    3
    P073
    Nickel cyanide
    Nickel cyanide Ni(CN)
    2
    557-19-7
    P074
    Nicotine
    Pyridine, 3-(1-methyl-2-
    pyrrolidinyl)-, (S)-
    54-11-5
    P075
    Nicotine salts
    P075
    Nitric oxide
    Nitrogen oxide NO
    10102-43-
    9
    P076
    p-Nitroaniline
    Benzenamine, 4-nitro-
    100-01-6
    P077
    Nitrobenzene
    Benzene, nitro-
    98-95-3
    P078
    Nitrogen dioxide
    Nitrogen oxide NO
    2
    10102-44-
    0
    P078
    Nitrogen mustard
    Ethanamine, 2-chloro-N-(2-
    51-75-2
    101
    chloroethyl)-N-methyl-
    Nitrogen mus tard, hydro -
    chloride salt
    Nitrogen mustard N-oxide
    Ethanamine, 2-chloro-N-(2-
    chloro ethyl)-N-methyl-, N-
    oxide
    126-85-2
    Nitrogen mus tard, N-oxide,
    hydrochloride salt
    Nitroglycerin
    1,2,3-Propanetriol,
    trinitrate
    55-63-0
    P081
    p-Nitrophenol
    Phenol, 4-nitro-
    100-02-7
    U170
    2-Nitropropane
    Propane, 2-nitro-
    79-46-9
    U171
    Nitrosamines, N.O.S.
    35576-91-
    1
    N-Nitrosodi-n-butylamine
    1-Butanamine, N-butyl-N-
    nitroso-
    924-16-3
    U172
    N-Nitroso diethanolamine
    Ethanol, 2,2'-( nitroso -
    imino) bis-
    1116-54-7
    U173
    N-Nitrosodi ethylamine
    Ethanamine, N-ethyl-N-
    nitroso-
    55-18-5
    U174
    N-Nitrosodi methylamine
    Methanamine, N-methyl-N-
    nitroso-
    62-75-9
    P082
    N-Nitroso-N-ethylurea
    Urea, N-ethyl-N- nitroso-
    759-73-9
    U176
    N-Nitroso methyl ethylamine
    Ethanamine, N-methyl-N-
    nitroso-
    10595-95-
    6
    N-Nitroso-N-methylurea
    Urea, N-methyl-N-
    nitroso-
    684-93-5
    U177
    N-Nitroso-N-methylurethane
    Carbamic acid,
    methylnitroso-, ethyl
    ester
    615-53-2
    U178
    N-Nitroso methyl vinylamine
    Vinylamine, N-methyl-N-
    nitroso-
    4549-40-0
    P084
    N-Nitroso morpholine
    Morpholine, 4-nitroso-
    59-89-2
    N-Nitroso nornicotine
    Pyridine, 3-(1-nitroso-2-
    pyrrolidinyl)-, (S)-
    16543-55-
    8
    N-Nitroso piperidine
    Piperidine, 1-nitroso-
    100-75-4
    U179
    N-Nitroso pyrrolidine
    Pyrrolidine, 1-nitroso-
    930-55-2
    U180
    N-Nitroso sarcosine
    Glycine, N-methyl-N-
    nitroso-
    13256-22-
    9
    5-Nitro-o-tolu idine
    Benzenamine, 2-methyl-5-
    nitro-
    99-55-8
    U181
    Octamethylpyro phosphor amide
    Diphosphoramide,
    octamethyl-
    152-16-9
    P085
    Osmium tetroxide
    Osmium oxide OsO
    4
    , (T-4)
    20816-12-
    0
    P087
    Oxamyl
    Ethanimidothioc acid,
    2-(dimethyl amino)-N-
    [[(methyl amino)carbonyl] -
    oxy]-2-oxo -, methyl ester
    23135-22-
    0
    P194
    Paraldehyde
    1,3,5-Trioxane, 2,4,6-tri
    -
    methyl-
    123-63-7
    U182
    Parathion
    Phosphorothioic acid, O,O-
    diethyl O-(4-nitro
    phenyl)
    ester
    56-38-2
    P089
    Pebulate
    Carbamothioic acid,
    butyl-
    ethyl-, S-propyl ester
    1114-71-2
    U391
    Pentachloro benzene
    Benzene, pentachloro-
    608-93-5
    U183
    Pentachlorodi benzo-p-dioxins
    Pentachlorodi benzofurans
    Pentachloro ethane
    Ethane, pentachloro-
    76-01-7
    U184
    Pentachloro nitrobenzene (PCNB)
    Benzene, pentachloronitro-
    82-68-8
    U185
    Pentachloro phenol
    Phenol, pentachloro-
    87-86-5
    See
    102
    F027
    Phenacetin
    Acetamide, N-(4-
    ethoxyphenyl)-
    62-44-2
    U187
    Phenol
    Same
    108-95-2
    U188
    Phenylenediamine
    Benzenediamine
    25265-76-
    3
    Phenylmercury acetate
    Mercury, ( acetato-
    O)phenyl-
    62-38-4
    P092
    Phenylthiourea
    Thiourea, phenyl-
    103-85-5
    P093
    Phosgene
    Carbonic dichloride
    75-44-5
    P095
    Phosphine
    Same
    7803-51-2
    P096
    Phorate
    Phosphorodithioic acid,
    O,O-diethyl S-
    [(ethylthio)methyl] ester
    298-02-2
    P094
    Phthalic acid esters, N.O.S.
    Phthalic anhydride
    1,3-Isobenzofurandione
    85-44-9
    U190
    Physostigmine
    Pyrrolo [2,3-b] indol-5-ol,
    1,2,3,3a,8,8a-hexa
    hydro-
    1,3a,8-trimethyl -, methyl -
    carbamate (ester),
    (3aS-cis)-
    57-47-6
    P204
    Physostigmine salicylate
    Benzoic acid, 2 -hydroxy -,
    compound with (3aS
    -cis)-
    1,2,3,3a,8,8a-hexa
    hydro-
    1,3a,8-trimethyl pyrrolo -
    [2,3-b] indol-5-yl methyl -
    carbamate ester (1:1)
    57-64-7
    P188
    2-Picoline
    Pyridine, 2-methyl-
    109-06-8
    U191
    Polychlorinated biphenyls,
    N.O.S.
    Potassium cyanide
    Same
    151-50-8
    P098
    Potassium dimethyl dithio -
    carbamate
    Carbamodithioc acid,
    dimethyl, potassium salt
    128-03-0
    U383
    Potassium n-hydroxy methyl-n-
    methyl-dithio carbamate
    Carbamodithioc acid,
    (hydroxy methyl )methyl -,
    monopotassium salt
    51026-28-
    9
    U378
    Potassium n -methyl dithio -
    carbamate
    Carbamo dithioc acid,
    methyl- monopotassium salt
    137-41-7
    U377
    Potassium silver cyanide
    Argentate(1-), bis(cyano-
    C)-, potassium)
    506-61-6
    P099
    Potassium pentachlorophenate
    Pentachlorophenol,
    potassium salt
    7778736
    None
    Promecarb
    Phenol, 3 -methyl-5-(1-
    methyl ethyl) -, methyl
    carbamate
    2631-37-0
    P201
    Pronamide
    Benzamide, 3,5-dichloro-N-
    (1,1-di methyl-2-propynyl)-
    23950-58-
    5
    U192
    1,3-Propane sultone
    1,2-Oxathiolane, 2,2-
    dioxide
    1120-71-4
    U193
    Propham
    Carbamic acid, phenyl
    -,
    1-methyl ethyl ester
    122-42-9
    U373
    Propoxur
    Phenol, 2 -(1-methyl -
    ethoxy) -, methyl carbamate
    114-26-1
    U411
    n-Propylamine
    1-Propanamine
    107-10-8
    U194
    Propargyl alcohol
    2-Propyn-1-ol
    107-19-7
    P102
    Propylene dichloride
    Propane, 1,2-dichloro-
    78-87-5
    U083
    1,2-Propylen imine
    Aziridine, 2-methyl-
    75-55-8
    P067
    Propylthio uracil
    4(1H)- Pyrimidinone, 2,3-
    dihydro-6-propyl-2-thioxo-
    51-52-5
    Prosulfocarb
    Carbamothioic acid,
    dipropyl -, S-(phenyl -
    52888-80-
    9
    U387
    103
    methyl) ester
    Pyridine
    Same
    110-86-1
    U196
    Reserpine
    Yohimban-16-carboxylic
    acid, 11,17-dimethoxy-18-
    [(3,4,5-tri methoxy-
    benzoyl) oxy]-, methyl
    ester,
    (3beta,16beta,17alpha,18be
    ta,20alpha)-,
    50-55-5
    U200
    Resorcinol
    1,3-Benzenediol
    108-46-3
    U201
    Saccharin
    1,2-Benzisothiazol-3(2H)-
    one, 1,1-dioxide
    81-07-2
    U202
    Saccharin salts
    U202
    Safrole
    1,3-Benzodioxole, 5-(2-
    propenyl)-
    94-59-7
    U203
    Selenium
    Same
    7782-49-2
    Selenium compounds, N.O.S.
    Selenium dioxide
    Selenious acid
    7783-00-8
    U204
    Selenium sulfide
    Selenium sulfide SeS
    2
    7488-56-4
    U205
    Selenium, tetrakis(dimethyl-
    dithiocarbamate
    Carbamo dithioic acid,
    dimethyl -, tetraanhydro -
    sulfide with orthothio-
    selenious acid
    144-34-3
    U376
    Selenourea
    Same
    630-10-4
    P103
    Silver
    Same
    7440-22-4
    Silver com pounds, N.O.S.
    Silver cyanide
    Silver cyanide AgCN
    506-64-9
    P104
    Silvex (2,4,5-TP)
    Propanoic acid, 2-(2,4,5-
    trichlorophenoxy)-
    93-72-1
    See
    F027
    Sodium cyanide
    Sodium cyanide NaCN
    143-33-9
    P106
    Sodium dibutyl dithio carbamate
    Carbamodithioic acid,
    dibutyl -, sodium salt
    136-30-1
    U379
    Sodium diethyl dithio carbamate
    Carbamodithioic acid,
    diethyl -, sodium salt
    148-18-5
    U381
    Sodium dimethyl dithio carbamate
    Carbamodithioic acid,
    dimethyl -, sodium salt
    128-04-1
    U382
    Sodium pentachlorophenate
    Pentachlorophenol, sodium
    salt
    131522
    None
    Streptozotocin
    D-Glucose, 2-deoxy-2-
    [[methyl nitroso amino)ca-
    rbonyl]amino]-
    18883-66-
    4
    U206
    Strychnine
    Strychnidin-10-one
    57-24-9
    P108
    Strychnine salts
    P108
    Sulfallate
    Carbamodithioic acid,
    diethyl -, 2-chloro-2-
    propenyl ester
    95-06-7
    U277
    TCDD
    Dibenzo[ b,e][1,4]dioxin,
    2,3,7,8-tetrachloro-
    1746-01-6
    Tetrabutyl thiuram disulfide
    Thioperoxydicarbonic
    diamide, tetrabutyl
    1634-02-2
    U402
    Tetrabutylmethyl thiuram
    monosulfide
    Bis(dimethyl thiocarbamoyl )
    sulfide
    97-74-5
    U401
    1,2,4,5-Tetra chlorobenzene
    Benzene, 1,2,4,5-
    tetrachloro-
    95-94-3
    U207
    Tetrachlorodi benzo-p-dioxins
    Tetrachlorodi benzofurans
    Tetrachloro ethane , N.O.S.
    Ethane, tetrachloro-,
    N.O.S.
    25322-20-
    7
    1,1,1,2-Tetra chloro ethane
    Ethane, 1,1,1,2-
    tetrachloro-
    630-20-6
    U208
    1,1,2,2-Tetra chloro ethane
    Ethane, 1,1,2,2-
    79-34-5
    U209
    104
    tetrachloro-
    Tetrachloro ethylene
    Ethene, tetrachloro-
    127-18-4
    U210
    2,3,4,6-Tetra chloro phenol
    Phenol, 2,3,4,6-
    tetrachloro-
    58-90-2
    See
    F027
    2,3,4,6-Tetra chloro phenol,
    potassium salt
    Same
    53535276
    None
    2,3,4,6-Tetra chloro phenol,
    sodium salt
    Same
    25567559
    None
    Tetraethyl dithiopyrophosphate
    Thiodiphosphoric acid,
    tetraethyl ester
    3689-24-5
    P109
    Tetraethyl lead
    Plumbane, tetraethyl-
    78-00-2
    P110
    Tetraethyl pyrophosphate
    Diphosphoric acid,
    tetraethyl ester
    107-49-3
    P111
    Tetranitro methane
    Methane, tetranitro-
    509-14-8
    P112
    Thallium
    Same
    7440-28-0
    Thallium compounds
    Thallic oxide
    Thallium oxide Tl
    2
    O
    3
    1314-32-5
    P113
    Thallium (I) acetate
    Acetic acid, thallium (1+)
    salt
    563-68-8
    U214
    Thallium (I) carbonate
    Carbonic acid, dithallium
    (1+) salt
    6533-73-9
    U215
    Thallium (I) chloride
    Thallium chloride
    TlCl
    7791-12-0
    U216
    Thallium (I) nitrate
    Nitric acid, thallium (1+)
    salt
    10102-45-
    1
    U217
    Thallium selenite
    Selenious acid, dithallium
    (1+) salt
    12039-52-
    0
    P114
    Thallium (I) sulfate
    Sulfuric acid, dithallium
    (1+) salt
    7446-18-6
    P115
    Thioacetamide
    Ethanethioamide
    62-55-5
    U218
    Thiodicarb
    Ethanimido thioic acid,
    N,N'-[thiobis[( methyl -
    imino) carbonyloxy]]- bis-,
    dimethyl ester
    59669-26-
    0
    U410
    Thiofanox
    2-Butanone, 3,3-dimethyl-
    1-(methyl thio)-, O-
    [(methylamino)carbonyl]
    -
    oxime
    39196-18-
    4
    P045
    Thiophanate-methyl
    Carbamic acid,
    [1,2-phyenyl enebis( imino-
    carbono thioyl )]-bis-,
    dimethyl ester
    23564-05-
    8
    U409
    Thiomethanol
    Methanethiol
    74-93-1
    U153
    Thiophenol
    Benzenethiol
    108-98-5
    P014
    Thiosemicarb azide
    Hydrazinecarbothioamide
    79-19-6
    P116
    Thiourea
    Same
    62-56-6
    P219
    Thiram
    Thioperoxydicarbonic
    diamide [(H
    2
    N)C(S)]
    2
    S
    2
    ,
    tetramethyl-
    137-26-8
    U244
    Tirpate
    1,3-Dithiolane-2-carbox
    -
    aldehyde, 2,4 -dimethyl -,
    O-[(methyl amino)carbonyl]
    oxime
    26419-73-
    8
    P185
    Toluene
    Benzene, methyl-
    108-88-3
    U220
    Toluenediamine
    Benzenediamine, ar-methyl-
    25376-45-
    8
    U221
    Toluene-2,4-diamine
    1,3-Benzenediamine, 4-
    methyl-
    95-80-7
    Toluene-2,6-di amine
    1,3-Benzenediamine, 2-
    methyl-
    823-40-5
    Toluene-3,4-di amine
    1,2-Benzenediamine, 4-
    methyl-
    496-72-0
    105
    Toluene diisocyanate
    Benzene, 1,3-diisocyanato
    -
    methyl-
    26471-62-
    5
    U223
    o-Toluidine
    Benzenamine, 2-methyl-
    95-53-4
    U328
    o-Toluidine hydro chloride
    Benzeneamine, 2-methyl-,
    hydrochloride
    636-21-5
    U222
    p-Toluidine
    Benzenamine, 4-methyl-
    106-49-0
    U353
    Toxaphene
    Same
    8001-35-2
    P123
    Triallate
    Carbamothioic acid,
    bis-
    (1-methyl ethyl) -,
    S-(2,3,3-tri chloro-2-
    propenyl) ester
    2303-17-5
    U389
    1,2,4-Tri chloro benzene
    Benzene, 1,2,4-trichloro-
    120-82-1
    1,1,2-Tri chloro ethane
    Ethane, 1,1,2-trichloro-
    79-00-5
    U227
    Trichloro ethylene
    Ethene, trichloro-
    79-01-6
    U228
    Trichloromethanethiol
    Methanethiol, trichloro-
    75-70-7
    P118
    Trichloro monofluoro methane
    Methane, trichlorofluoro-
    75-69-4
    U121
    2,4,5-Tri chloro phenol
    Phenol, 2,4,5-trichloro-
    95-95-4
    See
    F027
    2,4,6-Tri chloro phenol
    Phenol, 2,4,6-trichloro-
    88-06-2
    See
    F027
    2,4,5-T
    Acetic acid, (2,4,5-
    trichloro phenoxy)-
    93-76-5
    See
    F027
    Trichloropro pane, N.O.S.
    25735-29-
    9
    1,2,3-Tri chloro propane
    Propane, 1,2,3-trichloro-
    96-18-4
    Triethylamine
    Ethanamine, N,N -diethyl -
    121-44-8
    U404
    O,O,O- Triethyl phosphoro thioate
    Phosphorothioic acid,
    O,O,O- triethyl ester
    126-68-1
    1,3,5-Trinitro benzene
    Benzene, 1,3,5-trinitro-
    99-35-4
    U234
    Tris(l- aziridinyl)phosphine
    sulfide
    Aziridine, 1,1',1"-phos
    -
    phinothioyl idynetris-
    52-24-4
    Tris(2,3-di bromopropyl)
    phosphate
    1-Propanol, 2,3-dibromo-,
    phosphate (3:1)
    126-72-7
    U235
    Trypan blue
    2,7-Naphthalenedisulfonic
    acid, 3,3'-[(3,3'-
    dimethyl [1,1'-biphenyl]-
    4,4'-diyl) bis(azo)]bis[5-
    amino-4-hydroxy-,
    tetrasodium salt
    72-57-1
    U236
    Uracil mustard
    2,4-(1H,3H)-
    Pyrimidinedione, 5-[
    bis(2-
    chloroethyl)amino]-
    66-75-1
    U237
    Vanadium pentoxide
    Vanadium oxide V
    2
    O
    5
    1314-62-1
    P120
    Vernolate
    Carbamothioc acid,
    dipropyl -, S-propyl ester
    1929-77-7
    U385
    Vinyl chloride
    Ethene, chloro-
    75-01-4
    U043
    Warfarin
    2H-1-Benzopyran-2-one, 4-
    hydroxy-3-(3-oxo-1-phenyl
    -
    butyl)-, when present at
    concentrations less than
    0.3%
    81-81-2
    U248
    Warfarin
    2H-1-Benzopyran-2-one, 4-
    hydroxy-3-(3-oxo-1-phenyl
    -
    butyl)-, when present at
    concentrations greater
    than 0.3%
    81-81-2
    P001
    Warfarin salts, when present
    at concentrations less than
    0.3%
    U248
    Warfarin salts, when present
    at concentrations greater than
    P001
    106
    0.3%
    Zinc cyanide
    Zinc cyanide Zn(CN)
    2
    557-21-1
    P121
    Zinc phosphide
    Zinc phosphide P
    2
    Zn
    3
    , when
    present at concentrations
    greater than 10%
    1314-84-7
    P122
    Zinc phosphide
    Zinc phosphide P
    2
    Zn
    3
    , when
    present at concentrations
    of 10% or less
    1314-84-7
    U249
    Ziram
    Zinc, bis(dimethyl carbamo -
    dithioato -S,S') - (T-4)-
    137-30-4
    P205
    Note: The abbreviation N.O.S. (not otherwise specified) signifies those
    members of the general class not specifically listed by name in this Section.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 722
    STANDARDS APPLICABLE TO GENERATORS OF HAZARDOUS WASTE
    SUBPART A: GENERAL
    Section
    722.110
    Purpose, Scope and Applicability
    722.111
    Hazardous Waste Determination
    722.112
    USEPA Identification Numbers
    SUBPART B: THE MANIFEST
    Section
    722.120
    General Requirements
    722.121
    Acquisition of Manifests
    722.122
    Number of Copies
    722.123
    Use of the Manifest
    SUBPART C: PRE-TRANSPORT REQUIREMENTS
    Section
    722.130
    Packaging
    722.131
    Labeling
    722.132
    Marking
    722.133
    Placarding
    722.134
    Accumulation Time
    SUBPART D: RECORDKEEPING AND REPORTING
    Section
    722.140
    Recordkeeping
    722.141
    Annual Reporting
    722.142
    Exception Reporting
    722.143
    Additional Reporting
    722.144
    Special Requirements for Generators of between 100 and 1000
    kilograms per month
    SUBPART E: EXPORTS OF HAZARDOUS WASTE
    Section
    722.150
    Applicability
    722.151
    Definitions
    722.152
    General Requirements
    722.153
    Notification of Intent to Export
    107
    722.154
    Special Manifest Requirements
    722.155
    Exception Report
    722.156
    Annual Reports
    722.157
    Recordkeeping
    722.158
    International Agreements
    SUBPART F: IMPORTS OF HAZARDOUS WASTE
    Section
    722.160
    Imports of Hazardous Waste
    SUBPART G: FARMERS
    Section
    722.170
    Farmers
    SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
    FOR RECOVERY WITHIN THE OECD
    Section
    262.180 Applicability
    262.181 Definitions
    262.182 General Conditions
    262.183 Notification and Consent
    262.184 Tracking Document
    262.185 Contracts
    262.186 Provisions Relating to Recognized Traders
    262.187 Reporting and Recordkeeping
    262.189 OECD Waste Lists
    722.Appendix A
    Hazardous Waste Manifest
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
    1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
    effective May 17, 1982; amended in R82-18, 51 PCB 31, at 7 Ill. Reg. 2518,
    effective February 22, 1983; amended in R84-9 at 9 Ill. Reg. 11950, effective
    July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1131, effective January 2,
    1986; amended in R86-1 at 10 Ill. Reg. 14112, effective August 12, 1986;
    amended in R86-19 at 10 Ill. Reg. 20709, effective December 2, 1986; amended
    in R86-46 at 11 Ill. Reg. 13555, effective August 4, 1987; amended in R87-5 at
    11 Ill. Reg. 19392, effective November 12, 1987; amended in R87-39 at 12 Ill.
    Reg. 13129, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 452,
    effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18523, effective
    November 13, 1989; amended in R90-10 at 14 Ill. Reg. 16653, effective
    September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9644, effective June 17,
    1991; amended in R91-1 at 15 Ill. Reg. 14562, effective October 1, 1991;
    amended in R91-13 at 16 Ill. Reg. 9833, effective June 9, 1992; amended in
    R92-1 at 16 Ill. Reg. 17696, effective November 6, 1992; amended in R93-4 at
    17 Ill. Reg. 20822, effective November 22, 1993; amended in R95-6 at 19 Ill.
    Reg. 9935, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11236,
    August 1, 1996 ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________,
    effective ____________________
    .
    SUBPART A: GENERAL
    Section 722.110
    Purpose, Scope and Applicability
    a)
    These regulations establish standards for generators of hazardous
    waste.
    108
    b)
    35 Ill. Adm. Code 721.105(c) and (d) must be used to determine the
    applicability of provisions of this Part that are dependent on
    calculations of the quantity of hazardous waste generated per
    month.
    c)
    A generator whothat treats, stores or disposes of hazardous waste
    on-site must only comply with the following Sections of this Part
    with respect to that waste: Section 722.111 for determining
    whether or not the generator has a hazardous waste, Section
    722.112 for obtaining an EPA identification number, Section
    722.140(c) and (d) for
    recordkeeping, Section 722.143 for
    additional reporting and, if applicable, Section 722.170 for
    farmers.
    d)
    Any person whothat exports or imports hazardous waste
    into the
    United States subject to the hazardous waste manifesting
    requirements of 35 Ill. Adm. Code 722 or subject to the universal
    waste management standards of 35 Ill. Adm. Code 733 to or from
    countries listed in Section 722.158(a)(1) for recovery
    must comply
    with the standards applicable to generators established in this
    Part722.Subpart H .
    e)
    A farmer whothat generates waste pesticides which are hazardous
    waste and whothat complies with all of the requirements of Section
    722.151 is not required to comply with other standards in this
    Part, or 35 Ill. Adm. Code 702, 703, 724 725 or 728 with respect
    to such pesticides.
    f)
    A person whothat generates a hazardous waste as defined by 35 Ill.
    Adm. Code 721 is subject to the compliance requirements and
    penalties prescribed in Title VIII and XII of the Environmental
    Protection Act if he does not comply with the requirements of this
    Part.
    g)
    An owner or operator
    whothat initiates a shipment of hazardous
    waste from a treatment, storage or disposal facility must comply
    with the generator standards established in this Part.
    BOARD NOTE: The provisions of Section 722.134 are applicable to
    the on-site accumulation of hazardous waste by generators.
    Therefore, the provisions of Section 722.134 only apply to owners
    or operators whothat are shipping hazardous waste which they
    generated at that facility. A generator
    whothat treats, stores or
    disposes of hazardous waste on-site must comply with the
    applicable standards and permit requirements set forth in 35 Ill.
    Adm. Code 702, 703, 724, 725, 726 and 728.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART C: PRE-TRANSPORT REQUIREMENTS
    Section 722.134
    Accumulation Time
    a)
    Except as provided in subsections (d), (e), or (f) below, a
    generator is exempt from all the requirements in 35 Ill. Adm. Code
    725.Subparts G and H, except for 35 Ill. Adm. Code 725.211 and
    725.214, and may accumulate hazardous waste on-site for 90 days or
    less without a permit or without having interim status, provided
    that:
    109
    1)
    The waste is placed:
    A)
    In containers and the generator complies with 35 Ill.
    Adm. Code 725.Subpart
    s I, AA, BB, and CC ; or
    B)
    In tanks and the generator complies with 35 Ill. Adm.
    Code 725.Subparts J
    , (except 35 Ill. Adm. Code
    725.297(c) and 725.300
    ), AA, BB, and CC
    ; or
    C)
    On drip pads and the generator complies with 35 Ill.
    Adm. Code 725.Subpart W and maintains the following
    records at the facility:
    i)
    A description of the procedures that will be
    followed to ensure that all wastes are removed
    from the drip pad and associated collection
    system at least once every 90 days, and
    ii)
    Documentation of each waste removal, including
    the quantity of waste removed from the drip pad
    and the sump or collection system and the date
    and time of removal; or
    D)
    In containment buildings and the generator complies
    with 35 Ill. Adm. Code 725.Subpart DD (has placed its
    Professional Engineer (PE) certification that the
    building complies with the design standards specified
    in 35 Ill. Adm. Code 725.1101 in the facility's
    operating record prior to the date of initial
    operation of the unit). The owner or operator shall
    maintain the following records at the facility:
    i)
    A written description of procedures to ensure
    that each waste volume remains in the unit for
    no more than 90 days, a written description of
    the waste generation and management practices
    for the facility showing that they are
    consistent with respecting the 90 day limit, and
    documentation that the procedures are complied
    with; or
    ii)
    Documentation that the unit is emptied at least
    once every 90 days.
    BOARD NOTE: The "in addition" hanging
    subsection that appears in the Federal rules
    after 40 CFR 262.34(a)(1)(iv)(B) is in the
    introduction to subsection (a) above.
    2)
    The date upon which each period of accumulation begins is
    clearly marked and visible for inspection on each container;
    3)
    While being accumulated on-site, each container and tank is
    labeled or marked clearly with the words "Hazardous Waste",
    and
    4)
    The generator complies with the requirements for treatment,
    storage, and disposal facility owners or operators in 35
    Ill. Adm. Code 725.Subparts C and D and with 35 Ill. Adm.
    Code 725.116 and 728.107(a)(4).
    110
    b)
    A generator that accumulates hazardous waste for more than 90 days
    is an operator of a storage facility and is subject to the
    requirements of 35 Ill. Adm. Code 724 and 725 and the permit
    requirements of 35 Ill. Adm. Code 702, 703 and 705 unless the
    generator has been granted an extension of the 90-day period. If
    hazardous wastes must remain on-site for longer than 90 days due
    to unforeseen, temporary, and uncontrollable circumstances, the
    generator may seek an extension of up to 30 days by means of a
    variance or provisional variance, pursuant to Section 37 of the
    Environmental Protection Act and 35 Ill. Adm. Code 180 (Agency
    procedural regulations).
    c)
    Accumulation near the point of generation.
    1)
    A generator may accumulate as much as 55 gallons of
    hazardous waste or one quart of acutely hazardous waste
    listed in 35 Ill. Adm. Code 721.133(e) in containers at or
    near any point of generation where wastes initially
    accumulate that is under the control of the operator of the
    process generating the waste without a permit or interim
    status and without complying with subsection (a) above,
    provided the generator:
    A)
    Complies with 35 Ill. Adm. Code 725.271, 725.272 and
    725.273(a), and
    B)
    Marks the generator's containers either with the words
    "Hazardous Waste" or with other words that identify
    the contents of the containers.
    2)
    A generator that accumulates either hazardous waste or
    acutely hazardous waste listed in 35 Ill. Adm. Code
    721.133(e) in excess of the amounts listed in subsection
    (c)(1) above at or near any point of generation must, with
    respect to that amount of excess waste, comply within three
    days with subsection (a) above or other applicable
    provisions of this Chapter. During the three day period the
    generator must continue to comply with subsection (c)(1)
    above. The generator must mark the container holding the
    excess accumulation of hazardous waste with the date the
    excess amount began accumulating.
    d)
    A generator that generates greater than 100 kilograms but less
    than 1000 kilograms of hazardous waste in a calendar month may
    accumulate hazardous waste on-site for 180 days or less without a
    permit or without having interim status provided that:
    1)
    The quantity of waste accumulated on-site never exceeds 6000
    kilograms;
    2)
    The generator complies with the requirements of 35 Ill. A
    dm.
    Code 725.Subpart I (except 35 Ill. Adm. Code 725.276 and
    725.278);
    3)
    The generator complies with the requirements of 35 Ill. Adm.
    Code 725.301;
    4)
    The generator complies with the requirements of subsections
    (a)(2) and (c)(3) above, 35 Ill. Adm. Code 725.Subpart C,
    and 35 Ill. Adm. Code 728.107(a)(4); and
    111
    5)
    The generator complies with the following requirements:
    A)
    At all times there must be at least one employee
    either on the premises or on call (i.e., available to
    respond to an emergency by reaching the facility
    within a short period of time) with the responsibility
    for coordinating all emergency response measures
    specified in subsection (d)(5)(D) below. The employee
    is the emergency coordinator.
    B)
    The generator shall post the following information
    next to the telephone:
    i)
    The name and telephone number of the emergency
    coordinator;
    ii)
    Location of fire extinguishers and spill control
    material and, if present, fire alarm; and
    iii)
    The telephone number of the fire depar
    tment,
    unless the facility has a direct alarm.
    C)
    The generator shall ensure that all employees are
    thoroughly familiar with proper waste handling and
    emergency procedures, relevant to their
    responsibilities during normal facility operations and
    emergencies;
    D)
    The emergency coordinator or designee shall respond to
    any emergencies that arise. The applicable responses
    are as follows:
    i)
    In the event of a fire, call the fire department
    or attempt to extinguish it using a fire
    extinguisher;
    ii)
    In the event of a spill, contain the flow of
    hazardous waste to the extent possible and, as
    soon as is practicable, clean up the hazardous
    waste and any contaminated materials or soil;
    iii)
    In the event of a fire, explosion, or other
    release that could threaten human health outside
    the facility, or when the generator has
    knowledge that a spill has reached surface
    water, the generator shall immediately notify
    the National Response Center (using its 24-hour
    toll free number 800-424-8802). The report must
    include the following information: the name,
    address, and U .S. EPA identification number (35
    Ill. Adm. Code 722.112) of the generator; the
    date, time, and type of incident (e.g., spill or
    fire); the quantity and type of hazardous waste
    involved in the incident; the extent of
    injuries, if any; and the estimated quantity and
    disposition of recoverable materials, if any.
    e)
    A generator that generates greater than 100 kilograms but less
    than 1000 kilograms of hazardous waste in a calendar month and
    that must transport the waste or offer the waste for
    transportation over a distance of 200 miles or more for off-site
    112
    treatment, storage, or disposal may accumulate hazardous waste on-
    site for 270 days or less without a permit or without having
    interim status, provided that the generator complies with the
    requirements of subsection (d) above.
    f)
    A generator that generates greater than 100 kilograms but less
    than 1000 kilograms of hazardous waste in a calendar month and
    that accumulates hazardous waste in quantities exceeding 6000 kg
    or accumulates hazardous waste for more than 180 days (or for more
    than 270 days if the generator must transport the waste or offer
    the waste for transportation over a distance of 200 miles or more)
    is an operator of a storage facility and is subject to the
    requirements of 35 Ill. Adm. Code 724 and 725 and the permit
    requirements of 35 Ill. Adm. Code 703 unless the generator has
    been granted an extension to the 180-day (or 270-day if
    applicable) period. If hazardous wastes must remain on-site for
    longer than 180 days (or 270 days if applicable) due to
    unforeseen, temporary, and uncontrollable circumstances, the
    generator may seek an extension of up to 30 days by means of
    variance or provisional variance pursuant to Section 37 of the
    Environmental Protection Act.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART E: EXPORTS OF HAZARDOUS WASTE
    Section 722.153
    Notification of Intent to Export
    a)
    The Board incorporates by reference 40 CFR 262.53
    (199196), as
    amended at 56 Fed. Reg. 43705, September 4, 1991
    . This Part
    incorporates no future editions or amendments.
    b)
    A primary exporter of hazardous waste shall notify USEPA in
    accordance with 40 CFR 262.53
    (1996) .
    c)
    The primary exporter shall send the Agency a copy of
    theeach
    notice sent to USEPA pursuant to subsection (b)
    above .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 722.156
    Annual Reports
    a)
    The Board incorporates by reference 40 CFR 262.56 (19
    9196), as
    amended at 56 Fed. Reg. 43705, September 4, 1991
    . This Part
    incorporates no future editions or amendments.
    b)
    Primary exporters of hazardous waste shall file with USEPA, no
    later than March 1 of each year, a report as specified in 40 CFR
    262.56 (1996) .
    c)
    The primary exporter shall send the Agency a copy of
    theeach
    report sent to USEPA.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 722.158
    International Agreements
    a)
    Any person that exports or imports hazardous waste subject to
    either the manifest requirements of this Part or the universal
    waste management standards of 35 Ill. Adm. Code 733 which is
    113
    shipped to or from designated member countries of the Organization
    for Economic Cooperation and Development (OECD), as defined in
    subsection (a)(1) below, for purposes of recovery is subject to
    the requirements of 722.Subpart H. The requirements of
    722.Subparts E and F do not apply where 722.Subpart H applies.
    1)
    For the purposes of this Subpart, the designated OECD
    countries are Australia, Austria, Belgium, Denmark, Finland,
    France, Germany, Greece, Iceland, Ireland, Italy, Japan,
    Luxembourg, Netherlands, New Zealand, Norway, Portugal,
    Spain, Sweden, Switzerland, Turkey, the United Kingdom, and
    the United States.
    2)
    Only for the purposes of transit under this Subpart, Canada
    and Mexico are considered OECD member countries.
    b)
    Any person that exports hazardous waste to or imports hazardous
    waste from any of a designated OECD member country for purposes
    other than recovery (e.g., incineration, disposal), Mexico (for
    any purpose), or Canada (for any purpose) remains subject to the
    requirements of 722.Subparts E and F.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
    FOR RECOVERY WITHIN THE OECD
    Section 722.180
    Applicability
    a)
    The requirements of this Subpart apply to imports and exports of
    wastes that are considered hazardous under U.S. national
    procedures and which are destined for recovery operations in any
    of the countries listed in Section 722.158(a)(1). A waste is
    considered hazardous under U.S. national procedures if it meets
    the definition of hazardous waste in 35 Ill. Adm. Code 721.103 and
    it is subject to either the manifesting requirements at 35 Ill.
    Adm. Code 722.Subpart B, to the universal waste management
    standards of 35 Ill. Adm. Code 733.
    b)
    Any person ( notifier, consignee, or recovery facility operator)
    that mixes two or more wastes (including hazardous and
    non-hazardous wastes) or otherwise subjects two or more wastes
    (including hazardous and non
    -hazardous wastes) to physical or
    chemical transformation operations, and thereby creates a new
    hazardous waste, becomes a generator and assumes all subsequent
    generator duties under this Subchapter and any
    notifier duties
    under this Subpart, as applicable.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.181
    Definitions
    The following definitions apply to this Subpart:
    "Competent authorities" means the regulatory authorities of
    concerned countries having jurisdiction over
    transfrontier
    movements of wastes destined for recovery operations.
    "Concerned countries" means the exporting and importing OECD
    member countries and any OECD member countries of transit.
    114
    "Consignee" means the person to whom possession or other form of
    legal control of the waste is assigned at the time the waste is
    received in the importing country.
    "Country of transit" means any designated OECD country in Section
    722.158(a)(1) and (a)(2) other than the exporting or importing
    country across which a
    transfrontier movement of wastes is planned
    or takes place.
    "Exporting country" means any designated OECD member country in
    Section 722.158(a)(1) from which a
    transfrontier movement of
    wastes is planned or has commenced.
    "Importing country" means any designated OECD country in Section
    722.158(a)(1) to which a
    transfrontier movement of wastes is
    planned or takes place for the purpose of submitting the wastes to
    recovery operations therein.
    "Notifier" means the person under the jurisdiction of the
    exporting country that has, or will have at the time the planned
    transfrontier movement commences, possession or other forms of
    legal control of the wastes and that proposes their
    transfrontier
    movement for the ultimate purpose of submitting them to recovery
    operations. When the United States (U.S.) is the exporting
    country, notifier is interpreted to mean a person domiciled in the
    U.S.
    "OECD area" means all land or marine areas under the national
    jurisdiction of any designated OECD member country in Section
    722.158. When the regulations refer to shipments to or from an
    OECD country, this means OECD area.
    "Recognized trader" means a person that, with appropriate
    authorization of concerned countries, acts in the role of
    principal to purchase and subsequently sell wastes; this person
    has legal control of such wastes from time of purchase to time of
    sale; such a person may act to arrange and facilitate
    transfrontier movements of wastes destined for recovery
    operations.
    "Recovery facility" means an entity which, under applicable
    domestic law, is operating or is authorized to operate in the
    importing country to receive wastes and to perform recovery
    operations on them.
    "Recovery operations" means activities leading to resource
    recovery, recycling, reclamation, direct re
    -use, or alternative
    uses, as listed in Table 2.B of the Annex of OECD Council Decision
    C(88)90(Final) of 27 May 1988, incorporated by reference in 35
    Ill. Adm. Code 720.111, which include the following activities:
    R1
    Use as a fuel (other than in direct incineration) or
    other means to generate energy,
    R2
    Solvent reclamation or regeneration,
    R3
    Recycling or reclamation of organic substances which
    are not used as solvents,
    R4
    Recycling or reclamation of metals and metal
    115
    compounds,
    R5
    Recycling or reclamation of other inorganic materials,
    R6
    Regeneration of acids or bases,
    R7
    Recovery of components used for pollution control,
    R8
    Recovery of components from catalysts,
    R9
    Used oil re -refining or other reuses of previously
    used oil,
    R10
    Land treatment resulting in benefit to agriculture or
    ecological improvement,
    R11
    Uses of residual materials obtained from any of the
    operations numbered R1 through R10,
    R12
    Exchange of wastes for submission to any of the
    operations numbered R1 through R11, and
    R13
    Accumulation of material intended for any operation in
    Table 2.B.
    "Transfrontier movement" means any shipment of wastes destined for
    recovery operations from an area under the national jurisdiction
    of one OECD member country to an area under the national
    jurisdiction of another OECD member country.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.182
    General Conditions
    a)
    Scope. The level of control for exports and imports of waste is
    indicated by assignment of the waste to a green, amber, or red
    list and by U.S. national procedures, as defined in Section
    722.180(a). The green, amber, and red lists are incorporated by
    reference in Section 722.89 (e).
    1)
    Wastes on the green list are subject to existing controls
    normally applied to commercial transactions, except as
    provided below:
    A)
    Green-list wastes that are considered hazardous under
    U.S. national procedures are subject to amber
    -list
    controls.
    B)
    Green-list wastes that are sufficiently contaminated
    or mixed with amber
    -list wastes, such that the waste
    or waste mixture is considered hazardous under U.S.
    national procedures, are subject to amber
    -list
    controls.
    C)
    Green-list wastes that are sufficiently contaminated
    or mixed with other wastes subject to red
    -list
    controls, such that the waste or waste mixture is
    considered hazardous under U.S. national procedures,
    must be handled in accordance with the red
    -list
    controls.
    116
    2)
    Wastes on the amber list that are considered hazardous under
    U.S. national procedures, as defined in Section 722.180(a),
    are subject to the amber
    -list controls of th
    is Subpart. If
    amber-list wastes are sufficiently contaminated or mixed
    with other wastes subject to red
    -list controls, such that
    the waste or waste mixture is considered hazardous under
    U.S. national procedures, the wastes must be handled in
    accordance with the red
    -list controls.
    3)
    Wastes on the red list that are considered hazardous under
    U.S. national procedures, as defined in Section 722.180(a),
    are subject to the red
    -list controls of this Subpart.
    BOARD NOTE: Some wastes on the amber or red lists are not
    listed or otherwise identified as hazardous under RCRA
    (e.g., polychlorinated
    biphenyls) and therefore are not
    subject to the amber
    - or red -list controls of this Subpart.
    Regardless of the status of the waste under RCRA, however,
    other federal environmental statutes (e.g., the Toxic
    Substances Control Act) may restrict certain waste imports
    or exports. Such restrictions continue to apply without
    regard to this Subpart.
    4)
    Wastes not yet assigned to a list are eligible for
    transfrontier movements, as follows:
    A)
    If such wastes are considered hazardous under U.S.
    national procedures, as defined in Section 722.180(a),
    these wastes are subject to the red
    -list controls; or
    B)
    If such wastes are not considered hazardous under U.S.
    national procedures, as defined in Section 722.80(a),
    such wastes may move as though they appeared on the
    green list.
    b)
    General conditions applicable to
    transfrontier movements of
    hazardous waste.
    1)
    The waste must be destined for recovery operations at a
    facility that, under applicable domestic law, is operating
    or is authorized to operate in the importing country;
    2)
    The transfrontier movement must be in compliance with
    applicable international transport agreements; and
    BOARD NOTE: These international agreements include, but are
    not limited to, the Chicago Convention (1944), ADR (1957),
    ADNR (1970), MARPOL Convention (1973/1978), SOLAS Convention
    (1974), IMDG Code (1985), COTIF (1985), and RID (1985).
    3)
    Any transit of waste through a non
    -OECD me mber country must
    be conducted in compliance with all applicable international
    and national laws and regulations.
    c)
    Provisions relating to re
    -export for recovery to a third country.
    1)
    Re-export of wastes subject to the amber
    -list control system
    from the U.S., as the importing country, to a third country
    listed in Section 722.158(a)(1) may occur only after a
    notifier in the U.S. provides notification to and obtains
    consent of the competent authorities in the third country,
    117
    the original exporting country, and new transit countries.
    The notification must comply with the notice and consent
    procedures in Section 722.183 for all concerned countries
    and the original exporting country. The competent
    authorities of the original exporting country, as well as
    the competent authorities of all other concerned countries,
    have 30 days to object to the proposed movement.
    A)
    The 30 -day period begins once the competent
    authorities of both the initial exporting country and
    new importing country issue
    Acknowledgements of
    Receipt of the notification.
    B)
    The transfrontier movement may commence if no
    objection has been lodged after the 30
    -day period has
    passed or immediately after written consent is
    received from all relevant OECD importing and transit
    countries.
    2)
    Re-export of waste subject to the red
    -list control system
    from the original importing country to a third country
    listed in Section 722.158(a)(1) may occur only following
    notification of the competent authorities of the third
    country, the original exporting country, and new transit
    countries by a notifier in the original importing country in
    accordance with Section 722.183. The
    transfrontier movement
    may not proceed until receipt by the original importing
    country of written consent from the competent authorities of
    the third country, the original exporting country, and new
    transit countries.
    3)
    In the case of re
    -export of amber or red
    -list wastes to a
    country other than those in Section 722.158(a)(1),
    notification to and consent of the competent authorities of
    the original OECD member country of export and any OECD
    member countries of transit is required as specified in
    subsections (c)(1) and (c)(2) above in addition to
    compliance with all international agreements and
    arrangements to which the first importing OECD member
    country is a party and all applicable regulatory
    requirements for exports from the first importing country.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.183
    Notification and Consent
    a)
    Applicability. Consent must be obtained from the competent
    authorities of the relevant OECD importing and transit countries
    prior to exporting hazardous waste destined for recovery
    operations subject to this Subpart. Hazardous wastes subject to
    amber-list controls are subject to the requirements of subsection
    (b) below; hazardous wastes subject to red
    -list controls are
    subject to the requirements of subsection (c) below; and wastes
    not identified on any list are subject to the requirements of
    subsection (d) below.
    b)
    Amber-list wastes. The export from the U.S. of hazardous wastes,
    as described in Section 722.180(a), that appear on the amber list
    is prohibited unless the notification and consent requirements of
    subsection (b)(1) or subsection (b)(2) below are met.
    118
    1)
    Transactions requiring specific consent:
    A)
    Notification. At least 45 days prior to commencement
    of the transfrontier movement, the
    notifier must
    provide written notification in English of the
    proposed transfrontier movement to the Office of
    Enforcement and Compliance Assurance, Office of
    Compliance, Enforcement Planning, Targeting and Data
    Division (2222A), Environmental Protection Agency, 401
    M St., SW., Washington, DC 20460, and the Illinois
    Environmental Protection Agency, Bureau of Land,
    Division of Land Pollution Control,
    P.O. Box 19276,
    Springfield, IL 62794-9276, with the words "Attention:
    OECD Export Notification" prominently displayed on the
    envelope. This notification must include all of the
    information identified in subsection (e) below. In
    cases where wastes having similar physical and
    chemical characteristics, the same United Nations
    classification, and the same RCRA waste codes are to
    be sent periodically to the same recovery facility by
    the same notifier, the notifier may submit one
    notification of intent to export these wastes in
    multiple shipments during a period of up to one year.
    B)
    Tacit consent. If no objection has been lodged by any
    concerned country (i.e., exporting, importing, or
    transit countries) to a notification provided pursuant
    to subsection (b)(1)(A) above within 30 days after the
    date of issuance of the Acknowledgment of Receipt of
    notification by the competent authority of the
    importing country, the
    transfrontier movement may
    commence. Tacit consent expires one calendar year
    after the close of the 30 day period;
    renotification
    and renewal of all consents is required for exports
    after that date.
    C)
    Written consent. If the competent authorities of all
    the relevant OECD importing and transit countries
    provide written consent in a period less than 30 days,
    the transfrontier movement may commence immediately
    after all necessary consents are received. Written
    consent expires for each relevant OECD importing and
    transit country one calendar year after the date of
    that country's consent unless otherwise specified;
    renotification and renewal of each expired consent is
    required for exports after that date.
    2)
    Shipments to facilities pre
    -approved by the competent
    authorities of the importing countries to accept specific
    wastes for recovery:
    A)
    The notifier must provide USEPA and the Agency the
    information identified in subsection (e) below in
    English, at least 10 days in advance of commencing
    shipment to a pre
    -approved facility. The notification
    should indicate that the recovery facility is
    pre-approved, and may apply to a single specific
    shipment or to multiple shipments as described in
    subsection (b)(1)(A) above. This information must be
    sent to the Office of Enforcement and Compliance
    Assurance, Office of Compliance, Enforcement Planning,
    119
    Targeting and Data Division (2222A), Environmental
    Protection Agency, 401 M St., SW., Washington, DC
    20460, and the Illinois Environmental Protection
    Agency, Bureau of Land, Division of Land Pollution
    Control, P.O. Box 19276, Springfield, IL 62794-9276,
    with the words "OECD Export
    Notification --Pre-approved
    Facility" prominently displayed on the envelope.
    B)
    Shipments may commence after the notification required
    in subsection (b)(1)(A) above has been received by the
    competent authorities of all concerned countries,
    unless the notifier has received information
    indicating that the competent authorities of one or
    more concerned countries objects to the shipment.
    c)
    Red-list wastes. The export from the U.S. of hazardous wastes, as
    described in Section 722.180(a), that appear on the red list is
    prohibited unless notice is given pursuant to subsection (b)(1)(A)
    above and the notifier receives written consent from the importing
    country and any transit countries prior to commencement of the
    transfrontier movement.
    d)
    Unlisted wastes. Wastes not assigned to the green, amber, or red
    list that are considered hazardous under U.S. national procedures,
    as defined in Section 722.180(a), are subject to the notification
    and consent requirements established for red
    -list wastes in
    accordance with subsection (c) above. Unlisted wastes that are
    not considered hazardous under U.S. national procedures, as
    defined in Section 722.80(a), are not subject to amber or red
    controls when exported or imported.
    e)
    Notification information. Notifications submitted under this
    Section must include:
    1)
    Serial number or other accepted identifier of the
    notification form;
    2)
    Notifier name and EPA identification number (if applicable),
    address, and telephone and
    telefax numbers;
    3)
    Importing recovery facility name, address, telephone and
    telefax numbers, and technologies employed;
    4)
    Consignee name (if not the owner or operator of the recovery
    facility) address, and telephone and
    telefax numbers;
    whether the consignee will engage in waste exchange or
    storage prior to delivering the waste to the final recovery
    facility; and identification of recovery operations to be
    employed at the final recovery facility;
    5)
    Intended transporters or their agents;
    6)
    Country of export and relevant competent authority and point
    of departure;
    7)
    Countries of transit and relevant competent authorities and
    points of entry and departure;
    8)
    Country of import and relevant competent authority and point
    of entry;
    120
    9)
    Statement of whether the notification is a single
    notification or a general notification. If general, include
    period of validity requested;
    10)
    Date foreseen for commencement of
    transfrontier movement;
    11)
    Designation of waste type(s) from the appropriate list
    (amber or red and waste list code), descriptions of each
    waste type, estimated total quantity of each, RCRA waste
    code, and United Nations number for each waste type; and
    12)
    Certification/Declaration signed by the
    notifier that states
    as follows:
    "I certify that the above information is complete and
    correct to the best of my knowledge. I also certify that
    legally -enforceable written contractual obligations have
    been entered into, and that any applicable insurance or
    other financial guarantees are or shall be in force covering
    the transfrontier movement.
    Name:-------------------------------------------------------
    Signature: --------------------------------------------------
    Date:------------------------------------------------------"
    BOARD NOTE: The U.S. does not currently require financial
    assurance; however, U.S. exporters may be asked by other
    governments to provide and certify to such assurance as a
    condition of obtaining consent to a proposed movement.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.184
    Tracking Document
    a)
    All U.S. parties subject to the contract provisions of Section
    722.185 must ensure that a tracking document meeting the
    conditions of Section 722.184(b) accompanies each
    transfrontier
    shipment of wastes subject to amber
    -list or red -list controls from
    the initiation of the shipment until it reaches the final recovery
    facility, including cases in which the waste is stored or
    exchanged by the consignee prior to shipment to the final recovery
    facility, except as provided in Section 262.184(a)(1) and (a)(2).
    1)
    For shipments of hazardous waste within the U.S. solely by
    water (bulk shipments only), the generator must forward the
    tracking document with the manifest to the last water (bulk
    shipment) transporter to handle the waste in the U.S. if
    exported by water, (in accordance with the manifest routing
    procedures at Section 722.123(c)).
    2)
    For rail shipments of hazardous waste within the U.S. which
    originate at the site of generation, the generator must
    forward the tracking document with the manifest (in
    accordance with the routing procedures for the manifest in
    Section 722.123(d)) to the next non
    -rail transporter, if
    any, or the last rail transporter to handle the waste in the
    U.S. if exported by rail.
    b)
    The tracking document must include all information required under
    121
    Section 722.183 (for notification) and the following:
    1)
    The date shipment commenced;
    2)
    The name (if not
    notifier), address, and telephone and
    telefax numbers of primary exporter;
    3)
    The company name and USEPA identification number of all
    transporters;
    4)
    Identification (license, registered name or registration
    number) of means of transport, including types of packaging;
    5)
    Any special precautions to be taken by transporters;
    6)
    A certification or declaration signed by
    notifier that no
    objection to the shipment has been lodged as follows:
    "I certify that the above information is complete and
    correct to the best of my knowledge. I also certify that
    legally -enforceable written contractual obligations have
    been entered into, that any applicable insurance or other
    financial guarantees are or shall be in force covering the
    transfrontier movement, and that:"
    "1. All necessary consents have been received;" OR
    "2. The shipment is directed at a recovery facility within
    the OECD area and no objection has been received from any of
    the concerned countries within the 30 day tacit consent
    period;" OR
    "3. The shipment is directed at a recovery facility
    pre-authorized for that type of waste within the OECD area;
    such an authorization has not been revoked, and no objection
    has been received from any of the concerned countries."
    (delete sentences that are not applicable)
    "Name: ------------------------------------------------------
    Signature: --------------------------------------------------
    Date:-------------------------------------------------"; and
    7)
    The appropriate signatures for each custody transfer (e.g.
    transporter, consignee, and owner or operator of the
    recovery facility).
    c)
    Notifiers also must comply with the special manifest requirements
    of 35 Ill. Adm. Code 722.154(a), (b), (c), (e), and (i) and
    consignees must comply with the import requirements of 35 Ill.
    Adm. Code 722.Subpart F.
    d)
    Each U.S. person that has physical custody of the waste from the
    time the movement commences until it arrives at the recovery
    facility must sign the tracking document (e.g. transporter,
    consignee, and owner or operator of the recovery facility).
    e)
    Within 3 working days of the receipt of imports subject to this
    Subpart, the owner or operator of the U.S. recovery facility must
    122
    send signed copies of the tracking document to the
    notifier, to
    the Office of Enforcement and Compliance Assurance, Office of
    Compliance, Enforcement Planning, Targeting and Data Division
    (2222A), Environmental Protection Agency, 401 M St., SW.,
    Washington, DC 20460, and to the competent authorities of the
    exporting and transit countries.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.185
    Contracts
    a)
    Transfrontier movements of hazardous wastes subject to amber or
    red control procedures are prohibited unless they occur under the
    terms of a valid written contract, chain of contracts, or
    equivalent arrangements (when the movement occurs between parties
    controlled by the same corporate or legal entity). Such contracts
    or equivalent arrangements must be executed by the
    notifier and
    the owner or operator of the recovery facility, and must specify
    responsibilities for each. Contracts or equivalent arrangements
    are valid for the purposes of this Section only if persons
    assuming obligations under the contracts or equivalent
    arrangements have appropriate legal status to conduct the
    operations specified in the contract or equivalent arrangement.
    b)
    Contracts or equivalent arrangements must specify the following
    names and USEPA identification numbers, where available:
    1)
    The generator of each type of waste;
    2)
    Each person that will have physical custody of the wastes;
    3)
    Each person that will have legal control of the wastes; and
    4)
    The recovery facility.
    c)
    Contracts or equivalent arrangements must specify which party to
    the contract will assume responsibility for alternate management
    of the wastes if its disposition cannot be carried out as
    described in the notification of intent to export. In such cases,
    contracts must specify the following:
    1)
    That the person having actual possession or physical control
    over the wastes will immediately inform the
    notifier and the
    competent authorities of the exporting and importing
    countries and, if the wastes are located in a country of
    transit, the competent authorities of that country; and
    2)
    That the person specified in the contract will assume
    responsibility for the adequate management of the wastes in
    compliance with applicable laws and regulations including,
    if necessary, arranging their return to the original country
    of export.
    d)
    Contracts must specify that the consignee will provide the
    notification required in Section 722.182(c) prior to re
    -export of
    controlled wastes to a third country.
    e)
    Contracts or equivalent arrangements must include provisions for
    financial guarantees, if required by the competent authorities of
    any concerned country, in accordance with applicable national or
    international law requirements.
    123
    BOARD NOTE: Financial guarantees so required are intended to
    provide for alternative recycling, disposal, or other means of
    sound management of the wastes in cases where arrangements for the
    shipment and the recovery operations cannot be carried out as
    foreseen. The U.S. does not require such financial guarantees at
    this time; however, some OECD countries do. It is the
    responsibility of the
    notifier to ascertain and comply with such
    requirements; in some cases, transporters or consignees may refuse
    to enter into the necessary contracts absent specific references
    or certifications to financial guarantees.
    f)
    Contracts or equivalent arrangements must contain provisions
    requiring each contracting party to comply with all applicable
    requirements of this Subpart.
    g)
    Upon request by USEPA or the Agency, U.S.
    notifiers, consignees,
    or recovery facilities shall submit to USEPA and the Agency copies
    of contracts, chain of contracts, or equivalent arrangements (when
    the movement occurs between parties controlled by the same
    corporate or legal entity). Information contained in the
    contracts or equivalent arrangements for which a claim of
    confidentiality is asserted in accordance with 35 Ill. Adm. Code
    120 will be treated as confidential and will be disclosed by the
    Agency only as provided in 35 Ill. Adm. Code 120.
    BOARD NOTE: Although the U.S. does not require routine submission
    of contracts at this time, OECD Council Decision C(92)39/FINAL
    allows members to impose such requirements. When other OECD
    countries require submission of partial or complete copies of the
    contract as a condition to granting consent to proposed movements,
    USEPA or the Agency will request the required information; absent
    submission of such information, some OECD countries may deny
    consent for the proposed movement.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.186
    Provisions Relating to Recognized Traders
    a)
    A recognized trader that takes physical custody of a waste and
    conducts recovery operations (including storage prior to recovery)
    is acting as the owner or operator of a recovery facility and must
    be so authorized in accordance with all applicable federal laws.
    b)
    A recognized trader acting as a
    notifier or consignee for
    transfrontier shipments of waste must comply with all the
    notifier
    or consignee requirements of this Subpart.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.187
    Reporting and Recordkeeping
    a)
    Annual reports. For all waste movements subject to this Subpart,
    persons (e.g., notifiers, recognized traders) that meet the
    definition of primary exporter in Section 722.151 shall file an
    annual report with the Office of Enforcement and Compliance
    Assurance, Office of Compliance, Enforcement Planning, Targeting
    and Data Division (2222A), U.S. Environmental Protection Agency,
    401 M St., SW., Washington, DC 20460 and the Illinois
    Environmental Protection Agency, Bureau of Land, Division of Land
    Pollution Control,
    P.O. Box 19276, Springfield, IL 62706-9276, no
    124
    later than March 1 of each year summarizing the types, quantities,
    frequency, and ultimate destination of all such hazardous waste
    exported during the previous calendar year. (If the primary
    exporter is required to file an annual report for waste exports
    that are not covered under this Subpart, the person filing may
    include all export information in one report provided the
    following information on exports of waste destined for recovery
    within the designated OECD member countries is contained in a
    separate Section). Such reports shall include the following
    information:
    1)
    The USEPA identification number, name, and mailing and site
    address of the notifier filing the report;
    2)
    The calendar year covered by the report;
    3)
    The name and site address of each final recovery facility;
    4)
    By final recovery facility, for each hazardous waste
    exported, a description of the hazardous waste, the USEPA
    hazardous waste number (from 35 Ill. Adm. Code 721.Subpart C
    or 721.Subpart D), the designation of waste type(s) from the
    OECD waste list and applicable waste code from the OECD
    lists, DOT hazard class, the name and USEPA identification
    number (where applicable) for each transporter used, the
    total amount of hazardous waste shipped pursuant to this
    Subpart, and number of shipments pursuant to each
    notification;
    5)
    In even numbered years, for each hazardous waste exported,
    except for hazardous waste produced by exporters of greater
    than 100 kilograms (kg) but less than 1000 kg in a calendar
    month, and except for hazardous waste for which information
    was already provided pursuant to Section 722.141:
    A)
    A description of the efforts undertaken during the
    year to reduce the volume and toxicity of waste
    generated; and
    B)
    A description of the changes in volume and toxicity of
    the waste actually achieved during the year in
    comparison to previous years to the extent such
    information is available for years prior to 1984; and
    6)
    A certification signed by the person acting as primary
    exporter that states as follows:
    "I certify under penalty of law that I have personally
    examined and am familiar with the information submitted in
    this and all attached documents, and that based on my
    inquiry of those individuals immediately responsible for
    obtaining the information, I believe that the submitted
    information is true, accurate, and complete. I am aware that
    there are significant penalties for submitting false
    information including the possibility of fine and
    imprisonment."
    b)
    Exception reports. Any person that meets the definition of
    primary exporter in Section 722.151 shall file with USEPA and the
    Agency an exception report in lieu of the requirements of Section
    722.142 if any of the following occurs:
    125
    1)
    The person has not received a copy of the tracking
    documentation signed by the transporter stating point of
    departure of the waste from the United States within 45 days
    from the date it was accepted by the initial transporter;
    2)
    Within 90 days from the date the waste was accepted by the
    initial transporter, the
    notifier has not received written
    confirmation from the recovery facility that the hazardous
    waste was received; or
    3)
    The waste is returned to the United States.
    c)
    Recordkeeping.
    1)
    Persons that meet the definition of primary exporter in
    Section 722.151 shall keep the following records:
    A)
    A copy of each notification of intent to export and
    all written consents obtained from the competent
    authorities of concerned countries, for a period of at
    least three years from the date the hazardous waste
    was accepted by the initial transporter;
    B)
    A copy of each annual report, for a period of at least
    three years from the due date of the report; and
    C)
    A copy of any exception reports and a copy of each
    confirmation of delivery (i.e., tracking
    documentation) sent by the recovery facility to the
    notifier, for at least three years from the date the
    hazardous waste was accepted by the initial
    transporter or received by the recovery facility,
    whichever is applicable.
    2)
    The periods of retention referred to in this Section are
    extended automatically during the course of any unresolved
    enforcement action regarding the regulated activity or as
    requested by USEPA or the Agency.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    Section 722.189
    OECD Waste Lists
    a)
    General. For the purposes of this Subpart, a waste is considered
    hazardous under U.S. national procedures, and hence subject to
    this Subpart, if the waste:
    1)
    Meets the Federal definition of hazardous waste in 35 Ill.
    Adm. Code 721.103; and
    2)
    Is subject to either the hazardous waste manifesting
    requirements of 35 Ill. Adm. Code 722.Subpart B or the
    universal waste management standards of 35 Ill. Adm. Code
    733.
    b)
    If a waste is hazardous under subsection (a) above and it appears
    on the amber or red list, it is subject to either the amber
    - or
    red-list requirements, as appropriate;
    c)
    If a waste is hazardous under subsection (a) above and it does not
    126
    appear on either amber or red lists, it is subject to the red
    -list
    requirements.
    d)
    The appropriate control procedures for hazardous wastes and
    hazardous waste mixtures are addressed in Section 722.182.
    e)
    The OECD Green List of Wastes (revised May 1994), Amber List of
    Wastes (revised May 1993), and Red List of Wastes (revised May
    1993), as set forth in Appendix 3, Appendix 4 and Appendix 5,
    respectively, to the OECD Council Decision C(92)39/FINAL
    (Concerning the Control of Transfrontier Movements of Wastes
    Destined for Recovery Operations), incorporated by reference in 35
    Ill. Adm. Code 720.111.
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 723
    STANDARDS APPLICABLE TO
    TRANSPORTERS OF HAZARDOUS WASTE
    SUBPART A: GENERAL
    Section
    723.110 Scope
    723.111 USEPA Identification Number
    723.112 Transfer Facility Requirements
    SUBPART B: COMPLIANCE WITH THE MANIFEST SYSTEM
    AND RECORDKEEPING
    Section
    723.120 The Manifest System
    723.121 Compliance with the Manifest
    723.122 Recordkeeping
    SUBPART C: HAZARDOUS WASTE DISCHARGES
    Section
    723.130 Immediate Action
    723.131 Discharge Clean Up
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R81
    -22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
    1982; amended and codified in R81
    -22, 45 PCB 17, at 6 Ill. Reg. 4828,
    effective May 17, 1982; amended in R84
    -9, at 9 Ill. Reg. 11961, effective July
    24, 1985; amended in R86
    -19, at 10 Ill. Reg. 20718, effective December 2,
    1986; amended in R86
    -46 at 11 Ill. Reg. 13570, effective August 4, 1987;
    amended in R87 -5 at 11 Ill. Reg. 19412, effective November 12, 1987; amended
    in R95-6 at 19 Ill. Reg. 9945, effective June 27, 1995
    ; amended in R96-10/R97-
    3/R97-5 at 21 Ill. Reg. ________, effective ____________________
    .
    SUBPART A: GENERAL
    Section 723.110
    Scope
    127
    a)
    These regulations establish standards which apply to persons
    transporting hazardous waste into, out of or through Illinois if
    the transportation requires a manifest under
    Part35 Ill. Adm. Code
    722.
    b)
    These regulations do not apply to on
    -site transportation of
    hazardous waste by generators or by owners or operators of
    permitted hazardous waste management facilities.
    c)
    A transporter of hazardous waste must also comply with
    Part35 Ill.
    Adm. Code 722, "Standards Applicable to Generators of Hazardous
    Waste", if he:
    1)
    Transports hazardous waste into the United States from
    abroad; or
    2)
    Mixes hazardous waste of different DOT shipping descriptions
    by placing them into a single container.
    BOARD NOTE: Transporters
    whothat store hazardous waste are
    required to comply with the storage standards in
    Parts35
    Ill. Adm. Code 724 and 725 and the permit requirements of 40
    CFR Part 122.
    d) Part 700 contains rules concerning application of other Board
    regulations. A transporter of hazardous waste subject to the
    manifesting requirements of 35 Ill. Adm. Code 722 or the waste
    management standards of 35 Ill. Adm. Code 733 that is being
    imported from or exported to any of the countries listed in 35
    Ill. Adm. Code 722.158(a)(1) for purposes of recovery is subject
    to this Subpart and to all other relevant requirements of 35 Ill.
    Adm. Code 722.Subpart H, including, but not limited to, 35 Ill.
    Adm. Code 722.184 for tracking documents.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART B: COMPLIANCE WITH THE MANIFEST SYSTEM
    AND RECORDKEEPING
    Section 723.120
    The Manifest System
    a)
    No acceptance without a manifest.
    1)
    A transporter shall not accept hazardous waste from a
    generator unless it is accompanied by a manifest signed in
    accordance with the provisions of 35 Ill. Adm. Code 722
    .120.
    In the case of exports
    other than those subject
    subject to
    35 Ill. Adm. Code 722.Subpart H
    , a transporter shall not
    accept such waste from a primary exporter or other person:
    1
    A)
    If the transporter knows the shipment does not conform
    with the USEPA Acknowledgement of Consent (as defined
    in 35 Ill. Adm. Code 722.151); and
    2
    B)
    Unless, in addition to a manifest signed in accordance
    with 35 Ill. Adm. Code 722.120, the waste is also
    accompanied by a USEPA Acknowledgement of Consent
    which, except for shipment by rail, is attached to the
    manifest (or shipping paper for exports by water (bulk
    shipment)).
    128
    2)
    For exports of hazardous waste subject to the requirements
    of 35 Ill. Adm. Code 722.Subpart H, a transporter may not
    accept hazardous waste without a tracking document that
    includes all information required by 35 Ill. Adm. Code
    722.184.
    b)
    Before transporting the hazardous waste, the transporter shall
    sign and date the manifest acknowledging acceptance of the
    hazardous waste from the generator. The transporter shall return
    a signed copy to the generator before leaving the generator's
    property.
    c)
    The transporter shall ensure that the manifest accompanies the
    hazardous waste. In the case of exports, the transporter shall
    ensure that a copy of the USEPA Acknowledgement of Consent also
    accompanies the hazardous waste.
    d)
    A transporter whothat delivers a hazardous waste to another
    transporter or to the designated facility shall:
    1)
    Obtain the date of delivery and the handwritten signature of
    that transporter or of the owner or operator of the
    designated facility on the manifest; and
    2)
    Retain one copy of the manifest in accordance with Section
    723.122; and
    3)
    Give the remaining copies of the manifest to the accepting
    transporter or designated facility.
    e)
    The requirements of subsections (c), (d) and (f) do not apply to
    water (bulk shipment) transporters if:
    1)
    The hazardous waste is delivered by water (bulk shipment) to
    the designated facility; and
    2)
    A shipping paper containing all the information required on
    the manifest (excluding the USEPA identification numbers,
    generator certification and signatures) accompanies the
    hazardous waste and, for exports, a USEPA Acknowledgement of
    Consent accompanies the hazardous waste; and
    3)
    The delivering transporter obtains the date of delivery and
    handwritten signature of the owner or operator designated
    facility on either the manifest or the shipping paper; and
    4)
    The person delivering the hazardous waste to the initial
    water (bulk shipment) transporter obtains the date of
    delivery and signature of the water (bulk shipment)
    transporter on the manifest and forwards it to the
    designated facility; and
    5)
    A copy of the shipping paper or manifest is retained by each
    water (bulk shipment) transporter in accordance with Section
    723.122.
    f)
    For shipments involving rail transportation, the requirements of
    subsections (c), (d) and (e) do not apply and the following
    requirements do apply:
    129
    1)
    When accepting hazardous waste from a non-rail transporter,
    the initial rail transporter shall:
    A)
    Sign and date the manifest acknowledging acceptance of
    the hazardous waste;
    B)
    Return a signed copy of the manifest to the non-rail
    transporter;
    C)
    Forward at least three copies of the manifest to:
    i)
    The next non-rail transporter, if any; or,
    ii)
    The designated facility, if the shipment is
    delivered to that facility by rail; or
    iii)
    The last rail transporter designated to handle
    the waste in the United States;
    D)
    Retain one copy of the manifest and rail shipping
    paper in accordance with Section 723.122.
    2)
    Rail transporters shall ensure that a shipping paper
    containing all the information required on the manifest
    (excluding the USEPA identification numbers, generator
    certification and signatures) and, for exports, a USEPA
    Acknowledgement of Consent accompanies the hazardous waste
    at all times.
    (Board Note:Intermediate rail transporters are not required
    to sign either the manifest or shipping paper.)
    3)
    When delivering hazardous waste to the designated facility,
    a rail transporter shall:
    A)
    Obtain the date of delivery and handwritten signature
    of the owner or operator of the designated facility on
    the manifest or the shipping paper (if the manifest
    has not been received by the facility); and
    B)
    Retain a copy of the manifest or signed shipping paper
    in accordance with Section 723.122.
    4)
    When delivering hazardous waste to a non-rail transporter a
    rail transporter shall:
    A)
    Obtain the date of delivery and the handwritten
    signature of the next non-rail transporter on the
    manifest; and
    B)
    Retain a copy of the manifest in accordance with
    Section 723.122.
    5)
    Before accepting hazardous waste from a rail transporter, a
    non-rail transporter shall sign and date the manifest and
    provide a copy to the rail transporter.
    g)
    Transporters whothat transport hazardous waste out of the United
    States shall:
    1)
    Indicate on the manifest the date the hazardous waste left
    130
    the United States; and
    2)
    Sign the manifest and retain one copy in accordance with
    Section 723.122(c); and
    3)
    Return a signed copy of the manifest to the generator; and
    4)
    Give a copy of the manifest to a United States Customs
    official at the point of departure from the United States.
    h)
    A transporter transporting hazardous waste from a generator
    whothat generates greater than 100 kilograms but less than 1000
    kilograms of hazardous waste in a calendar month need not comply
    with the requirements of this Section or those of Section 723.122
    provided that:
    1)
    The waste is being transported pursu
    ant to a reclamation
    agreement provided for in 35 Ill. Adm. Code 722.120(e);
    2)
    The transporter records, on a log or shipping paper, the
    following information for each shipment:
    A)
    The name, address and USEPA Identification Number (35
    Ill. Adm. Code 722.112) of the generator of the waste;
    B)
    The quantity of waste accepted;
    C)
    All shipping information required by the United States
    Department of Transportation;
    D)
    The date the waste is accepted; and
    3)
    The transporter carries this record
    when transporting waste
    to the reclamation facility; and
    4)
    The transporter retains these records for a period of at
    least three years after termination or expiration of the
    agreement.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 724
    STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS WASTE
    TREATMENT, STORAGE,
    AND DISPOSAL FACILITIES
    SUBPART A: GENERAL PROVISIONS
    Section
    724.101
    Purpose, Scope and Applicability
    724.103
    Relationship to Interim Status Standards
    SUBPART B: GENERAL FACILITY STANDARDS
    Section
    724.110
    Applicability
    724.111
    Identification Number
    724.112
    Required Notices
    131
    724.113
    General Waste Analysis
    724.114
    Security
    724.115
    General Inspection Requirements
    724.116
    Personnel Training
    724.117
    General Requirements for Ignitable, Reactive or Incompatible
    Wastes
    724.118
    Location Standards
    724.119
    Construction Quality Assurance Program
    SUBPART C: PREPAREDNESS AND PREVENTION
    Section
    724.130
    Applicability
    724.131
    Design and Operation of Facility
    724.132
    Required Equipment
    724.133
    Testing and Maintenance of Equipment
    724.134
    Access to Communications or Alarm System
    724.135
    Required Aisle Space
    724.137
    Arrangements with Local Authorities
    SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
    Section
    724.150
    Applicability
    724.151
    Purpose and Implementation of Contingency Plan
    724.152
    Content of Contingenc
    y Plan
    724.153
    Copies of Contingency Plan
    724.154
    Amendment of Contingency Plan
    724.155
    Emergency Coordinator
    724.156
    Emergency Procedures
    SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
    Section
    724.170
    Applicability
    724.171
    Use of Manifest System
    724.172
    Manifest Discrepancies
    724.173
    Operating Record
    724.174
    Availability, Retention and Disposition of Records
    724.175
    Annual Report
    724.176
    Unmanifested Waste Report
    724.177
    Additional Reports
    SUBPART F: RELEASES FROM SOLID WASTE MANAGEMENT UNIT
    S
    Section
    724.190
    Applicability
    724.191
    Required Programs
    724.192
    Groundwater Protection Standard
    724.193
    Hazardous Constituents
    724.194
    Concentration Limits
    724.195
    Point of Compliance
    724.196
    Compliance Period
    724.197
    General Groundwater Monitoring Requirements
    724.198
    Detection Monitoring Program
    724.199
    Compliance Monitoring Program
    724.200
    Corrective Action Program
    724.201
    Corrective Action for Solid Waste Management Units
    SUBPART G: CLOSURE AND POST-CLOSURE
    Section
    724.210
    Applicability
    724.211
    Closure Performance Standard
    724.212
    Closure Plan; Amendment of Plan
    724.213
    Closure; Time Allowed For Closure
    132
    724.214
    Disposal or Decontamination of Equipment, Structures and Soils
    724.215
    Certification of Closure
    724.216
    Survey Plat
    724.217
    Post-closure Care and Use of Property
    724.218
    Post-closure Plan; Amendment of Plan
    724.219
    Post-closure Notices
    724.220
    Certification of Completion of Post-closure Care
    SUBPART H: FINANCIAL REQUIREMENTS
    Section
    724.240
    Applicability
    724.241
    Definitions of Terms As Used
    In This Subpart
    724.242
    Cost Estimate for Closure
    724.243
    Financial Assurance for Closure
    724.244
    Cost Estimate for Post-closure Care
    724.245
    Financial Assurance for Post-closure Care
    724.246
    Use of a Mechanism for Financial Assurance of Both Closure and
    Post-closure Care
    724.247
    Liability Requirements
    724.248
    Incapacity of Owners or Operators, Guarantors or Financial
    Institutions
    724.251
    Wording of the Instruments
    SUBPART I: USE AND MANAGEMENT OF CONTAINERS
    Section
    724.270
    Applicability
    724.271
    Conditi on of Containers
    724.272
    Compatibility of Waste With Container
    724.273
    Management of Containers
    724.274
    Inspections
    724.275
    Containment
    724.276
    Special Requirements for Ignitable or Reactive Waste
    724.277
    Special Requirements for Incompatible Wastes
    724.278
    Closure
    724.279
    Air Emission Standards
    SUBPART J: TANK SYSTEMS
    Section
    724.290
    Applicability
    724.291
    Assessment of Existing Tank System's Integrity
    724.292
    Design and Installation of New Tank Systems or Components
    724.293
    Containment and Detection of
    Releases
    724.294
    General Operating Requirements
    724.295
    Inspections
    724.296
    Response to Leaks or Spills and Disposition of Leaking or unfit-
    for-use Tank Systems
    724.297
    Closure and Post-Closure Care
    724.298
    Special Requirements for Ignitable or Reactive Waste
    724.299
    Special Requirements for Incompatible Wastes
    724.300
    Air Emission Standards
    SUBPART K: SURFACE IMPOUNDMENTS
    Section
    724.320
    Applicability
    724.321
    Design and Operating Requirements
    724.322
    Action Leakage Rate
    724.323
    Response Actions
    724.326
    Monitoring and Inspection
    724.327
    Emergency Repairs; Contingency Plans
    724.328
    Closure and Post-closure Care
    724.329
    Special Requirements for Ignitable or Reactive Waste
    133
    724.330
    Special Requirements for Incompatible Wastes
    724.331
    Special Requirements for Hazardous Wastes F020, F021, F022, F023,
    F026 and F027
    724.332
    Air Emission Standards
    SUBPART L: WASTE PILES
    Section
    724.350
    Applicability
    724.351
    Design and Operating Requirements
    724.352
    Action Leakage Rate
    724.353
    Response Action Plan
    724.354
    Monitor ing and Inspection
    724.356
    Special Requirements for Ignitable or Reactive Waste
    724.357
    Special Requirements for Incompatible Wastes
    724.358
    Closure and Post-closure Care
    724.359
    Special Requirements for Hazardous Wastes F020, F021, F022, F023,
    F026 and F027
    SUBPART M: LAND TREATMENT
    Section
    724.370
    Applicability
    724.371
    Treatment Program
    724.372
    Treatment Demonstration
    724.373
    Design and Operating Requirements
    724.376
    Food-chain Crops
    724.378
    Unsaturated Zone Monitoring
    724.379
    Recordkeeping
    724.380
    Closure and Post-closure Care
    724.381
    Special Requirements for Ignitable or Reactive Waste
    724.382
    Special Requirements for Incompatible Wastes
    724.383
    Special Requirements for Hazardous Wastes F020, F021, F022, F023,
    F026 and F027
    SUBPART N: LANDFILLS
    Section
    724.400
    Applicability
    724.401
    Design and Operating Requirements
    724.402
    Action Leakage Rate
    724.403
    Monitoring and Inspection
    724.404
    Response Actions
    724.409
    Surveying and Recordkeeping
    724.410
    Closure and Post-closure Care
    724.412
    Special Requiremen
    ts for Ignitable or Reactive Waste
    724.413
    Special Requirements for Incompatible Wastes
    724.414
    Special Requirements for Bulk and Containerized Liquids
    724.415
    Special Requirements for Containers
    724.416
    Disposal of Small Containers of Hazardous Waste in
    Overpacked
    Drums (Lab Packs)
    724.417
    Special Requirements for Hazardous Wastes F020, F021, F022, F023,
    F026 and F027
    SUBPART O: INCINERATORS
    Section
    724.440
    Applicability
    724.441
    Waste Analysis
    724.442
    Principal Organic Hazardous Constituents (POHCs)
    724.443
    Performance Standards
    724.444
    Hazardous Waste Incinerator Permits
    724.445
    Operating Requirements
    724.447
    Monitoring and Inspections
    724.451
    Closure
    134
    SUBPART S: CORRECTIVE ACTION FOR SOLID WASTE MANAGEMENT UNITS
    Section
    724.652
    Corrective Action Management Units
    724.653
    Temporary Units
    SUBPART W: DRIP PADS
    Section
    724.670
    Applicability
    724.671
    Assessment of existing drip pad integrity
    724.672
    Design and installation of new drip pads
    724.673
    Design and operating requirements
    724.674
    Inspections
    724.675
    Closure
    SUBPART X: MISCELLANEOUS UNITS
    Section
    724.700
    Applicability
    724.701
    Environmental Performance Standards
    724.702
    Monitoring, Analysis, Inspection, Response, Reporting and
    Corrective Action
    724.703
    Post-closure Care
    SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
    Section
    724.930
    Applicability
    724.931
    Definitions
    724.932
    Standards: Process Vents
    724.933
    Standards: Closed-vent Systems and Control Devices
    724.934
    Test methods and procedures
    724.935
    Recordkeeping requirements
    724.936
    Reporting Requirements
    SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
    Section
    724.950
    Applicability
    724.951
    Definitions
    724.952
    Standards: Pumps in Light Liquid Service
    724.953
    Standards: Compressors
    724.954
    Standards: Pressure Relief Devices in Gas/Vapor Service
    724.955
    Standards: Sampling Connecting Systems
    724.956
    Standards: Open-ended Valves or Lines
    724.957
    Standards: Valves in Gas/Vapor or Light Liquid Service
    724.958
    Standards: Pumps, Valves, Pressure Relief Devices and Other
    Connectors
    724.959
    Standards: Delay of Repair
    724.960
    Standards: Closed-vent Systems and Control Devices
    724.961
    Alternative Percentage Standard for Valves
    724.962
    Skip Period Alternative for Valves
    724.963
    Test Methods and Procedures
    724.964
    Recordkeeping Requirements
    724.965
    Reporting Requirements
    SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
    SURFACE IMPOUNDMENTS, AND CONTAINERS
    Section
    724.980
    Applicability
    724.981
    Definitions
    724.982
    Standards: General
    724.983
    Waste Determination Procedures
    724.984
    Standards: Tanks
    135
    724.985
    Standards: Surface
    Impoundments
    724.986
    Standards: Containers
    724.987
    Standards: Closed-vent Systems and Control Devices
    724.988
    Inspection and Monitoring Requirements
    724.989
    Recordkeeping Requirements
    724.990
    Reporting Requirements
    724.991
    Alternative Control Requirements for Tanks
    SUBPART DD: CONTAINMENT BUILDINGS
    Section
    724.1100
    Applicability
    724.1101
    Design and operating standards
    724.1102
    Closure and Post-closure Care
    724.Appendix A
    Recordkeeping Instructions
    724.Appendix B
    EPA Report Form and Instructions (Repealed)
    724.Appendix D
    Cochran's Approximation to the
    Behrens-Fisher Student's T-
    Test
    724.Appendix E
    Examples of Potentially Incompatible Waste
    724.Appendix I
    Groundwater Monitoring List
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14059, effective
    October 12, 1983; amended in R84-9 at 9 Ill. Reg. 11964, effective July 24,
    1985; amended in R85-22 at 10 Ill. Reg. 1136, effective January 2, 1986;
    amended in R86-1 at 10 Ill. Reg. 14119, effective August 12, 1986; amended in
    R86-28 at 11 Ill. Reg. 6138, effective March 24, 1987; amended in R86-28 at 11
    Ill. Reg. 8684, effective April 21, 1987; amended in R86-46 at 11 Ill. Reg.
    13577, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19397,
    effective November 12, 1987; amended in R87-39 at 12 Ill. Reg. 13135,
    effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 458, effective
    December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18527, effective November
    13, 1989; amended in R90-2 at 14 Ill. Reg. 14511, effective August 22, 1990;
    amended in R90-10 at 14 Ill. Reg. 16658, effective September 25, 1990; amended
    in R90-11 at 15 Ill. Reg. 9654, effective June 17, 1991; amended in R91-1 at
    15 Ill. Reg. 14572, effective October 1, 1991; amended in R91-13 at 16 Ill.
    Reg. 9833, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17702,
    effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5806, effective
    March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20830, effective November 22,
    1993; amended in R93-16 at 18 Ill. Reg. 6973, effective April 26, 1994;
    amended in R94-7 at 18 Ill. Reg. 12487, effective July 29, 1994; amended in
    R94-17 at 18 Ill. Reg. 17601, effective November 23, 1994; amended in R95-6 at
    19 Ill. Reg. 9951, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg.
    11244, August 1, 1996
    ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________,
    effective ____________________
    .
    SUBPART B: GENERAL FACILITY STANDARDS
    Section 724.112
    Required Notices
    a)
    Receipt from a foreign source.
    1)
    The owner or operator of a facility that has arranged to
    receive hazardous waste from a foreign source must notify
    the Regional Administrator in writing at least four weeks in
    advance of the date the waste is expected to arrive at the
    facility. Notice of subsequent shipments of the same waste
    136
    from the same foreign source is not required.
    2)
    The owner or operator of a recovery facility that has
    arranged to receive hazardous waste subject to 35 Ill. Adm.
    Code 722.Subpart H must provide a copy of the tracking
    document bearing all required signatures to the
    notifier, to
    the Office of Enforcement and Compliance Assurance, Office
    of Compliance, Enforcement Planning, Targeting and Data
    Division (2222A), Environmental Protection Agency, 401 M
    St., SW., Washington, DC 20460; to the Bureau of Land,
    Division of Land Pollution Control, Illinois Environmental
    Protection Agency,
    P.O. Box 19276, Springfield, IL 62794-
    9276; and to the competent authorities of all other
    concerned countries within three working days of receipt of
    the shipment. The original of the signed tracking document
    must be maintained at the facility for at least three years.
    b)
    The owner or operator of a facility that receives hazardous waste
    from an off -site source (except where the owner or operator is
    also the generator) must inform the generator in writing that the
    owner or operator has the appropriate permit(s) for, and will
    accept, the waste the generator is shipping. The owner or
    operator must keep a copy of this written notice as part of the
    operating record.
    c)
    Before transferring ownership or operation of a facility during
    its operating life, or of a disposal facility during the
    post-closure care period, the owner or operator must notify the
    new owner or operator in writing of the requirements of this Part
    and 35 Ill. Adm. Code 702 and 703.
    BOARD NOTE: An owner's or operator's failure to noti
    fy the new
    owner or operator of the requirements of this Part in no way
    relieves the new owner or operator of his obligation to comply
    with all applicable requirements.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.113
    General Waste Analysis
    a)
    Analysis:
    1)
    Before an owner or operator treats, stores, or disposes of
    any hazardous wastes, or non-hazardous wastes if applicable
    under Section 724.213(d), the owner or operator shall obtain
    a detailed chemical and physical analysis of a
    representative sample of the wastes. At a minimum, the
    analysis must contain all the information that must be known
    to treat, store, or dispose of the waste in accordance with
    this Part and 35 Ill. Adm. Code 728.
    2)
    The analysis may include data developed under 35 Ill. Adm.
    Code 721 and existing published or documented data on the
    hazardous waste or on hazardous waste generated from similar
    processes.
    BOARD NOTE: For example, the facility's records of analyses
    performed on the waste before the effective date of these
    regulations or studies conducted on hazardous waste
    generated from processes similar to that which generated the
    waste to be managed at the facility may be included in the
    137
    data base required to comply with subsection (a)(1) above.
    The owner or operator of an off-site facility may arrange
    for the generator of the hazardous waste to supply part or
    all of the information required by subsection (a)(1) above,
    except as otherwise specified in 35 Ill. Adm. Code
    728.107(b) and (c). If the generator does not supply the
    information, and the owner or operator chooses to accept a
    hazardous waste, the owner or operator is responsible for
    obtaining the information required to comply with this
    Section.
    3)
    The analysis must be repeated as necessary to ensure that it
    is accurate and up to date. At a minimum, the analysis must
    be repeated:
    A)
    When the owner or operator is notified, or has reason
    to believe, that the process or operation generating
    the hazardous waste, or non-hazardous waste if
    applicable under Section 724.213(d), has changed; and
    B)
    For off-site facilities, when the results of the
    inspection required in subsection (a)(4) below
    indicate that the hazardous waste received at the
    facility does not match the waste designated on the
    accompanying manifest or shipping paper.
    4)
    The owner or operator of an off-site facility shall inspect
    and, if necessary, analyze each hazardous waste shipment
    received at the facility to determine whether it matches the
    identity of the waste specified on the accompanying manifest
    or shipping paper.
    b)
    The owner or operator shall develop and follow a written waste
    analysis plan that describes the procedures that it will carry out
    to comply with subsection (a) above. The owner or operator shall
    keep this plan at the facility. At a minimum, the plan must
    specify:
    1)
    The parameters for which each hazardous waste, or non-
    hazardous waste if applicable under Section 724.213(d), will
    be analyzed and the rationale for the selection of these
    parameters (i.e., how analysis for these parameters will
    provide sufficient information on the waste's properties to
    comply with subsection (a) above).
    2)
    The test methods that will be used to test for these
    parameters.
    3)
    The sampling method that will be used to obtain a
    representative sample of the waste to be analyzed. A
    representative sample may be obtained using either:
    A)
    One of the sampling methods described in 35 Ill. Adm.
    Code 721.Appendix A; or
    B)
    An equivalent sampling met
    hod.
    BOARD NOTE: See 35 Ill. Adm. Code 720.121.
    4)
    The frequency with which the initial analysis of the waste
    will be reviewed or repeated to ensure that the analysis is
    138
    accurate and up to date.
    5)
    For off-site facilities, the waste analyses that hazardous
    waste generators have agreed to supply.
    6)
    Where applicable, the methods that will be used to meet the
    additional waste analysis requirements for specific waste
    management methods as specified in Sections 724.117,
    724.414, 724.441, 724.934(d), 724.963(d), and 724.983 and 35
    Ill. Adm. Code 728.107.
    7)
    For surface impoundments exempted from land disposal
    restrictions under 35 Ill. Adm. Code 728.104(a), the
    procedures and schedules for:
    A)
    The sampling of impoundment contents;
    B)
    The analysis of test data; and
    C)
    The annual removal of residues that are not
    delisted
    under 35 Ill. Adm. Code 720.122 or which exhibit a
    characteristic of hazardous waste and either:
    i)
    Do not meet applicable treatment standards of 35
    Ill. Adm. Code 728.Subpart D; or
    ii)
    Where no treatment standards have been
    established, such residues are prohibited from
    land disposal under 35 Ill. Adm. Code 728.132 or
    728.139 or such residues are prohibited from
    land disposal under 35 Ill. Adm. Code
    728.133(f).
    8)
    For owners and operators seeking an exemption to the air
    emission standards of 724.Subpart CC in accordance with
    Section 724.982:
    A) TIf direct measurement is used for the waste
    determination, t he procedures and schedules for waste
    sampling and analysis and the analysis of test data to
    verify the exemption
    , and.
    B) Each generator's notice and certification of the
    volatile organic concentration in the waste if the
    waste is received from off
    siteIf knowledge of the
    waste is used for the waste determination, any
    information prepared by the facility owner or operator
    or by the generator of the waste, if the waste is
    received form off-site, that is used as the basis for
    knowledge of the waste
    .
    c)
    For off-site facilities, the waste analysis plan r
    equired in
    subsection (b) above must also specify the procedures that will be
    used to inspect and, if necessary, analyze each shipment of
    hazardous waste received at the facility to ensure that it matches
    the identity of the waste designated on the accompanying manifest
    or shipping paper. At a minimum, the plan must describe:
    1)
    The procedures that will be used to determine the identity
    of each movement of waste managed at the facility;
    139
    2)
    The sampling method that will be used to obtain a
    representative sample of the waste to be identified, if the
    identification method includes sampling; and
    3)
    The procedures that the owner or operator of an off-site
    landfill receiving containerized hazardous waste will use to
    determine whether a hazardous waste generator or
    treater has
    added a biodegradable
    sorbent to the waste in the container.
    BOARD NOTE: 35 Ill. Adm. Code 703 requires that the waste
    analysis plan be submitted with Part B of the permit
    application.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
    Section 724.171
    Use of Manifest System
    a)
    If a facility receives hazardous waste accompanied by a manifest,
    the owner or operator, or the owner or operator's agent, must:
    1)
    Sign and date each copy of the manifest to certify that the
    hazardous waste covered by the manifest was received;
    2)
    Note any significant discrepancies in the manifest (as
    defined in Section 724.172(a)) on each copy of the manifest;
    BOARD NOTE: The Board does not intend that the owner or
    operator of a facility whose procedures under Section
    724.113(c) include waste analysis must perform that analysis
    before signing the manifest and giving it to the
    transporter. Section 724.172(b), however, requires
    reporting an unreconciled discrepancy discovered during
    later analysis.
    3)
    Immediately give the transporter at least one copy of the
    signed manifest;
    4)
    Within 30 days after the delivery, send a copy of the
    manifest to the generator and to the Agency; and
    5)
    Retain at the facility a copy of each manifest for at least
    three years from the date of delivery.
    b)
    If a facility receives, from a rail or water (bulk shipment)
    transporter, hazardous waste which is accompanied by a shipping
    paper containing all the information required on the manifest
    (excluding the EPA identification numbers, generator's
    certification, and signatures), the owner or operator, or the
    owner or operator's agent, must:
    1)
    Sign and date each copy of the ma
    nifest or shipping paper
    (if the manifest has not been received) to certify that the
    hazardous waste covered by the manifest or shipping paper
    was received;
    2)
    Note any significant discrepancies (as defined in Section
    724.172(a)) in the manifest or shipping paper (if the
    manifest has not been received) on each copy of the manifest
    140
    or shipping paper.
    BOARD NOTE: The Board does not intend that the owner or
    operator of a facility whose procedures under Section
    724.113(c) include waste analysis must perform that analysis
    before signing the shipping paper and giving it to the
    transporter. Section 724.172(b), however, requires reporting
    an unreconciled discrepancy discovered during later
    analysis.
    3)
    Immediately give the rail or water (bulk shipment)
    transporter at least one copy of the manifest or shipping
    paper (if the manifest has not been received);
    4)
    Within 30 days after the delivery, send a copy of the signed
    and dated manifest to the generator and to the Agency;
    however, if the manifest has not been received within 30
    days after delivery, the owner or operator, or the owner or
    operator's agent, must send a copy of the shipping paper
    signed and dated to the generator; and
    BOARD NOTE: Section 722.123(c) requires the generator to
    send three copies of the manifest to the facility when
    hazardous waste is sent by rail or water (bulk shipment).
    5)
    Retain at the facility a copy of the manifest and shipping
    paper (if signed in lieu of the manifest at the time of
    delivery) for at least three years from the date of
    delivery.
    c)
    Whenever a shipment of hazardous waste is initiated from a
    facility, the owner or operator of that facility must comply with
    the requirements of 35 Ill. Adm. Code 722.
    BOARD NOTE: The provisions of 35 Ill. Adm. Code 722.134 are
    applicable to the on
    -site accumulation of hazardous wastes by
    generators. Therefore, the provisions of Section 722.134 only
    apply to owners or operators
    whothat are shipping hazardous waste
    which they generated at that facility.
    d)
    Within three working days of the receipt of a shipment subject to
    35 Ill. Adm. Code 722.Subpart H, the owner or operator of the
    facility must provide a copy of the tracking document bearing all
    required signatures to the
    notifier; to the Office of Enforcement
    and Compliance Assurance, Office of Compliance, Enforcement
    Planning, Targeting and Data Division (2222A), Environmental
    Protection Agency, 401 M St., SW., Washington, DC 20460; to the
    Bureau of Land, Division of Land Pollution Control, Illinois
    Environmental Protection Agency,
    P.O. Box 19276, Springfield, IL
    62794-9276; and to competent authorities of all other concerned
    countries. The original copy of the tracking document must be
    maintained at the facility for at least three years from the date
    of signature.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART I: USE AND MANAGEMENT OF CONTAINERS
    Section 724.279
    Air Emission Standards
    141
    The owner or operator shall manage all hazardous waste placed in a container
    in accordance with the requirements of 724.Subpart
    s AA, BB, and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART J: TANK SYSTEMS
    Section 724.300
    Air Emission Standards
    The owner or operator shall manage all hazardous waste placed in a tank in
    accordance with the requirements of 724.Subpart
    s AA, BB, and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART K: SURFACE IMPOUNDMENTS
    Section 724.332
    Air Emission Standards
    The owner or operator shall manage all hazardous waste placed in a surface
    impoundment in accordance with the requirements of 724.Subpart
    s BB and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART N: LANDFILLS
    Section 724.414
    Special Requirements for Bulk and Containerized Liquids
    a)
    This subsection corresponds with 40 CFR 264.314(a), which pertains
    to pre May 8, 1985 actions, a date long since passed. This
    statement maintains structural consistency with U
    .S. EPA rules.
    b)
    The placement of bulk or non
    -containerized liquid hazardous waste
    or hazardous waste containing free liquids (whether or not
    sorbents have been added) in any landfill is prohibited.
    c)
    To demonstrate the absence or presence of free liquids in either a
    containerized or a bulk waste, the following test must be used:
    Method 9095 (Paint Filter Liquids Test) as described in "Test
    Methods for Evaluating Solid Wastes, Physical/Chemical Methods",
    U.S. EPA Publication No. SW
    -846, incorporated by reference in 35
    Ill. Adm. Code 720.111.
    d)
    Containers holding free liquids must not be placed in a landfill
    unless;
    1)
    All free -standing liquid:
    A)
    has been removed by decanting or other methods;
    B)
    has been mixed with
    sorbent or solidified so that
    free-standing liquid is no longer observed; or
    C)
    has been otherwise eliminated; or
    2)
    The container is very small, such as an
    ampule; or
    3)
    The container is designed to hold free liquids for use other
    than storage, such as a battery or capacitor; or
    142
    4)
    The container is a lab pack as defined in Section 724.416
    and is disposed of in accordance with Section 724.416.
    e)
    Sorbents used to treat free liquids to be disposed of in landfills
    must be nonbiodegradable.
    Nonbiodegradable
    sorbents are:
    materials listed or described in subsection (e)(1) below;
    materials that pass one of the tests in subsection (e)(2) below;
    or materials that are determined by the Board to be
    nonbiodegradable through the 35 Ill. Adm. Code 106 adjusted
    standard process.
    1)
    Nonbiodegradable
    sorbents are:
    A)
    Inorganic minerals, other inorganic materials, and
    elemental carbon (e.g.,
    aluminosilicates, clays,
    smectites, Fuller's earth,
    bentonite, calcium
    bentonite, montmorillonite,
    calcined montmorillonite,
    kaolinite, micas (
    illite), vermiculites, zeolites;
    calcium carbonate (organic free limestone);
    oxides/hydroxides,
    alumina, lime, silica (sand),
    diatomaceous earth;
    perlite (volcanic glass); expanded
    volcanic rock; volcanic ash; cement kiln dust; fly
    ash; rice hull ash; activated charcoal (activated
    carbon)); or
    B)
    High molecular weight synthetic polymers (e.g.,
    polyethylene, high density polyethylene (HDPE),
    polypropylene, polystrene, poly urethane, polycrylate,
    polynorborene, polyisobutylene, ground synthetic
    rubber, cross-linked
    allylstrene and tertiary butyl
    copolymers). This does not include polymers derived
    from biological material or polymers specifically
    designed to be degradable; or
    C)
    Mixtures of these
    nonbiodegradable materials.
    2)
    Tests for nonbiodegradable
    sorbents:
    A)
    The sorbent material is determined to be
    nonbiodegradable under ASTM Method G21-70 (1984a)
    --
    "Standard Practice for Determining Resistance of
    Synthetic Polymer Materials to Fungi", incorporated by
    reference in 35 Ill. Adm. Code 720.111;
    or
    B)
    The sorbent material is determined to be
    nonbiodegradable under ASTM Method G22-76 (1984b)
    --
    "Standard Practice for Determining Resistance of
    Plastics to Bacteria", incorporated by reference in 35
    Ill. Adm. Code 720.111
    .; or
    C)
    The sorbent material is determined to be non-
    biodegradable under OECD test 301B [CO
    2
    Evolution
    (Modified Sturm Test)], incorporated by reference in
    35 Ill. Adm. Code 720.111.
    f)
    The placement of any liquid that is not a hazardous waste in a
    landfill is prohibited (35 Ill. Adm. Code 729.311).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    143
    SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
    Section 724.930
    Applicability
    a)
    This Subpart applies to owners and operators of facilities that
    treat, store or dispose of hazardous wastes (except as provided in
    Section 724.101).
    b)
    Except for Sections 724.934(d) and (e), this Subpart applies to
    process vents associated with distillation, fractionation, thin-
    film evaporation, solvent extraction, or air or steam stripping
    operations that manage hazardous wastes with organic
    concentrations of at least 10
    ppmw (parts per million by weight),
    if these operations are conducted in:
    1)
    Units that are subject to the permitting requirements of 35
    Ill. Adm. Code 703;
    or
    2)
    A unit (including a
    hHazardous waste recycling unit
    s) that
    areis not exempt from permitting under the provisions of 35
    Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
    unit that is not a 90
    -day tank or container) and that is
    located onat a hazardous waste management
    facilit iesy
    otherwise subject to the permitting requirements of 35 Ill.
    Adm. Code 703 .; or
    3)
    A unit that is exempt from permitting under the provisions
    of 35 Ill. Adm. Code 722.134(a) (i.e., a 90
    -day tank or
    container).
    c)
    If the owner or operator of process vents subject to the
    requirements of Sections 724.932 through 724.936 has received a
    RCRA permit prior to December 21, 1990, the requirements of
    Sections 724.932 through 724.936 must be incorporated when the
    permit is reissued under 35 Ill. Adm. Code 705.201 or reviewed
    under 35 Ill. Adm. Code 702.161.
    BOARD NOTE: The requirements of Sections 724.932 through 724.936
    apply to process vents on hazardous waste recycling units
    previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
    exemptions under 35 Ill. Adm. Code 721.104, 722.134 and 724.101(g)
    are not affected by these requirements.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.933
    Standards: Closed-vent Systems and Control Devices
    a)
    Compliance Required.
    1)
    Owners or operators of closed-vent systems and control
    devices used to comply with provisions of this Part shall
    comply with the provisions of this Section.
    2)
    The owner or operator of an exist
    ing facility that cannot
    install a closed-vent system and control device to comply
    with the provisions of this Subpart on the effective date
    that the facility becomes subject to the provisions of this
    Subpart shall prepare an implementation schedule that
    includes dates by which the closed-vent system and control
    device will be installed and in operation. The controls
    144
    must be installed as soon as possible, but the
    implementation schedule may allow up to
    1830 months after
    the effective date that the facility becomes subject to this
    Subpart for installation and startup. All units that begin
    operation after December 21, 1990, must comply with the
    rules immediately (i.e., must have control devices installed
    and operating on startup of the affected unit); the 2-year
    implementation schedule does not apply to these units.
    b)
    A control device involving vapor recovery (e.g., a condenser or
    adsorber) must be designed and operated to recover the organic
    vapors vented to it with an efficiency of 95 weight percent or
    greater unless the total organic emission limits of Section
    724.932(a)(1) for all affected process vents is attained at an
    efficiency less than 95 weight percent.
    c)
    An enclosed combustion device (e.g., a vapor incinerator, boiler,
    or process heater) must be designed and operated to reduce the
    organic emissions vented to it by 95 weight percent or greater; to
    achieve a total organic compound concentration of 20
    ppmv,
    expressed as the sum of the actual compounds and not in carbon
    equivalents, on a dry basis, corrected to 3 percent oxygen; or to
    provide a minimum residence time of 0.50 seconds at a minimum
    temperature of 760
    ยฐ
    C. If a boiler or process heater is used as
    the control device, then the vent stream must be introduced into
    the flame zone of the boiler or process heater.
    d)
    Flares:
    1)
    A flare must be designed for and operated with no visible
    emissions, as determined by the methods specified in
    subsection (e)(1), except for periods not to exceed a total
    of 5 minutes during any 2 consecutive hours.
    2)
    A flare must be operated with a flame present at all times,
    as determined by the methods specified in subsection
    (f)(2)(C) below.
    3)
    A flare must be used only if the net heating value of the
    gas being combusted is 11.2 MJ/
    scm (300 Btu/ scf) or greater
    and the flare is steam-assisted or air-assisted or if the
    net heating value of the gas being combusted is 7.45 MJ/
    scm
    (200 Btu/ scf) or greater and the flare is
    nonassisted. The
    net heating value of the gas being combusted must be
    determined by the methods specified in subsection (e)(2)
    below.
    4)
    Exit Velocity.
    A)
    A steam-assisted or
    nonassisted flare must be designed
    for and operated with an exit velocity, as determined
    by the methods specified in subsection (e)(3) below,
    less than 18.3 m/s (60 ft/s), except as provided in
    subsections (d)(4)(B) and (d)(4)(C) below.
    B)
    A steam-assisted or
    nonassisted flare designed for and
    operated with an exit velocity, as determined by the
    methods specified in subsection (e)(3) below, equal to
    or greater than 18.3 m/s (60 ft/s) but less than 122
    m/s (400 ft/s) is allowed if the net heating value of
    the gas being combusted is greater than 37.3 MJ/
    scm
    145
    (1000 Btu/ scf).
    C)
    A steam-assisted or
    nonassisted flare designed for and
    operated with an exit velocity, as determined by the
    methods specified in subsection (e)(3) below, less
    than the velocity, V, as determined by the method
    specified in subsection (e)(4) below and less than 122
    m/s (400 ft/s) is allowed.
    5)
    An air-assisted flare must be designed and op
    erated with an
    exit velocity less than the velocity, V, as determined by
    the method specified in subsection (e)(5) below.
    6)
    A flare used to comply with this Section must be steam-
    assisted, air-assisted, or
    nonassisted.
    e)
    Compliance determination and equations.
    1)
    Reference Method 22 in 40 CFR 60, incorporated by reference
    in 35 Ill. Adm. Code 720.111, must be used to determine the
    compliance of a flare with the visible emission provisions
    of this Subpart. The observation period is 2 hours and must
    be used according to Method 22.
    2)
    The net heating value of the gas being combusted in a flare
    must be calculated using the following equation:
    Where:
    H
    T
    is the net heating value of the sample in MJ/
    scm;
    where the net enthalpy per mole of
    offgas is based on
    combustion at 25
    ยฐ
    C and 760 mm Hg, but the standard
    temperature for determining the volume
    corrersponding
    to 1 mole is 20
    ยฐ
    C.
    K = 1.74 E -7 (1/ppm)(g
    mol/scm)(MJ/kcal) where
    standard temperature for (g
    mol/scm) 20
    ยฐ
    C.
    ฮฃ
    (Xi) means the sum of the values of X for each
    component i, from i=1 to n.
    C
    i
    is the concentration of sample component i in
    ppm
    on a wet basis, as measured for
    organics by Reference
    Method 18 in 40 CFR 60, and for carbon monoxide, by
    ASTM D 1946-90, incorporated by reference in 35 Ill.
    Adm. Code 720.111.
    H
    i
    is the net heat of combustion of sample component
    i, kcal/ gmol at 25
    ยฐ
    C and 760 mm Hg. The heats of
    combustion must be determined using ASTM D 2382,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, if published values are not available or
    cannot be calculated.
    T
    i=1
    n
    i
    i
    H
    = K
    C
    H
    ร—
    ร—
    โˆ‘
    146
    3)
    The actual exit velocity of a flare must be determined by
    dividing the volumetric flow rate (in units of standard
    temperature and pressure), as determined by Reference
    Methods 2, 2A, 2C, or 2D in 40 CFR 60, incorporated by
    reference in 35 Ill. Adm. Code 720.111, as appropriate, by
    the unobstructed (free) cross-sectional area of the flare
    tip.
    4)
    The maximum allowed velocity in m/s
    , V for a flare complying
    with subsection (d)(4)(C) must be determined by the
    following equation:
    Where:
    log
    10
    means logarithm to the base 10
    H
    T
    is the net heating value as determined in
    subsection (e)(2).
    5)
    The maximum allowed velocity in m/s, V for an air-assisted
    flare must be determined by the following equation:
    Where:
    H
    T
    is the net heating value as determined in
    subsection (e)(2) below.
    f)
    The owner or operator shall mo
    nitor and inspect each control
    device required to comply with this Section to ensure proper
    operation and maintenance of the control device by implementing
    the following requirements:
    1)
    Install, calibrate, maintain, and operate according to the
    manufacturer's specifications a flow indicator that provides
    a record of stream flow from each affected process vent to
    the control device at least once every hour. The flow
    indicator sensor must be installed in the vent stream at the
    nearest feasible point to the control device inlet but
    before the point at which the vent streams are combined.
    2)
    Install, calibrate, maintain, and operate according to the
    manufacturer's specifications a device to continuously
    monitor control device operation as specified below:
    A)
    For a thermal vapor incinerator, a temperature
    monitoring device equipped with a continuous recorder.
    The device must have accuracy of ยฑ1 percent of the
    temperature being monitored in
    ยฐ
    C or ยฑ0.5
    ยฐ
    C,
    whichever is greater. The temperature sensor must be
    installed at a location in the combustion chamber
    downstream of the combustion zone.
    10
    T
    V
    =
    H
    + 28.8
    31.7
    log
    max
    147
    B)
    For a catalytic vapor incinerator, a temperature
    monitoring device equipped with a continuous recorder.
    The device must be capable of monitoring temperature
    at two locations and have an accuracy of ยฑ1 percent of
    the temperature being monitored in
    ยฐ
    C or ยฑ0.5
    ยฐ
    C,
    whichever is greater. One temperature sensor must be
    installed in the vent stream at the nearest feasible
    point to the catalyst bed inlet and a second
    temperature sensor must be installed in the vent
    stream at the nearest feasible point to the catalyst
    bed outlet.
    C)
    For a flare, a heat sensing monitoring device equipped
    with a continuous recorder that indicates the
    continuous ignition of the pilot flame.
    D)
    For a boiler or process heater having a design heat
    input capacity less than 44 MW, a temperature
    monitoring device equipped with a continuous recorder.
    The device must have an accuracy of ยฑ1 percent of the
    temperature being monitored in
    ยฐ
    C or ยฑ0.5
    ยฐ
    C,
    whichever is greater. The temperature sensor must be
    installed at a location in the furnace downstream of
    the combustion zone.
    E)
    For a boiler or process heater having a design heat
    input capacity greater than or equal to 44 MW, a
    monitoring device equipped with a continuous recorder
    to measure parameters that indicate good combustion
    operating practices are being used.
    F)
    For a condenser, either:
    i)
    A monitoring device equipped with a continuous
    recorder to measure the concentration level of
    the organic compounds in the exhaust vent stream
    from the condenser; or
    ii)
    A temperature monitoring device equipped with a
    continuous recorder. The device must be capable
    of monitoring temperature
    at two locations and
    havewith an accuracy of ยฑ1 percent of the
    temperature being monitored in
    ยฐ
    C or ยฑ0.5
    ยฐ
    C,
    whichever is greater.
    OneThe temperature sensor
    must be installed at a location in the exhaust
    vent stream from the condenser
    , and a second
    temperature sensor must be installed at a
    location in the coolant fluid
    exiting the
    condenser (i.e., product side)
    .
    G)
    For a carbon adsorption system that regenerates the
    carbon bed directly in the control device such as a
    fixed-bed carbon
    adsorber, either:
    i)
    A monitoring device equipped with a continuous
    recorder to measure the concentration level of
    the organic compounds in the exhaust vent stream
    from the carbon bed, or
    ii)
    A monitoring device equipped with a continuous
    148
    recorder to measure a parameter that indicates
    the carbon bed is regenerated on a regular,
    predetermined time cycle.
    3)
    Inspect the readings from each monitoring device required by
    subsection (f)(1) and (f)(2) at least once each operating
    day to check control device operation and, if necessary,
    immediately implement the corrective measures necessary to
    ensure the control device operates in compliance with the
    requirements of this Section.
    g)
    An owner or operator using a carbon adsorption system such as a
    fixed-bed carbon
    adsorber that regenerates the carbon bed directly
    onsite in the control device shall replace the existing carbon in
    the control device with fresh carbon at a regular, predetermined
    time interval that is no longer than the carbon service life
    established as a requirement of Section 724.935(b)(4)(C)(vi).
    h)
    An owner or operator using a carbon adsorption system such as a
    carbon canister that does not regenerate the carbon bed directly
    onsite in the control device shall replace the existing carbon in
    the control device with fresh carbon on a regular basis by using
    one of the following procedures:
    1)
    Monitor the concentration level of the organic compounds in
    the exhaust vent stream from the carbon adsorption system on
    a regular schedule, and replace the existing carbon with
    fresh carbon immediately when carbon breakthrough is
    indicated. The monitoring frequency must be daily or at an
    interval no greater than 20 percent of the time required to
    consume the total carbon working capacity established as a
    requirement of Section 724.935(b)(4)(C)(vii), whichever is
    longer.
    2)
    Replace the existing carbon with fresh carbon at a regular,
    predetermined time interval that is less than the design
    carbon replacement interval established as a requirement of
    Section 724.935(b)(4)(C)(vii).
    i)
    An alternative operational or process parameter may be monitored
    if the operator demonstrates that the parameter will ensure that
    the control device is operated in conformance with these standards
    and the control device's design specifications.
    j)
    An owner or operator o
    f an affected facility seeking to comply
    with the provisions of this Part by using a control device other
    than a thermal vapor incinerator, catalytic vapor incinerator,
    flare, boiler, process heater, condenser, or carbon adsorption
    system is required to develop documentation including sufficient
    information to describe the control device operation and identify
    the process parameter or parameters that indicate proper operation
    and maintenance of the control device.
    k) Closed vent systems. A closed vent system must meet either of the
    following design requirements:
    1) CA closed-vent system
    s must be designed
    for andto operate d
    with no detectable emissions, as indicated by an instrument
    reading of less than 500
    ppmv above background
    and by visual
    inspections , as determined by the methods specified at
    Section 724.934(b)
    ., and by visual inspections; or
    149
    2) Closed-vent systems must be monitored to determine
    compliance with this Section during the initial leak
    detection monitoring, which must be conducted by the date
    that the facility becomes subject to the provisions of this
    Section annually, and at other times as specified in the
    RCRA permit. For the annual leak detection monitoring after
    the initial leak detection monitoring, the owner or operator
    is not required to monitor those closed-vent system
    components that operate in vacuum service or those closed-
    vent system joints, seams, or other connections that are
    permanently or semi-permanently sealed (e.g., a welded joint
    between two sections of metal pipe or a bolted and
    gasketed
    pipe flange). A closed -vent system must be designed to
    operate at a pressure below atmospheric pressure. The
    system must be equipped with at least one pressure gauge or
    other pressure measurement device that can be read from a
    readily accessible location to verify that negative pressure
    is being maintained in the closed
    -vent system when the
    control device is operating.
    3) Detectable emissions, as indicated by an instrument reading
    greater than 500
    ppm and visual inspections, must be
    controlled as soon as practicable, but not later than 15
    calendar days after the emission is detected.
    4) A first attempt at repair must be made no later than 5
    calendar days after the emission is detected..
    l)
    The owner or operator shall monitor and inspect each closed-vent
    system required to comply with this Section to ensure proper
    operation and maintenance of the closed
    -vent system by
    implementing the following requirements:
    1)
    Each closed -vent system that is used to comply with
    subsection (k)(1) above shall be inspected and monitored in
    accordance with the following requirements:
    A)
    An initial leak detection monitoring of the
    closed -vent system shall be conducted by the owner or
    operator on or before the date that the system becomes
    subject to this Section. The owner or operator shall
    monitor the closed
    -vent system components and
    connections using the procedures specified in Section
    724.934(b) to demonstrate that the closed
    -vent system
    operates with no detectable emissions, as indicated by
    an instrument reading of less than 500
    ppmv above
    background.
    B)
    After initial leak detection monitoring required in
    subsection (l)(1)(A) above, the owner or operator
    shall inspect and monitor the closed
    -vent system as
    follows:
    i)
    Closed -vent system joints, seams, or other
    connections that are permanently or
    semi-permanently sealed (e.g., a welded joint
    between two sections of hard piping or a bolted
    and gasketed ducting flange) must be visually
    inspected at least once per year to check for
    defects that could result in air pollutant
    150
    emissions. The owner or operator shall monitor
    a component or connection using the procedures
    specified in Section 724.934(b) to demonstrate
    that it operates with no detectable emissions
    following any time the component is repaired or
    replaced (e.g., a Section of damaged hard piping
    is replaced with new hard piping) or the
    connection is unsealed (e.g., a flange is
    unbolted).
    ii)
    Closed -vent system components or connections
    other than those specified in subsection
    (l)(1)(B)(i) above must be monitored annually
    and at other times as requested by the Regional
    Administrator, except as provided for in
    subsection (o) below, using the procedures
    specified in Section 724.934(b) to demonstrate
    that the components or connections operate with
    no detectable emissions.
    C)
    In the event that a defect or leak is detected, the
    owner or operator shall repair the defect or leak in
    accordance with the requirements of subsection (l)(3)
    below.
    D)
    The owner or operator shall maintain a record of the
    inspection and monitoring in accordance with the
    requirements specified in Section 724.935.
    2)
    Each closed -vent system that is used to comply with
    subsection (k)(2) above must be inspected and monitored in
    accordance with the following requirements:
    A)
    The closed -vent system must be visually inspected by
    the owner or operator to check for defects that could
    result in air pollutant emissions. Defects include,
    but are not limited to, visible cracks, holes, or gaps
    in ductwork or piping or loose connections.
    B)
    The owner or operator shall perform an initial
    inspection of the closed
    -vent system on or before the
    date that the system becomes subject to this Section.
    Thereafter, the owner or operator shall perform the
    inspections at least once every year.
    C)
    In the event that a defect or leak is detected, the
    owner or operator shall repair the defect in
    accordance with the requirements of subsection (l)(3)
    below.
    D)
    The owner or operator shall maintain a record of the
    inspection and monitoring in accordance with the
    requirements specified in Section 724.935.
    3)
    The owner or operator shall repair all detected defects as
    follows:
    A)
    Detectable emissions, as indicated by visual
    inspection or by an instrument reading greater than
    500 ppmv above background, must be controlled as soon
    as practicable, but not later than 15 calendar days
    151
    after the emission is detected, except as provided for
    in subsection (l)(3)(C) below.
    B)
    A first attempt at repair must be made no later than
    five calendar days after the emission is detected.
    C)
    Delay of repair of a closed
    -vent system for which
    leaks have been detected is allowed if the repair is
    technically infeasible without a process unit
    shutdown, or if the owner or operator determines that
    emissions resulting from immediate repair would be
    greater than the fugitive emissions likely to result
    from delay of repair. Repair of such equipment must
    be completed by the end of the next process unit
    shutdown.
    D)
    The owner or operator shall maintain a record of the
    defect repair in accordance with the requirements
    specified in Section 724.935.
    lm) CA closed-vent system
    s andor control device s used to comply with
    provisions of this Subpart must be operated at all times when
    emissions may be vented to
    themit.
    mn)
    The owner or operator using a carbon adsorption system
    to control
    air pollutant emissions
    shall document that all carbon removed
    that is a hazardous waste and that is removed
    from a carbon
    adsorption system to comply with subsections (g) and (h)
    abovethe
    control device is managed in one of the following manners
    ,
    regardless of the volatile organic concentration of the carbon
    :
    1)
    It is regenerated or reactivated in a thermal treatment unit
    that is permitted under 724.Subpart
    X,meets one of the
    following:
    A)
    The owner or operator of the unit has been issued a
    final permit under 35 Ill. Adm. Code 702, 703, and 705
    that implements the requirements of 724.Subpart X; or
    B)
    The unit is equipped with and operating air emission
    controls in accordance with the applicable
    requirements of 724.Subparts AA and CC or 35 Ill. Adm.
    Code 725.Subparts AA and CC; or
    C)
    The unit is equipped with and operating air emission
    controls in accordance with a national emission
    standard for hazardous air pollutants under 40 CFR 61
    or 40 CFR 63.
    2)
    It is incinerated
    by a process that is permitted under
    724.Subpart O, orin a hazardous waste incinerator for which
    the owner or operator has done either of the following:
    A)
    The owner or operator has been issued a final permit
    under 35 Ill. Adm. Code 702, 703, and 705 that
    implements the requirements of 724.Subpart O, or
    B)
    The owner or operator has certified compliance in
    accordance with the interim status requirements of 35
    Ill. Adm. Code 725.Subpart O.
    152
    3)
    It is burned in a boiler or industrial furnace
    that is
    permitted under 724.Subpart
    H.for which the owner or
    operator has done either of the following:
    A)
    The owner or operator has been issued a final permit
    under 35 Ill. Adm. Code 702, 703, and 705 that
    implements the requirements of 35 Ill. Adm. Code
    726.Subpart H, or
    B)
    The owner or operator has designed and operates the
    boiler or industrial furnace in accordance with the
    interim status requirements of 35 Ill. Adm. Code
    726.Subpart H.
    o)
    Any components of a closed
    -vent system that are designated, as
    described in Section 724.935(c)(9), as unsafe to monitor are
    exempt from the requirements of subsection (l)(1)(B)(ii) above if
    both of the following conditions are fulfilled:
    1)
    The owner or operator of the closed
    -vent system has
    determined that the components of the closed
    -vent system are
    unsafe to monitor because monitoring personnel would be
    exposed to an immediate danger as a consequence of complying
    with subsection (l)(1)(B)(ii) above; and
    2)
    The owner or operator of the closed
    -vent system adheres to a
    written plan that requires monitoring the closed
    -vent system
    components using the procedure specified in subsection
    (l)(1)(B)(ii) as frequently as practicable during
    safe-to-monitor times.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.934
    Test methods and procedures
    a)
    Each owner or operator subject to the provisions of this Subpart
    shall comply with the test methods and procedures requirements
    provided in this Section
    b)
    When a closed-vent system is tested for compliance with no
    detectable emissions, as required in Section 724.933(
    kl), the test
    must comply with the following requirements:
    1)
    Monitoring must comply with Reference Metho
    d 21 in 40 CFR
    60, incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The detection instrument must meet the performance criteria
    of Reference Method 21.
    3)
    The instrument must be calibrated before use on each day of
    its use by the procedures specified in Reference Method 21.
    4)
    Calibration gases must be:
    A)
    Zero air (less than 10
    ppm of hydrocarbon in air).
    B)
    A mixture of methane or n-hexane and air at a
    concentration of approximately, but less than, 10,000
    ppm methane or n-hexane.
    5)
    The background level must be determined as set forth in
    153
    Reference Method 21.
    6)
    The instrument probe must be traversed around all potential
    leak interfaces as close to the interface as possible as
    described in Reference Method 21.
    7)
    The arithmetic difference between the maximum concentration
    indicated by the instrument and the background level is
    compared with 500
    ppm for determining compliance.
    c)
    Performance tests to determine compliance with Section 724.932(a)
    and with the total organic compound concentration limit of Section
    724.933(c) must comply with the following:
    1)
    Performance tests to determine total organic compound
    concentrations and mass flow rates entering and exiting
    control devices must be conducted and data reduced in
    accordance with the following reference methods and
    calculation procedures:
    A)
    Method 2 in 40 CFR 60 for velocity and volumetric flow
    rate.
    B)
    Method 18 in 40 CFR 60 for organic content.
    C)
    Each performance test must consist of three separate
    runs, each run conducted for at least 1 hour under the
    conditions that exist when the hazardous waste
    management unit is operating at the highest load or
    capacity level reasonably expected to occur. For the
    purpose of determining total organic compound
    concentrations and mass flow rates, the average of
    results of all runs applies. The average must be
    computed on a time-weighed basis.
    D)
    Total organic mass flow rates must be determined by
    the following equation:
    F = K * Q * SUM( Ci * MWi)
    Where:
    F is the total organic mass flow rate, kg/h.
    K = 4.16 E -8, conversion factor for molar
    volume, kg- mol/cubic m, at 293 K and 760 mm Hg.
    Q = volumetric flow rate of gases entering or
    exiting control device,
    dscm/h, as determined by
    Method 2 in 40 CFR 60, incorporated by reference
    in 35 Ill. Adm. Code 720.111.
    SUM(Xi) means the sum of the values of X for
    each component i, from i=1 to n.
    n = number of organic compounds in the vent gas.
    Ci is the organic concentration in
    ppm, dry
    basis, of compound i in the vent gas, as
    determined by Method 18 in 40 CFR 60.
    154
    MWi is the molecular weight of organic compound
    i in the vent gas, kg/kg-
    mol.
    Where:
    E
    h
    = The total organic mass flow rate, kg/h.
    Q
    2sd
    = The volumetric flow rate of gases entering
    or exiting control device,
    dscm/h, as
    determined by Method 2 in 40 CFR 60,
    incorporated by reference in 35 Ill. Adm.
    Code 720.111.
    n = The number of organic compounds in the vent
    gas.
    C
    i
    = The organic concentration in
    ppm, dry
    basis, of compound i in the vent gas, as
    determined by Method 18 in 40 CFR 60.
    MW
    i
    = The molecular weight of organic compound i
    in the vent gas, kg/kg-
    mol.
    0.0416 = The conversion factor for molar volume,
    kg-mol/m
    3
    , at 293 K and 760 mm Hg.
    10
    -6
    = The conversion factor from
    ppm.
    E)
    The annual total organic emission rate must be
    determined by the following equation:
    A = F *
    ร—
    HOURS
    Where:
    A is total organic e
    mission rate, kg/y.
    F is the total organic mass flow rate, kg/h, as
    calculated in subsection (c)(1)(D)
    above .
    HOURS is the total annual hours of operation for
    the affected unit.
    F)
    Total organic emissions from all affected process
    vents at the facility must be determined by summing
    the hourly total organic mass emissions rates (F as
    determined in subsection (c)(1)(D)
    above ) and by
    summing the annual total organic mass emission rates
    (A as determined in subsection (c)(1)(E)
    above ) for
    all affected process vents at the facility.
    2)
    The owner or operator shall record such process information
    h
    2sd
    i
    i
    -6
    E
    = Q
    x(
    n
    i = 1
    C
    x MW
    )x0.0416x10
    โˆ‘
    155
    as is necessary to determine the conditions of the
    performance tests. Operations during periods of startup,
    shutdown and malfunction do not constitute representative
    conditions for the purpose of a performance test.
    3)
    The owner or operator of an affected facility shall provide,
    or cause to be provided, performance testing facilities as
    follows:
    A)
    Sampling ports adequate for the test methods speci
    fied
    in subsection (c)(1)
    above .
    B)
    Safe sampling platform(s).
    C)
    Safe access to sampling platform(s).
    D)
    Utilities for sampling and testing equipment.
    4)
    For the purpose of making compliance determinations, the
    time-weighted average of the results of the three runs must
    apply. In the event that a sample is accidentally lost or
    conditions occur in which one of the three runs must be
    discontinued because of forced shutdown, failure of an
    irreplaceable portion of the sample train, extreme
    meteorological conditions or other circumstances beyond the
    owner or operator's control, compliance may, upon the
    Agency's approval, be determined using the average of the
    results of the two other runs.
    d)
    To show that a process vent associated with a hazardous waste
    distillation, fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation is not subject to
    the requirements of this Subpart, the owner or operator shall make
    an initial determination that the time-weighted, annual average
    total organic concentration of the waste managed by the waste
    management unit is less than 10
    ppmw using one of the following
    two methods:
    1)
    Direct measurement of the organic concentration of the waste
    using the following procedures:
    A)
    The owner or operator shall take a minimum of four
    grab samples of waste for each wastestream managed in
    the affected unit under process conditions expected to
    cause the maximum waste organic concentration.
    B)
    For waste generated onsite, the grab sampl
    es must be
    collected at a point before the waste is exposed to
    the atmosphere such as in an enclosed pipe or other
    closed system that is used to transfer the waste after
    generation to the first affected distillation,
    fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation. For
    waste generated offsite, the grab samples must be
    collected at the inlet to the first waste management
    unit that receives the waste provided the waste has
    been transferred to the facility in a closed system
    such as a tank truck and the waste is not diluted or
    mixed with other waste.
    C)
    Each sample must be analyzed and the total organic
    156
    concentration of the sample must be computed using
    Method 9060 or 8240 of SW-846
    , (incorporated by
    reference under 35 Ill. Adm. Code 720.111.
    D)
    The arithmetic mean of the results of the analyses of
    the four samples apply for each wastestream managed in
    the unit in determining the time-weighted, annual
    average total organic concentration of the waste. The
    time-weighted average is to be calculated using the
    annual quantity of each waste stream processed and the
    mean organic concentration of each wastestream managed
    in the unit.
    2)
    Using knowledge of the waste to determine that its total
    organic concentration is less than 10
    ppmw. Documentation
    of the waste determination is required. Examples of
    documentation that must be used to support a determination
    under this subsection include:
    A)
    Production process information documenting that no
    organic compounds are used.
    B)
    Information that the waste is generated by a process
    that is identical to a process at the same or another
    facility that has previously been demonstrated by
    direct measurement to generate a wastestream having a
    total organic content less than 10
    ppmw, or
    C)
    Prior speciation analysis results on the same
    wastestream where it is also documented that no
    process changes have occurred since that analysis that
    could affect the waste total organic concentration.
    e)
    The determination that di
    stillation, fractionation, thin-film
    evaporation, solvent extraction, or air or steam stripping
    operations which manage hazardous wastes with time-weighted,
    annual average total organic concentrations less than 10
    ppmw must
    be made as follows:
    1)
    By the effective date that the facility becomes subject to
    the provisions of this Subpart or by the date when the waste
    is first managed in a waste management unit, whichever is
    later; and
    2)
    For continuously generated waste, annually; or
    3)
    Whenever there is a change in the waste being managed or a
    change in the process that generates or treats the waste.
    f)
    When an owner or operator and the Agency do not agree on whether a
    distillation, fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation manages a
    hazardous waste with organic concentrations of at least 10
    ppmw
    based on knowledge of the waste, the procedures in Method 8240 in
    SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111,
    must be used to resolve the dispute.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.935
    Recordkeeping requirements
    157
    a)
    Compliance Required.
    1)
    Each owner or operator subject to the provisions of this
    Subpart shall comply with the
    recordkeeping requirements of
    this Section.
    2)
    An owner or operator of more than one hazardous waste
    management unit subject to the provisions of this Subpart
    may comply with the
    recordkeeping requirements for these
    hazardous waste management units in one
    recordkeeping system
    if the system identifies each record by each hazardous waste
    management unit.
    b)
    Owners and operators shall record the following information in the
    facility operating record:
    1)
    For facilities that comply with the provisions of Section
    724.933(a)(2), an implementation schedule that includes
    dates by which the closed-vent system and control device
    will be installed and in operation. The schedule must also
    include a rationale of why the installation cannot be
    completed at an earlier date. The implementation schedule
    must be in the facility operating record by the effective
    date that the facility becomes subject to the provisions of
    this Subpart.
    2)
    Up-to-date documentation of compliance with the process vent
    standards in Section 724.932, including:
    A)
    Information and data identifying all affected process
    vents, annual throughput and operating hours of each
    affected unit, estimated emission rates for each
    affected vent and for the overall facility (i.e., the
    total emissions for all affected vents at the
    facility), and the approximate location within the
    facility of each affected unit (e.g., identify the
    hazardous waste management units on a facility plot
    plan).
    B)
    Information and data supporting determination of vent
    emissions and emission reductions achieved by add-on
    control devices based on engineering calculations or
    source tests. For the purpose of determining
    compliance, determinations of vent emissions and
    emission reductions must be made using operating
    parameter values (e.g., temperatures, flow rates, or
    vent stream organic compounds and concentrations) that
    represent the conditions that result in maximum
    organic emissions, such as when the waste management
    unit is operating at the highest load or capacity
    level reasonably expected to occur. If the owner or
    operator takes any action (e.g., managing a waste of
    different composition or increasing operating hours of
    affected waste management units) that would result in
    an increase in total organic emissions from affected
    process vents at the facility, then a new
    determination is required.
    3)
    Where an owner or operator chooses to use test data to
    determine the organic removal efficiency or total organic
    compound concentration achieved by the control device, a
    158
    performance test plan. The test plan must include:
    A)
    A description of how it is determined that the planned
    test is going to be conducted when the hazardous waste
    management unit is operating at the highest load or
    capacity level reasonably expected to occur. This
    must include the estimated or design flow rate and
    organic content of each vent stream and define the
    acceptable operating ranges of key process and control
    device parameters during the test program.
    B)
    A detailed engineering description of the closed-vent
    system and control device including:
    i)
    Manufacturer's name and model number of control
    device.
    ii)
    Type of control device.
    iii)
    Dimensions of the control device.
    iv)
    Capacity.
    v)
    Construction materials.
    C)
    A detailed description of sampling and monitoring
    procedures, including sampling and monitoring
    locations in the system, the equipment to be used,
    sampling and monitoring frequency, and planned
    analytical procedures for sample analysis.
    4)
    Documentation of compliance with Section 724.933 must
    include the following information:
    A)
    A list of all information references and sources used
    in preparing the documentation.
    B)
    Records including the dates of each compliance test
    required by Section 724.933(k).
    C)
    If engineering calculations are used, a design
    analysis, specifications, drawings, schematics, and
    piping and instrumentation diagrams based on the
    appropriate sections of APTI Course 415 (incorporated
    by reference in 35 Ill. Adm. Code 720.111) or other
    engineering texts, approved by the Agency, that
    present basic control device design information.
    Documentation provided by the control device
    manufacturer or vendor that describes the control
    device design in accordance with subsections
    (b)(4)(C)(i) through (vii)
    , below , may be used to
    comply with this requirement. The design analysis
    must address the vent stream characteristics and
    control device operation parameters as specified
    below.
    i)
    For a thermal vapor incinerator, the design
    analysis must consider the vent stream
    composition, constituent concentrations and flow
    rate. The design analysis must also establish
    the design minimum and average temperature in
    159
    the combustion zone and the combustion zone
    residence time.
    ii)
    For a catalytic va
    por incinerator, the design
    analysis must consider the vent stream
    composition, constituent concentrations, and
    flow rate. The design analysis must also
    establish the design minimum and average
    temperatures across the catalyst bed inlet and
    outlet.
    iii)
    For a boiler or process heater, the design
    analysis must consider the vent stream
    composition, constituent concentrations and flow
    rate. The design analysis must also establish
    the design minimum and average flame zone
    temperatures, combustion zone residence time and
    description of method and location where the
    vent stream is introduced into the combustion
    zone.
    iv)
    For a flare, the design analysis must consider
    the vent stream composition, constituent
    concentrations, and flow rate. The design
    analysis must also consider the requirements
    specified in Section 724.933(d).
    v)
    For a condenser, the design analysis must
    consider the vent stream composition,
    constituent concentrations, flow rate, relative
    humidity and temperature. The design analysis
    must also establish the design outlet organic
    compound concentration level, design average
    temperature of the condenser exhaust vent stream
    and design average temperatures of the coolant
    fluid at the condenser inlet and outlet.
    vi)
    For a carbon adsorption system such as a fixed-
    bed adsorber that regenerates the carbon bed
    directly onsite in the control device, the
    design analysis must consider the vent stream
    composition, constituent concentrations, flow
    rate, relative humidity and temperature. The
    design analysis must also establish the design
    exhaust vent stream organic compound
    concentration level, number and capacity of
    carbon beds, type and working capacity of
    activated carbon used for carbon beds, design
    total steam flow over the period of each
    complete carbon bed regeneration cycle, duration
    of the carbon bed steaming and cooling/drying
    cycles, design carbon bed temperature after
    regeneration, design carbon bed regeneration
    time and design service life of carbon.
    vii)
    For a carbon adsorpt
    ion system such as a carbon
    canister that does not regenerate the carbon bed
    directly onsite in the control device, the
    design analysis must consider the vent stream
    composition, constituent concentrations, flow
    rate, relative humidity and temperature. The
    160
    design analysis must also establish the design
    outlet organic concentration level, capacity of
    carbon bed, type and working capacity of
    activated carbon used for carbon bed and design
    carbon replacement interval based on the total
    carbon working capacity of the control device
    and source operating schedule.
    D)
    A statement signed and dated by the owner or operator
    certifying that the operating parameters used in the
    design analysis reasonably represent the conditions
    that exist when the hazardous waste management unit is
    or would be operating at the highest load or capacity
    level reasonably expected to occur.
    E)
    A statement signed and dated by the owner or operator
    certifying that the control device is designed to
    operate at an efficiency of 95 percent or greater
    unless the total organic concentration limit of
    Section 724.932(a) is achieved at an efficiency less
    than 95 weight percent or the total organic emission
    limits of Section 724.932(a) for affected process
    vents at the facility are attained by a control device
    involving vapor recovery at an efficiency less than 95
    weight percent. A statement provided by the control
    device manufacturer or vendor certifying that the
    control equipment meets the design specifications may
    be used to comply with this requirement.
    F)
    If performance tests are used to demonstrate
    compliance, all test results.
    c)
    Design documentation and monitoring operating and inspection
    information for each closed-vent system and control device
    required to comply with the provisions of this Part must be
    recorded and kept up-to-date in the facility operating record.
    The information must include:
    1)
    Description and date of each modification that is made to
    the closed-vent system or control device design.
    2)
    Identification of
    operating parameter, description of
    monitoring device, and diagram of monitoring sensor location
    or locations used to comply with Section 724.933(f)(1) and
    (2).
    3)
    Monitoring, operating and inspection information required by
    Section 724.933(f) through (k).
    4)
    Date, time and duration of each period that occurs while the
    control device is operating when any monitored parameter
    exceeds the value established in the control device design
    analysis as specified below:
    A)
    For a thermal vapor incinerator d
    esigned to operate
    with a minimum residence time of 0.50 second at a
    minimum temperature of 760 C, any period when the
    combustion temperature is below 760 C.
    B)
    For a thermal vapor incinerator designed to operate
    with an organic emission reduction efficiency of 95
    161
    weight percent or greater, any period when the
    combustion zone temperature is more than 28 C below
    the design average combustion zone temperature
    established as a requirement of subsection
    (b)(4)(C)(i) , above.
    C)
    For a catalytic vapor inci
    nerator, any period when:
    i)
    Temperature of the vent stream at the catalyst
    bed inlet is more than 28 C below the average
    temperature of the inlet vent stream established
    as a requirement of subsection (b)(4)(C)(ii)
    ,
    above; or
    ii)
    Temperature difference across the catalyst bed
    is less than 80 percent of the design average
    temperature difference established as a
    requirement of subsection (b)(4)(C)(ii)
    , above.
    D)
    For a boiler or process heater, any period when:
    i)
    Flame zone temperature is
    more than 28 C below
    the design average flame zone temperature
    established as a requirement of subsection
    (b)(4)(C)(iii) , above; or
    ii)
    Position changes where the vent stream is
    introduced to the combustion zone from the
    location established as a requirement of
    subsection (b)(4)(C)(iii)
    , above.
    E)
    For a flare, period when the pilot flame is not
    ignited.
    F)
    For a condenser that complies with Section
    724.933(f)(2)(F)(i), any period when the organic
    compound concentration level or readings of organic
    compounds in the exhaust vent stream from the
    condenser are more than 20 percent greater than the
    design outlet organic compound concentration level
    established as a requirement of subsection
    (b)(4)(C)(v) , above.
    G)
    For a condenser that complies with Section
    724.933(f)(2)(F)(ii), any period when:
    i)
    Temperature of the exhaust vent stream from the
    condenser is more than 6 C above the design
    average exhaust vent stream temperature
    established as a requirement of subsection
    (b)(4)(C)(v) , above.
    ii)
    Temperature of the coolant fluid exiting the
    condenser is more than 6 C above the design
    average coolant fluid temperature at the
    condenser outlet established as a requirement of
    subsection (b)(4)(C)(v)
    , above.
    H)
    For a carbon adsorption system such as a fixed-bed
    carbon adsorber that regenerates the carbon bed
    directly onsite in the control device and complies
    162
    with Section 724.933(f)(2)(G)(i), any period when the
    organic compound concentration level or readings of
    organic compounds in the exhaust vent stream from the
    carbon bed are more than 20 percent greater than the
    design exhaust vent stream organic compound
    concentration level established as a requirement of
    subsection (b)(4)(C)(vi)
    , above.
    I)
    For a carbon adsorption system such as a fixed-bed
    carbon adsorber that regenerates the carbon bed
    directly onsite in the control device and complies
    with Section 724.933(f)(2)(G)(ii), any period when the
    vent stream continues to flow through the control
    device beyond the predetermined carbon bed
    regeneration time established as a requirement of
    subsection (b)(4)(C)(vi)
    , above.
    5)
    Explanation for each period recorded under subsection
    (c)(4) , above, of the cause for control device operating
    parameter exceeding the design value and the measures
    implemented to correct the control device operation.
    6)
    For a carbon adsorption system operated subject to
    requirements specified in Section 724.933(g) or (h)(2), any
    date when existing carbon in the control device is replaced
    with fresh carbon.
    7)
    For a carbon adsorption system operated subject to
    requirements specified in Section 724.933(h)(1), a log that
    records:
    A)
    Date and time when control device is monitored for
    carbon breakthrough and the monitoring device reading.
    B)
    Date when existing carbon in the control device is
    replaced with fresh carbon.
    8)
    Date of each control device startup and shutdown.
    9)
    An owner or operator designating any components of a closed-
    vent system as unsafe to monitor pursuant to Section
    724.933(o) shall record in a log that is kept in the
    facility operating record the identification of closed
    -vent
    system components that are designated as unsafe to monitor
    in accordance with the requirements of Section 724.933(o),
    an explanation for each closed
    -vent system component stating
    why the closed -vent system component is unsafe to monitor,
    and the plan for monitoring each closed
    -vent system
    component.
    10)
    When each leak is detected as specified in Section
    724.933(l), the following information must be recorded:
    A)
    The instrument identification number, the closed
    -vent
    system component identification number, and the
    operator name, initials, or identification number.
    B)
    The date the leak was detected and the date of first
    attempt to repair the leak.
    C)
    The date of successful repair of the leak.
    163
    D)
    Maximum instrument reading measured by Method 21 of 40
    CFR 60, appendix A, incorporated by reference in 35
    Ill. Adm. Code 720.111, after it is successfully
    repaired or determined to be
    nonrepairable.
    E)
    "Repair delayed" and the reason for the delay if a
    leak is not repaired within 15 calendar days after
    discovery of the leak.
    i)
    The owner or operator may develop a written
    procedure that identifies the conditions that
    justify a delay of repair. In such cases,
    reasons for delay of repair may be documented by
    citing the relevant sections of the written
    procedure.
    ii)
    If delay of repair was caused by depletion of
    stocked parts, there must be documentation that
    the spare parts were sufficiently stocked
    on-site before depletion and the reason for
    depletion.
    d)
    Records of the monitoring, operating
    , and inspection information
    required by subsections (c)(3) through
    (c)(810), above, needmust
    be kept onlyat least 3 years following the date of each
    occurrence, measurement, corrective action, or record
    .
    e)
    For a control device other than a thermal vapor incinerator,
    catalytic vapor incinerator, flare, boiler, process heater,
    condenser or carbon adsorption system, the Agency shall specify
    the appropriate recordkeeping requirements.
    f)
    Up-to-date information and data used to determine whether or not a
    process vent is subject to the requirements in Section 724.932,
    including supporting documentation as required by Section
    724.934(d)(2), when application of the knowledge of the nature of
    the hazardous wastestream or the process by which it was produced
    is used, must be recorded in a log that is kept in the facility
    operating record.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
    Section 724.950
    Applicability
    a)
    The regulations in this Subpart apply to owners and operators of
    facilities that treat, store, or dispose of hazardous wastes
    (except as provided in Section 724.101).
    b)
    Except as provided in Section 724.964(k), this Subpart applies to
    equipment that contains or contacts hazardous wastes with organic
    concentrations of at least 10 percent by weight that are managed
    in one of the following
    :
    1) UA units that areis subject to the RCRA permitting
    requirements of 35 Ill. Adm. Code
    702, 703, and 705 , or
    2)
    HA unit (including a h
    azardous waste recycling unit
    s) that
    164
    areis not exempt from permitting under the provisions of 35
    Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
    unit that is not a "90-day" tank or container) and that is
    located onat a hazardous waste management
    facilit iesy
    otherwise subject to the permitting requirements of 35 Ill.
    Adm. Code 702, 703, and 705 ., or
    3)
    A unit that is exempt from permitting under the provisions
    of 35 Ill. Adm. Code 722.134(a) (i.e., a "90
    -day" tank or
    container).
    c)
    If the owner or operator of equipment subject to the requirements
    of Sections 724.952 through 724.965 has received a RCRA permit
    prior to December 21, 1990, the requirements of Sections 724.952
    through 724.965 must be incorporated when the permit is reissued
    under 35 Ill. Adm. Code 705.201 or reviewed under 35 Ill. Adm.
    Code 702.161.
    d)
    Each piece of equipment to which this Subpart applies must be
    marked in such a manner that it can be distinguished readily from
    other pieces of equipment.
    e)
    Equipment that is in vacuum service is excluded from the
    requirements of Sections 724.952 to 724.960, if it is identified
    as required in Section 724.964(g)(5).
    f)
    Equipment that contains or contacts hazardous waste with an
    organic concentration of at least 10 percent by weight for a
    period of less than 300 hours per calendar year is excluded from
    the requirements of Sections 264.952 through 264.960 if it is
    identified as required in Section 724.964(g)(6).
    BOARD NOTE: The requirements of Sections 724.952 through 724.965
    apply to equipment associated with hazardous waste recycling units
    previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
    exemptions under 35 Ill. Adm. Code 721.104
    , 722.134 and 724.101(g)
    are not affected by these requirements.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.955
    Standards: Sampling Connecting Systems
    a)
    Each sampling connection
    system must be equipped with a closed
    -
    purge, closed-loop, or
    system or closed-vent system.
    This system
    must collect the sample purge for return to the process or for
    routing to the appropriate treatment system. Gases displaced
    during filling of the sample container are not required to be
    collected or captured.
    b)
    Each closed-purge
    , closed-loop, or
    system or closed-vent system as
    required in subsection (a) must
    meet one of the following
    requirements :
    1)
    Return the purged
    hazardous waste stream process fluid
    directly to the hazardous waste management
    process line with
    no detectable emissions to atmosphere
    ; or
    2)
    Collect and recycle the purged
    hazardous waste stream with
    no detectable emissions to
    atmosphere process fluid ; or
    3)
    Be designed and operated to capture and transport all the
    165
    purged hazardous wastestream process fluid to waste
    management unit that complies with the applicable
    requirements of Sections 724.984 through 724.986 or
    a
    control device that complies with the requirements of
    Section 724.960.
    c)
    In-situ sampling systems
    and sampling systems without purges
    are
    exempt from the requirements of subsections (a) and (b)
    above .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.958
    Standards: Pumps, Valves, Pressure Relief Devices and Other
    Connectors
    a)
    Pumps and valves in heavy liquid service, pressure relief devices
    in light liquid or heavy liquid service and flanges and other
    connectors must be monitored within 5 days by the method specified
    in Section 724.963(b), if evidence of a potential leak is found by
    visual, audible, olfactory, or any other detection method.
    b)
    If an instrument reading of 10,000
    ppm or greater is measured, a
    leak is detected.
    c)
    Repairs
    1)
    When a leak is detected, it must be repaired as soon as
    practicable, but not later than 15 calendar days after it is
    detected, except as provided in Section 724.959.
    2)
    The first attempt at repair must be made no later than 5
    calendar days after each leak is detected.
    d)
    First at tempts at repair include, but are not limited to, the best
    practices described under Section 724.957(e).
    e)
    Any connector that is inaccessible or is ceramic or ceramic-lined
    (e.g., porcelain, glass, or glass
    -lined) is exempt from the
    monitoring requirements of subsection (a) above and from the
    recordkeeping requirements of Section 724.964.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.964
    Recordkeeping Requirements
    a)
    Lumping Units
    1)
    Each owner or operator
    subject to the provisions of this
    Subpart shall comply with the
    recordkeeping requirements of
    this Section.
    2)
    An owner or operator of more than one hazardous waste
    management unit subject to the provisions of this Subpart
    may comply with the
    recordkeeping requirements for these
    hazardous waste management units in one
    recordkeeping system
    if the system identifies each record by each hazardous waste
    management unit.
    b)
    Owners and operators shall record the following information in the
    facility operating record:
    1)
    For each piece of equipment to which this Subpart applies:
    166
    A)
    Equipment identification number and hazardous waste
    management unit identification.
    B)
    Approximate locations within the facility (e.g.,
    identify the hazardous waste management unit on a
    facility plot plan).
    C)
    Type of equipment (e.g., a pump or pipeline valve).
    D)
    Percent-by-weight total
    organics in the hazardous
    wastestream at the equipment.
    E)
    Hazardous waste state at the equipment (e.g., gas-
    vapor or liquid).
    F)
    Method of compliance with the standard (e.g., "monthly
    leak detection and repair" or "equipped with dual
    mechanical seals").
    2)
    for facilities than comply with the provisions of Section
    724.933(a)(2), an implementation schedule as specified in
    that Section.
    3)
    Where an owner or operator chooses to use test data to
    demonstrate the organic removal efficiency or total organic
    compound concentration achieved by the control device, a
    performance test plan as specified in Section 724.935(b)(3).
    4)
    Documentation of compliance with Section 724.960, including
    the detailed design documentation or performance test
    results specified in Section 724.935(b)(4).
    c)
    When each leak is detected as specified in Sections 724.952,
    724.953, 724.957 or 724.958, the following requirements apply:
    1)
    A weatherproof and readily visible identification, marked
    with the equipment identification number, the date evidence
    of a potential leak was found in accordance with Section
    724.958(a), and the date the leak was detected, must be
    attached to the leaking equipment.
    2)
    The identification on equipment except on a valve, may be
    removed after it has been repaired.
    3)
    The identification on a valve may be removed after it has
    been monitored for 2 successive months as specified in
    Section 724.957(c) and no leak has been detected during
    those 2 months.
    d)
    When each leak is detected as specified in Sections 724.952,
    724.953, 724.957 or 724.958, the following information must be
    recorded in an inspection log and must be kept in the facility
    operating record:
    1)
    The instrument and operator identification numbers and the
    equipment identification number.
    2)
    The date evidence of a potential leak was found in
    accordance with Section 724.958(a).
    167
    3)
    The date the leak was detected and the dates of each attempt
    to repair the leak.
    4)
    Repair methods applied in each attempt to repair the leak.
    5)
    "Above 10,000", if the maximum instrument reading measured
    by the methods specified in Section 724.963(b) after each
    repair attempt is equal to or greater than 10,000
    ppm.
    6)
    "Repair delayed" and the reason for the delay if a leak is
    not repaired within 15 calendar days after discovery of the
    leak.
    7)
    Documentation supporting the delay of repair of a valve in
    compliance with Section 724.959(c).
    8)
    The signature of the owner or operator (or designate) whose
    decision it was that repair could not be effected without a
    hazardous waste management unit shutdown.
    9)
    The expected date of successful repair of the leak if a le
    ak
    is not repaired within 15 calendar days.
    10)
    The date of successful repair of the leak.
    e)
    Design documentation and monitoring, operating and inspection
    information for each closed-vent system and control device
    required to comply with the provisions of Section 724.960 must be
    recorded and kept up-to-date in the facility operating record as
    specified in Section 724.935(c)(1) and
    (c)(2), and monitoring,
    operating and inspection information in Section 724.935(c)(3)
    through (c)(8).
    f)
    For a control d evice other than a thermal vapor incinerator,
    catalytic vapor incinerator, flare, boiler, process heater,
    condenser, or carbon adsorption system, the Agency shall specify
    the appropriate recordkeeping requirements, indicating proper
    operation and maintenance of the control device, in the RCRA
    permit.
    g)
    The following information pertaining to all equipment subject to
    the requirements in Sections 724.952 through 724.960 must be
    recorded in a log that is kept in the facility operating record:
    1)
    A list o f identification numbers for equipment (except
    welded fittings) subject to the requirements of this
    Subpart.
    2)
    List of Equipment
    A)
    A list of identification numbers for equipment that
    the owner or operator elects to designate for no
    detectable emissions, as indicated by an instrument
    reading of less than 500
    ppm above background, under
    the provisions of Sections 724.952(e), 724.953(i) and
    724.957(f).
    B)
    The designation of this equipment as subject to the
    requirements of Sections 724.952(e), 724.953(i) or
    724.957(f) must be signed by the owner or operator.
    168
    3)
    A list of equipment identification numbers for pressure
    relief devices required to comply with Section 724.954(a).
    4)
    Compliance tests.
    A)
    The dates of each compliance test required in Sections
    724.952(e), 724.953(i), 724.954 and 724.957(f).
    B)
    The background level measured during each compliance
    test.
    C)
    The maximum instrument reading measured at the
    equipment during each compliance test.
    5)
    A list of identification numbe
    rs for equipment in vacuum
    service.
    6)
    Identification, either by list or location (area or group)
    of equipment that contains or contacts hazardous waste with
    an organic concentration of at least 10 percent by weight
    for a period of less than 300 hours per year.
    h)
    The following information pertaining to all valves subject to the
    requirements of Section 724.957(g) and (h) must be recorded in a
    log that is kept in the facility operating record:
    1)
    A list of identification numbers for valves that are
    designated as unsafe to monitor, an explanation for each
    valve stating why the valve is unsafe to monitor, and the
    plan for monitoring each valve.
    2)
    A list of identification numbers for valves that are
    designated as difficult to monitor, an explanation for each
    valve stating why the valve is difficult to monitor, and the
    planned schedule for monitoring each valve.
    i)
    The following information must be recorded in the facility
    operating record for valves complying with Section 724.962:
    1)
    A schedule o f monitoring.
    2)
    The percent of valves found leaking during each monitoring
    period.
    j)
    The following information must be recorded in a log that is kept
    in the facility operating record:
    1)
    Criteria required in Section 724.952(d)(5)(B) and
    724.953(e)(2) and an explanation of the design criteria.
    2)
    Any changes to these criteria and the reasons for the
    changes.
    k)
    The following information must be recorded in a log that is kept
    in the facility operating record for use in determining exemptions
    as provided in Section 724.950 and other specific Subparts:
    1)
    An analysis determining the design capacity of the hazardous
    waste management unit.
    2)
    A statement listing the hazardous waste influent to and
    169
    effluent from each hazardous waste management unit subject
    to the requirements in Sections 724.960 and an analysis
    determining whether these hazardous wastes are heavy
    liquids.
    3)
    An up-to-date analysis and the supporting information and
    data used to determine whether or not equipment is subject
    to the requirements in Sections 724.952 through 724.960.
    The record must include supporting documentation as required
    by Section 724.963(d)(3) when application of the knowledge
    of the nature of the hazardous wastestream or the process by
    which it was produced is used. If the owner or operator
    takes any action (e.g., changing the process that produced
    the waste) that could result in an increase in the total
    organic content of the waste contained in or contacted by
    equipment determined not to be subject to the requirements
    in Sections 724.952 through 724.960, then a new
    determination is required.
    l)
    Records of the equipment leak information required by subsection
    (d) above and the operating information required by subsection (e)
    above need be kept only 3 years.
    m)
    The owner or operator of any facility that is subject to this
    Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61,
    Subpart V, incorporated by reference in 35 Ill. Adm. Code 720.111,
    may elect to determine compliance with this Subpart by
    documentation either pursuant to Section 724.964, or pursuant to
    those provisions of 40 CFR 60 or 61, to the extent that the
    documentation under the regulation at 40 CFR 60 or 61 duplicates
    the documentation required under this Subpart. The documentation
    under the regulation at 40 CFR 60 or 61 must be kept with or made
    readily available with the facility operating record.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
    SURFACE IMPOUNDMENTS, AND CONTAINERS
    Section 724.980
    Applicability
    a)
    The requirements of this Subpart apply, effective October 6, 1996,
    to owners and operators of all facilities that treat, store, or
    dispose of hazardous waste in tanks, surface
    impoundments, or
    containers subject to 724.Subparts I, J, or K, except as Section
    724.101 and subsection (b) below provide otherwise.
    BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
    (Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828
    (May 19, 1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed.
    Reg. 28508 (June 5, 1996), USEPA delayed the effective date until
    October 6, 1996. If action by USEPA or a decision of a federal
    court changes the effectiveness of these regulations, the Board
    does not intend that the 724.Subpart CC rules be enforceable to
    the extent that they become more stringent that the federal
    regulations upon which they are based.
    b)
    The requirements of this Subpart do not apply to the following
    waste management units at the facility:
    170
    1)
    A waste management unit that holds hazardous waste placed in
    the unit before October 6, 1996, and in which no hazardous
    waste is added to the unit on or after this date.
    2)
    A container that has a design capacity less than or equal to
    0.1 m
    3
    (3.5 ft
    3
    or 26.4 gal).
    3)
    A tank in which an owner or operator has stopped adding
    hazardous waste and the owner or operator has begun
    implementing or completed closure pursuant to an approved
    closure plan.
    4)
    A surface impoundment in whic
    h an owner or operator has
    stopped adding hazardous waste (except to implement an
    approved closure plan) and the owner or operator has begun
    implementing or completed closure pursuant to an approved
    closure plan.
    5)
    A waste management unit that is used solely for on-site
    treatment or storage of hazardous waste that is generated as
    the result of implementing remedial activities required
    pursuant to the Act or Board regulations or under the
    corrective action authorities of RCRA sections 3004(u),
    3004(v) or 3008(h); CERCLA authorities; or similar federal
    or state authorities.
    6)
    A waste management unit that is used solely for the
    management of radioactive mixed waste in accordance with all
    applicable regulations under the authority of the Atomic
    Energy Act (42 U.S.C. 2011 et seq.) and the Nuclear Waste
    Policy Act.
    7)
    A hazardous waste management unit that the owner or operator
    certifies is equipped with and operating air emission
    controls in accordance with the requirements of an
    applicable federal Clean Air Act regulation codified under
    40 CFR 60, 61, or 63. For the purpose of complying with
    this subsection, a tank for which the air emission control
    includes an enclosure, as opposed to a cover, must be in
    compliance with the enclosure and control device
    requirements of Section 724.984(i), except as provided in
    Section 724.982(c)(5).
    8)
    A tank that has a process vent, as defined in 35 Ill. Adm.
    Code 724.931.
    c)
    For the owner and operator of a facility subject to this Subpart
    and whothat received a final RCRA permit prior to October 6, 1996,
    the requirements of this Subpart shall be incorporated into the
    permit when the permit is reissued, renewed, or modified in
    accordance with the requirements of 35 Ill. Adm. Code 703 and 705.
    Until such date when the owner and operator receives a final
    permit incorporating the requirements of this Subpart, the owner
    and operator is subject to the requirements of 35 Ill. Adm. Code
    725.Subpart CC.
    d)
    The requirements of this Subpart, except for the
    recordkeeping
    requirements specified in Section 724.989(i) are stayed for a tank
    or container used for the management of hazardous waste generated
    by organic peroxide manufacturing and its associated laboratory
    operations, when the owner or operator of the unit meets all of
    171
    the following conditions:
    1)
    The owner or operator identifies that the tank or container
    receives hazardous waste generated by an organic peroxide
    manufacturing process producing more than one functional
    family of organic peroxides or multiple organic peroxides
    within one functional family, that one or more of these
    organic peroxides could potentially undergo self-
    accelerating thermal decomposition at or below ambient
    temperatures, and that organic peroxides are the predominant
    products manufactured by the process. For the purposes of
    this subsection, "organic peroxide" means an organic
    compound that contains the bivalent
    -O-O- structure and
    which may be considered to be a
    sturctural derivative of
    hydrogen peroxide where one or both of the hydrogen atoms
    has been replaced by an organic radical.
    2)
    The owner or operator prepares documentation, in accordance
    with Section 724.989(i), explaining why an undue safety
    hazard would be created if air emission controls specified
    in Sections 724.984 through 724.987 are installed and
    operated on the tanks and containers used at the facility to
    manage the hazardous waste generated by the organic peroxide
    manufacturing process or processes meeting the conditions of
    subsection (d)(1) above.
    3)
    The owner or opera
    tor notifies the Agency in writing that
    hazardous waste generated by an organic peroxide
    manufacturing process or processes meeting the conditions of
    subsection (d)(1) above are managed at the facility in tanks
    or containers meeting the conditions of subsection (d)(2)
    above. The notification must state the name and address of
    the facility and be signed and dated by an authorized
    representative of the facility owner or operator.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.982
    Standards: General
    a)
    This Section applies to the management of hazardous waste in
    tanks, surface impoundments, and containers subject to this
    Subpart.
    b)
    The owner or operator shall control air emissions from each waste
    management unit in accordance with standards specified in Section
    724.984 through 724.987, as applicable to the waste management
    unit, except as provided for in subsection (c) below.
    c)
    A waste management
    unittank, surface impoundment, or container
    is
    exempt ed from standards specified in Sections 724.984 through
    724.987, as applicable, provided that all hazardous waste placed
    in the waste management unit is
    determined by the owner or
    operator to meet
    either one of the following
    conditions :
    1) The average VO concentration of
    theA tank, surface
    impoundment, or container for which all
    hazardous waste
    entering the unit has an average VO concentration
    at the
    point of waste origination
    isof less than 100500 parts per
    million by weight (
    ppmw). The average VO concentration
    shall be determined by the procedures specified in Section
    724.983(a). The owner or operator shall review and update,
    172
    as necessary, this determination at least once every 12
    months following the date of the initial determination for
    the hazardous waste streams entering the unit.
    2) TA tank, surface impoundment, or container for which t
    he
    organic content of
    all the hazardous waste
    entering the
    waste management unit
    has been reduced by an organic
    destruction or removal process that achieves any one of the
    following conditions:
    A)
    The process removes or destroys the
    organics contained
    in the hazardous waste to a level such that the
    average VO concentration of the hazardous waste at the
    point of waste treatment is less than the exit
    concentration limit (C
    t
    ) established for the process.
    The average VO concentration of the hazardous waste
    at the point of waste treatment and the exit
    concentration limit for the process shall be
    determined using the procedures specified in Section
    724.983(b).
    B)
    The proce ss removes or destroys the
    organics contained
    in the hazardous waste to a level such that the
    organic reduction efficiency (R) for the process is
    equal to or greater than 95 percent, and the average
    VO concentration of the hazardous waste at the point
    of waste treatment is less than
    50100 ppmw. The
    organic reduction efficiency for the process and the
    average VO concentration of the hazardous waste at the
    point of waste treatment shall be determined using the
    procedures specified in Section 724.983(b).
    C)
    The process removes or destroys the
    organics contained
    in the hazardous waste to a level such that the actual
    organic mass removal rate (MR) for the process is
    equal to or greater than the required organic mass
    removal rate (RMR) established for the process. The
    required organic mass removal rate and the actual
    organic mass removal rate for the process shall be
    determined using the procedures specified in Section
    724.983(b).
    D)
    The process is a biological process that destroys or
    degrades the organics contained in the hazardous waste
    so that either of the following conditions is met:
    i)
    The organic reduction efficiency (R) for the
    process is equal to or greater than 95 percent,
    and the organic biodegradation efficiency (
    R
    bio
    )
    for the process is equal to or greater than 95
    percent. The organic reduction efficiency and
    the organic biodegradation efficiency for the
    process shall be determined
    in accordance
    withusing the procedures specified in Section
    724.983(b).
    ii)
    The total actual organic m
    ass biodegradation
    rate ( MR
    bio
    ) for all hazardous waste treated by
    the process is equal to or greater than the
    required organic mass removal rate (RMR). The
    required organic mass removal rate and the
    173
    actual organic mass
    biodegradation rate for the
    process shall be determined using the procedures
    specified in Section 724.983(b).
    E)
    The process removes or destroys the
    organics contained
    in the hazardous waste and meets all of the following
    conditions:
    i) All of the materials entering the process are
    hazardous wastes.
    ii)
    From the point of waste origination through the
    point where the hazardous waste enters the
    treatment process, the hazardous waste is
    continuously managed in waste management units
    whichthat use air emission controls in
    accordance with the standards specified in
    Sections 724.984 through 724.987, as applicable
    to the waste management unit.
    ii)
    From the point of waste origination through the
    point where the hazardous waste enters the
    treatment process, any transfer of the hazardous
    waste is accomplished through continuous
    hard-piping or other closed system transfer that
    does not allow exposure of the waste to the
    atmosphere.
    BOARD NOTE: The USEPA considers a drain system
    that meets the requirements of 40 CFR 63,
    subpart RR, "National Emission Standards for
    Individual Drain Systems", to be a closed
    system.
    iii)
    The average VO concentration of the hazardous
    waste at the point of waste treatment is less
    than the lowest average VO concentration at the
    point of waste origination, determined for each
    of the individual hazardous waste streams
    entering the process
    , or 100500 ppmw, whichever
    value is lower. The average VO concentration of
    each individual hazardous waste stream at the
    point of waste origination shall be determined
    using the procedure
    s specified in Section
    724.983(a). The average VO concentration of the
    hazardous waste at the point of waste treatment
    shall be determined using the procedure
    s
    specified in Section 724.983(b).
    F)
    A process that removes or destroys the
    organics
    contained in the hazardous waste to a level such that
    the organic reduction efficiency (R) for the process
    is equal to or greater than 95 percent and the owner
    or operator certifies that the average VO
    concentration at the point of waste origination for
    each of the individual waste streams entering the
    process is less than 10,000
    ppmw. The organic
    reduction efficiency for the process and the average
    VO concentration of the hazardous waste at the point
    of waste origination shall be determined using the
    procedures specified in Section 724.983(b) and Section
    174
    724.983(a), respectively.
    FG)
    A hazardous waste incinerator for which
    either of the
    owner or operator has
    either following conditions is
    true:
    i) BThe owner or operator has b
    een issued a final
    permit under 35 Ill. Adm. Code
    702, 703, and
    705, and designs and operates the unit in
    accordance with that implements the requirements
    of 724726.Subpart OH; or
    ii) HThe owner or operator h
    as certified
    compliance designed and operates the incinerator
    in accordance with the interim status
    requirements of 35 Ill. Adm. Code 725.Subpart O.
    GH)
    A boiler or industrial furnace for which
    either of the
    owner or operator has
    either following conditions is
    true:
    i) BThe owner or operator has b
    een issued a final
    permit under 35 Ill. Adm. Code
    702, 703, and
    705, and designs and operates the unit in
    accordance with that implements the requirements
    of 724726.Subpart H; or
    ii)
    The owner or operator h
    as certified
    compliance designed and operates the boiler or
    industrial furnace in accordance
    with the
    interim status requirements of 35 Ill. Adm. Code
    726.Subpart H.
    I)
    For the purpose of determining the performance of an
    organic destruction or removal process in accordance
    with the conditions in each of subsections (c)(2)(A)
    through (c)(2)(F) above, the owner or operator shall
    account for VO concentrations determined to be below
    the limit of detection of the analytical method by
    using the following VO concentration:
    i)
    If Method 25D in 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, is used for the analysis, one
    -half the
    blank value determined in the method.
    ii)
    If any other analytical method is used, one
    -half
    the limit of detection established for the
    method.
    3)
    A tank used for biological treatment of hazardous waste in
    accordance with the requirements of subsection (c)(2)(D)
    above.
    4)
    A tank, surface impoundment, or container for which all
    hazardous waste placed in the unit fulfills either of the
    following conditions:
    A)
    It meets the numerical concentration limits for
    organic hazardous constituents, applicable to the
    hazardous waste, as specified in 35 Ill. Adm. Code
    175
    728.Table T; or
    B)
    It has been treated by the treatment technology
    established by USEPA for the waste in 35 Ill. Adm.
    Code 728.142(a), or treated by an equivalent method of
    treatment approved by the Agency pursuant to 35 Ill.
    Adm. Code 728.142(b).
    5)
    A tank used for bulk feed of hazardous waste to a waste
    incinerator and all of the following conditions are met:
    A)
    The tank is located inside an enclosure vented to a
    control device that is designed and operated in
    accordance with all applicable requirements specified
    under 40 CFR 61, subpart FF, "National Emission
    Standards for Benzene Waste Operations", incorporated
    by reference in 35 Ill. Adm. Code 720.111, for a
    facility at which the total annual benzene quantity
    from the facility waste is equal to or greater than 10
    megagrams (11 tons) per year;
    B)
    The enclosure and control device serving the tank were
    installed and began operation prior to November 25,
    1996; and
    C)
    The enclosure is designed and operated in accordance
    with the criteria for a permanent total enclosure as
    specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. The enclosure may have permanent or
    temporary openings to allow worker access; passage of
    material into or out of the enclosure by conveyor,
    vehicles, or other mechanical or electrical equipment;
    or to direct air flow into the enclosure. The owner
    or operator shall perform the verification procedure
    for the enclosure as specified in Section 5.0 to
    "Procedure T --Criteria for and Verification of a
    Permanent or Temporary Total Enclosure" annually.
    d) When a process is used for the purpose of treating a hazardous
    waste to meet one of the sets of conditions specified in
    subsections (c)(2)(A) through (c)(2)(E) above, each material
    removed from or exiting the process that is not a hazardous waste
    but which has an average VO concentration equal to or greater than
    100 ppmw shall be managed in a waste management unit in accordance
    with the requirements of subsection (b) above.
    ed)
    The Agency may at any time perform or request that the owner or
    operator perform a waste determination for a hazardous waste
    managed in a tank, surface impoundment, or container that is
    exempted from using air emission controls under the provisions of
    this Section as follows:
    1)
    The waste determination for average VO concentration of a
    hazardous waste at the point of waste origination shall be
    performed using direct measurement in accordance with the
    applicable requirements of Section 724.983(a). The waste
    determination for a hazardous waste at the point of waste
    treatment shall be performed in accordance with the
    176
    applicable requirements of Section 724.983(b).
    2)
    In performing a waste determination pursuant to subsection
    (d)(1) above, the sample preparation and analysis shall be
    conducted as follows:
    A)
    In accordance with the method used by the owner or
    operator to perform the waste analysis, except in the
    case specified in subsection (d)(2)(B) below.
    B)
    If the Agency determines that the method used by the
    owner or operator was not appropriate for the
    hazardous waste managed in the tank, surface
    impoundment, or container, then the Agency may choose
    an appropriate method.
    23)
    Where the owner or operator is requested to perform the
    waste determination, the Agency may elect to have an
    authorized representative observe the collection of the
    hazardous waste samples used for the analysis.
    34)
    Where the results of the waste determination performed or
    requested by the Agency do not agree with the results of a
    waste determination performed by the owner or operator using
    knowledge of the waste, then the results of the waste
    determination performed in accordance with the requirements
    of subsection ( ed)(1) above shall be used to establish
    compliance with the requirements of this Subpart.
    45)
    Where the owner or operator has used an averaging period
    greater than one hour for determining the average VO
    concentration of a hazardous waste at the point of waste
    origination, the Agency may elect to establish compliance
    with this Subpart by performing or requesting that the owner
    or operator perform a waste determination using direct
    measurement based on waste samples collected within a one-
    hour period as follows:
    A)
    The average VO concentration of t
    he hazardous waste at
    the point of waste origination shall be determined by
    direct measurement in accordance with the requirements
    of Section 724.983(a).
    B)
    Results of the waste determination performed or
    requested by the Agency showing that the average VO
    concentration of the hazardous waste at the point of
    waste origination is equal to or greater than
    100500
    ppmw shall constitute noncompliance with this Subpart,
    except in a case as provided for in subsection
    (ed)(4)(C) below.
    C)
    Where the average
    VO concentration of the hazardous
    waste at the point of waste origination previously has
    been determined by the owner or operator using an
    averaging period greater than one hour to be less than
    100500 ppmw but because of normal operating process
    variations the VO concentration of the hazardous waste
    determined by direct measurement for any given one-
    hour period may be equal to or greater than
    100500
    ppmw, information that was used by the owner or
    operator to determine the average VO concentration of
    177
    the hazardous waste (e.g., test results, measurements,
    calculations, and other documentation) and recorded in
    the facility records in accordance with the
    requirements of Section 724.983(a) and Section 724.989
    shall be considered by the Agency together with the
    results of the waste determination performed or
    requested by the Agency in establishing compliance
    with this Subpart.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.983
    Waste Determination Procedures
    a)
    Waste det ermination procedure for average volatile organic (VO)
    concentration of a hazardous waste at the point of waste
    origination.
    1)
    An owner or operator shall determine the average VO
    concentration at the point of waste origination for each
    hazardous waste placed in
    a waste management unit
    s exempted
    under the provisions of Section 724.982(c)(1) from using air
    emission controls in accordance with standards specified in
    Section 724.984 through Section 724.987, as applicable to
    the waste management unit.
    2)
    The average VO concentration
    of a hazardous waste
    at the
    point of waste origination
    for a hazardous waste
    shallmay be
    determined in accordance with the procedures specified in 35
    Ill. Adm. Code 725.984(a)(2) through (a)(
    64).
    b)
    Waste determination procedures for treated hazardous waste.
    1)
    An owner or operator shall perform the applicable waste
    determination s for each treated hazardous waste placed in
    a
    waste management unit
    s exempted under the provisions of
    Section 724.982(c)(2) from using air emission controls in
    accordance with standards specified in Section
    s 724.984
    through 724.987, as applicable to the waste management unit.
    2)
    The waste determination for a treated hazardous waste shall
    be performed in accordance with the procedures specified in
    35 Ill. Adm. Code 725.984(b)(2) through (b)(
    109), as
    applicable to the treated hazardous waste.
    c)
    Procedure to determine the maximum organic vapor pressure of a
    hazardous waste in a tank.
    1)
    An owner or operator shall determine the maximum organic
    vapor pressure for each hazardous waste placed in
    a tanks
    using air emission Tank Level 1 controls in accordance with
    standards specified in Section 724.984(c).
    2)
    The maximum organic vapor pressure of the hazardous waste
    shallmay be determined in accordance with the procedures
    specified in 35 Ill. Adm. Code 725.984(c)(2) through (c)(4).
    d)
    The procedure for determining no detectable organic emissions for
    the purpose of complying with this Subpart must be conducted in
    accordance with the procedures specified in 40 CFR 265.984(d).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    178
    Section 724.984
    Standards: Tanks
    a) This Section applies to owners and operators of tanks subject to
    this Subpart into which any hazardous waste is placed, except for
    the following tanks:
    1) A tank in which all hazardous waste entering the tank meets
    the conditions specified in Section 724.982(c), or
    2) A tank used for biological treatment of hazardous waste in
    accordance with the requirements of Section
    724.982(c)(2)(D).
    b) The owner or operator shall place the hazardous waste into one of
    the following tanks:
    1) A tank equipped with a cover (e.g., a fixed roof) that is
    vented through a closed-vent system to a control device in
    accordance with the requirements specified in subsection (d)
    below;
    2) A tank equipped with a fixed roof and internal floating roof
    in accordance with the requirements of Section 724.991;
    3) A tank equipped with an external floating roof in accordance
    with the requirements of Section 724.991; or
    4) A pressure tank that is designed to operate as a closed
    system such that the tank operates with no detectable
    organic emissions at all times that hazardous waste is in
    the tank except as provided for in subsection (g) below.
    c) As an alternative to complying with subsection (b) above, an owner
    or operator may place hazardous waste in a tank equipped with a
    cover (e.g., a fixed roof) meeting the requirements specified in
    subsection (d)(1) below when the hazardous waste is determined to
    meet all of the following conditions:
    1) The hazardous waste is not mixed, stirred, agitated, or
    circulated within the tank by the owner or operator using a
    process that results in splashing, frothing, or visible
    turbulent flow on the waste surface during normal process
    operations;
    2) The hazardous waste in the tank is not heated by the owner
    or operator except during conditions requiring that the
    waste be heated to prevent the waste from freezing or to
    maintain adequate waste flow conditions for continuing
    normal process operations;
    3) The hazardous waste in the tank is not treated by the owner
    or operator using a waste stabilization process or a process
    that produces an exothermic reaction; and
    4) The maximum organic vapor pressure of the hazardous waste in
    the tank, as determined using the procedure specified in
    Section 724.983(c), is less than the following applicable
    value:
    A) If the tank design capacity is equal to or greater
    179
    than 151 m
    3
    (5333 ft
    3
    or 39,887 gal), then the maximum
    organic vapor pressure shall be less than 5.2
    kPa
    (0.75 psia or 39 mm Hg);
    B) If the tank design capacity is equal to or greater
    than 75 m
    3
    (2649 ft
    3
    or 19,810 gal) but less than 151
    m
    3
    (5333 ft
    3
    or 39,887 gal), then the maximum organic
    vapor pressure shall be less than 27.6
    kPa (4.0 psia
    or 207 mm Hg); or
    C) If the tank design capacity is less than 75 m
    3
    (2649
    ft
    3
    or 19,810 gal), then the maximum organic vapor
    pressure shall be less than 76.6
    kPa (11.1 psia or 574
    mm Hg).
    d) To comp ly with subsection (b)(1) above, the owner or operator
    shall design, install, operate, and maintain a cover that vents
    the organic vapors emitted from hazardous waste in the tank
    through a closed-vent system connected to a control device.
    1) The cover shall be designed and operated to meet the
    following requirements:
    A) The cover and all cover openings (e.g., access
    hatches, sampling ports, and gauge wells) shall be
    designed to operate with no detectable organic
    emissions when all cover openings are secured in a
    closed, sealed position; and
    B) Each cover opening shall be secured in a closed,
    sealed position (e.g., covered by a
    gasketed lid or
    cap) at all times that hazardous waste is in the tank
    except as provided for in subsection (f) below.
    2) The closed-vent system and control device shall be designed
    and operated in accordance with the requirements of Section
    724.987.
    e) The owner and operator shall install, operate, and maintain
    enclosed pipes or other closed-systems to:
    BOARD NOTE: U .S. EPA considers a drain system that meets the
    requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
    a "closed-system". The Board intends that this meaning be
    included in the use of that term for the purposes of this Subpart.
    1) Transfer all hazardous waste to the tank from another tank,
    surface impoundment, or container subject to this Subpart
    except for those hazardous wastes that meet the conditions
    specified in Section 724.982(c); and
    2) Transfer all hazardous waste from the tank to
    another tank,
    surface impoundment, or container subject to this Subpart
    except for those hazardous wastes that meet the conditions
    specified in Section 724.982(c).
    f) Each cover opening shall be secured in a closed, sealed position
    (e.g., covered by a
    gasketed lid) at all times that hazardous
    waste is in the tank except when it is necessary to use the cover
    opening to:
    180
    1) Add, remove, inspect, or sample the material in the tank;
    2) Inspect, maintain, repair, or replace equipment located
    inside the tank; or
    3) Vent gases or vapors from the tank to a closed-vent system
    connected to a control device that is designed and operated
    in accordance with the requirements of Section 724.987.
    g) One or more safety devices that vent directly to the atmosphere
    may be used on the tank, cover, closed-vent system, or control
    device provided each safety device meets all of the following
    conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the tank or closed-vent system
    connected to a control device; and
    2) The safety device remains in a closed, sealed position at
    all times, except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the tank, cover, closed-vent
    system, or control device in accordance with good
    engineering and safety practices for handling flammable,
    combustible, explosive, or other hazardous materials. An
    example of an unplanned event is a sudden power outage.
    a)
    The provisions of this Section apply to the control of air
    pollutant emissions from tanks for which Section 724.982(b)
    references the use of this Section for such air emission control.
    b)
    The owner or operator shall control air pollutant emissions from
    each tank subject to this Section in accordance with the following
    requirements, as applicable:
    1)
    For a tank that manages hazardous waste that meets all of
    the conditions specified in subsections (b)(1)(A) through
    (b)(1)(C) below, the owner or operator shall control air
    pollutant emissions from the tank in accordance with the
    Tank Level 1 controls specified in subsection (c) below or
    the Tank Level 2 controls specified in subsection (d) below.
    A)
    The hazardous waste in the tank has a maximum organic
    vapor pressure that is less than the maximum organic
    vapor pressure limit for the tank's design capacity
    category as follows:
    i)
    For a tank design capacity equal to or greater
    than 151 m
    3
    (39,900 gal), the maximum organic
    vapor pressure limit for the tank is 5.2
    kPa
    (0.75 psig).
    ii)
    For a tank design capacity equal to or greater
    than 75 m
    3
    (19,800 gal) but less than 151 m
    3
    (39,900 gal), the maximum organic vapor pressure
    limit for the tank is 27.6
    kPa (4.00 psig).
    iii)
    For a tank design capacity less than 75 m
    3
    (19,800 gal), the maximum organic vapor pressure
    limit for the tank is 76.6
    kPa (11.1 psig).
    181
    B)
    The hazardous waste in the tank is not heated by the
    owner or operator to a temperature that is greater
    than the temperature at which the maximum organic
    vapor pressure of the hazardous waste is determined
    for the purpose of complying with subsection (b)(1)(A)
    above.
    C)
    The hazardous waste in the tank is not treated by the
    owner or operator using a waste stabilization process,
    as defined in 35 Ill. Adm. Code 725.981.
    2)
    For a tank that manages hazardous waste that does not meet
    all of the conditions specified in subsections (b)(1)(A)
    through (b)(1)(C) above, the owner or operator shall control
    air pollutant emissions from the tank by using Tank Level 2
    controls in accordance with the requirements of subsection
    (d) below. Examples of tanks required to use Tank Level 2
    controls include a tank used for a waste stabilization
    process and a tank for which the hazardous waste in the tank
    has a maximum organic vapor pressure that is equal to or
    greater than the maximum organic vapor pressure limit for
    the tank's design capacity category as specified in
    subsection (b)(1)(A) above.
    c)
    Owners and operators controlling air pollutant emissions from a
    tank using Tank Level 1 controls must meet the requirements
    specified in subsections (c)(1) through (c)(4) below:
    1)
    The owner or operator shall determine the maximum organic
    vapor pressure for a hazardous waste to be managed in the
    tank using Tank Level 1 controls before the first time the
    hazardous waste is placed in the tank. The maximum organic
    vapor pressure must be determined using the procedures
    specified in Section 724.983(c). Thereafter, the owner or
    operator shall perform a new determination whenever changes
    to the hazardous waste managed in the tank could potentially
    cause the maximum organic vapor pressure to increase to a
    level that is equal to or greater than the maximum organic
    vapor pressure limit for the tank design capacity category
    specified in subsection (b)(1)(A) below, as applicable to
    the tank.
    2)
    The tank must be equipped with a fixed roof designed to meet
    the following specifications:
    A)
    The fixed roof and its closure devices must be
    designed to form a continuous barrier over the entire
    surface area of the hazardous waste in the tank. The
    fixed roof may be a separate cover installed on the
    tank (e.g., a removable cover mounted on an open
    -top
    tank) or may be an integral part of the tank
    structural design (e.g., a horizontal cylindrical tank
    equipped with a hatch).
    B)
    The fixed roof must be installed in a manner such that
    there are no visible cracks, holes, gaps, or other
    open spaces between roof Section joints or between the
    interface of the roof edge and the tank wall.
    C)
    Each opening in the fixed roof must be either:
    182
    i)
    Equipped with a closure device designed to
    operate such that when the closure device is
    secured in the closed position there are no
    visible cracks, holes, gaps, or other open
    spaces in the closure device or between the
    perimeter of the opening and the closure device;
    or
    ii)
    Connected by a closed
    -vent system that is vented
    to a control device. The control device must
    remove or destroy
    organics in the vent stream,
    and it must be operating whenever hazardous
    waste is managed in the tank.
    D)
    The fixed roof and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and will maintain the integrity of the
    fixed roof and closure devices throughout their
    intended service life. Factors to be considered when
    selecting the materials for and designing the fixed
    roof and closure devices must include the following:
    the organic vapor permeability; the effects of any
    contact with the hazardous waste or its vapors managed
    in the tank; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    used for the tank on which the fixed roof is
    installed.
    3)
    Whenever a hazardous waste is in the tank, the fixed roof
    must be installed with each closure device secured in the
    closed position, except as follows:
    A)
    Opening of closure devices or removal of the fixed
    roof is allowed at the following times:
    i)
    To provide access to the tank for performing
    routine inspection, maintenance, or other
    activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample the
    liquid in the tank, or when a worker needs to
    open a hatch to maintain or repair equipment.
    Following completion of the activity, the owner
    or operator shall promptly secure the closure
    device in the closed position or reinstall the
    cover, as applicable, to the tank.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of tank.
    B)
    Opening of a spring
    -loaded pressure -vacuum relief
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the tank internal pressure in accordance
    with the tank design specifications. The device must
    be designed to operate with no detectable organic
    emissions when the device is secured in the closed
    position. The settings at which the device opens must
    be established such that the device remains in the
    183
    closed position whenever the tank internal pressure is
    within the internal pressure operating range
    determined by the owner or operator based on the tank
    manufacturer recommendations, applicable regulations,
    fire protection and prevention codes, standard
    engineering codes and practices, or other requirements
    for the safe handling of flammable, ignitable,
    explosive, reactive, or hazardous materials. Examples
    of normal operating conditions that may require these
    devices to open are during those times when the tank
    internal pressure exceeds the internal pressure
    operating range for the tank as a result of loading
    operations or diurnal ambient temperature
    fluctuations.
    C)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    4)
    The owner or operator shall inspect the air emission control
    equipment in accordance with the following requirements.
    A)
    The fixed roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to,
    visible cracks, holes, or gaps in the roof sections or
    between the roof and the tank wall; broken, cracked,
    or otherwise damaged seals or gaskets on closure
    devices; and broken or missing hatches, access covers,
    caps, or other closure devices.
    B)
    The owner or operator shall perform an initial
    inspection of the fixed roof and its closure devices
    on or before the date that the tank becomes subject to
    this Section. Thereafter, the owner or operator shall
    perform the inspections at least once every year
    except under the special conditions provided for in
    subsection (l) below.
    C)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    D)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 724.989(b).
    d)
    Owners and operators controlling air pollutant emissions from a
    tank using Tank Level 2 controls must use one of the following
    tanks:
    1)
    A fixed -roof tank equipped with an internal floating roof in
    accordance with the requirements specified in subsection (e)
    below;
    2)
    A tank equipped with an external floating roof in accordance
    with the requirements specified in subsection (f) below;
    3)
    A tank vented through a closed
    -vent system to a control
    device in accordance with the requirements specified in
    184
    subsection (g) below;
    4)
    A pressure tank designed and operated in accordance with the
    requirements specified in subsection (h) below; or
    5)
    A tank located inside an enclosure that is vented through a
    closed -vent system to an enclosed combustion control device
    in accordance with the requirements specified in subsection
    (i) below.
    e)
    The owner or operator that controls air pollutant emissions from a
    tank using a fixed roof with an internal floating roof shall meet
    the requirements specified in subsections (e)(1) through (e)(3)
    below.
    1)
    The tank must be equipped with a fixed roof and an internal
    floating roof in accordance with the following requirements:
    A)
    The internal floating roof must be designed to float
    on the liquid surface except when the floating roof
    must be supported by the leg supports.
    B)
    The internal floating roof must be equipped with a
    continuous seal between the wall of the tank and the
    floating roof edge that meets either of the following
    requirements:
    i)
    A single continuous seal that is either a
    liquid -mounted seal or a metallic shoe seal, as
    defined in 35 Ill. Adm. Code 725.981; or
    ii)
    Two continuous seals mounted one above the
    other. The lower seal may be a vapor
    -mounted
    seal.
    C)
    The internal floating roof must meet the following
    specifications:
    i)
    Each opening in a
    noncontact internal floating
    roof except for automatic bleeder vents (vacuum
    breaker vents) and the rim space vents is to
    provide a projection below the liquid surface.
    ii)
    Each opening in the internal floating roof must
    be equipped with a
    gasketed cover or a
    gasketed
    lid except for leg sleeves, automatic bleeder
    vents, rim space vents, column wells, ladder
    wells, sample wells, and stub drains.
    iii)
    Each penetration of the internal floating roof
    for the purpose of sampling must have a slit
    fabric cover that covers at least 90 percent of
    the opening.
    iv)
    Each automatic bleeder vent and rim space vent
    must be gasketed.
    v)
    Each penetration of the internal floating roof
    that allows for passage of a ladder must have a
    gasketed sliding cover.
    185
    vi)
    Each penetration of the internal floating roof
    that allows for passage of a column supporting
    the fixed roof must have a flexible fabric
    sleeve seal or a
    gasketed sliding cover.
    2)
    The owner or operator shall operate the tank in accordance
    with the following requirements:
    A)
    When the floating roof is resting on the leg supports,
    the process of filling, emptying, or refilling must be
    continuous and must be completed as soon as practical.
    B)
    Automatic bleeder vents are to be set closed at all
    times when the roof is floating, except when the roof
    is being floated off or is being landed on the leg
    supports.
    C)
    Prior to filling the tank, each cover, access hatch,
    gauge float well or lid on any opening in the internal
    floating roof must be bolted or fastened closed (i.e.,
    no visible gaps). Rim space vents must be set to open
    only when the internal floating roof is not floating
    or when the pressure beneath the rim exceeds the
    manufacturer's recommended setting.
    3)
    The owner or operator shall inspect the internal floating
    roof in accordance with the procedures specified as follows:
    A)
    The floating roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to
    any of the following: when the internal floating roof
    is not floating on the surface of the liquid inside
    the tank; when liquid has accumulated on top of the
    internal floating roof; when any portion of the roof
    seals have detached from the roof rim; when holes,
    tears, or other openings are visible in the seal
    fabric; when the gaskets no longer close off the
    hazardous waste surface from the atmosphere; or when
    the slotted membrane has more than 10 percent open
    area.
    B)
    The owner or operator shall inspect the internal
    floating roof components as follows, except as
    provided in subsection (e)(3)(C) below:
    i)
    Visually inspect the internal floating roof
    components through openings on the fixed
    -roof
    (e.g., manholes and roof hatches) at least once
    every 12 months after initial fill, and
    ii)
    Visually inspect the internal floating roof,
    primary seal, secondary seal (if one is in
    service), gaskets, slotted membranes, and sleeve
    seals (if any) each time the tank is emptied and
    degassed and at least once every 10 years.
    C)
    As an alternative to performing the inspections
    specified in subsection (e)(3)(B) above for an
    internal floating roof equipped with two continuous
    186
    seals mounted one above the other, the owner or
    operator may visually inspect the internal floating
    roof, primary and secondary seals, gaskets, slotted
    membranes, and sleeve seals (if any) each time the
    tank is emptied and degassed and at least every five
    years.
    D)
    Prior to each inspection required by subsection
    (e)(3)(B) or (e)(3)(C) above, the owner or operator
    shall notify the Agency in advance of each inspection
    to provide the Agency with the opportunity to have an
    observer present during the inspection. The owner or
    operator shall notify the Agency of the date and
    location of the inspection as follows:
    i)
    Prior to each visual inspection of an internal
    floating roof in a tank that has been emptied
    and degassed, written notification must be
    prepared and sent by the owner or operator so
    that it is received by the Agency at least 30
    calendar days before refilling the tank, except
    when an inspection is not planned, as provided
    for in subsection (e)(3)(D)(ii) below.
    ii)
    When a visual inspection is not planned and the
    owner or operator could not have known about the
    inspection 30 calendar days before refilling the
    tank, the owner or operator shall notify the
    Agency as soon as possible, but no later than
    seven calendar days before refilling of the
    tank. This notification may be made by
    telephone and immediately followed by a written
    explanation for why the inspection is unplanned.
    Alternatively, written notification, including
    the explanation for the unplanned inspection,
    may be sent so that it is received by the Agency
    at least seven calendar days before refilling
    the tank.
    E)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    F)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 724.989(b).
    f)
    The owner or operator that controls air pollutant emissions from a
    tank using an external floating roof must meet the requirements
    specified in subsections (f)(1) through (f)(3) below.
    1)
    The owner or operator shall design the external floating
    roof in accordance with the following requirements:
    A)
    The external floating roof must be designed to float
    on the liquid surface except when the floating roof
    must be supported by the leg supports.
    B)
    The floating roof must be equipped with two continuous
    seals, one above the other, between the wall of the
    tank and the roof edge. The lower seal is referred to
    187
    as the primary seal, and the upper seal is referred to
    as the secondary seal.
    i)
    The primary seal must be a liquid
    -mounted seal
    or a metallic shoe seal, as defined in 35 Ill.
    Adm. Code 725.981. The total area of the gaps
    between the tank wall and the primary seal must
    not exceed 212 square centimeters (cm
    2
    ) per
    meter (10.0 square inches (in
    2
    ) per foot) of
    tank diameter, and the width of any portion of
    these gaps must not exceed 3.8 centimeters (cm)
    (1.5 in). If a metallic shoe seal is used for
    the primary seal, the metallic shoe seal must be
    designed so that one end extends into the liquid
    in the tank and the other end extends a vertical
    distance of at least 61 cm (24 in) above the
    liquid surface.
    ii)
    The secondary seal must be mounted above the
    primary seal and cover the annular space between
    the floating roof and the wall of the tank. The
    total area of the gaps between the tank wall and
    the secondary seal must not exceed 21.2 cm
    2
    per
    meter (1.00 in
    2
    per foot) of tank diameter, and
    the width of any portion of these gaps must not
    exceed 1.3 cm (0.51 in).
    C)
    The external floating roof must meet the following
    specifications:
    i)
    Except for automatic bleeder vents (vacuum
    breaker vents) and rim space vents, each opening
    in a noncontact external floating roof must
    provide a projection below the liquid surface.
    ii)
    Except for automatic bleeder vents, rim space
    vents, roof drains, and leg sleeves, each
    opening in the roof must be equipped with a
    gasketed cover, seal, or lid.
    iii)
    Each access hatch and each gauge float well must
    be equipped with a cover designed to be bolted
    or fastened when the cover is secured in the
    closed position.
    iv)
    Each automatic bleeder vent and each rim space
    vent must be equipped with a gasket.
    v)
    Each roof drain that empties into the liquid
    managed in the tank must be equipped with a
    slotted membrane fabric cover that covers at
    least 90 percent of the area of the opening.
    vi)
    Each unslotted and slotted guide pole well must
    be equipped with a
    gasketed sliding cover or a
    flexible fabric sleeve seal.
    vii)
    Each unslotted guide pole must be equipped with
    a gasketed cap on the end of the pole.
    viii)
    Each slotted guide pole must be equipped with a
    188
    gasketed float or other device which closes off
    the liquid surface from the atmosphere.
    ix)
    Each gauge hatch and each sample well must be
    equipped with a gasketed cover.
    2)
    The owner or operator shall operate the tank in accordance
    with the following requirements:
    A)
    When the floating roof is resting on the leg supports,
    the process of filling, emptying, or refilling must be
    continuous and must be completed as soon as practical.
    B)
    Except for automatic bleeder vents, rim space vents,
    roof drains, and leg sleeves, each opening in the roof
    must be secured and maintained in a closed position at
    all times except when the closure device must be open
    for access.
    C)
    Covers on each access hatch and each gauge float well
    must be bolted or fastened when secured in the closed
    position.
    D)
    Automatic bleeder vents must be set closed at all
    times when the roof is floating, except when the roof
    is being floated off or is being landed on the leg
    supports.
    E)
    Rim space vents must be set to open only at those
    times that the roof is being floated off the roof leg
    supports or when the pressure beneath the rim seal
    exceeds the manufacturer's recommended setting.
    F)
    The cap on the end of each
    unslotted guide pole must
    be secured in the closed position at all times except
    when measuring the level or collecting samples of the
    liquid in the tank.
    G)
    The cover on each gauge hatch or sample well must be
    secured in the closed position at all times except
    when the hatch or well must be opened for access.
    H)
    Both the primary seal and the secondary seal must
    completely cover the annular space between the
    external floating roof and the wall of the tank in a
    continuous fashion except during inspections.
    3)
    The owner or operator shall inspect the external floating
    roof in accordance with the procedures specified as follows:
    A)
    The owner or operator shall measure the external
    floating roof seal gaps in accordance with the
    following requirements:
    i)
    The owner or operator shall perform measurements
    of gaps between the tank wall and the primary
    seal within 60 calendar days after initial
    operation of the tank following installation of
    the floating roof and, thereafter, at least once
    every five years.
    189
    ii)
    The owner or operator shall perform measurements
    of gaps between the tank wall and the secondary
    seal within 60 calendar days after initial
    operation of the tank following installation of
    the floating roof and, thereafter, at least once
    every year.
    iii)
    If a tank ceases to hold hazardous waste for a
    period of one year or more, subsequent
    introduction of hazardous waste into the tank
    must be considered an initial operation for the
    purposes of subsections (f)(3)(A)(i) and
    (f)(3)(A)(ii) above.
    iv)
    The owner or operator shall determine the total
    surface area of gaps in the primary seal and in
    the secondary seal individually using the
    procedure of subsection (f)(3)(D) below.
    v)
    In the event that the seal gap measurements do
    not conform to the specifications in subsection
    (f)(1)(B) above, the owner or operator shall
    repair the defect in accordance with the
    requirements of subsection (k) below.
    vi)
    The owner or operator shall maintain a record of
    the inspection in accordance with the
    requirements specified in Section 724.989(b).
    B)
    The owner or operator shall visually inspect the
    external floating roof in accordance with the
    following requirements:
    i)
    The floating roof and its closure devices must
    be visually inspected by the owner or operator
    to check for defects that could result in air
    pollutant emissions. Defects include, but are
    not limited to any of the following conditions:
    holes, tears, or other openings in the rim seal
    or seal fabric of the floating roof; a rim seal
    detached from the floating roof; all or a
    portion of the floating roof deck being
    submerged below the surface of the liquid in the
    tank; broken, cracked, or otherwise damaged
    seals or gaskets on closure devices; and broken
    or missing hatches, access covers, caps, or
    other closure devices.
    ii)
    The owner or operator shall perform an initial
    inspection of the external floating roof and its
    closure devices on or before the date that the
    tank becomes subject to this Section.
    Thereafter, the owner or operator shall perform
    the inspections at least once every year except
    for the special conditions provided for in
    subsection (l) below.
    iii)
    In the event that a defect is detected, the
    owner or operator shall repair the defect in
    accordance with the requirements of subsection
    (k) below.
    190
    iv)
    The owner or operator shall maintain a record of
    the inspection in accordance with the
    requirements specified in Section 724.989(b).
    C)
    Prior to each inspection required by subsection
    (f)(3)(A) or (f)(3)(B), the owner or operator shall
    notify the Agency in advance of each inspection to
    provide the Agency with the opportunity to have an
    observer present during the inspection. The owner or
    operator shall notify the Agency of the date and
    location of the inspection as follows:
    i)
    Prior to each inspection to measure external
    floating roof seal gaps as required under
    subsection (f)(3)(A) above, written notification
    must be prepared and sent by the owner or
    operator so that it is received by the Agency at
    least 30 calendar days before the date the
    measurements are scheduled to be performed.
    ii)
    Prior to each visual inspection of an external
    floating roof in a tank that has been emptied
    and degassed, written notification must be
    prepared and sent by the owner or operator so
    that it is received by the Agency at least 30
    calendar days before refilling the tank, except
    when an inspection is not planned as provided
    for in subsection (f)(3)(C)(iii) below.
    iii)
    When a visual inspection is not planned and the
    owner or operator could not have known about the
    inspection 30 calendar days before refilling the
    tank, the owner or operator shall notify the
    Agency as soon as possible, but no later than
    seven calendar days before refilling of the
    tank. This notification may be made by
    telephone and immediately followed by a written
    explanation for why the inspection is unplanned.
    Alternatively, written notification, including
    the explanation for the unplanned inspection,
    may be sent so that it is received by the Agency
    at least seven calendar days before refilling
    the tank.
    D)
    Procedure for determining the total surface area of
    gaps in the primary seal and the secondary seal:
    i)
    The seal gap measurements must be performed at
    one or more floating roof levels when the roof
    is floating off the roof supports.
    ii)
    Seal gaps, if any, must be measured around the
    entire perimeter of the floating roof in each
    place where a 0.32 cm (0.125 in) diameter
    uniform probe passes freely (without forcing or
    binding against the seal) between the seal and
    the wall of the tank and measure the
    circumferential distance of each such location.
    iii)
    For a seal gap measured under subsection (f)(3)
    191
    above, the gap surface area must be determined
    by using probes of various widths to measure
    accurately the actual distance from the tank
    wall to the seal and multiplying each such width
    by its respective
    circumferential distance.
    iv)
    The total gap area must be calculated by adding
    the gap surface areas determined for each
    identified gap location for the primary seal and
    the secondary seal individually, and then
    dividing the sum for each seal type by the
    nominal perimeter of the tank. These total gap
    areas for the primary seal and secondary seal
    are then compared to the respective standards
    for the seal type, as specified in subsection
    (f)(1)(B) above.
    BOARD NOTE: Subsections (f)(3)(D)(i) through
    (f)(3)(D)(iv) correspond with 40 CFR
    264.1084(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4),
    which the Board has codified here to comport
    with Illinois Administrative Code format
    requirements.
    g)
    The owner or operator that controls air pollutant emissions from a
    tank by venting the tank to a control device shall meet the
    requirements specified in subsections (g)(1) through (g)(3) below.
    1)
    The tank must be covered by a fixed roof and vented directly
    through a closed -vent system to a control device in
    accordance with the following requirements:
    A)
    The fixed roof and its closure devices must be
    designed to form a continuous barrier over the entire
    surface area of the liquid in the tank.
    B)
    Each opening in the fixed roof not vented to the
    control device must be equipped with a closure device.
    If the pressure in the vapor
    headspace underneath the
    fixed roof is less than atmospheric pressure when the
    control device is operating, the closure devices must
    be designed to operate such that when the closure
    device is secured in the closed position there are no
    visible cracks, holes, gaps, or other open spaces in
    the closure device or between the perimeter of the
    cover opening and the closure device. If the pressure
    in the vapor headspace underneath the fixed roof is
    equal to or greater than atmospheric pressure when the
    control device is operating, the closure device must
    be designed to operate with no detectable organic
    emissions.
    C)
    The fixed roof and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and will maintain the integrity of the
    fixed roof and closure devices throughout their
    intended service life. Factors to be considered when
    selecting the materials for and designing the fixed
    roof and closure devices must include the following:
    organic vapor permeability; the effects of any contact
    192
    with the liquid and its vapor managed in the tank; the
    effects of outdoor exposure to wind, moisture, and
    sunlight; and the operating practices used for the
    tank on which the fixed roof is installed.
    D)
    The closed -vent system and control device must be
    designed and operated in accordance with the
    requirements of Section 724.987.
    2)
    Whenever a hazardous waste is in the tank, the fixed roof
    must be installed with each closure device secured in the
    closed position and the vapor
    headspace underneath the fixed
    roof vented to the control device except as follows:
    A)
    Venting to the control device is not required, and
    opening of closure devices or removal of the fixed
    roof is allowed at the following times:
    i)
    To provide access to the tank for performing
    routine inspection, maintenance, or other
    activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample
    liquid in the tank, or when a worker needs to
    open a hatch to maintain or repair equipment.
    Following completion of the activity, the owner
    or operator shall promptly secure the closure
    device in the closed position or reinstall the
    cover, as applicable, to the tank.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of a tank.
    B)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    3)
    The owner or operator shall inspect and monitor the air
    emission control equipment in accordance with the following
    procedures:
    A)
    The fixed roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to
    any of the following: visible cracks, holes, or gaps
    in the roof sections or between the roof and the tank
    wall; broken, cracked, or otherwise damaged seals or
    gaskets on closure devices; and broken or missing
    hatches, access covers, caps, or other closure
    devices.
    B)
    The closed -vent system and control device must be
    inspected and monitored by the owner or operator in
    accordance with the procedures specified in Section
    724.987.
    C)
    The owner or operator shall perform an initial
    inspection of the air emission control equipment on or
    before the date that the tank becomes subject to this
    Section. Thereafter, the owner or operator shall
    193
    perform the inspections at least once every year
    except for the special conditions provided for in
    subsection (l) below.
    D)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    E)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 724.989(b).
    h)
    The owner or operator that controls air pollutant emissions by
    using a pressure tank must meet the following requirements.
    1)
    The tank must be designed not to vent to the atmosphere as a
    result of compression of the vapor
    headspace in the tank
    during filling of the tank to its design capacity.
    2)
    All tank openings must be equipped with closure devices
    designed to operate with no detectable organic emissions as
    determined using the procedure specified in Section
    724.983(d).
    3)
    Whenever a hazardous waste is in the tank, the tank must be
    operated as a closed system that does not vent to the
    atmosphere except in the event that a safety device, as
    defined in 35 Ill. Adm. Code 725.981, is required to open to
    avoid an unsafe condition.
    i)
    The owner or operator that controls air pollutant emissions by
    using an enclosure vented through a closed
    -vent system to an
    enclosed combustion control device must meet the requirements
    specified in subsections (i)(1) through (i)(4) below.
    1)
    The tank must be located inside an enclosure. The enclosure
    must be designed and operated in accordance with the
    criteria for a permanent total enclosure, as specified in
    "Procedure T --Criteria for and Verification of a Permanent
    or Temporary Total Enclosure" under 40 CFR 52.741, appendix
    B, incorporated by reference in 35 Ill. Adm. Code 720.111.
    The enclosure may have permanent or temporary openings to
    allow worker access; passage of material into or out of the
    enclosure by conveyor, vehicles, or other mechanical means;
    entry of permanent mechanical or electrical equipment; or
    direct airflow into the enclosure. The owner or operator
    shall perform the verification procedure for the enclosure,
    as specified in Section 5.0 to "Procedure T
    --Criteria for
    and Verification of a Permanent or Temporary Total
    Enclosure", initially when the enclosure is first installed
    and, thereafter, annually.
    2)
    The enclosure must be vented through a closed
    -vent system to
    an enclosed combustion control device that is designed and
    operated in accordance with the standards for either a vapor
    incinerator, boiler, or process heater specified in Section
    724.987.
    3)
    Safety devices, as defined in 35 Ill. Adm. Code 725.981, may
    be installed and operated as necessary on any enclosure,
    closed -vent system, or control device used to comply with
    194
    the requirements of subsections (i)(1) and (i)(2) above.
    4)
    The owner or operator shall inspect and monitor the
    closed -vent system and control device as specified in
    Section 724.987.
    j)
    The owner or operator shall transfer hazardous waste to a tank
    subject to this Section in accordance with the following
    requirements:
    1)
    Transfer of hazardous waste, except as provided in
    subsection (j)(2) below, to the tank from another tank
    subject to this Section or from a surface impoundment
    subject to Section 724.985 must be conducted using
    continuous hard -piping or another closed system that does
    not allow exposure of the hazardous waste to the atmosphere.
    For the purpose of complying with this provision, an
    individual drain system is considered to be a closed system
    when it meets the requirements of 40 CFR 63, subpart RR,
    "National Emission Standards for Individual Drain Systems",
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The requirements of subsection (j)(1) above do not apply
    when transferring a hazardous waste to the tank under any of
    the following conditions:
    A)
    The hazardous waste meets the average VO concentration
    conditions specified in Section 724.982(c)(1) at the
    point of waste origination.
    B)
    The hazardous waste has been treated by an organic
    destruction or removal process to meet the
    requirements in Section 724.982(c)(2).
    k)
    The owner or operator shall repair each defect detected during an
    inspection performed in accordance with the requirements of
    subsection (c)(4), (e)(3), (f)(3), or (g)(3) above, as follows:
    1)
    The owner or operator shall make first efforts at repair of
    the defect no later than five calendar days after detection,
    and repair must be completed as soon as possible but no
    later than 45 calendar days after detection except as
    provided in subsection (k)(2) below.
    2)
    Repair of a defect may be delayed beyond 45 calendar days if
    the owner or operator determines that repair of the defect
    requires emptying or temporary removal from service of the
    tank and no alternative tank capacity is available at the
    site to accept the hazardous waste normally managed in the
    tank. In this case, the owner or operator shall repair the
    defect the next time the process or unit that is generating
    the hazardous waste managed in the tank stops operation.
    Repair of the defect must be completed before the process or
    unit resumes operation.
    l)
    Following the initial inspection and monitoring of the cover, as
    required by the applicable provisions of this Subpart, subsequent
    inspection and monitoring may be performed at intervals longer
    than one year under the following special conditions:
    1)
    In the case when inspecting or monitoring the cover would
    195
    expose a worker to dangerous, hazardous, or other unsafe
    conditions, then the owner or operator may designate a cover
    as an "unsafe to inspect and monitor cover" and comply with
    all of the following requirements:
    A)
    Prepare a written explanation for the cover stating
    the reasons why the cover is unsafe to visually
    inspect or to monitor, if required.
    B)
    Develop and implement a written plan and schedule to
    inspect and monitor the cover, using the procedures
    specified in the applicable Section of this Subpart,
    as frequently as practicable during those times when a
    worker can safely access the cover.
    2)
    In the case when a tank is buried partially or entirely
    underground, an owner or operator is required to inspect and
    monitor, as required by the applicable provisions of this
    Section, only those portions of the tank cover and those
    connections to the tank (e.g., fill ports, access hatches,
    gauge wells, etc.) that are located on or above the ground
    surface.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.985
    Standards: Surface
    Impoundments
    a) This Section applies to owners and operators of surface
    impoundments subject to this Subpart into which any hazardous
    waste is placed except for the following surface
    impoundments:
    1) A surface impoundment in which all hazardous waste entering
    the surface impoundment meets the conditions specified in
    Section 724.982(c); or
    2) A surface impoundment used for biological treatment of
    hazardous waste in accordance with the requirements of
    Section 724.982(c)(2)(D).
    b) The owner or operator shall place the hazardous waste into a
    surface impoundment equipped with a cover (e.g., an air-supported
    structure or a rigid cover) that is vented through a closed-vent
    system to a control device meeting the requirements specified in
    subsection (d) below.
    c) As an alternative to complying with subsection (b) above, an owner
    or operator may place hazardous waste in a surface impoundment
    equipped with a floating membrane cover meeting the requirements
    specified in subsection (e) below when the hazardous waste is
    determined to meet all of the following conditions:
    1) The hazardous waste is not mixed, stirred, agitated, or
    circulated within the surface impoundment by the owner or
    operator using a process that results in splashing,
    frothing, or visible turbulent flow on the waste surface
    during normal process operations;
    2) The hazardous waste in the surface impoundment is not heated
    by the owner or operator; and
    3) The hazardous waste is not treated by the owner or operator
    196
    using a waste stabilization process or a process that
    produces an exothermic reaction.
    d) To comply with subsection (b)(1) above, the owner or operator
    shall design, install, operate, and maintain a cover that vents
    the organic vapors emitted from hazardous waste in the surface
    impoundment through a closed-vent system connected to a control
    device.
    1) The cover shall be designed and operated to meet the
    following requirements:
    A) The cover and all cover openings (e.g., access
    hatches, sampling ports, and gauge wells) shall be
    designed to operate with no detectable organic
    emissions when all cover openings are secured in a
    closed, sealed position;
    B) Each cover opening shall be secured in the closed,
    sealed position (e.g., covered by a
    gasketed lid or
    cap) at all times that hazardous waste is in the
    surface impoundment, except as provided for in
    subsection (g) below; and
    C) The closed-vent system and control device shall be
    designed and operated in accordance with Section
    724.987.
    e) To comply wit h subsection (c) above, the owner or operator shall
    design, install, operate, and maintain a floating membrane cover
    that meets all of the requirements specified in 35 Ill. Adm. Code
    725.986(e)(1) through (e)(4).
    f) The owner or operator shall install, operate, and maintain
    enclosed pipes or other closed-systems to
    BOARD NOTE: U.S. EPA considers a drain system that meets the
    requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
    a "closed-system". The Board intends that this meaning be
    included in the use of that term for the purposes of this Subpart.
    1) Transfer all hazardous waste to the surface impoundment from
    another tank, surface impoundment, or container subject to
    this Subpart except for those hazardous wastes that meet the
    conditions specified in Section 724.982(c); and
    2) Transfer all hazardous waste from the surface impoundment to
    another tank, surface impoundment, or container subject to
    this Subpart except for those hazardous wastes that meet the
    conditions specified in Section 724.982(c).
    g) Each cover opening shall be secured in the closed, sealed position
    (e.g., a cover by a
    gasketed lid or cap) at all times that
    hazardous waste is in the surface impoundment except when it is
    necessary to use the cover opening to:
    1) Add, remove, inspect, or sample the material in the surface
    impoundment;
    2) Inspect, maintain, repair, or replace equipment located
    underneath the cover;
    197
    3) Remove treatment residues from the surface impoundment in
    accordance with the requirements of 35 Ill. Adm. Code 728.4;
    or
    4) Vent gases or vapors from the surface impoundment to a
    closed-vent system connected to a control device that is
    designed and operated in accordance with the requirements of
    Section 724.987.
    h) One or more safety devices that vent directly to the atmosphere
    may be installed on the cover, closed-vent system, or control
    device provided each device meets all of the following conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the surface impoundment or the
    closed-vent system connected to a control device; and
    2) The safety device remains in a closed, sealed position at
    all times, except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the cover, closed-vent system, or
    control device in accordance with good engineering and
    safety practices for handling flammable, combustible,
    explosive, or other hazardous materials. An example of an
    unplanned event is a sudden power outage.
    a)
    The provisions of this Section apply to the control of air
    pollutant emissions from surface
    impoundments for which Section
    724.982(b) references the use of this Section for such air
    emission control.
    b)
    The owner or operator shall control air pollutant emissions from
    the surface impoundment by installing and operating either of the
    following:
    1)
    A floating membrane cover in accordance with the provisions
    specified in subsection (c) below; or
    2)
    A cover that is vented through a closed
    -vent system to a
    control device in accordance with the provisions specified
    in subsection (d) below.
    c)
    The owner or operator that controls air pollutant emissions from a
    surface impoundment using a floating membrane cover must meet the
    requirements specified in subsections (c)(1) through (c)(3) below.
    1)
    The surface impoundment must be equipped with a floating
    membrane cover designed to meet the following
    specifications:
    A)
    The floating membrane cover must be designed to float
    on the liquid surface during normal operations and
    form a continuous barrier over the entire surface area
    of the liquid.
    B)
    The cover must be fabricated from a synthetic membrane
    material that is either:
    i)
    High density polyethylene (HDPE) with a
    thickness no less than 2.5 millimeters (mm)
    198
    (0.098 in); or
    ii)
    A material or a composite of different materials
    determined to have both organic permeability
    properties that are equivalent to those of the
    material listed in subsection (c)(1)(B)(i) above
    and chemical and physical properties that
    maintain the material integrity for the intended
    service life of the material.
    C)
    The cover must be installed in such a manner that
    there are no visible cracks, holes, gaps, or other
    open spaces between cover section seams or between the
    interface of the cover edge and its foundation
    mountings.
    D)
    Except as provided for in subsection (c)(1)(E) below,
    each opening in the floating membrane cover must be
    equipped with a closure device so designed as to
    operate that when the closure device is secured in the
    closed position there are no visible cracks, holes,
    gaps, or other open spaces in the closure device or
    between the perimeter of the cover opening and the
    closure device.
    E)
    The floating membrane cover may be equipped with one
    or more emergency cover drains for removal of
    stormwater. Each emergency cover drain must be
    equipped with a slotted membrane fabric cover that
    covers at least 90 percent of the area of the opening
    or a flexible fabric sleeve seal.
    F)
    The closure devices must be made of suitable materials
    that will minimize exposure of the hazardous waste to
    the atmosphere, to the extent practical, and will
    maintain the integrity of the closure devices
    throughout their intended service life. Factors to be
    considered when selecting the materials of
    construction and designing the cover and closure
    devices must include the following: the organic vapor
    permeability; the effects of any contact with the
    liquid and its vapor managed in the surface
    impoundment; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    used for the surface impoundment on which the floating
    membrane cover is installed.
    2)
    Whenever a hazardous waste is in the surface impoundment,
    the floating membrane cover must float on the liquid and
    each closure device must be secured in the closed position,
    except as follows:
    A)
    Opening of closure devices or removal of the cover is
    allowed at the following times:
    i)
    To provide access to the surface impoundment for
    performing routine inspection, maintenance, or
    other activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample the
    liquid in the surface impoundment, or when a
    199
    worker needs to open a hatch to maintain or
    repair equipment. Following completion of the
    activity, the owner or operator shall promptly
    replace the cover and secure the closure device
    in the closed position, as applicable.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of surface impoundment.
    B)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    3)
    The owner or operator shall inspect the floating membrane
    cover in accordance with the following procedures:
    A)
    The floating membrane cover and its closure devices
    must be visually inspected by the owner or operator to
    check for defects that could result in air pollutant
    emissions. Defects include, but are not limited to,
    visible cracks, holes, or gaps in the cover section
    seams or between the interface of the cover edge and
    its foundation mountings; broken, cracked, or
    otherwise damaged seals or gaskets on closure devices;
    and broken or missing hatches, access covers, caps, or
    other closure devices.
    B)
    The owner or operator shall perform an initial
    inspection of the floating membrane cover and its
    closure devices on or before the date that the surface
    impoundment becomes subject to this Section.
    Thereafter, the owner or operator shall perform the
    inspections at least once every year except for the
    special conditions provided for in subsection (g)
    below.
    C)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (f) below.
    D)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 724.989(c).
    d)
    The owner or operator that controls air pollutant emissions from a
    surface impoundment using a cover vented to a control device shall
    meet the requirements specified in subsections (d)(1) through
    (d)(3) below.
    1)
    The surface impoundment must be covered by a cover and
    vented directly through a closed
    -vent system to a control
    device in accordance with the following requirements:
    A)
    The cover and its closure devices must be designed to
    form a continuous barrier over the entire surface area
    of the liquid in the surface impoundment.
    B)
    Each opening in the cover not vented to the control
    device must be equipped with a closure device. If the
    pressure in the vapor
    headspace underneath the cover
    is less than atmospheric pressure when the control
    200
    device is operating, the closure devices must be
    designed to operate such that when the closure device
    is secured in the closed position there are no visible
    cracks, holes, gaps, or other open spaces in the
    closure device or between the perimeter of the cover
    opening and the closure device. If the pressure in
    the vapor headspace underneath the cover is equal to
    or greater than atmospheric pressure when the control
    device is operating, the closure device must be
    designed to operate with no detectable organic
    emissions using the procedure specified in Section
    724.983(d).
    C)
    The cover and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and will maintain the integrity of the
    cover and closure devices throughout their intended
    service life. Factors to be considered when selecting
    the materials for and designing the cover and closure
    devices must include the following: the organic vapor
    permeability; the effects of any contact with the
    liquid or its vapors managed in the surface
    impoundment; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    used for the surface impoundment on which the cover is
    installed.
    D)
    The closed -vent system and control d
    evice must be
    designed and operated in accordance with the
    requirements of Section 724.987.
    2)
    Whenever a hazardous waste is in the surface impoundment,
    the cover must be installed with each closure device secured
    in the closed position and the vapor
    headspace underneath
    the cover vented to the control device except as follows:
    A)
    Venting to the control device is not required, and
    opening of closure devices or removal of the cover is
    allowed at the following times:
    i)
    To provide access to the surface impoundment for
    performing routine inspection, maintenance, or
    other activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample
    liquid in the surface impoundment, or when a
    worker needs to open a hatch to maintain or
    repair equipment. Following completion of the
    activity, the owner or operator shall promptly
    secure the closure device in the closed position
    or reinstall the cover, as applicable, to the
    surface impoundment.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of surface impoundment.
    B)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    201
    3)
    The owner or operator shall inspect and monitor the air
    emission control equipment in accordance with the following
    procedures:
    A)
    The surface impoundment cover and its closure devices
    shall be visually inspected by the owner or operator
    to check for defects that could result in air
    pollutant emissions. Defects include, but are not
    limited to, visible cracks, holes, or gaps in the
    cover section seams or between the interface of the
    cover edge and its foundation mountings; broken,
    cracked, or otherwise damaged seals or gaskets on
    closure devices; and broken or missing hatches, access
    covers, caps, or other closure devices.
    B)
    The closed -vent system and control device must be
    inspected and monitored by the owner or operator in
    accordance with the procedures specified in Section
    724.987.
    C)
    The owner or operator shall perform an initial
    inspection of the air emission control equipment on or
    before the date that the surface impoundment becomes
    subject to this Section. Thereafter, the owner or
    operator shall perform the inspections at least once
    every year except for the special conditions provided
    for in subsection (g) below.
    D)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (f) below.
    E)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 724.989(c).
    e)
    The owner or operator shall transfer hazardous waste to a surface
    impoundment subject to this Section in accordance with the
    following requirements:
    1)
    Transfer of hazardous waste, except as provided in
    subsection (e)(2) below, to the surface impoundment from
    another surface impoundment subject to this Section or from
    a tank subject to Section 724.984 must be conducted using
    continuous hard-piping or another closed system that does
    not allow exposure of the waste to the atmosphere. For the
    purpose of complying with this provision, an individual
    drain system is considered to be a closed system when it
    meets the requirements of 40 CFR 63, Subpart RR, "National
    Emission Standards for Individual Drain Systems",
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The requirements of subsection (e)(1) above do not apply
    when transferring a hazardous waste to the surface
    impoundment under either of the following conditions:
    A)
    The hazardous waste meets the average VO concentration
    conditions specified in Section 724.982(c)(1) at the
    point of waste origination.
    B)
    The hazardous waste has been treated by an organic
    202
    destruction or removal process to meet the
    requirements in Section 724.982(c)(2).
    f)
    The owner or operator shall repair each defect detected during an
    inspection performed in accordance with the requirements of
    subsection (c)(3) or (d)(3) above as follows:
    1)
    The owner or operator shall make first efforts at repair of
    the defect no later than five calendar days after detection
    and repair must be completed as soon as possible but no
    later than 45 calendar days after detection except as
    provided in subsection (f)(2) below.
    2)
    Repair of a defect may be delayed beyond 45 calendar days if
    the owner or operator determines that repair of the defect
    requires emptying or temporary removal from service of the
    surface impoundment and no alternative capacity is available
    at the site to accept the hazardous waste normally managed
    in the surface impoundment. In this case, the owner or
    operator shall repair the defect the next time the process
    or unit that is generating the hazardous waste managed in
    the surface impoundment stops operation. Repair of the
    defect must be completed before the process or unit resumes
    operation.
    g)
    Following the initial inspection and monitoring of the cover as
    required by the applicable provisions of this Subpart, subsequent
    inspection and monitoring may be performed at intervals longer
    than one year in the case when inspecting or monitoring the cover
    would expose a worker to dangerous, hazardous, or other unsafe
    conditions. In this case, the owner or operator may designate the
    cover as an "unsafe to inspect and monitor cover" and comply with
    all of the following requirements:
    1)
    Prepare a written explanation for the cover stating the
    reasons why the cover is unsafe to visually inspect or to
    monitor, if required.
    2)
    Develop and implement a written plan and schedule to inspect
    and monitor the cover using the procedures specified in the
    applicable Section of this Subpart as frequently as
    practicable during those times when a worker can safely
    access the cover.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.986
    Standards: Containers
    a) This Section applies to the owners and operators of containers
    having design capacities greater than 0.1 m
    3
    (3.5 ft
    3
    or 26.4 gal)
    subject to this Subpart into which any hazardous waste is placed
    except for a container in which all hazardous waste entering the
    container meets the conditions specified in Section 724.982(c).
    b) An owner or operator shall manage hazardous waste in containers
    using the following procedures:
    1) The owner or operator shall place the hazardous waste into
    one of the following containers, except when a container is
    used for hazardous waste treatment as required by subsection
    (b)(2) below:
    203
    A) A container that is equipped with a cover which
    operates with no detectable organic emissions when all
    container openings (e.g., lids, bungs, hatches, and
    sampling ports) are secured in a closed, sealed
    position. The owner or operator shall determine that
    a container operates with no detectable emissions by
    testing each opening on the container for leaks in
    accordance with Method 21 in 40 CFR 60, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, the first time any portion of the hazardous
    waste is placed into the container. If a leak is
    detected and cannot be repaired immediately, the
    hazardous waste shall be removed from the container
    and the container not used to meet the requirements of
    this subsection until the leak is repaired and the
    container is retested.
    B) A container having a design capacity less than or
    equal to 0.46 m
    3
    (16.2 ft
    3
    or 122 gal) that is
    equipped with a cover and complies with all applicable
    Department of Transportation regulations on packaging
    hazardous waste for transport under 49 CFR 178,
    incorporated by reference at 35 Ill. Adm. Code
    720.111.
    i) A container that is managed in accordance with
    the requirements of 49 CFR 178, incorporated by
    reference at 35 Ill. Adm. Code 720.111, for the
    purpose of complying with this Subpart, is not
    subject to any exceptions to the 49 CFR 178
    regulations, except as noted in subsection
    (b)(1)(B)(ii) below.
    ii) A lab pack that is managed in accordance with
    the requirements of 49 CFR 178, incorporated by
    reference at 35 Ill. Adm. Code 720.111, for the
    purpose of complying with this Subpart, may
    comply with the exceptions for combination
    packagings specified in 49 CFR 173.12(b),
    incorporated by reference at 35 Ill. Adm. Code
    720.111.
    C) A container that is attached to or forms a part of any
    truck, trailer, or
    railcar and that has been
    demonstrated within the preceding 12 months to be
    organic vapor tight when all container openings are in
    a closed, sealed position (e.g., the container hatches
    or lids are gasketed and latched). For the purpose of
    meeting the requirements of this subsection, a
    container is organic vapor tight if the container
    sustains a pressure change of not more than 0.75
    kPa
    (0.11 psig or 5.6 mm Hg) within 5 minutes after it is
    pressurized to a minimum of 4.50
    kPa (0.65 psig or
    33.7 mm Hg). This condition is to be demonstrated
    using the pressure test specified in Method 27 of 40
    CFR 60, Appendix A, and a pressure measurement device
    which has a precision of ยฑ2.5 mm water and which is
    capable of measuring above the pressure at which the
    container is to be tested for vapor tightness.
    204
    2) An owner or operator treating hazardous waste in a container
    by either a waste stabilization process, any process that
    requires the addition of heat to the waste, or any process
    that produces an exothermic reaction shall meet the
    following requirements:
    A) Whenever it is necessary for the container to be open
    during the treatment process, the container shall be
    located inside an enclosure that is vented through a
    closed-vent system to a control device.
    B) The enclosure shall be a structure that is designed
    and operated in accordance with the following
    requirements:
    i) The enclosure shall be a structure that is
    designed and operated with sufficient airflow
    into the structure to capture the organic vapors
    emitted from the hazardous waste in the
    container and vent the vapors through the
    closed-vent system to the control device.
    ii) The enclosure may have permanent or temporary
    openings to allow worker access, passage of
    containers through the enclosure by conveyor or
    other mechanical means, entry of permanent
    mechanical or electrical equipment, or to direct
    airflow into the enclosure. The pressure drop
    across each opening in the enclosure shall be
    maintained at a pressure below atmospheric
    pressure so that whenever an open container is
    placed inside the enclosure no organic vapors
    released from the container exit the enclosure
    through the opening. The owner or operator
    shall determine that an enclosure achieves this
    condition by measuring the pressure drop across
    each opening in the enclosure. If the pressure
    within the enclosure is equal to or greater than
    atmospheric pressure then the enclosure does not
    meet the requirements of this Section.
    C) The closed-vent system and control device shall be
    designed and operated in accordance with the
    requirements of Section 724.987.
    3) An owner or operator transferring hazardous waste into a
    container having a design capacity greater than 0.46 m
    3
    (16.2 ft
    3
    or 122 gal) shall meet the following requirements:
    A) Hazardous waste transfer by pumping shall be performed
    using a conveyance system that uses a tube (e.g.,
    pipe, hose) to add the waste into the container.
    During transfer of the waste into the container, the
    cover shall remain in place and all container openings
    shall be maintained in a closed, sealed position
    except for those openings through which the tube
    enters the container and as provided for in subsection
    (c) below. The tube shall be positioned in a manner
    so that:
    i) The tube outlet continuously remains submerged
    205
    below the waste surface at all times waste is
    flowing through the tube;
    ii) The lower bottom edge of the tube outlet is
    located at a distance no greater than two inside
    diameters of the tube or 15.25 cm (6.0 in),
    whichever distance is greater, from the bottom
    of the container at all times waste is flowing
    through the tube; or
    iii) The tube is connected to a permanent port
    mounted on the bottom of the container so that
    the lower edge of the port opening inside the
    container is located at a distance equal to or
    less than 15.25 cm (6.0 in) from the container
    bottom.
    B) Hazardous waste transferred by a means other than
    pumping shall be performed such that during transfer
    of the waste into the container, the cover remains in
    place and all container openings are maintained in a
    closed, sealed position except for those openings
    through which the hazardous waste is added and as
    provided for in subsection (d) below.
    c) Each con tainer opening shall be maintained in a closed, sealed
    position (e.g., covered by a
    gasketed lid) at all times that
    hazardous waste is in the container except when it is necessary to
    use the opening to:
    1) Add, remove, inspect, or sample the material in the
    container;
    2) Inspect, maintain, repair, or replace equipment located
    inside the container; or
    3) Vent gases or vapors from a cover located over or enclosing
    an open container to a closed-vent system connected to a
    control device that is designed and operated in accordance
    with the requirements of Section 724.987.
    d) One or more safety devices that vent directly to the atmosphere
    may be used on the container, cover, enclosure, closed-vent
    system, or control device provided each device meets all of the
    following conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the container, cover, enclosure, or
    closed-vent system connected to a control device; and
    2) The safety device remains in a closed, s
    ealed position at
    all times except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the container, cover, enclosure,
    closed-vent system, or control device in accordance with
    good engineering and safety practices for handling
    flammable, combustible, explosive, or other hazardous
    materials. An example of an unplanned event is a sudden
    power outage.
    a)
    The provisions of this Section apply to the control of air
    206
    pollutant emissions from containers for which Section 724.982(b)
    references the use of this Section for such air emission control.
    b)
    General requirements.
    1)
    The owner or operator shall control air pollutant emissions
    from each container subject to this Section in accordance
    with the following requirements, as applicable to the
    container, except when the special provisions for waste
    stabilization processes specified in subsection (b)(2) below
    apply to the container.
    A)
    For a container having a design capacity greater than
    0.1 m
    3
    (26 gal) and less than or equal to 0.46 m
    3
    (120
    gal), the owner or operator shall control air
    pollutant emissions from the container in accordance
    with the Container Level 1 standards specified in
    subsection (c) below.
    B)
    For a container having a design capacity greater than
    0.46 m
    3
    (120 gal) that is not in light material
    service, the owner or operator shall control air
    pollutant emissions from the container in accordance
    with the Container Level 1 standards specified in
    subsection (c) below.
    C)
    For a container having a design capacity greater than
    0.46 m
    3
    (120 gal) that is in light material service,
    the owner or operator shall control air pollutant
    emissions from the container in accordance with the
    Container Level 2 standards specified in subsection
    (d) below.
    2)
    When a container having a design capacity greater than 0.1
    m
    3
    (26 gal) is used for treatment of a hazardous waste by a
    waste stabilization process, the owner or operator shall
    control air pollutant emissions from the container in
    accordance with the Container Level 3 standards specified in
    subsection (e) below at those times during the waste
    stabilization process when the hazardous waste in the
    container is exposed to the atmosphere.
    c)
    Container Level 1 standards.
    1)
    A container using Container Level 1 controls is one of the
    following:
    A)
    A container that meets the applicable U.S. Department
    of Transportation (USDOT) regulations on packaging
    hazardous materials for transportation, as specified
    in subsection (f) below.
    B)
    A container equipped with a cover and closure devices
    that form a continuous barrier over the container
    openings so that when the cover and closure devices
    are secured in the closed position there are no
    visible holes, gaps, or other open spaces into the
    interior of the container. The cover may be a
    separate cover installed on the container (e.g., a lid
    on a drum or a suitably secured tarp on a roll-off
    box) or may be an integral part of the container
    207
    structural design (e.g., a "portable tank" or bulk
    cargo container equipped with a screw
    -type cap).
    C)
    An open -top container in which an organic
    -vapor
    suppressing barrier is placed on or over the hazardous
    waste in the container such that no hazardous waste is
    exposed to the atmosphere. One example of such a
    barrier is application of a suitable organic
    -vapor
    suppressing foam.
    2)
    A container used to meet the requirements of subsection
    (c)(1)(B) or (c)(1)(C) above must be equipped with covers
    and closure devices, as applicable to the container, that
    are composed of suitable materials to minimize exposure of
    the hazardous waste to the atmosphere and to maintain the
    equipment integrity for as long as it is in service.
    Factors to be considered in selecting the materials of
    construction and designing the cover and closure devices
    must include the following: the organic vapor permeability;
    the effects of contact with the hazardous waste or its vapor
    managed in the container; the effects of outdoor exposure of
    the closure device or cover material to wind, moisture, and
    sunlight; and the operating practices for which the
    container is intended to be used.
    3)
    Whenever a hazardous waste is in a container using Container
    Level 1 controls, the owner or operator shall install all
    covers and closure devices for the container, as applicable
    to the container, and secure and maintain each closure
    device in the closed position except as follows:
    A)
    Opening of a closure device or cover is allowed for
    the purpose of adding hazardous waste or other
    material to the container as follows:
    i)
    In the case when the container is filled to the
    intended final level in one continuous
    operation, the owner or operator shall promptly
    secure the closure devices in the closed
    position and install the covers, as applicable
    to the container, upon conclusion of the filling
    operation.
    ii)
    In the case when discrete quantities or batches
    of material intermittently are added to the
    container over a period of time, the owner or
    operator shall promptly secure the closure
    devices in the closed position and install
    covers, as applicable to the container, upon
    either the container being filled to the
    intended final level; the completion of a batch
    loading after which no additional material will
    be added to the container within 15 minutes; the
    person performing the loading operation leaving
    the immediate vicinity of the container; or the
    shutdown of the process generating the material
    being added to the container, whichever
    condition occurs first.
    B)
    Opening of a closure device or cover is allowed for
    the purpose of removing hazardous waste from the
    208
    container as follows:
    i)
    For the purpose of meeting the requirements of
    this Section, an empty container, as defined in
    35 Ill. Adm. Code 721.107(b), may be open to the
    atmosphere at any time (i.e., covers and closure
    devices are not required to be secured in the
    closed position on an empty container).
    ii)
    In the case when discrete quantities or batches
    of material are removed from the container but
    the container does not meet the conditions to be
    an empty container as defined in 35 Ill. Adm.
    Code 721.107(b), the owner or operator shall
    promptly secure the closure devices in the
    closed position and install covers, as
    applicable to the container, upon the completion
    of a batch removal after which no additional
    material will be removed from the container
    within 15 minutes or the person performing the
    unloading operation leaves the immediate
    vicinity of the container, whichever condition
    occurs first.
    C)
    Opening of a closure device or cover is allowed when
    access inside the container is needed to perform
    routine activities other than transfer of hazardous
    waste. Examples of such activities include those
    times when a worker needs to open a port to measure
    the depth of or sample the material in the container,
    or when a worker needs to open a manhole hatch to
    access equipment inside the container. Following
    completion of the activity, the owner or operator
    shall promptly secure the closure device in the closed
    position or reinstall the cover, as applicable to the
    container.
    D)
    Opening of a spring
    -loaded pressure -vacuum relief
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the internal pressure of the container in
    accordance with the container design specifications.
    The device must be designed to operate with no
    detectable organic emissions when the device is
    secured in the closed position. The settings at which
    the device opens must be established such that the
    device remains in the closed position whenever the
    internal pressure of the container is within the
    internal pressure operating range determined by the
    owner or operator based on container manufacturer
    recommendations, applicable regulations, fire
    protection and prevention codes, standard engineering
    codes and practices, or other requirements for the
    safe handling of flammable, ignitable, explosive,
    reactive, or hazardous materials. Examples of normal
    operating conditions that may require these devices to
    open are during those times when the internal pressure
    of the container exceeds the internal pressure
    operating range for the container as a result of
    loading operations or diurnal ambient temperature
    209
    fluctuations.
    E)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    4)
    The owner or operator of containers using Container Level 1
    controls shall inspect the containers and their covers and
    closure devices as follows:
    A)
    In the case when a hazardous waste already is in the
    container at the time the owner or operator first
    accepts possession of the container at the facility
    and the container is not emptied (i.e., does not meet
    the conditions for an empty container as specified in
    35 Ill. Adm. Code 721.107(b)) within 24 hours after
    the container is accepted at the facility, the owner
    or operator shall visually inspect the container and
    its cover and closure devices to check for visible
    cracks, holes, gaps, or other open spaces into the
    interior of the container when the cover and closure
    devices are secured in the closed position. If a
    defect is detected, the owner or operator shall repair
    the defect in accordance with the requirements of
    subsection (c)(4)(C) below.
    B)
    In the case when a container used for managing
    hazardous waste remains at the facility for a period
    of one year or more, the owner or operator shall
    visually inspect the container and its cover and
    closure devices initially and thereafter, at least
    once every 12 months, to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (c)(4)(C) below.
    C)
    When a defect is detected for the container, cover, or
    closure devices, the owner or operator shall make
    first efforts at repair of the defect no later than 24
    hours after detection and repair must be completed as
    soon as possible but no later than five calendar days
    after detection. If repair of a defect cannot be
    completed within five calendar days, then the
    hazardous waste must be removed from the container and
    the container must not be used to manage hazardous
    waste until the defect is repaired.
    5)
    The owner or operator shall maintain at the facility a copy
    of the procedure used to determine that containers with
    capacity of 0.46 m
    3
    (120 gal) or greater, which do not meet
    applicable DOT regulations, as specified in subsection (f)
    below, are not managing hazardous waste in light material
    service.
    d)
    Container Level 2 standards.
    1)
    A container using Container Level 2 controls is one of the
    following:
    210
    A)
    A container that meets the applicable U.S. Department
    of Transportation (USDOT) regulations on packaging
    hazardous materials for transportation as specified in
    subsection (f) below.
    B)
    A container that operates with no detectable organic
    emissions, as defined in 35 Ill. Adm. Code 725.981,
    and determined in accordance with the procedure
    specified in subsection (g) below.
    C)
    A container that has been demonstrated within the
    preceding 12 months to be vapor
    -tight by using 40 CFR
    60, appendix A, Method 27, incorporated by reference
    in 35 Ill. Adm. Code 720.111, in accordance with the
    procedure specified in subsection (h) below.
    2)
    Transfer of hazardous waste in or out of a container using
    Container Level 2 controls must be conducted in such a
    manner as to minimize exposure of the hazardous waste to the
    atmosphere, to the extent practical, considering the
    physical properties of the hazardous waste and good
    engineering and safety practices for handling flammable,
    ignitable, explosive, reactive, or other hazardous
    materials. Examples of container loading procedures that
    the EPA considers to meet the requirements of this
    subsection include using any one of the following: a
    submerged -fill pipe or other sub
    merged -fill method to load
    liquids into the container; a vapor
    -balancing system or a
    vapor-recovery system to collect and control the vapors
    displaced from the container during filling operations; or a
    fitted opening in the top of a container through which the
    hazardous waste is filled and subsequently purging the
    transfer line before removing it from the container opening.
    3)
    Whenever a hazardous waste is in a container using Container
    Level 2 controls, the owner or operator shall install all
    covers and closure devices for the container, and secure and
    maintain each closure device in the closed position, except
    as follows:
    A)
    Opening of a closure device or cover is allowed for
    the purpose of adding hazardous waste or other
    material to the container as follows:
    i)
    In the case when the container is filled to the
    intended final level in one continuous
    operation, the owner or operator shall promptly
    secure the closure devices in the closed
    position and install the covers, as applicable
    to the container, upon conclusion of the filling
    operation.
    ii)
    In the case when discrete quantities or
    batches of material intermittently are
    added to the container over a period of
    time, the owner or operator shall promptly
    secure the closure devices in the closed
    position and install covers, as applicable
    to the container, upon either the
    container being filled to the intended
    211
    final level; the completion of a batch
    loading after which no additional material
    will be added to the container within 15
    minutes; the person performing the loading
    operation leaving the immediate vicinity
    of the container; or the shutdown of the
    process generating the material being
    added to the container, whichever
    condition occurs first.
    B)
    Opening of a closure device or cover is allowed for
    the purpose of removing hazardous waste from the
    container as follows:
    i)
    For the purpose of meeting the requirements of
    this Section, an empty container as defined in
    35 Ill. Adm. Code 721.107(b) may be open to the
    atmosphere at any time (i.e., covers and closure
    devices are not required to be secured in the
    closed position on an empty container).
    ii)
    In the case when discrete quantities or batches
    of material are removed from the container but
    the container does not meet the conditions to be
    an empty container as defined in 35 Ill. Adm.
    Code 721.107(b), the owner or operator shall
    promptly secure the closure devices in the
    closed position and install covers, as
    applicable to the container, upon the completion
    of a batch removal after which no additional
    material will be removed from the container
    within 15 minutes or the person performing the
    unloading operation leaves the immediate
    vicinity of the container, whichever condition
    occurs first.
    C)
    Opening of a closure device or cover is allowed when
    access inside the container is needed to perform
    routine activities other than transfer of hazardous
    waste. Examples of such activities include those
    times when a worker needs to open a port to measure
    the depth of or sample the material in the container,
    or when a worker needs to open a manhole hatch to
    access equipment inside the container. Following
    completion of the activity, the owner or operator
    shall promptly secure the closure device in the closed
    position or reinstall the cover, as applicable to the
    container.
    D)
    Opening of a spring
    -loaded, pressure
    -vacuum relief
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the internal pressure of the container in
    accordance with the container design specifications.
    The device must be designed to operate with no
    detectable organic emission when the device is secured
    in the closed position. The settings at which the
    device opens must be established such that the device
    remains in the closed position whenever the internal
    pressure of the container is within the internal
    212
    pressure operating range determined by the owner or
    operator based on container manufacturer
    recommendations, applicable regulations, fire
    protection and prevention codes, standard engineering
    codes and practices, or other requirements for the
    safe handling of flammable, ignitable, explosive,
    reactive, or hazardous materials. Examples of normal
    operating conditions that may require these devices to
    open are during those times when the internal pressure
    of the container exceeds the internal pressure
    operating range for the container as a result of
    loading operations or diurnal ambient temperature
    fluctuations.
    E)
    Opening of a safety device, as defined in 35 Ill. Adm.
    Code 725.981, is allowed at any time conditions
    require doing so to avoid an unsafe condition.
    4)
    The owner or operator of containers using Container Level 2
    controls shall inspect the containers and their covers and
    closure devices as follows:
    A)
    In the case when a hazardous waste already is in the
    container at the time the owner or operator first
    accepts possession of the container at the facility
    and the container is not emptied (i.e., does not meet
    the conditions for an empty container as specified in
    35 Ill. Adm. Code 721.107(b)) within 24 hours after
    the container arrives at the facility, the owner or
    operator shall visually inspect the container and its
    cover and closure devices to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (d)(4)(C) below.
    B)
    In the case when a container used for managing
    hazardous waste remains at the facility for a period
    of one year or more, the owner or operator shall
    visually inspect the container and its cover and
    closure devices initially and thereafter, at least
    once every 12 months, to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (d)(4)(C) below.
    C)
    When a defect is detected for the container, cover, or
    closure devices, the owner or operator shall make
    first efforts at repair of the defect no later than 24
    hours after detection, and repair must be completed as
    soon as possible but no later than five calendar days
    after detection. If repair of a defect cannot be
    completed within five calendar days, then the
    hazardous waste must be removed from the container and
    the container must not be used to manage hazardous
    waste until the defect is repaired.
    213
    e)
    Container Level 3 standards.
    1)
    A container using Container Level 3 controls is one of the
    following:
    A)
    A container that is vented directly through a
    closed -vent system to a control device in accordance
    with the requirements of subsection (e)(2)(B) below.
    B)
    A container that is vented inside an enclosure which
    is exhausted through a closed
    -vent system to a control
    device in accordance with the requirements of
    subsections (e)(2)(A) and (e)(2)(B) below.
    2)
    The owner or operator shall meet the following requirements,
    as applicable to the type of air emission control equipment
    selected by the owner or operator:
    A)
    The container enclosure must be designed and operated
    in accordance with the criteria for a permanent total
    enclosure as specified in "Procedure T
    --Criteria for
    and Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. The enclosure may have permanent or
    temporary openings to allow worker access; passage of
    containers through the enclosure by conveyor or other
    mechanical means; entry of permanent mechanical or
    electrical equipment; or direct airflow into the
    enclosure. The owner or operator shall perform the
    verification procedure for the enclosure as specified
    in Section 5.0 to "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" initially when the enclosure is first
    installed and, thereafter, annually.
    B)
    The closed -vent system and control device must be
    designed and operated in accordance with the
    requirements of Section 724.987.
    3)
    Safety devices, as defined in 35 Ill. Adm. Code 725.981, may
    be installed and operated as necessary on any container,
    enclosure, closed
    -vent system, or control device used to
    comply with the requirements of subsection (e)(1) above.
    4)
    Owners and operators using Container Level 3 controls in
    accordance with the provisions of this Subpart shall inspect
    and monitor the closed
    -vent systems and control devices as
    specified in Section 724.987.
    5)
    Owners and operators that use Container Level 3 controls in
    accordance with the provisions of this Subpart shall prepare
    and maintain the records specified in Section 724.989(d).
    f)
    For the purpose of compliance with subsection (c)(1)(i) or
    (d)(1)(A) above, containers must be used that meet the applicable
    U.S. Department of Transportation (DOT) regulations on packaging
    hazardous materials for transportation as follows:
    1)
    The container meets the applicable requirements specified in
    214
    49 CFR 178, "Specifications for Packaging", or 49 CFR 179,
    "Specifications for Tank Cars", both incorporated by
    reference in 35 Ill. Adm. Code 720.111.
    2)
    Hazardous waste is managed in the container in accordance
    with the applicable requirements specified in 49 CFR 107,
    Subpart B, "Exemptions"; 49 CFR 172, "Hazardous Materials
    Table, Special Provisions, Hazardous Materials
    Communications, Emergency Response Information, and Training
    Requirements"; 49 CFR 173, "
    Shippers --General Requirements
    for Shipments and Packages"; and 49 CFR 180, "Continuing
    Qualification and Maintenance of
    Packagings", each
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    3)
    For the purpose of complying with this Subpart, no
    exceptions to the 49 CFR 178 or 179 regulations are allowed,
    except as provided for in subsection (f)(4) below.
    4)
    For a lab pack that is managed in accordance with the
    requirements of 49 CFR 178, incorporated by reference in 35
    Ill. Adm. Code 720.111, for the purpose of complying with
    this Subpart, an owner or operator may comply with the
    exceptions for combination
    packagings specified in 49 CFR
    173.12(b).
    g)
    The owner or operator shall use the procedure specified in Section
    724.983(d) for determining a container operates with no detectable
    organic emissions for the purpose of complying with subsection
    (d)(1)(B) above.
    1)
    Each potential leak interface (i.e., a location where
    organic vapor leakage could occur) on the container, its
    cover, and associated closure devices, as applicable to the
    container, must be checked. Potential leak interfaces that
    are associated with containers include, but are not limited
    to the following: the interface of the cover rim and the
    container wall; the periphery of any opening on the
    container or container cover and its associated closure
    device; and the sealing seat interface on a spring
    -loaded
    pressure -relief valve.
    2)
    The test must be performed when the container is filled with
    a material having a volatile organic concentration
    representative of the range of volatile organic
    concentrations for the hazardous wastes expected to be
    managed in this type of container. During the test, the
    container cover and closure devices must be secured in the
    closed position.
    h)
    Procedure for determining a container to be vapor
    -tight using
    Method 27 of 40 CFR 60, appendix A for the purpose of complying
    with subsection (d)(1)(C) above.
    1)
    The test must be performed in accordance with Method 27 of
    40 CFR 60, appendix A, incorporated by reference in 35 Ill.
    Adm. Code 720.111.
    2)
    A pressure measurement device must be used that has a
    precision of ยฑ 2.5 mm (0.098 in) water and that is capable
    of measuring above the pressure at which the container is to
    be tested for vapor tightness.
    215
    3)
    If the test results determined by Method 27 indicate that
    the container sustains a pressure change less than or equal
    to 750 Pascals (0.11 psig) within five minutes after it is
    pressurized to a minimum of 4,500
    Pascals (0.65 psig), then
    the container is determined to be vapor
    -tight.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.987
    Standards: Closed-vent Systems and Control Devices
    a)
    This Section applies to each closed-vent system and control device
    installed and operated by the owner or operator to control air
    emissions in accordance with standards of this Subpart.
    b)
    The closed-vent system shall meet the following req
    uirements:
    1)
    The closed-vent system shall route the gases, vapors, and
    fumes emitted from the hazardous waste in the waste
    management unit to a control device that meets the
    requirements specified in subsection (c) below.
    2)
    The closed-vent system shall be designed and operated in
    accordance with the requirements specified in Section
    724.933(k).
    3) If the closed-vent system contains one or more bypass
    devices that could be used to divert all or a portion of the
    gases, vapors, or fumes from entering the control device,
    the owner or operator shall meet the following requirements:
    A) For each bypass device, except as provided for in
    subsection (b)(3)(B) below, the owner or operator
    shall either:
    i) Install, calibrate, maintain, and operate a flow
    indicator at the inlet to the bypass device that
    indicates at least once every 15 minutes whether
    gas, vapor, or fume flow is present in the
    bypass device; or
    ii) Secure a valve installed at the inlet to the
    bypass device in the closed position using a
    car-seal or a lock-and-key type configuration.
    The owner or operator shall visually inspect the
    seal or closure mechanism at least once every
    month to verify that the valve is maintained in
    the closed position.
    B) Low leg drains, high point bleeds, analyzer vents,
    open-ended valves or lines, and safety devices are not
    subject to the requirements of subsection (b)(3)(A)
    above.
    3)
    When the closed -vent system includes bypass devices that
    could be used to divert the gas or vapor stream to the
    atmosphere before entering the control device, each bypass
    device must be equipped with either a flow indicator, as
    specified in subsection (b)(3)(A) below, or a seal or
    locking device, as specified in subsection (b)(3)(B) below.
    For the purpose of complying with this subsection, low leg
    216
    drains, high point bleeds, analyzer vents, open
    -ended valves
    or lines, spring loaded pressure relief valves, and other
    fittings used for safety purposes are not considered to be
    bypass devices.
    A)
    If a flow indicator is used to comply with subsection
    (b)(3) above, the indicator must be installed at the
    inlet to the bypass line used to divert gases and
    vapors from the closed
    -vent system to the atmosphere
    at a point upstream of the control device inlet. For
    the purposes of this subsection, a flow indicator
    means a device that indicates the presence of either
    gas or vapor flow in the bypass line.
    B)
    If a seal or locking device is used to comply with
    subsection (b)(3) above, the device must be placed on
    the mechanism by which the bypass device position is
    controlled (e.g., valve handle or damper lever) when
    the bypass device is in the closed position such that
    the bypass device cannot be opened without breaking
    the seal or removing the lock. Examples of such
    devices include, but are not limited to, a car
    -seal or
    a lock -and-key configuration valve. The owner or
    operator shall visually inspect the seal or closure
    mechanism at least once every month to verify that the
    bypass mechanism is maintained in the closed position.
    4)
    The closed -vent system must be inspected and monitored by
    the owner or operator in accordance with the procedure
    specified in Section 724.933(l).
    c)
    The control device shall meet the following requirements:
    1)
    The control device shall be one of the following devices:
    A)
    A control device designed and operated to reduce the
    total organic content of the inlet vapor stream vented
    to the control device by at least 95 percent by
    weight;
    B)
    An enclosed combustion device designed and operated in
    accordance with the requirements of Section
    724.933(c); or
    C)
    A flare designed and operated in accordance with the
    requirements of Section 724.933(d).
    2) The control device shall be operating at all times when
    gases, vapors, or fumes are vented from the waste management
    unit through the closed-vent system to the control device.
    2)
    The owner or operator that elects to use a closed
    -vent
    system and control device to comply with the requirements of
    this Section shall comply with the requirements specified in
    subsections (c)(2)(A) through (c)(2)(F) below.
    A)
    Periods of planned routine maintenance of the control
    device, during which the control device does not meet
    the specifications of subsections (c)(1)(A),
    (c)(1)(B), or (c)(1)(C) above, as applicable, must not
    exceed 240 hours per year.
    217
    B)
    The specifications and requirements in subsections
    (c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
    devices do not apply during periods of planned routine
    maintenance.
    C)
    The specifications and requirements in subsections
    (c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
    devices do not apply during a control device system
    malfunction.
    D)
    The owner or operator shall demonstrate compliance
    with the requirements of subsection (c)(2)(A) above
    (i.e., planned routine maintenance of a control
    device, during which the control device does not meet
    the specifications of subsections (c)(1)(A),
    (c)(1)(B), or (c)(1)(C) above, as applicable, must not
    exceed 240 hours per year) by recording the
    information specified in Section 724.989(e)(1)(E).
    E)
    The owner or operator shall correct control device
    system malfunctions as soon as practicable after their
    occurrence in order to minimize excess emissions of
    air pollutants.
    F)
    The owner or operator shall operate the closed
    -vent
    system so that gases, vapors, or fumes are not
    actively vented to the control device during periods
    of planned maintenance or control device system
    malfunction (i.e., periods when the control device is
    not operating or not operating normally), except in
    cases when it is necessary to vent the gases, vapors,
    or fumes to avoid an unsafe condition or to implement
    malfunction corrective actions or planned maintenance
    actions.
    3)
    The owner or operator using a carbon adsorption system to
    comply with subsection (c)(1) above shall operate and
    maintain the control device in accordance with the following
    requirements:
    A)
    Following the initial startup of the control device,
    all activated carbon in the control device shall be
    replaced with fresh carbon on a regular basis in
    accordance with the requirements of Section 724.933(g)
    or Section 724.933(h).
    B)
    All carbon removed from the control device shall be
    managed in accordance with the requirements of Section
    724.933( mn).
    4)
    An owner or operator using a control device other than a
    thermal vapor incinerator, flare, boiler, process heater,
    condenser, or carbon adsorption system to comply with
    subsection (c)(1) above shall operate and maintain the
    control device in accordance with the requirements of
    Section 724.933(j).
    5)
    The owner or operator shall demonstrate that a control
    device achieves the performance requirements of subsection
    (c)(1) above, as follows:
    218
    A)
    An owner or operator shall demonstrate using either a
    performance test, as specified in subsection (c)(5)(C)
    below, or a design analysis, as specified in
    subsection (c)(5)(D) below, the performance of each
    control device except for the following:
    i)
    A flare;
    ii)
    A boiler or process heater with a design heat
    input capacity of 44 megawatts or greater;
    iii)
    A boiler or process heater into which the vent
    stream is introduced with the primary fuel;
    iv)
    A boiler or process heater industrial furnace
    burning hazardous waste for which the owner or
    operator has been issued a final permit under 35
    Ill. Adm. Code 702, 703, and 705 and designs has
    designed and operates the unit in accordance
    with the interim status requirements of 35 Ill.
    Adm. Code 726.Subpart H; or
    v)
    A boiler or process heater industrial furnace
    burning hazardous waste for which the owner or
    operator has certified compliance designed and
    operates in accordance
    with the interim status
    requirements of 35 Ill. Adm. Code 726.Subpart H.
    B)
    An owner or operator shall demonstrate the performance
    of each flare in accordance with the requirements
    specified in Section 724.933(e).
    C)
    For a performance test conducted to meet the
    requirements of subsection (c)(5)(A) above, the owner
    or operator shall use the test methods and procedures
    specified in Section 724.934(c)(1) through (c)(4).
    D)
    For a design analysis conducted to meet the
    requirements of subsection (c)(5)(A) above, the design
    analysis shall meet the requirements specified in
    Section 724.935(b)(4)(C).
    E)
    The owner or operator shall demonstrate that a carbon
    adsorption system achieves the performance
    requirements of subsection (c)(1) above based on the
    total quantity of
    organics vented to the atmosphere
    from all carbon adsorption system equipment that is
    used for organic adsorption, organic
    desorption or
    carbon regeneration, organic recovery, and carbon
    disposal.
    6)
    If the owner or operator and the Agency do not agree on a
    demonstration of control device performance using a design
    analysis then the disagreement shall be resolved using the
    results of a performance test performed by the owner or
    operator in accordance with the requirements of subsection
    (c)(5)(C) above. The Agency may choose to have an
    authorized representative observe the performance test.
    7)
    The control device must be inspected and monitored by the
    219
    owner or operator in accordance with the procedures
    specified in 35 Ill. Adm. Code 724.933(f)(2) and 35 Ill.
    Adm. Code 724.933(l). The readings from each monitoring
    device required by 35 Ill. Adm. Code 724.933(f)(2) must be
    inspected at least once each operating day to check control
    device operation. Any necessary corrective measures must be
    immediately implemented to ensure the control device is
    operated in compliance with the requirements of this
    Section.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.988
    Inspection and Monitoring Requirements
    a) This Section applies to an owner or operator using air emission
    controls in accordance with the requirements of Sections 724.984
    through 724.987.
    b) Each cover used in accordance with requirements of Section 724.984
    through 724.986 shall be visually inspected and monitored for
    detectable organic emissions by the owner or operator using the
    procedure specified in 35 Ill. Adm. Code 725.989(f)(1) through
    (f)(7), except as follows:
    1) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in 35 Ill.
    Adm. Code 725.989(f)(1) through (f)(7) for the following
    tank covers:
    A) A tank internal floating roof that is inspected and
    monitored in accordance with the requirements of
    Section 724.991; or
    B) A tank external floating roof that is inspected and
    monitored in accordance with the requirements of
    Section 724.991.
    2) If a tank is buried partia
    lly or entirely underground, an
    owner or operator is required to perform the cover
    inspection and monitoring requirements specified in 35 Ill.
    Adm. Code 725.989(f)(1) through (f)(7) only for those
    portions of the tank cover and those connections to the tank
    cover or tank body (e.g., fill ports, access hatches, gauge
    wells, etc.) that extend to or above the ground surface and
    can be opened to the atmosphere.
    3) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in 35 Ill.
    Adm. Code 725.989(f)(1) through (f)(7) for a container that
    meets all requirements specified in either Section
    724.986(b)(1)(B) or (b)(1)(C).
    4) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in 35 Ill.
    Adm. Code 725.989(f)(1) through (f)(7) for an enclosure used
    to control air emissions from containers in accordance with
    the requirements of Section 724.986(b)(2).
    c) Each closed-vent system used in accordance with the
    requirements
    of Section 724.987 shall be inspected and monitored by the owner
    or operator in accordance with the procedure specified in Section
    220
    724.933(k).
    d) Each control device used in accordance with the requirements of
    Section 724.987 shall be inspected and monitored by the owner or
    operator in accordance with the procedures specified in Sections
    724.933(f) (2) and 724.933(i). The readings from each monitoring
    device required by Section 724.933(f)(2) shall be inspected at
    least once each operating day to check control device operation.
    Any necessary corrective measures should be immediately
    implemented to ensure the control device is operated in compliance
    with the requirements of Section 264.987.
    e) The owner or operator shall develop and implement a written plan
    and schedule to perform all inspection and monitoring requirements
    of this section. The owner or operator shall incorporate this
    plan and schedule into the facility inspection plan required under
    Section 724.115.
    a)
    The owner or operator shall inspect and monitor air emission
    control equipment used to comply with this Subpart in accordance
    with the applicable requirements specified in Section 724.984
    through Section 724.987.
    b)
    The owner or operator shall develop and implement a written plan
    and schedule to perform the inspections and monitoring required by
    subsection (a) above. The owner or operator shall incorporate
    this plan and schedule into the facility inspection plan required
    under 35 Ill. Adm. Code 724.115.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.989
    Recordkeeping Requirements
    a) Each owner or operator of a facility subject to requirements in
    this Subpart shall record and maintain the following information
    as applicable:
    1) Documentation for each cover installed on a tank in
    accordance with the requirements of Section 724.984(b)(2) or
    (b)(3) that includes information prepared by the owner or
    operator or provided by the cover manufacturer or vendor
    describing the cover design, and certification by the owner
    or operator that the cover meets the applicable design
    specifications as listed in 35 Ill. Adm. Code 725.991(c).
    2) Documentation for each floating membrane cover installed on
    a surface impoundment in accordance with the requirements of
    Section 724.985(c) that includes information prepared by the
    owner or operator or provided by the cover manufacturer or
    vendor describing the cover design, and certification by the
    owner or operator that the cover meets the specifications
    listed in 35 Ill. Adm. Code 725.986(e).
    3) Documentation for each enclosure used to control air
    emissions from containers in accordance with the
    requirements of Section 724.986(b)(2)(A) that includes
    information prepared by the owner or operator or provided by
    the manufacturer or vendor describing the enclosure design,
    and certification by the owner or operator that the
    enclosure meets the specifications listed in Section
    724.986(b)(2)(B).
    221
    4) Documentation for each closed-vent system and control device
    installed in accordance with the requirements of Section
    724.987 that includes:
    A) Certification that is signed and dated by the owner or
    operator stating that the control device is designed
    to operate at the performance level documented by a
    design analysis as specified in subsection (a)(4)(B)
    below or by performance tests as specified in
    subsection (a)(4)(C) below when the tank, surface
    impoundment, or container is or would be operating at
    capacity or the highest level reasonably expected to
    occur.
    B) If a design analysis is used, then design
    documentation as specified in Section 724.935(b)(4).
    The documentation shall include information prepared
    by the owner or operator or provided by the control
    device manufacturer or vendor that describes the
    control device design in accordance with Section
    724.935(b)(4)(C) and certification by the owner or
    operator that the control equipment meets the
    applicable specifications.
    C) If performance tests are used, then a performance test
    plan as specified in Section 724.935(b)(3) and all
    test results.
    D) Information as required by Section 724.935(c)(1) and
    (c)(2).
    5) Records for all Method 27 tests performed by the owner or
    operator for each container used to meet the requirements of
    Section 724.986(b)(1)(C).
    6) Records for all visual inspections conducted in accordance
    with the requirements of Section 724.988.
    7) Records for all monitoring for detectable organic emissions
    conducted in accordance with the requirements of Section
    724.988.
    8) Records of the date of each attempt to repair a leak, repair
    methods applied, and the date of successful repair.
    9) Records for all continuous monitoring conducted in
    accordance with the requirements of Section 724.988.
    10) Records of the management of carbon removed from a carbon
    adsorption system conducted in accordance with Section
    724.987(c)(3)(B).
    11) Records for all inspections of each cover installed on a
    tank in accordance with the requirements of Section
    724.984(b)(2) or (b)(3) that includes information as listed
    in 35 Ill. Adm. Code 725.991(c).
    b) An owner or operator electing to use air emission controls for a
    tank in accordance with the conditions specified in Section
    724.984(c) shall record the following information:
    222
    1) Date and time each waste sample is collected for direct
    measurement of maximum organic vapor pressure in accordance
    with Section 724.983(c).
    2) Results of each determination of the maximum organic vapor
    pressure of the waste in a tank performed in accordance with
    Section 724.983(c).
    3) Records specifying the tank dimensions and design capacity.
    c) An owner or operator electing to use air emission controls for a
    tank in accordance with the requirements of Section 724.991 shall
    record the information required by Section 724.991(c).
    d) An owner or operator electing not to use air emission controls for
    a particular tank, surface impoundment, or container subject to
    this Subpart in accordance with the conditions specified in
    Section 724.982(c) shall record the information used by the owner
    or operator for each waste determination (e.g., test results,
    measurements, calculations, and other documentation) in the
    facility operating log. If analysis results for waste samples are
    used for the waste determination, then the owner or operator shall
    record the date, time, and location that each waste sample is
    collected in accordance with applicable requirements of Section
    724.983.
    e) An owner or operator electing to comply with requirements in
    accordance with Section 724.982(c)(2)(E) or Section
    724.982(c)(2)(F) shall record the identification number for the
    incinerator, boiler, or industrial furnace in which the hazardous
    waste is treated.
    f) An owner or operator designating a cover as unsafe to inspect and
    monitor pursuant to 35 Ill. Adm. Code 725.989(f)(5) or difficult
    to inspect and monitor pursuant to 35 Ill. Adm. Code 725.989(f)(6)
    shall record in a log that is kept in the facility operating
    record the following information:
    1) A list of identification numbers for tank
    s with covers that
    are designated as unsafe to inspect and monitor in
    accordance with the requirements of 35 Ill. Adm. Code
    725.989(f)(5), an explanation for each cover stating why the
    cover is unsafe to inspect and monitor, and the plan and
    schedule for inspecting and monitoring each cover.
    2) A list of identification numbers for tanks with covers that
    are designated as difficult to inspect and monitor in
    accordance with the requirements of 35 Ill. Adm. Code
    725.989(f)(6), an explanation for each cover stating why the
    cover is difficult to inspect and monitor, and the plan and
    schedule for inspecting and monitoring each cover.
    g) All records required by subsections (a) through (f) above, except
    as required in subsections (a)(1) through (a)(4), shall be
    maintained in the operating record for a minimum of 3 years. All
    records required by subsections (a)(1) through (a)(4) above shall
    be maintained in the operating record until the air emission
    control equipment is replaced or otherwise no longer in service.
    a)
    Each owner or operator of a facility subject to requirements in
    223
    this Subpart shall record and maintain the information specified
    in subsections (b) through (i) below, as applicable to the
    facility. Except for air emission control equipment design
    documentation and information required by subsection (i) below,
    records required by this Section must be maintained in the
    operating record for a minimum of three years. Air emission
    control equipment design documentation must be maintained in the
    operating record until the air emission control equipment is
    replaced or is otherwise no longer in service. Information
    required by subsection (i) below must be maintained in the
    operating record for as long as the tank or container is not using
    air emission controls specified in Sections 724.984 through
    724.987, in accordance with the conditions specified in Section
    724.984(d).
    b)
    The owner or operator of a tank using air emission controls in
    accordance with the requirements of Section 724.984 shall prepare
    and maintain records for the tank that include the following
    information:
    1)
    For each tank using air emission controls in accordance with
    the requirements of Section 724.984, the owner or operator
    shall record:
    A)
    A tank identification number (or other unique
    identification description as selected by the owner or
    operator).
    B)
    A record for each inspection required by Section
    724.984 that includes the following information:
    i)
    Date inspection was conducted.
    ii)
    For each defect detected during the inspection,
    the following information: the location of the
    defect, a description of the defect, the date of
    detection, and corrective action taken to repair
    the defect. In the event that repair of the
    defect is delayed in accordance with the
    provisions of Section 724.984, the owner or
    operator shall also record the reason for the
    delay and the date that completion of repair of
    the defect is expected.
    2)
    In addition to the information required by subsection (b)(1)
    above, the owner or operator shall record the following
    information, as applicable to the tank:
    A)
    The owner or operator using a fixed roof to comply
    with the Tank Level 1 control requirements specified
    in Section 724.984(c) shall prepare and maintain
    records for each determination for the maximum organic
    vapor pressure of the hazardous waste in the tank
    performed in accordance with the requirements of
    Section 724.984(c). The records must include the date
    and time the samples were collected, the analysis
    method used, and the analysis results.
    B)
    The owner or operator using an internal floating roof
    to comply with the Tank Level 2 control requirements
    specified in Section 724.984(e) shall prepare and
    224
    maintain documentation describing the floating roof
    design.
    C)
    Owners and operators using an external floating roof
    to comply with the Tank Level 2 control requirements
    specified in Section 724.984(f) shall prepare and
    maintain the following records:
    i)
    Documentation describing the floating roof
    design and the dimensions of the tank.
    ii)
    Records for each seal gap inspection required by
    Section 724.984(f)(3) describing the results of
    the seal gap measurements. The records must
    include the date that the measurements were
    performed, the raw data obtained for the
    measurements, and the calculations of the total
    gap surface area. In the event that the seal
    gap measurements do not conform to the
    specifications in Section 724.984(f)(1), the
    records must include a description of the
    repairs that were made, the date the repairs
    were made, and the date the tank was emptied, if
    necessary.
    D)
    Each owner or operator using an enclosure to comply
    with the Tank Level 2 control requirements specified
    in Section 724.984(i) shall prepare and maintain the
    following records:
    i)
    Records for the most recent set of calculations
    and measurements performed by the owner or
    operator to verify that the enclosure meets the
    criteria of a permanent total enclosure as
    specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    ii)
    Records required for the closed
    -vent system and
    control device in accordance with the
    requirements of subsection (e) below.
    c)
    The owner or operator of a surface impoundment using air emission
    controls in accordance with the requirements of Section 724.985
    shall prepare and maintain records for the surface impoundment
    that include the following information:
    1)
    A surface impoundment identification number (or other unique
    identification description as selected by the owner or
    operator).
    2)
    Documentation describing the floating membrane cover or
    cover design, as applicable to the surface impoundment, that
    includes information prepared by the owner or operator or
    provided by the cover manufacturer or vendor describing the
    cover design, and certification by the owner or operator
    that the cover meets the specifications listed in Section
    724.985(c).
    225
    3)
    A record for each inspection required by Section 724.985
    that includes the following information:
    A)
    Date inspection was conducted.
    B)
    For each defect detected during the inspection the
    following information: the location of the defect, a
    description of the defect, the date of detection, and
    corrective action taken to repair the defect. In the
    event that repair of the defect is delayed in
    accordance with the provisions of Section 724.985(f),
    the owner or operator shall also record the reason for
    the delay and the date that completion of repair of
    the defect is expected.
    4)
    For a surface impoundment equipped with a cover and vented
    through a closed -vent system to a control device, the owner
    or operator shall prepare and maintain the records specified
    in subsection (e).
    d)
    The owner or operator of containers using Container Level 3 air
    emission controls in accordance with the requirements of Section
    724.986 shall prepare and maintain records that include the
    following information:
    1)
    Records for the most recent set of calculations and
    measurements performed by the owner or operator to verify
    that the enclosure meets the criteria of a permanent total
    enclosure as specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total Enclosure"
    under 40 CFR 52.741, appendix B, incorporated by reference
    in 35 Ill. Adm. Code 720.111.
    2)
    Records required for the closed
    -vent system and control
    device in accordance with the requirements of subsection (e)
    below.
    e)
    The owner or operator using a closed
    -vent system and control
    device in accordance with the requirements of Section 724.987
    shall prepare and maintain records that include the following
    information:
    1)
    Documentation for the closed
    -vent system and control device
    that includes:
    A)
    Certification that is signed and dated by the owner or
    operator stating that the control device is designed
    to operate at the performance level documented by a
    design analysis as specified in subsection (e)(1)(B)
    of this Section or by performance tests as specified
    in subsection (e)(1)(C) below when the tank, surface
    impoundment, or container is or would be operating at
    capacity or the highest level reasonably expected to
    occur.
    B)
    If a design analysis is used, then design
    documentation, as specified in Section 724.935(b)(4).
    The documentation must include information prepared
    by the owner or operator or provided by the control
    device manufacturer or vendor that describes the
    control device design in accordance with Section
    226
    724.935(b)(4)(C) and certification by the owner or
    operator that the control equipment meets the
    applicable specifications.
    C)
    If performance tests are used, then a performance test
    plan as specified in Section 724.935(b)(3) and all
    test results.
    D)
    Information as required by Section 724.935(c)(1) and
    Section 724.935(c)(2), as applicable.
    E)
    An owner or operator shall record, on a semiannual
    basis, the information specified in subsections
    (e)(1)(E)(i) and (e)(1)(E)(ii) below for those planned
    routine maintenance operations that would require the
    control device not to meet the requirements of Section
    724.987(c)(1)(A), (c)(1)(B), or (c)(1)(C) above, as
    applicable.
    i)
    A description of the planned routine maintenance
    that is anticipated to be performed for the
    control device during the next six-month period.
    This description must include the type of
    maintenance necessary, planned frequency of
    maintenance, and lengths of maintenance periods.
    ii)
    A description of the planned routine maintenance
    that was performed for the control device during
    the previous six -month period. This description
    must include the type of maintenance performed
    and the total number of hours during those six
    months that the control device did not meet the
    requirements of Section 724.987(c)(1)(A),
    (c)(1)(B), or (c)(1)(C), as applicable, due to
    planned routine maintenance.
    F)
    An owner or operator shall record the information
    specified in subsections (e)(1)(F)(i) through
    (e)(1)(F)(iii) below for those unexpected control
    device system malfunctions that would require the
    control device not to meet the requirements of Section
    724.987 (c)(1)(A), (c)(1)(B), or (c)(1)(C) above, as
    applicable.
    i)
    The occurrence and duration of each malfunction
    of the control device system.
    ii)
    The duration of each period during a malfunction
    when gases, vapors, or fumes are vented from the
    waste management unit through the closed
    -vent
    system to the control device while the control
    device is not properly functioning.
    iii)
    Actions taken during periods of malfunction to
    restore a malfunctioning control device to its
    normal or usual manner of operation.
    G)
    Records of the management of carbon removed from a
    carbon adsorption system conducted in accordance with
    Section 724.987(c)(3)(B).
    227
    f)
    The owner or operator of a tank, surface impoundment, or container
    exempted from standards in accordance with the provisions of
    Section 724.982(c) shall prepare and maintain the following
    records, as applicable:
    1)
    For tanks, surface
    impoundments, or containers exempted
    under the hazardous waste organic concentration conditions
    specified in Section 724.982(c)(1) or (c)(2), the owner or
    operator shall record the information used for each waste
    determination (e.g., test results, measurements,
    calculations, and other documentation) in the facility
    operating log. If analysis results for waste samples are
    used for the waste determination, then the owner or operator
    shall record the date, time, and location that each waste
    sample is collected in accordance with applicable
    requirements of Section 724.983.
    2)
    For tanks, surface
    impoundments, or containers exempted
    under the provisions of Section 724.982(c)(2)(G) or Section
    724.982(c)(2)(H), the owner or operator shall record the
    identification number for the incinerator, boiler, or
    industrial furnace in which the hazardous waste is treated.
    g)
    An owner or operator designating a cover as "unsafe to inspect and
    monitor" pursuant to Section 724.984(l) or Section 724.985(g)
    shall record in a log that is kept in the facility operating
    record the following information: the identification numbers for
    waste management units with covers that are designated as "unsafe
    to inspect and monitor", the explanation for each cover stating
    why the cover is unsafe to inspect and monitor, and the plan and
    schedule for inspecting and monitoring each cover.
    h)
    The owner or operator of a facility that is subject to this
    Subpart and to the control device standards in 40 CFR 60, Subpart
    VV or 40 CFR 61, Subpart V, incorporated by reference in 35 Ill.
    Adm. Code 720.111, may elect to demonstrate compliance with the
    applicable Sections of this Subpart by documentation either
    pursuant to this Subpart, or pursuant to the provisions of 40 CFR
    60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
    documentation required by 40 CFR 60 or 61 duplicates the
    documentation required by this Section.
    i)
    For each tank or container not using air emission controls
    specified in Sections 724.984 through 724.987 in accordance with
    the conditions specified in Section 724.980(d), the owner or
    operator shall record and maintain the following information:
    1)
    A list of the individual organic peroxide compounds
    manufactured at the facility that meet the conditions
    specified in Section 724.980(d)(1).
    2)
    A description of how the hazardous waste containing the
    organic peroxide compounds identified pursuant to subsection
    (i)(1) above are managed at the facility in tanks and
    containers. This description must include the following
    information:
    A)
    For the tanks used at the facility to ma
    nage this
    hazardous waste, sufficient information must be
    provided to describe
    the following for
    each tank: a
    facility identification number for the tank, the
    228
    purpose and placement of this tank in the management
    train of this hazardous waste, and the procedures used
    to ultimately dispose of the hazardous waste managed
    in the tanks.
    B)
    For containers used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to describe each tank: a facility
    identification number for the container or group of
    containers, the purpose and placement of this
    container or group of containers in the management
    train of this hazardous waste, and the procedures used
    to ultimately dispose of the hazardous waste managed
    in the containers.
    3)
    An explanation of why managing the hazardous waste
    containing the organic peroxide compounds identified
    pursuant to subsection (i)(1) above in the tanks or
    containers identified pursuant to subsection (i)(2) above
    would create an undue safety hazard if the air emission
    controls specified in Sections 724.984 through 724.987 were
    installed and operated on these waste management units.
    This explanation must include the following information:
    A)
    For tanks used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to explain
    the following : how use of
    the required air emission controls on the tanks
    would affect the tank design features and
    facility operating procedures currently used to
    prevent an undue safety hazard during management
    of this hazardous waste in the tanks; and why
    installation of safety devices on the required
    air emission controls, as allowed under
    Section
    724.984(g) this Subpart , would not address those
    situations in which evacuation of tanks equipped
    with these air emission controls is necessary
    and consistent with good engineering and safety
    practices for handling organic peroxides.
    B)
    For containers used at the facility to manage
    this hazardous waste, sufficient information
    must be provided to explain
    the following : how
    use of the required air emission controls on the
    tanks would affect the container design features
    and handling procedures currently used to
    prevent an undue safety hazard during management
    of this hazardous waste in the containers; and
    why installation of safety devices on the
    required air emission controls, as allowed under
    Section 724.986(d)
    this Subpart , would not
    address those situations in which evacuation of
    containers equipped with these air emission
    controls is necessary and consistent with good
    engineering and safety practices for handling
    organic peroxides.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.990
    Reporting Requirements
    229
    a)
    Each owner or operator managing hazardous waste in a tank, surface
    impoundment, or container exempted from using air emission
    controls under the provisions of Section 724.982(c) shall report
    to the Agency each occurrence when hazardous waste is placed in
    the waste management unit in noncompliance with the conditions
    specified in Section 724.982(c)(1) or (c)(2), as applicable.
    Examples of such occurrences include placing in the waste
    management unit a hazardous waste having an average VO
    concentration equal to or greater than
    100500 ppmw at the point of
    waste origination or placing in the waste management unit a
    treated hazardous waste that fails to meet the applicable
    conditions specified in Section 724.982(c)(2)(A) through
    (c)(2)( EF). The owner or operator shall submit a written report
    within 15 calendar days of the time that the owner or operator
    becomes aware of the occurrence. The written report shall contain
    the U.S. EPA identification number, the facility name and address,
    a description of the noncompliance event and the cause, the dates
    of the noncompliance, and the actions taken to correct the
    noncompliance and prevent re
    occurrence of the noncompliance. The
    report shall be signed and dated by an authorized representative
    of the owner or operator.
    b)
    Each owner or operator using air emission contro
    ls on a tank in
    accordance with the requirements Section 724.984(c) shall report
    to the Agency each occurrence when hazardous waste is managed in
    the tank in noncompliance with the conditions specified in Section
    724.984 (c)(1) through (c)(4)
    (b). The owner or operator shall
    submit a written report within 15 calendar days of the time that
    the owner or operator becomes aware of the occurrence. The
    written report shall contain the U
    .S. EPA identification number,
    the facility name and address, a description of the noncompliance
    event and the cause, the dates of the noncompliance, and the
    actions taken to correct the noncompliance and prevent
    reoccurrence of the noncompliance. The report shall be signed and
    dated by an authorized representative of the owner or operator.
    c)
    Each owner or operator using a control device in accordance with
    the requirements of Section 724.987 shall submit a semiannual
    written report to the Agency excepted as provided for in
    subsection (d) below. The report shall describe each occurrence
    during the previous 6-month period when
    either of the two
    following events occurs:
    a control device is operated
    continuously for 24 hours or longer in noncompliance with the
    applicable operating values defined in Section 724.935(c)(4) or
    when a flare is operated with visible emissions
    for five minutes
    or longer in a two-hour period,
    as defined in Section 724.933(d).
    The written report shall include the U. S. EPA identification
    number, the facility name and address, and an explanation why the
    control device could not be returned to compliance within 24
    hours, and actions taken to correct the noncompliance. The report
    shall be signed and dated by an authorized representative of the
    owner or operator.
    d)
    A report to the Agency in accordance with the requirements of
    subsection (c) above is not required for a 6-month period during
    which all control devices subject to this Subpart are operated by
    the owner or operator so that both of the following conditions
    result: during no period of 24 hours or longer did a control
    device operate continuously in noncompliance with the applicable
    operating values defined in Section 724.935(c)(4)
    orand ano flare
    was operate d with visible emissions
    for five minutes or longer in
    230
    a two-hour period
    , as defined in Section 724.933(d).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 724.991
    Alternative Control Requirements for Tanks
    (Repealed)
    a) This Section applies to owners and operators of tanks that elect
    to comply with Section 724.984(b)(2) or Section 724.984(b)(3).
    1) The owner or operator that elects to comply with Section
    724.984(b)(2) shall design, install, operate, and maintain a
    fixed roof and internal floating roof that meet the
    requirements specified in 35 Ill. Adm. Code 725.991(a)(1)(A)
    through (a)(1)(I).
    2) The owner or operator that elects to comply with Section
    724.984(b)(3) shall design, install, operate, and maintain
    an external floating roof that meets the requirements
    specified in 35 Ill. Adm. Code 725.991(a)(2)(A) through
    (a)(2)(C).
    3) The owner or operator may elect to comply with Section
    264.984(b)(2) or (b)(3) using an alternative means of
    emission limitation as specified in 35 Ill. Adm. Code
    725.991(a)(3).
    b) The owner or operator shall inspect and monitor the control
    equipment in accordance with the following requirements:
    1) For a tank equipped with a fixed roof and internal floating
    roof in accordance with the requirements of subsection
    (a)(1) above, the owner or operator shall perform the
    inspection and monitoring requirements specified in 35 Ill.
    Adm. Code 725.991(b)(1).
    2) For a tank equipped with an external floating roof in
    accordance with the requirements of subsection (a)(2) above,
    the owner or operator shall perform the inspection and
    monitoring requirements specified in 35 Ill. Adm. Code
    725.991(b)(2).
    c) The owner or operator shall record the following information in
    the operating record in accordance with the requirements of
    Section 724.989(a)(1) and (a)(11):
    1) For a tank equipp
    ed with a fixed roof and internal floating
    roof in accordance with the requirements of subsection
    (a)(1) above, the owner or operator shall record the
    information listed in 35 Ill. Adm. Code 725.991(c)(1).
    2) For a tank equipped with an external floating roof in
    accordance with the requirements of subsection (a)(1) above,
    the owner or operator shall record the information listed in
    35 Ill. Adm. Code 725.991(c)(2).
    (Source: R
    epealed at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    231
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 725
    INTERIM STATUS STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS
    WASTE TREATMENT, STORAGE, AND DISPOSAL FACILITIES
    SUBPART A: GENERAL PROVISIONS
    Section
    725.101
    Purpose, Scope and Applicability
    725.104
    Imminent Hazard Action
    SUBPART B: GENERAL FACILITY STANDARDS
    Section
    725.110
    Applicability
    725.111
    USEPA Identification Number
    725.112
    Required N otices
    725.113
    General Waste Analysis
    725.114
    Security
    725.115
    General Inspection Requirements
    725.116
    Personnel Training
    725.117
    General Requirements for Ignitable, Reactive, or Incompatible
    Wastes
    725.118
    Location Standards
    725.119
    Construction Quality Assurance Program
    SUBPART C: PREPAREDNESS AND PREVENTION
    Section
    725.130
    Applicability
    725.131
    Maintenance and Operation of Facility
    725.132
    Required Equipment
    725.133
    Testing and Maintenance of Equipment
    725.134
    Access to Communications or Alarm System
    725.135
    Required Aisle Space
    725.137
    Arrangements with Local Authorities
    SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
    Section
    725.150
    Applicability
    725.151
    Purpose and Implementation of Contingency Plan
    725.152
    Content of Contingency Plan
    725.153
    Copies of Contingency Plan
    725.154
    Amendment of Contingency Plan
    725.155
    Emergency Coordinator
    725.156
    Emergency Procedures
    SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
    Section
    725.170
    Applicability
    725.171
    Use of Manifest System
    725.172
    Manifest Discrepancies
    725.173
    Operating Record
    725.174
    Availability, Retention and Disposition of Records
    725.175
    Annual Report
    725.176
    Unmanifested Waste Report
    725.177
    Additional Reports
    SUBPART F: GROUNDWATER MONITORING
    Section
    725.190
    Applicability
    725.191
    Groundwater Monitoring System
    725.192
    Sampling and Analysis
    232
    725.193
    Preparation, Evaluation and Response
    725.194
    Recordkeeping and Reporting
    SUBPART G: CLOSURE AND POST-CLOSURE
    Section
    725.210
    Applicability
    725.211
    Closure Performance Standard
    725.212
    Closure Plan; Amendment of Plan
    725.213
    Closure; Time Allowed for Closure
    725.214
    Disposal or Decontamination of Equipment, Structures and Soils
    725.215
    Certification of Closure
    725.216
    Survey Plat
    725.217
    Post-closure Care and Use of Property
    725.218
    Post-closure Plan; Amendment of Plan
    725.219
    Post-Closure Notices
    725.220
    Certification of Completion of Post-Closure Care
    SUBPART H: FINANCIAL REQUIREMENTS
    Section
    725.240
    Applicability
    725.241
    Definitions of Terms as Used in this Subpart
    725.242
    Cost Estimate for Closure
    725.243
    Financial Assurance for Closure
    725.244
    Cost Estimate for Post-closure Care
    725.245
    Financial Assurance for Post-closure Monitoring and Maintenance
    725.246
    Use of a Mechanism for Financial Assurance of Both Closure and
    Post-closure Care
    725.247
    Liability Requirements
    725.248
    Incapacity of Owners or Operators, Guarantors or Financial
    Institutions
    725.251
    Promulgation of Forms (Repealed)
    SUBPART I: USE AND MANAGEMENT OF CONTAINERS
    Section
    725.270
    Applicability
    725.271
    Conditi on of Containers
    725.272
    Compatibility of Waste with Container
    725.273
    Management of Containers
    725.274
    Inspections
    725.276
    Special Requirements for Ignitable or Reactive Waste
    725.277
    Special Requirements for Incompatible Wastes
    725.278
    Air Emission Standards
    SUBPART J: TANK SYSTEMS
    Section
    725.290
    Applicability
    725.291
    Assessment of Existing Tank System's Integrity
    725.292
    Design and Installation of New Tank Systems or Components
    725.293
    Containment and Detection of Releases
    725.294
    General Operating R
    equirements
    725.295
    Inspections
    725.296
    Response to leaks or spills and disposition of Tank Systems
    725.297
    Closure and Post-Closure Care
    725.298
    Special Requirements for Ignitable or Reactive Waste
    725.299
    Special Requirements for Incompatible Wastes
    725.300
    Waste Analysis and Trial Tests
    725.301
    Generators of 100 to 1000 kg/mo
    725.302
    Air Emission Standards
    SUBPART K: SURFACE IMPOUNDMENTS
    Section
    233
    725.320
    Applicability
    725.321
    Design and Operating Requirements
    725.322
    Action Leakage Rate
    725.323
    Respons e Actions
    725.324
    Containment System
    725.325
    Waste Analysis and Trial Tests
    725.326
    Monitoring and Inspections
    725.328
    Closure and Post-Closure Care
    725.329
    Special Requirements for Ignitable or Reactive Waste
    725.330
    Special Requirements for Incompatible Wastes
    725.331
    Air Emission Standards
    SUBPART L: WASTE PILES
    Section
    725.350
    Applicability
    725.351
    Protection from Wind
    725.352
    Waste Analysis
    725.353
    Containment
    725.354
    Design and Operating Requirements
    725.355
    Action Leakage Rates
    725.356
    Special Re quirements for Ignitable or Reactive Waste
    725.357
    Special Requirements for Incompatible Wastes
    725.358
    Closure and Post-Closure Care
    725.359
    Response Actions
    725.360
    Monitoring and Inspection
    SUBPART M: LAND TREATMENT
    Section
    725.370
    Applicability
    725.372
    General Operating Requirements
    725.373
    Waste Analysis
    725.376
    Food Chain Crops
    725.378
    Unsaturated Zone (Zone of Aeration) Monitoring
    725.379
    Recordkeeping
    725.380
    Closure and Post-closure
    725.381
    Special Requirements for Ignitable or Reactive Waste
    725.382
    Special Requirements for Incompatible Wastes
    SUBPART N: LANDFILLS
    Section
    725.400
    Applicability
    725.401
    Design Requirements
    725.402
    Action Leakage Rate
    725.403
    Response Actions
    725.404
    Monitoring and Inspection
    725.409
    Surveying and Recordkeeping
    725.410
    Closure and Post-Closure
    725.412
    Special Requirements for Ignitable or Reactive Waste
    725.413
    Special Requirements for Incompatible Wastes
    725.414
    Special Requirements for Liquid Wastes
    725.415
    Special Requirements for Containers
    725.416
    Disposal o f Small Containers of Hazardous Waste in
    Overpacked
    Drums (Lab Packs)
    SUBPART O: INCINERATORS
    Section
    725.440
    Applicability
    725.441
    Waste Analysis
    725.445
    General Operating Requirements
    725.447
    Monitoring and Inspection
    725.451
    Closure
    234
    725.452
    Interim Status Incinerators Burning Particular Hazardous Wastes
    SUBPART P: THERMAL TREATMENT
    Section
    725.470
    Other Thermal Treatment
    725.473
    General Operating Requirements
    725.475
    Waste Analysis
    725.477
    Monitoring and Inspections
    725.481
    Closure
    725.482
    Open Bur ning; Waste Explosives
    725.483
    Interim Status Thermal Treatment Devices Burning Particular
    Hazardous Waste
    SUBPART Q: CHEMICAL, PHYSICAL AND BIOLOGICAL TREATMENT
    Section
    725.500
    Applicability
    725.501
    General Operating Requirements
    725.502
    Waste Analysis and Trial Tests
    725.503
    Inspections
    725.504
    Closure
    725.505
    Special Requirements for Ignitable or Reactive Waste
    725.506
    Special Requirements for Incompatible Wastes
    SUBPART R: UNDERGROUND INJECTION
    Section
    725.530
    Applicability
    SUBPART W: DRIP PADS
    Section
    725.540
    Applicability
    725.541
    Assessment of existing drip pad integrity
    725.542
    Design and installation of new drip pads
    725.543
    Design and operating requirements
    725.544
    Inspections
    725.545
    Closure
    SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
    Section
    725.930
    Applicability
    725.931
    Definitions
    725.932
    Standards: Process Vents
    725.933
    Standards: Closed-vent Systems and Control Devices
    725.934
    Test methods and procedures
    725.935
    Recordkeeping Requirements
    SUBPART BB: AIR EMISSION STAND
    ARDS FOR EQUIPMENT LEAKS
    Section
    725.950
    Applicability
    725.951
    Definitions
    725.952
    Standards: Pumps in Light Liquid Service
    725.953
    Standards: Compressors
    725.954
    Standards: Pressure Relief Devices in Gas/Vapor Service
    725.955
    Standards: Sampling Connecting Systems
    725.956
    Standards: Open-ended Valves or Lines
    725.957
    Standards: Valves in Gas/Vapor or Light Liquid Service
    725.958
    Standards: Pumps, Valves, Pressure Relief Devices, Flanges and
    Other Connectors
    725.959
    Standards: Delay of Repair
    725.960
    Standards: Closed-vent Systems and Control Devices
    725.961
    Percent Leakage Alternative for Valves
    725.962
    Skip Period Alternative for Valves
    235
    725.963
    Test Methods and Procedures
    725.964
    Recordkeeping Requirements
    SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
    SURFACE IMPOUNDMENTS, AND CONTAINERS
    Section
    725.980
    Applicability
    725.981
    Definitions
    725.982
    Schedule for Implementation of Air Emission Standards
    725.983
    Standards: General
    725.984
    Waste Determination Procedures
    725.985
    Standards: Tanks
    725.986
    Standards: Surface
    Impoundments
    725.987
    Standards: Containers
    725.988
    Standards: Closed-vent Systems and Control Devices
    725.989
    Inspection and Monitoring Requirements
    725.990
    Recordkeeping Requirements
    725.991
    Alternative Tank Emission Control Requirements
    (Repealed)
    SUBPART DD: CONTAINMENT BUILDINGS
    Section
    725.1100
    Applicability
    725.1101
    Design and operating standards
    725.1102
    Closure and Post Closure-Care
    725.Appendix A
    Recordkeeping Instructions
    725.Appendix B
    EPA Report Form and Instructions
    (Repealed)
    725.Appendix C
    EPA Interim Primary Drinking Water Standards
    725.Appendix D
    Tests for Significance
    725.Appendix E
    Examples of Potentially Incompatible Waste
    725.Appendix F
    Compounds With Henry's Law Constant Less Than 0.1 Y/X (at
    25
    ยฐ
    C)
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
    1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
    effective May 17, 1982; amended in R82-18, 51 PCB 831, at 7 Ill. Reg. 2518,
    effective February 22, 1983; amended in R82-19, 53 PCB 131, at 7 Ill. Reg.
    14034, effective October 12, 1983; amended in R84-9, at 9 Ill. Reg. 11869,
    effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1085, effective
    January 2, 1986; amended in R86-1 at 10 Ill. Reg. 14069, effective August 12,
    1986; amended in R86-28 at 11 Ill. Reg. 6044, effective March 24, 1987;
    amended in R86-46 at 11 Ill. Reg. 13489, effective August 4, 1987; amended in
    R87-5 at 11 Ill. Reg. 19338, effective November 10, 1987; amended in R87-26 at
    12 Ill. Reg. 2485, effective January 15, 1988; amended in R87-39 at 12 Ill.
    Reg. 13027, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 437,
    effective December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18354, effective
    November 13, 1989; amended in R90-2 at 14 Ill. Reg. 14447, effective August
    22, 1990; amended in R90-10 at 14 Ill. Reg. 16498, effective September 25,
    1990; amended in R90-11 at 15 Ill. Reg. 9398, effective June 17, 1991; amended
    in R91-1 at 15 Ill. Reg. 14534, effective October 1, 1991; amended in R91-13
    at 16 Ill. Reg. 9578, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg.
    17672, effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5681,
    effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20620, effective
    November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6771, effective April 26,
    1994; amended in R94-7 at 18 Ill. Reg. 12190, effective July 29, 1994; amended
    in R94-17 at 18 Ill. Reg. 17548, effective November 23, 1994; amended in R95-6
    at 19 Ill. Reg. 9566, effective June 27, 1995; amended in R95-20 at 20 Ill.
    Reg. 11078, August 1, 1996
    ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
    236
    ________, effective ____________________
    .
    SUBPART B: GENERAL FACILITY STANDARDS
    Section 725.112
    Required Notices
    a)
    Receipt from a foreign source.
    1)
    The owner or operator of a facility that has arranged to
    receive hazardous waste from a foreign source must notify
    the Regional Administrator in writing at least four weeks in
    advance of the date the waste is expected to arrive at the
    facility. Notice of subsequent shipments of the same waste
    from the same foreign source is not required.
    2)
    The owner or operator of a recovery facility that has
    arranged to receive hazardous waste subject to 35 Ill. Adm.
    Code 722.Subpart H must provide a copy of the tracking
    document bearing all required signatures to the
    notifier, to
    the Office of Enforcement and Compliance Assurance, Office
    of Compliance, Enforcement Planning, Targeting and Data
    Division (2222A), Environmental Protection Agency, 401 M
    St., SW., Washington, DC 20460; to the Bureau of Land,
    Division of Land Pollution Control, Illinois Environmental
    Protection Agency,
    P.O. Box 19276, Springfield, IL 62794-
    9276; and to the competent authorities of all other
    concerned countries within three working days of receipt of
    the shipment. The original of the signed tracking document
    must be maintained at the facility for at least three years.
    b)
    Before transferring ownership or operation of a facility during
    its operating life, or of a disposal facility during the
    post-closure care period, the owner or operator must notify the
    new owner or operator in writing of the requirements of this Part
    and 35 Ill. Adm. Code 702 and 703 (Also see 40 35 Ill. Adm. Code
    703.155.
    BOARD NOTE: An owner's or operator's failure to notify the new
    owner or operator of the requirements of this Part in no way
    relieves the new owner or operator of his obligation to comply
    with all applicable requirements.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.113
    General Waste Analysis
    a)
    Waste analysis:
    1)
    Before an owner or operator treats, stores, or disposes of
    any hazardous wastes, or non-hazardous wastes if applicable
    under Section 725.213(d), the owner or operator shall obtain
    a detailed chemical and physical analysis of a
    representative sample of the wastes. At a minimum, the
    analysis must contain all the information that must be known
    to treat, store, or dispose of the waste in accordance with
    this Part and 35 Ill. Adm. Code 728.
    2)
    The analysis may include data developed under 35 Ill. Adm.
    Code 721 and existing published or documented data on the
    hazardous waste or on waste generated from similar
    237
    processes.
    BOARD NOTE: For example, the facility's record of analyses
    performed on the waste before the effective date of these
    regulations or studies conducted on hazardous waste
    generated from processes similar to that which generated the
    waste to be managed at the facility may be included in the
    data base required to comply with subsection (a)(1) above,
    except as otherwise specified in 35 Ill. Adm. Code
    728.107(b) and (c). The owner or operator of an off-site
    facility may arrange for the generator of the hazardous
    waste to supply part or all of the information required by
    subsection (a)(1) above. If the generator does not supply
    the information and the owner or operator chooses to accept
    a hazardous waste, the owner or operator is responsible for
    obtaining the information required to comply with this
    Section.
    3)
    The analysis must be repeated as necessary to ensure that it
    is accurate and up to date. At a minimum, the analysis must
    be repeated:
    A)
    When the owner or operator is notified or has reason
    to believe that the process or operation generating
    the hazardous waste, or non-hazardous waste if
    applicable under Section 725.213(d), has changed; and
    B)
    For off-site facilities, when the
    results of the
    inspection required in subsection (a)(4) below
    indicate that the hazardous waste received at the
    facility does not match the waste designated on the
    accompanying manifest or shipping paper.
    4)
    The owner or operator of an off-site facility shall inspect
    and, if necessary, analyze each hazardous waste movement
    received at the facility to determine whether it matches the
    identity of the waste specified on the accompanying manifest
    or shipping paper.
    b)
    The owner or operator shall develop a
    nd follow a written waste
    analysis plan that describes the procedures that the owner or
    operator will carry out to comply with subsection (a) above. The
    owner or operator shall keep this plan at the facility. At a
    minimum, the plan must specify:
    1)
    The parameters for which each hazardous waste, or non-
    hazardous waste if applicable under Section 725.213(d), will
    be analyzed and the rationale for the selection of these
    parameters (i.e., how analysis for these parameters will
    provide sufficient information on the waste's properties to
    comply with subsection (a) above.
    2)
    The test methods that will be used to test for these
    parameters.
    3)
    The sampling method that will be used to obtain a
    representative sample of the waste to be analyzed. A
    representative sample may be obtained using either:
    A)
    One of the sampling methods described in 35 Ill. Adm.
    Code 721.Appendix A, or
    238
    B)
    An equivalent sampling method.
    BOARD NOTE: See 35 Ill. Adm. Code 720.120(c) for
    related discussion.
    4)
    The freque ncy with which the initial analysis of the waste
    will be reviewed or repeated to ensure that the analysis is
    accurate and up-to-date.
    5)
    For off-site facilities, the waste analyses that hazardous
    waste generators have agreed to supply.
    6)
    Where applicable, the methods that will be used to meet the
    additional waste analysis requirements for specific waste
    management methods, as specified in Sections 725.300,
    725.325, 725.352, 725.373, 725.414, 725.441, 725.475,
    725.502, 725.934(d), 725.963(d), and 725.984, and 35 Ill.
    Adm. Code 728.107.
    7)
    For surface impoundments exempted from land disposal
    restrictions under 35 Ill. Adm. Code 728.104(a), the
    procedures and schedules for:
    A)
    The sampling of impoundment contents;
    B)
    The analysis of test data; and
    C)
    The annual removal of residues that are not
    delisted
    under 35 Ill. Adm. Code 720.122 or that exhibit a
    characteristic of hazardous waste and either:
    i)
    Do not meet the applicable treatment standards
    of 35 Ill. Adm. Code 728.Subpart D, or
    ii)
    Where no treatment standards have been
    established: Such residues are prohibited from
    land disposal under 35 Ill. Adm. Code 728.132 or
    728.139.
    8)
    For owners and operators seeking an exemption to the air
    emission standards of 724.Subpart CC of this part in
    accordance with Section 725.983:
    A) TIf direct measurement is used for the waste
    determination, t he procedures and schedules for waste
    sampling and analysis and the analysis of test data to
    verify the exemption.
    B) Each generator's not
    ice and certification of the
    volatile organic concentration in the waste if the
    waste is received from
    offsite If knowledge of the
    waste is used for the waste determination, any
    information prepared by the facility owner or
    operator, or by the generator of the waste if the
    waste is received form off-site, that is used as the
    basis for knowledge of the waste
    .
    c)
    For off-site facilities, the waste analysis plan required in
    subsection (b) above must also specify the procedures that will be
    used to inspect and, if necessary, analyze each movement of
    239
    hazardous waste received at the facility to ensure that it matches
    the identity of the waste designated on the accompanying manifest
    or shipping paper. At a minimum, the plan must describe:
    1)
    The procedures that will be used to determine the identity
    of each movement of waste managed at the facility; and
    2)
    The sampling method that will be used to obtain a
    representative sample of the waste to be identified if the
    identification method includes sampling.
    3)
    The procedures that the owner or operator of an off-site
    landfill receiving containerized hazardous waste will use to
    determine whether a hazardous waste generator or
    treater has
    added a biodegradable
    sorbent to the waste in the container.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
    Section 725.171
    Use of Manifest System
    a)
    If a facility receives hazardous waste accompanied by a manifest,
    the owner or operator or his agent must:
    1)
    Sign and date each copy of the manifest to certify that the
    hazardous waste covered by the manifest was received;
    2)
    Note any significant discrepancies in the manifest, as
    defined in Section 725.172(a), on each copy of the manifest;
    BOARD NOTE: An owner or operator of a facility whose
    procedures under Section 725.113(c) include waste analysis
    need not perform that analysis before signing the manifest
    and giving it to the transporter. Section 725.172(b),
    however, requires the owner or operator to report any
    unreconciled discrepancy discovered during later analysis.
    3)
    Immediately give the transporter at least one copy of the
    signed manifest;
    4)
    Send a copy of the manifest to each of the generator and the
    Agency within 30 days of the date of delivery; and
    5)
    Retain at the facility a copy of each manifest for at least
    three years from the date of delivery.
    b)
    If a facility receives from a rail or water (bulk shipment)
    transporter hazardous waste that is accompanied by a shipping
    paper containing all the information required on the manifest
    (excluding the U .S. EPA identification numbers, generator's
    certification and signatures), the owner or operator or its agent
    must:
    1)
    Sign and date each copy of the manifest or shipping paper
    (if the manifest has not been received) to certify that the
    hazardous waste covered by the manifest or shipping paper
    was received;
    2)
    Note any significant discrepancies, as defined in Section
    240
    725.172(a), in the manifest or shipping paper (if the
    manifest has not been received) on each copy of the manifest
    or shipping paper;
    BOARD NOTE: The owner or operator of a facility whose
    procedures under Section 725.113(c) include waste analysis
    need not perform that analysis before signing the shipping
    paper and giving it to the transporter. Section 725.172(b),
    however, requires reporting an
    unreconciled discrepancy
    discovered during later analysis.
    3)
    Immediately give the rail or water (bulk shipment)
    transporter at least one copy of the manifest or shipping
    paper (if the manifest has not been received);
    4)
    Send a copy of the signed and dated manifest to the
    generator and to the Agency within 30 days after the
    delivery; however, if the manifest has not been received
    within 30 days after delivery, the owner or operator, or his
    agent, must send a copy of the shipping paper signed and
    dated to the generator; and
    BOARD NOTE: 35 Ill. Adm. Code 722.123(c) requires the
    generator to send three copies of the manifest to the
    facility when hazardous waste is sent by rail or water (bulk
    shipment).
    5)
    Retain at the facility a copy of the manifest and shipping
    paper (if signed in lieu of the manifest at the time of
    delivery) for at least three years from the date of
    delivery.
    c)
    Whenever a shipment of hazardous waste is initiated from a
    facility, the owner or operator of that facility must comply with
    the requirements of 35 Ill. Adm. Code 722.
    BOARD NOTE: The provisions of 35 Ill. Adm. Code 722.134 are
    applicable to the on
    -site accumulation
    of hazardous wastes by
    generators. Therefore, the provisions of 35 Ill. Adm. Code
    722.134 apply only to owners or operators that are shipping
    hazardous waste that they generated at that facility.
    d)
    Within three working days of the receipt of a shipment subject to
    35 Ill. Adm. Code 722.Subpart H, the owner or operator of the
    facility must provide a copy of the tracking document bearing all
    required signatures to the
    notifier; to the Office of Enforcement
    and Compliance Assurance, Office of Compliance, Enforcement
    Planning, Targeting and Data Division (2222A), Environmental
    Protection Agency, 401 M St., SW., Washington, DC 20460; to the
    Bureau of Land, Division of Land Pollution Control, Illinois
    Environmental Protection Agency,
    P.O. Box 19276, Springfield, IL
    62794-9276; and to competent authorities of all other concerned
    countries. The original copy of the tracking document must be
    maintained at the facility for at least three years from the date
    of signature.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART I: USE AND MANAGEMENT OF CONTAINERS
    241
    Section 725.278
    Air Emission Standards
    The owner or operator shall manage all hazardous waste placed in a container
    in accordance with the requirements of 724.Subpart
    s AA, BB, and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART J: TANK SYSTEMS
    Section 725.302
    Air Emission Standards
    The owner or operator shall manage all hazardous waste placed in a tank in
    accordance with the requirements of 724.Subparts AA, BB, and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART K: SURFACE IMPOUNDMENTS
    Section 725.331
    Air Emission Standards
    The owner or operator shall manage all hazardous waste placed in a surface
    impoundment in accordance with the requirements of 724.Subpart
    s BB and CC.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART N: LANDFILLS
    Section 725.414
    Special Requirements for Liquid Wastes
    a)
    This subsection corresponds with 40 CFR 265.314(a), which pertains
    to the placement of bulk or non-containerized liquid waste or
    waste containing free liquids in a landfill prior to May 8, 1985.
    This statement maintains structural consistency with U
    .S. EPA
    rules.
    b)
    The placement of bulk or non
    -containerized liquid hazardous waste
    or hazardous waste containing free liquids (whether or not
    sorbents have been added) in any landfill is prohibited.
    c)
    Containers holding free liquids must not be placed in a lan
    dfill
    unless;
    1)
    All free -standing liquid:
    A)
    has been removed by decanting or other methods;
    B)
    has been mixed with
    sorbent or solidified so that
    free-standing liquid is no longer observed; or
    C)
    has been otherwise eliminated; or
    2)
    The container is very small, such as an
    ampule; or
    3)
    The container is designed to hold free liquids for use other
    than storage, such as a battery or capacitor; or
    4)
    The container is a lab pack as defined in Section 724.416
    and is disposed of in accordance with Section 724.416.
    242
    d)
    To demonstrate the absence or presence of free liquids in either a
    containerized or a bulk waste, the following test must be used:
    Method 9095 (Paint Filter Liquids Test), as described in "Test
    Methods for Evaluating Solid Wastes, Physical/Chemical Methods",
    U.S. EPA Publication No. SW
    -846, incorporated by reference in 35
    Ill. Adm. Code 720.111.
    e)
    The placement of any liquids that is not a hazardous waste in a
    landfill is prohibited (35 Ill. Adm. Code 729.311).
    f)
    Sorbents used to treat free liquids to be disposed of in landfills
    must be nonbiodegradable.
    Nonbiodegradable
    sorbents are:
    materials listed or described in subsection (f)(1) below;
    materials that pass one of the tests in subsection (f)(2) below;
    or materials that are determined by Board to be
    nonbiodegradable
    through the 35 Ill. Adm. Code 106 adjusted standard process.
    1)
    Nonbiodegradable
    sorbents are:
    A)
    Inorganic minerals, other inorganic materials, and
    elemental carbon (e.g.,
    aluminosilicates, clays,
    smectites, Fuller's earth,
    bentonite, calcium
    bentonite, montmorillonite,
    calcined montmorillonite,
    kaolinite, micas (
    illite), vermiculites, zeolites;
    calcium carbonate (organic free limestone);
    oxides/hydroxides,
    alumina, lime, silica (sand),
    diatomaceous earth;
    perlite (volcanic glass); expanded
    volcanic rock; volcanic ash; cement kiln dust; fly
    ash; rice hull ash; activated charcoal/activated
    carbon); or
    B)
    High molecular weight synthetic polymers (e.g.,
    polyethylene, high density polyethylene (HDPE),
    polypropylene, polystyrene, polyurethane,
    polyacrylate, polynorborene, polysobutylene, ground
    synthetic rubber, cross-linked
    allylstyrene and
    tertiary butyl copolymers). This does not include
    polymers derived from biological material or polymers
    specifically designed to be degradable; or
    C)
    Mixtures of these
    nonbiodegradable materials.
    2)
    Tests for nonbiodegradable
    sorbents.
    A)
    The sorbent material is determined to be
    nonbiodegradable under ASTM Method G21-70 (1984a)
    --
    "Standard Practice for Determining Resistance of
    Synthetic Polymer Materials to Fungi", incorporated by
    reference in 35 Ill. Adm. Code 720.111;
    or
    B)
    The sorbent material is determined to be
    nonbiodegradable under ASTM Method G22-76 (1984b)
    --
    "Standard Practice for Determining Resistance of
    Plastics to Bacteria", incorporated by reference in 35
    Ill. Adm. Code 720.111
    ; or
    C)
    The sorbent material is determined to be non-
    biodegradable under OECD test 301B [CO
    2
    Evolution
    (Modified Sturm Test)], incorporated by reference in
    35 Ill. Adm. Code 720.111.
    243
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
    Section 725.930
    Applicability
    a)
    This Subpart applies to owners and operators of facilities that
    treat, store or dispose of hazardous wastes (except as provided in
    Section 725.101).
    b)
    Except for Section
    s 725.934(d) and 725.935 (e), this Subpart
    applies to process vents associated with distillation,
    fractionation, thin-film evaporation, solvent extraction, or air
    or steam stripping operations that manage hazardous wastes with
    organic concentrations of at least 10
    ppmw (parts per million by
    weight), if these operations are conducted in
    one of the
    following :
    1) UA units that areis subject to the permitting requirements
    of 35 Ill. Adm. Code
    702, 703, and 705 ; or
    2) HA unit (including a h
    azardous waste recycling unit
    s) that
    areis not exempt from permitting under the provisions of 35
    Ill. Adm. Code 262.34(a) (i.e., a hazardous waste recycling
    unit that is not a 90-day tank or container) and that is
    located on a hazardous waste management
    facilities facility
    otherwise subject to the permitting requirements of 35 Ill.
    Adm. Code 702, 703, and 705 .
    BOARD NOTE: The requirements of Sections 725.932 through
    725.936 apply to process vents on hazardous waste recycling
    units previously exempt under 35 Ill. Adm. Code
    721.106(c)(1). Other exemptions under 35 Ill. Adm. Code
    721.104, 722.134 and 725.101(c) are not affected by these
    requirements.
    c)
    Agency deci sions pursuant to this Part must be made in writing,
    are in the nature of permit decisions pursuant to Section 39 of
    the Environmental Protection Act and may be appealed to the Board
    pursuant to 35 Ill. Adm. Code 105.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.933
    Standards: Closed-vent Systems and Control Devices
    a)
    Compliance Required.
    1)
    Owners or operators of closed-vent systems and control
    devices used to comply with provisions of this Part shall
    comply with the provisions of this Section.
    2)
    The owner or operator of an existing facility that cannot
    install a closed-vent system and control device to comply
    with the provisions of this Subpart on the effective date
    that the facility becomes subject to the provisions of this
    Subpart shall prepare an implementation schedule that
    includes dates by which the closed-vent system and control
    device will be installed and in operation. The controls
    must be installed as soon as possible, but the
    244
    implementation schedule may allow up to
    1830 months after
    the effective date that the facility becomes subject to this
    Subpart for installation and startup. All units that begin
    operation after December 21, 1990, must comply with the
    rules immediately (i.e., must have control devices installed
    and operating on startup of the affected unit); the 2-year
    implementation schedule does not apply to these units.
    b)
    A control device involving vapor recovery (e.g., a condenser or
    adsorber) must be designed and operated to recover the organic
    vapors vented to it with an efficiency of 95 weight percent or
    greater unless the total organic emission limits of Section
    725.932(a)(1) for all affected process vents is attained at an
    efficiency less than 95 weight percent.
    c)
    An enclosed combustion device (e.g., a vapor incinerator, boiler,
    or process heater) must be designed and operated to reduce the
    organic emissions vented to it by 95 weight percent or greater; to
    achieve a total organic compound concentration of 20
    ppmv,
    expressed as the sum of the actual compounds, not carbon
    equivalents, on a dry basis corrected to 3 percent oxygen; or to
    provide a minimum residence time of 0.50 seconds at a minimum
    temperature of 760
    ยฐ
    C. If a boiler or process heater is used as
    the control device, then the vent stream must be introduced into
    the flame combustion zone of the boiler or process heater.
    d)
    Flares
    1)
    A flare must be designed for and operated with no visible
    emissions as determined by the methods specified in
    subsection (e)(1) below except for periods not to exceed a
    total of 5 minutes during any 2 consecutive hours.
    2)
    A flare must be operated with a flame present at all times,
    as determined by the methods specified in subsection
    (f)(2)(c) below.
    3)
    A flare must be used only if the net heating value of the
    gas being combusted is 11.2 MJ/
    scm (300 Btu/ scf) or greater
    if the flare is steam-assisted or air-assisted, or if the
    net heating value of the gas being combusted is 7.45 MJ/
    scm
    (200 Btu/ scf) or greater if the flare is
    nonassisted. The
    net heating value of the gas being combusted must be
    determined by the methods specified in subsection (e)(2)
    below.
    4)
    Exit Velocity.
    A)
    A steam-assisted or
    nonassisted flare must be designed
    for and operated with an exit velocity, as determined
    by the methods specified in subsection (e)(3) below,
    less than 18.3 m/s (60 ft/s), except as provided in
    subsections (d)(4)(B) and (d)(4)(C) below.
    B)
    A steam-assisted or
    nonassisted flare designed for and
    operated with an exit velocity, as determined by the
    methods specified in subsection (e)(3) below, equal to
    or greater than 18.3 m/s (60 ft/s) but less than 122
    m/s (400 ft/s) is allowed if the net heating value of
    the gas being combusted is greater than 37.3 MJ/
    scm
    (1000 Btu/ scf).
    245
    C)
    A steam-assisted or
    nonassisted flare designed for and
    operated with an exit velocity, as determined by the
    methods specified in subsection (e)(3) below, less
    than the velocity, V as determined by the method
    specified in subsection (e)(4) and less than 122 m/s
    (400 ft/s) is allowed.
    5)
    An air-assisted flare must be designed and operated with an
    exit velocity less than the velocity, V as determined by the
    method specified in subsection (e)(5) below.
    6)
    A flare used to comply with this Section must be steam-
    assisted, air-assisted, or
    nonassisted.
    e)
    Compliance determination and equations.
    1)
    Reference Method 22 in 40 CFR 60, incorporated by reference
    in 35 Ill. Adm. Code 720.111, must be used to determine the
    compliance of a flare with the visible emission provisions
    of this Subpart. The observation period is 2 hours and must
    be used according to Method 22.
    2)
    The net heating value of the gas being combusted in a flare
    must be calculated using the following equation:
    Where:
    H
    T
    is the net heating value of the sample in MJ/
    scm;
    where the net enthalpy per mole of
    offgas is based on
    combustion at 25
    ยฐ
    C and 760 mm Hg, but the standard
    temperature for determining the volume
    corrersponding
    to 1 mole is 20
    ยฐ
    C.
    K = 1.74
    ร—
    10
    -7
    (1/ppm)(g mol/scm)(MJ/kcal) where
    standard temperature for (g
    mol/scm) 20
    ยฐ
    C.
    ฮฃ
    X
    i
    means the sum of the values of X for each
    component i, from i=1 to n.
    C
    i
    is the concentration of sample component i in
    ppm
    on a wet basis, as measured for
    organics by Reference
    Method 18 in 40 CFR 60, and for carbon monoxide, by
    ASTM D 1946-90, incorporated by reference in 35 Ill.
    Adm. Code 720.111.
    H
    i
    is the net heat of combustion of sample component
    i, kcal/ gmol at 25
    ยฐ
    C and 760 mm Hg. The heats of
    combustion must be determined using ASTM D 2382-88,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, if published values are not available or
    T
    i
    i
    H
    = K
    i
    n
    C
    H
    ร—
    =
    โˆ‘
    ร—
    1
    246
    cannot be calculated.
    3)
    The actual exit velocity of a flare must be determined by
    dividing the volumetric flow rate (in units of standard
    temperature and pressure), as determined by Reference
    Methods 2, 2A, 2C, or 2D in 40 CFR 60, incorporated by
    reference in 35 Ill. Adm. Code 720.111, as appropriate, by
    the unobstructed (free) cross-sectional area of the flare
    tip.
    4)
    The maximum allowed velocity in m/s, V for a flare complying
    with subsection (d)(4)(C) above must be determined by the
    following equation:
    Where:
    Log
    10
    means logarithm to the base 10
    H
    T
    is the net heating value as determined in
    subsection (e)(2) above.
    5)
    The maximum allowed velocity in m/s, V for an air-assisted
    flare must be determined by the following equation:
    Where:
    H
    T
    is the net heating value as determined in
    subsection (e)(2) above.
    f)
    The owner or operator shall monitor and inspect each control
    device required to comply with this Section to ensure proper
    operation and maintenance of the control device by implementing
    the following requirements:
    1)
    Install, calibrate, maintain, and operate according to the
    manufacturer's specifications a flow indicator that provides
    a record of vent stream flow from each affected process vent
    to the control device at least once every hour. The flow
    indicator sensor must be installed in the vent stream at the
    nearest feasible point to the control device inlet but
    before being combined with other vent streams.
    2)
    Install, calibrate, maintain, and operate according to the
    manufacturer's specifications a device to continuously
    monitor control device operation as specified below:
    A)
    For a thermal vapor incinerator, a temperature
    monitoring device equipped with a continuous recorder.
    The device must have accuracy of ยฑ 1 percent of the
    temperature being monitored in
    ยฐ
    C or ยฑ 0.5
    ยฐ
    C,
    whichever is greater. The temperature sensor must be
    installed at a location in the combustion chamber
    log(
    )
    (
    .
    ) /
    .
    V
    H
    T
    =
    +
    288
    317
    V = 8.706 +0.7084 H
    T
    247
    downstream of the combustion zone.
    B)
    For a catalytic vapor incinerator, a temperature
    monitoring device equipped with a continuous recorder.
    The device must be capable of monitoring temperature
    at two locations and have an accuracy of ยฑ 1 percent
    of the temperature being monitored in C or ยฑ 0.5
    ยฐ
    C,
    whichever is greater. One temperature sensor must be
    installed in the vent stream at the nearest feasible
    point to the catalyst bed inlet and a second
    temperature sensor must be installed in the vent
    stream at the nearest feasible point to the catalyst
    bed outlet.
    C)
    For a flare, a heat sensing monitoring device equipped
    with a continuous recorder that indicates the
    continuous ignition of the pilot flame.
    D)
    For a boiler or process heater having a design heat
    input capacity less than 44 MW, a temperature
    monitoring device equipped with a continuous recorder.
    The device must have an accuracy of ยฑ 1 percent of
    the temperature being monitored in
    ยฐ
    C or ยฑ 0.5
    ยฐ
    C,
    whichever is greater. The temperature sensor must be
    installed at a location in the furnace downstream of
    the combustion zone.
    E)
    For a boiler or process heater having a design heat
    input capacity greater than or equal to 44 MW, a
    monitoring device equipped with a continuous recorder
    to measure parameters that indicates good combustion
    operating practices are being used.
    F)
    For a condenser, either:
    i)
    A monitoring device equipped with a continuous
    recorder to measure the concentration level of
    the organic compounds in the exhaust vent stream
    from the condenser; or
    ii)
    A temperature monitoring device equipped with a
    continuous recorder. The device must be capable
    of monitoring temperature
    at two locations and
    havewith an accuracy of ยฑ1 percent of the
    temperature being monitored in
    degrees Celsius
    (
    ยฐ
    C) or ยฑ0.5
    ยฐ
    C, whichever is greater.
    OneThe
    temperature sensor must be installed at a
    location in the exhaust vent stream from the
    condenser , and a second temperature sensor must
    be installed at a location in the coolant fluid
    exiting the condenser
    (i.e., product side)
    .
    G)
    For a carbon adsorption system such as a fixed-bed
    carbon adsorber that regenerates the carbon bed
    directly in the control device, either:
    i)
    A monitoring device equipped with a continuous
    recorder to measure the concentration level of
    the organic compounds in the exhaust vent stream
    from the carbon bed; or
    248
    ii)
    A monitoring device equipped with a continuous
    recorder to measure a parameter that indicates
    the carbon bed is regenerated on a regular,
    predetermined time cycle.
    3)
    Inspect the readings from each monitoring device required by
    subsection (f)(1) and (f)(2) above at least once each
    operating day to check control device operation and, if
    necessary, immediately implement the corrective measures
    necessary to ensure the control device operates in
    compliance with the requirements of this Section.
    g)
    An owner or operator using a carbon adsorption system such as a
    fixed-bed carbon
    adsorber that regenerates the carbon bed directly
    onsite in the control device shall replace the existing carbon in
    the control device with fresh carbon at a regular, predetermined
    time interval that is no longer than the carbon service life
    established as a requirement of Section 725.935(b)(4)(C)(vi).
    h)
    An owner or operator using a carbon adsorption system, such as a
    carbon canister, that does not regenerate the carbon bed directly
    onsite in the control device shall replace the existing carbon in
    the control device with fresh carbon on a regular basis by using
    one of the following procedures:
    1)
    Monitor the concentration level of the organic compounds in
    the exhaust vent stream from the carbon adsorption system on
    a regular schedule, and replace the existing carbon with
    fresh carbon immediately when carbon breakthrough is
    indicated. The monitoring frequency must be daily or at an
    interval no greater than 20 percent of the time required to
    consume the total carbon working capacity established as a
    requirement of Section 725.935(b)(4)(C)(vii), whichever is
    longer.
    2)
    Replace the existing carbon with fresh carbon at a regular,
    predetermined time interval that is less than the design
    carbon replacement interval established as a requirement of
    Section 725.935(b)(4)(C)(vii).
    i)
    An owner or operator of an affected facility seeking to comply
    with the provisions of this Part by using a control device other
    than a thermal vapor incinerator, catalytic vapor incinerator,
    flare, boiler, process heater, condenser, or carbon adsorption
    system is required to develop documentation including sufficient
    information to describe the control device operation and identify
    the process parameter or parameters that indicate proper operation
    and maintenance of the control device.
    j) Closed vent systems. A closed vent system must meet either of the
    following design requirements:
    1) CA closed-vent system
    s must be designed
    for andto operate d
    with no detectable emissions, as indicated by an instrument
    reading of less than 500
    ppmv above background
    and by visual
    inspections , as determined by the methods specified at
    Section 725.934(b)
    ., and by visual inspections; or
    2) Closed-vent systems must be monitored to determine
    compliance with this Section during the initial leak
    detection monitoring, which must be conducted by the date
    249
    that the facility becomes subject to the provisions of this
    Section annually, and at other times as specified by the
    Agency pursuant to Section 725.930(c). For the annual leak
    detection monitoring after the initial leak detection
    monitoring, the owner or operator is not required to monitor
    those closed-vent system components that continuously
    operate in vacuum service or those closed-vent system
    joints, seams, or other connections that are permanently or
    semi-permanently sealed (e.g., a welded joint between two
    sections of metal pipe or a bolted and
    gasketed pipe
    flange). A closed -vent s ystem must be designed to operate at
    a pressure below atmospheric pressure. The system must be
    equipped with at least one pressure gauge or other pressure
    measurement device that can be read from a readily
    accessible location to verify that negative pressure is
    being maintained in the closed
    -vent system when the control
    device is operating.
    3) Detectable emissions, as indicated by an instrument reading
    greater than 500
    ppm and visual inspections, must be
    controlled as soon as practicable, but not later than 15
    calendar days after the emission is detected.
    4) A first attempt at repair must be made no later than 5
    calendar days after the emission is detected..
    k)
    The owner or operator shall monitor and inspect each closed-vent
    system required to comply with this Section to ensure proper
    operation and maintenance of the closed
    -vent system by
    implementing the following requirements:
    1)
    Each closed -vent system that is used to comply with
    subsection (j)(1) above shall be inspected and monitored in
    accordance with the following requirements:
    A)
    An initial leak detection monitoring of the
    closed -vent system shall be conducted by the owner or
    operator on or before the date that the system becomes
    subject to this Section. The owner or operator shall
    monitor the closed
    -vent system components and
    connections using the procedures specified in Section
    725.934(b) to demonstrate that the closed
    -vent system
    operates with no detectable emissions, as indicated by
    an instrument reading of less than 500
    ppmv above
    background.
    B)
    After initial leak detection monitoring required in
    subsection (k)(1)(A) above, the owner or operator
    shall inspect and monitor the closed
    -vent system as
    follows:
    i)
    Closed -vent system joints, seams, or other
    connections that are permanently or
    semi-permanently sealed (e.g., a welded joint
    between two Sections of hard piping or a bolted
    and gasketed ducting flange) must be visually
    inspected at least once per year to check for
    defects that could result in air pollutant
    emissions. The owner or operator shall monitor
    a component or connection using the procedures
    specified in Section 725.934(b) to demonstrate
    250
    that it operates with no detectable emissions
    following any time the component is repaired or
    replaced (e.g., a Section of damaged hard piping
    is replaced with new hard piping) or the
    connection is unsealed (e.g., a flange is
    unbolted).
    ii)
    Closed -vent system components or connections
    other than those specified in subsection
    (k)(1)(B)(i) above must be monitored annually
    and at other times as requested by the Regional
    Administrator, except as provided for in
    subsection (n) below, using the procedures
    specified in Section 725.934(b) to demonstrate
    that the components or connections operate with
    no detectable emissions.
    C)
    In the event that a defect or leak is detected, the
    owner or operator shall repair the defect or leak in
    accordance with the requirements of subsection (k)(3)
    below.
    D)
    The owner or operator shall maintain a record of the
    inspection and monitoring in accordance with the
    requirements specified in Section 725.935.
    2)
    Each closed -vent system that is used to comply with
    subsection (j)(2) above must be inspected and monitored in
    accordance with the following requirements:
    A)
    The closed -vent system must be visually inspected by
    the owner or operator to check for defects that could
    result in air pollutant emissions. Defects include,
    but are not limited to, visible cracks, holes, or gaps
    in ductwork or piping or loose connections.
    B)
    The owner or operator shall perform an initial
    inspection of the closed
    -vent system on or before the
    date that the system becomes subject to this Section.
    Thereafter, the owner or operator shall perform the
    inspections at least once every year.
    C)
    In the event that a defect or leak is detected, the
    owner or operator shall repair the defect in
    accordance with the requirements of subsection (k)(3)
    below.
    D)
    The owner or operator shall maintain a record of the
    inspection and monitoring in accordance with the
    requirements specified in Section 725.935.
    3)
    The owner or operator shall repair all detected defects as
    follows:
    A)
    Detectable emissions, as indicated by visual
    inspection or by an instrument reading greater than
    500 ppmv above background, must be controlled as soon
    as practicable, but not later than 15 calendar days
    after the emission is detected, except as provided for
    in subsection (k)(3)(C) below.
    251
    B)
    A first attempt at repair must be made no later than
    five calendar days after the emission is detected.
    C)
    Delay of repair of a closed
    -vent system for which
    leaks have been detected is allowed if the repair is
    technically infeasible without a process unit
    shutdown, or if the owner or operator determines that
    emissions resulting from immediate repair would be
    greater than the fugitive emissions likely to result
    from delay of repair. Repair of such equipment must
    be completed by the end of the next process unit
    shutdown.
    D)
    The owner or operator shall maintain a record of the
    defect repair in accordance with the requirements
    specified in Section 725.935.
    kl) CA closed-vent system
    s andor control device s used to comply with
    provisions of this Subpart must be operated at all times when
    emissions may be vented to
    themit.
    lm)
    The owner or operator using a carbon adsorption system
    to control
    air pollutant emissions
    shall document that all carbon removed
    that is a hazardous waste and that is removed
    from the control
    device is managed in one of the following manners
    , regardless of
    the volatile organic concentration of the carbon
    :
    1)
    It is regenerated or reactivated in a thermal treatment unit
    that is permitted under 35 Ill. Adm. Code 724.Subpart X or
    725.Subpart P,meets one of the following:
    A)
    The owner or operator of the unit has been issued a
    final permit under 35 Ill. Adm. Code 702, 703, and 705
    that implements the requirements of 35 Ill. Adm. Code
    724.Subpart X; or
    B)
    The unit is equipped with and operating air emission
    controls in accordance with the applicable
    requirements of 725.Subparts AA and CC or 35 Ill. Adm.
    Code 724; or
    C)
    The unit is equipped with and operating air emission
    controls in accordance with a national emission
    standard for hazardous air pollutants under 40 CFR 61
    or 40 CFR 63.
    2)
    It is incinerated
    by a process that is permitted under 35
    Ill. Adm. Code 724.Subpart O or 725.Subpart O,
    orin a
    hazardous waste incinerator for which the owner or operator
    has done either of the following:
    A)
    The owner or operator has been issued a final permit
    under 35 Ill. Adm. Code 702, 703, and 705 that
    implements the requirements of 35 Ill. Adm. Code
    724.Subpart O, or
    B)
    The owner or operator has designed and operates the
    incinerator in accordance with the interim status
    requirements of 725.Subpart O; or
    3)
    It is burned in a boiler or industrial furnace
    that is
    252
    permitted under 35 Ill. Adm. Code 726.Subpart
    H.for which
    the owner or operator has done either of the following:
    A)
    The owner or operator has been issued a final permit
    under 35 Ill. Adm. Code 702, 703, and 705 that
    implements the requirements of 35 Ill. Adm. Code
    726.Subpart H, or
    B)
    The owner or operator has designed and operates the
    boiler or industrial furnace in accordance with the
    interim status requirements of 35 Ill. Adm. Code
    726.Subpart H.
    n)
    Any components of a closed
    -vent system that are designated, as
    described in Section 725.935(c)(9), as unsafe to monitor are
    exempt from the requirements of subsection (k)(1)(B)(ii) above if
    both of the following conditions are fulfilled:
    1)
    The owner or operator of the closed
    -vent system has
    determined that the components of the closed
    -vent system are
    unsafe to monitor because monitoring personnel would be
    exposed to an immediate danger as a consequence of complying
    with subsection (k)(1)(B)(ii) above; and
    2)
    The owner or operator of the closed
    -vent system adheres to a
    written plan that requires monitoring the closed
    -vent system
    components using the procedure specified in subsection
    (k)(1)(B)(ii) as frequently as practicable during
    safe-to-monitor times.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.934
    Test Methods and Procedures
    a)
    Each owner or operator subject to the provisions of this Subpart
    shall comply with the test methods and procedures requirements
    provided in this Section
    b)
    When a closed-vent system is tested for compliance with no
    detectable emissions, as required in Section 725.933(
    jk), the test
    must comply with the following requirements:
    1)
    Monitoring must comply with Reference Method 21 in 40 CF
    R
    60, incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The detection instrument must meet the performance criteria
    of Reference Method 21.
    3)
    The instrument must be calibrated before use on each day of
    its use by the procedures specified in Reference Method 21.
    4)
    Calibration gases must be:
    A)
    Zero air (less than 10
    ppm of hydrocarbon in air).
    B)
    A mixture of methane or n-hexane and air at a
    concentration of approximately, but less than, 10,000
    ppm methane or n-hexane.
    5)
    The background level must be determined as set forth in
    Reference Method 21.
    253
    6)
    The instrument probe must be traversed around all potential
    leak interfaces as close to the interface as possible as
    described in Reference Method 21.
    7)
    The arithmetic difference between the maximum concentration
    indicated by the instrument and the background level is
    compared with 500
    ppm for determining compliance.
    c)
    Performance tests to determine compliance with Section 725.932(a)
    and with the total organic compound concentration limit of Section
    725.933(c) must comply with the following:
    1)
    Performance tests to determine total organic compound
    concentrations and mass flow rates entering and exiting
    control devices must be conducted and data reduced in
    accordance with the following reference methods and
    calculation procedures:
    A)
    Method 2 in 40 CFR 60 for velocity and volumetric flow
    rate.
    B)
    Method 18 in 40 CFR 60 for organic content.
    C)
    Each performance test must consist of three separate
    runs, each run conducted for at least 1 hour under the
    conditions that exist when the hazardous waste
    management unit is operating at the highest load or
    capacity level reasonably expected to occur. For the
    purpose of determining total organic compound
    concentrations and mass flow rates, the average of
    results of all runs applies. The average must be
    computed on a time-weighed basis.
    D)
    Total organic mass flow rates must be determined by
    the following equation:
    F = K * Q * SUM( Ci * MWi)
    Where:
    F is the total organic mass flow rate, kg/h.
    K = 4.16 E -8, conversion factor for molar
    volume, kg- mol/cubic m, at 293 K and 760 mm Hg.
    Q = volumetric flow rate of gases entering or
    exiting control device,
    dscm/h, as determined by
    Method 2 in 40 CFR 60, incorporated by reference
    in 35 Ill. Adm. Code 720.111.
    SUM(Xi) means the sum of the values of X for
    each component i, from i=1 to n.
    n = number of organic compounds in the vent gas.
    Ci is the organic concentration in
    ppm, dry
    basis, of compound i in the vent gas, as
    determined by Method 18 in 40 CFR 60.
    MWi is the molecular weight of organic compound
    254
    i in the vent gas, kg/kg-
    mol.
    Where:
    E
    h
    = The total organic mass flow rate, kg/h.
    Q
    2sd
    = The volumetric flow rate of gases entering
    or exiting control device,
    dscm/h, as
    determined by Method 2 in 40 CFR 60,
    incorporated by reference in 35 Ill. Adm.
    Code 720.111.
    n = The number of organic compounds in the vent
    gas.
    C
    i
    = The organic concentration in
    ppm, dry
    basis, of compound i in the vent gas, as
    determined by Method 18 in 40 CFR 60.
    MW
    i
    = The molecular weight of organic compound i
    in the vent gas, kg/kg-
    mol.
    0.0416 = The conversion factor for molar volume,
    kg-mol/m
    3
    , at 293 K and 760 mm Hg.
    10
    -6
    = The conversion factor from
    ppm.
    E)
    The annual total organic emission rate must be
    determined by the following equation:
    A = F *
    ร—
    HOURS
    Where:
    A is total organic emission rate,
    kg/y.
    F is the total organic mass flow rate, kg/h, as
    calculated in subsection (c)(1)(D)
    above .
    HOURS is the total annual hours of operation for
    the affected unit.
    F)
    Total organic emissions from all affected process
    vents at the facility must be determined by summing
    the hourly total organic mass emissions rates (F as
    determined in subsection (c)(1)(D)
    above ) and by
    summing the annual total organic mass emission rates
    (A as determined in subsection (c)(1)(E)
    above ) for
    all affected process vents at the facility.
    2)
    The owner or operator shall record such process information
    as is necessary to determine the conditions of the
    h
    2sd
    i
    i
    -6
    E
    = Q
    x(
    n
    i = 1
    C
    x MW
    )x0.0416x10
    โˆ‘
    255
    performance tests. Operations during periods of startup,
    shutdown and malfunction do not constitute representative
    conditions for the purpose of a performance test.
    3)
    The owner or operator of an affected facility shall provide,
    or cause to be provided, performance testing facilities as
    follows:
    A)
    Sampling ports adequate for the test methods specified
    in subsection (c)(1)
    above .
    B)
    Safe sampling platform(s).
    C)
    Safe access to sampling platform(s).
    D)
    Utilities for sampling and testing equipment.
    4)
    For the purpose of making compliance determinations, the
    time-weighted average of the results of the three runs must
    apply. In the event that a sample is accidentally lost or
    conditions occur in which one of the three runs must be
    discontinued because of forced shutdown, failure of an
    irreplaceable portion of the sample train, extreme
    meteorological conditions or other circumstances beyond the
    owner or operator's control, compliance may, upon the
    Agency's approval, be determined using the average of the
    results of the two other runs.
    d)
    To show that a process vent associated with a hazardous waste
    distillation, fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation is not subject to
    the requirements of this Subpart, the owner or operator shall make
    an initial determination that the time-weighted, annual average
    total organic concentration of the waste managed by the waste
    management unit is less than 10
    ppmw using one of the following
    two methods:
    1)
    Direct measurement of the organic concentration of the waste
    using the following procedures:
    A)
    The owner or operator shall take a minimum of four
    grab samples of waste for each wastestream managed in
    the affected unit under process conditions expected to
    cause the maximum waste organic concentration.
    B)
    For waste generated onsite, the grab samples must be
    collected at a point before the waste is exposed to
    the atmosphere such as in an enclosed pipe or other
    closed system that is used to transfer the waste after
    generation to the first affected distillation,
    fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation. For
    waste generated offsite, the grab samples must be
    collected at the inlet to the first waste management
    unit that receives the waste provided the waste has
    been transferred to the facility in a closed system
    such as a tank truck and the waste is not diluted or
    mixed with other waste.
    C)
    Each sample must be analyzed and the total organic
    concentration of the sample must be computed using
    256
    Method 9060 or 8240 of SW-846
    , (incorporated by
    reference under 35 Ill. Adm. Code 720.111.
    D)
    The arithmetic mean of the results of the analyses of
    the four samples apply for each wastestream managed in
    the unit in determining the time-weighted, annual
    average total organic concentration of the waste. The
    time-weighted average is to be calculated using the
    annual quantity of each waste stream processed and the
    mean organic concentration of each wastestream managed
    in the unit.
    2)
    Using knowledge of the waste to determine that its total
    organic concentration is less than 10
    ppmw. Documentation
    of the waste determination is required. Examples of
    documentation that must be used to support a determination
    under this subsection include:
    A)
    Production process information documenting that no
    organic compounds are used.
    B)
    Information that the waste is generated by a process
    that is identical to a process at the same or another
    facility that has previously been demonstrated by
    direct measurement to generate a wastestream having a
    total organic content less than 10
    ppmw, or
    C)
    Prior speciation analysis results on the same
    wastestream where it is documented that no process
    changes have occurred since that analysis that could
    affect the waste total organic concentration.
    e)
    The determination that distillation, fracti
    onation, thin-film
    evaporation, solvent extraction, or air or steam stripping
    operations which manage hazardous wastes with time-weighted,
    annual average total organic concentrations less than 10
    ppmw must
    be made as follows:
    1)
    By the effective date that the facility becomes subject to
    the provisions of this Subpart or by the date when the waste
    is first managed in a waste management unit, whichever is
    later; and
    2)
    For continuously generated waste, annually; or
    3)
    Whenever there is a change in th
    e waste being managed or a
    change in the process that generates or treats the waste.
    f)
    When an owner or operator and the Agency do not agree on whether a
    distillation, fractionation, thin-film evaporation, solvent
    extraction, or air or steam stripping operation manages a
    hazardous waste with organic concentrations of at least 10
    ppmw
    based on knowledge of the waste, the procedures in Method 8240 in
    SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111,
    must be used to resolve the dispute.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.935
    Recordkeeping Requirements
    a)
    Compliance Required.
    257
    1)
    Each owner or operator subject to the provisions of this
    Subpart shall comply with the
    recordkeeping requirements of
    this Section.
    2)
    An owner or operator of more than one hazardous waste
    management unit subject to the provisions of this Subpart
    may comply with the
    recordkeeping requirements for these
    hazardous waste management units in one
    recordkeeping system
    if the system identifies each record by each hazardous waste
    management unit.
    b)
    Owners and operators shall record the following information in the
    facility operating record:
    1)
    For facilities that comply with the provisions of Section
    725.933(a)(2), an implementation schedule that includes
    dates by which the closed-vent system and control device
    will be installed and in operation. The schedule must also
    include a rationale of why the installation cannot be
    completed at an earlier date. The implementation schedule
    must be in the facility operating record by the effective
    date that the facility becomes subject to the provisions of
    this Subpart.
    2)
    Up-to-date documentation of compliance with the process vent
    standards in Section 725.932, including:
    A)
    Information and data identifying all affected process
    vents, annual throughput and operating hours of each
    affected unit, estimated emission rates for each
    affected vent and for the overall facility (i.e., the
    total emissions for all affected vents at the
    facility), and the approximate location within the
    facility of each affected unit (e.g., identify the
    hazardous waste management units on a facility plot
    plan).
    B)
    Information and data supporting determination of vent
    emissions and emission reductions achieved by add-on
    control devices based on engineering calculations or
    source tests. For the purpose of determining
    compliance, determinations of vent emissions and
    emission reductions must be made using operating
    parameter values (e.g., temperatures, flow rates, or
    vent stream organic compounds and concentrations) that
    represent the conditions that result in maximum
    organic emissions, such as when the waste management
    unit is operating at the highest load or capacity
    level reasonably expected to occur. If the owner or
    operator takes any action (e.g., managing a waste of
    different composition or increasing operating hours of
    affected waste management units) that would result in
    an increase in total organic emissions from affected
    process vents at the facility, then a new
    determination is required.
    3)
    Where an owner or operator chooses to use test date to
    determine the organic removal efficiency or total organic
    compound concentration achieved by the control device, a
    performance test plan. The test plan must include:
    258
    A)
    A description of how it is determined that the planned
    test is going to be conducted when the hazardous waste
    management unit is operating at the highest load or
    capacity level reasonably expected to occur. This
    must include the estimated or design flow rate and
    organic content of each vent stream and define the
    acceptable operating ranges of key process and control
    device parameters during the test program.
    B)
    A detailed engineering description of the closed-vent
    system and control device including:
    i)
    Manufacturer's name and model number of control
    device.
    ii)
    Type of control device.
    iii) Dimensions of the control device.
    iv)
    Capacity.
    v)
    Construction materials.
    C)
    A detailed description of s
    ampling and monitoring
    procedures, including sampling and monitoring
    locations in the system, the equipment to be used,
    sampling and monitoring frequency, and planned
    analytical procedures for sample analysis.
    4)
    Documentation of compliance with Section 725.933 must
    include the following information:
    A)
    A list of all information references and sources used
    in preparing the documentation.
    B)
    Records, including the dates of each compliance test
    required by Section 725.933(j).
    C)
    If engineering calculations are used, a design
    analysis, specifications, drawings, schematics, and
    piping and instrumentation diagrams based on the
    appropriate sections of APTI Course 415 (incorporated
    by reference in 35 Ill. Adm. Code 720.111) or other
    engineering texts, approved by the Agency, that
    present basic control device design information.
    Documentation provided by the control device
    manufacturer or vendor that describes the control
    device design in accordance with subsections
    (b)(4)(C)(i) through (vii)
    , below , may be used to
    comply with this requirement. The design analysis
    must address the vent stream characteristics and
    control device operation parameters as specified
    below.
    i)
    For a thermal vapor incinerator, the design
    analysis must consider the vent stream
    composition, constituent concentrations and flow
    rate. The design analysis must also establish
    the design minimum and average temperature in
    the combustion zone and the combustion zone
    259
    residence time.
    ii)
    For a catalytic vapor incinerator, the
    design
    analysis must consider the vent stream
    composition, constituent concentrations, and
    flow rate. The design analysis must also
    establish the design minimum and average
    temperatures across the catalyst bed inlet and
    outlet.
    iii)
    For a boiler or process heater, the design
    analysis must consider the vent stream
    composition, constituent concentrations and flow
    rate. The design analysis must also establish
    the design minimum and average flame zone
    temperatures, combustion zone residence time and
    description of method and location where the
    vent stream is introduced into the combustion
    zone.
    iv)
    For a flare, the design analysis must consider
    the vent stream composition, constituent
    concentrations, and flow rate. The design
    analysis must also consider the requirements
    specified in Section 725.933(d).
    v)
    For a condenser, the design analysis must
    consider the vent stream composition,
    constituent concentrations, flow rate, relative
    humidity and temperature. The design analysis
    must also establish the design outlet organic
    compound concentration level, design average
    temperature of the condenser exhaust vent stream
    and design average temperatures of the coolant
    fluid at the condenser inlet and outlet.
    vi)
    For a carbon adsorption system such as a fixed-
    bed adsorber that regenerates the carbon bed
    directly onsite in the control device, the
    design analysis must consider the vent stream
    composition, constituent concentrations, flow
    rate, relative humidity and temperature. The
    design analysis must also establish the design
    exhaust vent stream organic compound
    concentration level, number and capacity of
    carbon beds, type and working capacity of
    activated carbon used for carbon beds, design
    total steam flow over the period of each
    complete carbon bed regeneration cycle, duration
    of the carbon bed steaming and cooling/drying
    cycles, design carbon bed temperature after
    regeneration, design carbon bed regeneration
    time and design service life of carbon.
    vii)
    For a carbon adsorption system such as a
    carbon
    canister that does not regenerate the carbon bed
    directly onsite in the control device, the
    design analysis must consider the vent stream
    composition, constituent concentrations, flow
    rate, relative humidity and temperature. The
    design analysis must also establish the design
    260
    outlet organic concentration level, capacity of
    carbon bed, type and working capacity of
    activated carbon used for carbon bed and design
    carbon replacement interval based on the total
    carbon working capacity of the control device
    and source operating schedule.
    D)
    A statement signed and dated by the owner or operator
    certifying that the operating parameters used in the
    design analysis reasonably represent the conditions
    that exist when the hazardous waste management unit is
    or would be operating at the highest load or capacity
    level reasonably expected to occur.
    E)
    A statement signed and dated by the owner or operator
    certifying that the control device is designed to
    operate at an efficiency of 95 percent or greater
    unless the total organic concentration limit of
    Section 725.932(a) is achieved at an efficiency less
    than 95 weight percent or the total organic emission
    limits of Section 725.932(a) for affected process
    vents at the facility are attained by a control device
    involving vapor recovery at an efficiency less than 95
    weight percent. A statement provided by the control
    device manufacturer or vendor certifying that the
    control equipment meets the design specifications may
    be used to comply with this requirement.
    F)
    If performance tests are used to demonstrate
    compliance, all test results.
    c)
    Design documentation and monitoring operating and inspection
    information for each closed-vent system and control device
    required to comply with the provisions of this Part must be
    recorded and kept up-to-date in the facility operating record.
    The information must include:
    1)
    Description and date of each modification that is made to
    the closed-vent system or control device design.
    2)
    Identification of operating parameter,
    description of
    monitoring device, and diagram of monitoring sensor location
    or locations used to comply with Section 725.933(f)(1) and
    (2).
    3)
    Monitoring, operating and inspection information required by
    Section 725.933(f) through (k).
    4)
    Date, time and duration of each period that occurs while the
    control device is operating when any monitored parameter
    exceeds the value established in the control device design
    analysis as specified below:
    A)
    For a thermal vapor incinerator designed to operate
    with a minimum residence time of 0.50 second at a
    minimum temperature of 760 C, any period when the
    combustion temperature is below 760 C.
    B)
    For a thermal vapor incinerator designed to operate
    with an organic emission reduction efficiency of 95
    percent or greater, any period when the combustion
    261
    zone temperature is more than 28 C below the design
    average combustion zone temperature established as a
    requirement of subsection (b)(4)(C)(i)
    , above.
    C)
    For a catalytic vapor incinerator, any period when:
    i)
    Temperature of the vent stream at the catalyst
    bed inlet is more than 28 C below the average
    temperature of the inlet vent stream established
    as a requirement of subsection (b)(4)(C)(ii)
    ,
    above; or
    ii)
    Temperature difference across the catalyst bed
    is less than 80 percent of the design average
    temperature difference established as a
    requirement of subsection (b)(4)(C)(ii)
    , above.
    D)
    For a boiler or process heater, any period when:
    i)
    Flame zone temperature is more than 28 C below
    the design average flame zone temperature
    established as a requirement of subsection
    (b)(4)(C)(iii) , above; or
    ii)
    Position changes where the vent stream is
    introduced to the combustion zone from the
    location established as a requirement of
    subsection (b)(4)(C)(iii)
    , above.
    E)
    For a flare, period when the pilot flame is not
    ignited.
    F)
    For a condenser that complies with Section
    725.933(f)(2)(F)(i), any period when the organic
    compound concentration level or readings of organic
    compounds in the exhaust vent stream from the
    condenser are more than 20 percent greater than the
    design outlet organic compound concentration level
    established as a requirement of subsection
    (b)(4)(C)(v) , above.
    G)
    For a condenser that complies with Section
    725.933(f)(2)(F)(ii), any period when:
    i)
    Temperature of the exhaust vent stream from the
    condenser is more than 6 C above the design
    average exhaust vent stream temperature
    established as a requirement of subsection
    (b)(4)(C)(v) , above.
    ii)
    Temperature of the coo
    lant fluid exiting the
    condenser is more than 6 C above the design
    average coolant fluid temperature at the
    condenser outlet established as a requirement of
    subsection (b)(4)(C)(v)
    , above.
    H)
    For a carbon adsorption system such as a fixed-bed
    carbon adsorber that regenerates the carbon bed
    directly onsite in the control device and complies
    with Section 725.933(f)(2)(G)(i), any period when the
    organic compound concentration level or readings of
    organic compounds in the exhaust vent stream from the
    262
    carbon bed are more than 20 percent greater than the
    design exhaust vent stream organic compound
    concentration level established as a requirement of
    subsection (b)(4)(C)(vi)
    , above.
    I)
    For a carbon adsorption system such as a fixed-bed
    carbon adsorber that regenerates the carbon bed
    directly onsite in the control device and complies
    with Section 725.933(f)(2)(G)(ii), any period when the
    vent stream continues to flow through the control
    device beyond the predetermined carbon bed
    regeneration time established as a requirement of
    subsection (b)(4)(C)(vi)
    , above.
    5)
    Explanation for each period recorded under subsection
    (c)(4) , above, of the cause for control device operating
    parameter exceeding the design value and the measures
    implemented to correct the control device operation.
    6)
    For carbon adsorption systems operated subject to
    requirements specified in Section 725.933(g) or (h)(2), any
    date when existing carbon in the control device is replaced
    with fresh carbon.
    7)
    For carbon adsorption systems opera
    ted subject to
    requirements specified in Section 725.933(h)(1), a log that
    records:
    A)
    Date and time when control device is monitored for
    carbon breakthrough and the monitoring device reading.
    B)
    Date when existing carbon in the control device is
    replaced with fresh carbon.
    8)
    Date of each control device startup and shutdown.
    9)
    An owner or operator designating any components of a closed-
    vent system as unsafe to monitor pursuant to Section
    725.933(n) shall record in a log that is kept in the
    facility operating record the identification of closed
    -vent
    system components that are designated as unsafe to monitor
    in accordance with the requirements of Section 725.933(n),
    an explanation for each closed
    -vent system component stating
    why the closed -vent system component is unsafe to monitor,
    and the plan for monitoring each closed
    -vent system
    component.
    10)
    When each leak is detected as specified in Section
    725.933(k), the following information must be recorded:
    A)
    The instrument identification number, the closed
    -vent
    system component identification number, and the
    operator name, initials, or identification number.
    B)
    The date the leak was detected and the date of first
    attempt to repair the leak.
    C)
    The date of successful repair of the leak.
    D)
    Maximum instrument reading measured by Method 21 of 40
    CFR 60, appendix A, incorporated by reference in 35
    263
    Ill. Adm. Code 720.111, after it is successfully
    repaired or determined to be
    nonrepairable.
    E)
    "Repair delayed" and the reason for the delay if a
    leak is not repaired within 15 calendar days after
    discovery of the leak.
    i)
    The owner or operator may develop a written
    procedure that identifies the conditions that
    justify a delay of repair. In such cases,
    reasons for delay of repair may be documented by
    citing the relevant sections of the written
    procedure.
    ii)
    If delay of repair was caused by depletion of
    stocked parts, there must be documentation that
    the spare parts were sufficiently stocked
    on-site before depletion and the re
    ason for
    depletion.
    d)
    Records of the monitoring, operating and inspection information
    required by subsections (c)(3) through (
    810), above , need be kept
    only 3 must be maintained by the owner or
    operater for at least
    three years following the date of each occurrence, measurement,
    corrective action, or record
    .
    e)
    For a control device other than a thermal vapor incinerator,
    catalytic vapor incinerator, flare, boiler, process heater,
    condenser or carbon adsorption system, monitoring and inspection
    information indicating proper operation and maintenance of the
    control device must be recorded in the facility operating record.
    f)
    Up-to-date information and data used to determine whether or not a
    process vent is subject to the requirements in Section 725.932,
    including supporting documentation as required by Section
    725.934(d)(2), when application of the knowledge of the nature of
    the hazardous wastestream or the process by which it was produced
    is used, must be recorded in a log that is kept in the facility
    operating record.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
    Section 725.950
    Applicability
    a)
    The regulations in this Subpart apply to owners and operators of
    facilities that treat, store, or dispose of hazardous wastes
    (except as provided in Section 725.101).
    b)
    Except as provided in Section 725.964(
    jk), this Subpart applies to
    equipment that contains or contacts hazardous wastes with organic
    concentrations of at least 10 percent by weight that are managed
    in one of the following
    :
    1) UA units that areis subject to the RCRA permitting
    requirements of 35 Ill. Adm. Code
    702, 703, and 705 , or
    2) HA unit (including a h
    azardous waste recycling unit
    s) that
    areis not exempt from permitting under the provisions of 35
    264
    Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
    unit that is not a "90-day" tank or container) and that is
    located onat a hazardous waste management
    facilit iesy
    otherwise subject to the permitting requirements of 35 Ill.
    Adm. Code 702, 703, and 705 ., or
    3)
    A unit that is exempt from permitting under the provisions
    of 35 Ill. Adm. Code 722.134(a) (i.e., a "90
    -day" tank or
    container).
    c)
    Each piece of equipment to which this Subpart applies must be
    marked in such a manner that it can be distinguished readily from
    other pieces of equipment.
    d)
    Equipment that is in vacuum service is excluded from the
    requirements of Sections 725.952 to 725.960, if it is identified
    as required in Section 725.964(g)(5).
    e)
    Equipment that contains or contacts hazardous waste with an
    organic concentration of at least 10 percent by weight for a
    period of less than 300 hours per calendar year is excluded from
    the requirements of Sections 265.952 through 265.960 if it is
    identified as required in Section 725.964(g)(6).
    BOARD NOTE: The requirements of Sections 725.952 through 725.964
    apply to equipment associated with hazardous waste recycling units
    previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
    exemptions under 35 Ill. Adm. Code 721.104
    , 722.134 and 725.101(e)
    are not affected by these requirements.
    ef)
    Agency decisions pursuant to this Part must be made in writing,
    are in the nature of permit decisions pursuant to Section 39 of
    the Environmental Protection Act and may be appealed to the Board
    pursuant to 35 Ill. Adm. Code 105.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.955
    Standards: Sampling Connecting Systems
    a)
    Each sampling connection syst
    em must be equipped with a closed
    -
    purge, closed-loop, or
    system or closed-vent system.
    This system
    must collect the sample purge for return to the process or for
    routing to the appropriate treatment system. Gases displaced
    during filling of the sample container are not required to be
    collected or captured.
    b)
    Each closed-purge
    , closed-loop, or
    system or closed-vent system as
    required in subsection (a) must
    meet one of the following
    requirements :
    1)
    Return the purged
    hazardous waste stream process fluid
    directly to the hazardous waste management
    process line with
    no detectable emissions to atmosphere
    ; or
    2)
    Collect and recycle the purged
    hazardous waste stream with
    no detectable emissions to
    atmosphere process fluid ; or
    3)
    Be designed and operated to capture and transport all the
    purged hazardous wastestream process fluid to waste
    management unit that complies with the applicable
    requirements of Sections 725.985 through 725.987 or
    a
    265
    control device that complies with the requirements of
    Section 725.960.
    c)
    In-situ sampling systems
    and sampling systems without purges
    are
    exempt from the requirements of subsections (a) and (b)
    above .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.958
    Standards: Pumps, Valves, Pressure Relief Devices, Flanges
    and other Connectors
    a)
    Pumps and valves in heavy liquid service, pressure relief devices
    in light liquid or heavy liquid service and flanges and other
    connectors must be monitored within 5 days by the method specified
    in Section 725.963(b), if evidence of a potential leak is found by
    visual, audible, olfactory, or any other detection method.
    b)
    If an instrument reading of 10,000
    ppm or greater is measured, a
    leak is detected.
    c)
    Repairs
    1)
    When a leak is detected, it must be repaired as soon as
    practicable, but not later than 15 calendar days after it is
    detected, except as provided in Section 725.959.
    2)
    The first attempt at repair must be made no later than 5
    calendar days after each leak is detected.
    d)
    First attempts at repair include, but are not limited to, the best
    practices described under Section 725.957(e).
    e)
    Any connector that is inaccessible or is ceramic or ceramic-lined
    (e.g., porcelain, glass, or glass
    -lined) is exempt from the
    monitoring requirements of subsection (a) above and from the
    recordkeeping requirements of Section 725.964.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.964
    Recordkeeping Requirements
    a)
    Lumping Units
    1)
    Each owner or ope
    rator subject to the provisions of this
    Subpart shall comply with the
    recordkeeping requirements of
    this Section.
    2)
    An owner or operator of more than one hazardous waste
    management unit subject to the provisions of this Subpart
    may comply with the
    recordkeeping requirements for these
    hazardous waste management units in one
    recordkeeping system
    if the system identifies each record by each hazardous waste
    management unit.
    b)
    Owners and operators shall record the following information in the
    facility operating record:
    1)
    For each piece of equipment to which this Subpart applies:
    A)
    Equipment identification number and hazardous waste
    management unit identification.
    266
    B)
    Approximate locations within the facility (e.g.,
    identify the hazardous waste management unit on a
    facility plot plan).
    C)
    Type of equipment (e.g., a pump or pipeline valve).
    D)
    Percent-by-weight total
    organics in the hazardous
    wastestream at the equipment.
    E)
    Hazardous waste state at the equipment (e.g. gas/vapor
    or liquid).
    F)
    Method of compliance with the standard (e.g. "monthly
    leak detection and repair" or "equipped with dual
    mechanical seals").
    2)
    for facilities than comply with the provisions of Section
    725.933(a)(2), an implementation schedule as specified in
    that Section.
    3)
    Where an owner or operator chooses to use test data to
    demonstrate the organic removal efficiency or total organic
    compound concentration achieved by the control device, a
    performance test plan as specified in Section 725.935(b)(3).
    4)
    Documentation of compliance with Section 725.960, including
    the detailed design documentation or performance test
    results specified in Section 725.935(b)(4).
    c)
    When each leak is detected as specified in Sections 725.952,
    725.953, 725.957 or 725.958, the following requirements apply:
    1)
    A weatherproof and readily visible identification, marked
    with the equipment identification number, the date evidence
    of a potential leak was found in accordance with Section
    725.958(a), and the date the leak was detected, must be
    attached to the leaking equipment.
    2)
    The identification on equipment except on a valve, may be
    removed after it has been repaired.
    3)
    The identification on a valve may be removed after it has
    been monitored for 2 successive months as specified in
    Section 725.957(c) and no leak has been detected during
    those 2 months.
    d)
    When each leak is detected as specified in Sections 725.952,
    725.953, 725.957 or 725.958, the following information must be
    recorded in an inspection log and must be kept in the facility
    operating record:
    1)
    The instrument and operator identification numbers and the
    equipment identification number.
    2)
    The date evidence of a potential leak was found in
    accordance with Section 725.958(a).
    3)
    The date the leak was detected and the dates of each attempt
    to repair the leak.
    267
    4)
    Repair methods applied in each attempt to repair the leak.
    5)
    "Above 10,000", if the maximum instrument reading measured
    by the methods specified in Section 725.963(b) after each
    repair attempt is equal to or greater than 10,000
    ppm.
    6)
    "Repair delayed" and the reason for the delay if a leak is
    not repaired within 15 calendar days after discovery of the
    leak.
    7)
    Documentation supporting the delay of repair of a valve in
    compliance with Section 725.959(c).
    8)
    The signature of the owner or operator (or designate) whose
    decision it was that repair could not be effected without a
    hazardous waste management unit shutdown.
    9)
    The expected date of successful repair of the leak if a
    leak
    is not repaired within 15 calendar days.
    10)
    The date of successful repair of the leak.
    e)
    Design documentation and monitoring, operating and inspection
    information for each closed-vent system and control device
    required to comply with the provisions of Section 725.960 must be
    recorded and kept up-to-date in the facility operating record as
    specified in Section 725.935(c)(1) and
    (c)(2), and monitoring,
    operating and inspection information in Section 725.935(c)(3)
    through (c)(8).
    f)
    For a contro l device other than a thermal vapor incinerator,
    catalytic vapor incinerator, flare, boiler, process heater,
    condenser, or carbon adsorption system, monitoring and inspection
    information indicating proper operation and maintenance of the
    control device must be recorded in the facility operating record.
    g)
    The following information pertaining to all equipment subject to
    the requirements in Sections 725.952 through 725.960 must be
    recorded in a log that is kept in the facility operating record:
    1)
    A list of identification numbers for equipment (except
    welded fittings) subject to the requirements of this
    Subpart.
    2)
    List of Equipment
    A)
    A list of identification numbers for equipment that
    the owner or operator elects to designate for no
    detectable emissions, as indicated by an instrument
    reading of less than 500
    ppm above background, under
    the provisions of Sections 725.952(e), 725.953(i) and
    725.957(f).
    B)
    The designation of this equipment as subject to the
    requirements of Sections 725.952(e), 725.953(i) or
    725.957(f) must be signed by the owner or operator.
    3)
    A list of equipment identification numbers for pressure
    relief devices required to comply with Section 725.954(a).
    4)
    Compliance tests.
    268
    A)
    The dates of each compliance test required in Sections
    725.952(e), 725.953(i), 725.954
    , and 725.957(f).
    B)
    The background level measured during each compliance
    test.
    C)
    The maximum instrument reading measured at the
    equipment during each compliance test.
    5)
    A list of identification nu
    mbers for equipment in vacuum
    service.
    6)
    Identification, either by list or location (area or group)
    of equipment that contains or contacts hazardous waste with
    an organic concentration of at least 10 percent by weight
    for a period of less than 300 hours per year.
    h)
    The following information pertaining to all valves subject to the
    requirements of Section 725.957(g) and (h) must be recorded in a
    log that is kept in the facility operating record:
    1)
    A list of identification numbers for valves that ar
    e
    designated as unsafe to monitor, an explanation for each
    valve stating why the valve is unsafe to monitor, and the
    plan for monitoring each valve.
    2)
    A list of identification numbers for valves that are
    designated as difficult to monitor, an explanation for each
    valve stating why the valve is difficult to monitor, and the
    planned schedule for monitoring each valve.
    i)
    The following information must be recorded in the facility
    operating record for valves complying with Section 725.962:
    1)
    A schedul e of monitoring.
    2)
    The percent of valves found leaking during each monitoring
    period.
    j)
    The following information must be recorded in a log that is kept
    in the facility operating record:
    1)
    Criteria required in Section 725.952(d)(5)(B) and
    725.953(e)(2) and an explanation of the criteria.
    2)
    Any changes to these criteria and the reasons for the
    changes.
    k)
    The following information must be recorded in a log that is kept
    in the facility operating record for use in determining exemptions
    as provided in Section 725.950 and other specific Subparts:
    1)
    An analysis determining the design capacity of the hazardous
    waste management unit.
    2)
    A statement listing the hazardous waste influent to and
    effluent from each hazardous waste management unit subject
    to the requirements in Sections 725.960 and an analysis
    determining whether these hazardous wastes are heavy
    liquids.
    269
    3)
    An up-to-date analysis and the supporting information and
    data used to determine whether or not equipment is subject
    to the requirements in Sections 725.952 through 725.960.
    The record must include supporting documentation as required
    by Section 725.963(d)(3) when application of the knowledge
    of the nature of the hazardous wastestream or the process by
    which it was produced is used. If the owner or operator
    takes any action (e.g., changing the process that produced
    the waste) that could result in an increase in the total
    organic content of the waste contained in or contacted by
    equipment determined not to be subject to the requirements
    in Sections 725.952 through 725.960, then a new
    determination is required.
    l)
    Records of the equipment leak information required by subsection
    (d) (above) and the operating information required by subsection
    (e) (above) need be kept only 3 years.
    m)
    The owner or operator of any facility that is subject to this
    Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61,
    Subpart V, incorporated by reference in 35 Ill. Adm. Code 720.111,
    may elect to determine compliance with this Subpart by
    documentation either pursuant to Section 725.964, or pursuant to
    those provisions of 40 CFR 60 or 61, to the extent that the
    documentation under the regulation at 40 CFR 60 or 61 duplicates
    the documentation required under this Subpart. The documentation
    under the regulation at 40 CFR 60 or 61 must be kept with or made
    readily available with the facility operating record.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
    SURFACE IMPOUNDMENTS, AND CONTAINERS
    Section 725.980
    Applicability
    a)
    The requirements of this Subpart apply, effective October 6, 1996,
    to owners and operators of all facilities that treat, store, or
    dispose of hazardous waste in tanks, surface
    impoundments, or
    containers that are subject to 725.Subpart I, J, or K, except as
    Section 725.101 and subsection (b) below provide otherwise.
    BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
    (Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828
    (May 19, 1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed.
    Reg. 28508 (June 5, 1996), USEPA delayed the effective date until
    October 6, 1996. If action by USEPA or a decision of a federal
    court changes the effectiveness of these regulations, the Board
    does not intend that 725.Subpart CC be enforceable to the extent
    that it becomes more stringent that the federal regulations upon
    which they are based.
    b)
    The requirements of this Subpart do not apply to the following
    waste management units at the facility:
    1)
    A waste management unit that holds hazardous waste placed in
    the unit before October 6, 1996 and in which no hazardous
    waste is added to the unit on or after this date.
    270
    2)
    A container that has a design capacity less than or equal to
    0.1 m
    3
    (3.5 ft
    3
    or 26.4 gal).
    3)
    A tank in which an owner or operator has stopped adding
    hazardous waste and the owner or operator has begun
    implementing or completed closure pursuant to an approved
    closure plan.
    4)
    A surface impoundment in which an
    owner or operator has
    stopped adding hazardous waste (except to implement an
    approved closure plan) and the owner or operator has begun
    implementing or completed closure pursuant to an approved
    closure plan.
    5)
    A waste management unit that is used solely for on-site
    treatment or storage of hazardous waste that is generated as
    the result of implementing remedial activities required
    pursuant to the Act or Board regulations or under the
    corrective action authorities of RCRA sections 3004(u),
    3004(v) or 3008(h); CERCLA authorities; or similar federal
    or state authorities.
    6)
    A waste management unit that is used solely for the
    management of radioactive mixed waste in accordance with all
    applicable regulations under the authority of the Atomic
    Energy Act (42 U.S.C. 2011 et seq.) and the Nuclear Waste
    Policy Act.
    7)
    A hazardous waste management unit that the owner or operator
    certifies is equipped with and operating air emission
    controls in accordance with the requirements of an
    applicable federal Clean Air Act regulation codified under
    40 CFR 60, 61, or 63. For the purpose of complying with
    this subsection, a tank for which the air emission control
    includes an enclosure, as opposed to a cover, must be in
    compliance with the enclosure and control device
    requirements of Section 725.985(i), except as provided in
    Section 725.983(c)(5).
    8)
    A tank that has a process vent, as defined in 35 Ill. Adm.
    Code 725.931.
    c)
    For the owner and operator of a facility subject to this Subpart
    whothat has received a final RCRA permit prior to October 6, 1996,
    the following requirements apply:
    1)
    The requirements of 35 Ill. Adm. Code 724.Subpart CC must be
    incorporated into the permit when the permit is reissued,
    renewed, or modified in accordance with the requirements of
    35 Ill. Adm. Code 703 and 705.
    2)
    Until the date when the permit is reissued, renewed, or
    modified in accordance with the requirements of 35 Ill. Adm.
    Code 703 and 705, the owner and operator is subject to the
    requirements of this Subpart.
    d)
    The re quirements of this Subpart, except for the
    recordkeeping
    requirements specified in Section 725.990(i) are stayed for a tank
    or container used for the management of hazardous waste generated
    by organic peroxide manufacturing and its associated laboratory
    operations, when the owner or operator of the unit meets all of
    271
    the following conditions:
    1)
    The owner or operator identifies that the tank or container
    receives hazardous waste generated by an organic peroxide
    manufacturing process producing more than one functional
    family of organic peroxides or multiple organic peroxides
    within one functional family, that one or more of these
    organic peroxides could potentially undergo self-
    accelerating thermal decomposition at or below ambient
    temperatures, and that organic peroxides are the predominant
    products manufactured by the process. For the purposes of
    this subsection, "organic peroxide" means an organic
    compound that contains the bivalent
    -O-O- structure and
    which may be considered to be a
    sturctural derivative of
    hydrogen peroxide where one or both of the hydrogen atoms
    has been replaced by an organic radical.
    2)
    The owner or operator prepares documentation, in accordance
    with Section 725.990(i), explaining why an undue safety
    hazard would be created if air emission controls specified
    in Sections 725.985 through 725.988 are installed and
    operated on the tanks and containers used at the facility to
    manage the hazardous waste generated by the organic peroxide
    manufacturing process or processes meeting the conditions of
    subsection (d)(1) above.
    3)
    The owner or operator notifies the Agency in writing that
    hazardous waste generated by an organic peroxide
    manufacturing process or processes meeting the conditions of
    subsection (d)(1) above are managed at the facility in tanks
    or containers meeting the conditions of subsection (d)(2)
    above. The notification must state the name and address of
    the facility and be signed and dated by an authorized
    representative of the facility owner or operator.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.981
    Definitions
    As used in this Subpart and in 35 Ill. Adm. Code 724, all terms not defined
    herein shall have the meaning given to them in the Act and 35 Ill. Adm. Code
    720 through 726.
    "Average volatile organic concentration" or "average VO
    concentration" means the mass-weighted average volatile organic
    concentration of a hazardous waste, as determined in accordance
    with the requirements of Section 725.984.
    "Closure device" means a cap, hatch, lid, plug, seal, valve, or
    other type of fitting that blocks an opening in a cover so that
    when the device is secured in the closed position it prevents or
    reduces air pollutant emissions to the atmosphere. Closure
    devices include devices that are detachable from the cover (e.g.,
    a sampling port cap), manually operated (e.g., a hinged access lid
    or hatch), or automatically operated (e.g., a spring
    -loaded
    pressure relief valve).
    "Continuous seal" means a seal that forms a continuous closure
    that completely covers the space between the edge of the floating
    roof and the wall of a tank. A continuous seal may be a
    vapor-mounted seal, liquid
    -mounted seal, or metallic shoe seal. A
    272
    continuous seal may be constructed of fastened segments so as to
    form a continuous seal.
    "Cover" means a device
    or system that is placed on orprovides a
    continuous barrier
    over athe hazardous waste
    such that the entire
    hazardous waste surface area is enclosed and
    sealed managed in a
    unit to prevent or reduce air emissions to the atmosphere. A
    cover may have openings
    (such as access hatches, sampling ports,
    and gauge wells ) that are necessary for operation, inspection,
    maintenance, or repair of the unit on which the cover is
    installed
    provided that each opening is closed and sealed when not in
    used.
    Examples of covers include a fixed roof installed on a tank, a
    floating membrane cover installed on a surface impoundment, a lid
    installed on a drum, or an enclosure in which an open container is
    placed during waste
    treatment. A cover may be a separate piece of
    equipment which can be detached and removed from the unit or a
    cover may be formed by structural features permanently integrated
    into the design of the unit.
    "Enclosure" means a structure that surrounds a tank or container,
    captures organic vapors emitted from the tank or container, and
    vents the captured vapors through a closed
    -vent system to a
    control device.
    "External floating roof" means a pontoon
    -type or double-deck type
    floating roofcover that rests on the surface of a hazardous waste
    being managed in a tank
    that haswith no fixed roof.
    "Fixed roof" means a
    rigid cover that is installed mounted on a
    unit in a stationary position
    so that itand does not move with
    fluctuations in the level of the
    hazardous waste placed material
    managed in a tankthe unit .
    "Floating membrane cover" means a cover consisting of a synthetic
    flexible membrane material that rests upon and is supported by the
    hazardous waste being managed in a surface impoundment.
    "Floating roof" m
    eans a pontoon-type or double-deck-
    typecover
    consisting of a double deck, pontoon single deck, or internal
    floating cover that rests upon and is supported by the
    hazardous
    wastematerial being managed in a tankcontained , and is equipped
    with a closure continuous seal or seals to close the space between
    the cover edge and the tank wall
    .
    "Hard-piping" means pipe or tubing that is manufactured and
    properly installed in accordance with relevant standards and good
    engineering practices.
    "In light material service" means the container is used to manage
    a material for which both of the following conditions apply: the
    vapor pressure of one or more of the organic constituents in the
    material is greater than 0.3
    kilopascals ( kPa) at 20
    ยฐ
    C (1.2 inches
    H
    2
    O at 68
    ยฐ
    F); and the total concentration of the pure organic
    constituents having a vapor pressure greater than 0.3
    kPa at 20
    ยฐ
    C
    (1.2 inches H
    2
    O at 68
    ยฐ
    F) is equal to or greater than 20 percent by
    weight.
    "Internal floating roof" means a
    floating roofcover that rests or
    floats on the material surface (but not necessarily in complete
    contact with it)
    of a hazardous waste being managed
    inside a tank
    273
    that has a fixed roof.
    "Liquid-mounted seal" means a foam or liquid-filled primary seal
    mounted in contact with the hazardous waste between the tank wall
    and the floating roof, continuously around the circumference of
    the tank.
    "Malfunction" means any sudden, infrequent, and not reasonably
    preventable failure of air pollution control equipment, process
    equipment, or a process to operate in a normal or usual manner. A
    failure that is caused in part by poor maintenance or careless
    operation is not a malfunction.
    "Maximum organic vapor pressure" means the equilibrium partial
    pressure exerted by the hazardous waste contained in a tank,
    determined at the temperature equal to either:
    The local maximum monthly average temperature as reported by
    the National Weather Service, when the hazardous waste is
    stored or treated at ambient temperature, or
    The highest calendar-m
    onth average temperature of the
    hazardous waste, when the hazardous waste is stored at
    temperatures above the ambient temperature or when the
    hazardous waste is stored or treated at temperatures below
    the ambient temperature.
    "Maximum organic vapor pressure" means the sum of the individual
    organic constituent partial pressures exerted by the material
    contained in a tank at the maximum vapor pressure
    -causing
    conditions (i.e., temperature, agitation, pH effects of combining
    wastes, etc.) reasonably expected to occur in the tank. For the
    purpose of this Subpart, maximum organic vapor pressure is
    determined using the procedures specified in Section 725.984(c).
    "Metallic shoe seal" means a continuous seal that is constructed
    of metal sheets that are held vertically against the wall of the
    tank by springs, weighted levers, or other mechanisms and which is
    connected to the floating roof by braces or other means. A
    flexible coated fabric (envelope) spans the annular space between
    the metal sheet and the floating roof.
    "No detectable organic emissions" means no escape of
    organics from
    a device or system
    to the atmosphere, as determined
    : using the
    procedure specified in Section 725.984(d).
    By an instrument reading less than 500 parts per million by
    volume ( ppmv) above the background level at each joint,
    fitting, and seal, when measured in accordance with the
    requirements of Method 21 in 40 CFR 60, Appendix A, and
    By no visible openings or defects in the device or system
    such as rips, tears, or gaps.
    "Point of waste origination" means as follows:
    When the facility owner or operator is the generator of the
    hazardous waste, the "point of waste origination" means the
    point where a solid waste produced by a system, process, or
    waste management unit is determined to be a hazardous waste,
    as defined in 35 Ill. Adm. Code 721.
    274
    BOARD NOTE: In this case, this term is being used in a
    manner similar to the use of the term "point of generation"
    in air standards established for waste management operations
    under authority of the federal Clean Air Act in 40 CFR 60,
    61, and 63.
    When the facility owner and operator are not the generator
    of the hazardous waste, "point of waste origination" means
    the point where the owner or operator accepts delivery or
    takes possession of the hazardous waste.
    "Point of waste treatment" means the point where a hazardous waste
    to be treated in accordance with Section 725.983(c)(2)
    exits a
    waste management unit used to destroy, degrade, or remove
    organics
    in the hazardous waste
    the treatment process
    . Any waste
    determination must be made before the waste is conveyed, handled,
    or otherwise managed in a manner that allows the waste to
    volatilize to the atmosphere.
    "Safety device" means a closure device, such as a pressure relief
    valve, frangible disc, fusible plug, or any other type of device,
    which functions exclusively to prevent physical damage or
    permanent deformation to a unit or its air emission control
    equipment by venting gases or vapors directly to the atmosphere
    during unsafe conditions resulting from an unplanned, accidental,
    or emergency event. For the purpose of this Subpart, a safety
    device is not used for routine venting of gases or vapors from the
    vapor headspace underneath a cover such as during filling of the
    unit or to adjust the pressure in this vapor
    headspace in response
    to normal daily diurnal ambient temperature fluctuations. A
    safety device is designed to remain in a closed position during
    normal operations and open only when the internal pressure, or
    another relevant parameter, exceeds the device threshold setting
    applicable to the air emission control equipment as determined by
    the owner or operator based on manufacturer recommendations,
    applicable regulations, fire protection and prevention codes,
    standard engineering codes and practices, or other requirements
    for the safe handling of flammable, ignitable, explosive,
    reactive, or hazardous materials.
    "Single -seal system" means a floating roof having one continuous
    seal. This seal may be vapor
    -mounte d, liquid -mounted, or a
    metallic shoe seal.
    "Vapor-mounted seal" means a
    foam-filled primary seal mounted
    continuous ly around the circumference of the tank so that there is
    an annular seal that is mounted so that there is a
    vapor space
    underneath between the hazardous waste in the unit and the bottom
    of the seal. The annular vapor space is bounded by the bottom of
    the primary seal, the tank wall, the hazardous waste surface, and
    the floating roof.
    "Volatile organic concentration" or "VO concentration"
    means the
    fraction by weight of organic compounds
    contained in a hazardous
    waste expressed in terms of parts per million (
    ppmw), as
    determined by direct measurement
    , using Method 25D,
    or by
    knowledge of the waste, in accordance with the requirements of
    Section 725.984. For the purpose of determining the VO
    concentration of a hazardous waste, organic compounds with a
    Henry's law constant value of at least 0.1 mole-fraction-in-the-
    275
    gas-phase/mole-fraction-in the liquid-phase (0.1 Y/X) (which can
    also be expressed as 1.8
    ร—
    10
    -6
    atmospheres/gram
    -mole/m
    3
    ) at 25
    ยฐ
    C
    (77
    ยฐ
    F) must be included. Section 725.Appendix F presents a list
    of compounds known to have a Henry's law constant value less than
    the cutoff level.
    "Waste determination" means performing all applicable procedures
    in accordance with the requirements of Section 725.984 to
    determine whether a hazardous waste meets standards specified in
    this Subpart. Examples of a waste determination include
    performing the procedures in accordance with the requirements of
    Section 725.984 to determine the average VO concentration of a
    hazardous waste at the point of waste origination, determining the
    average VO concentration of a hazardous waste at the point of
    waste treatment and comparing the results to the exit
    concentration limit specified for the process used to treat the
    hazardous waste,
    determining the organic reduction efficiency and
    the organic biodegradation efficiency for a biological process
    used to treat a hazardous waste and comparing the results to the
    applicable standards, or determining the maximum volatile organic
    vapor pressure for a hazardous waste in a tank and comparing the
    results to the applicable standards.
    "Waste stabilization process" means any physical or chemical
    process used to either reduce the mobility of hazardous
    constituents in a hazardous waste or eliminate free liquids as
    determined by Test Method 9095 (Paint Filter Liquids Test) in
    "Test Methods for Evaluating Solid Waste, Physical/Chemical
    Methods", incorporated by reference in Section 720.111. A waste
    stabilization process includes mixing the hazardous waste with
    binders or other materials and curing the resulting hazardous
    waste and binder mixture. Other synonymous terms used to refer to
    this process are "waste fixation" or "waste solidification".
    This
    does not include the addition of absorbent materials to the
    surface of a waste to absorb free liquid without mixing,
    agitation, or subsequent curing.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.983
    Standards: General
    a)
    This Section applies to the management of hazardous waste in
    tanks, surface impoundments, and containers subject to this
    Subpart.
    b)
    The owner or operator shall control air emissions from each waste
    management unit in accordance with standards specified in Sections
    725.985 through Section 725.988, as applicable to the waste
    management unit, except as provided for in subsection (c) below.
    c)
    A waste management
    unittank, surface impoundment, or container
    is
    exempted from standards specified in Section
    s 725.985 through
    Section 725.988, provided that all hazardous waste placed in the
    waste management unit is
    determined by the owner or operator to
    meet either one of the following
    conditions :
    1) The average VO concentration of
    theA tank, surface
    impoundment, or container for which all
    hazardous waste
    entering the unit has an average VO concentration
    at the
    point of waste origination
    isof less than 100500 parts per
    million by weight (
    ppmw). The average VO concentration must
    276
    be determined by the procedures specified in Section
    725.984(a). The owner or operator shall review and update,
    as necessary, this determination at least once every 12
    months following the date of the initial determination for
    the hazardous waste streams entering the unit.
    2) TA tank, surface impoundment, or container for which t
    he
    organic content of
    all the hazardous waste
    entering the
    waste management unit
    has been reduced by an organic
    destruction or removal process that achieves any one of the
    following conditions:
    A)
    The process removes or destroys the
    organics contained
    in the hazardous waste to such a level that the
    average VO concentration of the hazardous waste at the
    point of waste treatment is less than the exit
    concentration limit (C
    t
    ) established for the process.
    The average VO concentration of the hazardous waste
    at the point of waste treatment and the exit
    concentration limit for the process must be determined
    using the procedures specified in Section 725.984(b).
    B)
    The process removes or destroys the
    organics contained
    in the hazardous waste to such a level that the
    organic reduction efficiency (R) for the process is
    equal to or greater than 95 percent, and the average
    VO concentration of the hazardous waste at the point
    of waste treatment is less than
    50100 ppmw. The
    organic reduction efficiency for the process and the
    average VO concentration of the hazardous waste at the
    point of waste treatment must be determined using the
    procedures specified in Section 725.984(b).
    C)
    The process removes or destroys the
    organics contained
    in the hazardous waste to a level such that the actual
    organic mass removal rate (MR) for the process is
    equal to or greater than the required organic mass
    removal rate (RMR) established for the process. The
    required organic mass removal rate and the actual
    organic mass removal rate for the process shall be
    determined using the procedures specified in Section
    724.983(b).
    D)
    The process is a biological process that destroys or
    degrades the organics contained in the hazardous waste
    so that either of the following conditions is met:
    i)
    The organic reduction efficiency (R) for the
    process is equal to or greater than 95 percent,
    and the organic biodegradation efficiency (
    R
    bio
    )
    for the process is equal to or greater than 95
    percent. The organic reduction efficiency and
    the organic biodegradation efficiency for the
    process must be determined
    in accordance
    withusing the procedures specified in Section
    725.984(b).
    ii)
    The total actual organic mass
    biodegradation
    rate ( MR
    bio
    ) for all hazardous waste treated by
    the process is equal to or greater than the
    required organic mass removal rate (RMR). The
    277
    required organic mass removal rate and the
    actual organic mass
    biodegradation rate for the
    process must be determined using the procedures
    specified in Section 725.984(b).
    E)
    The process is one that removes or destroys the
    organics contained in the hazardous waste and meets
    all of the following conditions:
    i) All of the materials entering the proc
    ess are
    hazardous wastes.
    ii)
    From the point of waste origination through the
    point where the hazardous waste enters the
    treatment process, the hazardous waste is
    continuously managed in waste management units
    that use air emission controls in accordance
    with the standards specified in Section 725.985
    through Section 725.988, as applicable to the
    waste management unit.
    ii)
    From the point of waste origination through the
    point where the hazardous waste enters the
    treatment process, any transfer of the hazardous
    waste is accomplished through continuous
    hard-piping or other closed system transfer that
    does not allow exposure of the waste to the
    atmosphere.
    BOARD NOTE: The USEPA considers a drain system
    that meets the requirements of 40 CFR 63,
    subpart RR, "National Emission Standards for
    Individual Drain Systems", to be a closed
    system.
    iii)
    The average VO concentration of the hazardous
    waste at the point of waste treatment is less
    than the lowest average VO concentration at the
    point of waste origination determined for each
    of the individual hazardous waste streams
    entering the process or
    100500 ppmw, whichever
    value is lower. The average VO concentration of
    each individual hazardous waste stream at the
    point of waste origination must be determined
    using the procedure
    s specified in Section
    725.984(a). The average VO concentration of the
    hazardous waste at the point of waste treatment
    must be determined using the procedure
    s
    specified in Section 725.984(b).
    F)
    A process that removes or destroys the
    organics
    contained in the hazardous waste to a level such that
    the organic reduction efficiency (R) for the process
    is equal to or greater than 95 percent and the owner
    or operator certifies that the average VO
    concentration at the point of waste origination for
    each of the individual waste streams entering the
    process is less than 10,000
    ppmw. The organic
    reduction efficiency for the process and the average
    VO concentration of the hazardous waste at the point
    of waste origination shall be determined using the
    278
    procedures specified in Section 724.983(b) and Section
    724.983(a), respectively.
    FG)
    A hazardous waste incinerator for which
    either of the
    owner or operator has
    either following conditions is
    true:
    i) BThe owner or operator has b
    een issued a final
    permit under 35 Ill. Adm. Code
    702, 703, and
    705, and designs and operates the unit in
    accordance with that implements the requirements
    of 724726.Subpart OH; or
    ii)
    The owner or operator has
    certified compliance
    for the unitdesigned and operates the
    incinerator in accordance
    with the interim
    status requirements of 725.Subpart O.
    GH)
    A boiler or industrial furnace for which
    either of the
    owner or operator has
    either following conditions is
    true:
    i) BThe owner or operator has b
    een issued a final
    permit under 35 Ill. Adm. Code
    702, 703, and
    705, and designs and operates the unit in
    accordance with that implements the requirements
    of 35 Ill. Adm. Code 726.Subpart H, or
    ii)
    The owner or operator has
    certified
    compliance designed and operates the industrial
    furnace or incinerator in accordance
    for the
    unit with the interim status requirements of 35
    Ill. Adm. Code 726.Subpart H.
    I)
    For the purpose of determining the performance of an
    organic destruction or removal process in accordance
    with the conditions in each of subsections (c)(2)(A)
    through (c)(2)(F) above, the owner or operator shall
    account for VO concentrations determined to be below
    the limit of detection of the analytical method by
    using the following VO concentration:
    i)
    If Method 25D in 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, is used for the analysis, one
    -half the
    blank value determined in the method.
    ii)
    If any other analytical method is used, one
    -half
    the limit of detection established for the
    method.
    3)
    A tank used for biological treatment of hazardous waste in
    accordance with the requirements of subsection (c)(2)(D)
    above.
    4)
    A tank, surface impoundment, or container for which all
    hazardous waste placed in the unit fulfills either of the
    following two conditions:
    A)
    It meets the numerical concentration limits for
    organic hazardous constituents, applicable to the
    279
    hazardous waste, as specified in 35 Ill. Adm. Code
    728.Table T; or
    B)
    It has been treated by the treatment technology
    established by USEPA for the waste in 35 Ill. Adm.
    Code 728.142(a), or treated by an equivalent method of
    treatment approved by the Agency pursuant to 35 Ill.
    Adm. Code 728.142(b).
    5)
    A tank used for bulk feed of hazardous waste to a waste
    incinerator and all of the following conditions are met:
    A)
    The tank is located inside an enclosure vented to a
    control device that is designed and operated in
    accordance with all applicable requirements specified
    under 40 CFR 61, subpart FF, "National Emission
    Standards for Benzene Waste Operations", incorporated
    by reference in 35 Ill. Adm. Code 720.111, for a
    facility at which the total annual benzene quantity
    from the facility waste is equal to or greater than 10
    megagrams (11 tons) per year;
    B)
    The enclosure and control device serving the tank were
    installed and began operation prior to November 25,
    1996; and
    C)
    The enclosure is designed and operated in accordance
    with the criteria for a permanent total enclosure as
    specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. The enclosure may have permanent or
    temporary openings to allow worker access; passage of
    material into or out of the enclosure by conveyor,
    vehicles, or other mechanical or electrical equipment;
    or to direct air flow into the enclosure. The owner
    or operator shall perform the verification procedure
    for the enclosure as specified in Section 5.0 to
    "Procedure T --Criteria for and Verification of a
    Permanent or Temporary Total Enclosure" annually.
    d) When a process is used for the purpose of treating a hazardous
    waste to meet one of the sets of conditions specified in
    subsections (c)(2)(A) through (c)(2)(E) above, each material
    removed from or exiting the process that is not a hazardous waste
    but which has an average VO concentration equal to or greater than
    100 ppmw shall be managed in a waste management unit in accordance
    with the requirements of subsection (b) above.
    ed)
    The Agency may at any time perform or request that the owner or
    operator perform a waste determination for a hazardous waste
    managed in a tank, surface impoundment, or container that is
    exempted from using air emission controls under the provisions of
    this Section as follows:
    1)
    The waste determination for average VO concentration of a
    hazardous waste at the point of waste origination must be
    performed using direct measurement in accordance with the
    applicable requirements of Section 725.984(a). The waste
    determination for a hazardous waste at the point of waste
    280
    treatment must be performed in accordance with the
    applicable requirements of Section 725.984(b).
    2)
    In performing a waste determination pursuant to subsection
    (d)(1) above, the sample preparation and analysis shall be
    conducted as follows:
    A)
    In accordance with the method used by the owner or
    operator to perform the waste analysis, except in the
    case specified in subsection (d)(2)(B) below.
    B)
    If the Agency determines that the method used by the
    owner or operator was not appropriate for the
    hazardous waste managed in the tank, surface
    impoundment, or container, then the Agency may choose
    an appropriate method.
    23)
    Where the owner or operator
    is requested to perform the
    waste determination, the Agency may elect to have an
    authorized representative observe the collection of the
    hazardous waste samples used for the analysis.
    34)
    Where the results of the waste determination performed or
    requested by the Agency do not agree with the results of a
    waste determination performed by the owner or operator using
    knowledge of the waste, then the results of the waste
    determination performed in accordance with the requirements
    of subsection ( ed)(1) above must be used to establish
    compliance with the requirements of this Subpart.
    45)
    Where the owner or operator has used an averaging period
    greater than one hour for determining the average VO
    concentration of a hazardous waste at the point of waste
    origination, the Agency may elect to establish compliance
    with this Subpart by performing or requesting that the owner
    or operator perform a waste determination using direct
    measurement, based on waste samples collected within a 1-
    hour period as follows:
    A)
    The average VO concentration of the hazardous waste at
    the point of waste origination must be determined by
    direct measurement in accordance with the requirements
    of Section 725.984(a).
    B)
    Results of the waste determination performed or
    requested by the Agency showing that the average VO
    concentration of the hazardous waste at the point of
    waste origination is equal to or greater than
    100500
    ppmw shall constitute noncompliance with this Subpart,
    except in a case as provided for in subsection
    (ed)(4)(C) below.
    C)
    Where the average VO concentration of the hazardous
    waste at the point of waste origination previously has
    been determined by the owner or operator using an
    averaging period greater than one hour to be less than
    100500 ppmw but because of normal operating process
    variations the VO concentration of the hazardous waste
    determined by direct measurement for any given 1-hour
    period may be equal to or greater than
    100500 ppmw,
    information that was used by the owner or operator to
    281
    determine the average VO concentration of the
    hazardous waste (e.g., test results, measurements,
    calculations, and other documentation) and recorded in
    the facility records in accordance with the
    requirements of Sections 725.984(a) and 725.990 must
    be considered by the Agency together with the results
    of the waste determination performed or requested by
    the Agency in establishing compliance with this
    Subpart.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.984
    Waste Determination Pro
    cedures
    a)
    Waste determination procedure for volatile organic (VO)
    concentration of a hazardous waste at the point of waste
    origination.
    1)
    An owner or operator shall determine the average VO
    concentration at the point of waste origination for each
    hazardous waste placed in a waste management unit exempted
    under the provisions of Section 725.983(c)(1) from using air
    emission controls in accordance with standards specified in
    Section 725.985 through Section 725.988, as applicable to
    the waste management unit.
    2) When the facility owner or operator is the generator of the
    hazardous waste,
    tThe owner or operator shall determine the
    average VO concentration of
    thea hazardous waste
    at the
    point of waste origination must be determined
    using either
    direct measurement, as specified in subsection (a)(
    53)
    below, or by knowledge of the waste, as specified in
    subsection (a)( 64) below , for each hazardous waste generated
    as follows: .
    A) When the hazardous waste is generated as part of a
    continuous process, the owner or operator shall:
    i) Perform an initial waste determination of the
    average VO concentration of the waste stream
    before the first time any portion of the
    material in the waste stream is placed in a
    waste management unit subject to this Subpart
    and thereafter update the information used for
    the waste determination at least once every 12
    months following the date of the initial waste
    determination; and
    ii) Perform a new waste determination whenever
    changes to the source generating the waste
    stream are reasonably likely to cause the
    average VO concentration of the hazardous waste
    to increase to a level that is equal to or
    greater than the applicable VO concentration
    limits specified in Section 725.983.
    B) When the hazardous waste is generated as part of a
    batch process that is performed repeatedly but not
    necessarily continuously, the owner or operator shall:
    i) Perform an initial waste determination of the
    282
    average VO concentration for one or more
    representative waste batches generated by the
    process, before the first time any portion of
    the material in the batches is placed in a waste
    management unit subject to this Subpart, and
    thereafter update the information used for the
    waste determination at least once every 12
    months following the date of the initial waste
    determination; and
    ii) Perform a new waste determination whenever
    changes to the process generating the waste
    batches are reasonably likely to cause the
    average VO concentration of the hazardous waste
    to increase to a level that is equal to or
    greater than the applicable VO concentration
    limits specified in Section 725.983.
    3) When the facility owner and operator is not the generator of
    the hazardous waste, the owner or operator shall determine
    the average VO concentration of the hazardous waste using
    either direct measurement, as specified in subsection (a)(5)
    below, or knowledge of the waste, as specified in subsection
    (a)(6) below, for each hazardous waste entering the facility
    as follows:
    A) When the hazardous waste
    enters the facility as a
    continuous flow of material through a pipeline or
    other means (e.g., wastewater stream), the owner or
    operator shall:
    i) Perform an initial waste determination of the
    waste stream before the first time any portion
    of the material in the waste stream is placed in
    a waste management unit subject to this Subpart,
    and thereafter update the information used for
    the waste determination at least once every 12
    months following the date of the initial waste
    determination; and
    ii) Perform a new waste determination whenever
    changes to the source generating the waste
    stream are reasonably likely to cause the
    average VO concentration of the hazardous waste
    to increase to a level that is equal to or
    greater than the applicable VO concentration
    limits specified in Section 725.983.
    B) When the hazardous waste enters the facility in a
    container, the owner or operator shall perform a waste
    determination for the material held in each container.
    4) Where the average VO concentration of
    the hazardous waste is
    determined by the owner or operator to be less than 100
    ppmw, but because of normal operating variations in the
    source or process generating the hazardous waste the VO
    concentration of the hazardous waste may be equal to or
    greater than 100
    ppmw at any given time during the averaging
    period, the owner or operator shall prepare and enter in the
    facility operating record information that specifies the
    following:
    283
    A) The maximum and minimum VO concentration values for
    the hazardous waste that occur during that averaging
    period used for the waste determination;
    B) The operating conditions or circumstances under which
    the VO concentration of the hazardous waste will be
    equal to or greater than 100
    ppmw; and
    C) The information and calculations used by the owner or
    operator to determine the average VO concentration of
    the hazardous waste.
    53) Procedure for using
    dDirect measurement to determine average
    VO concentration of a hazardous waste at the point of waste
    origination.
    A)
    Identification.
    The owner or operator shall identify
    and record the point of waste origination for the
    hazardous waste. All waste samples used to determine
    the average VO concentration of the hazardous waste
    must be collected at this point.
    B) The owner or operator shall designate and record the
    averaging period to be used for determining the
    average VO concentration for the hazardous waste. The
    averaging period must not exceed one year. An initial
    waste determination must be performed for each
    averaging period.
    B)
    Sampling. Samples of the hazardous waste stream must
    be collected at the point of waste origination in a
    manner such that volatilization of
    organics contained
    in the waste and in the subsequent sample is minimized
    and an adequately representative sample is collected
    and maintained for analysis by the selected method.
    i)
    The averaging period to be used for determining
    the average VO concentration for the hazardous
    waste stream on a mass
    -weighted average basis
    must be designated and recorded. The averaging
    period can represent any time interval that the
    owner or operator determines is appropriate for
    the hazardous waste stream but must not exceed
    one year.
    ii)
    A sufficient number of samples, but no less than
    four samples, must be collected for the
    hazardous waste stream to represent the complete
    range of compositions and quantities that occur
    during the entire averaging period due to normal
    variations in the operating conditions for the
    source or process generating the hazardous waste
    stream. Examples of such normal variations are
    seasonal variations in waste quantity or
    fluctuations in ambient temperature.
    iii)
    All samples must be collected and handled in
    accordance with written procedures prepared by
    the owner or operator and documented in a site
    sampling plan. This plan must describe the
    284
    procedure by which representative samples of the
    hazardous waste stream are collected such that a
    minimum loss of organics occurs throughout the
    sample collection and handling process, and by
    which sample integrity is maintained. A copy of
    the written sampling plan must be maintained
    on-site in the facility operating records. An
    example of an acceptable sampling plan includes
    a plan incorporating sample collection and
    handling procedures in accordance with the
    requirements specified in "Test Methods for
    Evaluating Solid Waste, Physical/Chemical
    Methods," EPA Publication SW
    -846, incorporated
    by reference in 35 Ill. Adm. Code 720.111, or in
    Method 25D in 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    C) The owner or operator shall identify each discrete
    quantity of the material composing the hazardous waste
    represented by the averaging period designated in
    subsection (a)(5)(B) above. An example of a discrete
    quantity of material composing a hazardous waste
    generated as part of a continuous process is the
    quantity of material generated during a process
    operating mode defined by a specific set of operating
    conditions that are normal for the process. An
    example of a discrete quantity of material composing a
    hazardous waste generated as part of a batch process
    that is performed repeatedly but not necessarily
    continuously is the total quantity of material
    composing a single batch generated by the process. An
    example of a discrete quantity of material composing a
    hazardous waste delivered to a facility in a container
    is the total quantity of material held in the
    container.
    C)
    Analysis. Each collected sample must be prepared and
    analyzed in accordance with one or more of the methods
    listed in subsections (a)(3)(C)(i) through
    (a)(3)(C)(ix), including appropriate quality assurance
    and quality control (QA/QC) checks and use of target
    compounds for calibration. If Method 25D in 40 CFR
    60, appendix A, incorporated by reference in 35 Ill.
    Adm. Code 720.111 is not used, then one or more
    methods should be chosen that are appropriate to
    ensure that the waste determination accounts for and
    reflects all organic compounds in the waste with
    Henry's law constant values at least 0.1 mole-
    fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
    phase (0.1 Y/X) [which can also be expressed as 1.8 x
    10
    -6
    atmospheres/gram
    -mole/m
    3
    ] at 25
    ยฐ
    C (77
    ยฐ
    F). Each
    of the analytical methods listed in subsections
    (a)(3)(C)(ii) through (a)(3)(C)(vii) below has an
    associated list of approved chemical compounds, for
    which USEPA considers the method appropriate for
    measurement. If an owner or operator uses USEPA
    Method 624, 625, 1624, or 1625 in 40 CFR 136, appendix
    A, incorporated by reference in 35 Ill. Adm. Code
    720.111, to analyze one or more compounds that are not
    on that method's published list, the Alternative Test
    285
    Procedure contained in 40 CFR 136.4 and 136.5,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, must be followed. If an owner or operator
    uses USEPA Method 8260(B) or 8270(C) in "Test Methods
    for Evaluating Solid Waste, Physical/Chemical
    Methods", EPA Publication SW
    -846, incorporated by
    reference in 35 Ill. Adm. Code 720.111, to analyze one
    or more compounds that are not on that method's
    published list, the procedures in subsection
    (a)(3)(C)(viii) below must be followed. At the
    owner's or operator's discretion, the concentration of
    each individual chemical constituent measured in the
    waste by a method other than Method 25D may be
    corrected to the concentration had it been measured
    using Method 25D by multiplying the measured
    concentration by the constituent
    -specific adjustment
    factor (f
    m25D
    ), as specified in subsection (a)(4)(C)
    below. Constituent
    -specific adjustment fa
    ctors (f
    m25D
    )
    can be obtained by contacting the USEPA, Waste and
    Chemical Processes Group, Office of Air Quality
    Planning and Standards, Research Triangle Park, NC
    27711.
    i)
    Method 25D in 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    ii)
    Method 624 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    iii)
    Method 625 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. Perform corrections to the compounds
    for which the analysis is being conducted based
    on the "accuracy as recovery" using the factors
    in Table 7 of the method.
    iv)
    Method 1624 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    v)
    Method 1625 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    vi)
    Method 8260(B) in "Test Methods for Evaluating
    Solid Waste, Physical/Chemical Methods", EPA
    Publication SW -846, incorporated by reference in
    35 Ill. Adm. Code 720.111. Maintain a formal
    quality assurance program consistent with the
    requirements of Method 8260(B). The quality
    assurance program must include the elements set
    forth in subsection (a)(3)(E) below.
    vii)
    Method 8270(C) in "Test Methods for Evaluating
    Solid Waste, Physical/Chemical Methods", EPA
    Publication SW -846, incorporated by reference in
    35 Ill. Adm. Code 720.111. Maintain a formal
    quality assurance program consistent with the
    requirements of Method 8270(C). The quality
    286
    assurance program must include the elements set
    forth in subsection (a)(3)(E) below.
    viii)
    Any other USEPA standard method that has been
    validated in accordance with "Alternative
    Validation Procedure for EPA Waste and
    Wastewater Methods", 40 CFR 63, appendix D,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. As an alternative, other EPA standard
    methods may be validated by the procedure
    specified in subsection (a)(3)(C)(ix) below.
    ix)
    Any other analysis method that has been
    validated in accordance with the procedures
    specified in Section 5.1 or Section 5.3, and the
    corresponding calculations in Section 6.1 or
    Section 6.3, of Method 301 in 40 CFR 63,
    appendix A, incorporated by reference in 35 Ill.
    Adm. Code 720.111. The data are acceptable if
    they meet the criteria specified in Section
    6.1.5 or Section 6.3.3 of Method 301. If
    correction is required under Section 6.3.3 of
    Method 301, the data are acceptable if the
    correction factor is within the range 0.7 to
    1.30. Other Sections of Method 301 are not
    required.
    D) The following procedure must be used measure the VO
    concentration for each discrete quantity of material
    identified in subsection (a)(5)(C) above:
    i) A sufficient number of samples, but in no case
    fewer than four, must be collected to represent
    the organic composition for the entire discrete
    quantity of hazardous waste being tested. All
    of the samples must be collected within a 1-hour
    period. Sufficient information must be prepared
    and recorded to document the waste quantity
    represented by the samples and, as applicable,
    the operating conditions for the source or
    process generating the hazardous waste
    represented by the samples.
    ii) Each sample must be collected in accordance with
    the requirements specified in "Test Methods for
    Evaluating Solid Waste, Physical/Chemical
    Methods", incorporated by reference in Section
    720.111.
    iii) Each collected sample must be prepared and
    analyzed in accordance with the requirements of
    Method 25D in 40 CFR 60, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    iv) The measured VO concentration for the discrete
    quantity of hazardous waste must be determined
    by using the results for all samples analyzed in
    accordance with subsection (a)(5)(D)(iii) above
    and the following equation:
    287
    C =
    1
    n
    x
    n
    i = 1
    C
    i
    โˆ‘
    Where:
    C = Measured VO concentration of the
    discrete quantity of hazardous
    waste, in ppmw.
    i = Individual sample "i" of the
    hazardous waste collected in
    accordance with the requirements of
    SW-846.
    n = Total number of samples of hazardous
    waste collected (at least 4) within
    a 1-hour period.
    C
    i
    = VO concentration measured by Method
    25D for sample "i", in
    ppmw.
    E) The average VO concentration of the hazardous waste
    must be determined using the following procedure:
    i) When the facility owner or operator is the
    generator of the hazardous waste, a sufficient
    number of VO concentration measurements for the
    hazardous waste must be performed in accordance
    with the requirements of subsection (a)(5)(D)
    above to represent the complete range of
    hazardous waste organic compositions and
    quantities that occur during the entire
    averaging period due to normal variations in the
    operating conditions for each process operating
    mode identified for the source or process
    generating the hazardous waste.
    ii) When the facility owner or operator is not the
    generator of the hazardous waste, a sufficient
    number of VO concentration measurements for the
    hazardous waste must be performed in accordance
    with the requirements of subsection (a)(5)(D)
    above to represent the complete range of
    hazardous waste organic compositions and
    quantities that occur in the hazardous waste as
    received at the facility during the entire
    averaging period.
    iiiD) Calculations. The average VO concentration
    of the
    hazardous waste at the point of waste origination
    (C)
    on a mass-weighted basis
    must be calculated by using
    the results for all
    VO measurements performed samples
    analyzed in accordance with subsection (a)(
    53)(DC)
    above and the following equation:
    288
    =
    T
    j
    j
    C
    1
    Q
    x
    m
    j = 1
    ( Q
    x C
    )
    โˆ‘
    C =
    1
    Q
    x
    n
    i = 1
    ( Q
    x C )
    T
    i
    i
    โˆ‘
    Where:
    C
    ave
    C =Average VO concentration of the hazardous
    waste at the point of waste
    origination on a mass-weighted
    basis, in ppmw.
    ji =
    Individual discrete quantity sample "ji" of
    the hazardous waste
    for which a VO
    concentration measurement is determined in
    accordance with the requirements of
    subsection (a)(5)(D) above
    .
    mn =
    Total number of VO concentration
    measurements determined in accordance with
    the requirements of subsection (a)(5)(D)
    abovesamples of the hazardous waste
    collected (at least four)
    for the
    averaging period (not to exceed one year)
    .
    Q
    j
    Q
    i
    = Mass of the discrete quantity quantity of
    the hazardous waste
    stream
    represented by C
    j
    C
    i
    , in kg /hr.
    Q
    T
    =
    Total mass quantity of the hazardous waste
    forduring the averaging period, in kg
    /hr.
    C
    j
    C
    i
    = Measured VO concentration of
    discrete
    quantity sample "ji", as for the
    hazardous waste determined in
    accordance with the requirements of
    subsection (a)( 53)(DC) above, in
    ppmw.
    E)
    The quality assurance
    progarm elements required under
    subsections (a)(3)(C)(vi) and (a)(3)(C)(vii) above are
    as follows:
    i)
    Documentation of site
    -specific procedures to
    minimize the loss of compounds due to
    volatilization, biodegradation, reaction, or
    sorption during the sample collection, storage,
    preparation, introduction, and analysis steps.
    ii)
    Measurement of the overall accuracy and
    precision of the specific procedures.
    BOARD NOTE: Subsections (a)(3)(E)(i) and
    (a)(3)(E)(ii) correspond with 40 CFR
    289
    265.984(a)(3)(iii)(F)(1), (a)(3)(iii)(F)(2),
    (a)(3)(iii)(G)(1), and (a)(3)(iii)(G)(2), which
    the Board has codified here to comport with
    Illinois Administrative Code format
    requirements.
    6) Procedure for using knowledge of the waste to determine the
    average VO concentration of a hazardous waste at the point
    of waste origination.
    A) The owner or operator shall identify and record the
    point of waste origination for the hazardous waste.
    All information used to determine the average VO
    concentration of the hazardous waste must be based on
    the hazardous waste composition at this point.
    B) The owner or operator shall designate and record the
    averaging period to be used for determining the
    average VO concentration for the hazardous waste. The
    averaging period must not exceed one year. An initial
    waste determination must be performed for each
    averaging period.
    C) The owner or opera
    tor shall prepare and record
    sufficient information that documents the average VO
    concentration for the hazardous waste. Information
    may be used that is prepared by either the facility
    owner or operator or by the generator of the hazardous
    waste. Examples of information that may be used as
    the basis for knowledge of the waste include: organic
    material balances for the source or process generating
    the waste; VO concentration measurements for the same
    type of waste performed in accordance with the
    procedure specified in subsection (a)(5)(D) above;
    previous individual organic constituent test data for
    the waste that are still applicable to the current
    waste management practices; documentation that the
    waste is generated by a process for which no
    organics-
    containing materials are used; previous test data for
    other locations managing the same type of waste; or
    other knowledge based on manifests, shipping papers,
    or waste certification notices.
    D) If test data other than VO concentration measurements
    performed in accordance with the procedure specified
    in subsection (a)(5)(D) above are used as the basis
    for knowledge of the waste, then the owner or operator
    shall document the test method, sampling protocol, and
    the means by which sampling variability and analytical
    variability are accounted for in the determination of
    the average VO concentration. For example, an owner
    or operator may use individual organic constituent
    concentration test data that are validated in
    accordance with Method 301 in 40 CFR 63, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, as the basis for knowledge of the waste.
    4)
    Use of owner or operator knowledge to determine average VO
    concentration of a hazardous waste at the point of waste
    origination.
    290
    A)
    Documentation must be prepared that presents the
    information used as the basis for the owner's or
    operator's knowledge of the hazardous waste stream's
    average VO concentration. Examples of information
    that may be used as the basis for knowledge include
    the following: material balances for the source or
    process generating the hazardous waste stream;
    constituent -specific chemical test data for the
    hazardous waste stream from previous testing that are
    still applicable to the current waste stream; previous
    test data for other locations managing the same type
    of waste stream; or other knowledge based on
    information included in manifests, shipping papers, or
    waste certification notices.
    B)
    If test data are used as the basis for knowledge, then
    the owner or operator shall document the test method,
    sampling protocol, and the means by which sampling
    variability and analytical variability are accounted
    for in the determination of the average VO
    concentration. For example, an owner or operator may
    use organic concentration test data for the hazardous
    waste stream that are validated in accordance with
    Method 301 in 40 CFR 63, appendix A, incorporated by
    reference in 35 Ill. Adm. Code 720.111, as the basis
    for knowledge of the waste.
    C)
    An owner or operator using chemical
    constituent -specific concentration test data as the
    basis for knowledge of the hazardous waste may adjust
    the test data to the corresponding average VO
    concentration value which would have been obtained had
    the waste samples been analyzed using Method 25D in 40
    CFR 60, appendix A, incorporated by reference in 35
    Ill. Adm. Code 720.111. To adjust these data, the
    measured concentration for each individual chemical
    constituent contained in the waste is multiplied by
    the appropriate constituent
    -specific adju stment factor
    (f
    m25D
    ).
    D)
    In the event that the Agency and the owner or operator
    disagree on a determination of the average VO
    concentration for a hazardous waste stream using
    knowledge, then the results from a determination of
    average VO concentration using direct measurement as
    specified in subsection (a)(3) above must be used to
    establish compliance with the applicable requirements
    of this Subpart. The Agency may perform or request
    that the owner or operator perform this determination
    using direct measurement.
    b)
    Waste determination procedures for treated hazardous waste.
    1)
    An owner or operator shall perform the applicable waste
    determination for each treated hazardous waste placed in a
    waste management unit exempted under the provisions of
    Section 725.983(c)(2) from using air emission controls in
    accordance with standards specified in Section
    s 725.985
    through Section 725.988, as applicable to the waste
    management unit.
    291
    2) The owner or operator shall perform a waste determination
    for each discrete quantity of treated hazardous waste as
    follows:
    A) When the hazardous waste is treated by a continuous
    process, the owner or operator shall:
    i) Perform an initial waste determination for the
    treated waste stream before the first time any
    portion of the material in the waste stream is
    placed in a waste management unit subject to
    this Subpart, and thereafter update the
    information used for the waste determination at
    least once every 12 months following the date of
    the initial waste determination; and
    ii) Perform a new waste determination whenever
    changes to the hazardous waste streams fed to
    the process are reasonably likely to cause the
    characteristics of the hazardous waste at the
    point of waste treatment to change to levels
    that fail to achieve the applicable conditions
    specified in Section 725.983(c)(2).
    B) When the hazardous waste is treated by a batch process
    that is performed repeatedly but not necessarily
    continuously, the owner or operator shall:
    i) Perform an initial waste
    determination for the
    treated hazardous waste in one or more
    representative batches treated by the process,
    and thereafter update the information used for
    the waste determination at least once every 12
    months following the date of the initial waste
    determination; and
    ii) Perform a new waste determination whenever
    changes to the hazardous waste treated by the
    process are reasonably likely to cause the
    characteristics of the hazardous waste at the
    point of waste treatment to change to levels
    that fail to achieve the applicable conditions
    specified in Section 725.983(c)(2).
    32)
    The owner or operator shall designate and record the
    specific provision in Section 725.983(c)(2)
    forunder which
    the waste determination is being performed. The waste
    determination for the treated hazardous waste must be
    performed using the applicable procedures specified in
    subsections (b)( 43) through (b)( 109) below.
    43)
    Procedure to determine the average VO concentration of a
    hazardous waste at the point of waste treatment.
    A)
    Identification.
    The owner or operator shall identify
    and record the point of waste treatment for the
    hazardous waste. All waste samples used to determine
    the average VO concentration of the hazardous waste
    must be collected at this point.
    B) The owner or operator shall designate and record the
    292
    averaging period to be used for determining the
    average VO concentration for the hazardous waste. The
    averaging period must not exceed one year. An initial
    waste determination must be performed for each
    averaging period.
    C) The owner or operator shall identify each discrete
    quantity of the material composing the hazardous waste
    represented by the averaging period designated in
    subsection (b)(4)(B) above.
    D) The following procedure shall be used to measure the
    VO concentration for each discrete quantity of
    material identified in subsection (b)(4)(C) above:
    i) A sufficient number of samples, but in no case
    fewer than four samples, must be collected to
    represent the organic composition for the entire
    discrete quantity of hazardous waste being
    tested. All of the samples must be collected
    within a 1-hour period. Sufficient information
    must be prepared and recorded to document the
    waste quantity represented by the samples and,
    as applicable, the operating conditions for the
    process treating the hazardous waste represented
    by the samples.
    ii) Each sample must be collected in accordance with
    the requirements specified in "Test Methods for
    Evaluating Solid Waste, Physical/Chemical
    Methods", incorporated by reference in 35 Ill.
    Adm. Code 720.111.
    iii) Each collected sample must be prepared and
    analyzed in accordance with the requirements of
    Method 25D in 40 CFR 60, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    iv) The measured VO concentration for the discrete
    quantity of hazardous waste must be determined
    by using the results for all samples analyzed in
    accordance with subsection (a)(5)(D)(iii) above
    and the following equation:
    C =
    1
    n
    x
    n
    i = 1
    C
    i
    โˆ‘
    Where:
    C = Measured VO concentration of the
    discrete quantity of hazardous
    waste, in ppmw.
    i = Individual sample "i" of the
    hazardous waste collected in
    accordance with the requirements of
    SW-846.
    293
    n = Total number of samples of hazardous
    waste collected (at least 4) within
    a 1-hour period.
    C
    i
    = VO concentration measured by Method
    25D for sample "i", in
    ppmw.
    B)
    Sampling. Samples of the hazardous waste stream must
    be collected at the point of waste treatment in a
    manner such that volatilization of
    organics contained
    in the waste and in the subsequent sample is minimized
    and an adequately representative sample is collected
    and maintained for analysis by the selected method.
    i)
    The averaging period to be used for determining
    the average VO concentration for the hazardous
    waste stream on a mass
    -weighted average basis
    must be designated and recorded. The averaging
    period can represent any time interval that the
    owner or operator determines is appropriate for
    the hazardous waste stream but must not exceed
    one year.
    ii)
    A sufficient number of samples, but no less than
    four samples, must be collected for the
    hazardous waste stream to represent the complete
    range of compositions and quantities that occur
    during the entire averaging period due to normal
    variations in the operating conditions for the
    process treating the hazardous waste stream.
    Examples of such normal variations are seasonal
    variations in waste quantity or fluctuations in
    ambient temperature.
    iii)
    All samples must be collected and handled in
    accordance with written procedures prepared by
    the owner or operator and documented in a site
    sampling plan. This plan must describe the
    procedure by which representative samples of the
    hazardous waste stream are collected such that a
    minimum loss of organics occurs throughout the
    sample collection and handling process, and by
    which sample integrity is maintained. A copy of
    the written sampling plan must be maintained
    on-site in the facility operating
    records. An
    example of an acceptable sampling plan includes
    a plan incorporating sample collection and
    handling procedures in accordance with the
    requirements specified in "Test Methods for
    Evaluating Solid Waste, Physical/Chemical
    Methods," EPA Publication No. SW
    -846,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, or in Method 25D in 40 CFR 60, appendix
    A, incorporated by reference in 35 Ill. Adm.
    Code 720.111.
    C)
    Analysis. Each collected sample must be prepared and
    analyzed in accordance with one or more of the methods
    listed in subsections (b)(3)(C)(i) through
    (b)(3)(C)(ix) below, including appropriate quality
    294
    assurance and quality control (QA/QC) checks and use
    of target compounds for calibration. If Method 25D in
    40 CFR 60, appendix A is not used, then one or more
    methods should be chosen that are appropriate to
    ensure that the waste determination accounts for and
    reflects all organic compounds in the waste with
    Henry's law constant values at least 0.1 mole-
    fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
    phase (0.1 Y/X) [which can also be expressed as 1.8 x
    10
    -6
    atmospheres/gram-mole/m
    3
    ] at 25 degrees Celsius.
    Each of the analytical methods listed in subsections
    (b)(3)(C)(ii) through (b)(3)(C)(vi) below has an
    associated list of approved chemical compounds, for
    which USEPA considers the method appropriate for
    measurement. If an owner or operator uses EPA Method
    624, 625, 1624, or 1625 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, to analyze one or more compounds that are not
    on that method's published list, the Alternative Test
    Procedure contained in 40 CFR 136.4 and 136.5,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, must be followed. If an owner or operator
    uses EPA Method 8260(B) or 8270(C) in "Test Methods
    for Evaluating Solid Waste, Physical/Chemical
    Methods", EPA Publication SW-846, incorporated by
    reference in 35 Ill. Adm. Code 720.111, to analyze one
    or more compounds that are not on that method's
    published list, the procedures in subsection
    (b)(3)(C)(viii) above must be followed. At the
    owner's or operator's discretion, the concentration of
    each individual chemical constituent measured in the
    waste by a method other than Method 25D may be
    corrected to the concentration had it been measured
    using Method 25D by multiplying the measured
    concentration by the constituent-specific adjustment
    factor (f
    m25D
    ) as specified in subsection (a)(4)(C)
    below. Constituent-specific adjustment factors (f
    m25D
    )
    can be obtained by contacting the USEPA, Waste and
    Chemical Processes Group, Office of Air Quality
    Planning and Standards, Research Triangle Park, NC
    27711.
    i)
    Method 25D in 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    ii)
    Method 624 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    iii)
    Method 625 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. Perform corrections to the compounds
    for which the analysis is being conducted based
    on the "accuracy as recovery" using the factors
    in Table 7 of the method.
    iv)
    Method 1624 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    295
    v)
    Method 1625 in 40 CFR 136, appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    vi)
    Method 8260(B) in "Test Methods for Evaluating
    Solid Waste, Physical/Chemical Methods", EPA
    Publication SW-846, incorporated by reference in
    35 Ill. Adm. Code 720.111. Maintain a formal
    quality assurance program consistent with the
    requirements of Method 8260(B). The quality
    assurance program must include the elements set
    forth in subsection (b)(3)(E) below.
    vii)
    Method 8270(C) in "Test Methods for Evaluating
    Solid Waste, Physical/Chemical Methods", EPA
    Publication SW-846, incorporated by reference in
    35 Ill. Adm. Code 720.111. Maintain a formal
    quality assurance program consistent with the
    requirements of Method 8270(C). The quality
    assurance program must include the elements set
    forth in subsection (b)(3)(E) below.
    viii)
    Any other EPA standard method that has been
    validated in accordance with "Alternative
    Validation Procedure for EPA Waste and
    Wastewater Methods", 40 CFR 63, appendix D,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. As an alternative, other EPA standard
    methods may be validated by the procedure
    specified in subsection (b)(3)(C)(ix) below.
    ix)
    Any other analysis method that has been
    validated in accordance with the procedures
    specified in Section 5.1 or Section 5.3, and the
    corresponding calculations in Section 6.1 or
    Section 6.3, of Method 301 in 40 CFR 63,
    appendix A. The data are acceptable if they
    meet the criteria specified in Section 6.1.5 or
    Section 6.3.3 of Method 301. If correction is
    required under Section 6.3.3 of Method 301, the
    data are acceptable if the correction factor is
    within the range 0.7 to 1.30. Other Sections of
    Method 301 are not required.
    E) The average VO concentration of the hazardous waste at
    the point of waste treatment must be determined using
    the following procedure:
    i) When the facility owner or operator is the
    generator of the hazardous waste, a sufficient
    number of VO concentration measurements for the
    hazardous waste must be performed in accordance
    with the requirements of subsection (b)(4)(D)
    above to represent the complete range of
    hazardous waste organic compositions and
    quantities treated by the process during the
    entire averaging period.
    iiD)
    Calculations. The average VO concentration
    of the
    hazardous waste at the point of waste treatment
    (C) on
    a mass-weighted basis
    must be calculated by using the
    296
    results for all VO measurements performed samples
    analyzed in accordance with subsection (b)(
    43)(DC)
    above and the following equation:
    ave
    T
    j
    j
    C
    =
    1
    Q
    x
    m
    j = 1
    ( Q
    x C
    )
    โˆ‘
    C =
    1
    Q
    x
    n
    i = 1
    ( Q
    x C )
    T
    i
    i
    โˆ‘
    Where:
    C
    ave
    C =Average VO concentration of the hazardous
    waste at the point of waste
    origination treatment on a
    mass-weighted basis , in ppmw.
    ji =
    Individual discrete quantity sample "ji" of
    the hazardous waste
    for which a VO
    concentration measurement is determined in
    accordance with the requirements of
    subsection (b)(4)(D) above
    .
    mn =
    Total number of VO concentration
    measurements determined in accordance with
    the requirements of subsection (b)(4)(D)
    abovesamples of the hazardous waste
    collected (at least 4)
    for the averaging
    period (not to exceed 1 year)
    .
    Q
    j
    Q
    i
    = Mass of the discrete quantity of the
    hazardous waste stream represented
    by C
    j
    C
    i
    , in kg /hr.
    Q
    T
    =
    Total mass quantity of the hazardous waste
    forduring the averaging period, in kg
    /hr.
    C
    j
    C
    i
    = Measured VO concentration of
    discrete
    quantity sample "ji", as for the
    hazardous waste determined in
    accordance with the requirements of
    subsection (b)( 43)(DC) above, in
    ppmw.
    54)
    Procedure to determine the exit concentration limit (C
    t
    ) for
    a treated hazardous waste.
    A)
    The point of waste origination for each hazardous
    waste treated by the process at the same time must be
    identified.
    B)
    If a sing le hazardous waste stream is identified in
    subsection (b)( 54)(A) above, then the exit
    concentration limit (C
    t
    ) must be 100500 ppmw.
    C)
    If more than one hazardous waste stream is identified
    297
    in subsection (b)(
    54)(A) above, then the
    average VO
    concentration of each hazardous waste stream at the
    point of waste origination must be determined in
    accordance with the requirements of subsection (a)
    above. The exit concentration limit (C
    t
    ) must be
    calculated by using the results determined for each
    individual hazardous waste stream and the following
    equation:
    t
    x
    x
    y
    x
    y
    C
    =
    m
    x = 1
    (Q
    x C
    )+
    n
    y = 1
    ( Q
    x100ppmw)
    m
    x = 1
    Q
    +
    n
    y = 1
    Q
    โˆ‘
    โˆ‘
    โˆ‘
    โˆ‘
    Where:
    C
    t
    =
    Exit concentration limit for treated
    hazardous waste, in
    ppmw.
    x =
    Individual hazardous waste stream "x" that
    has an average VO concentration less than
    100500 ppmw at the point of waste
    origination, as determined in accordance
    with the requirements of
    Section
    725.984 subsection (a) above .
    y =
    Individual hazardous waste stream "y" that
    has an average VO concentration equal to
    or greater than 100500 ppmw at the point
    of waste origination, as determined in
    accordance with the requirements of
    Section 725.984 subsection (a) above .
    m =
    Total number of "x" hazardous waste
    streams treated by process.
    n =
    Total number of "y" hazardous waste
    streams treated by process.
    Q
    x
    =
    Annual mass quantity of hazardous waste
    stream "x", in kg/yr.
    Q
    y
    =
    Annual mass quantity of hazardous waste
    stream "y", in kg/yr.
    C
    x
    =
    Average VO concentration of hazardous
    waste stream "x" at the point of waste
    origination, as determined in accordance
    with the requirements of
    Section
    725.984 subsection (a) above , in ppmw.
    65)
    Procedure to determine the organic reduction efficiency (R)
    for a treated hazardous waste.
    A)
    The organic reduction efficiency
    (R) for a treatment
    298
    process must be determined based on results for a
    minimum of three consecutive runs.
    The sampling time
    for each run must be one hour.
    B) The point of eachAll hazardous waste stream
    s entering
    the process and eachall hazardous waste stream
    s
    exiting the treatment process that is to be included
    in the calculation of the organic reduction efficiency
    for the process must be identified.
    The owner or
    operator shall prepare a sampling plan for measuring
    these streams that accurately reflects the retention
    time of the hazardous waste in the process.
    C)
    For each run, the following information must be
    determined for each hazardous waste stream identified
    in subsection (b)(
    65)(B) above, using the following
    procedures:
    i)
    The mass quantity of each hazardous waste stream
    entering the process (
    Q
    b
    ) and the mass quantity
    of each hazardous waste stream exiting the
    process ( Q
    a
    ) must be determined.
    ii)
    The average VO concentration
    at the point of
    waste origination
    of each hazardous waste stream
    entering the process (
    C
    b
    C
    b
    ) during the run must
    be measured determined in accordance with the
    requirements of subsections (a)(
    53)(D)(i)
    through (a)(5)(D)(iv)
    belowabove. The average
    VO concentration
    at the point of waste treatment
    of each hazardous waste stream exiting the
    process ( C
    a
    C
    a
    ) during the run must be determined
    in accordance with the requirements of
    subsection (b)( 43)(D) belowabove. Samples must
    be collected as follows: For a continuous
    process, the samples of the hazardous waste
    entering and samples of the hazardous waste
    exiting the process must be collected
    concurrently. For a batch process, the samples
    of the hazardous waste entering the process must
    be collected at the time that the hazardous
    waste is placed in the process. The samples of
    the hazardous waste exiting the process must be
    collected as soon as practicable after the time
    when the process stops operation or the final
    treatment cycle ends.
    D)
    The waste volatile organic mass flow entering the
    process ( E
    b
    ) and the waste volatile organic mass flow
    exiting the process (
    E
    a
    ) must be calculated by using
    the results determined in accordance with subsection
    (b)(65)(C) above and the following equations:
    b
    6
    bj
    bj
    E
    =
    1
    10
    m
    j = 1
    ( Q
    x C
    )
    โˆ‘
    299
    a
    6
    aj
    aj
    E
    =
    1
    10
    m
    j = 1
    (Q
    x C
    )
    โˆ‘
    b
    6
    bj
    bj
    E
    =
    1
    10
    m
    j = 1
    ( Q
    xC
    )
    โˆ‘
    a
    6
    aj
    aj
    E
    =
    1
    10
    m
    j = 1
    ( Q
    xC
    )
    โˆ‘
    Where:
    E
    a
    =
    Waste volatile organic mass flow exiting
    the process, in kg/hr.
    E
    b
    =
    Waste volatile organic mass flow entering
    the process, in kg/hr.
    m =
    Total number of runs (at least 3)
    j =
    Individual run "j"
    Q
    bj
    =
    Mass quantity of hazardous waste entering
    the process during run "j", in kg/hr.
    Q
    aj
    =
    Average mass quantity of waste exiting
    the
    process during run "j", in kg/hr.
    C
    aj
    C
    aj
    =
    Measured VO concentration of
    hazardous waste exiting
    the process
    during run "j", as determined in
    accordance with the requirements of
    Section 725.984 subsection (b)(43)(D)
    above, in ppmw.
    C
    bj
    C
    bj
    =
    Measured VO concentration of
    hazardous waste entering
    the process
    during run "j", as determined in
    accordance with the requirements of
    Section 725.984 subsection 725.984
    (a)(53)(D)(i) through (a)(5)(D)(iv)
    above, in ppmw.
    E)
    The organic reduction efficiency of the process must
    be calculated by using the results determined in
    accordance with subsection (b)(
    65)(D) above and the
    following equation:
    R =
    E
    - E
    E
    x100%
    b
    a
    b
    300
    Where:
    R =
    Organic reduction efficiency,
    in percent.
    E
    b
    =
    Waste volatile organic mass flow entering
    the process as determined in accordance
    with the requirements of subsection
    (b)(65)(D) above, in kg/hr.
    E
    a
    =
    Waste volatile organic ma
    ss flow exiting
    the process as determined in accordance
    with the requirements of subsection
    (b)(65)(D) above, in kg/hr.
    76)
    Procedure to determine the organic
    biodegradation efficiency
    (R
    bio
    ) for a treated hazardous waste.
    A)
    The fraction of organics biodegraded (
    F
    bio
    ) must be
    determined using the procedure specified in 40 CFR 63,
    Appendix C, incorporated by reference in 35 Ill. Adm.
    Code 7 20.111.
    B)
    The organic biodegradation efficiency
    (R
    bio
    ) must be
    calculated by using the following equation:
    bio
    bio
    R
    = F
    x100%
    Where
    R
    bio
    = Organic biodegradation efficiency, in
    percent.
    F
    bio
    = Fraction of organic biodegraded
    , as
    determined in accordance with the
    requirements of subsection (b)(
    76)(A)
    above.
    87)
    Procedure to determine the required organic mass removal
    rate (RMR) for a treated hazardous waste.
    A) The point of waste origination for
    eachAll of the
    hazardous waste treated bystreams entering the
    treatment process at the same time
    must be identified.
    B) For each hazardous waste stream identified in
    subsection (b)(8)(A) above,
    theThe average VO
    concentration of the hazardous waste stream at the
    point of waste origination must be determined in
    accordance with the requirements of subsection (a)
    above.
    C)
    For each individual hazardous waste stream that has a
    n
    average volatile organic concentration equal to or
    greater than 100500 ppmw at the point of waste
    origination as determined in accordance with the
    requirements of subsection (b)(8)(B) above
    , the
    average volumetric flow rate of hazardous waste
    and
    the density of the hazardous waste stream
    at the point
    of waste origination
    and the density of the hazardous
    waste stream must be determined.
    301
    D)
    The required organic mass removal rate
    (RMR) for the
    hazardous waste must be calculated by using the
    results determined for each individual hazardous waste
    stream in accordance with the requirements of
    subsections (b)(8)(B) and (b)(8)(C)
    aboveaverage VO
    concentration, average volumetric flow rate, and
    density determined for each individual hazardous waste
    stream, and the following equation:
    RMR =
    n
    y = 1
    V
    x k
    x
    ( C
    -100ppmw)
    10
    y
    y
    y
    6
    โˆ‘
    ๏ฃฎ
    ๏ฃฐ
    ๏ฃฏ
    ๏ฃบ
    ๏ฃผ
    ๏ฃป
    RMR =
    n
    y = 1
    V
    x k
    x
    ( C
    - 500ppmw)
    10
    y
    y
    y
    6
    โˆ‘
    ๏ฃฎ
    ๏ฃฐ
    ๏ฃฏ
    ๏ฃบ
    ๏ฃผ
    ๏ฃป
    Where:
    RMR =
    Required organic mass removal rate, in kg/hr.
    y =
    Individual hazardous waste stream "y" that has
    an average volatile organic
    (VO) concentration
    equal to or greater than
    100500 ppmw at the
    point of waste origination, as determined in
    accordance with the requirements of
    Section
    725.984 subsection (a) above .
    n =
    Total number of "y" hazardous waste streams
    treated by process.
    V
    y
    =
    Average volumetric flow rate of hazardous waste
    stream "y" at the point of waste origination,
    in m
    3
    /hr.
    k
    y
    =
    Density of hazardous waste stream "y", in kg/m
    3
    C
    y
    =
    Average VO concentration of hazardous waste
    stream "y" at the point of waste origination
    , as
    determined in accordance with the requirements
    of Section 725.984 subsection (a) above , in ppmw.
    98)
    Procedure to determine the actual or
    ganic mass removal rate
    (MR) for a treated hazardous waste.
    A)
    The actual organic mass removal rate
    (MR) must be
    determined based on results for a minimum of three
    consecutive runs. The sampling time for each run must
    be one hour.
    B)
    The waste volatile organic mass flow entering the
    process ( E
    b
    ) and the waste volatile organic mass flow
    exiting the process (
    E
    a
    ) must be determined in
    accordance with the requirements of subsection
    (b)(65)(D) above.
    C)
    The actual organic mass removal rate
    (MR) must be
    302
    calculated by using the
    results mass flow rate
    determined in accordance with the requirements of
    subsection (b)( 98)(B) above and the following
    equation:
    MR = E
    - E
    b
    a
    Where:
    MR =
    Actual organic mass removal rate, in
    kg/hr.
    E
    b
    =
    Waste volatile organic mass flow entering
    process, as determined in accordance with
    the requirements of subsection (b)(
    65)(D)
    above, in kg/hr.
    E
    a
    =
    Waste volatile organic mass flow exiting
    process, as determined in accordance with
    the requirements of subsection (b)(
    65)(D)
    above, in kg/hr.
    109)
    Procedure to determine the actual organic mass
    biodegradation rate (
    MR
    bio
    ) for a treated hazardous waste.
    A)
    The actual organic mass
    biodegradation rate
    (MR
    bio
    )
    must be determined based on results for a minimum of
    three consecutive runs. The sampling time for each
    run must be one hour.
    B)
    The waste organic mass flow entering the process (
    E
    b
    )
    must be determined in accordance with the requirements
    of subsection (b)(
    65)(D) above.
    C)
    The fraction of organic biodegraded (
    F
    bio
    ) must be
    determined using the procedure specified in 40 CFR 63,
    Appendix C, incorporated by reference in 35 Ill. Adm.
    Code 720.111.
    D)
    The actual organic mass
    biodegradation rate
    (MR
    bio
    )
    must be calculated by using the mass flow rates and
    fraction of organic biodegraded determined in
    accordance with the requirements of subsections
    (b)(109)(B) and (b)( 109)(C) above and the following
    equation:
    bio
    b
    bio
    MR
    = E
    x F
    Where:
    MR
    bio
    =Actual organic mass
    biodegradation rate,
    in kg/hr.
    E
    b
    =
    Waste organic mass flow entering
    the
    process, as determined in accordance with
    the requirements of subsection (b)(
    65)(D)
    above, in kg/hr.
    F
    bio
    = Fraction of organic biodegraded, as
    determined in accordance with the
    303
    requirements of subsection (b)(
    109)(C)
    above.
    c)
    Procedure to determine the maximum organic vapor pressure of a
    hazardous waste in a tank.
    1)
    An owner or operator shall determine the maximum organic
    vapor pressure for each hazardous waste placed in a tank
    using air emission Tank Level 1 controls in accordance with
    standards specified in Section 725.985(c).
    2)
    An owner or operator shall use either direct measurement, as
    specified in subsection (c)(3) above, or knowledge of the
    waste, as specified by subsection (c)(4) above, to determine
    the maximum organic vapor pressure that is representative of
    the hazardous waste composition stored or treated in the
    tank.
    3) To determine the maximum organic vapor pressu
    re of the
    hazardous waste by direct measurement, the following
    procedure must be
    used:Direct measurement to determine the
    maximum organic vapor pressure of a hazardous waste.
    A) Representative Sampling. A sufficient number of
    samples of the waste contained in the tank
    must be
    collected to be representative of the waste contained
    in the tank . Sampling All samples must be conducted
    and handled in accordance with
    written procedures
    prepared by the owner or operator and documented in a
    site sampling plan. This plan must describe the
    procedure by which representative samples of the
    hazardous waste are collected such that a minimum loss
    of organics occurs throughout the sample collection
    and handling process and by which sample integrity is
    maintained. A copy of the written sampling plan must
    be maintained on -site in the facility operating
    records. An example of an acceptable sampling plan
    includes a plan incorporating sample collection and
    handling procedures in accordance with
    the
    requirements specified in "Test Methods for Evaluating
    Solid Waste, Physical/Chemical Methods",
    USEPA
    Publication No. SW
    -846, incorporated by reference in
    35 Ill. Adm. Code 720.111
    , or in Method 25D in 40 CFR
    60, appendix A, incorporated by reference in 35 Ill.
    Adm. Code 720.111
    .
    B)
    Analysis. Any appropriate one of the following
    methods may be used to analyze the samples and compute
    the maximum organic vapor pressure
    of the hazardous
    waste, as appropriate :
    i)
    Method 25E in 40 CFR 60, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111;
    ii)
    Methods described in American Petroleum
    Institute Publication 2517, incorporated by
    reference in 35 Ill. Adm. Code 720.111;
    iii)
    Methods obtained from standard reference texts;
    304
    iv)
    ASTM Method D 2879-92, incorporated by reference
    in 35 Ill. Adm. Code 720.111
    ); or
    v)
    Any other method approved by the Agency
    for this
    use by the owner or operator
    .
    4) To determine the maximum organic vapor pressure of the
    hazardous waste by knowledge, sufficient information must be
    prepared and recorded that documents the maximum organic
    vapor pressure of the hazardous waste in the tank. Examples
    of information that may be used include: documentation that
    the waste is generated by a process for which no
    organics-
    containing materials are used or that the waste is generated
    by a process for which at other locations it previously has
    been determined by direct measurement that the waste maximum
    organic vapor pressure is less than the maximum vapor
    pressure limit for the appropriate design capacity category
    specified for the tank.
    4)
    Use of knowledge to determine the maximum organic vapor
    pressure of the hazardous waste. Documentation must be
    prepared and recorded that presents the information used as
    the basis for the owner's or operator's knowledge that the
    maximum organic vapor pressure of the hazardous waste is
    less than the maximum vapor pressure limit listed in Section
    725.985(b)(1)(A) for the applicable tank design capacity
    category. An example of information that may be used is
    documentation that the hazardous waste is generated by a
    process for which at other locations it previously has been
    determined by direct measurement that the waste maximum
    organic vapor pressure is less than the maximum vapor
    pressure limit for the appropriate tank design capacity
    category.
    d)
    Procedure for determining no detectable organic emissions for the
    purpose of complying with this Subpart:
    1)
    The test must be conducted in accordance with the procedures
    specified in Method 21 of 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    Each potential leak interface (i.e., a location where
    organic vapor leakage could occur) on the cover and
    associated closure devices must be checked. Potential leak
    interfaces that are associated with covers and closure
    devices include, but are not limited to any of the
    following: the interface of the cover and its foundation
    mounting, the periphery of any opening on the cover and its
    associated closure device, and the sealing seat interface on
    a spring -loaded pressure relief valve.
    2)
    The test must be performed when the unit contains a
    hazardous waste having an organic concentration
    representative of the range of concentrations for the
    hazardous waste expected to be managed in the unit. During
    the test, the cover and closure devices must be secured in
    the closed position.
    3)
    The detection instrument must meet the performance criteria
    of Method 21 of 40 CFR 60, appendix A, incorporated by
    reference in 35 Ill. Adm. Code 720.111, except the
    instrument response factor criteria in Section 3.1.2(a) of
    305
    Method 21 must be for the average composition of the organic
    constituents in the hazardous waste placed in the waste
    management unit, not for each individual organic
    constituent.
    4)
    The detection instrument must be calibrated before use on
    each day of its use by the procedures specified in Method 21
    of 40 CFR 60, appendix A, incorporated by reference in 35
    Ill. Adm. Code 720.111.
    5)
    Calibration gases must be as follows:
    A)
    Zero air (less than 10
    ppmv hydrocarbon in air), and
    B)
    A mixture of methane in air at a concentration of
    approximately, but less than, 10,000
    ppmv.
    6)
    The background level must be determined according to the
    procedures in Method 21 of 40 CFR 60, appendix A,
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    7)
    Each potential leak interface must be checked by traversing
    the instrument probe around the potential leak interface as
    close to the interface as possible, as described in Method
    21 of 40 CFR 60, appendix A, incorporated by reference in 35
    Ill. Adm. Code 720.111. In the case when the configuration
    of the cover or closure device prevents a complete traverse
    of the interface, all accessible portions of the interface
    must be sampled. In the case when the configuration of the
    closure device prevents any sampling at the interface and
    the device is equipped with an enclosed extension or horn
    (e.g., some pressure relief devices), the instrument probe
    inlet must be placed at approximately the center of the
    exhaust area to the atmosphere.
    8)
    The arithmetic difference between the maximum organic
    concentration indicated by the instrument and the background
    level must be compared with the value of 500
    ppmv except
    when monitoring a seal around a rotating shaft that passes
    through a cover opening, in which case the comparison must
    be as specified in subsection (d)(9) below. If the
    difference is less than 500
    ppmv, then the potential leak
    interface is determined to operate with no detectable
    organic emissions.
    9)
    For the seals around a rotating shaft that passes through a
    cover opening, the arithmetic difference between the maximum
    organic concentration indicated by the instrument and the
    background level must be compared with the value of 10,000
    ppmw. If the difference is less than 10,000
    ppmw, then the
    potential leak interface is determined to operate with no
    detectable organic emissions.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.985
    Standards: T anks
    a) This Section applies to owners and operators of tanks subject to
    this Subpart into which any hazardous waste is placed except for
    the following tanks:
    306
    1) A tank in which all hazardous waste entering the tank meets
    the conditions specified in Section 725.983(c); or
    2) A tank used for biological treatment of hazardous waste in
    accordance with the requirements of Section
    725.983(c)(2)(D).
    a)
    The provisions of this Section apply to the control of air
    pollutant emissions from tanks for which Section 725.983(b)
    references the use of this Section for such air emission control.
    b)
    The owner or operator shall
    place the hazardous waste into one of
    the following tankscontrol air pollutant emissions from each tank
    subject to this Section in accordance with the following
    requirements, as applicable
    :
    1) A tank equipped with a cover (e.g., a fixed roof) that is
    vented through a closed-vent system to a control device in
    accordance with the requirements specified in subsection (d)
    below;
    2) A tank eq uipped with a fixed roof and internal floating roof
    in accordance with the requirements of Section 725.991;
    3) A tank equipped with an external floating roof in accordance
    with the requirements of Section 725.991; or
    4) A pressure tank that is designed to operate as a closed
    system such that the tank operates with no detectable
    organic emissions at all times that hazardous waste is in
    the tank except as provided for in subsection (g) below.
    c) As an alternative to complying with subsection (b) above
    , an owner
    or operator may place hazardous waste in a tank equipped with a
    cover (e.g., a fixed roof) meeting the requirements specified in
    subsection (d)(1) below when the hazardous waste is determined to
    meet all of the following conditions:
    1) The hazardous waste is neither mixed, stirred, agitated, nor
    circulated within the tank by the owner or operator using a
    process that results in splashing, frothing, or visible
    turbulent flow on the waste surface during normal process
    operations;
    2) The hazar dous waste in the tank is not heated by the owner
    or operator except during conditions requiring that the
    waste be heated to prevent the waste from freezing or to
    maintain adequate waste flow conditions for continuing
    normal process operations;
    3) The hazardous waste in the tank is not treated by the owner
    or operator using a waste stabilization process or a process
    that produces an exothermic reaction; and
    4) The maximum organic vapor pressure of the hazardous waste in
    the tank as determined using the procedure specified in
    Section 725.984(c) is less than the following applicable
    value:
    1)
    For a tank that manages hazardous waste which meets all of
    the conditions specified in subsections (b)(1)(A) through
    307
    (b)(1)(C) below, the owner or operator shall control air
    pollutant emissions from the tank in accordance with the
    Tank Level 1 controls specified in subsection (c) below or
    the Tank Level 2 controls specified in subsection (d) below.
    A)
    The hazardous waste in the tank has a maximum organic
    vapor pressure that is less than the maximum organic
    vapor pressure limit for the tank's design capacity
    category, as follows:
    Ai) If theFor a tank design capacity
    is equal to or
    greater than 151 m
    3
    (5333 ft
    3
    or 39,887 gal),
    then the maximum organic vapor pressure
    must be
    less thanlimit for the tank is
    5.2 kPa (0.75
    psia or 39 mm Hg);
    Bii) If theFor a tank design capacity
    is equal to or
    greater than 75 m
    3
    (2649 ft
    3
    or 19,810 gal) but
    less than 151 m
    3
    (5333 ft
    3
    or 39,887 gal),
    then
    the maximum organic vapor pressure
    must be less
    thanlimit for the tank is
    27.6 kPa (4.0 psia or
    207 mm Hg); or
    Ciii) If theFor a tank design capacity is less than 75
    m
    3
    (2649 ft
    3
    or 19,810 gal),
    then the maximum
    organic vapor pressure then the maximum organic
    vapor pressure must be less thanlimit for the
    tank is 76.6 kPa (11.1 psia or 574 mm Hg).
    d) To comply with subsection (b)(1) above, the owner or operator
    shall design, install, operate, and maintain a cover that vents
    the organic vapors emitted from hazardous waste in the tank
    through a closed-vent system connected to a control device.
    1) The cover must be designed and operated to meet the
    following requirements:
    A) The cover and all cover openings (e.g., access
    hatches, sampling ports, and gauge wells) must be
    designed to operate with no detectable organic
    emissions when all cover openings are secured in a
    closed, sealed position.
    B) Each cover opening must be secured in a closed, sealed
    position (e.g., covered by a
    gasketed lid or cap) at
    all times that hazardous waste is in the tank except
    as provided for in subsection (f) below.
    2) The closed-vent system and control device must be designed
    and operated in accordance with the requirements of Section
    725.988.
    e) The owner and operator shall install, operate, and maintain
    enclosed pipes or other closed systems for the transfer of
    hazardous waste as described in subsection (e)(1) or (e)(2) below.
    BOARD NOTE: U.S. EPA considers a drain system that meets the
    requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
    a "closed-system". The Board intends that this meaning be
    included in the use of that term for the purposes of this Subpart.
    308
    1) Transfer all hazardous waste to the tank from another tank,
    surface impoundment, or container subject to this Subpart,
    except for those hazardous wastes that meet the conditions
    specified in Section 725.983(c); and
    2) Transfer all hazardous waste from the tank to another tank,
    surface impoundment, or container subject to this Subpart,
    except for those hazardous wastes that meet the conditions
    specified in Section 725.983(c).
    f) Each cover opening must be secured in a closed, sealed position
    (e.g., covered by a
    gasketed lid) at all times that hazardous
    waste is in the tank except when it is necessary to use the cover
    opening to:
    1) Add, remove, inspect, or sample the material in the tank;
    2) Inspect, maintain, repair, or replace equipment located
    inside the tank; or
    3) Vent gases or vapors from the tank to a closed-vent system
    connected to a control device that is designed and operated
    in accordance with the requirements of Section 725.988.
    g) One or more safety devices that vent directly to the atmosphere
    may be used on the tank, cover, closed-vent system, or control
    device provided each safety device meets all of the following
    conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the tank or the closed-vent system
    connected to a control device; and
    2) The safety device remains in a closed, se
    aled position at
    all times except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the tank, cover, closed-vent
    system, or control device in accordance with good
    engineering and safety practices for handling flammable,
    combustible, explosive, or other hazardous materials. An
    example of an unplanned event is a sudden power outage.
    B)
    The hazardous waste in the tank is not heated by the
    owner or operator to a temperature that is greater
    than the temperature at which the maximum organic
    vapor pressure of the hazardous waste is determined
    for the purpose of complying with subsection (b)(1)(A)
    above.
    C)
    The hazardous waste in the tank is not treated by the
    owner or operator using a waste stabilization process,
    as defined in Section 725.981.
    2)
    For a tank that manages hazardous waste that does not meet
    all of the conditions specified in subsections (b)(1)(A)
    through (b)(1)(C) above, the owner or operator shall control
    air pollutant emissions from the tank by using Tank Level 2
    controls in accordance with the requirements of subsection
    (d) below. Examples of tanks required to use Tank Level 2
    controls include the following: a tank used for a waste
    stabilization process and a tank for which the hazardous
    309
    waste in the tank has a maximum organic vapor pressure that
    is equal to or greater than the maximum organic vapor
    pressure limit for the tank's design capacity category, as
    specified in subsection (b)(1)(A) above.
    c)
    Owners and operators controlling air pollutant emissions from a
    tank using Tank Level 1 controls shall meet the requirements
    specified in subsections (c)(1) through (c)(4) below:
    1)
    The owner or operator shall determine the maximum organic
    vapor pressure for a hazardous waste to be managed in the
    tank using Tank Level 1 controls before the first time the
    hazardous waste is placed in the tank. The maximum organic
    vapor pressure must be determined using the procedures
    specified in Section 725.984(c). Thereafter, the owner or
    operator shall perform a new determination whenever changes
    to the hazardous waste managed in the tank could potentially
    cause the maximum organic vapor pressure to increase to a
    level that is equal to or greater than the maximum organic
    vapor pressure limit for the tank design capacity category
    specified in subsection (b)(1)(A) above, as applicable to
    the tank.
    2)
    The tank must be equipped with a fixed roof designed to meet
    the following specifications:
    A)
    The fixed roof and its closure devices must be
    designed to form a continuous barrier over the entire
    surface area of the hazardous waste in the tank. The
    fixed roof may be a separate cover installed on the
    tank (e.g., a removable cover mounted on an open
    -top
    tank) or may be an integral part of the tank
    structural design (e.g., a horizontal cylindrical tank
    equipped with a hatch).
    B)
    The fixed roof must be installed in a manner such that
    there are no visible cracks, holes, gaps, or other
    open spaces between roof Section joints or between the
    interface of the roof edge and the tank wall.
    C)
    Each opening in the fixed roof must be either:
    i)
    Equipped with a closure device designed to
    operate such that when the closure device is
    secured in the closed position there are no
    visible cracks, holes, gaps, or other open
    spaces in the closure device or between the
    perimeter of the opening and the closure device;
    or
    ii)
    Connected by a closed
    -vent system that is vented
    to a control device. The control device must
    remove or destroy
    organics in the vent stream,
    and it must be operating whenever hazardous
    waste is managed in the tank.
    D)
    The fixed roof and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and which will maintain the integrity of
    the fixed roof and closure devices throughout their
    310
    intended service life. Factors to be considered when
    selecting the materials for and designing the fixed
    roof and closure devices must include the following:
    organic vapor permeability; the effects of any contact
    with the hazardous waste or its vapors managed in the
    tank; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    used for the tank on which the fixed roof is
    installed.
    3)
    Whenever a hazardous waste is in the tank, the fixed roof
    must be installed with each closure device secured in the
    closed position, except as follows:
    A)
    Opening of closure devices or removal of the fixed
    roof is allowed at the following times:
    i)
    To provide access to the tank for performing
    routine inspection, maintenance, or other
    activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample the
    liquid in the tank, or when a worker needs to
    open a hatch to maintain or repair equipment.
    Following completion of the activity, the owner
    or operator shall promptly secure the closure
    device in the closed position or reinstall the
    cover, as applicable, to the tank.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of tank.
    B)
    Opening of a spring
    -loaded pressure -vacuum relief
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the tank internal pressure in accordance
    with the tank design specifications. The device must
    be designed to operate with no detectable organic
    emissions when the device is secured in the closed
    position. The settings at which the device opens must
    be established such that the device remains in the
    closed position whenever the tank internal pressure is
    within the internal pressure operating range
    determined by the owner or operator based on the tank
    manufacturer recommendations; applicable regulations;
    fire protection and prevention codes; standard
    engineering codes and practices; or other requirements
    for the safe handling of flammable, ignitable,
    explosive, reactive, or hazardous materials. Examples
    of normal operating conditions that may require these
    devices to open are during those times when the tank
    internal pressure exceeds the internal pressure
    operating range for the tank as a result of loading
    operations or diurnal ambient temperature
    fluctuations.
    C)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    311
    4)
    The owner or operator shall inspect the air emission control
    equipment in accordance with the following requirements.
    A)
    The fixed roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to,
    visible cracks, holes, or gaps in the roof Sections or
    between the roof and the tank wall; broken, cracked,
    or otherwise damaged seals or gaskets on closure
    devices; and broken or missing hatches, access covers,
    caps, or other closure devices.
    B)
    The owner or operator shall perform an initial
    inspection of the fixed roof and its closure devices
    on or before the date that the tank becomes subject to
    this Section. Thereafter, the owner or operator shall
    perform the inspections at least once every year,
    except under the special conditions provided for in
    subsection (l) below.
    C)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    D)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 725.990(b).
    d)
    Owners and operators controlling air pollutant emissions from a
    tank using Tank Level 2 controls shall use one of the following
    tanks:
    1)
    A fixed -roof tank equipped with an internal floating roof in
    accordance with the requirements specified in subsection (e)
    below;
    2)
    A tank equipped with an external floating roof in accordance
    with the requirements specified in subsection (f) below;
    3)
    A tank vented through a closed
    -vent system to a control
    device in accordance with the requirements specified in
    subsection (g) below;
    4)
    A pressure tank designed and operated in accordance with the
    requirements specified in subsection (h) below; or
    5)
    A tank located inside an enclosure that is vented through a
    closed -vent system to an enclosed combustion control device
    in accordance with the requirements specified in subsection
    (i) below.
    e)
    The owner or operator that controls air pollutant emissions from a
    tank using a fixed
    -roof with an internal floating roof shall meet
    the requirements specified in subsections (e)(1) through (e)(3)
    below.
    1)
    The tank must be equipped with a fixed roof and an internal
    floating roof in accordance with the following requirements:
    A)
    The internal floating roof must be designed to float
    312
    on the liquid surface except when the floating roof
    must be supported by the leg supports.
    B)
    The internal floating roof must be equipped with a
    continuous seal between the wall of the tank and the
    floating roof edge that meets either of the following
    requirements:
    i)
    A single continuous seal that is either a
    liquid -mounted seal or a metallic shoe seal, as
    defined in Section 725.981; or
    ii)
    Two continuous seals mounted one above the
    other. The lower seal may be a vapor
    -mounted
    seal.
    C)
    The internal floating roof must meet the following
    specifications:
    i)
    Each opening in a
    noncontact internal floating
    roof except for automatic bleeder vents (vacuum
    breaker vents) and the rim space vents is to
    provide a projection below the liquid surface.
    ii)
    Each opening in the internal floating roof must
    be equipped with a
    gasketed cover or a
    gasketed
    lid except for leg sleeves, automatic bleeder
    vents, rim space vents, column wells, ladder
    wells, sample wells, and stub drains.
    iii)
    Each penetration of the internal floating roof
    for the purpose of sampling must have a slit
    fabric cover that covers at least 90 percent of
    the opening.
    iv)
    Each automatic bleeder vent and rim space vent
    must be gasketed.
    v)
    Each penetration of the internal floating roof
    that allows for passage of a ladder must have a
    gasketed sliding cover.
    vi)
    Each penetration of the internal floating roof
    that allows for passage of a column supporting
    the fixed roof must have a flexible fabric
    sleeve seal or a
    gasketed sliding cover.
    2)
    The owner or operator shall operate the tank in accordance
    with the following requirements:
    A)
    When the floating roof is resting on the leg supports,
    the process of filling, emptying, or refilling must be
    continuous and must be completed as soon as practical.
    B)
    Automatic bleeder vents are to be set closed at all
    times when the roof is floating, except when the roof
    is being floated off or is being landed on the leg
    supports.
    C)
    Prior to filling the tank, each cover, access hatch,
    gauge float well or lid on any opening in the internal
    313
    floating roof must be bolted or fastened closed (i.e.,
    no visible gaps). Rim space vents are to be set to
    open only when the internal floating roof is not
    floating or when the pressure beneath the rim exceeds
    the manufacturer's recommended setting.
    3)
    The owner or operator shall inspect the internal floating
    roof in accordance with the procedures specified as follows:
    A)
    The floating roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to
    the following: when the internal floating roof is not
    floating on the surface of the liquid inside the tank;
    when liquid has accumulated on top of the internal
    floating roof; when any portion of the roof seals have
    detached from the roof rim; when holes, tears, or
    other openings are visible in the seal fabric; when
    the gaskets no longer close off the hazardous waste
    surface from the atmosphere; or when the slotted
    membrane has more than 10 percent open area.
    B)
    The owner or operator shall inspect the internal
    floating roof components as follows, except as
    provided in subsection (e)(3)(C) below:
    i)
    Visually inspect the internal floating roof
    components through openings on the fixed
    -roof
    (e.g., manholes and roof hatches) at least once
    every 12 months after initial fill, and
    ii)
    Visually inspect the internal floating roof,
    primary seal, secondary seal (if one is in
    service), gaskets, slotted membranes, and sleeve
    seals (if any) each time the tank is emptied and
    degassed and at least once every 10 years.
    C)
    As an alternative to performing the inspections
    specified in subsection (e)(3)(B) above for an
    internal floating roof equipped with two continuous
    seals mounted one above the other, the owner or
    operator may visually inspect the internal floating
    roof, primary and secondary seals, gaskets, slotted
    membranes, and sleeve seals (if any) each time the
    tank is emptied and degassed and at least every five
    years.
    D)
    Prior to each inspection required by subsection
    (e)(3)(B) or (e)(3)(C) above, the owner or operator
    shall notify the Agency in advance of each inspection
    to provide the Agency with the opportunity to have an
    observer present during the inspection. The owner or
    operator shall notify the Agency of the date and
    location of the inspection as follows:
    i)
    Prior to each visual inspection of an internal
    floating roof in a tank that has been emptied
    and degassed, written notification must be
    prepared and sent by the owner or operator so
    that it is received by the Agency at least 30
    314
    calendar days before refilling the tank, except
    when an inspection is not planned, as provided
    for in subsection (e)(3)(D)(ii) below.
    ii)
    When a visual inspection is not planned and the
    owner or operator could not have known about the
    inspection 30 calendar days before refilling the
    tank, the owner or operator shall notify the
    Agency as soon as possible, but no later than
    seven calendar days before refilling of the
    tank. This notification may be made by
    telephone and immediately followed by a written
    explanation for why the inspection is unplanned.
    Alternatively, written notification, including
    the explanation for the unplanned inspection,
    may be sent so that it is received by the
    Regional Administrator at least seven calendar
    days before refilling the tank.
    E)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    F)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 725.990(b).
    f)
    The owner or operator that controls air pollutant emissions from a
    tank using an external floating roof shall meet the requirements
    specified in subsections (f)(1) through (f)(3) below.
    1)
    The owner or operator shall design the external floating
    roof in accordance with the following requirements:
    A)
    The external floating roof must be designed to float
    on the liquid surface except when the floating roof
    must be supported by the leg supports.
    B)
    The floating roof must be equipped with two continuous
    seals, one above the other, between the wall of the
    tank and the roof edge. The lower seal is referred to
    as the primary seal, and the upper seal is referred to
    as the secondary seal.
    i)
    The primary seal must be a liquid
    -mounted seal
    or a metallic shoe seal, as defined in Section
    725.981. The total area of the gaps between the
    tank wall and the primary seal must not exceed
    212 square centimeters (cm
    2
    ) per meter (10.0 in
    2
    per foot) of tank diameter, and the width of any
    portion of these gaps must not exceed 3.8
    centimeters (cm) (1.5 inches). If a metallic
    shoe seal is used for the primary seal, the
    metallic shoe seal must be designed so that one
    end extends into the liquid in the tank and the
    other end extends a vertical distance of at
    least 61 centimeters above the liquid surface.
    ii)
    The secondary seal must be mounted above the
    primary seal and cover the annular space between
    the floating roof and the wall of the tank. The
    315
    total area of the gaps between the tank wall and
    the secondary seal must not exceed 21.2 cm
    2
    per
    meter (1.0 in
    2
    per foot) of tank diameter, and
    the width of any portion of these gaps must not
    exceed 1.3 cm (0.5 inch).
    C)
    The external floating roof must meet the following
    specifications:
    i)
    Except for automatic bleeder vents (vacuum
    breaker vents) and rim space vents, each opening
    in a noncontact external floating roof must
    provide a projection below the liquid surface.
    ii)
    Except for automatic bleeder vents, rim space
    vents, roof drains, and leg sleeves, each
    opening in the roof must be equipped with a
    gasketed cover, seal, or lid.
    iii)
    Each access hatch and each gauge float well must
    be equipped with a cover designed to be bolted
    or fastened when the cover is secured in the
    closed position.
    iv)
    Each automatic bleeder vent and each rim space
    vent must be equipped with a gasket.
    v)
    Each roof drain that empties into the liquid
    managed in the tank must be equipped with a
    slotted membrane fabric cover that covers at
    least 90 percent of the area of the opening.
    vi)
    Each unslotted and slotted guide pole well must
    be equipped with a
    gasketed sliding cover or a
    flexible fabric sleeve seal.
    vii)
    Each unslotted guide pole must be equipped with
    a gasketed cap on the end of the pole.
    viii)
    Each slotted guide pole must be equipped with a
    gasketed float or other device which closes off
    the liquid surface from the atmosphere.
    ix)
    Each gauge hatch and each sample well must be
    equipped with a gasketed cover.
    2)
    The owner or operator shall operate the tank in accordance
    with the following requirements:
    A)
    When the floating roof is resting on the leg supports,
    the process of filling, emptying, or refilling must be
    continuous and must be completed as soon as practical.
    B)
    Except for automatic bleeder vents, rim space vents,
    roof drains, and leg sleeves, each opening in the roof
    must be secured and maintained in a closed position at
    all times except when the closure device must be open
    for access.
    C)
    Covers on each access hatch and each gauge float well
    must be bolted or fastened when secured in the closed
    316
    position.
    D)
    Automatic bleeder vents must be set closed at all
    times when the roof is floating, except when the roof
    is being floated off or is being landed on the leg
    supports.
    E)
    Rim space vents must be set to open only at those
    times that the roof is being floated off the roof leg
    supports or when the pressure beneath the rim seal
    exceeds the manufacturer's recommended setting.
    F)
    The cap on the end of each
    unslotted guide pole must
    be secured in the closed position at all times except
    when measuring the level or collecting samples of the
    liquid in the tank.
    G)
    The cover on each gauge hatch or sample well must be
    secured in the closed position at all times except
    when the hatch or well must be opened for access.
    H)
    Both the primary seal and the secondary seal must
    completely cover the annular space between the
    external floating roof and the wall of the tank in a
    continuous fashion except during inspections.
    3)
    The owner or operator shall inspect the external floating
    roof in accordance with the procedures specified as follows:
    A)
    The owner or operator shall measure the external
    floating roof seal gaps in accordance with the
    following requirements:
    i)
    The owner or operator shall perform measurements
    of gaps between the tank wall and the primary
    seal within 60 calendar days after initial
    operation of the tank following installation of
    the floating roof and, thereafter, at least once
    every five years.
    ii)
    The owner or operator shall perform measurements
    of gaps between the tank wall and the secondary
    seal within 60 calendar days after initial
    operation of the tank following installation of
    the floating roof and, thereafter, at least once
    every year.
    iii)
    If a tank ceases to hold hazardous waste for a
    period of one year or more, subsequent
    introduction of hazardous waste into the tank
    must be considered an initial operation for the
    purposes of subsections (f)(3)(A)(i) and
    (f)(3)(A)(ii) above.
    iv)
    The owner or operator shall determine the total
    surface area of gaps in the primary seal and in
    the secondary seal individually using the
    procedure set forth in subsection (f)(4)(D)
    below.
    v)
    In the event that the seal gap measurements do
    317
    not conform to the specifications in subsection
    (f)(1)(B) below, the owner or operator must
    repair the defect in accordance with the
    requirements of subsection (k) below.
    vi)
    The owner or operator shall maintain a record of
    the inspection in accordance with the
    requirements specified in Section 725.990(b).
    B)
    The owner or operator shall visually inspect the
    external floating roof in accordance with the
    following requirements:
    i)
    The floating roof and its closure devices must
    be visually inspected by the owner or operator
    to check for defects that could result in air
    pollutant emissions. Defects include, but are
    not limited to any of the following: holes,
    tears, or other openings in the rim seal or seal
    fabric of the floating roof; a rim seal detached
    from the floating roof; all or a portion of the
    floating roof deck being submerged below the
    surface of the liquid in the tank; broken,
    cracked, or otherwise damaged seals or gaskets
    on closure devices; and broken or missing
    hatches, access covers, caps, or other closure
    devices.
    ii)
    The owner or operator shall perform an initial
    inspection of the external floating roof and its
    closure devices on or before the date that the
    tank becomes subject to this Section.
    Thereafter, the owner or operator shall perform
    the inspections at least once every year except
    for the special conditions provided for in
    subsection (l) below.
    iii)
    In the event that a defect is detected, the
    owner or operator shall repair the defect in
    accordance with the requirements of subsection
    (k) below.
    iv)
    The owner or operator shall maintain a record of
    the inspection in accordance with the
    requirements specified in Section 725.990(b).
    C)
    Prior to each inspection required by subsection
    (f)(3)(A) or (f)(3)(B) above, the owner or operator
    shall notify the Agency in advance of each inspection
    to provide the Agency with the opportunity to have an
    observer present during the inspection. The owner or
    operator shall notify the Agency of the date and
    location of the inspection as follows:
    i)
    Prior to each inspection to measure external
    floating roof seal gaps as required under
    subsection (f)(3)(A) above, written notification
    must be prepared and sent by the owner or
    operator so that it is received by the Agency at
    least 30 calendar days before the date the
    measurements are scheduled to be performed.
    318
    ii)
    Prior to each visual inspection of an external
    floating roof in a tank that has been emptied
    and degassed, written notification must be
    prepared and sent by the owner or operator so
    that it is received by the Agency at least 30
    calendar days before refilling the tank except
    when an inspection is not planned, as provided
    for in subsection (f)(3)(C)(iii) above.
    iii)
    When a visual inspection is not planned and the
    owner or operator could not have known about the
    inspection 30 calendar days before refilling the
    tank, the owner or operator shall notify the
    Agency as soon as possible, but no later than
    seven calendar days before refilling of the
    tank. This notification may be made by
    telephone and immediately followed by a written
    explanation for why the inspection is unplanned.
    Alternatively, written notification, including
    the explanation for the unplanned inspection,
    may be sent so that it is received by the
    Regional Administrator at least seven calendar
    days before refilling the tank.
    D)
    Procedure for determining gaps in the primary seal and
    in the secondary seal for the purposes of subsection
    (f)(3)(A)(iv) above:
    i)
    The seal gap measurements must be performed at
    one or more floating roof levels when the roof
    is floating off the roof supports.
    ii)
    Seal gaps, if any, must be measured around the
    entire perimeter of the floating roof in each
    place where a 0.32
    -cm (_-inch) diameter uniform
    probe passes freely (without forcing or binding
    against the seal) between the seal and the wall
    of the tank and measure the
    circumferential
    distance of each such location.
    iii)
    For a seal gap measured under subsection (f)(3)
    above, the gap surface area must be determined
    by using probes of various widths to measure
    accurately the actual distance from the tank
    wall to the seal and multiplying each such width
    by its respective
    circumferential distance.
    iv)
    The total gap area must be calculated by adding
    the gap surface areas determined for each
    identified gap location for the primary seal and
    the secondary seal individually, and then
    dividing the sum for each seal type by the
    nominal perimeter of the tank. These total gap
    areas for the primary seal and secondary seal
    are then are compared to the respective
    standards for the seal type, as specified in
    subsection (f)(1)(B) above.
    BOARD NOTE: Subsections (f)(3)(D)(i) through
    (f)(3)(D)(iv) correspond with 40 CFR
    319
    265.1085(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4),
    which the Board has codified here to comport
    with Illinois Administrative Code format
    requirements.
    g)
    The owner or operator that controls air pollutant emissions from a
    tank by venting the tank to a control device shall meet the
    requirements specified in subsections (g)(1) through (g)(3) below.
    1)
    The tank must be covered by a fixed roof and vented directly
    through a closed -vent system to a control device in
    accordance with the following requirements:
    A)
    The fixed roof and its closure devices must be
    designed to form a continuous barrier over the entire
    surface area of the liquid in the tank.
    B)
    Each opening in the fixed roof not vented to the
    control device must be equipped with a closure device.
    If the pressure in the vapor
    headspace underneath the
    fixed roof is less than atmospheric pressure when the
    control device is operating, the closure devices must
    be designed to operate such that when the closure
    device is secured in the closed position there are no
    visible cracks, holes, gaps, or other open spaces in
    the closure device or between the perimeter of the
    cover opening and the closure device. If the pressure
    in the vapor headspace underneath the fixed roof is
    equal to or greater than atmospheric pressure when the
    control device is operating, the closure device must
    be designed to operate with no detectable organic
    emissions.
    C)
    The fixed roof and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and will maintain the integrity of the
    fixed roof and closure devices throughout their
    intended service life. Factors to be considered when
    selecting the materials for and designing the fixed
    roof and closure devices must include the following:
    organic vapor permeability; the effects of any contact
    with the liquid and its vapor managed in the tank; the
    effects of outdoor exposure to wind, moisture, and
    sunlight; and the operating practices used for the
    tank on which the fixed roof is installed.
    D)
    The closed -vent sys tem and control device must be
    designed and operated in accordance with the
    requirements of Section 725.988.
    2)
    Whenever a hazardous waste is in the tank, the fixed roof
    must be installed with each closure device secured in the
    closed position and the vapor
    headspace underneath the fixed
    roof vented to the control device except as follows:
    A)
    Venting to the control device is not required, and
    opening of closure devices or removal of the fixed
    roof is allowed at the following times:
    i)
    To provide access to the tank for performing
    320
    routine inspection, maintenance, or other
    activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample
    liquid in the tank, or when a worker needs to
    open a hatch to maintain or repair equipment.
    Following completion of the activity, the owner
    or operator shall promptly secure the closure
    device in the closed position or reinstall the
    cover, as applicable, to the tank.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of a tank.
    B)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    3)
    The owner or operator shall inspect and monitor the air
    emission control equipment in accordance with the following
    procedures:
    A)
    The fixed roof and its closure devices must be
    visually inspected by the owner or operator to check
    for defects that could result in air pollutant
    emissions. Defects include, but are not limited to
    any of the following: visible cracks, holes, or gaps
    in the roof sections or between the roof and the tank
    wall; broken, cracked, or otherwise damaged seals or
    gaskets on closure devices; and broken or missing
    hatches, access covers, caps, or other closure
    devices.
    B)
    The closed -vent system and control device must be
    inspected and monitored by the owner or operator in
    accordance with the procedures specified in Section
    725.988.
    C)
    The owner or operator shall perform an initial
    inspection of the air emission control equipment on or
    before the date that the tank becomes subject to this
    Section. Thereafter, the owner or operator shall
    perform the inspections at least once every year
    except for the special conditions provided for in
    subsection (l) below.
    D)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (k) below.
    E)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 725.990(b).
    h)
    The owner or operator that controls air pollutant emissions by
    using a pressure tank must meet the following requirements.
    1)
    The tank shall be designed not to vent to the atmosphere as
    a result of compression of the vapor
    headspace in the tank
    during filling of the tank to its design capacity.
    321
    2)
    All tank openings must be equipped with closure devices
    designed to operate with no detectable organic emissions as
    determined using the procedure specified in Section
    725.984(d).
    3)
    Whenever a hazardous waste is in the tank, the tank must be
    operated as a closed system that does not vent to the
    atmosphere except in the event that a safety device, as
    defined in Section 725.981, is required to open to avoid an
    unsafe condition.
    i)
    The owner or operator that controls air pollutant emissions by
    using an enclosure vented through a closed
    -vent system to an
    enclosed combustion control device shall meet the requirements
    specified in subsections (i)(1) through (i)(4) below.
    1)
    The tank must be located inside an enclosure. The enclosure
    must be designed and operated in accordance with the
    criteria for a permanent total enclosure, as specified in
    "Procedure T --Criteria for and Verification of a Permanent
    or Temporary Total Enclosure" under 40 CFR 52.741, appendix
    B, incorporated by reference in 35 Ill. Adm. Code 720.111.
    The enclosure may have permanent or temporary openings to
    allow worker access; passage of material into or out of the
    enclosure by conveyor, vehicles, or other mechanical means;
    entry of permanent mechanical or electrical equipment; or
    direct airflow into the enclosure. The owner or operator
    shall perform the verification procedure for the enclosure
    as specified in Section 5.0 to "Procedure T
    --Criteria for
    and Verification of a Permanent or Temporary Total
    Enclosure" initially when the enclosure is first installed
    and, thereafter, annually.
    2)
    The enclosure must be vented through a closed
    -vent system to
    an enclosed combustion control device that is designed and
    operated in accordance with the standards for either a vapor
    incinerator, boiler, or process heater specified in Section
    725.988.
    3)
    Safety devices, as defined in Section 725.981, may be
    installed and operated as necessary on any enclosure,
    closed-vent system, or control device used to comply with
    the requirements of subsections (i)(1) and (i)(2) above.
    4)
    The owner or operator shall inspect and monitor the
    closed -vent system and control device, as specified in
    Section 725.988.
    j)
    The owner or operator shall transfer hazardous waste to a tank
    subject to this Section in accordance with the following
    requirements:
    1)
    Transfer of hazardous waste, except as provided in
    subsection (j)(2) below, to the tank from another tank
    subject to this Section or from a surface impoundment
    subject to Section 725.986 must be conducted using
    continuous hard -piping or another closed system that does
    not allow exposure of the hazardous waste to the atmosphere.
    For the purpose of complying with this provision, an
    individual drain system is considered to be a closed system
    when it meets the requirements of 40 CFR 63, subpart RR,
    322
    "National Emission Standards for Individual Drain Systems",
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The requirements of subsection (j)(1) above do not apply
    when transferring a hazardous waste to the tank under any of
    the following conditions:
    A)
    The hazardous waste meets the average VO concentration
    conditions specified in Section 725.983(c)(1) at the
    point of waste origination.
    B)
    The hazardous waste has been treated by an organic
    destruction or removal process to meet the
    requirements in Section 725.983(c)(2).
    k)
    The owner or operator shall repair each defect detected during an
    inspection performed in accordance with the requirements of
    subsections (c)(4), (e)(3), (f)(3), or (g)(3) above as follows:
    1)
    The owner or operator shall make first efforts at repair of
    the defect no later than five calendar days after detection,
    and repair shall be completed as soon as possible but no
    later than 45 calendar days after detection except as
    provided in subsection (k)(2) below.
    2)
    Repair of a defect may be delayed beyond 45 calendar days if
    the owner or operator determines that repair of the defect
    requires emptying or temporary removal from service of the
    tank and no alternative tank capacity is available at the
    site to accept the hazardous waste normally managed in the
    tank. In this case, the owner or operator shall repair the
    defect the next time the process or unit that is generating
    the hazardous waste managed in the tank stops operation.
    Repair of the defect must be completed before the process or
    unit resumes operation.
    l)
    Following the initial inspection and monitoring of the cover as
    required by the applicable provisions of this Subpart, subsequent
    inspection and monitoring may be performed at intervals longer
    than one year under the following special conditions:
    1)
    Where inspecting or monitoring the cover would expose a
    worker to dangerous, hazardous, or other unsafe conditions,
    then the owner or operator may designate a cover as an
    "unsafe to inspect and monitor cover" and comply with all of
    the following requirements:
    A)
    Prepare a written explanation for the cover stating
    the reasons why the cover is unsafe to visually
    inspect or to monitor, if required.
    B)
    Develop and implement a written plan and schedule to
    inspect and monitor the cover, using the procedures
    specified in the applicable Section of this Subpart,
    as frequently as practicable during those times when a
    worker can safely access the cover.
    2)
    In the case when a tank is buried partially or entirely
    underground, an owner or operator is required to inspect and
    monitor, as required by the applicable provisions of this
    Section, only those portions of the tank cover and those
    323
    connections to the tank (e.g., fill ports, access hatches,
    gauge wells, etc.) that are located on or above the ground
    surface.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.986
    Standards: Surface
    Impoundments
    a)
    The provisions of t
    his Section appliesy to owners and operators
    ofthe control of air pollutant emissions from
    surface impoundments
    subject to this Subpart into which any hazardous waste is placed
    except for the following surface
    impoundments: for which Section
    725.983(b) of this Subpart references the use of this Section for
    such air emission control.
    1) A surface impoundment in which all hazardous waste entering
    the surface impoundment meets the conditions specified in
    Section 725.983(c); or
    2) A surface impoundment used for biological treatment of
    hazardous waste in accordance with the requirements of
    Section 725.983(c)(2)(iv).
    b)
    The owner or operator shall
    place the hazardous waste into a
    surface impoundment equipped with a cover (e.g., an air-supported
    structure or a rigid cover) that is vented through a closed-vent
    system to a control device meeting the requirements specified in
    subsection (d) below. control air pollutant emissions from the
    surface impoundment by installing and operating either of the
    following:
    1)
    A floating membrane cover in accordance with the provisions
    specified in subsection (c) below; or
    2)
    A cover that is vented through a closed
    -vent system to a
    control device in accordance with the provisions specified
    in subsection (d) below.
    c) As an alternative to complying with subsection (b) above, an owner
    or operator may place hazardous waste in a surface impoundment
    equipped with a floating membrane cover meeting the requirements
    specified in subsection (e) below when the hazardous waste is
    determined to meet all of the following conditions:
    1) The hazardous waste is neither mixed, stirred, agitated, nor
    circulated within the surface impoundment by the owner or
    operator using a process that results in splashing,
    frothing, or visible turbulent flow on the waste surface
    during normal process operations;
    2) The hazardous waste in the surface impoundment is not heated
    by the owner or operator; and
    3) The hazardous waste in the surface impoundment is not
    treated by the owner or operator using a waste stabilization
    process or a process that produces an exothermic reaction.
    d) To comply with subsection (b)(1) above, the owner or operator
    shall design, install, operate, and maintain a cover that vents
    the organic vapors emitted from hazardous waste in the surface
    impoundment through a closed-vent system connected to a control
    324
    device.
    1) The cover must be designed, installed, operated, and
    maintained to meet the following requirements:
    A) The cover and all cover openings (e.g., access
    hatches, sampling ports, and gauge wells) must be
    designed to operate with no detectable organic
    emissions when all cover openings are secured in a
    closed, sealed position.
    B) Each cover opening must be secured in the closed,
    sealed position (e.g., covered by a
    gasketed lid or
    cap) at all times that hazardous waste is in the
    surface impoundment, except as provided for in
    subsection (g) below.
    C) The closed-v ent system and control device must be
    designed and operated in accordance with Section
    725.988.
    e) To comply with subsection (c) above, the owner or operator shall
    design, install, operate, and maintain a floating membrane cover
    that meets all of the following requirements:
    1) The floating membrane cover must be designed, installed, and
    operated such that at all times when hazardous waste is in
    the surface impoundment, the entire surface area of the
    hazardous waste is enclosed by the cover, and any air spaces
    underneath the cover are not vented to the atmosphere except
    during conditions specified in subsection (h) below.
    2) The floating membrane cover and all cover openings (e.g.,
    access hatches, sampling ports, and gauge wells) must be
    designed to operate with no detectable organic emissions
    when all cover openings are secured in a closed, sealed
    position.
    3) Each cover opening must be secured in a closed, sealed
    position (e.g., covered by a
    gasketed lid or cap) at all
    times that hazardous waste is in the surface impoundment
    except as provided for in subsections (g)(1) through (g)(3)
    below.
    4) The synthetic membrane material used for the floating
    membrane cover must be either:
    A) High density polyethylene with a thickness no less
    than 2.5 mm; or
    B) A material or a composite of different materials
    determined to have the following properties:
    i) Organic permeability properties that are
    equivalent to those of the material specified in
    subsection (e)(4)(A) above; and
    ii) Chemical an d physical properties that maintain
    the material integrity for as long as the cover
    is in use. Factors that must be considered in
    selecting the material include: the effects of
    325
    contact with the waste managed in the
    impoundment, weather exposure, and cover
    installation and operation practices.
    f) The owner or operator shall install, operate, and maintain
    enclosed pipes or other closed systems for the transfer of
    hazardous waste as described in subsection (f)(1) or (f)(2) below.
    BOARD NOTE: U.S. EPA c
    onsiders a drain system that meets the
    requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
    a "closed-system". The Board intends that this meaning be
    included in the use of that term for the purposes of this Subpart.
    1) Transfer all hazardous waste to the surface impoundment from
    another tank, surface impoundment, or container subject to
    this Subpart, except for those hazardous wastes that meet
    the conditions specified in Section 725.983(c); and
    2) Transfer all hazardous waste from the
    surface impoundment to
    another tank, surface impoundment, or container subject to
    this Subpart, except for those hazardous wastes that meet
    the conditions specified in Section 725.983(c).
    g) Each cover opening must be secured in the closed, sealed position
    (e.g., covered by a
    gasketed lid or cap) at all times that
    hazardous waste is in the surface impoundment except when it is
    necessary to use the cover opening to:
    1) Add, remove, inspect, or sample the material in the surface
    impoundment;
    2) Inspec t, maintain, repair, or replace equipment located
    underneath the cover;
    3) Remove treatment residues from the surface impoundment in
    accordance with the requirements of 35 Ill. Adm. Code
    728.104; or
    4) Vent gases or vapors from the surface impoundment to a
    closed-vent system connected to a control device that is
    designed and operated in accordance with the requirements of
    Section 725.988.
    h) One or more safety devices that vent directly to the atmosphere
    may be installed on the cover, closed-vent system, or control
    device provided each device meets all of the following conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the surface impoundment or the
    closed-vent system connected to a control device; and
    2) The safety device remains in a closed, sealed position at
    all times except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the cover, closed-vent system, or
    control device in accordance with good engineering and
    safety practices for handling flammable, combustible,
    explosive, or other hazardous materials. An example of an
    unplanned event is a sudden power outage.
    c)
    The owner or operator that controls air pollutant emissions from a
    326
    surface impoundment using a floating membrane cover must meet the
    requirements specified in subsections (c)(1) through (c)(3) below.
    1)
    The surface impoundment must be equipped with a floating
    membrane cover designed to meet the following
    specifications:
    A)
    The floating membrane cover must be designed to float
    on the liquid surface during normal operations and
    form a continuous barrier over the entire surface area
    of the liquid.
    B)
    The cover must be fabricated from a synthetic membrane
    material that is either:
    i)
    High density polyethylene (HDPE) with a
    thickness no less than 2.5 millimeters (mm)
    (0.10 inch); or
    ii)
    A material or a composite of different materials
    determined to have both organic permeability
    properties that are equivalent to those of the
    material listed in subsection (c)(1)(B)(i) above
    and chemical and physical properties that
    maintain the material integrity for the intended
    service life of the material.
    C)
    The cover must be installed in a manner such that
    there are no visible cracks, holes, gaps, or other
    open spaces between cover Section seams or between the
    interface of the cover edge and its foundation
    mountings.
    D)
    Except as provided for in subsection (c)(1)(E) below,
    each opening in the floating membrane cover must be
    equipped with a closure device so designed as to
    operate when that the closure device is secured in the
    closed position there are no visible cracks, holes,
    gaps, or other open spaces in the closure device or
    between the perimeter of the cover opening and the
    closure device.
    E)
    The floating membrane cover may be equipped with one
    or more emergency cover drains for removal of
    stormwater. Each emergency cover drain must be
    equipped with a slotted membrane fabric cover that
    covers at least 90 percent of the area of the opening
    or a flexible fabric sleeve seal.
    F)
    The closure devices must be made of suitable materials
    that will minimize exposure of the hazardous waste to
    the atmosphere, to the extent practical, and will
    maintain the integrity of the closure devices
    throughout their intended service life. Factors to be
    considered when selecting the materials of
    construction and designing the cover and closure
    devices must include the following: the organic vapor
    permeability; the effects of any contact with the
    liquid and its vapor managed in the surface
    impoundment; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    327
    used for the surface impoundment on which the floating
    membrane cover is installed.
    2)
    Whenever a hazardous waste is in the surface impoundment,
    the floating membrane cover must float on the liquid and
    each closure device must be secured in the closed position
    except as follows:
    A)
    Opening of closure devices or removal of the cover is
    allowed at the following times:
    i)
    To provide access to the surface impoundment for
    performing routine inspection, maintenance, or
    other activities needed for normal operations.
    Examples of such activities include those times
    when a worker needs to open a port to sample the
    liquid in the surface impoundment, or when a
    worker needs to open a hatch to maintain or
    repair equipment. Following completion of the
    activity, the owner or operator shall promptly
    replace the cover and secure the closure device
    in the closed position, as applicable.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of surface impoundment.
    B)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    3)
    The owner or operator shall inspect the floating membrane
    cover in accordance with the following procedures:
    A)
    The floating membrane cover and its closure devices
    must be visually inspected by the owner or operator to
    check for defects that could result in air pollutant
    emissions. Defects include, but are not limited to,
    visible cracks, holes, or gaps in the cover Section
    seams or between the interface of the cover edge and
    its foundation mountings; broken, cracked, or
    otherwise damaged seals or gaskets on closure devices;
    and broken or missing hatches, access covers, caps, or
    other closure devices.
    B)
    The owner or operator shall perform an initial
    inspection of the floating membrane cover and its
    closure devices on or before the date that the surface
    impoundment becomes subject to this Section.
    Thereafter, the owner or operator shall perform the
    inspections at least once every year except for the
    special conditions provided for in subsection (g)
    below.
    C)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (f) below.
    D)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 725.990(c).
    328
    d)
    The owner or operator that controls air pollutant emissions from a
    surface impoundment using a cover vented to a control device shall
    meet the requirements specified in subsections (d)(1) through
    (d)(3) below.
    1)
    The surface impoundment must be covered by a cover and
    vented directly through a closed
    -vent system to a control
    device in accordance with the following requirements:
    A)
    The cover and its closure devices must be designed to
    form a continuous barrier over the entire surface area
    of the liquid in the surface impoundment.
    B)
    Each opening in the cover not vented to the control
    device must be equipped with a closure device. If the
    pressure in the vapor
    headspace underneath the cover
    is less than atmospheric pressure when the control
    device is operating, the closure devices must be
    designed to operate such that when the closure device
    is secured in the closed position there are no visible
    cracks, holes, gaps, or other open spaces in the
    closure device or between the perimeter of the cover
    opening and the closure device. If the pressure in
    the vapor headspace underneath the cover is equal to
    or greater than atmospheric pressure when the control
    device is operating, the closure device must be
    designed to operate with no detectable organic
    emissions using the procedure specified in Section
    725.984(d).
    C)
    The cover and its closure devices must be made of
    suitable materials that will minimize exposure of the
    hazardous waste to the atmosphere, to the extent
    practical, and will maintain the integrity of the
    cover and closure devices throughout their intended
    service life. Factors to be considered when selecting
    the materials for and designing the cover and closure
    devices must include the following: the organic vapor
    permeability; the effects of any contact with the
    liquid or its vapors managed in the surface
    impoundment; the effects of outdoor exposure to wind,
    moisture, and sunlight; and the operating practices
    used for the surface impoundment on which the cover is
    installed.
    D)
    The closed -vent system and control device must be
    designed and operated in accordance with the
    requirements of Section 725.988.
    2)
    Whenever a hazardous waste is in the surface impoundment,
    the cover must be installed with each closure device secured
    in the closed position and the vapor
    headspace underneath
    the cover vented to the control device except as follows:
    A)
    Venting to the control device is not required, and
    opening of closure devices or removal of the cover is
    allowed at the following times:
    i)
    To provide access to the surface impoundment for
    performing routine inspection, maintenance, or
    other activities needed for normal operations.
    329
    Examples of such activities include those times
    when a worker needs to open a port to sample
    liquid in the surface impoundment, or when a
    worker needs to open a hatch to maintain or
    repair equipment. Following completion of the
    activity, the owner or operator shall promptly
    secure the closure device in the closed position
    or reinstall the cover, as applicable, to the
    surface impoundment.
    ii)
    To remove accumulated sludge or other residues
    from the bottom of surface impoundment.
    B)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    3)
    The owner or operator shall inspect and monitor the air
    emission control equipment in accordance with the following
    procedures:
    A)
    The surface impoundment cover and its closure devices
    must be visually inspected by the owner or operator to
    check for defects that could result in air pollutant
    emissions. Defects include, but are not limited to,
    visible cracks, holes, or gaps in the cover Section
    seams or between the interface of the cover edge and
    its foundation mountings; broken, cracked, or
    otherwise damaged seals or gaskets on closure devices;
    and broken or missing hatches, access covers, caps, or
    other closure devices.
    B)
    The closed -vent system and control device must be
    inspected and monitored by the owner or operator in
    accordance with the procedures specified in Section
    725.988.
    C)
    The owner or operator shall perform an initial
    inspection of the air emission control equipment on or
    before the date that the surface impoundment becomes
    subject to this Section. Thereafter, the owner or
    operator shall perform the inspections at least once
    every year except for the special conditions provided
    for in subsection (g) below.
    D)
    In the event that a defect is detected, the owner or
    operator shall repair the defect in accordance with
    the requirements of subsection (f) below.
    E)
    The owner or operator shall maintain a record of the
    inspection in accordance with the requirements
    specified in Section 725.990(c).
    e)
    The owner or operator shall transfer hazardous waste to a surface
    impoundment subject to this Section in accordance with the
    following requirements:
    1)
    Transfer of hazardous waste, except as provided in
    subsection (e)(2) below, to the surface impoundment from
    another surface impoundment subject to this Section or from
    a tank subject to Section 725.985 must be conducted using
    330
    continuous hard-piping or another closed system that does
    not allow exposure of the waste to the atmosphere. For the
    purpose of complying with this provision, an individual
    drain system is considered to be a closed system when it
    meets the requirements of 40 CFR 63, subpart RR, "National
    Emission Standards for Individual Drain Systems",
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    2)
    The requirements of subsection (e)(1) above do not apply
    when transferring a hazardous waste to the surface
    impoundment under either of the following conditions:
    A)
    The hazardous waste meets the average VO concentration
    conditions specified in Section 725.983(c)(1) at the
    point of waste origination.
    B)
    The hazardous waste has been treated by an organic
    destruction or removal process to meet the
    requirements in Section 725.983(c)(2).
    f)
    The owner or operator shall repair each defect detected during an
    inspection performed in accordance with the requirements of
    subsection (c)(3) or (d)(3) above as follows:
    1)
    The owner or operator shall make first efforts at repair of
    the defect no later than five calendar days after detection,
    and repair must be completed as soon as possible but no
    later than 45 calendar days after detection except as
    provided in subsection (f)(2) below.
    2)
    Repair of a defect may be delayed beyond 45 calendar days if
    the owner or operator determines that repair of the defect
    requires emptying or temporary removal from service of the
    surface impoundment and no alternative capacity is available
    at the site to accept the hazardous waste normally managed
    in the surface impoundment. In this case, the owner or
    operator shall repair the defect the next time the process
    or unit that is generating the hazardous waste managed in
    the tank stops operation. Repair of the defect must be
    completed before the process or unit resumes operation.
    g)
    Following the initial inspection and monitoring of the cover as
    required by the applicable provisions of this Subpart, subsequent
    inspection and monitoring may be performed at intervals longer
    than one year in the case when inspecting or monitoring the cover
    would expose a worker to dangerous, hazardous, or other unsafe
    conditions. In this case, the owner or operator may designate the
    cover as an "unsafe to inspect and monitor cover" and comply with
    all of the following requirements:
    1)
    Prepare a written explanation for the cover stating the
    reasons why the cover is unsafe to visually inspect or to
    monitor, if required.
    2)
    Develop and implement a written plan and schedule to inspect
    and monitor the cover using the procedures specified in the
    applicable Section of this Subpart as frequently as
    practicable during those times when a worker can safely
    access the cover.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    331
    Section 725.987
    Standards: Containers
    a)
    The provisions of t
    his Section appliesy to the owners and
    operators ofcontrol of air pollutant emissions from
    containers
    having design capacities greater than 0.1 m
    3
    (3.5 ft
    3
    or 26.4 gal)
    subject to this Subpart into which any hazardous waste is placed,
    except for a container in which all hazardous waste entering the
    container meets the conditions specified in Section 725.983(c).
    for
    which Section 725.983(b) references the use of this Section for
    such air emission control.
    b) An owner or operator shall manage hazardous waste in containers
    using the following procedures:
    1) The owner or operator shall place the hazardous waste into
    one of the following containers, except when a container is
    used for hazardous waste treatment as required by subsection
    (b)(2) below:
    A) A container that is equipped with a cover that
    operates with no detectable organic emissions when all
    container openings (e.g., lids, bungs, hatches, and
    sampling ports) are secured in a closed, sealed
    position. The owner or operator shall determine that
    a container operates with no detectable emissions by
    testing each opening on the container for leaks in
    accordance with Method 21 in 40 CFR 60, Appendix A,
    incorporated by reference in 35 Ill. Adm. Code
    720.111, the first time any portion of the hazardous
    waste is placed into the container. If a leak is
    detected and cannot be repaired immediately, the
    hazardous waste must be removed from the container and
    the container not used to meet the requirements of
    this subsection until the leak is repaired and the
    container is retested.
    B) A container having a desig
    n capacity less than or
    equal to 0.46 m
    3
    (16.2 ft
    3
    or 121.5 gal) that is
    equipped with a cover and complies with all applicable
    U.S. Department of Transportation regulations on
    packaging hazardous waste for transport under 49 CFR
    178, incorporated by reference in 35 Ill. Adm. Code
    720.111.
    i) A container that is managed in accordance with
    the requirements of 49 CFR 178 for the purpose
    of complying with this Subpart is not subject to
    any exceptions to the 49 CFR 178 regulations,
    except as noted in subsection (b)(1)(B)(ii)
    above.
    ii) A lab pack that is managed in accordance with
    the requirements of 49 CFR 178 for the purpose
    of complying with this Subpart may comply with
    the exceptions for combination
    packagings
    specified in 49 CFR 173.12(b).
    C) A container that is attached to or forms a part of any
    truck, trailer, or
    railcar and that has been
    demonstrated within the preceding 12 months to be
    332
    organic vapor tight when all container openings are in
    a closed, sealed position (e.g., the container hatches
    or lids are gasketed and latched). For the purpose of
    meeting the requirements of this subsection, a
    container is organic vapor tight if the container
    sustains a pressure change of not more than 0.75
    kPa
    (0.11 psig or 5.6 mm Hg) within 5 minutes after it is
    pressurized to a minimum of 4.5
    kPa (0.65 psig or 33.7
    mm Hg). This condition is to be demonstrated using
    the pressure test specified in Method 27 of 40 CFR 60,
    Appendix A, incorporated by reference in 35 Ill. Adm.
    Code 720.111, and a pressure measurement device that
    has a precision of ยฑ 2.5 mm water and that is capable
    of measuring above the pressure at which the container
    is to be tested for vapor tightness.
    2) An owner or operator treating hazardous waste in a container
    by either a waste stabilization process, any process that
    requires the addition of heat to the waste, or any process
    that produces an exothermic reaction must meet the following
    requirements:
    A) Whenever it is necessary for the container to be open
    during the treatment process, the container must be
    located inside an enclosure that is vented through a
    closed-vent system to a control device.
    B) The enclosure must be a structure that is designed and
    operated in accordance with the following
    requirements:
    i) The enclosure must be a structure that is
    designed and operated with sufficient airflow
    into the structure to capture the organic vapors
    emitted from the hazardous waste in the
    container and vent the vapors through the
    closed-vent system to the control device.
    ii) The enclosure may have permanent or temporary
    openings to allow worker access, passage of
    containers through the enclosure by conveyor or
    other mechanical means, entry of permanent
    mechanical or electrical equipment, or to direct
    airflow into the enclosure. The pressure drop
    across each opening in the enclosure must be
    maintained at a pressure below atmospheric
    pressure such that whenever an open container is
    placed inside the enclosure no organic vapors
    released from the container exit the enclosure
    through the opening. The owner or operator
    shall determine that an enclosure achieves this
    condition by measuring the pressure drop across
    each opening in the enclosure. If the pressure
    within the enclosure is equal to or greater than
    atmospheric pressure then the enclosure does not
    meet the requirements of this Section.
    C) The closed-vent system and control device must be
    designed and operated in accordance with the
    requirements of Section 725.988.
    333
    3) An owner or operator transferring hazardous wast
    e into a
    container having a design capacity greater than 0.46 m
    3
    (16.2 ft
    3
    or 121.5 gal) shall meet the following
    requirements:
    A) Hazardous waste transfer by pumping must be performed
    using a conveyance system that uses a tube (e.g.,
    pipe, hose) to add the waste into the container.
    During transfer of the waste into the container, the
    cover must remain in place and all container openings
    must be maintained in a closed, sealed position except
    for those openings through which the tube enters the
    container and as provided for in subsection (c) below.
    The tube must be positioned in a manner such that
    either the:
    i) Tube outlet continuously remains submerged below
    the waste surface at all times waste is flowing
    through the tube;
    ii) Lower bottom edge of the tube outlet is located
    at a distance no greater than two inside
    diameters of the tube or 15.25 cm (0.50 ft or
    6.0 in), whichever distance is greater, from the
    bottom of the container at all times waste is
    flowing through the tube; or
    iii) Tube is connected to a permanent port mounted on
    the bottom of the container so that the lower
    edge of the port opening inside the container is
    located at a distance equal to or less than
    15.25 cm (0.50 ft or 6.0 in) from the container
    bottom.
    B) Hazardous waste transferred by a means other than
    pumping must be performed such that during transfer of
    the waste into the container, the cover remains in
    place and all container openings are maintained in a
    closed, sealed position except for those openings
    through which the hazardous waste is added and as
    provided for in subsection (d) below.
    c) Each container opening must be maintained in a closed, sealed
    position (e.g., covered by a
    gasketed lid) at all times that
    hazardous waste is in the container except when it is necessary to
    use the opening to:
    1) Add, remove, inspect, or sample the material in the
    container;
    2) Inspect, maintain, repair, or replace equipment located
    inside the container; or
    3) Vent gases or vapors from a cover located over or
    enclosing
    an open container to a closed-vent system connected to a
    control device that is designed and operated in accordance
    with the requirements of Section 725.988.
    d) One or more safety devices that vent directly to the atmosphere
    may be used on the container, cover, enclosure, closed-vent
    system, or control device provided each device meets all of the
    334
    following conditions:
    1) The safety device is not used for planned or routine venting
    of organic vapors from the container, cover, enclosure, or
    closed-vent system connected to a control device; and
    2) The safety device remains in a closed, sealed position at
    all times except when an unplanned event requires that the
    device open for the purpose of preventing physical damage or
    permanent deformation of the container, cover, enclosure,
    closed-vent system, or control device in accordance with
    good engineering and safety practices for handling
    flammable, combustible, explosive, or other hazardous
    materials. An example of an unplanned event is a sudden
    power outage.
    b)
    General requirements.
    1)
    The owner or operator shall control air pollutant emissions
    from each container subject to this Section in accordance
    with the following requirements, as applicable to the
    container, except when the special provisions for waste
    stabilization processes specified in subsection (b)(2) below
    apply to the container.
    A)
    For a container having a design capacity greater than
    0.1 m
    3
    (26 gal) and less than or equal to 0.46 m
    3
    (120
    gal), the owner or operator shall control air
    pollutant emissions from the container in accordance
    with the Container Level 1 standards specified in
    subsection (c) below.
    B)
    For a container having a design capacity greater than
    0.46 m
    3
    (120 gal) that is not in light material
    service, the owner or operator shall control air
    pollutant emissions from the container in accordance
    with the Container Level 1 standards specified in
    subsection (c) below.
    C)
    For a container having a design capacity greater than
    0.46 m
    3
    (120 gal) that is in light material service,
    the owner or operator shall control air pollutant
    emissions from the container in accordance with the
    Container Level 2 standards specified in subsection
    (d) below.
    2)
    When a container having a design capacity greater than 0.1
    m
    3
    (26 gal) is used for treatment of a hazardous waste by a
    waste stabilization process, the owner or operator shall
    control air pollutant emissions from the container in
    accordance with the Container Level 3 standards specified in
    subsection (e) below at those times during the waste
    stabilization process when the hazardous waste in the
    container is exposed to the atmosphere.
    c)
    Container Level 1 standards.
    1)
    A container using Container Level 1 controls is one of the
    following:
    A)
    A container that meets the applicable U.S. Department
    335
    of Transportation (DOT) regulations on packaging
    hazardous materials for transportation, as specified
    in subsection (f) below.
    B)
    A container equipped with a cover and closure devices
    that form a continuous barrier over the container
    openings so that when the cover and closure devices
    are secured in the closed position there are no
    visible holes, gaps, or other open spaces into the
    interior of the container. The cover may be a
    separate cover installed on the container (e.g., a lid
    on a drum or a suitably secured tarp on a roll
    -off
    box) or may be an integral part of the container
    structural design (e.g., a "portable tank" or bulk
    cargo container equipped with a screw
    -type cap).
    C)
    An open-top container in which an organic
    -vapor
    suppressing barrier is placed on or over the hazardous
    waste in the container such that no hazardous waste is
    exposed to the atmosphere. One example of such a
    barrier is application of a suitable organic-vapor
    suppressing foam.
    2)
    A container used to meet the requirements of subsection
    (c)(1)(B) or (c)(1)(C) above must be equipped with covers
    and closure devices, as applicable to the container, that
    are composed of suitable materials to minimize exposure of
    the hazardous waste to the atmosphere and to maintain the
    equipment integrity for as long as it is in service.
    Factors to be considered in selecting the materials of
    construction and designing the cover and closure devices
    must include the following: the organic vapor permeability,
    the effects of contact with the hazardous waste or its vapor
    managed in the container; the effects of outdoor exposure of
    the closure device or cover material to wind, moisture, and
    sunlight; and the operating practices for which the
    container is intended to be used.
    3)
    Whenever a hazardous waste is in a container using Container
    Level 1 controls, the owner or operator shall install all
    covers and closure devices for the container, as applicable
    to the container, and secure and maintain each closure
    device in the closed position except as follows:
    A)
    Opening of a closure device or cover is allowed for
    the purpose of adding hazardous waste or other
    material to the container as follows:
    i)
    In the case when the container is filled to the
    intended final level in one continuous
    operation, the owner or operator shall promptly
    secure the closure devices in the closed
    position and install the covers, as applicable
    to the container, upon conclusion of the filling
    operation.
    ii)
    In the case when discrete quantities or batches
    of material intermittently are added to the
    container over a period of time, the owner or
    operator shall promptly secure the closure
    devices in the closed position and install
    336
    covers, as applicable to the container, upon
    either the container being filled to the
    intended final level; the completion of a batch
    loading after which no additional material will
    be added to the container within 15 minutes; the
    person performing the loading operation leaving
    the immediate vicinity of the container; or the
    shutdown of the process generating the material
    being added to the container, whichever
    condition occurs first.
    B)
    Opening of a closure device or cover is allowed for
    the purpose of removing hazardous waste from the
    container as follows:
    i)
    For the purpose of meeting the requirements of
    this Section, an empty container, as defined in
    35 Ill. Adm. Code 721.107(b), may be open to the
    atmosphere at any time (i.e., covers and closure
    devices are not required to be secured in the
    closed position on an empty container).
    ii)
    In the case when discrete quantities or batches
    of material are removed from the container but
    the container does not meet the conditions to be
    an empty container, as defined in 35 Ill. Adm.
    Code 721.107(b), the owner or operator shall
    promptly secure the closure devices in the
    closed position and install covers, as
    applicable to the container, upon the completion
    of a batch removal after which no additional
    material will be removed from the container
    within 15 minutes or the person performing the
    unloading operation leaves the immediate
    vicinity of the container, whichever condition
    occurs first.
    C)
    Opening of a closure device or cover is allowed when
    access inside the container is needed to perform
    routine activities other than transfer of hazardous
    waste. Examples of such activities include those
    times when a worker needs to open a port to measure
    the depth of or sample the material in the container,
    or when a worker needs to open a manhole hatch to
    access equipment inside the container. Following
    completion of the activity, the owner or operator
    shall promptly secure the closure device in the closed
    position or reinstall the cover, as applicable to the
    container.
    D)
    Opening of a spring
    -loaded, pressure
    -vacuum rel ief
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the container internal pressure in
    accordance with the design specifications of the
    container. The device must be designed to operate
    with no detectable organic emissions when the device
    is secured in the closed position. The settings at
    which the device opens must be established such that
    the device remains in the closed position whenever the
    337
    internal pressure of the container is within the
    internal pressure operating range determined by the
    owner or operator based on container manufacturer
    recommendations, applicable regulations, fire
    protection and prevention codes, standard engineering
    codes and practices, or other requirements for the
    safe handling of flammable, ignitable, explosive,
    reactive, or hazardous materials. Examples of normal
    operating conditions that may require these devices to
    open are during those times when the internal pressure
    of the container exceeds the internal pressure
    operating range for the container as a result of
    loading operations or diurnal ambient temperature
    fluctuations.
    E)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    4)
    The owner or operator of containers using Container Level 1
    controls must inspect the containers and their covers and
    closure devices as follows:
    A)
    In the case when a hazardous waste already is in the
    container at the time the owner or operator first
    accepts possession of the container at the facility
    and the container is not emptied (i.e., does not meet
    the conditions for an empty container as specified in
    35 Ill. Adm. Code 721.107(b)) within 24 hours after
    the container is accepted at the facility, the owner
    or operator shall visually inspect the container and
    its cover and closure devices to check for visible
    cracks, holes, gaps, or other open spaces into the
    interior of the container when the cover and closure
    devices are secured in the closed position. If a
    defect is detected, the owner or operator shall repair
    the defect in accordance with the requirements of
    subsection (c)(4)(C) below.
    B)
    In the case when a container used for managing
    hazardous waste remains at the facility for a period
    of one year or more, the owner or operator shall
    visually inspect the container and its cover and
    closure devices initially and thereafter, at least
    once every 12 months, to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (c)(4)(C) below.
    C)
    When a defect is detected for the container, cover, or
    closure devices, the owner or operator shall make
    first efforts at repair of the defect no later than 24
    hours after detection, and repair must be completed as
    soon as possible but no later than five calendar days
    after detection. If repair of a defect cannot be
    completed within five calendar days, then the
    hazardous waste must be removed from the container and
    the container must not be used to manage hazardous
    338
    waste until the defect is repaired.
    5)
    The owner or operator shall maintain at the facility a copy
    of the procedure used to determine that containers with
    capacity of 0.46 m
    3
    (120 gal) or greater, which do not meet
    applicable USDOT regulations as specified in subsection (f)
    below, are not managing hazardous waste in light material
    service.
    d)
    Container Level 2 standards.
    1)
    A container using Container Level 2 controls is one of the
    following:
    A)
    A container that meets the applicable U.S. Department
    of Transportation (USDOT) regulations on packaging
    hazardous materials for transportation as specified in
    subsection (f) below.
    B)
    A container that operates with no detectable organic
    emissions, as defined in Section 725.981, and
    determined in accordance with the procedure specified
    in subsection (g) below.
    C)
    A container that has been demonstrated within the
    preceding 12 months to be vapor
    -tight by using 40 CFR
    60, appendix A, Method 27, incorporated by reference
    in 35 Ill. Adm. Code 720.111, in accordance with the
    procedure specified in subsection (h) below.
    2)
    Transfer of hazardous waste in or out of a container using
    Container Level 2 controls must be conducted in such a
    manner as to minimize exposure of the hazardous waste to the
    atmosphere, to the extent practical, considering the
    physical properties of the hazardous waste and good
    engineering and safety practices for handling flammable,
    ignitable, explosive, reactive or other hazardous materials.
    Examples of container loading procedures that the EPA
    considers to meet the requirements of this subsection
    include using any one of the following: a submerged
    -fill
    pipe or other submerged
    -fill method to load liquids into the
    container; a vapor
    -balancing system or a vapor
    -recovery
    system to collect and control the vapors displaced from the
    container during filling operations; or a fitted opening in
    the top of a container through which the hazardous waste is
    filled and subsequently purging the transfer line before
    removing it from the container opening.
    3)
    Whenever a hazardous waste is in a container using Container
    Level 2 controls, the owner or operator shall install all
    covers and closure devices for the container, and secure and
    maintain each closure device in the closed position except
    as follows:
    A)
    Opening of a closure device or cover is allowed for
    the purpose of adding hazardous waste or other
    material to the container as follows:
    i)
    In the case when the container is filled to the
    intended final level in one continuous
    operation, the owner or operator shall promptly
    339
    secure the closure devices in the closed
    position and install the covers, as applicable
    to the container, upon conclusion of the filling
    operation.
    ii)
    In the case when discrete quantities or batches
    of material intermittently are added to the
    container over a period of time, the owner or
    operator shall promptly secure the closure
    devices in the closed position and install
    covers, as applicable to the container, upon
    either the container being filled to the
    intended final level; the completion of a batch
    loading after which no additional material will
    be added to the container within 15 minutes; the
    person performing the loading operation leaving
    the immediate vicinity of the container; or the
    shutdown of the process generating the material
    being added to the container, whichever
    condition occurs first.
    B)
    Opening of a closure device or cover is allowed for
    the purpose of removing hazardous waste from the
    container as follows:
    i)
    For the purpose of meeting the requirements of
    this Section, an empty container as defined in
    35 Ill. Adm. Code 721.107(b) may be open to the
    atmosphere at any time (i.e., covers and closure
    devices are not required to be secured in the
    closed position on an empty container).
    ii)
    In the case when discrete quantities or batches
    of material are removed from the container but
    the container does not meet the conditions to be
    an empty container as defined in 35 Ill. Adm.
    Code 721.107(b), the owner or operator shall
    promptly secure the closure devices in the
    closed position and install covers, as
    applicable to the container, upon the completion
    of a batch removal after which no additional
    material will be removed from the container
    within 15 minutes or the person performing the
    unloading operation leaves the immediate
    vicinity of the container, whichever condition
    occurs first.
    C)
    Opening of a closure device or cover is allowed when
    access inside the container is needed to perform
    routine activities other than transfer of hazardous
    waste. Examples of such activities include those
    times when a worker needs to open a port to measure
    the depth of or sample the material in the container,
    or when a worker needs to open a manhole hatch to
    access equipment inside the container. Following
    completion of the activity, the owner or operator
    shall promptly secure the closure device in the closed
    position or reinstall the cover, as applicable to the
    container.
    D)
    Opening of a spring
    -loaded, pressure
    -vacuum relief
    340
    valve, conservation vent, or similar type of pressure
    relief device which vents to the atmosphere is allowed
    during normal operations for the purpose of
    maintaining the internal pressure of the container in
    accordance with the container design specifications.
    The device must be designed to operate with no
    detectable organic emission when the device is secured
    in the closed position. The settings at which the
    device opens must be established such that the device
    remains in the closed position whenever the internal
    pressure of the container is within the internal
    pressure operating range determined by the owner or
    operator based on container manufacturer
    recommendations, applicable regulations, fire
    protection and prevention codes, standard engineering
    codes and practices, or other requirements for the
    safe handling of flammable, ignitable, explosive,
    reactive, or hazardous materials. Examples of normal
    operating conditions that may require these devices to
    open are during those times when the internal pressure
    of the container exceeds the internal pressure
    operating range for the container as a result of
    loading operations or diurnal ambient temperature
    fluctuations.
    E)
    Opening of a safety device, as defined in Section
    725.981, is allowed at any time conditions require
    doing so to avoid an unsafe condition.
    4)
    The owner or operator of containers using Container Level 2
    controls shall inspect the containers and their covers and
    closure devices as follows:
    A)
    In the case when a hazardous waste already is in the
    container at the time the owner or operator first
    accepts possession of the container at the facility
    and the container is not emptied (i.e., does not meet
    the conditions for an empty container as specified in
    35 Ill. Adm. Code 721.107(b)) within 24 hours after
    the container arrives at the facility, the owner or
    operator shall visually inspect the container and its
    cover and closure devices to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (d)(4)(C) below.
    B)
    In the case when a container used for managing
    hazardous waste remains at the facility for a period
    of one year or more, the owner or operator shall
    visually inspect the container and its cover and
    closure devices initially and thereafter, at least
    once every 12 months, to check for visible cracks,
    holes, gaps, or other open spaces into the interior of
    the container when the cover and closure devices are
    secured in the closed position. If a defect is
    detected, the owner or operator shall repair the
    defect in accordance with the requirements of
    subsection (d)(4)(C) below.
    341
    C)
    When a defect is detected for the container, cover, or
    closure devices, the owner or operator shall make
    first efforts at repair of the defect no later than 24
    hours after detection, and repair must be completed as
    soon as possible but no later than five calendar days
    after detection. If repair of a defect cannot be
    completed within five calendar days, then the
    hazardous waste must be removed from the container and
    the container must not be used to manage hazardous
    waste until the defect is repaired.
    e)
    Container Level 3 standards.
    1)
    A container using Container Level 3 controls is one of the
    following:
    A)
    A container that is vented directly through a
    closed -vent system to a control device in accordance
    with the requirements of subsection (e)(2)(B) below.
    B)
    A container that is vented inside an enclosure which
    is exhausted through a closed
    -vent system to a control
    device in accordance with the requirements of
    subsections (e)(2)(A) and (e)(2)(B) below.
    2)
    The owner or operator shall meet the following requirements,
    as applicable to the type of air emission control equipment
    selected by the owner or operator:
    A)
    The container enclosure must be designed and operated
    in accordance with the criteria for a permanent total
    enclosure as specified in "Procedure T
    --Criteria for
    and Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111. The enclosure may have permanent or
    temporary openings to allow worker access; passage of
    containers through the enclosure by conveyor or other
    mechanical means; entry of permanent mechanical or
    electrical equipment; or direct airflow into the
    enclosure. The owner or operator shall perform the
    verification procedure for the enclosure as specified
    in Section 5.0 to "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" initially when the enclosure is first
    installed and, thereafter, annually.
    B)
    The closed -vent system and control device must be
    designed and operated in accordance with the
    requirements of Section 725.988.
    3)
    Safety devices, as defined in Section 725.981, may be
    installed and operated as necessary on any container,
    enclosure, closed
    -vent system, or control device used to
    comply with the requirements of subsection (e)(1) above.
    4)
    Owners and operators using Container Level 3 controls in
    accordance with the provisions of this Subpart shall inspect
    and monitor the closed
    -vent systems and control devices, as
    specified in Section 725.988.
    342
    5)
    Owners and operators that use Container Level 3 controls in
    accordance with the provisions of this Subpart shall prepare
    and maintain the records specified in Section 725.990(d).
    f)
    For the purpose of compliance with subsection (c)(1)(A) or
    (d)(1)(A) above, containers must be used that meet the applicable
    U.S. Department of Transportation (USDOT) regulations on packaging
    hazardous materials for transportation as follows:
    1)
    The container meets the applicable requirements specified in
    49 CFR 178, "Specifications for Packaging", or 49 CFR 179,
    "Specifications for Tank Cars", both incorporated by
    reference in 35 Ill. Adm. Code 720.111.
    2)
    Hazardous waste is managed in the container in accordance
    with the applicable requirements specified in 49 CFR 107,
    subpart B, "Exemptions"; 49 CFR 172, "Hazardous Materials
    Table, Special Provisions, Hazardous Materials
    Communications, Emergency Response Information, and Training
    Requirements"; 49 CFR 173, "
    Shippers --General Requirements
    for Shipments and Packages"; and 49 CFR 180, "Continuing
    Qualification and Maintenance of
    Packagings", each
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    3)
    For the purpose of complying with this Subpart, no
    exceptions to the 49 CFR 178 or 179 regulations are allowed,
    except as provided for in subsection (f)(4) below.
    4)
    For a lab pack that is managed in accordance with the
    requirements of 49 CFR 178 for the purpose of complying with
    this Subpart, an owner or operator may comply with the
    exceptions for combination
    packagings specified in 49 CFR
    173.12(b), incorporated by reference in 35 Ill. Adm. Code
    720.111.
    g)
    The owner or operator shall use the procedure specified in Section
    725.984(d) for determining a container operates with no detectable
    organic emissions for the purpose of complying with subsection
    (d)(1)(ii) of this Section.
    1)
    Each potential leak interface (i.e., a location where
    organic vapor leakage could occur) on the container, its
    cover, and associated closure devices, as applicable to the
    container, must be checked. Potential leak interfaces that
    are associated with containers include, but are not limited
    to: the interface of the cover rim and the container wall;
    the periphery of any opening on the container or container
    cover and its associated closure device; and the sealing
    seat interface on a spring
    -loaded pressure -relief valve.
    2)
    The test must be performed when the container is filled with
    a material having a volatile organic concentration
    representative of the range of volatile organic
    concentrations for the hazardous wastes expected to be
    managed in this type of container. During the test, the
    container cover and closure devices must be secured in the
    closed position.
    h)
    Procedure for determining a container to be vapor
    -tight using
    Method 27 of 40 CFR 60, appendix A for the purpose of complying
    343
    with subsection (d)(1)(C) above.
    1)
    The test must be performed in accordance with Method 27 of
    40 CFR 60, appendix A, incorporated by reference in 35 Ill.
    Adm. Code 720.111.
    2)
    A pressure measurement device must be used that has a
    precision of ยฑ2.5 mm (0.10 inch) water and that is capable
    of measuring above the pressure at which the container is to
    be tested for vapor tightness.
    3)
    If the test results determined by Method 27 indicate that
    the container sustains a pressure change less than or equal
    to 750 Pascals (0.11 psig) within five minutes after it is
    pressurized to a minimum of 4,500
    Pascals (0.65 psig), then
    the container is determined to be vapor
    -tight.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.988
    Standards: Closed-vent Systems and Control Devices
    a)
    This Section applies to each closed-vent system and control device
    installed and operated by the owner or operator to control air
    emissions in accordance with standards of this Subpart.
    b)
    The closed-vent system must meet the following requirements:
    1)
    The closed-vent system must route the gases, vapors, and
    fumes emitted from the hazardous waste in the waste
    management unit to a control device that meets the
    requirements specified in subsection (c) below.
    2)
    The closed-vent system must be designed and operated in
    accordance with the requirements specified in Section
    725.933(j).
    3) IfWhen the closed-vent system
    contains one or moreincludes
    bypass devices that could be used to divert
    all or a portion
    of the gas es, or vapors, or fumes from entering the control
    device, the owner or operator shall meet the following
    requirements: stream to the atmosphere before entering the
    control device, each bypass device must be equipped with
    either a flow indicator as specified in subsection (b)(3)(A)
    below or a seal or locking device as specified in subsection
    (b)(3)(B) below. For the purpose of complying with this
    subsection, low leg drains, high point bleeds, analyzer
    vents, open -ended valves or lines, spring
    -loaded pressure
    relief valves, and other fittings used for safety purposes
    are not considered to be bypass devices.
    A) For each bypass device except as provided for in
    subsection (b)(3)(B) below, the owner or operator
    shall either:
    i) Install, calibrate, maintain, and operate a flow
    indicator at the inlet to the bypass device that
    indicates at least once every 15 minutes whether
    gas, vapor, or fume flow is present in the
    bypass device; or
    ii) Secure the valve installed at the inlet to the
    344
    bypass device in the closed position using a
    car-seal or a lock-and-key type configuration.
    The owner or operator shall visually inspect the
    seal or closure mechanism at least once every
    month to verify that the valve is maintained in
    the closed position.
    B) Low leg drains, high point bleeds, analyzer vents,
    open-ended valves or lines, and safety devices are not
    subject to the requirements of subsection (b)(3)(A)
    above.
    A)
    If a flow indicator is used to comply with subsection
    (b)(3) below, the indicator must be installed at the
    inlet to the bypass line used to divert gases and
    vapors from the closed
    -vent system to the atmosphere
    at a point upstream of the control device inlet. For
    the purposes of this subsection, a flow indicator
    means a device which indicates the presence of either
    gas or vapor flow in the bypass line.
    B)
    If a seal or locking device is used to comply with
    subsection (b)(3) below, the device must be placed on
    the mechanism by which the bypass device position is
    controlled (e.g., valve handle or damper lever) when
    the bypass device is in the closed position such that
    the bypass device cannot be opened without breaking
    the seal or removing the lock. Examples of such
    devices include, but are not limited to, a car
    -seal or
    a lock -and-key configuration valve. The owner or
    operator shall visually inspect the seal or closure
    mechanism at least once every month to verify that the
    bypass mechanism is maintained in the closed position.
    4)
    The closed -vent system must be inspected and monitored by
    the owner or operator in accordance with the procedure
    specified in Section 725.933(k).
    c)
    The control device must meet the following requirements:
    1)
    The control device
    must be one of the following devices:
    A)
    A control device designed and operated to reduce the
    total organic content of the inlet vapor stream vented
    to the control device by at least 95 percent by
    weight;
    B)
    An enclosed combustion device designed and operated in
    accordance with the requirements of Section
    725.933(c); or
    C)
    A flare designed and operated in accordance with the
    requirements of Section 725.933(d).
    2) The control device must be operating at all times when
    gases, vapors, or fumes are vented from the waste management
    unit through the closed-vent system to the control device.
    2)
    The owner or operator that elects to use a closed
    -vent
    system and control device to comply with the requirements of
    this Section shall comply with the requirements specified in
    345
    subsections (c)(2)(A) through (c)(2)(G) below.
    A)
    Periods of planned routine maintenance of the control
    device, during which the control device does not meet
    the specifications of subsections (c)(1)(A),
    (c)(1)(B), or (c)(1)(C) above, as applicable, must not
    exceed 240 hours per year.
    B)
    The specifications and requirements in subsections
    (c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
    devices do not apply during periods of planned routine
    maintenance.
    C)
    The specifications and requirements in subsections
    (c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
    devices do not apply during a control device system
    malfunction.
    D)
    The owner or operator shall demonstrate compliance
    with the requirements of subsection (c)(2)(A) above
    (i.e., planned routine maintenance of a control
    device, during which the control device does not meet
    the specifications of subsections (c)(1)(i),
    (c)(1)(B), or (c)(1)(C) above, as applicable, must not
    exceed 240 hours per year) by recording the
    information specified in Section 725.990(e)(1)(E).
    E)
    The owner or operator shall correct control device
    system malfunctions as soon as practicable after their
    occurrence in order to minimize excess emissions of
    air pollutants.
    F)
    The owner or operator shall operate the closed
    -vent
    system so that gases, vapors, or fumes are not
    actively vented to the control device during periods
    of planned maintenance or control device system
    malfunction (i.e., periods when the control device is
    not operating or not operating normally), except in
    cases when it is necessary to vent the gases, vapors,
    or fumes to avoid an unsafe condition or to implement
    malfunction corrective actions or planned maintenance
    actions.
    3)
    The owner or operator using a carbon adsorptio
    n system to
    comply with subsection (c)(1) above shall operate and
    maintain the control device in accordance with the following
    requirements:
    A)
    Following the initial startup of the control device,
    all activated carbon in the control device must be
    replaced with fresh carbon on a regular basis in
    accordance with the requirements of Section 725.933(g)
    or 725.933(h).
    B)
    All carbon removed from the control device must be
    managed in accordance with the requirements of Section
    725.933( lm).
    4)
    An owner or operator using a control device other than a
    thermal vapor incinerator, flare, boiler, process heater,
    condenser, or carbon adsorption system to comply with
    346
    subsection (c)(1) above shall operate and maintain the
    control device in accordance with the requirements of
    Section 725.933(i).
    5)
    The owner or operator shall demonstrate that a control
    device achieves the performance requirements of subsection
    (c)(1) above as follows:
    A)
    An owner or operator shall demonstrate using either a
    performance test, as specified in subsection (c)(5)(C)
    below, or a design analysis, as specified in
    subsection (c)(5)(D) below, the performance of each
    control device except for the following:
    i)
    A flare;
    ii)
    A boiler or process heater with a design heat
    input capacity of 44 megawatts or greater;
    iii)
    A boiler or process heater into which the vent
    stream is introduced with the primary fuel;
    iv)
    A boiler or process heater industrial furnace
    burning hazardous waste for which the owner or
    operator has been issued a final permit
    under 35
    Ill. Adm. Code 702, 703, and 705 and that ishas
    designed and operated operates in accordance with
    the requirements of 35 Ill. Adm. Code
    726.Subpart H; or
    v)
    A boiler or process heater industrial furnace
    burning hazardous waste for which the owner or
    operator has certified compliance designed and
    operates in accordance
    with the interim status
    requirements of 35 Ill. Adm. Code 726.Subpart H.
    B)
    An owner or operator shall demonstrate the performance
    of each flare in accordance with the requirements
    specified in Section 725.933(e).
    C)
    For a performance test conducted to meet the
    requirements of subsection (c)(5)(A) above, the owner
    or operator shall use the test methods and procedures
    specified in Section 725.934(c)(1) through (c)(4).
    D)
    For a design analysis conducted to meet the
    requirements of subsection (c)(5)(A) above, the design
    analysis must meet the requirements specified in
    Section 725.935(b)(4)(C).
    E)
    The owner or operator shall demonstrate that a carbon
    adsorption system achieves the performance
    requirements of subsection (c)(1) above based on the
    total quantity of
    organics vented to the atmosphere
    from all carbon adsorption system equipment that is
    used for organic adsorption, organic
    desorption or
    carbon regeneration, organic recovery, and carbon
    disposal.
    6)
    If the owner or operator and the Agency do not agree on a
    demonstration of control device performance using a design
    347
    analysis, then the disagreement must be resolved using the
    results of a performance test performed by the owner or
    operator in accordance with the requirements of subsection
    (c)(5)(C) above. The Agency may choose to have an
    authorized representative observe the performance test.
    7)
    The control device must be inspected and monitored by the
    owner or operator in accordance with the procedures
    specified in Section 265.933(f)(2) and (k). The readings
    from each monitoring device required by Section
    265.933(f)(2) must be inspected at least once each operating
    day to check control device operation. Any necessary
    corrective measures must be immediately implemented to
    ensure the control device is operated in compliance with the
    requirements of this Section.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.989
    Inspection and Monitoring Requirements
    a) This Section applies to
    anThe owner or operator
    usingshall inspect
    and monitor air emission control
    s equipment used to comply with
    this Subpart in accordance with the requirements
    ofspecified in
    Sections 725.985 through 725.988.
    b) Each cover used in accordance with requirements of Sections
    725.985 through 725.987 must be visually inspected and monitored
    for detectable organic emissions by the owner or operator using
    the procedure specified in subsection (f) below, except as
    follows:
    1) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in
    subsection (f) below for the following tank covers:
    A) A tank internal floating roof that is inspect
    ed and
    monitored in accordance with the requirements of
    Section 725.991; or
    B) A tank external floating roof that is inspected and
    monitored in accordance with the requirements of
    Section 725.991.
    2) If a tank is buried partially or entirely underground, an
    owner or operator is required to perform the cover
    inspection and monitoring requirements specified in
    subsection (f) below only for those portions of the tank
    cover and those connections to the tank cover or tank body
    (e.g., fill ports, access hatches, gauge wells, etc.) that
    extend to or above the ground surface and can be opened to
    the atmosphere.
    3) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in
    subsection (f) below for a container that meets all
    requirements specified in either Section 725.987(b)(1)(B) or
    (b)(1)(C).
    4) An owner or operator is exempted from performing the cover
    inspection and monitoring requirements specified in
    subsection (f) below for an enclosure used to control air
    348
    emissions from containers in accordance with the
    requirements of Section 725.987(b)(2).
    b)
    The owner or operator shall develop and implement a written plan
    and schedule to perform the inspections and monitoring required by
    subsection (a) above. The owner or operator shall incorporate
    this plan and schedule into the facility inspection plan required
    under Section 265.115.
    c) Each closed-vent system used in accordance with the requirements
    of Section 725.988 must be inspected and monitored by the owner or
    operator in accordance with the procedure specified in Section
    725.933(j).
    d) Each control device used in accordance with the requirements of
    Section 725.988 must be inspected and monitored by the owner or
    operator in accordance with the procedure specified in Section
    725.933(f).
    e) The owner or operator shall develop and implement a written plan
    and schedule to perform all inspection and monitoring requirements
    of this section. The owner or operator shall incorporate this
    plan and schedule into the facility inspection plan required under
    35 Ill. Adm. Code 725.115.
    f) Inspection and monitoring of a cover in accordance with the
    requirements of subsection (b) above must be performed as follows:
    1) The cover and all cover openings must be initially visually
    inspected and monitored for detectable organic emissions on
    or before the date that the tank, surface impoundment, or
    container using the cover becomes subject to the provisions
    of this Subpart and at other times as requested by the
    Agency.
    2) At least once every 6 months following the initial visual
    inspection and monitoring for detectable organic emissions
    required under subsection (f)(1) above, the owner and
    operator shall visually inspect and monitor the cover and
    each cover opening except for following cover openings:
    A) A cover opening that has continuously remained in a
    closed, sealed position for the entire period since
    the last time the cover opening was visually inspected
    and monitored for detectable emissions;
    B) A cover opening that is designated as unsafe to
    inspect and monitor in accordance with subsection
    (f)(5) below;
    C) A cover opening on a cover installed and placed in
    operation before December 6, 1994 that is designated
    as difficult to inspect and monitor in accordance with
    subsection (f)(6) below.
    3) To visually inspect a cover, the owner or operator shall
    view the entire cover surface and each cover opening in a
    closed, sealed position for evidence of any defect that may
    affect the ability of the cover or cover opening to continue
    to operate with no detectable organic emissions. A visible
    hole, gap, tear, or split in the cover surface or a cover
    349
    opening is defined as a leak that must be repaired in
    accordance with subsection (f)(7) below.
    4) To monitor a cover for detectable organic emissions, the
    owner or operator shall use the following procedure:
    A) Method 21 in 40 CFR 60, appendix A, incorporated by
    reference in 35 Ill. Adm. Code 720.111, to test each
    cover seal and cover connection for detectable organic
    emissions. Seals on floating membrane covers must be
    monitored around the entire perimeter of the cover at
    locations spaced no greater than 3 meters apart.
    B) For all cover connections and seals except for the
    seals around a rotating shaft that passes through a
    cover opening, if the monitoring instrument indicates
    detectable organic emissions (i.e., an instrument
    concentration reading greater than 500
    ppmv plus the
    background level), then a leak is detected. Each
    detected leak must be repaired in accordance with
    subsection (f)(7) below.
    C) For the seals around a rotating shaft that passes
    through a cover opening, if the monitoring instrument
    indicates a concentration reading greater than 10,000
    ppmv, then a leak is detected. Each detected leak
    must be repaired in accordance with subsection (f)(7)
    below.
    5) An owner or operator may designate a cover as an unsafe to
    inspect and monitor cover if all of the following conditions
    are met:
    A) The owner or operator determines that inspe
    ction or
    monitoring of the cover would expose a worker to
    dangerous, hazardous, or other unsafe conditions.
    B) The owner or operator develops and implements a
    written plan and schedule to inspect the cover using
    the procedure specified in subsection (f)(3) above and
    monitor the cover using the procedure specified in
    subsection (f)(4) below as frequently as practicable
    during those times when a worker can safely access the
    cover.
    6) An owner or operator may designate a cover installed and
    placed in operation before December 6, 1994, as a difficult
    to inspect and monitor cover if all of the following
    conditions are met:
    A) The owner or operator determines that inspection or
    monitoring the cover requires elevating a worker to a
    height greater than 2 meters (6.6 ft) above a support
    surface; and
    B) The owner and operator develops and implements a
    written plan and schedule to inspect the cover using
    the procedure specified in subsection (f)(3) above,
    and to monitor the cover using the procedure specified
    in subsection (f)(4) above at least once per calendar
    year.
    350
    7) When a leak is detected by either of the methods specified
    in subsection (f)(3) or (f)(4) above, the owner or operator
    shall repair the leak in the following manner:
    A) The owner or operator shall make a first attempt at
    repairing the leak no later than 5 calendar days after
    the leak is detected. Repair of the leak must be
    completed as soon as practicable, but no later than 15
    calendar days after the leak is detected. If repair
    of the leak cannot be completed within the 15-day
    period, except as provided in subsection (f)(7)(B)
    below, then the owner or operator shall not add
    hazardous waste to the tank, surface impoundment, or
    container on which the cover is installed until the
    repair of the leak is completed.
    B) Repair of a leak detected on a cover installed on a
    tank or surface impoundment may be delayed beyond 15
    calendar days if the owner or operator determines that
    both of the following conditions occur:
    i) Repair of the leak requires first emptying the
    contents of the tank or surface impoundment; and
    ii) Temporary removal of the tank or surface
    impoundment from service will result in the
    unscheduled cessation of production from the
    process unit or operation of the waste
    management unit that is generating the hazardous
    waste managed in the tank or surface
    impoundment.
    C) Repair of a leak determined by the owner or operator
    to meet the conditions specified in subsection
    (f)(7)(B) above must be performed at the next time the
    process, system, or waste management unit that is
    generating the hazardous waste managed in the tank or
    surface impoundment stops operation for any reason.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.990
    Recordkeeping Requirements
    a)
    Each owner or operator of a facility subject to requirements in
    this Subpart shall record and maintain the
    following information
    specified in subsections (b) through (i) of this Section,
    as
    applicable : to the facility. Except for air emission control
    equipment design documentation and information required by
    subsection (i) below, records required by this Section must be
    maintained in the operating record for a minimum of three years.
    Air emission control equipment design documentation must be
    maintained in the operating record until the air emission control
    equipment is replaced or is otherwise no longer in service.
    Information required by subsection (i) below must be maintained in
    the operating record for as long as the tank or container is not
    using air emission controls specified in Sections 264.984 through
    264.987, in accordance with the conditions specified in Section
    724.984(d).
    1) Documentation for each cover installed on a tank in
    351
    accordance with the requirements of Section 725.985(b)(2) or
    (b)(3) that includes information prepared by the owner or
    operator or provided by the cover manufacturer or vendor
    describing the cover design, and certification by the owner
    or operator that the cover meets the applicable design
    specifications as listed in Section 725.991(c).
    2) Documentation for each floating membrane cover installed on
    a surface impoundment in accordance with the requirements of
    Section 725.986(c) that includes information prepared by the
    owner or operator or provided by the cover manufacturer or
    vendor describing the cover design, and certification by the
    owner or operator that the cover meets the specifications
    listed in Section 725.986(e).
    3) Documentation for each enclosure used to control air
    emissions from containers in accordance with the
    requirements of Section 725.987(b)(2)(A) that includes
    information prepared by the owner or operator or provided by
    the manufacturer or vendor describing the enclosure design,
    and certification by the owner or operator that the
    enclosure meets the specifications listed in Section
    725.987(b)(2)(B).
    4) Documentation for each closed-vent system and control device
    installed in accordance with the requirements of Section
    725.988 that includes:
    A) Certificatio n that is signed and dated by the owner or
    operator stating that the control device is designed
    to operate at the performance level documented by a
    design analysis, as specified in subsection (a)(4)(B)
    below, or by performance tests, as specified in
    subsection (a)(4)(C) below, when the tank, surface
    impoundment, or container is or would be operating at
    capacity or the highest level reasonably expected to
    occur.
    B) If a design analysis is used, then design
    documentation as specified in Section 725.935(b)(4).
    The documentation must include information prepared by
    the owner or operator or provided by the control
    device manufacturer or vendor that describes the
    control device design in accordance with Section
    725.935(b)(4)(C) and certification by the owner or
    operator that the control equipment meets the
    applicable specifications.
    C) If performance tests are used, then a performance test
    plan as specified in Section 725.935(b)(3) and all
    test results.
    D) Information as required by Sections 725.935(c)
    (1) and
    725.935(c)(2).
    5) Records for all Method 27 tests performed by the owner or
    operator for each container used to meet the requirements of
    Section 725.987(b)(1)(C).
    6) Records for all visual inspections conducted in accordance
    with the requirements of Section 725.989.
    352
    7) Records for all monitoring for detectable organic emissions
    conducted in accordance with the requirements of Section
    725.989.
    8) Records of the date of each attempt to repair a leak, repair
    methods applied, and the date of successful repair.
    9) Records for all continuous monitoring conducted in
    accordance with the requirements of Section 725.989.
    10) Records of the management of carbon removed from a carbon
    adsorption system conducted in accordance with Section
    725.988(c)(3)(B).
    11) Records for all inspections of each cover installed on a
    tank in accordance with the requirements of Section
    725.985(b)(2) or (b)(3) that includes information as listed
    in Section 725.991(c).
    b) AnThe owner or operator
    electing to useof a tank using air
    emission controls
    for a tank in accordance with the
    conditions
    specified inrequirements of Section 725.985 (c) shall record prepare
    and maintain records for the tank that include
    the following
    information:
    1) The date and time each waste sample is collected for direct
    measurement of maximum organic vapor pressure in accordance
    with Section 725.984(c).
    1)
    For each tank using air emission controls in accordance with
    the requirements of Section 725.985 of this Subpart, the
    owner or operator shall record:
    A)
    A tank identification number (or other unique
    identification description as selected by the owner or
    operator).
    B)
    A record for each inspection required by Section
    725.985 that includes the following information:
    i)
    Date inspection was conducted.
    ii)
    For each defect detected during the inspection,
    the following information: the location of the
    defect, a description of the defect, the date of
    detection, and corrective action taken to repair
    the defect. In the event that repair of the
    defect is delayed in accordance with the
    provisions of Section 725.985, the owner or
    operator shall also record the reason for the
    delay and the date that completion of repair of
    the defect is expected.
    2) The results of each determination for the maximum organic
    vapor pressure of the waste in the tank performed in
    accordance with Section 725.984(c).
    2)
    In addition to the information required by subsection (b)(1)
    above, the owner or operator shall record the following
    information, as applicable to the tank:
    353
    A)
    The owner or operator using a fixed roof to comply
    with the Tank Level 1 control requirements specified
    in Section 725.985(c) shall prepare and maintain
    records for each determination for the maximum organic
    vapor pressure of the hazardous waste in the tank
    performed in accordance with the requirements of
    Section 725.985(c). The records must include the date
    and time the samples were collected, the analysis
    method used, and the analysis results.
    B)
    The owner or operator using an internal floating roof
    to comply with the Tank Level 2 control requirements
    specified in Section 725.985(e) shall prepare and
    maintain documentation describing the floating roof
    design.
    C)
    Owners and operators using an external floating roof
    to comply with the Tank Level 2 control requirements
    specified in Section 725.985(f) shall prepare and
    maintain the following records:
    i)
    Documentation describing the floating roof
    design and the dimensions of the tank.
    ii)
    Records for each seal gap inspection required by
    Section 725.985(f)(3) describing the results of
    the seal gap measurements. The records must
    include the date that the measurements were
    performed, the raw data obtained for the
    measurements, and the calculations of the total
    gap surface area. In the event that the seal
    gap measurements do not conform to the
    specifications in Section 725.985(f)(1), the
    records must include a description of the
    repairs that were made, the date the repairs
    were made, and the date the tank was emptied, if
    necessary.
    D)
    Each owner or operator using an enclosure to comply
    with the Tank Level 2 control requirements specified
    in Section 725.985(i) shall prepare and maintain the
    following records:
    i)
    Records for the most recent set of calculations
    and measurements performed by the owner or
    operator to verify that the enclosure meets the
    criteria of a permanent total enclosure as
    specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total
    Enclosure" under 40 CFR 52.741, appendix B,
    incorporated by reference in 35 Ill. Adm. Code
    720.111.
    ii)
    Records required for the closed
    -vent system and
    control device in accordance with the
    requirements of subsection (e) below.
    3) The records specifying the tank dimensions and design
    capacity.
    354
    c) An owner or operator electing to use air emission controls for a
    tank in accordance with the requirements of Section 725.991 shall
    record the information required by Section 725.991(c).
    c)
    The owner or operator of a surface impoundment using air emission
    controls in accordance with the requirements of Section 725.986
    shall prepare and maintain records for the surface impoundment
    that include the following information:
    1)
    A surface impoundment identification number (or other unique
    identification description as selected by the owner or
    operator).
    2)
    Documentation describing the floating membrane cover or
    cover design, as applicable to the surface impoundment, that
    includes information prepared by the owner or operator or
    provided by the cover manufacturer or vendor describing the
    cover design, and certification by the owner or operator
    that the cover meets the specifications listed in Section
    725.986(c).
    3)
    A record for each inspection required by Section 725.986
    that includes the following information:
    A)
    Date inspection was conducted.
    B)
    For each defect detected during the inspection the
    following information: the location of the defect, a
    description of the defect, the date of detection, and
    corrective action taken to repair the defect. In the
    event that repair of the defect is delayed in
    accordance with the provisions of Section 725.986(f),
    the owner or operator shall also record the reason for
    the delay and the date that completion of repair of
    the defect is expected.
    4)
    For a surface impoundment equipped with a cover and vented
    through a closed -vent system to a control device, the owner
    or operator shall prepare and maintain the records specified
    in subsection (e) below.
    d) An owner or operator electing not to
    use air emission controls for
    a particular tank, surface impoundment, or container subject to
    this Subpart in accordance with the conditions specified in
    Section 725.983(c) shall record the information used by the owner
    or operator for each waste determination (e.g., test results,
    measurements, calculations, and other documentation) in the
    facility operating log. If analysis results for waste samples are
    used for the waste determination, then the owner or operator shall
    record the date, time, and location that each waste sample is
    collected in accordance with applicable requirements of Section
    725.984.
    d)
    The owner or operator of containers using Container Level 3 air
    emission controls in accordance with the requirements of Section
    725.987 shall prepare and maintain records that include the
    following information:
    1)
    Records for the most recent set of calculations and
    measurements performed by the owner or operator to verify
    that the enclosure meets the criteria of a permanent total
    355
    enclosure as specified in "Procedure T
    --Criteria for and
    Verification of a Permanent or Temporary Total Enclosure"
    under 40 CFR 52.741, appendix B, incorporated by reference
    in 35 Ill. Adm. Code 720.111.
    2)
    Records required for the closed
    -vent system and control
    device in accordance with the requirements of subsection (e)
    below.
    e) An owner or operator electing to comply with requirements in
    accordance with Section 725.983(c)(2)(E) or (c)(2)(F) shall record
    the identification number for the incinerator, boiler, or
    industrial furnace in which the hazardous waste is treated.
    e)
    The owner or operator using a closed
    -vent system and control
    device in accordance with the requirements of Section 725.988
    shall prepare and maintain records that include the following
    information:
    1)
    Documentation for the closed
    -vent system and control device
    that includes:
    A)
    Certification that is signed and dated by the owner or
    operator stating that the control device is designed
    to operate at the performance level documented by a
    design analysis as specified in subsection (e)(1)(B)
    below or by performance tests as specified in
    subsection (e)(1)(C) below when the tank, surface
    impoundment, or container is or would be operating at
    capacity or the highest level reasonably expected to
    occur.
    B)
    If a design analysis is used, then design
    documentation, as specified in Section 265.935(b)(4).
    The documentation must include information prepared
    by the owner or operator or provided by the control
    device manufacturer or vendor that describes the
    control device design in accordance with Section
    265.1035(b)(4)(C) and certification by the owner or
    operator that the control equipment meets the
    applicable specifications.
    C)
    If performance tests are used, then a performance test
    plan as specified in Section 265.935(b)(3) and all
    test results.
    D)
    Information as required by 40 CFR 265.1035(c)(1) and
    Section 725.935(c)(2), as applicable.
    E)
    An owner or operator shall record, on a semiannual
    basis, the information specified in subsections
    (e)(1)(E)(i) and (e)(1)(E)(ii) below for those planned
    routine maintenance operations that would require the
    control device not to meet the requirements of Section
    725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as
    applicable.
    i)
    A description of the planned routine maintenance
    that is anticipated to be performed for the
    control device during the next six-month period.
    This description must include the type of
    356
    maintenance necessary, planned frequency of
    maintenance, and lengths of maintenance periods.
    ii)
    A description of the planned routine maintenance
    that was performed for the control device during
    the previous six -month period. This description
    must include the type of maintenance performed
    and the total number of hours during those six
    months that the control device did not meet the
    requirements of Section 725.988(c)(1)(A),
    (c)(1)(B), or (c)(1)(C), as applicable, due to
    planned routine maintenance.
    F)
    An owner or operator shall record the information
    specified in subsections (e)(1)(F)(i) through
    (e)(1)(F)(iii) below for those unexpected control
    device system malfunctions that would require the
    control device not to meet the requirements of Section
    725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as
    applicable.
    i)
    The occurrence and duration of each malfunction
    of the control device system.
    ii)
    The duration of each period during a malfunction
    when gases, vapors, or fumes are vented from the
    waste management unit through the closed
    -vent
    system to the control device while the control
    device is not properly functioning.
    iii)
    Actions taken during periods of malfunction to
    restore a malfunctioning control device to its
    normal or usual manner of operation.
    G)
    Records of the management of carbon removed from a
    carbon adsorption system conducted in accordance with
    Section 725.988(c)(3)(B).
    f)
    The owner or operator of a tank, surface impoundment, or container
    exempted from standards in accordance with the provisions of
    Section 725.983(c) of this Subpart shall prepare and maintain the
    following records, as applicable:
    1)
    For tanks, surface
    impoundments, or containers exempted
    under the hazardous waste organic concentration conditions
    specified in Section 725.983 (c)(1) or (c)(2) of this
    Subpart, the owner or operator shall record the information
    used for each waste determination (e.g., test results,
    measurements, calculations, and other documentation) in the
    facility operating log. If analysis results for waste
    samples are used for the waste determination, then the owner
    or operator shall record the date, time, and location that
    each waste sample is collected in accordance with applicable
    requirements of Section 725.984 of this Subpart.
    2)
    For tanks, surface
    impoundments, or containers exempted
    under the provisions of Section 725.983(c)(2)(vii) or
    Section 725.983(c)(2)(viii) of this Subpart, the owner or
    operator shall record the identification number for the
    incinerator, boiler, or industrial furnace in which the
    hazardous waste is treated.
    357
    fg)
    An owner or operator designating a cover as
    "unsafe to inspect and
    monitor " pursuant to Section
    725.989(f)(5) 725.985(l) or difficult
    to inspect and monitor pursuant to Section 725.989(f)(6)
    shall
    record in a log that is kept in the facility operating record the
    following information:
    the identification numbers for waste
    management units with covers that are designated as "unsafe to
    inspect and monitor", the explanation for each cover stating why
    the cover is unsafe to inspect and monitor, and the plan and
    schedule for inspecting and monitoring each cover.
    1) A list of identification numbers for tanks with covers that
    are designated as unsafe to inspect and monitor in
    accordance with the requirements of Section 725.989(f)(5),
    an explanation for each cover stating why the cover is
    unsafe to inspect and monitor, and the plan and schedule for
    inspecting and monitoring each cover.
    2) A list of identification numbers for tanks with covers that
    are designated as difficult to inspect and monitor in
    accordance with the requirements of Section 725.989(f)(6),
    an explanation for each cover stating why the cover is
    difficult to inspect and monitor, and the plan and schedule
    for inspecting and monitoring each cover.
    g) All records required by subsections (a) through (f) above, except
    as required in subsections (a)(1) through (a)(4) above, must be
    maintained in the operating record for a minimum of 3 years. All
    records required by subsections (a)(1) through (a)(4) above must
    be maintained in the operating record until the air emission
    control equipment is replaced or otherwise no longer in service.
    h)
    The owner or operator of a facility that is subject to this
    Subpart and to the control device standards in 40 CFR 60, Subpart
    VV, or 40 CFR 61, Subpart V, incorporated by reference in 35 Ill.
    Adm. Code 270.111, may elect to demonstrate compliance with the
    applicable Sections of this Subpart by documentation either
    pursuant to this Subpart, or pursuant to the provisions of 40 CFR
    60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
    documentation required by 40 CFR 60 or 61 duplicates the
    documentation required by this Section.
    i)
    For each tank or container not using air emission controls
    specified in Sections 725.985 through 725.988 in accordance with
    the conditions specified in Section 725.980(d), the owner or
    operator shall record and maintain the following information:
    1)
    A list of the individual organic peroxide compounds
    manufactured at the facility that meet the conditions
    specified in Section 725.980(d)(1).
    2)
    A description of how the hazardous wast
    e containing the
    organic peroxide compounds identified pursuant to subsection
    (i)(1) are managed at the facility in tanks and containers.
    This description must include the following information:
    A)
    For the tanks used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to describe each tank: a facility
    identification number for the tank, the purpose and
    placement of this tank in the management train of this
    358
    hazardous waste, and the procedures used to ultimately
    dispose of the hazardous waste managed in the tanks.
    B)
    For containers used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to describe
    the following for
    each
    tankcontainer : a facility identification number for
    the container or group of containers, the purpose and
    placement of this container or group of containers in
    the management train of this hazardous waste, and the
    procedures used to ultimately dispose of the hazardous
    waste managed in the containers.
    B)
    For containers used at the facility to manage these
    hazardous wastes, sufficient information must be
    provided to describe: A facility identification number
    for the container or group of containers; the purpose
    and placement of this container, or group of
    containers, in the management train of this hazardous
    waste; and the procedures used to ultimately dispose
    of the hazardous waste handled in the containers.
    3)
    An explanation of why managing the hazardous waste
    containing the organic peroxide compounds identified
    pursuant to subsection (i)(1) above in the tanks or
    containers identified pursuant to subsection (i)(2) above
    would create an undue safety hazard if the air emission
    controls specified in Sections 725.985 through 725.988 were
    installed and operated on these waste management units.
    This explanation must include the following information:
    A)
    For tanks used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to explain: how use of the required air
    emission controls on the tanks would affect the tank
    design features and facility operating procedures
    currently used to prevent an undue safety hazard
    during the management of this hazardous waste in the
    tanks; and why installation of safety devices on the
    required air emission controls, as allowed under
    Section 725.985(g)
    this Subpart , would not address
    those situations in which evacuation of tanks equipped
    with these air emission controls is necessary and
    consistent with good engineering and safety practices
    for handling organic peroxides.
    B)
    For containers used at the facility to manage this
    hazardous waste, sufficient information must be
    provided to explain: how use of the required air
    emission controls on the
    tankscontainers would affect
    the container design features and handling procedures
    currently used to prevent an undue safety hazard
    during management of this hazardous waste in the
    containers; and why installation of safety devices on
    the required air emission controls, as allowed under
    Section 725.987(d)
    this Subpart , would not address
    those situations in which evacuation of containers
    equipped with these air emission controls is necessary
    and consistent with good engineering and safety
    practices for handling organic peroxides.
    359
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.991
    Alternative Tank Emission Control Requirements
    (Repealed)
    a) This Section applies to owners and operators of tanks electing to
    comply with Section 725.985(b)(2) or (b)(3).
    1) The owner or operator electing to comply with Section
    725.985(b)(2) shall design, install, operate, and maintain a
    fixed roof and internal floating roof that meet the
    following requirements.
    A) The fixed roof must comply with the requirements of
    Section 725.985(d)(1). The internal floating roof
    must rest or float on the waste surface (but not
    necessarily in complete contact with it) inside a tank
    that has a fixed roof. The internal floating roof
    must be floating on the waste surface at all times,
    except during initial fill and during those intervals
    when the tank is completely emptied or subsequently
    emptied and refilled. When the roof is resting on the
    leg supports, the process of filling, emptying, or
    refilling must be
    as continuous as possible, based on
    the amount of waste and the nature of the waste
    handling operation,
    and must be accomplished as
    rapidly as possible.
    B) Each internal floating roof must be equipped with one
    of the following closure devices between the wall of
    the tank and the edge of the internal floating roof:
    i) A foam- or liquid-filled seal mounted in contact
    with the waste (liquid-mounted seal). A liquid-
    mounted seal means a foam- or liquid-filled seal
    mounted in contact with the waste between the
    wall of the tank and the floating roof
    continuously around the circumference of the
    tank.
    ii) Two seals mounted one above the other so that
    each forms a continuous closure that completely
    covers the space between the wall of the tank
    and the edge of the internal floating roof. The
    lower seal may be vapor-mounted, but both must
    be continuous.
    iii) A mechanical shoe seal. A mechanical shoe seal
    is a metal sheet held vertically against the
    wall of the tank by springs or weighted levers
    and is connected by braces to the floating roof.
    A flexible coated fabric (envelope) spans the
    annular space between the metal sheet and the
    floating roof.
    C) Each opening in a
    noncontact internal floating roof
    except for automatic bleeder vents (vacuum breaker
    vents) and the rim space vents is to provide a
    projection below the waste surface.
    D) Each opening in the internal floating roof except for
    leg sleeves, automatic bleeder vents, rim space vents,
    360
    column wells, ladder wells, sample wells, and stub
    drains is to be equipped with a cover or lid that is
    to be maintained in a closed position at all times
    (i.e., no visible gap), except when the device is in
    actual use. The cover or lid must be equipped with a
    gasket. Covers on each access hatch and automatic
    gauge float well must be bolted, except when they are
    in use.
    E) Automatic bleeder vents must be equipped with a gasket
    and are to be closed at all times when the roof is
    floating, except when the roof is being floated off or
    is being landed on the roof leg supports.
    F) Rim space vents must be equipped with a gasket and are
    to be set to open only when the internal floating roof
    is not floating or at the manufacturer's recommended
    setting.
    G) Each penetration of the internal floating roof for the
    purpose of sampling must be a sample well. The sample
    well must have a slit fabric cover that covers at
    least 90 percent of the opening.
    H) Each penetration of the internal floating roof that
    allows for passage of a column supporting the fixed
    roof must have a flexible fabric sleeve seal or a
    gasketed sliding cover.
    I) Each penetration of the internal floating roof that
    allows for passage of a ladder must have a
    gasketed
    sliding cover.
    2) The owner or operator electing to comply with Section
    725.985(b)(3) shall design, install, operate, and maintain
    an external floating roof that meets the following
    requirements:
    A) Each external floating roof must be equipped with a
    closure device between the wall of the tank and the
    roof edge. The closure device is to consist of two
    seals, one above the other. The lower seal is
    referred to as the primary seal, and the upper seal is
    referred to as the secondary seal.
    i) The primary seal must be either a mechanical
    shoe seal or a liquid-mounted seal. Except as
    provided in subsection (b)(2)(D) below, the seal
    must completely cover the annular space between
    the edge of the floating roof and tank wall.
    ii) The secondary seal must completely cover the
    annular space between the external floating roof
    and the wall of the tank in a continuous fashion
    except as allowed in subsection (b)(2)(D) below.
    B) Except for automatic bleeder vents and rim space
    vents, each opening in a
    noncontact external floating
    roof must provide a projection below the waste
    surface. Except for automatic bleeder vents, rim
    space vents, roof drains, and leg sleeves, each
    361
    opening in the roof is to be equipped with a
    gasketed
    cover, seal, or lid that is to be maintained in a
    closed position at all times (i.e., no visible gap),
    except when the device is in actual use. Automatic
    bleeder vents are to be closed at all times when the
    roof is floating, except when the roof is being
    floated off or is being landed on the roof leg
    supports. Rim vents are to be set to open when the
    roof is being floated off the roof leg supports or at
    the manufacturer's recommended setting. Automatic
    bleeder vents and rim space vents are to be
    gasketed.
    Each emergency roof drain is to be provided with a
    slotted membrane fabric cover that covers at least 90
    percent of the area of the opening.
    C) The roof must be floating on the waste at all times
    (i.e., off the roof leg supports), except during
    initial fill until the roof is lifted off leg supports
    and when the tank is completely emptied and
    subsequently refilled. The process of filling,
    emptying, or refilling when the roof is resting on the
    leg supports must be continuous and must be
    accomplished as rapidly as possible.
    3) The owner or operator may elect to comply with Section
    725.985(b)(2) or (b)(3) using an alternative means of
    emission limitation for which U.S. EPA has published a
    Federal Register notice in accordance with the requirements
    of 40 CFR 60.114b permitting its use as an alternative means
    for the purpose of compliance with 40 CFR 60.112b.
    b) Monitoring and inspection of
    the control equipment described in
    subsection (a) above must be conducted as follows:
    1) After installation, owners and operators of internal
    floating roofs shall:
    A) Visually inspect the internal floating roof, the
    primary seal, and the secondary seal (if one is in
    service), prior to filling the tank with waste. If
    there are holes, tears, or other openings in the
    primary seal, the secondary seal, or the seal fabric,
    or defects in the internal floating roof, or both, the
    owner or operator shall repair the items before
    filling the tank.
    B) For tanks equipped with a liquid-mounted or mechanical
    shoe primary seal, visually inspect the internal
    floating roof and the primary seal or the secondary
    seal (if one is in service) through manholes and roof
    hatches on the fixed roof at least once every 12
    months after initial fill. If the internal floating
    roof is not resting on the surface of the waste inside
    the tank, or there is liquid accumulated on the roof,
    or the seal is detached, or there are holes or tears
    in the seal fabric, the owner or operator shall repair
    the items or empty and remove the tank from service
    within 45 days. If a failure that is detected during
    inspections required in this subsection cannot be
    repaired within 45 days and if the tank cannot be
    emptied within 45 days, the Agency may grant the owner
    362
    or operator a provisional variance pursuant to Section
    35(b) of the Act that extends this time for up to 30
    days. Such a request for an extension must comply
    with 35 Ill. Adm. Code 180, and it must document that
    alternate capacity is unavailable and specify a
    schedule of actions the owner or operator will take
    that will assure that the control equipment will be
    repaired or the tank will be emptied as soon as
    possible.
    C) For tanks equipped with a double-seal system as
    specified in subsection (a)(1)(A)(ii) above:
    i) Visually inspect the tank, as specified in
    subsection (b)(1)(D) below, at least every 5
    years; or
    ii) Visually inspect the tank as specified in
    subsection (b)(1)(B) above.
    D) Visually inspect the internal floating roof, the
    primary seal, the secondary seal (if one is in
    service), gaskets, slotted membranes, and sleeve seals
    (if any) each time the tank is emptied and degassed.
    If the internal floating roof has defects; the primary
    seal has holes, tears, or other openings in the seal
    or the seal fabric; the secondary seal has holes,
    tears, or other openings in the seal or the seal
    fabric; the gaskets no longer close off the waste
    surfaces from the atmosphere; or the slotted membrane
    has more than 10 percent open area, the owner or
    operator shall repair the items as necessary, so that
    none of the conditions specified in this subsection
    exist before refilling the tank with waste. In no
    event may inspections conducted in accordance with
    this provision occur at intervals greater than 10
    years, in the case of tanks conducting the annual
    visual inspection as specified in subsection (b)(1)(B)
    above, or at intervals no greater than 5 years, in the
    case of tanks specified in subsection (b)(1)(C) above.
    E) Notify the Agency in writing at least 30 days prior to
    the filling or refilling of each tank for which an
    inspection is required by subsections (b)(1)(A) and
    (b)(1)(D) above, to afford the Agency the opportunity
    to have an observer present. If the inspection
    required by subsection (b)(1)(D) above is not planned
    and the owner or operator could not have known about
    the inspection 30 days in advance of refilling the
    tank, the owner or operator shall notify the Agency at
    least 7 days prior to the refilling of the tank.
    Notification must be made by telephone immediately
    followed by written documentation demonstrating why
    the inspection was unplanned. Alternatively, this
    notification, including the written documentation, may
    be made in writing and sent by express mail so that it
    is received by the Agency at least 7 days prior to the
    refilling.
    2) After installation, the owner or operator of an external
    floating roof shall:
    363
    A) Determine the gap areas and maximum gap widt
    hs between
    the primary seal and the wall of the tank and between
    the secondary seal and the wall of the tank according
    to the following frequency:
    i) Measurements of gaps between the tank wall and
    the primary seal (seal gaps) must be performed
    during the hydrostatic testing of the tank or
    within 60 days of the initial fill with waste
    and at least once every five years thereafter.
    ii) Measurements of gaps between the tank wall and
    the secondary seal must be performed within 60
    days of the initial fill with waste and at least
    once per year thereafter.
    iii) If any tank ceases to hold waste for a period of
    one year or more, subsequent introduction of
    waste into the tank must be considered an
    initial fill for the purposes of subsections
    (b)(2)(A)(i) and (b)(2)(A)(ii) above.
    B) Determine the gap widths and areas in the primary and
    secondary seals individually by the following
    procedures:
    i) Measure seal gaps, if any, at one or more
    floating roof levels when the roof is floating
    off the roof leg supports.
    ii) Measure seal gaps around the entire
    circumference of the tank in each place where a
    0.32-cm diameter uniform probe passes freely
    (without forcing or binding against the seal)
    between the seal and the wall of the tank and
    measure the circumferential distance of each
    such location.
    iii) Determine the total surface area of each gap
    described in subsection (b)(2)(B)(ii) above by
    using probes of various widths to measure
    accurately the actual distance from the tank
    wall to the seal and multiplying each such width
    by its respective circumferential distance.
    C) Add the gap surface area of each gap location for the
    primary seal and the secondary seal individually and
    divide the sum for each seal by the nominal diameter
    of the tank and compare each ratio to the respective
    standards in subsection (b)(2)(D) below.
    D) Make necessary repairs or empty the tank within 45
    days of identification in any inspection for seals not
    meeting the following requirements:
    i) The accumulated area
    of gaps between the tank
    wall and the mechanical shoe or liquid-mounted
    primary seal must not exceed 212 cm
    2
    per meter
    (10.0 in
    2
    per foot) of tank diameter, and the
    width of any portion of any gap must not exceed
    364
    3.81 cm (1.50 in). One end of the mechanical
    shoe is to extend into the waste contained in
    the tank, and the other end is to extend a
    minimum vertical distance of 61 cm (24.0 in)
    above the waste surface. There are to be no
    holes, tears, or other openings in the shoe,
    seal fabric, or seal envelope.
    ii) The secondary seal is to meet the following
    requirements: The secondary seal is to be
    installed above the primary seal so that it
    completely covers the space between the roof
    edge and the tank wall except as provided in
    subsection (b)(2)(B)(iii) above. The
    accumulated area of gaps between the tank wall
    and the secondary seal must not exceed 21.2 cm
    2
    per meter (1.00 in
    2
    per foot) of tank diameter,
    and the width of any portion of any gap must not
    exceed 1.27 cm (0.500 in). There are to be no
    holes, tears, or other openings in the seal or
    seal fabric.
    E) If a failure that is detected during inspections
    required in subsection (b)(2)(A) above cannot be
    repaired within 45 days and if the tank cannot be
    emptied within 45 days, the Agency may grant the owner
    or operator a provisional variance pursuant to Section
    35(b) of the Act that extends this time for up to 30
    days. Such a request for an extension must comply
    with 35 Ill. Adm. Code 180, and it must include a
    demonstration of the unavailability of alternate
    capacity and a specification of a schedule that will
    assure that the control equipment will be repaired or
    the tank will be emptied as soon as possible.
    F) Notify the Agency 30 days in advance of any gap
    measurements required by subsection (b)(2)(A) above,
    to afford the Agency the opportunity to have an
    observer present.
    G) Visually inspect the external floating roof, the
    primary seal, secondary seal, and fittings each time
    the vessel is emptied and degassed.
    i) If the external fl
    oating roof has defects, the
    primary seal has holes, tears, or other openings
    in the seal or the seal fabric, or the secondary
    seal has holes, tears, or other openings in the
    seal or the seal fabric, the owner or operator
    shall repair the items as necessary so that none
    of the conditions specified in this subsection
    exist before filling or refilling the tank with
    waste.
    ii) For all the inspections required by subsection
    (b)(2)(G), the owner or operator shall notify
    the Agency in writing at least 30 days prior to
    the filling or refilling of each tank to afford
    the Agency the opportunity to inspect the tank
    prior to refilling. If the inspection required
    by this subsection is not planned and the owner
    365
    or operator could not have known about the
    inspection 30 days in advance of refilling the
    tank, the owner or operator shall notify the
    Agency at least seven days prior to the
    refilling of the tank. Notification must be
    made by telephone immediately followed by
    written documentation demonstrating why the
    inspection was unplanned. Alternatively, this
    notification, including the written
    documentation, may be made in writing and sent
    by express mail so that it is received by the
    Agency at least seven days prior to the
    refilling.
    c) Owners and operators that elect to install and operate the control
    equipment in subsection (a) above shall include the following
    information in the operating record in accordance with the
    requirements of Section 725.990(a)(1) and (a)(11):
    1) Internal floating roof.
    A) Document ation that describes the control equipment
    design and certifies that the control equipment meets
    the specifications of subsections (a)(1) and (b)(1)
    above.
    B) Records of each inspection performed as required by
    subsections (b)(1)(A) through (b)(1)(D) above. Each
    record must identify the tank on which the inspection
    was performed and must contain the date the tank was
    inspected and the observed condition of each component
    of the control equipment (seals, internal floating
    roof, and fittings).
    C) If any of the conditions described in subsection
    (b)(1)(B) above are detected during the annual visual
    inspection required by subsection (b)(1)(B) above, the
    records must identify the tank, the nature of the
    defects, and the date the tank was emptied or the
    nature of and date the repair was made.
    D) After each inspection required by subsection (b)(1)(C)
    above that finds holes or tears in the seal or seal
    fabric, or defects in the internal floating roof, or
    other control equipment defects listed in subsection
    (b)(1)(B) above, the records must identify the tank
    and the reason it did not meet the specifications of
    subsection (a)(1) or (b)(1)(C) above and describe each
    repair made.
    2) External floating roof.
    A) Documentation that describes the control equipment
    design and certifies that the control equipment meets
    the specifications of subsections (a)(2) and (b)(2)(B)
    through (b)(2)(D) above.
    B) Records of each gap measurement performed as required
    by subsection (b)(2) above. Each record must identify
    the tank in which the measurement was performed, the
    date of measurement, the raw data obtained in the
    366
    measurement, and the calculations described in
    subsections (b)(2)(B) and (b)(2)(C) above.
    C) Records for each seal gap measurement that detects
    gaps exceeding the limitations specified by subsection
    (b)(2)(D) above that identifies the tank, the date the
    tank was emptied or the repairs made, and the nature
    of the repair.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 725.Appendix F
    Compounds With Henry's Law Constant Less Than 0.1 Y/X
    (At 25 degrees Celsius)
    Compound name
    CAS No.
    Acetaldol
    107-89-1
    Acetamide
    60-35-5
    1-Acetyl -2-thiourea
    591-08-2
    3-Acetyl -5-hydroxypiperidine
    2-Acetylaminofluorene
    53-96-3
    3-Acetylpiperidine
    618-42-8
    Acrylamide
    79-06-1
    Acrylic acid
    79-10-7
    Adenine
    73-24-5
    Adipic acid
    124-04-9
    Adiponitrile
    111-69-3
    Alachlor
    15972-60
    Aldicarb
    116-06-3
    Ametryn
    4-Aminobiphenyl
    92-67-1
    4-Aminopyridine
    504-24-5
    Aniline
    62-53-3
    o-Anisidine
    90-04-0
    Anthraquinone
    84-65-1
    Atrazine
    1912-24-9
    Benzenearsonic acid
    98-05-5
    Benzenesulfonic acid
    98-11-3
    Benzidine
    92-87-5
    Benzo(a)anthracene
    56-55-3
    Benzo(a)pyrene
    50-32-8
    Benzo(ghi)perylene
    191-24-2
    Benzo(k)fluoranthene
    207-08-9
    Benzoic acid
    65-85-0
    Benzyl alcohol
    100-51-6
    gamma-BHC
    58-89-9
    bis(2-Ethylhexyl)phthalate
    117-81-7
    Bromochloromethyl acetate
    Bromoxynil
    Butyric acid
    107-92-6
    Caprolactam (hexahydro-2H-azepin-2-one)
    105-60-2
    Catechol
    120-80-9
    Cell wall
    Cellulose (carboxymethylcellulose)
    9000-11-7
    2-Chloracetophe none
    93-76-5
    3-Chloro -2,5-diketopyrrolidine
    Chloro -1,2-ethane diol
    p-Chloro-m-cresol
    59-50-7
    Chloroacetic acid
    79-11-8
    p-Chloroaniline
    106-47-8
    367
    p-Chlorobenzophenone
    134-85-0
    Chlorobenzylate
    510-15-6
    Chlorhydrin (3-Chloro-1,2-propanediol)
    96-24-2
    4-Chlorophenol
    106-48-9
    Chlorophenol polymers
    1-(o-Chlorophenyl)thiourea
    5344-82-1
    Chrysene
    218-01-9
    Citric acid
    77-92-9
    Creosote
    8001-58-
    Cresol (mixed isomers)
    1319-77-3
    m-Cresol
    108-39-4
    o-Cresol
    95-48-7
    p-Cresol
    106-44-5
    4-Cumylphenol
    27576-86
    Cyanide
    57-12-5
    4-Cyanomethyl benzoate
    Diazinon
    Dibenzo(a,h)anthracene
    53-70-3
    3,5-Dibromo -4-hydroxybenzonitrile
    1689-84-5
    Dibutylphthalate
    84-74-2
    2,6-Dichloro -4-nitroaniline
    99-30-9
    2,5-Dichloroaniline (N,N-dichloroaniline)
    95-82-9
    2,6-Dichlorobenzonitrile
    1194-65-6
    2,5-Dichlorophenol
    3,4-Dichlorotetrahydrofuran
    3511-19
    Dichlorvos
    Diethanolamine
    N,N-Diethylaniline
    91-66-7
    Diethyl phosphorothioate
    126-75-0
    N,N-Diethylpropionamide
    15299-99
    Diethylene glycol
    111-46-6
    Diethylene glycol dimethyl ether (dimethyl Carbitol)
    Diethylene glycol monobutyl ether (butyl Carbitol)
    112-34-5
    Diethylene glycol monoethyl ether acetate (Carbitol acetate)
    112-15-2
    Diethylene glycol monoethyl ether (Carbitol Cellosolve)
    111-90-0
    Diethylene glycol monomethyl ether (methyl Carbitol)
    111-77-3
    N,N-Diethylhydrazine
    Diethylthiophosphate benzo-m-ethyl-p-ether
    Dimethoate
    60-51-5
    2,3-Dimethoxystrychnidin
    -10-one
    357-57-3
    Dimethylcarbamoyl chloride
    Dimethyl disulfide
    624-92-0
    Dimethylformamide
    68-12-2
    Dimethylphthalate
    131-11-3
    4-Dimethylaminoazobenzene
    60-11-7
    7,12-Dimethylbenz(a)anthracene
    57-97-6
    3,3-Dimethylbenzidine
    119-93-7
    1,1-Dimethylhydrazine
    57-14-7
    Dimethylsulfone
    Dimethylsulfoxide
    67-68-5
    4,6-Dinitro -o-cresol
    534-52-1
    1,2-Diphenylhydrazine
    122-66-7
    Dipropylene glycol (1,1'-oxydi-2-propanol)
    110-98-5
    Endrin
    72-20-8
    Epinephrine
    51-43-4
    mono-Ethanolamine
    141-43-5
    Ethyl carbamate (urethane)
    5-17-96
    Ethyl morpholine (ethyl diethylene oxime)
    Ethylene glycol
    107-21-1
    Ethylene glycol monobutyl ether (butyl Cellosolve)
    111-76-2
    368
    Ethylene glycol monoethyl ether (Cellosolve)
    110-80-5
    Ethylene glycol monoethyl ether acetate (Cellosolve acetate)
    111-15-9
    Ethylene glycol monomethyl ether (methyl Cellosolve)
    109-86-4
    Ethylene glycol monophenyl ether (phenyl Cellosolve)
    122-99-6
    Ethylene glycol monopropyl ether (propyl Cellosolve)
    2807-30-9
    Ethylene thiourea (2-imidazolidinethione)
    9-64-57
    3-Ethylphenol
    620-17-7
    Fluoroacetic acid, sodium salt
    62-74-8
    Formaldehyde
    50-00-0
    Formamide
    7-51-27
    Formic acid
    64-18-6
    Fumaric acid
    110-17-8
    Glutaric acid
    110-94-1
    Glycerin (Glycerol)
    56-81-5
    Glycinamide
    598-41-4
    Glyphosate
    Guthion
    Gylcidol
    556-52-5
    Hexamethylene-1,6-diisocyanate (1,6-diisocyanatohexane)
    822-06-0
    Hexamethyl phosphoramide
    680-31-9
    Hexanoic acid
    142-62-1
    Hydrazine
    302-01-2
    Hydrocyanic acid
    74-90-8
    Hydroquinone
    123-31-9
    Hydroxy -2-propionitrile
    109-78-4
    Indeno(1,2,3 -cd)pyrene
    193-39-5
    Lead acetate
    301-04-2
    Lead subacetate (lead acetate, monobasic)
    1335-32-6
    Leucine
    61-90-5
    Malathion
    121-75-5
    Maleic acid
    110-16-7
    Maleic anhydride
    108-31-6
    Mesityl oxide
    141-79-7
    Methane sulfonic acid
    75-75-2
    Methomyl
    16752-77
    p-Methoxyphenol
    150-76-5
    1-Methyl -2-methoxyaziridine
    Methylacrylate
    96-33-3
    4,4'-Methylene -bis-(2 -chloroaniline)
    101-14-4
    Methylene diphenyl diisocyanate (diphenyl methane diisocyanate)
    101-68-8
    4,4-Methylenedianiline
    101-77-9
    Methylene diphenylamine (MDA)
    5-Methylfurfural
    620-02-0
    Methylhydrazine
    60-34-4
    Methyliminoacetic acid
    Methylparathion
    298-00-0
    Methyl sulfuric acid
    77-78-1
    4-Methylthiophenol
    106-45-6
    Monomethyl formamide (n-methylformamide)
    123-39-7
    Nabam
    alpha-Naphthol
    90-15-3
    beta-Naphthol
    135-19-3
    alpha-Naphthylamine
    134-32-7
    beta-Naphthylamine
    91-59-8
    Neopentyl glycol
    126-30-7
    Niacinamide
    98-92-0
    o-Nitroaniline
    88-74-4
    Nitroglycerin
    55-63-0
    2-Nitrophenol
    88-75-5
    369
    4-Nitrophenol
    100-02-7
    N-Nitroso -n-methylurea
    684-93-5
    N-Nitrosodimethylamine
    62-75-9
    Nitrosoguanidine
    674-81-7
    N-Nitrosomorpholine (4-nitrosomorpholine)
    59-89-2
    Oxalic acid
    144-62-7
    Parathion
    56-38-2
    Pentaerythritol
    115-77-5
    Phenacetin
    62-44-2
    Phenol
    108-95-2
    Phenyl mercuric acetate
    62-38-4
    Phenylacetic acid
    103-82-2
    m-Phenylene diamine
    108-45-2
    o-Phenylene diamine
    95-54-5
    p-Phenylene diamine
    106-50-3
    Phorate
    298-02-2
    Phthalic anhydride
    85-44-9
    alpha-Picoline (2-methyl pyridine)
    109-06-8
    1,3-Propane sulfone
    1120-71-4
    beta-Propiolactone
    57-57-8
    Proporur (Baygon)
    Propylene glycol
    57-55-6
    Pyrene
    129-00-0
    Pyridinium bromide
    Quinoline
    91-22-5
    Quinone (p-benzoquinone)
    106-51-4
    Resorcinol
    108-46-3
    Simazine
    122-34-9
    Sodium acetate
    127-09-3
    Sodium formate
    141-53-7
    Strychnine
    57-24-9
    Succinic acid
    110-15-6
    Succinimide
    123-56-8
    Sulfanilic acid
    121-47-1
    Terephthalic acid
    100-21-0
    Tetraethyldithiopyrophosphate
    3689-24-5
    Tetraethylenepentamine
    112-57-2
    Thiofanox
    39196-18
    Thiosemicarbazide
    79-19-6
    2,4-Toluene diamine
    95-80-7
    2,4-Toluene diisocyanate
    584-84-9
    2,6-Toluenediamine
    823-40-5
    3,4-Toluenediamine
    496-72-0
    p-Toluic acid
    99-94-5
    m-Toluidine
    108-44-1
    1,1,2-Trichloro-1,2,2-trifluoroethane
    76-13-1
    Triethanolamine
    102-71-6
    Triethylene glycol dimethyl ether
    Tripropylene glycol
    24800-44-0
    Warfarin
    81-81-2
    3,4-Xylenol (3,4-dimethylphenol)
    95-65-8
    (Source: Added at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 726
    370
    STANDARDS FOR THE MANAGEMENT OF SPECIFIC HAZARDOUS WASTE
    AND SPECIFIC TYPES OF HAZARDOUS WASTE MANAGEMENT FACILITIES
    SUBPART C: RECYCLABLE MATERIALS USED IN A MANNER
    CONSTITUTING DISPOSAL
    Section
    726.120
    Applicability
    726.121
    Standards applicable to generators and transporters of materials
    used in a manner that constitutes disposal
    726.122
    Standards applicable to storers, who are not the ultimate users,
    of materials that are to be used in a manner that constitutes
    disposal
    726.123
    Standards Applicable to Users of Materials that are Used in a
    Manner that Constitutes Disposal
    SUBPART D: HAZARDOUS WASTE BURNED FOR ENERGY RECOVERY
    Section
    726.130
    Applicability (Repealed)
    726.131
    Prohibitions (Repealed)
    726.132
    Standards applicab
    le to generators of hazardous waste fuel
    (Repealed)
    726.133
    Standards applicable to transporters of hazardous waste fuel
    (Repealed)
    726.134
    Standards applicable to marketers of hazardous waste fuel
    (Repealed)
    726.135
    Standards applicable to burners of hazardous waste fuel (Repealed)
    726.136
    Conditional exemption for spent materials and by-products
    exhibiting a characteristic of hazardous waste (Repealed)
    SUBPART E: USED OIL BURNED FOR ENERGY RECOVERY (Repealed)
    Section
    726.140
    Applicability (Repealed)
    726.141
    Prohibitions (Repealed)
    726.142
    Standards applicable to generators of used oil burned for energy
    recovery (Repealed)
    726.143
    Standards applicable to marketers of used oil burned for energy
    recovery (Repealed)
    726.144
    Standards applicable to burners of used oil burned for energy
    recovery (Repealed)
    SUBPART F: RECYCLABLE MATERIALS UTILIZED FOR PRECIOUS METAL
    RECOVERY
    Section
    726.170
    Applicability and requirements
    SUBPART G: SPENT LEAD-ACID BATTERIES BEING RECLAIMED
    Section
    726.180
    Applicabi lity and requirements
    SUBPART H: HAZARDOUS WASTE BURNED IN BOILERS
    AND INDUSTRIAL FURNACES
    Section
    726.200
    Applicability
    726.201
    Management prior to Burning
    726.202
    Permit standards for Burners
    726.203
    Interim Status Standards for Burners
    726.204
    Standards to Control Organic Emissions
    726.205
    Standards to control PM
    726.206
    Standards to Control Metals Emissions
    726.207
    Standards to control HCl and Chlorine Gas Emissions
    726.208
    Small quantity On-site Burner Exemption
    371
    726.209
    Low risk waste Exemption
    726.210
    Waiver of DRE trial burn for Boilers
    726.211
    Standards for direct Transfer
    726.212
    Regulation of Residues
    726.219
    Extensions of Time
    726.Appendix A
    Tier I and Tier II Feed Rate and Emissions Screening Limits
    for Metals
    726.Appendix B
    Tier I Feed Rate Screening Limits for Total Chlorine
    726.Appendix C
    Tier II Emission Rate Screening Limits for Free Chlorine and
    Hydrogen Chloride
    726.Appendix D
    Reference Air Concentrations
    726.Appendix E
    Risk Specific Doses
    726.Appendix F
    Stack Plume Rise
    726.Appendix G
    Health-Based Limits for Exclusion of Waste-Derived Residues
    726.Appendix H
    Potential PICs for Determination of Exclusion of Waste-
    Derived Residues
    726.Appendix I
    Methods Manual for Compliance with BIF Regulations
    726.Appendix J
    Guideline on Air Quality Models
    726.Appendix K
    Lead-Bearing Materials That May be Processed in Exempt Lead
    Smelters
    726.Appendix L
    Nickel or Chromium-Bearing Materials that may be Processed
    in Exempt Nickel-Chromium Recovery Furnaces
    726.Appendix M
    Mercury-Bearing Wastes That May Be
    Processed in Exempt
    Mercury Recovery Units
    726.Table A
    Exempt Quantities for Small Quantity Burner Exemption
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R85-22 at 10 Ill. Reg. 1162, effective January 2, 1986;
    amended in R86-1 at 10 Ill. Reg. 14156, effective August 12, 1986; amended in
    R87-26 at 12 Ill. Reg. 2900, effective January 15, 1988; amended in R89-1 at
    13 Ill. Reg. 18606, effective November 13, 1989; amended in R90-2 at 14 Ill.
    Reg. 14533, effective August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9727,
    effective June 17, 1991; amended in R91-13 at 16 Ill. Reg. 9858, effective
    June 9, 1992; amended in R92-10 at 17 Ill. Reg. 5865, effective March 26,
    1993; amended in R93-4 at 17 Ill. Reg. 20904, effective November 22, 1993;
    amended in R94-7 at 18 Ill. Reg. 12500, effective July 29, 1994; amended in
    R95-6 at 19 Ill. Reg. 10006, effective June 27, 1995; amended in R95-20 at 20
    Ill. Reg. 11263, August 1, 1996
    ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
    ________, effective ____________________
    .
    SUBPART F: RECYCLABLE MATERIALS UTILIZED FOR PRECIOUS METAL
    RECOVERY
    Section 726.170
    Applicability and requirements
    a)
    The regulations of this subpart apply to recyclable materials that
    are reclaimed to recover economically significant amounts of gold,
    silver, platinum, paladium, irradium, osmium, rhodium, ruthenium,
    or any combination of these.
    b)
    Persons whothat generate, transport or store recyclable materials
    that are regulated under this Subpart are subject to the following
    requirements:
    1)
    Notification requirements under Section 3010 of the Resource
    Conservation and Recovery Act;
    372
    2)
    35 Ill. Adm. Code 722.Subpart B (for generators), 35 Ill.
    Adm. Code 723.120 and 121 (for transporters), and 35 Ill.
    Adm. Code 725.171 and 725.172 (for persons
    whothat store) .;
    and
    3)
    For precious metals exported to or imported from designated
    OECD member countries for recovery, 35 Ill. Adm. Code
    722.Subpart H and 725.112(a)(2). For precious metals
    exported to or imported from non-OECD countries for
    recovery, 35 Ill. Adm. Code 722.Subparts E and F.
    c)
    Persons whothat store recycled materials that are regulated under
    this Subpart shall keep the following records to document that
    they are not accumulating these materials speculatively (as
    defined in 35 Ill. Adm. Code 721.101(c);
    1)
    Records showing the volume of these materials stored at the
    beginning of the calendar year;
    2)
    The amount of these mater
    ials generated or received during
    the calendar year; and
    3)
    The amount of materials remaining at the end of the calendar
    year.
    d)
    Recyclable materials that are regulated under this Subpart that
    are accumulated speculatively (as defined in 35 Ill. Adm. Code
    721.101(c)) are subject to all applicable provisions of 35 Ill.
    Adm. Code 722 through 725, and 35 Ill. Adm. Code 702, 703 and 705.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 728
    LAND DISPOSAL RESTRICTIONS
    SUBPART A: GENERAL
    Section
    728.101
    Purpose, Scope and Applicability
    728.102
    Definitions
    728.103
    Dilution Prohibited as a Substitute for Treatment
    728.104
    Treatment Surface Impoundment Exemption
    728.105
    Procedures for case-by-case Extensions to an Effective Date
    728.106
    Petitions to Allow Land Disposal of a Waste Prohibited under
    Subpart C
    728.107
    Waste Analysis and Recordkeeping
    728.108
    Landfill and Surface Impoundment Disposal Restrictions (Repealed)
    728.109
    Special Rules for Characteristic Wastes
    SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION
    AND ESTABLISHMENT OF TREATMENT STANDARDS
    Section
    728.110
    First Third (Repealed)
    728.111
    Second Third (Repealed)
    728.112
    Third Third (Repealed)
    728.113
    Newly Listed Wastes
    373
    728.114
    Surface Impoundment exemptions
    SUBPART C: PROHIBITION ON LAND DISPOSAL
    Section
    728.130
    Waste Specific Prohibitions -- Solvent
    Wastes
    728.131
    Waste Specific Prohibitions -- Dioxin-Containing Wastes
    728.132
    Waste Specific Prohibitions -- California List Wastes
    728.133
    Waste Specific Prohibitions: First Third Wastes
    728.134
    Waste Specific Prohibitions -- Second Third Wastes
    728.135
    Waste Specific Prohibitions -- Third Third Wastes
    728.136
    Waste Specific Prohibitions -- Newly Listed Wastes
    728.137
    Waste Specific Prohibitions -- Ignitable and Corrosive
    Characteristic Wastes Whose Treatment Standards Were Vacated
    728.138
    Waste-Specifi c Prohibitions: Newly-Identified Organic Toxicity
    Characteristic Wastes and Newly-Listed Coke By-Product and
    Chlorotoluene Production Wastes
    728.139 Statutory Prohibitions
    Waste-Specific Prohibitions: End-of-pipe
    CWA, CWA-Equivalent, and Class I Nonhazardous Waste Injection Well
    Treatment Standards; Spent Aluminum Potliners; and Carbamate
    Wastes
    SUBPART D: TREATMENT STANDARDS
    Section
    728.140
    Applicability of Treatment Standards
    728.141
    Treatment Standards Expressed as Concentrations in Waste Extract
    728.142
    Treatment Standards Expressed as Specified Technologies
    728.143
    Treatment Standards Expressed as Waste Concentrations
    728.144
    Adjustment of Treatment Standard
    728.145
    Treatment Standards for Hazardous Debris
    728.146
    Alternative Treatment Standards Based on HTMR
    728.148
    Universal Treatment Standards
    SUBPART E: PROHIBITIONS ON STORAGE
    Section
    728.150
    Prohibitions on Storage of Restricted Wastes
    728.Appendix A
    Toxicity Characteristic Leaching Procedure (TCLP)
    728.Appendix B
    Treatment Standards (As con
    centrations in the Treatment
    Residual Extract)
    728.Appendix C
    List of Halogenated Organic Compounds
    728.Appendix D
    Wastes Excluded from Lab Packs
    728.Appendix E
    Organic Lab Packs (Repealed)
    728.Appendix F
    Technologies to Achieve Deactivation of Characteristics
    728.Appendix G
    Federal Effective Dates
    728.Appendix H
    National Capacity LDR Variances for UIC Wastes
    728.Appendix I
    EP Toxicity Test Method and Structural Integrity Test
    728.Appendix J
    Recordkeeping, Notification, and Certification Requirements
    728.Appendix K
    Metal Bearing Wastes Prohibited From Dilution in a
    Combustion Unit According to Section 728.103(c)
    728.Table A
    Constituent Concentrations in Waste Extract (CCWE)
    728.Table B
    Constituent Concentrations in Wastes (CCW)
    728.Table C
    Technology Codes and Description of Technology-Based
    Standards
    728.Table D
    Technology-Based Standards by RCRA Waste Code
    728.Table E
    Standards for Radioactive Mixed Waste
    728.Table F
    Alternative Treatment Standards for Hazardous Debris
    728.Table G
    Alternative Treatm
    ent Standards Based on HMTR
    728.Table H
    Wastes Excluded from CCW Treatment Standards
    728.Table T
    Treatment Standards for Hazardous Wastes
    728.Table U
    Universal Treatment Standards (UTS)
    374
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R87-5 at 11 Ill. Reg. 19354, effective November 12, 1987;
    amended in R87-39 at 12 Ill. Reg. 13046, effective July 29, 1988; amended in
    R89-1 at 13 Ill. Reg. 18403, effective November 13, 1989; amended in R89-9 at
    14 Ill. Reg. 6232, effective April 16, 1990; amended in R90-2 at 14 Ill. Reg.
    14470, effective August 22, 1990; amended in R90-10 at 14 Ill. Reg. 16508,
    effective September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9462,
    effective June 17, 1991; amendment withdrawn at 15 Ill. Reg. 14716, October
    11, 1991; amended in R91-13 at 16 Ill. Reg. 9619, effective June 9, 1992;
    amended in R92-10 at 17 Ill. Reg. 5727, effective March 26, 1993; amended in
    R93-4 at 17 Ill. Reg. 20692, effective November 22, 1993; amended in R93-16 at
    18 Ill. Reg. 6799, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
    12203, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17563,
    effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9660, effective
    June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11100, August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    SUBPART A: GENERAL
    Section 728.101
    Purpose, Scope and Appli
    cability
    a)
    This Part identifies hazardous wastes that are restricted from
    land disposal and defines those limited circumstances under which
    an otherwise prohibited waste may continue to be land disposed.
    b)
    Except as specifically provided otherwise in this Part or 35 Ill.
    Adm. Code 721, the requirements of this Part apply to persons that
    generate or transport hazardous waste and to owners and operators
    of hazardous waste treatment, storage, and disposal facilities.
    c)
    Restricted wastes may continue t
    o be land disposed as follows:
    1)
    Where persons have been granted an extension to the
    effective date of a prohibition under Subpart C or pursuant
    to Section 728.105, with respect to those wastes covered by
    the extension;
    2)
    Where persons have been granted an exemption from a
    prohibition pursuant to a petition under Section 728.106,
    with respect to those wastes and units covered by the
    petition;
    3) WA wastes that areis hazardous only because
    theyit exhibit s
    a hazardous characteristic of hazardous waste
    and that areis
    otherwise prohibited
    from land disposal
    under this Part
    areis not prohibited from land disposal
    if the waste s:
    A)
    Are disposed into a nonhazardous or hazardous waste
    injection well, as defined in 35 Ill. Adm. Code
    704.106(a); and
    B)
    Do not exhibit any prohibited characteristic of
    hazardous waste identified in 35 Ill. Adm. Code
    721.Subpart C at the point of injection; and
    C) If, at the point of generation, the injected wastes
    375
    include D001 High TOC subcategory wastes or D012-D017
    pesticide wastes that are prohibited under Section
    728.117(c), those wastes have been treated to meet the
    treatment standards of Section 728.140 prior to
    injection.
    4)
    A waste that is hazardous only because it exhibits a
    characteristic of hazardous waste and which is otherwise
    prohibited under this Part is not prohibited if the waste
    meets any of the following criteria, unless the waste is
    subject to a specified method of treatment other than DEACT
    in Section 728.140 or is D003 reactive cyanide:
    A)
    The waste is managed in a treatment system which
    subsequently discharges to waters of the U.S. pursuant
    to a permit issued under 35 Ill. Adm. Code 309; or
    B)
    The waste is treated for purposes of the pretreatment
    requirements of 35 Ill. Adm. Code 307 and 310; or
    C)
    The waste is managed in a zero discharge system
    engaged in Clean Water Act-equivalent treatment, as
    defined in Section 728.137(a); and
    D)
    The waste no longer exhibits a prohibited
    characteristic of hazardous waste at the point of land
    disposal (i.e., placement in a surface impoundment).
    d)
    This Part does not affect the availability of a waiver under
    Section 121(d)(4) of the Comprehensive Environmental Response,
    Compensation, and Liability Act of 1980 (CERCLA) (42 U.S.C.
    ยงยง 9601 et seq.).
    e)
    The following hazardous wastes are not subject to any provision of
    this Part:
    1)
    Wastes generated by small quantity generators of less than
    100 kg of non-acute hazardous waste or less than 1 kg of
    acute hazardous waste per month, as defined in 35 Ill. Adm.
    Code 721.105;
    2)
    Waste pesticides that a farmer disposes of pursuant to 35
    Ill. Adm. Code 722.170;
    3)
    Wastes identified or listed as hazardous after November 8,
    1984, for which USEPA has not promulgated land disposal
    prohibitions or treatment standards;
    or
    4)
    De minimis losses
    of waste that exhibits a characteristic of
    hazardous waste to wastewater s treatment systems of
    commercial chemical product or chemical intermediates that
    are ignitable (D001) or corrosive (D002) or that are organic
    constituents that exhibit the characteristic of toxicity
    (D012-D043) and that contain underlying hazardous
    constituents, as defined in Section 728.102 of this Part,
    are not considered to be prohibited waste
    s and are defined
    as follows: . "De minimis" is defined as l
    A)
    Losses from normal material handling operations (e.g.,
    spills from the unloading or transfer of materials
    from bins or other containers or leaks from pipes,
    376
    valves, or other devices used to transfer materials);
    minor leaks of process equipment, storage tanks, or
    containers; leaks from well-maintained pump packings
    and seals; sample purging
    s; relief device discharges;
    discharges from safety showers and rinsing and
    cleaning of personal safety equipment; and rinsate
    from empty containers or from containers that are
    rendered empty by that rinsing;
    and laboratory waste
    that does not exceed one per cent of the total flow of
    wastewater into the facility's headworks on an annual
    basis, or with a combined annualized average
    concentration not exceeding one part per million (ppm)
    in the headworks of the facility's wastewater
    treatment or pretreatment facility; or
    B)
    Decharacterized waste that is injected into Class I
    nonhazardous wells in which the decharacterized
    waste's combined volume is less than one per cent of
    the total flow at the wellhead on an annualized basis
    and no greater than 10,000 gallons per day, and in
    which any underlying hazardous constituents in the
    characteristic waste are present at the point of
    generation at levels less than 10 times the treatment
    standards found at Section 728.148.
    5)
    Land disposal prohibitions for hazardous characteristic
    wastes do not apply to laboratory wastes displaying the
    characteristic of ignitability (D001), corrosivity (D002),
    or organic toxicity (D012 through D043) that are mixed with
    other plant wastewaters at facilities whose ultimate
    discharge is subject to regulation under the CWA (including
    wastewaters at facilities that have eliminated the discharge
    of wastewater), provided that the annualized flow of
    laboratory wastewater into the facility's headwork does not
    exceed one percent or that the laboratory wastes' combined
    annualized average concentration does not exceed one part
    per million in the facility's headworks.
    f)
    A universal waste handler or universal waste transporter (as
    defined in 35 Ill. Adm. Code 720.110) is exempt from Sections
    728.107 and 268.150 for the hazardous wastes listed below. Such a
    handler or transporter is subject to regulation under 35 Ill. Adm.
    Code 733.
    1)
    Batteries, as described in 35 Ill. Adm. Code 733.102;
    2)
    Pesticides, as described in 35 Ill. Adm. Code 733.103; and
    3)
    Thermostats, as described in 35 Ill. Adm. Code 733.104.
    g)
    This Part is cumulative with the land disposal restrictions of 35
    Ill. Adm. Code 729. The Environmental Protection Agency (Agency)
    shall not issue a wastestream authorization pursuant to 35 Ill.
    Adm. Code 709 or Sections 22.6 or 39(h) of the Environmental
    Protection Act [415 ILCS 5/22.6 or 39(h)] unless the waste meets
    the requirements of this Part as well as 35 Ill. Adm. Code 729.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.102 Definitions
    377
    When used in this Part, the following terms have the meanings given below.
    All other terms have the meanings given under 35 Ill. Adm. Code 702.110,
    720.102, or 721.103.
    "Agency" means the Illinois Environmental Protection Agency.
    "Board" means the Illinois Pollution Control Board.
    "CERCLA" means the Comprehensive Environmental Respons
    e,
    Compensation, and Liability Act of 1980 (42 U.S.C. 9601 et seq.)
    "Debris" means solid material exceeding a 60 mm particle size that
    is intended for disposal and that is: a manufactured object;
    plant or animal matter; or natural geologic material. However,
    the following materials are not debris: any material for which a
    specific treatment standard is provided in 728.Subpart D, namely
    lead acid batteries, cadmium batteries, and radioactive lead
    solids; process residuals, such as smelter slag and residues from
    the treatment of waste, wastewater, sludges, or air emission
    residues; and intact containers of hazardous waste that are not
    ruptured and that retain at least 75% of their original volume. A
    mixture of debris that has not been treated to the standards
    provided by Section 728.145 of this Part and other material is
    subject to regulation as debris if the mixture is comprised
    primarily of debris, by volume, based on visual inspection.
    "End-of-pipe" refers to the point where effluent is discharged to
    the environment.
    "Halogenated organic compounds" or "HOCs" means those compounds
    having a carbon-halogen bond that are listed under Section
    728.Appendix C.
    "Hazardous constituent or constituents" means those constituents
    listed in 35 Ill. Adm. Code 721.Appendix H.
    "Hazardous debris" means debris that contains a hazardous waste
    listed in 35 Ill. Adm. Code 721.Subpart D or that exhibits a
    characteristic of hazardous waste identified in 35 Ill. Adm. Code
    721.Subpart C.
    "Inorganic metal-bearing waste" is one for which USEPA has
    established treatment standards for metal hazardous constituents
    that does not otherwise contain significant organic or cyanide
    content, as described in Section 728.103(b)(1), and which is
    specifically listed in Section 728.Appendix K.
    "Inorganic Ssolid Ddebris" are nonfriable inorganic solids that
    are incapable of passing through a 9.5 mm standard sieve and that
    require cutting or crushing and grinding in mechanical sizing
    equipment prior to stabilization, limited to the following
    inorganic or metal materials:
    Metal slags (either dross or scoria).
    Glassified slag.
    Glass.
    Concrete (excluding cementitious or pozzolanic stabilized
    hazardous wastes).
    378
    Masonry and refractory bricks.
    Metal cans, containers, drums, or tanks.
    Metal nuts, bolts, pipes, pumps, valves, appliances, or
    industrial equipment.
    Scrap metal, as defined in 35 Ill. Adm. Code 721.101(c)(6).
    "Land disposal" means placement in or on the land, except in a
    corrective action management unit, and includes, but is not
    limited to, placement in a landfill, surface impoundment, waste
    pile, injection well, land treatment facility, salt dome
    formation, salt bed formation, underground mine, or cave or
    placement in a concrete vault or bunker intended for disposal
    purposes.
    "Nonwastewaters" are wastes that do not meet the criteria for
    "wastewaters" in this Section.
    "Polychlorinated biphenyls" or "PCBs" are halogenated organic
    compounds defined in accordance with 40 CFR 761.3, incorporated by
    reference in 35 Ill. Adm. Code 720.111.
    "ppm" means parts per million.
    "RCRA corrective action" means corrective action taken under 35
    Ill. Adm. Code 724.200 or 725.193, 40 CFR 264.100 or 265.93
    (199496), or similar regulations in other States with RCRA
    programs authorized by U
    .S. EPA pursuant to 40 CFR 271 (19
    9496).
    "Stormwater impoundments" are surface impoundments that receive
    wet weather flow and which receive process waste only during wet
    weather events.
    "Underlying hazardous constitue
    nt" means any regulated constituent
    listed in Section 728.Table U, "Universal Treatment Standards
    (UTS)", except fluoride, vanadium , and zinc, that can reasonably
    be expected to be present
    , at the point of generation of the
    hazardous waste , at a concentration above the constituent-specific
    UTS treatment standard.
    "U.S. EPA" or "USEPA" means the United States Environmental
    Protection Agency.
    "Wastewaters" are wastes that contain less than 1% by weight total
    organic carbon (TOC) and less than 1% by weight total suspended
    solids (TSS) , with the following exceptions:
    F001, F002, F003, F004, and F005 solvent
    -water mixtures that
    contain less than 1% by weight TOC or less than 1% by weight
    total F001, F002, F003, F004, and F005 solvent constituents
    listed in Table A.
    K011, K013, and K014 wastewaters (as generated) that contain
    less than 5% by weight TOC and less than 1% by weight TSS.
    K103 and K104 wastewaters that contain less than 4% by
    weight TOC and less than 1% by weight TSS
    .
    379
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.103
    Dilution Prohibited as a Substitute for Treatment
    a)
    Except as provided in subsection (b) below, no generator,
    transporter, handler
    , or owner or operator of a treatment,
    storage , or disposal facility shall in any way dilute a restricted
    waste or the residual from treatment of a restricted waste as a
    substitute for adequate treatment to achieve compliance with
    728.Subpart D of this Part , to circumvent the effective date of a
    prohibition in 728.Subpart C of this Part , to otherwise avoid a
    prohibition in 728.Subpart C of this Part , or to circumvent a land
    disposal restriction imposed by RCRA section 3004
    .
    b)
    Dilution of waste
    s that areis hazardous only because
    theyit
    exhibit s a characteristic
    of hazardous waste
    in a treatment system
    whichthat treats wastes subsequently discharged to a water of the
    State pursuant to an NPDES permit issued under 35 Ill. Adm. Code
    309, that treats wastes in a CWA-equivalent treatment system,
    or
    whichthat treats wastes for purposes of pretreatment requirements
    under 35 Ill. Adm. Code 310 is not impermissible dilution for
    purposes of this Section unless a method
    other than DEACT
    has been
    specified in Section 728.140
    as the treatment standard
    in Section
    728.142, or unless the waste is a D003 reactive cyanide wastewater
    or nonwastewater.
    c)
    Combustion of waste designated by any of the USEPA hazardous waste
    codes listed in Section 728.Appendix J is prohibited, unless the
    waste can be demonstrated to comply with one or more of the
    following criteria at the point of generation or after any bona
    fide treatment, such as cyanide destruction prior to combustion,
    (unless otherwise specifically prohibited from combustion):
    1)
    The waste contains hazardous organic constituents or cyanide
    at levels exceeding the constituent-specific treatment
    standard found in Section 728.148;
    2)
    The waste consists of organic, debris-like materials (e.g.,
    wood, paper, plastic, or cloth) contaminated with an
    inorganic metal-bearing hazardous waste;
    3)
    The waste has reasonable heating value, such as greater than
    or equal to 5000 BTU per pound, at the point of generation;
    4)
    The waste is co-generated with wastes for which combustion
    is a required method of treatment;
    5)
    The waste is subject to any federal or state requirements
    necessitating reduction of organics (including biological
    agents); or
    6)
    The waste contains greater than one percent Total Organic
    Carbon (TOC).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.107
    Waste Analysis and Recordkeeping
    a)
    Except as specified in Section 728.132, where a generator's waste
    is listed in 35 Ill. Adm. Code 721.Subpart D or if the waste
    exhibits one or more of the characteristics set out at 35 Ill.
    380
    Adm. Code 721.Subpart C, the generator shall test its waste, or
    test an extract using the Toxicity Characteristic Leaching
    Procedure, Method 1311, in "Test Methods for Evaluating Solid
    Waste, Physical/Chemical Methods", U
    .S. EPA Publication SW-846, as
    incorporated by reference in 35 Ill. Adm. Code 720.111, or use
    knowledge of the waste to determine if the waste is restricted
    from land disposal under this Part. If the generator determines
    that its waste displays the characteristic of ignitability (D001)
    (and is not in the High TOC Ignitable Liquids Subcategory or is
    not treated by CMBST or RORGS of Section 728.Table C
    of this Part )
    or the waste displays the characteristic of corrosivity (D002)
    ,
    reactivity (D003), or organic toxicity (D012 through D043),
    and
    the waste is prohibited under Section
    s 728.137, or the waste
    displays the characteristic of organic toxicity (D012-D043) and is
    prohibited under
    Section 728.138,
    and 728.139, the generator shall
    determine what underlying hazardous constituents (as defined in
    Section 728.102), are reasonably expected to be present in the
    D001, D002, D003, or D012 through D043 waste.
    1)
    If a generator determines that it is managing a restricted
    waste under this Part and the waste does not meet the
    applicable treatment standards set forth in 728.Subpart D or
    exceeds the applicable prohibition levels set forth in
    Section 728.132 or 728.139, the generator shall
    notify
    thesend a one-time written notice to each
    treatment or
    storage facility
    in writing with eachthe initial shipment of
    waste. No further notification is necessary until such time
    that the waste or facility change, in which case a new
    notification must be sent and a copy placed in the
    generator's file.
    The notice must include the following
    information:
    A)
    U.S. EPA hazardous waste number;
    B)
    The waste constituents that the treater will monitor,
    if monitoring will not include all regulated
    constituents, for wastes F001 through F005, F039,
    D001, D002, D003, and D012 through D043
    , and wastes
    prohibited pursuant to Section 728.132 or Section
    3004(d) of the Resource Conservation and Recovery Act,
    referenced in Section 728.139
    . The generator must
    also include whether the waste is a nonwastewater or
    wastewater (as defined in Section 728.102 (d) and (f))
    and indicate the subcategory of the waste (such as
    "D003 reactive cyanide") if applicable;
    C)
    The manifest number associated with the shipment of
    waste;
    D)
    For hazardous debris, the contaminants subject to
    treatment, as provided by Section 728.145(b), and the
    following statement: "This hazardous debris is
    subject to the alternative treatment standards of 35
    Ill. Adm. Code 728.145
    "; and
    E)
    Waste analysis data, where available
    ; and.
    F) The date on which the waste is subject to the
    prohibitions.
    2)
    If a generator determines that it is managing a restricted
    381
    waste under this Part and determines that the waste can be
    land disposed without further treatment, with
    eachthe
    initial shipment of waste the generator shall submit a
    one-
    time written notice and a certification to
    theeach
    treatment, storage, or land disposal facility stating that
    the waste meets the applicable treatment standards set forth
    in 728.Subpart D and setting forth the applicable
    prohibition levels set forth in Section 728.132 or RCRA
    Section 3004(d), referenced in Section 728.139. A generator
    of hazardous debris that is excluded from the definition of
    hazardous waste under 35 Ill. Adm. Code 721.103(e)(2), 35
    Ill. Adm. Code 728.103(f)(2), or 35 Ill. Adm. Code 720.122
    (i.e. debris that is delisted), however, is not subject to
    these notification and certififcation requirements.
    If the
    waste changes, the generator shall send a new notice and
    certification to the receiving facility, and place a copy in
    its files.
    A)
    The notice must include the following information:
    i)
    U.S. EPA hazardous waste number;
    ii)
    The waste constituents that the treater will
    monitor, if monitoring will not include all
    regulated constituents, for wastes F001 through
    F005, F039, D001, D002,
    D003, and D012 through
    D043, and wastes prohibited pursuant to Section
    728.132 or Section 3004(d) of the Resource
    Conservation and Recovery Act, referenced in
    Section 728.139 . The generator must also
    include whether the waste is a nonwastewater or
    wastewater (as defined in Section 728.102 (d)
    and (f)) and indicate the subcategory of the
    waste (such as "D003 reactive cyanide") if
    applicable;
    iii)
    The manifest number associated with the shipment
    of waste; and
    iv)
    Waste analysis data, where available.
    B)
    The certification must be signed by an authorized
    representative and must state the following:
    I certify under penalty of law that I personally have
    examined and am familiar with the waste through
    analysis and testing or through knowledge of the waste
    to support this certification that the waste complies
    with the treatment standards specified in 35 Ill. Adm.
    Code 728.Subpart D and all applicable prohibitions set
    forth in 35 Ill. Adm. Code 728.132, 728.139, or
    Section 3004(d) of the Resource Conservation and
    Recovery Act. I believe that the information I
    submitted is true, accurate, and complete. I am aware
    that there are significant penalties for submitting a
    false certification, including the possibility of a
    fine and imprisonment.
    3)
    If a generat or's waste is subject to an exemption from a
    prohibition on the type of land disposal method utilized for
    the waste (such as, but not limited to, a case-by-case
    382
    extension under Section 728.105, an exemption under Section
    728.106, an extension under Section 728.101(c)(3), or a
    nationwide capacity variance under 40 CFR 268.Subpart C
    (199496)), the generator shall submit a
    one-time written
    notice with eachthe initial shipment of the waste to
    theeach
    facility receiving the generator's waste stating that the
    waste is not prohibited from land disposal.
    If the waste
    changes, the generator shall send a new notice and
    certification to the receiving facility, and place a copy in
    its files. The notice must include the following
    information:
    A)
    U.S. EPA hazardous waste number;
    B)
    The waste constituents that the treater will monitor,
    if monitoring will not include all regulated
    constituents, for wastes F001 through F005, F039,
    D001, D002, D003, and D012 through D043. The
    generator must also include whether the waste is a
    nonwastewater or wastewater (as defined in Section
    728.102 (d) and (f)) and indicate the subcategory of
    the waste (such as "D003 reactive cyanide") if
    applicable;
    C)
    The manifest number associated with the shipment
    of waste;
    D)
    Waste analysis data, where available;
    E)
    For hazardous debris, when using the alternative
    treatment technologies provided by Section 728.145:
    i)
    The contaminants subject to treatment, as
    provided by Section 728.145(b);
    ii)
    An indication that these con
    taminants are being
    treated to comply with Section 728.145;
    F)
    For hazardous debris when using the treatment
    standards for the contaminating waste(s) in Section
    728.140: the requirements described in subsections
    (a)(3)(A) through (a)(3)(D) above and subsection
    (a)(3)(G) below; and,
    G)
    The date on which the waste is subject to the
    prohibitions.
    4)
    If a generator is managing a prohibited waste in tanks,
    containers, or containment buildings regulated under 35 Ill.
    Adm. Code 722.134 and is treating such waste in tanks,
    containers, or containment buildings to meet applicable
    treatment standards under 728.Subpart D, the generator shall
    develop and follow a written waste analysis plan that
    describes the procedures the generator will carry out to
    comply with the treatment standards. (A generator treating
    hazardous debris under the alternative treatment standards
    of Section 728.Table F, however, is not subject to these
    waste analysis requirements.) The plan must be kept on-site
    in the generator's records, and the following requirements
    must be met:
    383
    A)
    The waste analysis plan must be based on a detailed
    chemical and physical analysis of a representative
    sample of the prohibited wastes being treated, and it
    must contain all information necessary to treat the
    wastes in accordance with the requirements of this
    Part, including the selected testing frequency.
    B)
    Such plan must be filed with the Agency a minimum of
    30 days prior to the treatment activity, with delivery
    verified.
    C)
    Wastes shipped off-
    site pursuant to this subsection
    must comply with the notification requirements of
    Section 728.107(a)(2).
    5)
    If a generator determines whether the waste is restricted
    based solely on the generator's knowledge of the waste, the
    generator shall retain all supporting data used to make this
    determination on-site in the generator's files. If a
    generator determines whether the waste is restricted based
    on testing the waste or an extract developed using the test
    method described in Section 728.Appendix A, the generator
    shall retain all waste analysis data on site in its files.
    6)
    If a generator determines, subsequent to the time of
    generation, that it is managing a restricted waste that is
    excluded from the definition of hazardous or solid waste or
    exempt from regulation as a RCRA hazardous waste under 35
    Ill. Adm. Code 721.102 through 721.106, the generator shall
    place, in the facility's file, a one-time notice stating
    such generation, the subsequent exclusion from the
    definition of hazardous or solid waste or exemption from
    regulation as a RCRA hazardous waste, and the disposition of
    the waste.
    7)
    A generator shall retain on-site a copy of all notices,
    certifications, demonstrations, waste analysis data, and
    other documentation produced pursuant to this Section for at
    least five years from the date that the waste that is the
    subject of such documentation was last sent to on-site or
    off-site treatment, storage, or disposal. The five year
    record retention period is automatically extended during the
    course of any unresolved enforcement action regarding the
    regulated activity, or as requested by the Agency. The
    requirements of this subsection apply to solid wastes even
    when the hazardous characteristic is removed prior to
    disposal, when the waste is excluded from the definition of
    hazardous or solid waste under 35 Ill. Adm. Code 721.102
    through 721.106, or when the waste is exempted from
    regulation as a RCRA hazardous waste subsequent to the point
    of generation.
    8)
    If a generator is managing a lab pack that
    contains wastes
    identified in Section 728.Appendix D and wishes to use the
    alternative treatment standard under Section 728.142(c),
    with each shipment of waste the generator shall submit a
    notice to the treatment facility in accordance with
    subsection (a)(1) above, except that underlying hazardous
    constituents need not be determined. The generator shall
    also comply with the requirements in subsections (a)(5) and
    (a)(6) above and shall submit the following certification,
    384
    which must be signed by an authorized representative:
    I certify under penalty of law that I personally have
    examined and am familiar with the waste and that the lab
    pack does not contain any of the wastes identified in 35
    Ill. Adm. Code 728.Appendix D. I am aware that there are
    significant penalties for submitting a false certification,
    including the possibility of fine or imprisonment.
    9)
    This subsection corresponds with 40 CFR 268.7(a)(9), marked
    "reserved" by U .S. EPA at 59 Fed. Reg. 48045 (Sept. 19,
    1994). This statement maintains structural consistency with
    federal regulations.
    10)
    Small quantity generators with tolling agreements pursuant
    to 35 Ill. Adm. Code 722.120(e) shall comply with the
    applicable notification and certification requirements of
    subsection (a) above for the initial shipment of the waste
    subject to the agreement. Such generators shall retain on-
    site a copy of the notification and certification, together
    with the tolling agreement, for at least three years after
    termination or expiration of the agreement. The three-year
    record retention period is automatically extended following
    notification pursuant to Section 31(d) of the Environmental
    Protection Act until either any subsequent enforcement
    action is resolved or until the Agency notifies the
    generator documents need not be retained.
    b)
    Treatment facilities shall test their wastes according to the
    frequency specified in their waste analysis plans, as required by
    35 Ill. Adm. Code 724.113 or 725.113. Such testing must be
    performed as provided in subsections (b)(1), (b)(2), and (b)(3)
    below.
    1)
    For wastes with treatment standards expressed as
    concentrations in the waste extract (Section 728.141), the
    owner or operator of the treatment facility shall test the
    treatment residues or an extract of such residues developed
    using the test method described in Section 728.Appendix A to
    assure that the treatment residues or extract meet the
    applicable treatment standards.
    2)
    For wastes prohibited under Section 728.132 or 728.139 that
    are not subject to any treatment standards under 728.Subpart
    D, the owner or operator of the treatment facility shall
    test the treatment residues according to the generator
    testing requirements specified in Section 728.132 to assure
    that the treatment residues comply with the applicable
    prohibitions.
    3)
    For wastes with treatment standards expressed as
    concentrations in the waste (Section 728.143), the owner or
    operator of the treatment facility shall test the treatment
    residues (not an extract of such residues) to assure that
    the treatment residues meet the applicable treatment
    standards.
    4)
    A notice must be sent with
    eachthe initial waste shipment to
    theeach land disposal facility that includes the following
    information, except that debris excluded from the definition
    of the hazardous waste under 35 Ill. Adm. Code 721.103(e)
    385
    (i.e., debris treated by an extraction or destruction
    technology provided by Section 728.Table F, and debris that
    is delisted) is subject to the notififcation and
    certification requirments of subsection (d) below rather
    than these notification requirments
    :. No further
    notification is necessary until such time that the waste or
    receiving facility change, in which case a new notice must
    be sent and a copy placed in the treatment facility's file.
    A)
    U.S. EPA hazardous waste number;
    B)
    The waste constituents that the treater will monitor,
    if monitoring will not include all regulated
    constituents, for wastes F001 through F005, F039,
    D001, D002, D003, and D012 through D043
    , and wastes
    prohibited pursuant to Section 728.132 or Section
    3004(d) of the Resource Conservation and Recovery Act,
    referenced in Section 728.139
    . The generator must
    also include whether the waste is a nonwastewater or
    wastewater (as defined in Section 728.102 (d) and (f))
    and indicate the subcategory of the waste (such as
    "D003 reactive cyanide
    ") if applicable;
    C)
    The manifest number associated with the shipment of
    waste; and
    D)
    Waste analysis data, where available.
    5)
    The treatment facility owner or operator shall submit a
    certification with each shipment of waste or treatment
    residue of a restricted waste to the land disposal facility
    stating that the waste or treatment residue has been treated
    in compliance with the treatment standards specified in
    728.Subpart D and the applicable prohibitions set forth in
    Section 728.132 or 728.139. Debris excluded from the
    definiton of hazardous waste under 35 Ill. Adm. Code
    721.103(e) (i.e., debris treated by an extraction or
    destruction technology provided by Section 728.Table F, and
    debris that is delisted), however, is subject to the
    notififcation and certication requirements of subsection (d)
    below rather than the certification requirements of this
    subsection.
    A)
    For wastes with treatment standards expressed as
    concentrations in the waste extract or in the waste
    (Sections 728.141 or 728.143), or for wastes
    prohibited under Section 728.132 or 728.139 that are
    not subject to any treatment standards under
    728.Subpart D, the certification must be signed by an
    authorized representative and must state the
    following:
    I certify under penalty of law that I have
    personally examined and am familiar with the
    treatment technology and operation of the
    treatment process used to support this
    certification and that, based on my inquiry of
    those individuals immediately responsible for
    obtaining this information, I believe that the
    treatment process has been operated and
    maintained properly, so as to comply with the
    386
    performance levels specified in 35 Ill. Adm.
    Code 728.Subpart D and all applicable
    prohibitions set forth in 35 Ill. Adm. Code
    728.132 or 728.139 or Section 3004(d) of the
    Resource Conservation and Recovery Act without
    impermissible dilution of the prohibited waste.
    I am aware that there are significant penalties
    for submitting a false certification, including
    the possibility of fine and imprisonment.
    B)
    For wastes with treatment standards expressed as
    technologies (Section 728.142), the certification must
    be signed by an authorized representative and must
    state the following:
    I certify under penalty of law that the waste
    has been treated in accordance with the
    requirements of 35 Ill. Adm. Code 728.142. I am
    aware that there are significant penalties for
    submitting a false certification, including the
    possibility of fine and imprisonment.
    C)
    For wastes with treatment standards expressed as
    concentrations in the waste pursuant to Section
    728.143, if compliance with the treatment standards in
    728.Subpart D is based in part or in whole on the
    analytical detection limit alternative specified in
    Section 728.143(c), the certification also must state
    the following:
    I certify under penalty of law that I have
    personally examined and am familiar with the
    treatment technology and operation of the
    treatment process used to support this
    certification and that, based on my inquiry of
    those individuals immediately responsible for
    obtaining this information, I believe that the
    nonwastewater organic constituents have been
    treated by incineration in units operated in
    accordance with 35 Ill. Adm. Code 724.Subpart O
    or 35 Ill. Adm. Code 725.Subpart O, or by
    combustion in fuel substitution units operating
    in accordance with applicable technical
    requirements, and I have been unable to detect
    the nonwastewater organic constituents despite
    having used best good faith efforts to analyze
    for such constituents. I am aware that there
    are significant penalties for submitting a false
    certification, including the possibility of fine
    and imprisonment.
    D)
    For characteristic wastes D001, D002,
    D003, and D012
    through D043 that are subject to the treatment
    standards in Section 728.140 (other than those
    expressed as a required method of treatment), that are
    reasonably expected to contain underlying hazardous
    constituents (as defined in Section 728.102(i)
    ), that
    are treated on-site to remove the hazardous
    characteristic, and that are then sent off-site for
    treatment of underlying hazardous constituents, the
    certification must state the following:
    387
    I certify under penalty of law that the waste
    has been treated in accordance with the
    requirements of 35 Ill. Adm. Code 728.140 to
    remove the hazardous characteristic. This
    decharacterized waste contains underlying
    hazardous constituents that require further
    treatment to meet universal treatment standards.
    I am aware that there are significant penalties
    for submitting a false certification, including
    the possibility of fine and imprisonment.
    E)
    For characteristic wastes D001, D002, D003, and D012
    through D043 that contain underlying hazardous
    constituents, as defined in Section 728.102(i), and
    which are treated on-site to remove the hazardous
    characteristic and to treat underlying hazardous
    constituents to levels set forth in the Sections
    728.148 and 728.Table U Universal Treatment Standards,
    the certification must state the following:
    I certify under penalty of law that the waste
    has been treated in accordance with the
    requirements of 35 Ill. Adm. Code 728.140 to
    remove the hazardous characteristic, and that
    underlying hazardous constituents, as defined in
    Section 728.102, have been treated on-site to
    meet the Sections 728.148 and 728.Table U
    Universal Treatment Standards. I am aware that
    there are significant penalties for submitting a
    false certification, including the possibility
    of fine and imprisonment.
    6)
    If the waste or treatment residue will be further managed at
    a different treatment or storage facility, the treatment,
    storage, or disposal facility sending the waste or treatment
    residue off-site must comply with the notice and
    certification requirements applicable to generators under
    this Section.
    7)
    Where the wastes are recyclable materials used in a manner
    constituting disposal subject to the provisions of 35 Ill.
    Adm. Code 726.120(b), regarding treatment standards and
    prohibition levels, the owner or operator of a treatment
    facility (i.e. the recycler) is not required to notify the
    receiving facility pursuant to subsection (b)(4) above.
    With each shipment of such wastes the owner or operator of
    the recycling facility shall submit a certification
    described in subsection (b)(5) above and a notice that
    includes the information listed in subsection (b)(4) above
    (except the manifest number) to the Agency. The recycling
    facility also shall keep records of the name and location of
    each entity receiving the hazardous waste-derived product.
    c)
    Except where the owner or operator is disposing of any waste that
    is a recyclable material used in a manner constituting disposal
    pursuant to 35 Ill. Adm. Code 726.120(b), the owner or operator of
    any land disposal facility disposing any waste subject to
    restrictions under this Part shall:
    1)
    Have copies of the notice and certification specified in
    388
    subsection (a) or (b) above and the certification specified
    in Section 728.108, if applicable.
    2)
    Test the waste, or an extract of the waste or treatment
    residue developed using the test method described in Section
    728.Appendix A or using any methods required by generators
    under Section 728.132, to assure that the waste or treatment
    residue is in compliance with the applicable treatment
    standards set forth in 728.Subpart D and all applicable
    prohibitions set forth in Sections 728.132 or 728.139. Such
    testing must be performed according to the frequency
    specified in the facility's waste analysis plan as required
    by 35 Ill. Adm. Code 724.113 or 725.113.
    3)
    Where the owner or operator is disposing of any waste that
    is subject to the prohibitions under Section 728.133(f) but
    not subject to the prohibitions set forth in Section
    728.132, the owner or operator shall ensure that such waste
    is the subject of a certification according to the
    requirements of Section 728.108 prior to disposal in a
    landfill or surface impoundment unit, and that such disposal
    is in accordance with the requirements of Section
    728.105(h)(2). The same requirement applies to any waste
    that is subject to the prohibitions under Section 728.133(f)
    and also is subject to the statutory prohibitions in the
    codified prohibitions in Section 728.139 or Section 728.132.
    4)
    Where the owner or oper
    ator is disposing of any waste that
    is a recyclable material used in a manner constituting
    disposal subject to the provisions of 35 Ill. Adm. Code
    726.120(b), the owner or operator is not subject to
    subsections (c)(1) through (c)(3) above with respect to such
    waste.
    d)
    A generator or treater that first claims that hazardous debris is
    excluded from the definition of hazardous waste under 35 Ill. Adm.
    Code 721.103(e) (i.e., debris treated by an extraction or
    destruction technology provided by Section 728.Table F, and debris
    that has been delisted) is subject to the following notification
    and certification requirements:
    1)
    A one-time notification must be submitted to the Agency
    including the following information:
    A)
    The name and address of the RCRA Subtitle D (municipal
    solid waste landfill) facility receiving the treated
    debris;
    B)
    A description of the hazardous debris as initially
    generated, including the applicable U
    .S. EPA hazardous
    waste numbers; and
    C)
    For debris excluded under 35 Ill. Ad
    m. Code
    728.103(f)(2) 721.103(e)(1) , the technology from
    Section 728.Table F used to treat the debris.
    2)
    The notification must be updated if the debris is shipped to
    a different facility and, for debris excluded 35 Ill. Adm.
    Code 721.2(d)(1), if a different type of debris is treated
    or if a different technology is used to treat the debris.
    389
    3)
    For debris excluded under 35 Ill. Adm. Code
    728.103(f)(2) 721.103(e)(1) , the owner or operator of the
    treatment facility shall document and certify compliance
    with the treatment standards of Section 728.Table F, as
    follows:
    A)
    Records must be kept of all inspections, evaluations,
    and analyses of treated debris that are made to
    determine compliance with the treatment standards;
    B)
    Records must be kept of any data or information the
    treater obtains during treatment of the debris that
    identifies key operating parameters of the treatment
    unit; and
    C)
    For each shipment of treated debris, a certification
    of compliance with the treatment standards must be
    signed by an authorized representative and placed in
    the facility's files. The certification must state
    the following: "I certify under penalty of law that
    the debris has been treated in accordance with the
    requirements of 35 Ill. Adm. Code 728.145. I am aware
    that there are significant penalties for making a
    false certification, including the possibility of fine
    and imprisonment."
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.109
    Special Rules for Characteristic Wa
    stes
    a)
    The initial generator of a solid waste shall determine each U
    .S.
    EPA hazardous waste number (waste code) applicable to the waste in
    order to determine the applicable treatment standards under
    728.Subpart D. For purposes of this Part, the waste must carry
    the waste code for any applicable listing under 35 Ill. Adm. Code
    721.Subpart D. In addition, the waste must carry one or more of
    the waste codes under 35 Ill. Adm. Code 721.Subpart C where the
    waste exhibits a characteristic, except in the case when the
    treatment standard for the waste code listed in 35 Ill. Adm. Code
    721.Subpart D operates in lieu of the standard for the waste code
    under 35 Ill. Adm. Code 721.Subpart C, as specified in subsection
    (b) below. If the generator determines that its waste displays
    thea characteristic of
    ignitability (D001)
    hazardous waste (and the
    waste is not in the a D004 through D011 waste, a
    High TOC Ignitable
    Liquids Subcategory
    D001 waste, orand is not treated by CMBST or
    RORGS, as described in Section 728.Table C
    ), that its waste
    displays the characteristic of corrosivity (D002) and is
    prohibited under Section 728.137, or that its waste displays the
    characteristic of toxicity (D012 through D043) and is prohibited
    under Section 728.138,
    the generator shall determine what
    underlying hazardous constituents (as defined in Section 728.102)
    are reasonably expected to be present
    in the D001, D002, or D012
    through D043 waste
    above the universal treatment standards set
    forth in Sections 728.148 and 728.Table U
    .
    b)
    Where a prohibited waste is both listed under 35 Ill. Adm. Code
    721.Subpart D and exhibits a characteristic under 35 Ill. Adm.
    Code 721.Subpart C, the treatment standard for the waste code
    listed in 35 Ill. Adm. Code 721.Subpart D will operate in lieu of
    the standard for the waste code under 35 Ill. Adm. Code
    721.Subpart C, provided that the treatment standard for the listed
    390
    waste includes a treatment standard for the constituent that
    causes the waste to exhibit the characteristic. Otherwise, the
    waste must meet the treatment standards for all applicable listed
    and characteristic waste codes.
    c)
    In addition to any applicable standards determined from the
    initial point of generation, no prohibited waste that exhibits a
    characteristic under 35 Ill. Adm. Code 721.Subpart C shall be land
    disposed unless the waste complies with the treatment standards
    under 728.Subpart D.
    d)
    A waste s that exhibits a characteristic is also subject to Section
    728.107 requirements, except that once the waste is no longer
    hazardous, a one time one-time notification and certification must
    be placed in the generator's or treater's files and sent to the
    Agency , except for those facilities described in subsection (f)
    below. The notification and certification that is placed in the
    generator's or treater's files must be updated if the process or
    operation generating the waste changes or if the subtitle D
    facility receiving the waste changes. However, the generator or
    treater need only notify the Agency on an annual basis if such
    changes occur. Such notification and certification should be sent
    to the Agency by the end of the year, but no later than December
    31.
    1)
    The notification must include the following information:
    A) TFor a characteristic waste other than one managed on
    site in a wastewater treatment system subject to the
    federal Clean Water Act (CWA), a zero-discharger
    engaged in CWA-equivalent treatment, or a Class I
    nonhazardous waste injection well, t
    he name and
    address of the RCRA Subtitle D (municipal solid waste
    landfill) facility receiving the waste shipment; and
    B) AFor a waste that exhibits a characteristic of
    hazardous waste, a
    description of the waste as
    initially generated, including the applicable U
    .S. EPA
    hazardous waste numbers, the treatability group(s),
    and the underlying hazardous constituents
    (as defined
    in Section 728.102(i)) in D001 and D002 wastes
    prohibited under Section 728.137 or D012 through D043
    wastes prohibited under Section 728.138
    .
    2)
    The certification must be signed by an authorized
    representative and must state the language found in Section
    728.107(b)(5)(A). If treatment removes the characteristic
    but does not treat underlying hazardous constituents, then
    the certification found in Section 728.107(b)(5)(D) applies.
    3)
    For a characteristic waste whose ultimate disposal will be
    into a Class I nonhazardous waste injection well, and for
    which compliance with the treatment standards set forth in
    Sections 728.148 and 728.Table U for underlying hazardous
    constituents is achieved through pollution prevention that
    meets the criteria set forth at 35 Ill. Adm. Code
    738.101(d), the following information must also be included:
    A)
    A description of the pollution prevention mechanism
    and when it was implemented if already complete;
    391
    B)
    The mass of each underlying hazardous constituent
    before pollution prevention;
    C)
    The mass of each underlying hazardous constituent that
    must be removed, adjusted to reflect variations in
    mass due to normal operating conditions; and
    D)
    The mass reduction of each underlying hazardous
    constituent that is achieved.
    e)
    For a decharacterized waste managed on-site in a wastewater
    treatment system subject to the federal Clean Water Act (CWA) or
    zero-dischargers engaged in CWA-equivalent treatment, compliance
    with the treatment standards set forth in Sections 728.148 and
    728.Table D must be monitored quarterly, unless the treatment is
    aggressive biological treatment, in which case compliance must be
    monitored annually. Monitoring results must be kept in on-site
    files for 5 years.
    f)
    For a decharacterized waste managed on-site in a wastewater
    treatment system subject to the federal Clean Water Act (CWA) for
    which all underlying hazardous constituents (as defined in Section
    728.102) are addressed by a CWA permit, this compliance must be
    documented and this documentation must be kept in on-site files.
    g)
    For a characteristic waste whose ultimate disposal will be into a
    Class I nonhazardous waste injection well that qualifies for the
    de minimis exclusion described in Section 728.101, information
    supporting that qualification must be kept in on-site files.
    (Source: Amended at 19 Ill. Reg. 9660, effective June 27, 1995)
    SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION
    AND ESTABLISHMENT OF TREATMENT STANDARDS
    Section 728.110
    First Third (Repealed)
    The Board incorporates by reference 40 CFR 268.10 (1991). This Section
    incorporates no later editions or amendments.
    (Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
    Section 728.111
    Second Thi rd (Repealed)
    The Board incorporates by reference 40 CFR 268.11 (1991). This Section
    incorporates no later editions or amendments.
    (Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
    Section 728.112
    Third Third (Repealed)
    The Board incorporates by reference 40 CFR 268.12 (1991). This Section
    incorporates no later editions or amendments.
    (Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
    SUBPART C: PROHIBITION ON LAND DISPOSAL
    Section 728.139 Statutory Prohibitions
    Waste-Specific Prohibitions: End-of-
    392
    pipe CWA, CWA-Equivalent, and Class I Nonhazardous Waste
    Injection Well Treatment Standards; Spent Aluminum
    Potliners; and Carbamate Wastes
    No person shall cause, threaten or allow the land disposal of any waste in
    violation of Section 3004 of the Resource Conservation and Recovery Act,
    incorporated by reference in 35 Ill. Adm. Code 720.111.
    a)
    The wastes specified in 35 Ill. Adm. Code 721.132 as EPA Hazardous
    Waste numbers K156-K159; and in 35 Ill. Adm. Code 721.133 as USEPA
    hazardous waste numbers P127, P128, P185, P188 through P192, P194,
    P196 through P199, P201 through P205, U271, U278 through U280,
    U364, U367, U372, U373, U387, U389, 394, U395, U404, and U409
    through U411 are prohibited from land disposal. In addition, soil
    and debris contaminated with these wastes are prohibited from land
    disposal.
    b)
    The wastes identified in 35 Ill. Adm. Code 721.123 as USEPA
    hazardous waste number D003 are prohibited from land disposal,
    other than those that are managed in a system whose discharge is
    regulated under 35 Ill. Adm. Code:Subtitle C, one that injects
    hazardous waste in Class I waste injection well regulated under 35
    Ill. Adm. Code 702, 704, and 730, or one that is a zero discharger
    that engages in federal Clean Water Act (CWA)-equivalent treatment
    before ultimate land disposal. This prohibition does not apply to
    unexploded ordnance and other explosive devices that have been the
    subject of an emergency response. (Such D003 wastes are
    prohibited unless they meet the treatment standard of DEACT before
    land disposal (see Section 728.140)).
    c)
    The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA
    hazardous waste number K088 are prohibited from land disposal. In
    addition, soil and debris contaminated with these wastes are
    prohibited from land disposal.
    d)
    Effective April 8, 1998, radioactive wastes mixed with waste
    designated by any of USEPA hazardous waste numbers K088, K156
    through K159, K161, P127, P128, P185, P188 through P192, P194,
    P196 through P199, P201 through P205, U271, U278 through U280,
    U364, U367, U372, U373, U387, U389, U394, U395, U404, and U409
    through U411 are prohibited from land disposal. In addition, soil
    and debris contaminated with these radioactive mixed wastes are
    prohibited from land disposal.
    e)
    Until April 8, 1998, the wastes included in subsections (a), (b),
    (c), and (d) above may be disposed in a landfill or surface
    impoundment only if such unit complies with the requirements of
    Section 728.105(h)(2).
    f)
    The requirements of subsections (a), (b), (c), and (d) of this
    Section do not apply if:
    1)
    The wastes meet the applicable treatment standards specified
    in 728.Subpart D;
    2)
    The person conducting the disposal has been granted an
    exemption from a prohibition under a petition pursuant to
    Section 728.106, with respect to those wastes and units
    covered by the petition;
    3)
    The wastes meet the applicable alternative treatment
    393
    standards established pursuant to a petition granted under
    Section 728.144; or
    4)
    The person conducting the disposal has been granted an
    extension to the effective date of a prohibition pursuant to
    Section 728.105, with respect to those wastes covered by the
    extension.
    g)
    To determine whether a hazardous waste identified in this Section
    exceeds the applicable treatment standards set forth in Section
    728.140, the initial generator must test a sample of the waste
    extract or the entire waste, depending on whether the treatment
    standards are expressed as concentrations in the waste extract or
    in the waste, or the generator may use knowledge of the waste. If
    a waste contains constituents in excess of the applicable
    728.Subpart D levels, the waste is prohibited from land disposal
    and all requirements of this Part are applicable to the waste,
    except as otherwise specified.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART D: TREATMENT STANDARDS
    Section 728.140
    Applicability of Treatment Standards
    a)
    A prohibited waste identified in Section 728.Table T, "Treatment
    Standards for Hazardous Wastes", may be land disposed only if it
    meets the requirements found in that Section. For each waste,
    Section 728.Table T identifies one of three types of treatment
    standard requirements:
    1)
    All hazardous constituents in the waste or in the treatment
    residue must be at or below the values found in that Section
    for that waste ("total waste standards");
    2)
    The hazardous constituents in the extract of the waste or in
    the extract of the treatment residue must be at or below the
    values found in that Section ("waste extract standards"); or
    3)
    The waste must be treated using the technology specified in
    that Section ("technology standard"), which is described in
    detail in Section 728.Table C, "Technology Codes and
    Description of Technology-Based Standards".
    b)
    For wastewaters, compliance with concentration level standards is
    based on maximums for any one day, except for D004 through D011
    wastes for which the previously promulgated treatment standards
    based on grab samples remain in effect. For all nonwastewaters,
    compliance with concentration level standards is based on grab
    sampling. For wastes covered by the waste extract standards, the
    test Method 1311, the Toxicity Characteristic Leaching Procedure,
    found in "Test Methods for Evaluating Solid Waste,
    Physical/Chemical Methods", U
    .S. EPA Publication SW-846,
    incorporated by reference in Section 720.111, must be used to
    measure compliance. An exception is made for D004 and D008, for
    which either of two test methods may be used: Method 1311 or
    Method 1310, the Extraction Procedure Toxicity Test, found in
    "Test Methods for Evaluating Solid Waste, Physical/Chemical
    Methods", U .S. EPA Publication SW-846, incorporated by reference
    in Section 720.111. For wastes covered by a technology standard,
    394
    the wastes may be land disposed after being treated using that
    specified technology or an equivalent treatment technology
    approved by the Agency pursuant to Section 728.142(b).
    c)
    When wastes with differing treatment standards for
    a constituent
    of concern are combined for purposes of treatment, the treatment
    residue must meet the lowest treatment standard for the
    constituent of concern.
    d)
    Notwithstanding the prohibitions specified in subsection (a)
    above, treatment and disposal facilities may demonstrate (and
    certify pursuant to 35 Ill. Adm. Code 728.107(b)(5)) compliance
    with the treatment standards for organic constituents specified by
    a footnote in Section 728.Table T, provided the following
    conditions are satisfied:
    1)
    The treatment standards for the organic constituents were
    established based on incineration in units operated in
    accordance with the technical requirements of 35 Ill. Adm.
    Code 724.Subpart O, or based on combustion in fuel
    substitution units operating in accordance with applicable
    technical requirements;
    2)
    The treatment or disposal facility has used the methods
    referenced in subsection (d)(1) above to treat the organic
    constituents; and
    3)
    The treatment or disposal facility may demonstrate
    compliance with organic constituents if good-faith
    analytical efforts achieve detection limits for the
    regulated organic constituents that do not exceed the
    treatment standards specified in this Section and Section
    728.Table T by an order of magnitude.
    e)
    For characteristic wastes (U
    .S. EPA hazardous waste numbers D001
    ,
    D002, and D012 through D003 and D018 through
    D043) that are
    subject to treatment standards
    set forth in Section 728.Table T,
    "Treatment Standards for Hazardous Wastes", all underlying
    hazardous constituents (as defined in Section 728.102(i)) must
    meet the universal treatment standards,
    foundset forth in Section s
    728.148 and 728.Table U prior to land disposal
    , as defined in
    Section 728.102(c)
    .
    f)
    The treatment standards for U
    .S. EPA hazardous waste numbers F001
    through F005 nonwastewater constituents carbon disulfide,
    cyclohexanone, or methanol apply to wastes that contain only one,
    two, or three of these constituents. Compliance is measured for
    these constituents in the waste extract from test Method 1311, the
    Toxicity Characteristic Leaching Procedure found in "Test Methods
    for Evaluating Solid Waste, Physical/Chemical Methods", U
    .S. EPA
    Publication SW-846, incorporated by reference in Section 720.111.
    If the waste contains any of these three constituents along with
    any of the other 25 constituents found in U
    .S. EPA hazardous waste
    numbers F001 through F005, then compliance with treatment
    standards for carbon disulfide, cyclohexanone, or methanol are not
    required.
    g)
    This subsection corresponds with 40 CFR 268.40(g), added at 61
    Fed. Reg. 43927 (Aug. 26, 1996), which has expired. This
    statement maintains structural consistency with the federal rules.
    395
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.144
    Adjustment of Treatment Standard
    a)
    Where the treatment standard is expressed as a concentration in a
    waste or waste extract and a waste cannot be treated to the
    specified level, or where the treatment technology is not
    appropriate to the waste, the generator or treatment facility may
    petition to the Board for an adjusted treatment standard. As
    justification, the petitioner shall demonstrate that, because the
    physical or chemical properties of the waste differ significantly
    from wastes analyzed in developing the treatment standard, the
    waste cannot be treated to specified level or by the specified
    methods.
    BOARD NOTE: 40 CFR 268.44 refers to these as "treat
    ability
    variances". The Board has not used this term in its rules to
    avoid confusion with the Board variances under Title IX of the
    Environmental Protection Act. The equivalent Board procedures are
    an "adjusted treatment standard" pursuant to sub
    sections (a)
    through (l), or a "treatability exception" adopted pursuant to
    subsections (m) et seq. While the latter is adopted by "identical
    in substance" rulemaking following a USEPA action, the former is
    an original Board action which will be the only mechanism
    following authorization to the State of this component of the RCRA
    program.
    b)
    Each petition mu st be submitted in accordance with the procedures
    in 35 Ill. Adm. Code 106.Subpart G.
    c)
    Each petition must include the following statement signed by the
    petitioner or an authorized representative:
    I certify under penalty of law that I have personally
    examined and am familiar with the information submitted in
    this petition and all attached documents, and that, based on
    my inquiry of those individuals immediately responsible for
    obtaining the information, I believe that the submitted
    information is true, accurate and complete. I am aware that
    there are significant penalties for submitting false
    information, including the possibility of fine and
    imprisonment.
    d)
    After receiving a petition for an adjusted treatment standard, the
    Board may request any additional information or samples which are
    necessary to evaluate the petition.
    e)
    The Board will give public notice and provide an opportunity for
    public comment, as provided in 35 Ill. Adm. Code 106. In
    conjunction with any updating of the RCRA regulations, the Board
    will maintain, in this Part, a listing of all adjusted treatment
    standards granted by the Board pursuant to this Section. A
    LISTING OF ALL ADJUSTED STANDARDS GRANTED PURSUANT TO THIS SECTION
    WILL BE PUBLISHED IN THE ILLINOIS REGISTER AND ENVIRONMENTAL
    REGISTER AT THE END OF EACH FISCAL YEAR. (Section 28.1(d)(3) of
    the Environmental Protection Act.)
    f)
    A generator, treatment facility or disposal facility that is
    managing a waste covered by an adjusted treatment standard shall
    comply with the waste analysis requirements for restricted wastes
    found under Section 728.107.
    396
    g)
    During the petition review process, the applicant is required to
    comply with all restrictions on land disposal under this Part once
    the effective date for the waste has been reached.
    h)
    Where the treatment standard is expressed as a concentration in a
    waste or waste extract and a waste generated under conditions
    specific to only one site cannot be treated to the specified
    level, or where treatment technology is not appropriate to the
    waste, the generator or treatment facility may petition the Board
    for a site-specific adjusted treatment standard. The petitioner
    shall demonstrate that, because the physical or chemical
    properties of the waste differs significantly from the waste
    analyzed in developing the treatment standard, the waste cannot be
    treated to specified levels or by the specified methods.
    i)
    Each petition for a site-specific adjusted treatment standard must
    include the information in 35 Ill. Adm. Code 720.120(b)(1) through
    (4).
    j)
    After receiving a petition for a site-specific adjusted treatment
    standard, the Board may request any additional information or
    samples which the Board determines are necessary to evaluate the
    petition.
    k)
    A generator, treatment facility or disposal facility which is
    managing a waste covered by a site-specific adjusted treatment
    standard shall comply with the waste analysis requirements for
    restricted wastes in Section 728.107.
    l)
    During the petition review process, the petitio
    ner for a site-
    specific adjusted treatment standard shall comply with all
    restrictions on land disposal under this Part once the effective
    date for the waste has been reached.
    m)
    If USEPA grants a treatability exception by regulatory action
    pursuant to 40 CFR 268.44 (19
    9196) and a person demonstrates that
    the treatability exception needs to be adopted as part of the
    Illinois RCRA program because the waste is generated or managed in
    Illinois, the Board will adopt the treatability exception by
    identical in substance rulemaking pursuant to Section 22.4(a) of
    the Environmental Protection Act.
    BOARD NOTE: The Board will adopt the treatability exception
    during a RCRA update Docket if a timely demonstration is made.
    Otherwise, the Board will assign the matter to a separate Docket.
    o)
    The facilities listed in Table H are excluded from the treatment
    standard under Section 728.143(a) and Table B, and are subject to
    the constituent concentrations listed in Table H.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.148
    Universal Treatment Standards
    Section 728.Table U, "Universal Treatment Standards (UTS)", identifies the
    hazardous constituents, along with the nonwastewater and wastewater treatment
    standard levels, that are used to regulate most prohibited hazardous wastes
    with numerical limits. For determining compliance with treatment standards
    for underlying hazardous constituents, as defined in Section 728.102(i), these
    treatment standards may not be exceeded. Compliance with these treatment
    397
    standards is measured by an analysis of grab samples, unless otherwise noted
    in Section 728.Table U.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.Appendix K
    Metal Bearing Wastes Prohibited From Dilution in a
    Combustion Unit According to Section 728.103(c)
    BOARD NOTE: A combustion unit is defined as any thermal technology subject to
    35 Ill. Adm. Code 724.Subpart O, 725.Subpart O, or 726.Subpart H.
    Waste code
    Waste description
    D004
    Toxicity Characteristic for Arsenic.
    D005
    Toxicity Characteristic for Barium.
    D006
    Toxicity Characteristic for Cadmium.
    D007
    Toxicity Characteristic for Chromium.
    D008
    Toxicity Characteristic for Lead.
    D009
    Toxicity Characteristic for Mercury.
    D010
    Toxicity Characteristic for Selenium.
    D011
    Toxicity Characteristic for Silver.
    F006
    Wastewater treatment sludges from electroplating operations except
    from the following processes: (1) sulfuric acid anodizing of
    aluminum; (2) tin plating carbon steel; (3) zinc plating basis) on
    carbon steel; (4) aluminum or zinc
    -plating on carbon steel; (5)
    cleaning/stripping associated with tin, zinc and aluminum plating
    on carbon steel; and (6) chemical etching and milling of aluminum.
    F007
    Spent cyanide plating bath solutions from electroplating
    operations.
    F008
    Plating bath residues from the bottom of plating baths from
    electroplating operations where cyanides are used in the process.
    F009
    Spent stripping and cleaning bath solutions from electroplating
    operations where cyanides are used in the process.
    F010
    Quenching bath residues from oil baths from metal treating
    operations where cyanides are used in the process.
    F011
    Spent cyanide solutions from salt bath pot cleaning from metal
    heat treating operations.
    F012
    Quenching waste water treatment sludges from metal heat treating
    operations where cyanides are used in the process.
    F019
    Wastewater treatment sludges from the chemical conversion coating
    of aluminum except from zirconium phosphating in aluminum car
    washing when such phosphating is an exclusive conversion coating
    process.
    K002
    Wastewater treatment sludge from the production of chrome yellow
    398
    and orange pigments.
    K003
    Wastewater treatment sludge from the production of molybdate
    orange pigments.
    K004
    Wastewater treatment sludge from the production of zinc yellow
    pigments.
    K005
    Wastewater treatment sludge from the production of chrome green
    pigments.
    K006
    Wastewater treatment sludge from the production of chrome oxide
    green pigments (anhydrous and hydrated).
    K007
    Wastewater treatment sludge from the production of iron blue
    pigments.
    K008
    Oven residue from the production of chrome oxide green pigments.
    K061
    Emission control dust/sludge from the primary production of steel
    in electric furnaces.
    K069
    Emission control dust/sludge from secondary lead smelting.
    K071
    Brine purification muds from the mercury cell processes in
    chlorine production, where separately prepurified brine is not
    used.
    K100
    Waste leaching solution from acid leaching of emission control
    dust/sludge from secondary lead smelting.
    K106
    Sludges from the mercury cell processes for making chlorine.
    P010
    Arsenic acid H
    3
    AsO
    4
    .
    P011
    Arsenic oxide As
    2
    O
    5
    .
    P012
    Arsenic trioxide.
    P013
    Barium cyanide.
    P015
    Beryllium.
    P029
    Copper (I) cyanide Cu(CN).
    P074
    Nickel (II) cyanide Ni(CN)
    2
    .
    P087
    Osmium (VIII) tetroxide OsO
    4
    .
    P099
    Potassium silver cyanide KAg(CN)
    2
    .
    P104
    Silver cyanide AgCN.
    P113
    Thallic (III) oxide Tl
    2
    O
    3
    .
    P114
    Thallium (I) selenite Tl
    2
    SeO
    3
    .
    P115
    Thallium (I) sulfate Tl
    2
    SO
    4
    .
    P119
    Ammonium (V) vanadate NH
    3
    VO
    3
    .
    399
    P120
    Vanadium (V) oxide V
    2
    O
    5
    .
    P121
    Zinc cyanide ZnCN.
    U032
    Calcium chromate CaCrO
    4
    .
    U145
    Lead phosphate.
    U151
    Mercury.
    U204
    Selenous acid H
    2
    SeO
    3
    .
    U205
    Selenium (IV) disulfide SeS
    2
    .
    U216
    Thallium (I) chloride TlCl.
    U217
    Thallium (I) nitrate TlNO
    3
    .
    (Source: Added at 21 Ill. Reg. ________, effective ____________________)
    Section 728.Table C
    Technology Codes and Description of Technology-Based
    Standards
    Technology
    code
    Description of technology-based standard
    ADGAS
    Ventin g of compressed gases into an absorbing or reacting media (i.e.,
    solid or liquid)--venting can be accomplished through physical release
    utilizing valves or piping; physical penetration of the container; or
    penetration through detonation.
    AMLGM
    Amalgamation of liquid, elemental mercury contaminated with radioactive
    materials utilizing inorganic reagents such as copper, zinc, nickel,
    gold, and sulfur that result in a nonliquid, semi-solid amalgam and
    thereby reducing potential emissions of elemental mercury vapors to the
    air.
    BIODG
    Biodegradation of organics or non-metallic inorganics (i.e., degradable
    inorganics that contain the elements of phosphorus, nitrogen, and
    sulfur) in units operated under either aerobic or anaerobic conditions
    such that a surrogate compound or indicator parameter has been substan
    -
    tially reduced in concentration in the residuals (e.g., total organic
    carbon (TOC) can often be used as an indicator parameter for the
    biodegrada tion of many organic constituents that cannot be directly
    analyzed in wastewater residues).
    CARBN
    Carbon adsorption (granulated or powdered) of non-metallic inorganics,
    organo-metallics, or organic constituents, operated so that a surrogate
    compound or indicator parameter has not undergone break
    through (e.g.,
    total organic carbon (TOC) can often be used as an indicator parameter
    for the adsorption of many organic constituents that cannot be directly
    analyzed in wastewater residues). Breakthrough occurs when the carbon
    has become saturated with the constituent (or indicator parameter) and
    substantial change in adsorption rate associated with that constituent
    occurs.
    CHOXD
    Chemical or electrolytic oxidation utilizing the following oxidation
    reagents (or waste reagents) or combinations or reagents:
    1)
    hypochlorite (e.g., bleach);
    400
    2)
    chlorine;
    3)
    chlorine dioxide;
    4)
    ozone or UV (ultraviolet light) assisted ozone;
    5)
    peroxides;
    6)
    persulfates;
    7)
    perchlorates;
    8)
    permangantes; or
    9)
    other oxidizing reagents of equivalent efficiency, performed in
    units operated so that a surrogate compound or indicator parameter
    has been substantially reduced in concentration in the residuals
    (e.g., total organic carbon (TOC) can often be used as an
    indicator parameter for the oxidation of many organic constit
    uents
    that cannot be directly analyzed in wastewater residues).
    Chemical oxidation specifically includes what is commonly referred
    to as alkaline chlorination.
    CHRED
    Chemical reduction utilizing the following reducing reagents (or waste
    reagents) or combinations of reagents:
    1)
    sulfur dioxide;
    2)
    sodium, potassium, or alkali salts of sulfites, bisulfites,
    metabisulfites, and polyethylene glycols (e.g., NaPEG and KPEG);
    3)
    sodium hydrosulfide;
    4)
    ferrous salts; or
    5)
    other reducing reagents of equivalent efficiency, performed in
    units operated such that a surrogate compound or indicator
    parameter has been substantially reduced in concentration in the
    residuals (e.g., total organic halogens (TOX) can often be used as
    an indicator parameter for the reduction of many halogenated
    organic constituents that cannot be directly analyzed in
    wastewater residues). Chemical reduction is commonly used for the
    reduction of hexavalent chromium to the trivalent state.
    CMBST
    Combustion in incinerators, boilers, or industrial furnaces operated in
    accordance with the applicable requirements of 35 Ill. Adm. Code
    724.Subpart O, 725.Subpart O, or 35 Ill. Adm. Code 726.Subpart H.
    DEACT
    Deactivation to remove the hazardous characteristics of a waste due to
    its ignitability, corrosivity, or reactivity.
    FSUBS
    Fuel substitution in units operated in accordance with applicable
    technical operating requirements.
    HLVIT
    Vitrification of high level mixed radioactive wastes in units in
    compliance with all applicable radioactive protection requirements under
    control of the federal Nuclear Regulatory Commission.
    IMERC
    Incineration of wastes containing organics and mercury in units operated
    in accordance with the technical operating requirements of 35 Ill. Adm.
    Code 724.Subpart O or 725.Subpart O. All wastewater and nonwastewater
    401
    residues derived from this process must then comply with the
    corresponding treatment standards per waste code with consideration of
    any applicable subcategories (e.g., high or low mercury sub
    categories).
    INCIN
    Incineration in units operated in accordance with the technical
    operating requirements of 35 Ill. Adm. Code 724.Subpart O or 725.Subpart
    O.
    LLEXT
    Liquid-liquid extraction (often referred to as solvent extraction) of
    organics from liquid wastes into an immiscible solvent for which the
    hazardous constituents have a greater solvent affinity, resulting in an
    extract high in organics that must undergo either incineration, reuse as
    a fuel, or other recovery or reuse and a raffinate (extracted liquid
    waste) proportionately low in organics that must undergo further
    treatment as specified in the standard.
    MACRO
    Macroencapsulation with surface coating materials such as polymeric
    organics (e.g., resins and plastics) or with a jacket of inert inorganic
    materials to substantially reduce surface exposure to potential leaching
    media. Macroencapsulation specifically does not include any material
    that would be classified as a tank or container according to 35 Ill.
    Adm. Code 720.110.
    NEUTR
    Neutralization with the following reagents (or waste reagents) or
    combinations of reagents:
    1)
    acids;
    2)
    bases; or
    3)
    water (including wastewaters) resulting in a pH greater than 2 but
    less than 12.5 as measured in the aqueous residuals.
    NLDBR
    No land disposal based on recycling.
    PRECP
    Chemical precipitation of metals and other inorganics as insoluble
    precipitates of oxides, hydroxides, carbonates, sulfides, sulfates,
    chlorides, fluorides, or phosphates. The following reagents (or waste
    reagents) are typically used alone or in combination:
    1)
    lime (i.e., containing oxides or hydroxides of calcium or
    magnesium;
    2)
    caustic (i.e., sodium or potassium hydroxides;
    3)
    soda ash (i.e., sodium carbonate);
    4)
    sodium sulfide;
    5)
    ferric sulfate or ferric chloride;
    6)
    alum; or
    7)
    sodium sulfate. Additional flocculating, coagulation, or similar
    reagents or processes that enhance sludge dewatering
    characteristics are not precluded from use.
    RBERY
    Thermal recovery of beryllium.
    RCGAS
    Recovery or reuse of compressed gases including techniques such as
    reprocessing of the gases for reuse or resale; filtering or adsorption
    402
    of impurities; remixing for direct reuse or resale; and use of the gas
    as a fuel source.
    RCORR
    Recovery of acids or bases utilizing one or more of the following
    recovery technologies:
    1)
    distillation (i.e., thermal concentration);
    2)
    ion exchange;
    3)
    resin or solid adsorption;
    4)
    reverse osmosis; or
    5)
    incineration for the recovery of acid
    --
    Note: this does not preclude the use of other physical phase
    separation or concentra
    tion techniques such as decantation,
    filtration (including ultrafiltration), and centrifugation, when
    used in conjunction with the above listed recovery technologies.
    RLEAD
    Thermal recovery of lead in secondary lead smelters.
    RMERC
    Retorting or roasting in a thermal processing unit capable of volatiliz
    -
    ing mercury and subsequently condensing the volatilized mercury for
    recovery. The retorting or roasting unit (or facility) must be subject
    to one or more of the following:
    a)
    A national emissions standard for hazardous air pollutants
    (NESHAP) for mercury (40 CFR 61, Subpart E);
    b)
    A best available control technology (BACT) or a lowest achievable
    emission rate (LAER) standard for mercury imposed pursuant to a
    prevention of significant deterioration (PSD) permit (including 35
    Ill. Adm. Code 201 through 203); or
    c)
    A state permit that establishes emission limitations (within
    meaning of Section 302 of the Clean Air Act) for mercury, includ
    -
    ing a permit issued pursuant to 35 Ill. Adm. Code 201. All
    wastewater and nonwastewater residues derived from this process
    must then comply with the corresponding treatment standards per
    waste code with consideration of any applicable subcategories
    (e.g., high or low mercury subcategories).
    RMETL
    Recovery of metals or inorganics utilizing one or more of the following
    direct physical or removal technologies:
    1)
    ion exchange;
    2)
    resin or solid (i.e., zeolites) adsorption;
    3)
    reverse osmosis;
    4)
    chelation or solvent extraction;
    5)
    freeze crystallization;
    6)
    ultrafiltration; or
    7)
    simple precipitation (i.e., crystallization)
    403
    Note: this does not preclude the use of other physical phase separation
    or concentration techniques such as decantation, filtration (including
    ultrafiltration), and centrifugation, when used in conjunction with the
    above listed recovery technologies.
    RORGS
    Recovery of organics utilizing one or more of the following technolo
    -
    gies:
    1)
    Distillation;
    2)
    thin film evaporation;
    3)
    steam stripping;
    4)
    carbon adsorption;
    5)
    critical fluid extraction;
    6)
    liquid-liquid extraction;
    7)
    precipitation or crystallization (including freeze
    crystallization); or
    8)
    chemical phase separation techniques (i.e., addition of acids,
    bases, demulsifiers, or similar chemicals).
    Note: This does not preclude the use of other physical phase separation
    techniques such as decantation, filtration (including ultrafiltration),
    and centrifugation, when used in conjunction with the above listed
    recovery technologies.
    RTHRM
    Thermal recovery of metals or inorganics from nonwastewaters in units
    defined as cement kilns, blast furnaces, smelting, melting and refining
    furnaces, combustion devices used to recover sulfur values from spent
    sulfuric acid and "other devices" determined by the Agency pursuant to
    35 Ill. Adm. Code 720.110, the definition of "industrial furnace".
    RZINC
    Resmelting in high temperature metal recovery units for the purpose of
    recovery of zinc.
    STABL
    Stabilization with the following reagents (or waste reagents) or
    combinations of reagents:
    1)
    Portland cement; or
    2)
    lime or pozzolans (e.g., fly ash and cement kiln dust)--this does
    not preclude the addition of reagents (e.g., iron salts, sili
    -
    cates, and clays) designed to enhance the set or cure time or
    compressive strength, or to overall reduce the leachability of the
    metal or inorganic.
    SSTRP
    Steam stripping of organics from liquid wastes utilizing direct
    application of steam to the wastes operated such that liquid and vapor
    flow rates, as well as, temperature and pressure ranges have been
    optimized, monitored, and maintained. These operating parameters are
    dependent upon the design parameters of the unit such as, the number of
    separation stages and the internal column design. Thus, resulting in a
    condensed extract high in organics that must undergo either incinera
    -
    tion, reuse as a fuel, or other recovery or reuse and an extracted
    wastewater that must undergo further treatment as specified in the
    standard.
    404
    WETOX
    Wet air oxidation performed in units operated such that a surrogate
    compound or indicator parameter has been substantially reduced in
    concentration in the residuals (e.g., total organic carbon (TOC) can
    often be used as an indicator parameter for the oxidation of many
    organic constituents that cannot be directly analyzed in wastewater
    residues).
    WTRRX
    Controlled reaction with water for highly reactive inorganic or organic
    chemicals with precautionary controls for protection of workers from
    potential violent reactions as well as precautionary controls for
    potential emissions of toxic or ignitable levels of gases released
    during the reaction.
    Note 1:
    When a combination of these technologies (i.e., a treatment train)
    is specified as a single treatment standard, the order of
    application is specified in Section 728.Table T by indicating the
    five letter technology code that must be applied first, then the
    designation "fb." (an abbreviation for "followed by"), then the
    five letter technology code for the technology that must be
    applied next, and so on.
    Note 2:
    When more than one technology (or treatment train) are specified
    as alternative treatment standards, the five letter technology
    codes (or the treatment trains) are separated by a semicolon (;)
    with the last technology preceded by the word "OR". This indi
    -
    cates that any one of these BDAT technologies or treatment trains
    can be used for compliance with the standard.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.Table T
    Treatment Standards for Hazardous Wastes
    Note: The treatment standards that heretofore appeared in tables in Sections
    728.141, 728.142, and 728.143 have been consolidated into this table.
    Waste Code
    Waste Des cription and Treat ment or Regulatory Sub
    category
    1
    Regulated Hazardous Constituent
    Wastewaters
    Nonwaste waters
    Common Name
    CAS
    2
    Number
    Concentration
    in mg/l
    3
    ; or
    Technology
    Code
    4
    Concentration
    in mg/kg
    35
    un-
    less noted as
    "mg/l TCLP";
    or Technology
    Code
    4
    D001
    9
    Ignitable Characteristic Wastes, except for the Section 721.121(a)(1) High TOC
    Subcategory , that are managed in non-CWA or non-CWA-equivalent or non-Class I
    SDWA systems .
    NA
    NA
    DEACT and meet
    Section
    728.148
    standards;
    8
    or
    RORGS; or
    CMBST
    DEACT and meet
    Section
    728.148
    standards;
    8
    or
    RORGS; or
    CMBST
    D001
    Ignitable Characteristic Wastes, except for the Section 721.121(a)(1) High TOC
    405
    Subcategory, that are managed in CWA or CWA-equivalent or Class I SDWA systems
    NA
    NA
    DEACT
    DEACT
    D001
    9
    High TOC Ignitable Characteristic Liquids Subcategory based on 35 Ill. Adm.
    Code 721.121(a)(1) - Greater than or equal to 10% total organic carbon.
    (Note: This subcategory consists of nonwastewaters only.)
    NA
    NA
    NA
    RORGS; or
    CMBST
    D002
    9
    Corrosive Characteristic Wastes
    that are managed in non-CWA or non-CWA
    equivalent or non-Class I SDWA systems
    .
    NA
    NA
    DEACT and meet
    Section
    728.148
    standards
    8
    DEACT and meet
    Section
    728.148
    standards
    8
    D002
    Corrosive Characteristic Wastes that are managed in CWA, CWA equivalent, or
    Class I SDWA systems.
    NA
    NA
    DEACT
    DEACT
    D002, D004, D005, D006, D007, D008, D009, D010, D011
    Radioactive high level wastes generated during the reprocessing of fuel rods.
    (Note: This subcategory consists of nonwastewaters only.)
    Corrosivity (pH)
    NA
    NA
    HLVIT
    Arsenic
    7440-38-2
    NA
    HLVIT
    Barium
    7440-39-3
    NA
    HLVIT
    Cadmium
    7440-43-9
    NA
    HLVIT
    Chromium (Total)
    7440-47-3
    NA
    HLVIT
    Lead
    7439-92-1
    NA
    HLVIT
    Mercury
    7439-97-6
    NA
    HLVIT
    Selenium
    7782-49-2
    NA
    HLVIT
    Silver
    7440-22-4
    NA
    HLVIT
    D003
    9
    Reactive Sulfides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
    NA
    NA
    DEACT
    DEACT
    D003
    9
    Explosive subcategory based on 35 Ill. Adm. Code 721.123(a)(6), (a)(7), and
    (a)(8).
    NA
    NA
    DEACT and meet
    Section
    728.148
    standards
    8
    DEACT and meet
    Section
    728.148
    standards
    8
    D003
    9
    Unexploded ordnance and other explosive devices that have been the subject of
    an emergency response.
    NA
    NA
    DEACT
    DEACT
    D003
    9
    Other Reactives Subcategory based on 35 Ill. Adm. Code 721.123(a)(1).
    NA
    NA
    DEACT and meet
    Section
    728.148
    standards
    8
    DEACT and meet
    Section
    728.148
    standards
    8
    D003
    9
    406
    Water Reactive Subcategory based on 35 Ill. Adm. Code 721.123(a)(2), (a)(3),
    and (a)(4).
    (Note: This subcategory consists of nonwastewaters only.)
    NA
    NA
    NA
    DEACT and meet
    Section
    728.148
    standards
    8
    D003
    9
    Reactive Cyanides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
    Cyanides (Total)
    7
    57-12-5
    --
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    D004
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for arsenic based on the extraction procedure (EP) in SW-846 Method
    1310.
    Arsenic
    7440-38-2
    5.0
    5.0 mg/l EP
    Arsenic; alternat
    ive
    6
    standard for
    nonwastewaters only.
    7440-38-2
    NA
    5.0 mg/l TCLP
    D005
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for barium based on the extraction procedure (EP) in SW-846 Method
    1310.
    Barium
    7440-39-3
    100
    100 mg/l TCLP
    D006
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for cadmium based on the extraction procedure (EP) in SW-846 Method
    1310.
    Cadmium
    7440-43-9
    1.0
    1.0 mg/l TCLP
    D006
    Cadmium -Containing Batteries Subcategory
    (Note: This subcategory consists of nonwastewaters only.)
    Cadmium
    7440-43-9
    NA
    RTHRM
    D007
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for chromium based on the extraction procedure (EP) in SW-846 Met
    hod
    1310.
    Chromium (Total)
    7440-47-3
    5.0
    5.0 mg/l TCLP
    D008
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for lead based on the extraction procedure (EP) in SW-846 Method
    1310.
    Lead
    7439-92-1
    5.0
    5.0 mg/l EP
    Lead; alternat ive
    6
    standard for
    nonwastewaters only
    7439-92-1
    NA
    5.0 mg/l TCLP
    D008
    Lead Acid Batteries Subcategory
    (Note: This standard only applies to lead acid batteries that are identified
    as RCRA hazardous wastes and that are not excluded elsewhere from regulation
    under the land disposal restrictions of this Part or exempted under other
    regulations (see 35 Ill. Adm. Code 726.180).
    This subcategory consists of
    nonwastewaters only.
    ).
    (Note: This subcategory consists of nonwastewaters only.)
    407
    Lead
    7439-92-1
    NA
    RLEAD
    D008
    Radioactive Lead Solids Subcategory
    (Note: These lead solids include, but are not limited to, all forms of lead
    shielding and other elemental forms of lead. These lead solids do not include
    treatment residuals such as hydroxide sludges, other wastewater treatment
    residuals, or incinerator ashes that can undergo conventional pozzolanic
    stabilization, nor do they include organo-lead materials that can be
    incinerated and stabilized as ash.
    This subcategory consists of
    nonwastewaters only.
    )
    (Note: This subcategory consists of nonwastewaters only.)
    Lead
    7439-92-1
    NA
    MACRO
    D009
    Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
    toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
    1310; and contain greater than or equal to 260 mg/kg total mercury that also
    contain organics and are not incinerator residues.
    (High Mercury-Organic
    Subcategory)
    (High Mercury-Organic Subcategory)
    Mercury
    7439-97-6
    NA
    IMERC; or
    RMERC
    D009
    Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
    toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
    1310; and contain greater than or equal to 260 mg/kg total mercury that are
    inorganic, including incinerator residues and residues from RMERC.
    (High
    Mercury-Inorganic Subcategory)
    (High Mercury-Inorganic Subcategory)
    Mercury
    7439-97-6
    NA
    RMERC
    D009
    Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
    toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
    1310; and contain less than 260 mg/kg total mercury.
    (Low Mercury
    Subcategory)
    (Low Mercury Subcategory)
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    All D009 wastewaters.
    Mercury
    7439-97-6
    0.20
    NA
    D009
    Elemental mercury contaminated with radioactive materials.
    (Note: This subcategory consists of nonwastewaters only.)
    Mercury
    7439-97-6
    NA
    AMLGM
    D009
    Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory.
    (Note: This subcategory consists of nonwastewaters only.)
    Mercury
    7439-97-6
    NA
    IMERC
    D010
    Wastes that exhibit, or are expected to exhibit, the characteristic
    orof
    toxicity for selenium based on the extraction procedure (EP) in SW-846 Method
    1310.
    Selenium
    7782-49-2
    1.0
    5.7 mg/l TCLP
    408
    D011
    Wastes that exhibit, or are expected to exhibit, the characteristic of
    toxicity for silver based on the extraction procedure (EP) in SW-846 Method
    1310.
    Silver
    7440-22-4
    5.0
    5.0 mg/l TCLP
    D012
    9
    Wastes that are TC for Endrin based on the TCLP in SW-846 Method 1311.
    Endrin
    72-20-8
    BIODG; or
    INCINCMBST
    0.13 and meet
    Section
    728.148
    standards
    8
    Endrin aldehyde
    7421-93-4
    BIODG; or
    INCINCMBST
    0.13 and meet
    Section
    728.148
    standards
    8
    D013
    9
    Wastes that are TC for Lindane based on the TCLP in SW-846 Method 1311.
    alpha-BHC
    319-84-6
    CARBN; or
    INCINCMBST
    0.066 and meet
    Section
    728.148
    standards
    8
    beta-BHC
    319-85-7
    CARBN; or
    INCINCMBST
    0.066 and meet
    Section
    728.148
    standards
    8
    delta-BHC
    319-86-8
    CARBN; or
    INCINCMBST
    0.066 and meet
    Section
    728.148
    standards
    8
    gamma-BHC (Lindane)
    58-89-9
    CARBN; or
    INCINCMBST
    0.066 and meet
    Section
    728.148
    standards
    8
    D014
    9
    Wastes that are TC for Methoxychlor based on the TCLP in SW-846 Method 1311.
    Methoxychlor
    72-43-5
    WETOX or
    INCINCMBST
    0.18 and meet
    Section
    728.148
    standards
    8
    D015
    9
    Wastes that are TC for Toxaphene based on the TCLP in SW-846 Method 1311.
    Toxaphene
    8001-35-2
    BIODG or
    INCINCMBST
    2.6 and meet
    Section
    728.148
    standards
    8
    D016
    9
    Wastes that are TC for 2,4-D (2,4-Dichloro
    phenoxyacetic acid) based on the
    TCLP in SW-846 Method 1311.
    2,4-D (2,4-Dichloro
    -
    phenoxy acetic acid)
    94-75-7
    CHOXD,;
    BIODG,; or
    INCINCMBST
    10 and meet
    Section
    728.148
    standards
    8
    D017
    9
    Wastes that are TC for 2,4,5-TP (Silvex) based on the TCLP in SW-846 Method
    1311.
    409
    2,4,5-TP (Silvex)
    93-72-1
    CHOXD or
    INCINCMBST
    7.9 and meet
    Section
    728.148
    standards
    8
    D018
    9
    Wastes that are TC for Benzene based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    Benzene
    71-43-2
    0.14 and meet
    Section
    728.148
    standards
    8
    10 and meet
    Section
    728.148
    standards
    8
    D019
    9
    Wastes that are TC for Carbon tetra
    chloride based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Carbon tetra chloride
    56-23-5
    0.057 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D020
    9
    Wastes that are TC for Chlordane based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033 and
    meet Section
    728.148
    standards
    8
    0.26 and meet
    Section
    728.148
    standards
    8
    D021
    9
    Wastes that are TC for Chloro
    benzene based on the TCLP in SW-846 Method 1311
    and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Chloro benzene
    108-90-7
    0.057 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D022
    9
    Wastes that are TC for Chloro
    form based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    Chloro form
    67-66-3
    0.046 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D023
    9
    Wastes that are TC for o-Cresol based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    o-Cresol `
    95-48-7
    0.11 and meet
    Section
    728.148
    standards
    8
    5.6 and meet
    Section
    728.148
    standards
    8
    D024
    9
    Wastes that are TC for m-Cresol based on the TCLP in SW-846 Method 1311
    and
    410
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    m-Cresol
    (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77 and meet
    Section
    728.148
    standards
    8
    5.6 and meet
    Section
    728.148
    standards
    8
    D025
    9
    Wastes that are TC for p-Cresol based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    p-Cresol
    (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77 and meet
    Section
    728.148
    standards
    8
    5.6 and meet
    Section
    728.148
    standards
    8
    D026
    9
    Wastes that are TC for Cresols (Total) based on the TCLP in SW-846 Method 1311
    and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Cresol-mixed isomers
    (Cresylic acid)
    (sum of o -, m-, and p-
    cresol con centrations)
    1319-77-3
    0.88 and meet
    Section
    728.148
    standards
    8
    11.2 and meet
    Section
    728.148
    standards
    8
    D027
    9
    Wastes that are TC for p-Dichloro
    benzene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    p-Dichloro benzene (1,4-
    Dichloro benzene)
    106-46-7
    0.090 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D028
    9
    Wastes that are TC for 1,2-Dichloro
    ethane based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    1,2-Dichloro ethane
    107-06-2
    0.21 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D029
    9
    Wastes that are TC for 1,1-Dichloro
    ethylene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    1,1-Dichloro ethylene
    75-35-4
    0.025 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D030
    9
    Wastes that are TC for 2,4-Dinitro
    toluene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    2,4-Dinitro toluene
    121-14-2
    0.32 and meet
    Section
    728.148
    standards
    8
    140 and meet
    Section
    728.148
    standards
    8
    411
    D031
    9
    Wastes that are TC for Heptachlor based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    Heptachlor
    76-44-8
    0.0012 and
    meet Section
    728.148
    standards
    8
    0.066 and meet
    Section
    728.148
    standards
    8
    Heptachlor epoxide
    1024-57-3
    0.016 and meet
    Section
    728.148
    standards
    8
    0.066 and meet
    Section
    728.148
    standards
    8
    D032
    9
    Wastes that are TC for Hexa
    chloro benzene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Hexachloro benzene
    118-74-1
    0.055 and meet
    Section
    728.148
    standards
    8
    10 and meet
    Section
    728.148
    standards
    8
    D033
    9
    Wastes that are TC for Hexa
    chloro butadiene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Hexachloro butadiene
    87-68-3
    0.055 and meet
    Section
    728.148
    standards
    8
    5.6 and meet
    Section
    728.148
    standards
    8
    D034
    9
    Wastes that are TC for Hexa
    chloro ethane based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Hexachloro ethane
    67-72-1
    0.055 and meet
    Section
    728.148
    standards
    8
    30 and meet
    Section
    728.148
    standards
    8
    D035
    9
    Wastes that are TC for Methyl ethyl ketone based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Methyl ethyl ketone
    78-93-3
    0.28 and meet
    Section
    728.148
    standards
    8
    36 and meet
    Section
    728.148
    standards
    8
    D036
    9
    Wastes that are TC for Nitro
    benzene based on the TCLP in SW-846 Method 1311
    and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Nitrobenzene
    98-95-3
    0.068 and meet
    Section
    728.148
    standards
    8
    14 and meet
    Section
    728.148
    standards
    8
    D037
    9
    Wastes that are TC for Penta
    chloro phenol based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    412
    systems only .
    Pentachloro phenol
    87-86-5
    0.089 and meet
    Section
    728.148
    standards
    8
    7.4 and meet
    Section
    728.148
    standards
    8
    D038
    9
    Wastes that are TC for Pyridine based on the TCLP in SW-846 Method 1311
    and
    that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
    only.
    Pyridine
    110-86-1
    0.014 and meet
    Section
    728.148
    standards
    8
    16 and meet
    Section
    728.148
    standards
    8
    D039
    9
    Wastes that are TC for Tetra
    chloro ethylene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Tetrachloro ethylene
    127-18-4
    0.056 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D040
    9
    Wastes that are TC for Trichloro
    ethylene based on the TCLP in SW-846 Method
    1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Trichloro ethylene
    79-01-6
    0.054 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    D041
    9
    Wastes that are TC for 2,4,5-Trichloro
    phenol based on the TCLP in SW-846
    Method 1311 and that are managed in non-CWA or non-CWA equivalent or non-Class
    I SDWA systems only
    .
    2,4,5-Trichloro phenol
    95-95-4
    0.18 and meet
    Section
    728.148
    standards
    8
    7.4 and meet
    Section
    728.148
    standards
    8
    D042
    9
    Wastes that are TC for 2,4,6-Trichloro
    phenol based on the TCLP in
    SW-846
    Method 1311 and that are managed in non-CWA or non-CWA equivalent or non-Class
    I SDWA systems only
    .
    2,4,6-Trichloro phenol
    88-06-2
    0.035 and meet
    Section
    728.148
    standards
    8
    7.4 and meet
    Section
    728.148
    standards
    8
    D043
    9
    Wastes that are TC for Vinyl chloride based on the TCLP in SW-846 Method 1311
    and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
    systems only .
    Vinyl chloride
    75-01-4
    0.27 and meet
    Section
    728.148
    standards
    8
    6.0 and meet
    Section
    728.148
    standards
    8
    F001, F002, F003, F004 & F005
    413
    F001, F002, F003, F004, or F005 solvent wastes that contain any combination of
    one or more of the following spent solvents: acetone, benzene, n-butyl
    alcohol, carbon disulfide, carbon tetra
    chloride, chlorinated fluoro
    carbons,
    chloro benzene, o-cresol, m-cresol, p-cresol, cyclo
    hexanone, o-dichloro
    benzene,
    2-ethoxyethanol, ethyl acetate, ethyl benzene, ethyl ether, isobutyl alcohol,
    methanol, methylene chloride, methyl ethyl ketone, methyl isobutyl ketone,
    nitrobenzene, 2-nitro propane , pyridine, tetra
    chloro ethylene, toluene, 1,1,1-
    trichloro ethane, 1,1,2-trichloro
    ethane, 1,1,2-trichloro-
    1,2,2-trifluoro -
    ethane, trichloro
    ethylene, trichloro
    monofluoro methane, or xylenes (except as
    specifically noted in other subcategories). See further details of these
    listings in 35 Ill. Adm. Code 721.131
    Acetone
    67-64-1
    0.28
    160
    Benzene
    71-43-2
    0.14
    10
    n-Butyl alcohol
    71-36-3
    5.6
    2.6
    Carbon disulfide
    75-15-0
    3.8
    NA
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro benzene
    108-90-7
    0.057
    6.0
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol
    (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol
    (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    Cresol-mixed isomers
    (Cresylic acid)
    (sum of o -, m-, and p-
    cresol con centrations)
    1319-77-3
    0.88
    11.2
    Cyclohexanone
    108-94-1
    0.36
    NA
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    Ethyl acetate
    141-78-6
    0.34
    33
    Ethyl benzene
    100-41-4
    0.057
    10
    Ethyl ether
    60-29-7
    0.12
    160
    Isobutyl alcohol
    78-83-1
    5.6
    170
    Methanol
    67-56-1
    5.6
    NA
    Methylene chloride
    75-9-2
    0.089
    30
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    Methyl isobutyl ketone
    108-10-1
    0.14
    33
    Nitrobenzene
    98-95-3
    0.068
    14
    Pyridine
    110-86-1
    0.014
    16
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    Toluene
    108-88-3
    0.080
    10
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    1,1,2-Trichloro-1,2,2-
    trifluoro ethane
    76-13-1
    0.057
    30
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Trichloro monofluoro -
    methane
    75-69-4
    0.020
    30
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    F001, F002, F003, F004 & F005
    F003 and F005 solvent wastes that contain any combination of one or more of
    the following three solvents as the only listed F001 through F005 solvents:
    carbon disulfide, cyclo
    hexanone, or methanol. (Formerly Section 728.141(c))
    Carbon disulfide
    75-15-0
    3.8
    4.8 mg/l TCLP
    Cyclohexanone
    108-94-1
    0.36
    0.75 mg/l TCLP
    414
    Methanol
    67-56-1
    5.6
    0.75 mg/l TCLP
    F001, F002, F003, F004 & F005
    F005 solvent waste containing 2-Nitro
    propane as the only list
    ed F001 through
    F005 solvent.
    2-Nitro propane
    79-46-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    F001, F002, F003, F004 & F005
    F005 solvent waste containing 2-Ethoxyethanol as the only listed F001 through
    F005 solvent.
    2-Ethoxyethanol
    110-80-5
    BIODG; or
    INCINCMBST
    INCINCMBST
    F006
    Wastewater treatment sludges from electroplating operations except from the
    following processes: (1) Sulfuric acid anodizing of aluminum; (2) tin plating
    on carbon steel; (3) zinc plating (segregated basis) on carbon steel; (4)
    aluminum or zinc-aluminum plating on carbon steel; (5) cleaning or stripping
    associated with tin, zinc, and aluminum plating on carbon steel; and (6)
    chemical etching and milling of aluminum.
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F007
    Spent cyanide plating bath solutions from electroplating operations.
    Cadmium
    7440-43-9
    NA
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F008
    Plating bath residues from the bottom of plating baths from electroplating
    operations where cyanides are used in the process.
    Cadmium
    7440-43-9
    NA
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F009
    Spent stripping and cleaning bath solutions from electroplating operations
    where cyanides are used in the process.
    Cadmium
    7440-43-9
    NA
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    415
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F010
    Quenching bath residues from oil baths from metal heat treating operations
    where cyanides are used in the process.
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.880.86
    NA
    F011
    Spent cyanide solutions from salt bath pot cleaning from metal heat treating
    operations.
    Cadmium
    7440-43-9
    NA
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F012
    Quenching wastewater treatment sludges from metal heat treating operations
    where cyanides are used in the process.
    Cadmium
    7440-43-9
    NA
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    F019
    Wastewater treatment sludges from the chemical conversion coating of aluminum
    except from zirconium phosphating in aluminum can washing when such
    phosphating is an exclusive conversion coating process.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    F020, F021, F022, F023, F026
    Wastes (except wastewater and spent carbon from hydrogen chloride
    purification) from the production or manufacturing use (as a reactant,
    chemical intermediate, or component in a formulating process) of: (1) tri- or
    tetrachloro phenol, or of intermediates used to produce their pesticide
    derivatives, excluding wastes from the production of Hexa
    chloro phene from
    highly purified 2,4,5-trichloro
    phenol (i.e., F020); (2) penta
    chloro phenol, or
    of intermediates used to produce its derivatives (i.e., F021); (3) tetra
    -,
    penta-, or hexa chloro benzenes under alkaline conditions (i.e., F022)
    .
    and Wwastes (except wastewater and spent carbon from hydrogen chloride
    purification) from the production of materials on equipment previously used
    for the production or manufacturing use (as a reactant, chemical intermediate,
    or component in a formulating process) of: (1) tri- or tetra
    chloro phenols,
    excluding wastes from equipment used only for the production of Hexa
    chloro -
    phene from highly purified 2,4,5-trichloro
    phenol (F023) ; or (2) tetra -,
    penta-, or hexa chloro benzenes under alkaline conditions (i.e., F026).
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Penta
    chloro -
    NA
    0.000035
    0.001
    416
    dibenzo furans)
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    2,4,5-Tri chloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Tri chloro phenol
    88-06-2
    0.035
    7.4
    2,3,4,6-Tetra chloro -
    phenol
    58-90-2
    0.030
    7.4
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    F024
    Process wastes, including but not limited to, distillation residues, heavy
    ends, tars, and reactor clean-out wastes, from, the production of certain
    chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These
    chlorinated aliphatic hydrocarbons are those having carbon chain lengths
    ranging from one to and including five, with varying amounts and positions of
    chlorine substitution. (This listing does not include wastewaters, wastewater
    treatment sludges, spent catalysts, and wastes listed in Section 721.131 or
    721.132.).
    All F024 wastes
    NA
    CMBST
    CMBST
    2-Chloro -1,3-butadiene
    126-99-8
    0.057
    0.28
    3-Chloropropylene
    107-05-1
    0.036
    30
    1,1-Dichloroethane
    75-34-3
    0.059
    6.0
    1,2-Dichloroethane
    107-06-2
    0.21
    6.0
    1,2-Dichloropropane
    78-87-5
    0.85
    18
    cis-1,3-Dichloropropylen
    e
    10061-01-5
    0.036
    18
    trans-1,3-Dichloro -
    propylene
    10061-02-6
    0.036
    18
    bis(2-Ethylhexyl) -
    phthalate
    117-81-7
    0.28
    28
    Hexachloroethane
    67-72-1
    0.055
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    F025
    Condensed light ends from the production of certain chlorinated aliphatic
    hydrocarbons, by free radical catalyzed processes. These chlorinated
    aliphatic hydrocarbons are those having carbon chain lengths ranging from one
    up to and including five, with varying amounts and positions of chlorine
    substitution. F025
    --Light Ends Subcategory.
    Carbon tetrachloride
    56-23-5
    0.057
    6.0
    Chloroform
    67-66-3
    0.046
    6.0
    1,2-Dichloroethane
    107-06-2
    0.21
    6.0
    1,1-Dichloroethylene
    75-35-4
    0.025
    6.0
    Methylene chloride
    75-9-2
    0.089
    30
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloroethylene
    79-01-6
    0.054
    6.0
    Vinyl chloride
    75-01-4
    0.27
    6.0
    F025
    Spent filters and filter aids, and spent desiccant wastes from the production
    of certain chlorinated aliphatic hydrocarbons, by free radical catalyzed
    processes. These chlorinated aliphatic hydrocarbons are those having carbon
    chain lengths ranging from one to and including five, with varying amounts and
    positions of chlorine substitution. F025
    --Spent Filters/A ids and Desiccants
    Subcategory.
    Carbon tetrachloride
    56-23-5
    0.057
    6.0
    417
    Chloroform
    67-66-3
    0.046
    6.0
    Hexachlorobenzene
    118-74-1
    0.055
    10
    Hexachlorobutadiene
    87-68-3
    0.055
    5.6
    Hexachloroethane
    67-72-1
    0.055
    30
    Methylene chloride
    75-9-2
    0.089
    30
    1,1,2-Trichloroethane
    79-00-5
    0.054
    6.0
    Trichloroethylene
    79-01-6
    0.054
    6.0
    Vinyl chloride
    75-01-4
    0.27
    6.0
    F027
    Discarded unused formulations contianing tri
    -, tetra -, or penta chloro phenol or
    discarded unused formulations containing compounds derived from these chloro
    -
    phenols. (This listing does not include formulations containing hexa
    chloro -
    phene synthesized from prepurified 2,4,5-trichloro
    phenol as the sole
    component.)
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Penta
    chloro -
    dibenzo furans)
    NA
    0.000035
    0.001
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    2,3,4,6-Tetra chloro -
    phenol
    58-90-2
    0.030
    7.4
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    F028
    Residues resulting from the incineration or thermal treatment of soil
    contaminated with USEPA hazardous waste numbers F020, F021, F023, F026, and
    F027.
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Penta
    chloro -
    dibenzo furans)
    NA
    0.000035
    0.001
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    2,3,4,6-Tetra chloro -
    phenol
    58-90-2
    0.030
    7.4
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    F024
    Process wastes, including but not limited to, distillation residues, heavy
    ends, tars, and reactor clean-out wastes, from the production of certain
    chlorinated aliphatic hydro
    carbons by free radical catalyzed processes. These
    418
    chlorinated aliphatic hydro
    carbons are those having carbon chain lengths
    ranging from one to and including five, with varying amounts and positions of
    chlorine substitution. (This listing does not include wastewaters, wastewater
    treatment sludges, spent catalysts, and wastes listed in 35 Ill. Adm. Code
    721.131 or 721.132.)
    All F024 wastes
    NA
    INCIN
    INCIN
    2-Chloro-1,3-buta
    diene
    126-99-8
    0.057
    0.28
    3-Chloro propylene
    107-05-1
    0.036
    30
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,2-Dichloro propane
    78-87-5
    0.85
    18
    cis-1,3-Dichloro -
    propylene
    10061-01-5
    0.036
    18
    trans-1,3-Dichloro
    -
    propylene
    10061-02-6
    0.036
    18
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Hexachloro ethane
    67-72-1
    0.055
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    F025
    Condensed light ends from the production of certain chlorinated aliphatic
    hydrocarbons, by free radical catalyzed processes. These chlorinated
    aliphatic hydro carbons are those having carbon chain lengths ranging from one
    to and including five, with varying amounts and positions of chlorine
    substitution.
    F025 - Light Ends Subcategory
    Carbon tetra chloride
    56-23-6
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,1-Dichloro ethylene
    75-35-4
    0.025
    6.0
    Methylene chloride
    75-9-2
    0.089
    30
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Vinyl chloride
    75-01-4
    0.27
    6.0
    F025
    Spent filters and filter aids, and spent desiccant wastes from the production
    of certain chlorinated aliphatic hydro
    carbons, by free radical catalyzed
    processes. These chlorinated aliphatic hydro
    carbons are those having carbon
    chain lengths ranging from one to and including five, with varying amounts and
    positions of chlorine substitution.
    F025 - Spent Filters or Aids and Desiccants Subcategory
    Carbon tetra chloride
    56-23-5
    0.067
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro ethane
    67-72-1
    0.055
    30
    Methylene chloride
    75-9-2
    0.089
    30
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Vinyl chloride
    75-01-4
    0.27
    6.0
    F037
    Petroleum refinery primary oil/water/solids separation sludge
    --Any sludge
    generated from the gravitational separation of oil/water/solids during the
    storage or treatment of process wastewaters and oily cooling wastewaters from
    petroleum refineries. Such sludges include, but are not limited to, those
    generated in: oil/water/solids separators; tanks and impoundments; ditches
    and other conveyances; sumps; and stormwater units receiving dry weather flow.
    419
    Sludge generated in stormwater units that do not receive dry weather flow,
    sludges generated from non-contact once-through cooling waters segregated for
    treatment from other process or oily cooling waters, sludges generated in
    agressive biological treatment units as defined in 35 Ill. Adm. Code
    721.131(b)(2) (including sludges generated in one or more additional units
    after wastewaters have been treated in agressive biological treatment units)
    and K051 wastes are not included in this listing.
    Acenaphthene
    83-32-9
    0.059
    NA
    Anthracene
    120-12-7
    0.059
    3.4
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Chrysene
    218-01-9
    0.059
    3.4
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    Ethylbenzene
    100-41-4
    0.057
    10
    Fluorene
    86-73-7
    0.059
    NA
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    F038
    Petroleum refinery secondary (emulsified) oil/water/solids separation sludge
    or float generated from the physical or chemical separation of
    oil/water/solids in process wastewaters and oily cooling wastewaters from
    petroleum refineries. Such wastes include, but are not limited to, all
    sludges and floats generated in: induced air floatation (IAF) units, tanks
    and impoundments, and all sludges generated in DAF units. Sludges generated
    in stormwater units that do not receive dry weather flow, sludges generated
    from non-contact once-through cooling waters segregated for treatment from
    other process or oily cooling waters, sludges and floats generated in
    agressive biological treatment units as defined in 35 Ill. Adm. Code
    721.131(b)(2) (including sludges and floats generated in one or more
    additional units after wastewaters have been treated in agressive biological
    units) and F037, K048, and K051 are not included in this listing.
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Chrysene
    218-01-9
    0.059
    3.4
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    Ethylbenzene
    100-41-4
    0.057
    10
    Fluorene
    86-73-7
    0.059
    NA
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    420
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    F039
    Leachate (liquids that have percolated through land disposed wastes) resulting
    from the disposal of more than one restricted waste classified as hazardous
    under 728.Subpart D. (Leachate resulting from the disposal of one or more of
    the following USEPA hazardous wastes and no other hazardous wastes retains its
    USEPA hazardous waste numbers: F020, F021, F022, F026, F027, or F028.).
    Acenaphthylene
    208-96-8
    0.059
    3.4
    Acenaphthene
    83-32-9
    0.059
    3.4
    Acetone
    67-64-1
    0.28
    160
    Acetonitrile
    75-05-8
    5.6
    NA
    Acetophenone
    96-86-2
    0.010
    9.7
    2-Acetyl aminofluorene
    53-96-3
    0.059
    140
    Acrolein
    107-02-8
    0.29
    NA
    Acrylonitrile
    107-13-1
    0.24
    84
    Aldrin
    309-00-2
    0.021
    0.066
    4-Aminobiphenyl
    92-67-1
    0.13
    NA
    Aniline
    62-53-3
    0.81
    14
    Anthracene
    120-12-7
    0.059
    3.4
    Aramite
    140-57-8
    0.36
    NA
    alpha-BHC
    319-84-6
    0.00014
    0.066
    beta-BHC
    319-85-7
    0.00014
    0.066
    delta-BHC
    319-86-8
    0.023
    0.066
    gamma-BHC
    58-89-9
    0.0017
    0.066
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Benzo(g,h,i) perylene
    191-24-2
    0.0055
    1.8
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Bromodichloro methane
    75-27-4
    0.35
    15
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    4-Bromo phenyl phenyl
    ether
    101-55-3
    0.055
    15
    n-Butyl alcohol
    71-36-3
    5.6
    2.6
    Butyl benzyl phthalate
    85-68-7
    0.017
    28
    2-sec-Butyl-4,6-dinitro
    -
    phenol (Dinoseb)
    88-85-7
    0.066
    2.5
    Carbon disulfide
    75-15-0
    3.8
    NA
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033
    0.26
    p-Chloro aniline
    106-47-8
    0.46
    16
    Chloro benzene
    108-90-7
    0.057
    6.0
    Chloro benzilate
    510-15-6
    0.10
    NA
    2-Chloro-1,3-buta
    diene
    126-99-8
    0.057
    NA
    Chloro dibromo methane
    124-48-1
    0.057
    15
    Chloro ethane
    75-00-3
    0.27
    6.0
    bis(2-Chloro ethoxy) -
    methane
    111-91-1
    0.036
    7.2
    421
    bis(2-Chloro ethyl) ether
    111-44-4
    0.033
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    bis(2-Chloro isopropyl) -
    ether
    108-60-1 39638-
    32-9
    0.055
    7.2
    p-Chloro-m-cresol
    59-50-7
    0.018
    14
    Chloro methane (Methyl
    chloride)
    74-87-3
    0.19
    30
    2-Chloro naphthalene
    91-58-7
    0.055
    5.6
    2-Chloro phenol
    95-57-8
    0.044
    5.7
    3-Chloro propylene
    107-05-1
    0.036
    30
    Chrysene
    218-01-9
    0.059
    3.4
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol
    (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol
    (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    Cyclohexanone
    108-94-1
    0.36
    NA
    1,2-Dibromo-3-chloro
    -
    propane
    96-12-8
    0.11
    15
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    Dibromo methane
    74-95-3
    0.11
    15
    2,4-D (2,4-Dichloro
    -
    phenoxy acetic acid)
    94-75-7
    0.72
    10
    o,p'-DDD
    53-19-0
    0.023
    0.0870.087
    p,p'-DDD
    72-54-8
    0.023
    0.087
    o,p'-DDE
    3424-82-6
    0.031
    0.087
    p,p'-DDE
    72-55-9
    0.031
    0.087
    o,p'-DDT
    789-02-6
    0.0039
    0.087
    p,p'-DDT
    50-29-3
    0.0039
    0.087
    Dibenz (a,h)anthra cene
    53-70-3
    0.055
    8.2
    Dibenz(a,e)pyrene
    192-65-4
    0.061
    NA
    m-Dichloro benzene
    541-73-1
    0.036
    6.0
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Dichloro difluoro methane
    75-71-8
    0.23
    7.2
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,1-Dichloro ethylene
    75-35-4
    0.025
    6.0
    trans-1,2-Dichloro
    -
    ethylene
    156-60-5
    0.054
    30
    2,4-Dichloro phenol
    120-83-2
    0.044
    14
    2,6-Dichloro phenol
    87-65-0
    0.044
    14
    1,2-Dichloro propane
    78-87-5
    0.85
    18
    cis-1,3-Dichloro -
    propylene
    10061-01-5
    0.036
    18
    trans-1,3-Dichloro
    -
    propylene
    10061-02-6
    0.036
    18
    Dieldrin
    60-57-1
    0.017
    0.13
    Diethyl phthalate
    84-66-2
    0.20
    28
    2-4-Dimethyl phenol
    105-67-9
    0.036
    14
    Dimethyl phthalate
    131-11-3
    0.047
    28
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    1,4-Dinitro benzene
    100-25-4
    0.32
    2.3
    4,6-Dinitro-o-cresol
    534-52-1
    0.28
    160
    2,4-Dinitro phenol
    51-28-5
    0.12
    160
    2,4-Dinitro toluene
    121-14-2
    0.32
    140
    422
    2,6-Dinitro toluene
    606-20-2
    0.55
    28
    Di-n-octyl phthalate
    117-84-0
    0.017
    28
    Di-n-propyl nitros amine
    621-64-7
    0.40
    14
    1,4-Dioxane
    123-91-1
    NA12.0
    170
    Diphenyl amine (difficult
    to distinguish from
    diphenyl nitros amine)
    122-39-4
    0.92
    13NA
    Diphenyl nitros amine
    (difficult to
    distinguish from
    diphenyl amine)
    86-30-6
    0.92
    NA
    1,2-Diphenyl hydrazine
    122-66-7
    0.087
    NA
    Disulfoton
    298-04-4
    0.017
    6.2
    Endosulfan I
    939-98-8
    0.023
    0.066
    Endosulfan II
    33213-6-5
    0.029
    0.13
    Endosulfan sulfate
    1-31-07-8 1031-
    07-8
    0.029
    0.13
    Endrin
    72-20-8
    0.0028
    0.13
    Endrin aldehyde
    7421-93-4
    0.025
    0.13
    Ethyl acetate
    141-78-6
    0.34
    33
    Ethyl cyanide (Propane
    -
    nitrile)
    107-12-0
    0.24
    360
    Ethyl benzene
    100-41-4
    0.057
    10
    Ethyl ether
    60-29-7
    0.12
    160
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Ethyl methacrylate
    97-63-2
    0.14
    160
    Ethylene oxide
    75-21-8
    0.12
    NA
    Famphur
    52-85-7
    0.017
    15
    Fluoranthene
    206-44-0
    0.068
    3.4
    Fluorene
    86-73-7
    0.059
    3.4
    Heptachlor
    76-44-8
    0.0012
    0.066
    Heptachlor epoxide
    1024-57-3
    0.016
    0.066
    Hexachloro benzene
    118-74-1
    0.055
    10
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    Hexachloro ethane
    67-72-1
    0.055
    30
    Hexachloro propylene
    1888-71-7
    0.035
    30
    Indeno (1,2,3-c,d)
    pyrene
    193-39-5
    0.0055
    3.4
    Iodomethane
    74-88-4
    0.19
    65
    Isobutyl alcohol
    78-83-1
    5.6
    170
    Isodrin
    465-73-6
    0.021
    0.066
    Isosafrole
    120-58-1
    0.081
    2.6
    Kepone
    143-50-8
    0.0011
    0.13
    Methacrylo nitrile
    126-98-7
    0.24
    84
    Methanol
    67-56-1
    5.6
    NA
    Methapyrilene
    91-80-5
    0.081
    1.5
    Methoxychlor
    72-43-5
    0.25
    0.18
    3-Methyl cholanthrene
    56-49-5
    0.0055
    15
    4,4-Methylene bis(2-
    chloro aniline)
    101-14-4
    0.50
    30
    Methylene chloride
    75-09-2
    0.089
    30
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    Methyl isobutyl ketone
    108-10-1
    0.14
    33
    Methyl methacrylate
    80-62-6
    0.14
    160
    423
    Methyl methan sulfonate
    66-27-3
    0.018
    NA
    Methyl parathion
    298-00-0
    0.014
    4.6
    Naphthalene
    91-20-3
    0.059
    5.6
    2-Naphthylamine
    91-59-8
    0.52
    NA
    p-Nitro aniline
    100-01-6
    0.028
    28
    Nitrobenzene
    98-95-3
    0.068
    14
    5-Nitro-o-toluidine
    99-55-8
    0.32
    28
    p-Nitro phenol
    100-02-7
    0.12
    29
    N-Nitroso diethyl amine
    55-18-5
    0.40
    28
    N-Nitroso dimethyl amine
    62-75-9
    0.40
    NA
    N-Nitroso-di-n-butyl
    -
    amine
    924-16-3
    0.40
    17
    N-Nitroso methyl ethyl-
    amine
    10595-95-6
    0.40
    2.3
    N-Nitroso morpholine
    59-89-2
    0.40
    2.3
    N-Nitroso piperidine
    100-75-4
    0.013
    35
    N-Nitroso pyrrolidine
    930-55-2
    0.013
    35
    Parathion
    56-38-2
    0.014
    4.6
    Total PCBs
    (sum of all PCB isomers,
    or all Aroclors)
    1336-36-3
    0.10
    10
    Pentachloro benzene
    608-93-5
    0.055
    10
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PcCDFs PeCDFs (All Penta -
    chloro dibenzo furans)
    NA
    0.000035
    0.001
    Pentachloro nitrobenzene
    82-68-8
    0.055
    4.8
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    Phenacetin
    62-44-2
    0.081
    16
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Phorate
    298-02-2
    0.021
    4.6
    Phthalic anhydride
    85-44-9
    0.055
    NA
    Pronamide
    23950-58-5
    0.093
    1.5
    Pyrene
    129-00-0
    0.067
    8.2
    Pyridine
    110-86-1
    0.014
    16
    Safrole
    94-59-7
    0.081
    22
    Silvex (2,4,5-TP)
    93-72-1
    0.72
    7.9
    2,4,5-T
    93-76-5
    0.72
    7.9
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    1,1,1,2-Tetra chloro -
    ethane
    630-20-6
    0.057
    6.0
    1,1,2,2-Tetra chloro -
    ethane
    79-34-6
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    2,3,4,6-Tetra chloro -
    phenol
    58-90-2
    0.030
    7.4
    Toluene
    108-88-3
    0.080
    10
    Toxaphene
    8001-35-2
    0.0095
    2.6
    Bromoform (Tribromo -
    methane)
    75-25-2
    0.63
    15
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Trichloro monofluoro -
    75-69-4
    0.020
    30
    424
    methane
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    1,2,3-Trichloro propane
    96-18-4
    0.85
    30
    1,1,2-Trichloro-1,2,2-
    trifluoro ethane
    76-13-1
    0.057
    30
    tris(2,3-Dibromo propyl)
    phosphate
    126-72-7
    0.11
    NA
    Vinyl chloride
    75-01-4
    0.27
    6.0
    Xylenes-mixed isomers
    (sum or o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    Barium
    7440-39-3
    1.2
    7.6 mg/l TCLP
    Beryllium
    7440-41-7
    0.82
    NA
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    NA
    Fluoride
    16964-48-8
    35
    NA
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Mercury
    7439-97-6
    0.15
    0.025 mg/l
    TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    Silver
    7440-22-4
    0.43
    0.30 mg/l TCLP
    Sulfide
    8496-25-8
    14
    NA
    Thallium
    7440-28-0
    1.4
    NA
    Vanadium
    7440-62-2
    4.3
    NA
    K001
    Bottom sediment sludge from the treatment of wastewaters from wood preserving
    processes that use creosote or penta
    chloro phenol.
    Naphthalene
    91-20-3
    0.059
    5.6
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    Phenanthrene
    85-01-8
    0.059
    5.6
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Lead
    7439-92-1
    0.690.37 mg/l
    TCLP
    0.37 mg/l TCLP
    K002
    Wastewater treatment sludge from the production of chrome yellow and orange
    pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K003
    Wastewater treatment sludge from the production of molybdate orange pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K004
    Wastewater treatment sludge from the production of zinc yellow pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    425
    K005
    Wastewater treatment sludge from the production of chrome green pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.25
    590
    K006
    Wastewater treatment sludge from the production of chrome oxide green pigments
    (anhydrous).
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K006
    Wastewater treatment sludge from the production of chrome oxide green pigments
    (hydrated).
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    NA
    K007
    Wastewater treatment sludge from the production of iron blue pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.25
    590
    K008
    Oven residue from the production of chrome oxide green pigments.
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K009
    Distillation bottoms from the production of acetaldehyde from ethylene.
    Chloro form
    67-66-3
    0.046
    6.0
    K010
    Distillation side cuts from the production of acetaldehyde from ethylene.
    Chloro form
    67-66-3
    0.046
    6.0
    K011
    Bottom stream from the wastewater stripper in the production of acrylonitrile.
    Acetonitrile
    75-05-8
    5.6
    1.838
    Acrylonitrile
    107-13-1
    0.24
    84
    Acrylamide
    79-06-1
    19
    23
    Benzene
    71-43-2
    0.14
    10
    Cyanide (Total)
    57-12-5
    1.2
    590
    K013
    Bottom stream from the acetonitrile column in the production of acrylonitrile.
    Acetonitrile
    75-05-8
    5.6
    1.838
    Acrylonitrile
    107-13-1
    0.24
    84
    Acrylamide
    79-06-1
    19
    23
    Benzene
    71-43-2
    0.14
    10
    Cyanide (Total)
    57-12-5
    1.2
    590
    K014
    Bottoms from the acetonitrile purification column in the production of
    acrylonitrile.
    Acetonitrile
    75-05-8
    5.6
    1.838
    Acrylonitrile
    107-13-1
    0.24
    84
    Acrylamide
    79-06-1
    19
    23
    Benzene
    71-43-2
    0.14
    10
    Cyanide (Total)
    57-12-5
    1.2
    590
    426
    K015
    Still bottoms from the distillation of benzyl chloride.
    Anthracene
    120-12-7
    0.059
    3.4
    Benzal chloride
    98-87-3
    0.055
    6.0
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Phenanthrene
    85-01-8
    0.059
    5.6
    Toluene
    108-88-3
    0.080
    10
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    85.0 mg/l TCLP
    K016
    Heavy ends or distillation residues from the production of carbon tetra
    -
    chloride.
    Hexachloro benzene
    118-74-1
    0.055
    10
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    Hexachloro ethane
    67-72-1
    0.055
    30
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    K017
    Heavy ends (still bottoms) from the purification column in the production of
    epichloro hydrin.
    bis(2-Chloro ethyl) ether
    111-44-4
    0.033
    6.0
    1,2-Dichloro propane
    78-87-5
    0.85
    18
    1,2,3-Trichloro propane
    96-18-4
    0.85
    30
    K018
    Heavy ends from the fractionation column in ethyl chloride production.
    Chloro ethane
    75-00-3
    0.27
    6.0
    Chloro methane
    74-87-3
    0.19
    NA
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro ethane
    67-72-1
    0.055
    30
    Pentachloro ethane
    76-01-7
    NA
    6.0
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    K019
    Heavy ends from the distillation of ethylene dichloride in ethylene dichloride
    production.
    bis(2-Chloro ethyl) ether
    111-44-4
    0.033
    6.0
    Chloro benzene
    108-90-7
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    NA
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    Fluorene
    86-73-7
    0.059
    NA
    Hexachloro ethane
    67-72-1
    0.055
    30
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    NA
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    427
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    K020
    Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer
    production.
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,1,2,2-Tetra chloro -
    ethane
    79-34-6
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    K021
    Aqueous spent antimony catalyst waste from fluoro
    methanes production.
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    K021
    Aqueous spent antimony catalyst waste from fluoro
    methanes production.
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    K022
    Distillation bottom tars from the production of phenol or acetone from cumene.
    Toluene
    108-88-3
    0.080
    10
    Acetophenone
    96-86-2
    0.010
    9.7
    Diphenylamine (difficult
    to distinguish from
    diphenyl nitros amine)
    122-39-4
    0.92
    13
    Diphenyl nitros amine
    (difficult to
    distinguish from
    diphenyl amine)
    86-30-6
    0.92
    13
    Phenol
    108-95-2
    0.039
    6.2
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    K023
    Distillation light ends from the production of phthalic anhydride from
    naphthalene.
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    100-21-0
    0.055
    28
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    85-44-9
    0.055
    28
    K024
    Distillation bottoms from the production of phthalic anhydride from
    naphthalene.
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    100-21-0
    0.055
    28
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    85-44-9
    0.055
    28
    428
    K025
    Distillation bottoms from the production of nitro
    benzene by the nitration of
    benzene.
    NA
    NA
    LLEXT fb SSTRP
    fb CARBN; or
    INCINCMBST
    INCINCMBST
    K026
    Stripping still tails from the production of methyl ethyl pyridines.
    NA
    NA
    INCINCMBST
    INCINCMBST
    K027
    Centrifuge and distillation residues from the toluene diisocyanate production.
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K028
    Spent catalyst from the hydro
    chlorinator rea ctor in the production of 1,1,1-
    trichloro ethane.
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    trans-1,2-Dichloro
    -
    ethylene
    156-60-5
    0.054
    30
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro ethane
    67-72-1
    0.055
    30
    Pentachloro ethane
    76-01-7
    NA
    6.0
    1,1,1,2-Tetra chloro -
    ethane
    630-20-6
    0.057
    6.0
    1,1,2,2-Tetra chloro -
    ethane
    79-34-6
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Cadmium
    7440-43-9
    0.69
    NA
    Chromium(Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    K029
    Waste from the product steam stripper in the production of 1,1,1-trichloro
    -
    ethane.
    Chloro form
    67-66-3
    0.046
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,1-Dichloro ethylene
    75-35-4
    0.025
    6.0
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    Vinyl chloride
    75-01-4
    0.27
    6.0
    K030
    Column bodies or heavy ends from the combined production of trichloro
    ethylene
    and perchloro ethylene.
    o-Dichloro benzene
    95-50-1
    0.088
    NA
    p-Dichloro benzene
    106-46-7
    0.090
    NA
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro ethane
    67-72-1
    0.055
    30
    Hexachloro propylene
    1888-71-7
    NA
    30
    Pentachloro benzene
    608-93-5
    NA
    10
    Pentachloro ethane
    76-01-7
    NA
    6.0
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    429
    K031
    By-product salts generated in the production of MSMA and cacodylic acid.
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    K032
    Wastewater treatment sludge from the production of chlordane.
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033
    0.26
    Heptachlor
    76-44-8
    0.0012
    0.066
    Heptachlor epoxide
    1024-57-3
    0.016
    0.066
    K033
    Wastewater and scrub water from the chlorination of cyclo
    pentadiene in the
    production of chlordane.
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    K034
    Filter solids from the filtration of hexa
    chloro cyclopentadiene in the
    production of chlordane.
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    K035
    Wastewater treatment sludges generated in the production of creosote.
    Acenaphthene
    83-32-9
    NA
    3.4
    Anthracene
    120-12-7
    NA
    3.4
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Chrysene
    218-01-9
    0.059
    3.4
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol
    (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol
    (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    Dibenz (a,h)anthra cene
    53-70-3
    NA
    8.2
    Fluoranthene
    206-44-0
    0.068
    3.4
    Fluorene
    86-73-7
    NA
    3.4
    Indeno(1,2,3-cd) pyrene
    193-39-5
    NA
    3.4
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    K036
    Still bottoms from toluene reclamation distillaiton in the production of
    disulfoton.
    Disulfoton
    298-04-4
    0.017
    6.2
    K037
    Wastewater treatment sludges from the production of disulfoton.
    Disulfoton
    298-04-4
    0.017
    6.2
    Toluene
    108-88-3
    0.080
    10
    430
    K038
    Wastewater from the washing and stripping of phorate production.
    Phorate
    298-02-2
    0.021
    4.6
    K039
    Filter cake from the filtration of diethyl
    phosphorodithioic acid in the
    production of phorate.
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K040
    Wastewater treatment sludge from the production of phorate.
    Phorate
    298-02-2
    0.021
    4.6
    K041
    Wastewater treatment sludge from the production of toxaphene.
    Toxaphene
    8001-35-2
    0.0095
    2.6
    K042
    Heavy ends or distillation residues from the distillation of tetra
    chloro -
    benzene in the production of 2,4,5-T.
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Pentachloro benzene
    608-93-5
    0.055
    10
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    K043
    2,6-Dichloro phenol waste from the production of 2,4-D.
    2,4-Dichloro phenol
    120-83-2
    0.044
    14
    2,6-Dichloro phenol
    187-65-0
    0.044
    14
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    2,3,4,6-Tetra chloro -
    phenol
    58-90-2
    0.030
    7.4
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Penta
    chloro -
    dibenzo furans)
    NA
    0.000035
    0.001
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    K044
    Wastewater treatment sludges from the manufacturing and processing of
    explosives.
    NA
    NA
    DEACT
    DEACT
    K045
    Spent carbon from the treatment of wastewater containing explosives.
    NA
    NA
    DEACT
    DEACT
    K046
    431
    Wastewater treatment sludges from the manufacturing, formulation and loading
    of lead-based initiating compounds.
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K047
    Pink or red water from TNT operations.
    NA
    NA
    DEACT
    DEACT
    K048
    Dissolved air flotation (DAF) float from the petroleum refining industry.
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Chrysene
    218-01-9
    0.059
    3.4
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    Ethylbenzene
    100-41-4
    0.057
    10
    Fluorene
    86-73-7
    0.059
    NA
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-33
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    K049
    Slop oil emulsion solids from the petroleum refining industry.
    Anthracene
    120-12-7
    0.059
    3.4
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Carbon disulfide
    75-15-0
    3.8
    NA
    Chrysene
    2218-01-9
    0.059
    3.4
    2,4-Dimethyl phenol
    105-67-9
    0.036
    NA
    Ethylbenzene
    100-41-4
    0.057
    10
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    K050
    Heat exchanger bundle cleaning sludge from the petroleum refining industry.
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Phenol
    108-95-2
    0.039
    6.2
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    432
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    K051
    API separator sludge from the petroleum refining industry.
    Acenaphthene
    83-32-9
    0.059
    NA
    Anthracene
    120-12-7
    0.059
    3.4
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    Chrysene
    2218-01-9
    0.059
    3.4
    Di-n-butyl phthalate
    105-67-9
    0.057
    28
    Ethylbenzene
    100-41-4
    0.057
    10
    Fluorene
    86-73-7
    0.059
    NA
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.08
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    K052
    Tank bottoms (leaded) from the petroleum refining industry.
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol
    (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol
    (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    2,4-Dimethyl phenol
    105-67-9
    0.036
    NA
    Ethylbenzene
    100-41-4
    0.057
    10
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Toluene
    108-88-3
    0.08
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Lead
    7439-92-1
    0.69
    NA
    Nickel
    7440-02-0
    NA
    5.0 mg/l TCLP
    K060
    Ammonia still lime sludge from coking operations.
    Benzene
    71-43-2
    0.14
    10
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Naphthalene
    91-20-3
    0.059
    5.6
    433
    Phenol
    108-95-2
    0.039
    6.2
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    K061
    Emission control dust or sludge from the primary production of steel in
    electric furnaces.
    Antimony
    7440-36-0
    NA
    2.1 mg/l TCLP
    Arsenic
    7440-38-2
    NA
    5.0 mg/l TCLP
    Barium
    7440-39-3
    NA
    7.6 mg/l TCLP
    Beryllium
    7440-41-7
    NA
    0.014 mg/l
    TCLP
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Selenium
    7782-49-2
    NA
    0.16 mg/l TCLP
    Silver
    7440-22-4
    NA
    0.30 mg/l TCLP
    Thallium
    NA7440-28-0
    NA
    0.078 mg/l
    TCLP
    Zinc
    7440-66-6
    NA
    5.3 mg/l TCLP
    K062
    Spent pickle liquor generated by steel finishing operations of facilities
    within the iron and steel industry (SIC Codes 331 and 332).
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    NA
    K069
    Emission control dust or sludge from secondary lead smelting. - Calcium
    sulfate (Low Lead) Subcategory
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K069
    Emission control dust or sludge from secondary lead smelting. - Non-Calcium
    sulfate (High Lead) Subcategory
    NA
    NA
    NA
    RLEAD
    K071
    K071 (Brine purification muds from the mercury cell process in chlorine
    production, where separately prepurified brine is not used) nonwastewaters
    that are residues from RMERC.
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    K071
    K071 (Brine purification muds from the mercury cell process in chlorine
    production, where separately prepurified brine is not used) nonwastewaters
    that are not residues from RMERC.
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    K071
    All K071 wastewaters.
    Mercury
    7439-97-6
    0.15
    NA
    K073
    Chlorinated hydro
    carbon waste from the purification step of the diaphragm cell
    process using graphite anodes in chlorine production.
    434
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Hexachloro ethane
    67-72-1
    0.055
    30
    Tetrachloro ethylene
    127-18-4
    0.0580.056
    6.0
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    K083
    Distillation bottoms from aniline production.
    Aniline
    62-53-3
    0.81
    14
    Benzene
    71-43-2
    0.14
    10
    Cyclohexanone
    108-94-1
    0.36
    NA
    Diphenyl amine
    (difficult to
    distinguish from
    diphenyl nitros amine)
    122-39-4
    0.92
    13
    Diphenyl nitros amine
    (difficult to
    distinguish from
    diphenyl amine)
    86-30-6
    0.92
    13
    Nitrobenzene
    98-95-3
    0.068
    14
    Phenol
    108-95-2
    0.039
    6.2
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    K084
    Wastewater treatment sludges generated during the production of veterinary
    pharmaceuticals from arsenic or organo-arsenic compounds.
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    K085
    Distillation or fractionation column bottoms from the production of chloro
    -
    benzenes.
    Benzene
    71-43-2
    0.14
    10
    Chloro benzene
    108-90-7
    0.057
    6.0
    m-Dichloro benzene
    541-73-1
    0.036
    6.0
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Total PCBs
    (sum of all PCB isomers,
    or all Aroclors)
    1336-36-3
    0.10
    10
    Pentachloro benzene
    608-93-5
    0.055
    10
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    K086
    Solvent wastes and sludges, caustic washes and sludges, or water washes and
    sludges from cleaning tubs and equipment used in the formulation of ink from
    pigments, driers, soaps, and stabilizers containing chromium and lead.
    Acetone
    67-64-1
    0.28
    160
    Acetophenone
    96-86-2
    0.010
    9.7
    bis(2-Ethyl hexyl)
    phthalate
    117-81-7
    0.28
    28
    n-Butyl alcohol
    71-36-3
    5.6
    2.6
    Butylbenzyl phthalate
    85-68-7
    0.017
    28
    Cyclohexanone
    108-94-1
    0.36
    NA
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    Diethyl phthalate
    84-66-2
    0.20
    28
    Dimethyl phthalate
    131-11-3
    0.047
    28
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    Di-n-octyl phthalate
    117-84-0
    0.017
    28
    435
    Ethyl acetate
    141-78-6
    0.34
    33
    Ethylbenzene
    100-41-4
    0.057
    10
    Methanol
    67-56-1
    5.6
    NA
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    Methyl isobutyl ketone
    108-10-1
    0.14
    33
    Methylene chloride
    75-09-2
    0.089
    30
    Naphthalene
    91-20-3
    0.059
    5.6
    Nitrobenzene
    98-95-3
    0.068
    14
    Toluene
    108-88-3
    0.080
    10
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K087
    Decanter tank tar sludge from coking operations.
    Acenaphthylene
    208-96-8
    0.059
    3.4
    Benzene
    71-43-2
    0.14
    10
    Chrysene
    218-01-9
    0.059
    3.4
    Fluoranthene
    206-44-0
    0.068
    3.4
    Indeno l(1,2,3-cd) pyrene
    193-39-5
    0.0055
    3.4
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenanthrene
    85-01-8
    0.059
    5.6
    Toluene
    108-88-3
    0.080
    10
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K088
    Spent potliners from primary aluminum reduction.
    Acenaphthene
    83-32-9
    0.059
    3.4
    Anthracene
    120-12-7
    0.059
    3.4
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Benzo(b)fluoranthene
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    207-08-9
    0.11
    6.8
    Benzo(g,h,i)perylene
    191-24-2
    0.0055
    1.8
    Chrysene
    218-01-9
    0.09
    34
    Dibenz(a,h)anthracene
    53-70-3
    0.055
    8.2
    Fluoranthene
    206-44-0
    0.068
    3.4
    Indeno(1,2,3 -c,d)pyrene
    193-39-5
    0.0055
    3.4
    Phenanthrene
    85-01-8
    0.059
    5.6
    Pyrene
    129-00-0
    0.067
    8.2
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    Barium
    7440-39-3
    1.2
    7.6 mg/l TCLP
    Beryllium
    7440-41-7
    0.82
    0.014 mg/l
    TCLP
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Mercury
    7439-97-6
    0.15
    0.025 mg/l
    TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    Silver
    7440-22-4
    0.43
    0.30 mg/l TCLP
    436
    Cyanide (Total)
    7
    57-12-5
    1.2
    590
    Cyanide (Amenable)
    7
    57-12-5
    0.86
    30
    Fluoride
    16984-48-8
    35
    48 mg/l TCLP
    K093
    Distillation light ends from the production of phthalic anhydride from ortho-
    xylene.
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    100-21-0
    0.055
    28
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    85-44-9
    0.055
    28
    K094
    Distillation bottoms from the production of phthalic anhydride from ortho-
    xylene.
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    100-21-0
    0.055
    28
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    85-44-9
    0.055
    28
    K095
    Distillation bottoms from the production of 1,1,1-trichloro
    ethane.
    Hexachloro ethane
    67-72-1
    0.055
    30
    Pentachloro ethane
    76-01-7
    0.055
    6.0
    1,1,1,2-Tetra chloro -
    ethane
    630-20-6
    0.057
    6.0
    1,1,2,2-Tetra chloro -
    ethane
    79-34-6
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    K096
    Heavy ends from the heavy ends column from the production of 1,1,1-trichloro
    -
    ethane.
    m-Dichloro benzene
    541-73-1
    0.036
    6.0
    Pentachloro ethane
    76-01-7
    0.055
    6.0
    1,1,1,2-Tetra chloro -
    ethane
    630-20-6
    0.057
    6.0
    1,1,2,2-Tetra chloro -
    ethane
    79-34-6
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    K097
    Vacuum stripper discharge from the chlordane chlorinator in the production of
    chlordane.
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033
    0.26
    Heptachlor
    76-44-8
    0.0012
    0.066
    Heptachlor epoxide
    1024-57-3
    0.016
    0.0680.066
    437
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    K098
    Untreated process wastewater from the production of toxaphene.
    Toxaphene
    8001-35-2
    0.0095
    2.6
    K099
    Untreated wastewater from the production of 2,4-D.
    2,4-Dichloro phenoxy-
    acetic acid
    94-75-7
    0.72
    10
    HxCDDs (All Hexa chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexa chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    PeCDDs (All Penta
    chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Penta
    chloro -
    dibenzo furans)
    NA
    0.000035
    0.001
    TCDDs (All Tetra chloro -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetra chloro -
    dibenzo furans)
    NA
    0.000063
    0.001
    K100
    Waste leaching solution from acid leaching of emission control dust or sludge
    from secondary lead smelting.
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    K101
    Distillation tar residues from the distillation of aniline-based compounds in
    the production of veterinary pharmaceuticals from arsenic or organo-arsenic
    compounds.
    o-Nitro aniline
    88-74-4
    0.27
    14
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    Cadmium
    7440-43-9
    0.69
    NA
    Lead
    7439-92-1
    0.69
    NA
    Mercury
    7439-97-6
    0.15
    NA
    K102
    Residue from the use of activated carbon for decolorization in the production
    of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.
    o-Nitro phenol
    88-75-5
    0.028
    13
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    Cadmium
    7440-43-9
    0.69
    NA
    Lead
    7439-92-1
    0.69
    NA
    Mercury
    7439-97-6
    0.15
    NA
    K103
    Process residues from aniline extraction from the production of aniline.
    Aniline
    62-53-3
    0.81
    14
    Benzene
    71-43-2
    0.14
    10
    2,4-Dinitro phenol
    51-28-5
    0.12
    160
    Nitrobenzene
    98-95-3
    0.068
    14
    Phenol
    108-95-2
    0.039
    6.2
    K104
    Combined wastewater streams generated from nitro
    benzene or aniline production.
    Aniline
    62-53-3
    0.81
    14
    438
    Benzene
    71-43-2
    0.14
    10
    2,4-Dinitro phenol
    51-28-5
    0.12
    160
    Nitrobenzene
    98-95-3
    0.068
    14
    Phenol
    108-95-2
    0.039
    6.2
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    K105
    Separated aqueous stream from the reactor product washing step in the
    production of chloro
    benzenes.
    Benzene
    71-43-2
    0.14
    10
    Chloro benzene
    108-90-7
    0.057
    6.0
    2-Chloro phenol
    95-57-8
    0.044
    5.7
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Phenol
    108-95-2
    0.039
    6.2
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    K106
    K106 (wastewater treatment sludge from the mercury cell process in chlorine
    production) nonwastewaters that contain greater than or equal to 260 mg/kg
    total mercury.
    Mercury
    7439-97-6
    NA
    RMERC
    K106
    K106 (wastewater treatment sludge from the mercury cell process in chlorine
    production) nonwastewaters that contain less than 260 mg/kg total mercury that
    are residues from RMERC.
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    K106
    Other K106 nonwastewaters that contain less than 260 mg/kg total mercury and
    are not residues from RMERC.
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    K106
    All K106 wastewaters.
    Mercury
    7439-97-6
    0.15
    NA
    K107
    Column bottoms from product separation from the production of 1,1-dimethyl
    -
    hydrazine (UDMH) from carboxylic acid hydrazides.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    CARBN; or
    BIODG fb CARBN
    INCINCMBST
    K108
    Condensed column overheads from product separation and condensed reactor vent
    gases from the production of 1,1-dimethyl
    hydrazine (UDMH) from ca
    rboxylic acid
    hydrazides.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    CARBN; or
    BIODG fb CARBN
    INCINCMBST
    K109
    Spent filter cartridges from product purification from the production of 1,1-
    dimethyl hydrazine (UDMH) from carboxylic acid hydrazides.
    NA
    NA
    INCINCMBST; or
    INCINCMBST
    439
    CHOXD fb
    CARBN; or
    BIODG fb CARBN
    K110
    Condensed column overheads from intermediate separation from the production of
    1,1-dimethyl hydrazine (UDMH) from carboxylic acid hydrazides.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    CARBN; or
    BIODG fb CARBN
    INCINCMBST
    K111
    Product washwaters from the production of dinitro
    toluene via nitration of
    toluene
    2,4-Dinitro toluene
    121-1-1
    0.32
    140
    2,6-Dinitro toluene
    606-20-2
    0.55
    28
    K112
    Reaction by-product water from the drying column in the production of
    toluenediamine via hydro
    genation of dinitro
    toluene.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    CARBN; or
    BIODG fb CARBN
    INCINCMBST
    K113
    Condensed liquid light ends from the purification of toluenediamine in the
    production of toluenediamine via hydro
    genation of dinitro
    toluene.
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K114
    Vicinals from the purification of toluenediamine in the production of
    toluenediamine via hydro
    genation of dinitro
    toluene.
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K115
    Heavy ends from the purification of toluenediamine in the production of
    toluenediamine via hydro
    genation of dinitro
    toluene.
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K116
    Organic condensate from the solvent recovery column in the production of
    toluene diisocyanate via phosgenation of toluenediamine.
    NA
    NA
    CARBN; or
    INCINCMBST
    CMBST
    K117
    Wastewater from the reactor vent gas scrubber in the production of ethylene
    dibromide via bromination of ethene.
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    Chloro form
    67-66-3
    0.046
    6.0
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    K118
    440
    Spent absorbent solids from purification of ethylene dibromide in the
    production of ethylene dibromide via bromination of ethene.
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    Chloro form
    67-66-3
    0.046
    6.0
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    K123
    Process wastewater (including supernates, filtrates, and washwaters) from the
    production of ethylene
    bisdithio carbamic acid and its salts.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN)
    INCINCMBST
    K124
    Reactor vent scrubber water from the production of ethylene
    bisdithio carbamic
    acid and its salts.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN)
    INCINCMBST
    K125
    Filtration, evaporation, and centrifugation solids from the production of
    ethylene bisdithio carbamic acid and its salts.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN)
    INCINCMBST
    K126
    Baghouse dust and floor sweepings in milling and packaging operations from the
    production or formulation of ethylene
    bisdithio carbamic acid and its salts.
    NA
    NA
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN)
    INCINCMBST
    K131
    Wastewater from the reactor and spent sulfuric acid from the acid dryer from
    the production of methyl bromide.
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    K132
    Spent absorbent and wastewater separator solids from the production of methyl
    bromide.
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    K136
    Still bottoms from the purification of ethylene dibromide in the production of
    ethylene dibromide via bromination of ethene.
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    Chloro form
    67-66-3
    0.046
    6.0
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    K141
    441
    Process residues from the recovery of coal tar, including, but not limited to,
    collecting sump residues from the production of coke or the recovery of coke
    by-products produced from coal. This listing does not include K087 (decanter
    tank tar sludge from coking operations).
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-2-8
    0.061
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    8.2
    Indeno(1,2,3-cd) pyrene
    193-39-5
    0.0055
    3.4
    K142
    Tar storage tank residues from the production of coke from coal or from the
    recovery of coke by-products produced from coal.
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    8.2
    Ideno(1,2,3-cd) pyrene
    193-39-5
    0.0055
    3.4
    K143
    Process residues from the recovery of light oil, including, but not limited
    to, those generated in stills, decanters, and wash oil recovery units from the
    recovery of coke by-products produced from coal.
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    K144
    Wastewater sump residues from light oil refining, including, but not limited
    to, intercepting or contamination sump sludges from the recovery of coke by-
    products produced from coal.
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    442
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    8.2
    K145
    Residues from naphthalene collection and recovery operations from the recovery
    of coke by-products produced from coal.
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    6.28.2
    Naphthalene
    91-20-3
    0.059
    5.6
    K147
    Tar storage tank residues from coal tar refining.
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    8.2
    Indeno(1,2,3-cd) pyrene
    193-39-5
    0.0055
    3.4
    K148
    Residues from coal tar distillation, including, but not limited to, still
    bottoms.
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Benzo(b)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from benzo
    -
    (b)fluoranthene)
    207-08-9
    0.11
    6.8
    Chrysene
    218-01-9
    0.059
    3.4
    Dibenz(a,h)anthra
    cene
    53-70-3
    0.055
    8.2
    Indeno(1,2,3-cd) pyrene
    193-39-5
    0.0055
    3.4
    K149
    Distillation bottoms from the production of alpha- (or methyl-) chlorinated
    toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with
    mixtures of these functional groups. (This waste does not include still
    bottoms from the distillations of benzyl chloride.)
    Chloro benzene
    108-90-7
    0.057
    6.0
    443
    Chloro form
    67-66-3
    0.046
    6.0
    Chloro methane
    74-87-3
    0.19
    30
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Pentachloro benzene
    608-93-5
    0.055
    10
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    Toluene
    108-88-3
    0.080
    10
    K150
    Organic residuals, excluding spent carbon adsorbent, from the spent chlorine
    gas and hydro chloric acid recovery processes associated with the production of
    alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl
    chlorides, and compounds with mixtures of these functional groups.
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Chloro methane
    74-87-3
    0.19
    30
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Pentachloro benzene
    608-93-5
    0.055
    10
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    1,1,2,2- Tetra chloro -
    ethane
    79-34-5
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    K151
    Wastewater treatment sludges, excluding neutralization and biological sludges,
    generated during the treatment of wastewaters from the production of alpha-
    (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl
    chlorides, and compounds with mixtures of these functional groups.
    Benzene
    71-43-2
    0.14
    10
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    Chloro form
    67-66-3
    0.046
    6.0
    Hexachloro benzene
    118-74-1
    0.055
    10
    Pentachloro benzene
    608-93-5
    0.055
    10
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    Toluene
    108-88-3
    0.080
    10
    K156
    Organic waste (including heavy ends, still bottoms, light ends, spent
    solvents, filtrates, and decantates) from the production of carbamates and
    carbamoyl oximes. (This listing does not apply to wastes generated from the
    manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
    10
    Acetonitrile
    75-05-8
    5.6
    38
    Acetophenone
    96-86-2
    0.010
    9.7
    Aniline
    62-53-3
    0.81
    14
    Benomyl
    17804-35-2
    0.056
    1.4
    Benzene
    71-43-2
    0.14
    10
    Carbaryl
    63-25-21
    0.006
    0.14
    Carbenzadim
    10605-21-7
    0.056
    1.4
    Carbofuran
    1563-66-2
    0.006
    0.14
    Carbosulfan
    55285-14-8
    0.028
    1.4
    Chlorobenzene
    108-90-7
    0.057
    6.0
    Chloroform
    67-66-3
    0.046
    6.0
    o-Dichlorobenzene
    95-50-1
    0.088
    6.0
    Methomyl
    16752-77-5
    0.028
    0.14
    Methylene chloride
    75-09-2
    0.089
    30
    444
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    Naphthalene
    91-20-3
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    Pyridine
    110-86-1
    0.014
    16
    Toluene
    108-88-3
    0.080
    10
    Triethylamine
    121-44-8
    0.081
    1.5
    K157
    Wastewaters (including scrubber waters, condenser waters, washwaters, and
    separation waters) from the production of carbamates and carbamoyl oximes.
    (This listing does not apply to wastes generated from the manufacture of 3-
    iodo-2-propyl-n-butylcarbamate.)
    10
    Carbon tetrachloride
    56-23-5
    0.057
    6.0
    Chloroform
    67-66-3
    0.046
    6.0
    Chloromethane
    74-87-3
    0.19
    30
    Methomyl
    16752-77-5
    0.028
    0.14
    Methylene chloride
    75-09-2
    0.089
    30
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    o-Phenylenediamine
    95-54-5
    0.056
    5.6
    Pyridine
    110-86-1
    0.014
    16
    Triethylamine
    121-44-8
    0.081
    1.5
    K158
    Bag house dusts and filter/separation solids from the production of carbamates
    and carbamoyl oximes. (This listing does not apply to wastes generated from
    the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
    10
    Benomyl
    17804-35-2
    0.056
    1.4
    Benzene
    71-43-2
    0.14
    10
    Carbenzadim
    10605-21-7
    0.056
    1.4
    Carbofuran
    1563-66-2
    0.006
    0.14
    Carbosulfan
    55285-14-8
    0.028
    1.4
    Chloroform
    67-66-3
    0.046
    6.0
    Methylene chloride
    75-09-2
    0.089
    30
    Phenol
    108-95-2
    0.039
    6.2
    K159
    Organics from the treatment of thiocarbamate wastes.
    10
    Benzene
    71-43-2
    0.14
    10
    Butylate
    2008-41-5
    0.042
    1.4
    EPTC (Eptam)
    759-94-4
    0.042
    1.4
    Molinate
    2212-67-1
    0.042
    1.4
    Pebulate
    1114-71-2
    0.042
    1.4
    Vernolate
    1929-77-7
    0.042
    1.4
    K161
    Purification solids (including filtration, evaporation, and centrifugation
    solids), baghouse dust and floor sweepings from the production of
    dithiocarbamate acids and their salts.
    10
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    Arsenic
    7440-38-2
    1.9
    5.0 mg/l TCLP
    Carbon disulfide
    75-15-0
    3.8
    4.8 mg/l TCLP
    Dithiocarbamates (total)
    NA
    0.028
    28
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    P001
    Warfarin, & salts, when present at con
    centrations greater than 0.3%
    Warfarin
    81-81-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    445
    P002
    1-Acetyl-2-thio urea
    1-Acetyl-2-thio urea
    591-08-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P003
    Acrolein
    Acrolein
    107-02-6 107-
    02-8
    0.29
    CMBST
    P004
    Aldrin
    Aldrin
    309-00-2
    0.021
    0.0680.066
    P005
    Allyl alcohol
    Allyl alcohol
    107-18-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    P006
    Aluminum phosphide
    Aluminum phosphide
    20859-73-
    620859-73-8
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    P007
    5-Aminomethyl-3-isoxazolol
    5-Aminomethyl-3-isoxa
    -
    zolol
    2763-96-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P008
    4-Aminopyridine
    4-Aminopyridine
    504-24-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P009
    Ammonium picrate
    Ammonium picrate
    131-74-8
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    P010
    Arsenic acid
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    P011
    Arsenic pentoxide
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    P012
    Arsenic trioxide
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    446
    P013
    Barium cyanide
    Barium
    7440-39-3
    NA
    7.6 mg/l TCLP
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P014
    Thiophenol (Benzen e thiol)
    Thiophenol (Benzene
    thiol)
    108-98-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P015
    Beryllium dust
    Beryllium
    7440-41-7
    RMETL;or RTHRM
    RMETL; or
    RTHRM
    P016
    Dichloro methyl ether (Bis(chloro
    methyl) ether)
    Dichloro methyl ether
    542-88-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P017
    Bromoacetone
    Bromoacetone
    598-31-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P018
    Brucine
    Brucine
    357-57-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P020
    2-sec-Butyl-4,6-dinitro
    phenol (Dinoseb)
    2-sec-Butyl-4,6-dinitro
    -
    phenol (Dinoseb)
    88-85-7
    0.066
    2.5
    P021
    Calcium cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P022
    Carbon disulfide
    Carbon disulfide
    75-15-0
    3.8
    INCINCMBST
    Carbon disulfide;
    alternate
    6
    standard for
    nonwastewaters only
    75-15-0
    NA
    4.8 mg/l TCLP
    P023
    Chloro acetaldehyde
    Chloro acetaldehyde
    107-20-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    447
    INCINCMBST
    P024
    p-Chloro aniline
    p-Chloro aniline
    106-47-8
    0.46
    16
    P026
    1-(o-Chloro phenyl) thiourea
    1-(o-Chloro phenyl) thio-
    urea
    5344-82-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P027
    3-Chloro propionitrile
    3-Chloro propio nitrile
    542-76-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P028
    Benzyl chloride
    Benzyl chloride
    100-44-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P029
    Copper cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P030
    Cyanides (soluble salts and complexes)
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P031
    Cyanogen
    Cyanogen
    460-19-5
    CHOXD; WETOX;
    or INCINCMBST
    CHOXD; WETOX;
    or INCINCMBST
    P033
    Cyanogen chloride
    Cyanogen chloride
    506-77-4
    CHOXD; WETOX;
    or INCINCMBST
    CHOXD; WETOX;
    or INCINCMBST
    P034
    2-Cyclo hexyl-4,6-dinitro
    phenol
    2-Cyclo hexyl-4,6-
    dinitro phenol
    131-89-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P036
    Dichloro phenyl arsine
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    P037
    Dieldrin
    Dieldrin
    60-57-1
    0.017
    0.13
    448
    P038
    Diethyl arsine
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    P039
    Disulfoton
    Disulfoton
    298-04-4
    0.017
    6.2
    P040
    O,O-Diethyl-O-pyrazinyl-phosphorothioate
    O,O-Diethyl-O-pyrazinyl
    -
    phosphoro thioate
    297-97-2
    CARBN; or
    INCINCMBST
    CMBST
    P041
    Diethyl-p-nitro phenyl phosphate
    Diethyl-p-nitrophenyl
    phosphate
    311-45-5
    CARBN; or
    INCINCMBST
    CMBST
    P042
    Epinephrine
    Epinephrine
    51-43-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P043
    Diisopropyl fluoro phosphate (DFP)
    Diisopropyl fluoro -
    phosphate (DFP)
    55-91-4
    CARBN; or
    INCINCMBST
    CMBST
    P044
    Dimethoate
    Dimethoate
    60-51-5
    CARBN; or
    INCINCMBST
    CMBST
    P045
    Thiofanox
    Thiofanox
    39196-18-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P046
    alpha,alpha-Dimethyl
    phenethyl amine
    alpha,alpha-Di methyl -
    phenethyl amine
    122-09-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P047
    4,6-Dinitro-o-cresol
    4,6-Dinitro-o-cresol
    543-52-1
    0.28
    160
    P047
    4,6-Dinitro-o-cresol salts
    NA
    NA
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    449
    P048
    2,4-Dinitro phenol
    2,4-Dinitro phenol
    51-28-5
    0.12
    160
    P049
    Dithio biuret
    Dithio biuret
    541-53-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P050
    Endosulfan
    Endosulfan I
    939-98-8
    0.023
    0.066
    Endosulfan II
    33213-6-5
    0.029
    0.13
    Endosulfan sulfate
    1031-07-8
    0.029
    0.13
    P051
    Endrin
    Endrin
    72-20-8
    0.0028
    0.13
    Endrin aldehyde
    7421-93-4
    0.025
    0.13
    P054
    Aziridine
    Aziridine
    151-56-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P056
    Fluorine
    Fluoride (measured in
    wastewaters only)
    16964-48-8
    35
    ADGAS fb NEUTR
    P057
    Fluoro acetamide
    Fluoro acetami de
    640-19-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P058
    Fluoro acetic acid, sodium salt
    Fluoro acetic acid,
    sodium salt
    62-74-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P059
    Heptachlor
    Heptachlor
    76-44-8
    0.0012
    0.066
    Heptachlor epoxide
    1024-57-3
    0.016
    0.066
    P060
    Isodrin
    Isodrin
    465-73-6
    0.021
    0.066
    P062
    Hexaethyl tetra phosphate
    Hexaethyl tetra phosphate
    757-58-4
    CARBN; or
    INCINCMBST
    CMBST
    450
    P063
    Hydrogen cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P064
    Isocyanic acid, ethyl ester
    Isocyanic acid, ethyl
    ester
    624-83-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P065
    P065 (mercury fulminate) nonwastewaters, regardless of their total mercury
    contant content , that are not incinerator residues or are not residues from
    RMERC.
    Mercury
    7439-97-6
    NA
    IMERC
    P065
    P065 (mercury fulminate) nonwastewaters that are either incinerator residues
    or are residues from RMERC; and contain greater than or equal to 260 mg/kg
    total mercury.
    Mercury
    7339-97-6
    NA
    RMERC
    P065
    P065 (mercury fulminate) nonwastewaters that are residues from RMERC and
    contain less than 260 mg/kg total mercury.
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    P065
    P065 (mercury fulminate) nonwastewaters that are incinerator residues and
    contain less than 260 mg/kg total mercury.
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    P065
    All P065 (mercury fulminate) wastewaters.
    Mercury
    7439-97-6
    0.15
    NA
    P066
    Methomyl
    Methomyl
    16752-77-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P067
    2-Methyl-aziridine
    2-Methyl-aziridine
    75-55-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P068
    Methyl hydrazine
    Methyl hydrazine
    60-34-4
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED,
    or CMBST
    P069
    451
    2-Methyl lactonitrile
    2-Methyl lactonitrile
    75-86-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P070
    Aldicarb
    Aldicarb
    116-06-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P071
    Methyl parathion
    Methyl parathion
    298-00-0
    0.014
    4.6
    P072
    1-Naphthyl-2-thio
    urea
    1-Naphthyl-2-thio
    urea
    86-88-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P073
    Nickel carbonyl
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    P074
    Nickel cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    P075
    Nicotine and salts
    Nicotine and salts
    54-11-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P076
    Nitric oxide
    Nitric oxide
    10102-43-9
    ADGAS
    ADGAS
    P077
    p-Nitro aniline
    p-Nitro aniline
    100-01-6
    0.028
    28
    P078
    Nitrogen dioxide
    Nitrogen dioxide
    10102-44-0
    ADGAS
    ADGAS
    P081
    Nitroglycerin
    Nitroglycerin
    55-63-0
    CHOXD; CHRED;
    CARBN; BIODG
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    P082
    N-Nitroso dimethyl amine
    452
    N-Nitroso dimethyl amine
    62-75-9
    0.40
    2.3
    P084
    N-Nitroso methyl vinylamine
    N-Nitroso methyl vinyl-
    amine
    4549-40-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P085
    Octamethyl pyrophosphoramide
    Octamethyl pyrophosphor -
    amide
    152-16-9
    CARBN; or
    INCINCMBST
    CMBST
    P087
    Osmium tetroxide
    Osmium tetroxide
    20816-12-0
    RMETL; or
    RTHRM
    RMETL; or
    RTHRM
    P088
    Endothall
    Endothall
    145-73-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    P089
    Parathion
    Parathion
    56-38-2
    0.014
    4.6
    P092
    P092 (phenyl mercuric acetate) nonwastewaters, regardless of their total
    mercury content, that are not incinerator residues or are not residues from
    RMERC.
    Mercury
    7439-97-6
    NA
    IMERC; or
    RMERC
    P092
    P092 (phenyl mercuric acetate) nonwastewaters that are either incinerator
    residues or are residues from RMERC; and still contain greater than or equal
    to 260 mg/kg total mercury.
    Mercury
    7439-97-6
    NA
    RMERC
    P092
    P092 (phenyl mercuric acetate) nonwastewaters that are residues from RMERC and
    contain less than 260 mg/kg total mercury.
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    P092
    P092 (phenyl mercuric acetate) nonwastewaters that are incinerator residues
    and contain less than 260 mg/kg total mercury.
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    P092
    All P092 (phenyl mercuric acetate) wastewaters.
    Mercury
    7439-97-6
    0.15
    NA
    P093
    Phenyl thiourea
    Phenyl thiourea
    103-85-5
    (WETOX or
    INCINCMBST
    453
    CHOXD) fb
    CARBN; or
    INCINCMBST
    P094
    Phorate
    Phorate
    298-02-2
    0.021
    4.6
    P095
    Phosgene
    Phosgene
    75-44-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P096
    Phosphine
    Phosphine
    7803-51-2
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    P097
    Famphur
    Famphur
    52-85-7
    0.017
    15
    P098
    Potassium cyanide.
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P099
    Potassium silver cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Silver
    7440-22-4
    0.43
    0.30 mg/l TCLP
    P101
    Ethyl cyanide (Propanenitrile)
    Ethyl cyanide
    (Propanenitrile)
    107-12-0
    0.24
    360
    P102
    Propargyl alcohol
    Propargyl alcohol
    107-19-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    P103
    Selenourea
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    P104
    Silver cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    Silver
    7440-22-4
    0.43
    0.30 mg/l TCLP
    P105
    Sodium azide
    Sodium azide
    26628-22-8
    CHOXD; CHRED;
    CARBN; BIODG;
    CHOXD; CHRED;
    or CMBST
    454
    or INCINCMBST
    P106
    Sodium cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P108
    Strychnine and salts
    Strychnine and salts
    57-24-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P109
    Tetraethyldithio pyrophosphate
    Tetraethyldithio pyro-
    phosphate
    3689-24-5
    CARBN; or
    INCINCMBST
    CMBST
    P110
    Tetraethyl lead
    leadLead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    P111
    Tetraethylpyrophosphate
    Tetraethylpyrophosphate
    107-49-3
    CARBN; or
    INCINCMBST
    CMBST
    P112
    Tetranitromethane
    Tetranitromethane
    509-14-8
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    P113
    Thallic oxide
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    P114
    Thallium selenite
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    P115
    Thallium (I) sulfate
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    P116
    Thiosemicarbazide
    Thiosemicarbazide
    79-19-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    P118
    Trichloro methanethiol
    Trichloro methane thiol
    75-70-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    455
    P119
    Ammonium vanadate
    Vanadium (measured in
    wastewaters only)
    7440-62-2
    4.3
    STABL
    P120
    Vanadium pentoxide
    Vanadium (measured in
    wastewaters only)
    7440-62-2
    4.3
    STABL
    P121
    Zinc cyanide
    Cyanides (Total)
    7
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    7
    57-12-5
    0.86
    30
    P122
    Zinc phosphide Zn
    3
    P
    2
    , when present at con
    centrations greater than 10%
    Zinc Phosphide
    1314-84-7
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    P123
    Toxaphene
    Toxaphene
    8001-35-2
    0.0095
    2.6
    P127
    Carbofuran
    10
    Carbofuran
    1563-66-2
    0.006
    0.14
    P128
    Mexacarbate
    10
    Mexacarbate
    315-18-4
    0.056
    1.4
    P185
    Tirpate
    10
    Tirpate
    26419-73-8
    0.056
    0.28
    P188
    Physostigimine salicylate
    10
    Physostigmine salicylate
    57-64-7
    0.056
    1.4
    P189
    Carbosulfan
    10
    Carbosulfan
    55285-14-8
    0.028
    1.4
    P190
    Metolcarb
    10
    Metolcarb
    1129-41-5
    0.056
    1.4
    P191
    Dimetilan
    10
    Dimetilan
    644-64-4
    0.056
    1.4
    P192
    Isolan
    10
    Isolan
    119-38-0
    0.056
    1.4
    P194
    Oxamyl
    10
    Oxamyl
    23135-22-0
    0.056
    0.28
    P196
    456
    Manganese dimethyldithiocarbamates (total)
    10
    Dithiocarbamates (total)
    NA
    0.028
    28
    P197
    Formparanate
    10
    Formparanate
    17702-57-7
    0.056
    1.4
    P198
    Formetanate hydrochloride
    10
    Formetanate hydro
    -
    chloride
    23422-53-9
    0.056
    1.4
    P199
    Methiocarb
    10
    Methiocarb
    2032-65-7
    0.056
    1.4
    P201
    Promecarb
    10
    Promecarb
    2631-37-0
    0.056
    1.4
    P202
    m-Cumenyl methylcarbamate
    10
    m-Cumenyl methyl -
    carbamate
    64-00-6
    0.056
    1.4
    P203
    Aldicarb sulfone
    10
    Aldicarb sulfone
    1646-88-4
    0.056
    0.28
    P204
    Physostigmine
    10
    Physostigmine
    57-47-6
    0.056
    1.4
    P205
    Ziram
    10
    Dithiocarbamates (total)
    NA
    0.028
    28
    U001
    Acetaldehyde
    Acetaldehyde
    75-07-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U002
    Acetone
    Acetone
    67-64-1
    0.28
    160
    U003
    Acetonitrile
    Acetonitrile
    75-05-8
    5.6
    INCINCMBST
    Acetonitrile; alternate
    6
    standard for
    nonwastewaters only
    75-05-8
    NA
    1.838
    U004
    Acetophenone
    Acetophenone
    98-86-2
    0.010
    9.7
    U005
    2-Acetylaminofluorene
    457
    2-Acetylaminofluorene
    53-96-3
    0.059
    140
    U006
    Acetyl chloride
    Acetyl chloride
    75-36-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U007
    Acrylamide
    Acrylamide
    79-06-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U008
    Acrylic acid
    Acrylic acid
    79-10-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U009
    Acrylonitrile
    Acrylonitrile
    107-13-1
    0.24
    84
    U010
    Mitomycin C
    Mitomycin C
    50-07-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U011
    Amitrole
    Amitrole
    61-82-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U012
    Aniline
    Aniline
    62-53-3
    0.81
    14
    U014
    Auramine
    Auramine
    492-80-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U015
    Azaserine
    Azaserine
    115-02-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U016
    Benz(c)acridine
    458
    Benz(c)acridine
    225-51-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U017
    Benzal chloride
    Benzal chloride
    98-87-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U018
    Benz(a)anthracene
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    U019
    Benzene
    Benzene
    71-43-2
    0.14
    10
    U020
    Benzenesulfonyl chloride
    Benzenesulfonyl chloride
    98-09-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U021
    Benzidine
    Benzidine
    92-87-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U022
    Benzo(a)pyrene
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    U023
    Benzotrichloride
    Benzotrichloride
    98-07-7
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U024
    bis(2-Chloro ethoxy) methane
    bis(2-Chloro ethoxy) -
    methane
    111-91-1
    0.036
    7.2
    U025
    bis(2-Chloro ethyl) ether
    bis(2-Chloro ethyl) ether
    111-44-4
    0.033
    6.0
    U026
    Chlornaphazine
    Chlornaphazine
    494-03-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U027
    459
    bis(2-Chloro isopropyl) ether
    bis(2-Chloro isopropyl) -
    ether
    108-60-1 39638-
    32-9
    0.055
    7.2
    U028
    bis(2-Ethyl hexyl) phthalate
    bis(2-Ethyl hexyl) -
    phthalate
    117-81-7
    0.28
    28
    U029
    Methyl bromide (Bromo
    methane)
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    U030
    4-Bromo phenyl phenyl ether
    4-Bromo phenyl phenyl
    ether
    101-55-3
    0.055
    15
    U031
    n-Butyl alcohol
    n-Butyl alcohol
    71-36-3
    5.6
    2.6
    U032
    Calcium chromate
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    U033
    Carbon oxyfluoride
    Carbon oxyfluoride
    353-50-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U034
    Trichloro acetaldehyde (Chloral)
    Trichloro acetaldehyde
    (Chloral)
    75-87-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U035
    Chlorambucil
    Chlorambucil
    305-03-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U036
    Chlordane
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033
    0.26
    U037
    Chloro benzene
    Chloro benzene
    108-90-7
    0.057
    6.0
    U038
    Chloro benzilate
    Chloro benzilate
    510-15-6
    0.10
    INCINCMBST
    U039
    460
    p-Chloro-m-cresol
    p-Chloro-m-cresol
    59-50-7
    0.018
    14
    U041
    Epichloro hydrin (1-Chloro-2,3-epoxypropane)
    Epichloro hydrin (1-
    Chloro-2,3-epoxypropane)
    106-89-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U042
    2-Chloro ethyl vinyl ether
    2-Chloro ethyl vinyl
    ether
    110-75-8
    0.062
    INCINCMBST
    U043
    Vinyl chloride
    Vinyl chloride
    75-01-4
    0.27
    6.0
    U044
    Chloro form
    Chloro form
    67-66-3
    0.046
    6.0
    U045
    Chloro methane (Methyl chloride)
    Chloro methane (Methyl
    chloride)
    74-87-3
    0.19
    30
    U046
    Chloro methyl methyl e ther
    Chloro methyl methyl
    ether
    107-30-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U047
    2-Chloro naphthalene
    2-Chloro naphthalene
    91-58-7
    0.055
    5.6
    U048
    2-Chloro phenol
    2-Chloro phenol
    95-57-8
    0.044
    5.7
    U049
    4-Chloro-o-toluidine hydro
    chloride
    4-Chloro-o-toluidine
    hydrochloride
    3165-93-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U050
    Chrysene
    Chrysene
    218-01-9
    0.059
    3.4
    U051
    Creosote
    Naphthalene
    91-20-3
    0.059
    5.6
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    Phenanthrene
    85-01-8
    0.059
    5.6
    Pyrene
    129-00-0
    0.067
    8.2
    Toluene
    108-88-3
    0.080
    10
    461
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    U052
    Cresols (Cresylic acid)
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    Cresol-mixed isomers
    (Cresylic acid)
    (sum of o -, m-, and p-
    cresol con centrations)
    1319-77-3
    0.88
    11.2
    U053
    Crotonaldehyde
    Crotonaldehyde
    4170-30-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U055
    Cumene
    Cumene
    98-82-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U056
    Cyclohexane
    Cyclohexane
    110-82-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U057
    Cyclohexanone
    Cyclohexanone
    108-94-1
    0.36
    CMBST
    Cyclohexanone;
    alternate
    6
    standard for
    nonwastewaters only
    108-94-1
    NA
    0.75 mg/l TCLP
    U058
    Cyclophosphamide
    Cyclophosphamide
    50-18-0
    CARBN; or
    INCINCMBST
    CMBST
    U059
    Daunomycin
    Daunomycin
    20830-81-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U060
    DDD
    o,p'-DDD
    53-19-0
    0.023
    0.087
    462
    p,p'-DDD
    72-54-8
    0.023
    0.087
    U061
    DDT
    o,p'-DDT
    789-02-6
    0.0039
    0.087
    p,p'-DDT
    50-29-3
    0.0039
    0.087
    o,p'-DDD
    53-19-0
    0.023
    0.087
    p,p'-DDD
    72-54-8
    0.023
    0.087
    o,p'-DDE
    3424-82-6
    0.031
    0.087
    p,p'-DDE
    72-55-9
    0.031
    0.087
    U062
    Diallate
    Diallate
    2303-16-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U063
    Dibenz(a,h)anthracene
    Dibenz(a,h)anthracene
    53-70-3
    0.055
    8.2
    U064
    Dibenz(a,i)pyrene
    Dibenz(a,i)pyrene
    189-55-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U066
    1,2-Dibromo-3-chloro
    propane
    1,2-Dibromo-3-chloro
    -
    propane
    96-12-8
    0.11
    15
    U067
    Ethylene dibromide (1,2-Dibromo
    ethane)
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    U068
    Dibromo methane
    Dibromo methane
    74-95-3
    0.11
    15
    U069
    Di-n-butyl phthalate
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    U070
    o-Dichloro benzene
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    U071
    m-Dichloro benzene
    m-Dichloro benzene
    541-73-1
    0.036
    6.0
    U072
    p-Dichloro benzene
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    U073
    3,3'-Dichloro benzidine
    463
    3,3'-Dichloro benzidine
    91-94-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U074
    1,4-Dichloro-2-butene
    cis-1,4-Dichloro-2-
    butene
    1476-11-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    trans-1,4-Dichloro-2-
    butene
    764-41-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U075
    Dichloro difluoro methane
    Dichloro difluoro methane
    75-71-8
    0.23
    7.2
    U076
    1,1-Dichloro ethane
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    U077
    1,2-Dichloro ethane
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    U078
    1,1-Dichloro ethylene
    1,1-Dichloro ethylene
    75-35-4
    0.025
    6.0
    U079
    1,2-Dichloro ethylene
    trans-1,2-Dichloro
    -
    ethylene
    156-60-5
    0.054
    30
    U080
    Methylene chloride
    Methylene chloride
    75-09-2
    0.089
    30
    U081
    2,4-Dichloro phenol
    2,4-Dichloro phenol
    120-83-2
    0.044
    14
    U082
    2,6-Dichloro phenol
    2,6-Dichloro phenol
    87-65-0
    0.044
    14
    U083
    1,2-Dichloro propane
    1,2-Dichloro propane
    78-87-5
    0.85
    18
    U084
    1,3-Dichloro propylene
    cis-1,3-Dichloro -
    propylene
    10061-01-5
    0.036
    18
    trans-1,3-Dichloro
    -
    propylene
    10061-02-6
    0.036
    18
    U085
    1,2:3,4-Diepoxybutane
    464
    1,2:3,4-Diepoxybutane
    1464-53-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U086
    N,N'-Diethyl hydrazine
    N,N'-Diethyl hydrazine
    1615-80-1
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U087
    O,O-Diethyl -S-methyl dithio phosphate
    O,O-Diethyl -S-methyl -
    dithio phosphate
    3288-58-2
    CARBN; or
    INCINCMBST
    CMBST
    U088
    Diethyl phthalate
    Diethyl phthalate
    84-66-2
    0.20
    28
    U089
    Diethyl stilbestrol
    Diethyl stilbestrol
    56-53-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U090
    Dihydro safrole
    Dihydro safrole
    94-58-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U091
    3,3'-Dimethoxybenzidine
    3,3'-Dimethoxybenzidine
    119-90-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U092
    Dimethyl amine
    Dimethyl amine
    124-40-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U093
    p-Dimethyl aminoazobenzene
    p-Dimethyl -
    aminoazobenzene
    60-11-7
    0.13
    INCINCMBST
    U094
    7,12-Dimethyl benz(a) anthracene
    7,12-Dimethyl benz(a) -
    anthracene
    57-97-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U095
    465
    3,3'-Dimethyl benzidine
    3,3'-Dimethyl benzidine
    119-93-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U096
    alpha, alpha-Dimethyl benzyl hydro
    peroxide
    alpha, alpha-Dimethyl
    benzyl hydro peroxide
    80-15-9
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U097
    Dimethyl carbamoyl chloride
    Dimethyl carbamoyl
    chloride
    79-44-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U098
    1,1-Dimethyl hydrazine
    1,1-Dimethyl hydrazine
    57-14-7
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U099
    1,2-Dimethyl hydrazine
    1,2-Dimethyl hydrazine
    540-73-8
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U101
    2,4-Dimethyl phenol
    2,4-Dimethyl phenol
    105-67-9
    0.036
    14
    U102
    Dimethyl phthalate
    Dimethyl phthalate
    131-11-3
    0.047
    28
    U103
    Dimethyl sulfate
    Dimethyl sulfate
    77-78-1
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U105
    2,4-Dinitro toluene
    2,4-Dinitro toluene
    121-14-2
    0.32
    140
    U106
    2,6-Dinitro toluene
    2,6-Dinitro toluene
    606-20-2
    0.55
    28
    U107
    Di-n-octyl phthalate
    Di-n-octyl phthalate
    117-84-0
    0.017
    28
    U108
    1,4-Dioxane
    1,4-Dioxane
    123-91-1
    (WETOX or
    CHOXD) fb
    CMBST
    466
    CARBN; or
    INCINCMBST
    1,4-Dioxane; alternate
    6
    standard for
    nonwastewaters only
    123-91-1
    NA
    170
    U109
    1,2-Diphenyl hydrazine
    1,2-Diphenyl hydrazine
    122-66-7
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    1,2-Diphenyl hydrazine;
    alternate
    6
    standard for
    wastewaters only
    122-66-7
    0.087
    NA
    U110
    Dipropyl amine
    Dipropyl amine
    142-84-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U111
    Di-n-propyl nitros amine
    Di-n-propyl nitros amine
    621-64-7
    0.40
    14
    U112
    Ethyl acetate
    Ethyl acetate
    141-78-8 141-
    78-6
    0.34
    33
    U113
    Ethyl acrylate
    Ethyl acrylate
    140-88-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U114
    Ethylene bisdithio carbamic acid salts and esters
    Ethylene bisdithio -
    carbamic acid
    111-54-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U115
    Ethylene oxide
    Ethylene oxide
    75-21-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CHOXD; or
    INCINCMBST
    Ethylene oxide;
    alternate
    6
    standard for
    wastewaters only
    75-21-8
    0.12
    NA
    U116
    Ethylene thio urea
    Ethylene thio urea
    96-45-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    467
    U117
    Ethyl ether
    Ethyl ether
    60-29-7
    0.12
    160
    U118
    Ethyl methacrylate
    Ethyl methacrylate
    97-63-2
    0.14
    160
    U119
    Ethyl methane sulfonate
    Ethyl methane sulfonate
    62-50-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U120
    Fluoranthene
    Fluoranthene
    206-44-0
    0.068
    3.4
    U121
    Trichloro monofluoro methane
    Trichloro monofluoro -
    methane
    75-69-4
    0.020
    30
    U122
    Formaldehyde
    Formaldehyde
    50-00-0
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U123
    Formic acid
    Formic acid
    64-18-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U124
    Furan
    Furan
    110-00-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U125
    Furfural
    Furfural
    98-01-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U126
    Glycidylaldehyde
    Glycidylaldehyde
    765-34-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U127
    468
    Hexachloro benzene
    Hexachloro benzene
    118-74-1
    0.055
    10
    U128
    Hexachloro butadiene
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    U129
    Lindane
    alpha-BHC
    319-84-6
    0.00014
    0.066
    beta-BHC
    319-85-7
    0.00014
    0.066
    delta-BHC
    319-86-8
    0.023
    0.066
    gamma-BHC (Lindane)
    58-89-9
    0.0017
    0.066
    U130
    Hexachloro cyclopentadiene
    Hexachloro cyclopenta-
    diene
    77-47-4
    0.057
    2.4
    U131
    Hexachloro ethane
    Hexachloro ethane
    67-72-1
    0.055
    30
    U132
    Hexachloro phene
    Hexachloro phene
    70-30-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U133
    Hydrazine
    Hydrazine
    302-01-2
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U134
    Hydrogen fluoride
    Fluoride (measured in
    wastewaters only)
    16964-48-8
    35
    ADGAS fb
    NEUTR; or
    NEUTR
    U135
    Hydrogen sulfide
    Hydrogen sulfide
    7783-06-4
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    U136
    Cacodylic acid
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    U137
    Indeno(1,2,3-c ,d)pyrene
    Indeno(1,2,3-c ,d)pyrene
    193-39-5
    0.0055
    3.4
    U138
    Iodomethane
    Iodomethane
    74-88-4
    0.19
    65
    U140
    Isobutyl alcohol
    469
    Isobutyl alcohol
    78-83-1
    5.6
    170
    U141
    Isosafrole
    Isosafrole
    120-58-1
    0.081
    2.6
    U142
    Kepone
    Kepone
    143-50-8
    0.0011
    0.13
    U143
    Lasiocarpine
    Lasiocarpine
    303-34-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U144
    Lead acetate
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    U145
    Lead phosphate
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    U146
    Lead subacetate
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    U147
    Maleic anhydride
    Maleic anhydride
    108-31-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U148
    Maleic hydrazide
    Maleic hydrazide
    123-33-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U149
    Malononitrile
    Malononitrile
    109-77-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U150
    Melphalan
    Melphalan
    148-82-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U151
    U151 (mercury) nonwastewaters that contain greater than or equal to 260 mg/kg
    total mercury.
    Mercury
    7439-97-6
    NA
    RMERC
    470
    U151
    U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury
    and that are residues from RMERC only.
    Mercury
    7439-97-6
    NA
    0.20 mg/l TCLP
    U151
    U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury
    and that are not residues from RMERC only.
    Mercury
    7439-97-6
    NA
    0.025 mg/l
    TCLP
    U151
    All U151 (mercury) wastewater.
    Mercury
    7439-97-6
    0.15
    NA
    U151
    Element Mercury Contaminated with Radioactive Materials
    Mercury
    7439-97-6
    NA
    AMLGM
    U152
    Methacrylonitrile
    Methacrylonitrile
    126-98-7
    0.24
    84
    U153
    Methanethiol
    Methanethiol
    74-93-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U154
    Methanol
    Methanol
    67-56-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    Methanol; alternate
    6
    set
    of standards for both
    wastewaters and
    nonwastewaters
    67-56-1
    5.6
    0.75 mg/l TCLP
    U155
    Methapyrilene
    Methapyrilene
    91-80-5
    0.081
    1.5
    U156
    Methyl chloro carbonate
    Methyl chloro carbonate
    79-22-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U157
    3-Methyl cholanthrene
    3-Methyl cholanthrene
    56-49-5
    0.0055
    15
    U158
    4,4'-Methylene bis(2-chloro
    aniline )
    4,4'-Methylene bis(2-
    chloro aniline)
    101-14-4
    0.50
    30
    471
    U159
    Methyl ethyl ketone
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    U160
    Methyl ethyl ketone peroxide
    Methyl ethyl ketone
    peroxide
    1338-23-4
    CHOXD; CHRED;
    CARBN; BIODG;
    or INCINCMBST
    CHOXD; CHRED;
    or CMBST
    U161
    Methyl isobutyl ketone
    Methyl isobutyl ketone
    108-10-1
    0.14
    33
    U162
    Methyl methacrylate
    Methyl methacrylate
    80-62-6
    0.14
    160
    U163
    N-Methyl-N'-nitro-N-nitroso
    guanidine
    N-Methyl-N'-nitro-N-
    nitroso guanidine
    70-25-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U164
    Methyl thiouracil
    Methyl thiouracil
    56-04-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U165
    Naphthalene
    Naphthalene
    91-20-3
    0.059
    5.6
    U166
    1,4-Naphthoquinone
    1,4-Naphthoquinone
    130-15-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U167
    1-Naphthylamine
    1-Naphthylamine
    134-32-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U168
    2-Naphthylamine
    2-Naphthylamine
    91-59-8
    0.52
    INCINCMBST
    U169
    Nitrobenzene
    Nitrobenzene
    98-95-3
    0.068
    14
    U170
    p-Nitro phenol
    472
    p-Nitro phenol
    100-02-7
    0.12
    29
    U171
    2-Nitro propane
    2-Nitro propane
    79-46-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U172
    N-Nitroso di-n-butyl amine
    N-Nitroso di-n-butyl amine
    924-16-3
    0.40
    17
    U173
    N-Nitroso diethanolamine
    N-Nitroso diethanolamine
    1116-54-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U174
    N-Nitroso diethyl amine
    N-Nitroso diethyl amine
    55-18-5
    0.40
    28
    U176
    N-Nitroso-N-ethyl
    urea
    N-Nitroso-N-ethyl
    urea
    759-73-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U177
    N-Nitroso-N-methyl
    urea
    N-Nitroso-N-methyl
    urea
    684-93-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U178
    N-Nitroso-N-methyl
    urethane
    N-Nitroso-N-methyl
    -
    urethane
    615-53-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U179
    N-Nitroso piperidine
    N-Nitroso piperidine
    100-75-4
    0.013
    35
    U180
    N-Nitroso pyrrolidine
    N-Nitroso pyrrolidine
    930-55-2
    0.013
    35
    U181
    5-Nitro-o-toluidine
    5-Nitro-o-toluidine
    99-55-8
    0.32
    28
    U182
    Paraldehyde
    Paraldehyde
    123-63-7
    (WETOX or
    CHOXD) fb
    CMBST
    473
    CARBN; or
    INCINCMBST
    U183
    Pentachloro benzene
    Pentachloro benzene
    608-93-5
    0.055
    10
    U184
    Pentachloro ethane
    Pentachloro ethane
    76-01-7
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    Pentachloro ethane;
    alternate
    6
    standards for
    both wastewaters and
    nonwastewaters
    76-01-7
    0.055
    6.0
    U185
    Pentachloro nitrobenzene
    Pentachloro nitrobenzene
    82-68-8
    0.055
    4.8
    U186
    1,3-Penta diene
    1,3-Penta diene
    504-60-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U187
    Phenacetin
    Phenacetin
    62-44-2
    0.081
    16
    U188
    Phenol
    Phenol
    108-95-2
    0.039
    6.2
    U189
    Phosphorus sulfide
    Phosphorus sulfide
    1314-80-3
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    U190
    Phthalic anhydride
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    100-21-0
    0.055
    28
    Phthalic anhydride
    (measured as Phthalic
    acid or Terephthalic
    acid)
    85-44-9
    0.055
    28
    U191
    2-Picoline
    2-Picoline
    109-06-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U192
    474
    Pronamide
    Pronamide
    23950-58-5
    0.093
    1.5
    U193
    1,3-Propane sultone
    1,3-Propane sultone
    1120-71-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U194
    n-Propyl amine
    n-Propyl amine
    107-10-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U196
    Pyridine
    Pyridine
    110-86-1
    0.014
    16
    U197
    p-Benzo quinone
    p-Benzo quinone
    106-51-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U200
    Reserpine
    Reserpine
    50-55-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U201
    Resorcinol
    Resorcinol
    108-46-3
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U202
    Saccharin and salts
    Saccharin
    81-07-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U203
    Safrole
    Safrole
    94-59-7
    0.081
    22
    U204
    Selenium dioxide
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    U205
    Selenium sulfide
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    475
    U206
    Streptozotocin
    Streptozotocin
    18883-66-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U207
    1,2,4,5-Tetra chloro benzene
    1,2,4,5-Tetra chloro -
    benzene
    95-94-3
    0.055
    14
    U208
    1,1,1,2-Tetra chloro ethane
    1,1,1,2-Tetra chloro -
    ethane
    630-20-6
    0.057
    6.0
    U209
    1,1,2,2-Tetra chloro ethane
    1,1,2,2-Tetra chloro -
    ethane
    79-34-5
    0.057
    6.0
    U210
    Tetrachloro ethylene
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    U211
    Carbon tetra chloride
    Carbon tetra chloride
    56-23-5
    0.057
    6.0
    U213
    Tetrahydrofuran
    Tetrahydrofuran
    109-99-9
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    U214
    Thallium (I) acetate
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    U215
    Thallium (I) carbonate
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    U216
    Thallium (I) chloride
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    U217
    Thallium (I) nitrate
    Thallium (measured in
    wastewaters only)
    7440-28-0
    1.4
    RTHRM; or
    STABL
    U218
    Thioacetamide
    Thioacetamide
    62-55-5
    (WETOX or
    CHOXD) fb
    INCINCMBST
    476
    CARBN; or
    INCINCMBST
    U219
    Thiourea
    Thiourea
    62-56-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U220
    Toluene
    Toluene
    108-88-3
    0.080
    10
    U221
    Toluenediamine
    Toluenediamine
    25376-45-8
    CARBN; or
    INCINCMBST
    CMBST
    U222
    o-Toluidine hydro
    chloride
    o-Toluidine hydro
    -
    chloride
    636-21-5
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U223
    Toluene diisocyanate
    Toluene diisocyanate
    26471-62-5
    CARBN; or
    INCINCMBST
    CMBST
    U225
    Bromoform (Tribromo methane)
    Bromoform (Tribromo -
    methane)
    75-25-2
    0.63
    15
    U226
    1,1,1-Trichloro ethane
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    U227
    1,1,2-Tricloroethane
    1,1,2-Tricloroethane
    79-00-5
    0.054
    6.0
    U228
    Trichloro ethylene
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    U234
    1,3,5-Trinitro benzene
    1,3,5-Trinitro benzene
    99-35-4
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U235
    tris-(2,3-Dibromo
    propyl)-phosphate
    tris-(2,3-Dibromo
    -
    propyl)-phosphate
    126-72-7
    0.11
    0.10
    U236
    477
    Trypan Blue
    Trypan Blue
    72-57-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U237
    Uracil mustard
    Uracil mustard
    66-75-1
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U238
    Urethane (Ethyl carbamate)
    Urethane (Ethyl
    carbamate)
    51-79-6
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U239
    Xylenes
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene con centrations)
    1330-20-7
    0.32
    30
    U240
    2,4-D (2,4-Dichloro
    phenoxyacetic acid)
    2,4-D (2,4-Dichloro
    -
    phenoxyacetic acid)
    94-75-7
    0.72
    10
    2,4-D (2,4-Dichloro
    -
    phenoxyacetic acid)
    salts and esters
    NA
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U243
    Hexachloro propylene
    Hexachloro propylene
    1888-71-7
    0.035
    30
    U244
    Thiram
    Thiram
    137-26-8
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    INCINCMBST
    U246
    Cyanogen bromide
    Cyanogen bromide
    506-68-3
    CHOXD; WETOX;
    or INCINCMBST
    CHOXD; WETOX;
    or INCINCMBST
    U247
    Methoxychlor
    Methoxychlor
    72-43-5
    0.25
    0.18
    U248
    Warfarin, & salts, when present at con
    centrations of 0.3% or less
    Warfarin
    81-81-2
    (WETOX or
    CHOXD) fb
    CARBN; or
    INCINCMBST
    CMBST
    478
    U249
    Zinc phosphide, Zn
    3
    P
    2
    , when present at con
    centrations of 10% or less
    Zinc Phosphide
    1314-84-7
    CHOXD; CHRED;
    or INCINCMBST
    CHOXD; CHRED;
    or INCINCMBST
    U271
    Benomyl
    10
    Benomyl
    17804-35-2
    0.056
    1.4
    U278
    Bendiocarb
    10
    Bendiocarb
    22781-23-3
    0.056
    1.4
    U279
    Carbaryl
    10
    Carbaryl
    63-25-2
    0.006
    0.14
    U280
    Barban
    10
    Barban
    101-27-9
    0.056
    1.4
    U328
    o-Toluidine
    o-Toluidine
    95-53-4
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN); or
    BIODG fb CARBN
    INCINCMBST; or
    Thermal
    Destruction
    U353
    p-Toluidine
    p-Toluidine
    106-49-0
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN); or
    BIODG fb CARBN
    INCINCMBST; or
    Thermal
    Destruction
    U359
    2-Ethoxyethanol
    2-Ethoxyethanol
    110-80-5
    INCINCMBST; or
    CHOXD fb
    (BIODG or
    CARBN); or
    BIODG fb CARBN
    CMBST
    U364
    Bendiocarb phenol
    10
    Bendiocarb phenol
    22961-82-6
    0.056
    1.4
    U367
    Carbofuran phenol
    10
    Carbofuran phenol
    1563-38-8
    0.056
    1.4
    U372
    Carbendazim
    10
    Carbendazim
    10605-21-7
    0.056
    1.4
    U373
    Propham
    10
    Propham
    122-42-9
    0.056
    1.4
    479
    U387
    Prosulfocarb
    10
    Prosulfocarb
    52888-80-9
    0.042
    1.4
    U389
    Triallate
    10
    Triallate
    2303-17-5
    0.042
    1.4
    U394
    A2213
    10
    A2213
    30558-43-1
    0.042
    1.4
    U395
    Diethylene glycol, dicarbamate
    10
    Diethylene glycol,
    dicarbamate
    5952-26-1
    0.056
    1.4
    U404
    Triethylamine
    10
    Triethylamine
    101-44-8
    0.081
    1.5
    U409
    Thiophanate -methyl
    10
    Thiophanate -methyl
    23564-05-8
    0.056
    1.4
    U410
    Thiodicarb
    10
    Thiodicarb
    59669-26-0
    0.019
    1.4
    U411
    Propoxur
    10
    Propoxur
    114-26-1
    0.056
    1.4
    Notes:
    1
    The waste descriptions provided in this table do not replace waste
    descriptions in 35 Ill. Adm. Code 721. Descriptions of Treatment or
    Regulatory Subcategories are provided, as needed, to distinguish between
    applicability of different standards.
    2
    CAS means Chemical Abstract Services. When the waste code or regulated
    constituents are described as a combination of a chemical with its salts
    or esters, the CAS number is given for the parent compound only.
    3
    Concentration standards for wastewaters are expressed in mg/l
    and are
    based on analysis of composite samples.
    4
    All treatment standards expressed as a Technology Code or combination of
    Technology Codes are explained in detail in 35 Ill. Adm. Code 728.Table
    C, "Technology Codes and Descriptions of Technology-Based Standards".
    "fb" inserted between waste codes denotes "followed by", so that the
    first-listed treatment is followed by the second-listed treatment. ";"
    separates alternative treatement schemes.
    5
    Except for Metals (EP or TCLP) and Cyanides (Total and Amenable) the
    nonwastewater treatment standards expressed as a con
    centration were
    established, in part, based upon incineration in units operated in
    accordance with the technical requirements of 35 Ill. Adm. Code
    724.Subpart O or 35 Ill. Adm. Code 725.Subpart O
    , or based upon
    combustion in fuel substitution units operating in accordance with
    480
    applicable technical requirements. A facility may comply with these
    treatment standards according to provisions in 35 Ill. Adm. Code
    728.140(d). All con
    centration standards for nonwastewaters are based on
    analysis of grab samples.
    6
    Where an alternate treatment standard or set of alternate standards has
    been indicated, a facility may comply with this alternate standard, but
    only for the Treatment or Regulatory Subcategory or physical form (i.e.,
    wastewater or nonwastewater) specified for that alternate standard.
    7
    Both Cyanide s (Total) and Cyanides (Amenable) for nonwastewaters are to
    be analyzed using Method 9010 or 9012, found in "Test Methods for
    Evaluating Solid Waste, Physical or Chemical Methods", USEPA Publication
    SW-846, as incorporated by reference in 35 Ill. Adm. Code 720.111, with
    a sample size of 10 grams and a distillation time of one hour and 15
    minutes.
    8
    These wastes, when rendered nonhazardous and then subsequently managed
    in CWA or CWA -equivalent systems are not subject to treatment standards.
    (See Section 728.101(c)(3) and (c)(4)).
    9
    These wastes, when rendered nonhazardous and then subsequently injected
    in a Class I SDWA well are not subject to treatment standards. (See 35
    Ill. Adm. Code 738.101(d)).
    10
    This footnote corresponds with note 10 to the table to 40 CFR 268.40,
    which has already expired by its own terms. This statement maintains
    structural consistency with the federal regulations.
    NA
    means not applicable.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 728.Table U
    Universal Treatment Standards (UTS)
    Regulated Con stituent-
    Common Name
    CAS
    1
    No.
    Wastewater
    Standard
    Concentration
    (in mg/l
    2
    )
    Nonwastewater
    Standard
    Concentration
    (in mg/kg
    3
    unless noted as
    "mg/l TCLP")
    A2213
    6
    30558-43-1
    0.042
    1.4
    Acenaphthylene
    208-96-8
    0.059
    3.4
    Acenaphthene
    83-32-9
    0.059
    3.4
    Acetone
    67-64-1
    0.28
    160
    Acetonitrile
    75-05-8
    5.6
    1.838
    Acetophenone
    96-86-2
    0.010
    9.7
    2-Acetylamino fluorene
    53-96-3
    0.059
    140
    Acrolein
    107-02-8
    0.29
    NA
    Acrylamide
    79-06-1
    19
    23
    Acrylonitrile
    107-13-1
    0.24
    84
    481
    Aldicarb Sulfone
    6
    1646-88-4
    0.056
    0.28
    Aldrin
    309-00-2
    0.021
    0.066
    4-Aminobiphenyl
    92-67-1
    0.13
    NA
    Aniline
    62-53-3
    0.81
    14
    Anthracene
    120-12-7
    0.059
    3.4
    Aramite
    140-57-8
    0.36
    NA
    alpha-BHC
    319-84-6
    0.00014
    0.066
    beta-BHC
    319-85-7
    0.00014
    0.066
    delta-BHC
    319-86-8
    0.023
    0.066
    gamma-BHC
    58-89-9
    0.0017
    0.066
    Barban
    6
    101-27-9
    0.056
    1.4
    Bendiocarb
    6
    22781-23-3
    0.056
    1.4
    Bendiocarb phenol
    6
    22961-82-6
    0.056
    1.4
    Benomyl
    6
    17804-35-2
    0.056
    1.4
    Benzene
    71-43-2
    0.14
    10
    Benz(a)anthracene
    56-55-3
    0.059
    3.4
    Benzal chloride
    98-87-3
    0.055
    6.0
    Benzene
    71-43-2
    0.14
    10
    Benzo(b)fluoranthene
    (difficult to
    distinguish from
    benzo(k)fluoranthene)
    205-99-2
    0.11
    6.8
    Benzo(k)fluoranthene
    (difficult to
    distinguish from
    benzo(b)fluoranthene)
    207-08-9
    0.11
    6.8
    Benzo(g,h,i)perylene
    191-24-2
    0.0055
    1.8
    Benzo(a)pyrene
    50-32-8
    0.061
    3.4
    Bromodichloro methane
    75-27-4
    0.35
    15
    Methyl bromide (Bromo
    -
    methane)
    74-83-9
    0.11
    15
    4-Bromo phenyl phenyl
    ether
    101-55-3
    0.055
    15
    n-Butyl alcohol
    71-36-3
    5.6
    2.6
    Butylate
    6
    2008-41-5
    0.042
    1.4
    482
    Butyl benzyl phthalate
    85-68-7
    0.017
    28
    2-sec-Butyl-4,6-dinitro
    -
    phenol (Dinoseb)
    88-85-7
    0.066
    2.5
    Carbaryl
    6
    63-25-2
    0.006
    0.14
    Carbenzadim
    6
    10605-21-7
    0.056
    1.4
    Carbofuran
    6
    1563-66-2
    0.006
    0.14
    Carbofuran phenol
    6
    1563-38-8
    0.056
    1.4
    Carbon disulfide
    75-15-0
    3.8
    4.8 mg/l TCLP
    Carbon tetrachloride
    56-23-5
    0.057
    6.0
    Carbosulfan
    6
    55285-14-8
    0.028
    1.4
    Chlordane (alpha and
    gamma isomers)
    57-74-9
    0.0033
    0.26
    p-Chloro aniline
    106-47-8
    0.46
    16
    Chloro benzene
    108-90-7
    0.057
    6.0
    Chloro benzilate
    510-15-6
    0.10
    NA
    2-Chloro-1,3-butadiene
    126-99-8
    0.057
    0.28
    Chloro dibromo methane
    124-48-1
    0.057
    15
    Chloro ethane
    75-00-3
    0.27
    6.0
    bis(2-Chloro -
    ethoxy)methane
    111-91-1
    0.036
    7.2
    bis(2-Chloro ethyl)ether
    111-44-4
    0.033
    6.0
    2-Chloro ethyl vinyl
    ether
    110-75-8
    0.062
    NA
    Chloro form
    67-66-3
    0.046
    6.0
    bis(2-Chloro -
    isopropyl)ether
    108-60-1 39638-
    32-9
    0.055
    7.2
    p-Chloro-m-cresol
    59-50-7
    0.018
    14
    2-Chloro ethyl vinyl
    ether
    110-75-8
    0.062
    NA
    Chloro methane (Methyl
    chloride)
    74-87-3
    0.19
    30
    2-Chloro naphthalene
    91-58-7
    0.055
    5.6
    2-Chloro phenol
    95-57-8
    0.044
    5.7
    3-Chloro propylene
    107-05-1
    0.036
    30
    483
    Chrysene
    218-01-9
    0.059
    3.4
    o-Cresol
    95-48-7
    0.11
    5.6
    m-Cresol (difficult to
    distinguish from p-
    cresol)
    108-39-4
    0.77
    5.6
    p-Cresol (difficult to
    distinguish from m-
    cresol)
    106-44-5
    0.77
    5.6
    m-Cumenyl methyl -
    carbamate
    6
    64-00-6
    0.056
    1.4
    Cyclohexanone
    108-94-1
    0.36
    0.75 mg/l TCLP
    1,2-Dibromo-3-chloro
    -
    propane
    96-12-8
    0.11
    15
    Ethylene dibromide (1,2-
    Dibromo ethane)
    106-93-4
    0.028
    15
    Dibromo methane
    74-95-3
    0.11
    15
    2,4-D (2,4-Dichloro
    -
    phenoxyacetic acid)
    94-75-7
    0.72
    10
    o,p'-DDD
    53-19-0
    0.023
    0.087
    p,p'-DDD
    72-54-8
    0.023
    0.087
    o,p'-DDE
    3424-82-6
    0.031
    0.087
    p,p'-DDE
    72-55-9
    0.031
    0.087
    o,p'-DDT
    789-02-6
    0.0039
    0.087
    p,p'-DDT
    50-29-3
    0.0039
    0.087
    Dibenz(a,h) anthra cene
    53-70-3
    0.055
    8.2
    Dibenz(a,e)pyrene
    192-65-4
    0.061
    NA
    1,2-Dibromo-3-chloro
    -
    propane
    96-12-8
    0.11
    15
    1,2-Dibromo -
    ethane/Ethylene
    dibromide
    106-93-4
    0.028
    15
    Dibromo methane
    74-95-3
    0.11
    15
    m-Dichloro benzene
    541-73-1
    0.036
    6.0
    o-Dichloro benzene
    95-50-1
    0.088
    6.0
    p-Dichloro benzene
    106-46-7
    0.090
    6.0
    Dichloro difluoro methane
    75-71-8
    0.23
    7.2
    484
    1,1-Dichloro ethane
    75-34-3
    0.059
    6.0
    1,2-Dichloro ethane
    107-06-2
    0.21
    6.0
    1,1-Dichloro ethylene
    75-35-4
    0.025
    6.0
    trans-1,2-Dichloro
    -
    ethylene
    156-60-5
    0.054
    30
    2,4-Dichloro phenol
    120-83-2
    0.044
    14
    2,6-Dichloro phenol
    87-65-0
    0.044
    14
    2,4-Dichloro -
    phenoxyacetic acid/2,4-D
    94-75-7
    0.72
    10
    1,2-Dichloro propane
    78-87-5
    0.85
    18
    cis-1,3-Dichloro -
    propylene
    10061-01-5
    0.036
    18
    trans-1,3-Dichloro
    -
    propylene
    10061-02-6
    0.036
    18
    Dieldrin
    60-57-1
    0.017
    0.13
    Diethylene glycol,
    dicarbamate
    6
    5952-26-1
    0.056
    1.4
    Diethyl phthalate
    84-66-2
    0.20
    28
    p-Dimethylaminoazo
    -
    benzene
    60-11-7
    0.13
    NA
    2,4-Dimethyl phenol
    105-67-9
    0.036
    14
    Dimethyl phthalate
    131-11-3
    0.047
    28
    Dimetilan
    6
    644-64-4
    0.056
    1.4
    Di-n-butyl phthalate
    84-74-2
    0.057
    28
    1,4-Dinitro benzene
    100-25-4
    0.32
    2.3
    4,6-Dinitro-o-cresol
    534-52-1
    0.28
    160
    2,4-Dinitro phenol
    51-28-5
    0.12
    160
    2,4-Dinitro toluene
    121-14-2
    0.32
    140
    2,6-Dinitro toluene
    606-20-2
    0.55
    28
    Di-n-octyl phthalate
    117-84-0
    0.017
    28
    p-Dimethylaminoazo
    -
    benzene
    60-11-7
    0.13
    NA
    Di-n-propylnitros
    amine
    621-64-7
    0.40
    14
    1,4-Dioxane
    123-91-1
    NA12.0
    170
    485
    Diphenylamine (difficult
    to distinguish from
    diphenylnitrosamine)
    122-39-4
    0.92
    13
    Diphenylnitros amine
    (difficult to
    distinguish from
    diphenylamine)
    86-30-6
    0.92
    13
    1,2-Diphenylhydrazine
    122-66-7
    0.087
    NA
    Disulfoton
    298-04-4
    0.017
    6.2
    Dithiocarbamates
    (total)
    6
    137-30-4
    0.028
    28
    Endosulfan I
    939-98-8 959-98-
    8
    0.023
    0.066
    Endosulfan II
    33213-6-5 33213-
    65-9
    0.029
    0.13
    Endosulfan sulfate
    1-31-07-8 1031-
    07-8
    0.029
    0.13
    Endrin
    72-20-8
    0.0028
    0.13
    Endrin aldehyde
    7421-93-4
    0.025
    0.13
    EPTC
    6
    759-94-4
    0.042
    1.4
    Ethyl acetate
    141-78-6
    0.34
    33
    Ethyl cyanide
    (Propanenitrile)
    107-12-0
    0.24
    360
    Ethyl benzene
    100-41-4
    0.057
    10
    Ethyl cyanide
    (Propanenitrile)
    107-12-0
    0.24
    360
    Ethyl ether
    60-29-7
    0.12
    160
    bis(2-Ethylhexyl)
    phthalate
    117-81-7
    0.28
    28
    Ethyl methacrylate
    97-63-2
    0.14
    160
    Ethylene oxide
    75-21-8
    0.12
    NA
    bis(2-Ethylhexyl)
    phthalate
    117-81-7
    0.28
    28
    Famphur
    52-85-7
    0.017
    15
    Fluoranthene
    206-44-0
    0.068
    3.4
    Fluorene
    86-73-7
    0.059
    3.4
    Formetanate hydro
    -
    chloride
    6
    23422-53-9
    0.056
    1.4
    486
    Formparanate
    6
    17702-57-7
    0.056
    1.4
    Heptachlor
    76-44-8
    0.0012
    0.066
    Heptachlor epoxide
    1024-57-3
    0.016
    0.066
    Hexachloro benzene
    118-74-1
    0.055
    10
    Hexachloro butadiene
    87-68-3
    0.055
    5.6
    Hexachloro -
    cyclopentadiene
    77-47-4
    0.057
    2.4
    HxCDDs (All Hexachloro
    -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    HxCDFs (All Hexachloro
    -
    dibenzofurans)
    NA
    0.000063
    0.001
    Hexachloro ethane
    67-72-1
    0.055
    30
    Hexachloro propylene
    1888-71-7
    0.035
    30
    Indeno (1,2,3-c,d)
    pyrene
    193-39-5
    0.0055
    3.4
    Iodomethane
    74-88-4
    0.19
    65
    Isobutyl alcohol
    78-83-1
    5.6
    170
    Isodrin
    465-73-6
    0.021
    0.066
    Isolan
    6
    119-38-0
    0.056
    1.4
    Isosafrole
    120-58-1
    0.081
    2.6
    Kepone
    143-50-8 143-50-
    0
    0.0011
    0.13
    Methacrylonitrile
    126-98-7
    0.24
    84
    Methanol
    67-56-1
    5.6
    0.75 mg/l TCLP
    Methapyrilene
    91-80-5
    0.081
    1.5
    Methiocarb
    6
    2032-65-7
    0.056
    1.4
    Methomyl
    6
    16752-77-5
    0.028
    0.14
    Methoxychlor
    72-43-5
    0.25
    0.18
    3-Methylcholanthrene
    56-49-5
    0.0055
    15
    4,4-Methylene bis(2-
    chloro aniline)
    101-14-4
    0.50
    30
    Methylene chloride
    75-09-2
    0.089
    30
    Methyl ethyl ketone
    78-93-3
    0.28
    36
    Methyl isobutyl ketone
    108-10-1
    0.14
    33
    487
    Methyl methacrylate
    80-62-6
    0.14
    160
    Methyl methansulfonate
    66-27-3
    0.018
    NA
    Methyl parathion
    298-00-0
    0.014
    4.6
    Metolcarb
    6
    1129-41-5
    0.056
    1.4
    Mexacarbate
    6
    315-18-4
    0.056
    1.4
    Molinate
    6
    2212-67-1
    0.042
    1.4
    Naphthalene
    91-20-3
    0.059
    5.6
    2-Naphthylamine
    91-59-8
    0.52
    NA
    o-Nitro aniline
    88-74-4
    0.27
    14
    p-Nitro aniline
    100-01-6
    0.028
    28
    Nitrobenzene
    98-95-3
    0.068
    14
    5-Nitro-o-toluidine
    99-55-8
    0.32
    28
    o-Nitro phenol
    88-75-5
    0.028
    13
    p-Nitro phenol
    100-02-7
    0.12
    29
    N-Nitroso diethyl amine
    55-18-5
    0.40
    28
    N-Nitroso dimethyl amine
    62-75-9
    0.40
    2.3
    N-Nitroso-di-n-butyl
    -
    amine
    924-16-3
    0.40
    17
    N-Nitroso methyl ethyl-
    amine
    10595-95-6
    0.40
    2.3
    N-Nitroso morpholine
    59-89-2
    0.40
    2.3
    N-Nitroso piperidine
    100-75-4
    0.013
    35
    N-Nitrosopyrrol idine
    930-55-2
    0.013
    35
    Oxamyl
    6
    23135-22-0
    0.056
    0.28
    Parathion
    56-38-2
    0.014
    4.6
    Total PCBs (sum of all
    PCB isomers, or all
    Aroclors)
    1336-36-3
    0.10
    10
    Pebulate
    6
    1114-71-2
    0.042
    1.4
    Pentachloro benzene
    608-93-5
    0.055
    10
    PeCDDs (All Pentachloro
    -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    PeCDFs (All Pentachloro
    -
    NA
    0.000035
    0.001
    488
    dibenzofurans)
    Pentachloro ethane
    76-01-7
    0.055
    6.0
    Pentachloro nitrobenzene
    82-68-8
    0.055
    4.8
    Pentachloro phenol
    87-86-5
    0.089
    7.4
    Phenacetin
    62-44-2
    0.081
    16
    Phenanthrene
    85-01-8
    0.059
    5.6
    Phenol
    108-95-2
    0.039
    6.2
    o-Phenylenediamine
    6
    95-54-5
    0.056
    5.6
    Phorate
    298-02-2
    0.021
    4.6
    Phthalic acid
    100-21-0
    0.055
    28
    Phthalic anhydride
    85-44-9
    0.055
    28
    Physostigmine
    6
    57-47-6
    0.056
    1.4
    Physostigmine
    salicylate
    6
    57-64-7
    0.056
    1.4
    Promecarb
    6
    2631-37-0
    0.056
    1.4
    Pronamide
    23950-58-5
    0.093
    1.5
    Propham
    6
    122-42-9
    0.056
    1.4
    Propoxur
    6
    114-26-1
    0.056
    1.4
    Prosulfocarb
    6
    52888-80-9
    0.042
    1.4
    Pyrene
    129-00-0
    0.067
    8.2
    Pyridine
    110-86-1
    0.014
    16
    Safrole
    94-59-7
    0.081
    22
    Silvex (2,4,5-TP)
    93-72-1
    0.72
    7.9
    2,4,5-T (2,4,5-
    Trichloro phenoxyacetic
    acid)
    93-76-5
    0.72
    7.9
    1,2,4,5-Tetrachloro
    -
    benzene
    95-94-3
    0.055
    14
    TCDDs (All Tetrachloro
    -
    dibenzo-p-dioxins)
    NA
    0.000063
    0.001
    TCDFs (All Tetrachloro
    -
    dibenzofurans)
    NA
    0.000063
    0.001
    1,1,1,2-Tetrachloro
    -
    ethane
    630-20-6
    0.057
    6.0
    489
    1,1,2,2-Tetrachloro
    -
    ethane
    79-34-6 79-34-5
    0.057
    6.0
    Tetrachloro ethylene
    127-18-4
    0.056
    6.0
    2,3,4,6-Tetrachloro
    -
    phenol
    58-90-2
    0.030
    7.4
    Thiodicarb
    6
    59669-26-0
    0.019
    1.4
    Thiophanate-methyl
    6
    23564-05-8
    0.056
    1.4
    Tirpate
    6
    26419-73-8
    0.056
    0.28
    Toluene
    108-88-3
    0.080
    10
    Toxaphene
    8001-35-2
    0.0095
    2.6
    Triallate
    6
    2303-17-5
    0.042
    1.4
    Bromoform ( Tribromo -
    methane (Bromoform )
    75-25-2
    0.63
    15
    1,2,4-Trichloro benzene
    120-82-1
    0.055
    19
    1,1,1-Trichloro ethane
    71-55-6
    0.054
    6.0
    1,1,2-Trichloro ethane
    79-00-5
    0.054
    6.0
    Trichloro ethylene
    79-01-6
    0.054
    6.0
    Trichloro monofluoro -
    methane
    75-69-4
    0.020
    30
    2,4,5-Trichloro phenol
    95-95-4
    0.18
    7.4
    2,4,6-Trichloro phenol
    88-06-2
    0.035
    7.4
    2,4,5-Trichloro phenoxy -
    acetic acid/2,4,5-T
    93-76-5
    0.72
    7.9
    1,2,3-Trichloro propane
    96-18-4
    0.85
    30
    1,1,2-Trichloro-1,2,2-
    trifluoro ethane
    76-13-1
    0.057
    30
    Triethylamine
    6
    101-44-8
    0.081
    1.5
    tris-(2,3-Dibromo
    propyl)
    phosphate
    126-72-7
    0.11
    0.10
    Vernolate
    6
    1929-77-7
    0.042
    1.4
    Vinyl chloride
    75-01-4
    0.27
    6.0
    Xylenes-mixed isomers
    (sum of o -, m-, and p-
    xylene concentrations)
    1330-20-7
    0.32
    30
    Antimony
    7440-36-0
    1.9
    2.1 mg/l TCLP
    490
    Arsenic
    7440-38-2
    1.4
    5.0 mg/l TCLP
    Barium
    7440-39-3
    1.2
    7.6 mg/l TCLP
    Beryllium
    7440-41-7
    0.82
    0.014 mg/l TCLP
    Cadmium
    7440-43-9
    0.69
    0.19 mg/l TCLP
    Chromium (Total)
    7440-47-3
    2.77
    0.86 mg/l TCLP
    Cyanides (Total)
    4
    57-12-5
    1.2
    590
    Cyanides (Amenable)
    4
    57-12-5
    0.86
    30
    Fluoride
    5
    16964-48-
    816984-48-8
    35
    NA
    Lead
    7439-92-1
    0.69
    0.37 mg/l TCLP
    Mercury-Nonwastewater
    from Retort
    7439-97-6
    NA
    0.20 mg/l TCLP
    Mercury-All Others
    7439-97-6
    0.15
    0.025 mg/l TCLP
    Nickel
    7440-02-0
    3.98
    5.0 mg/l TCLP
    Selenium
    7782-49-2
    0.82
    0.16 mg/l TCLP
    Silver
    7440-22-4
    0.43
    0.30 mg/l TCLP
    Sulfide
    8496-25-8 18496-
    25-8
    14
    NA
    Thallium
    7440-28-0
    1.4
    0.078 mg/l TCLP
    Vanadium
    5
    7440-62-2
    4.3
    0.23 mg/l TCLP
    Zinc
    5
    7440-66-6
    2.61
    5.3 mg/l TCLP
    1
    CAS means Chemical Abstract Services. When the waste code or regulated
    constituents are described as a combination of a chemical with its salts
    or esters, the CAS number is given for the parent compound only.
    2
    Concentration standards for wastewaters are expressed in mg/l are based
    on analysis of composite samples.
    3
    Except for metals (EP or TCLP) and cyanides (total and amenable), the
    nonwastewater treatment standards expressed as a concentration were
    established, in part, based on incineration in units operated in
    accordance with the technical requirements of 35 Ill. Adm. Code
    724.Subpart O or 35 Ill. Adm. Code 725.Subpart O or on combustion in
    fuel substitution units operating in accordance with applicable
    technical requirements. A facility may comply with these treatment
    standards according to provisions in 40 CFR 268.40(d). All
    concentration standards for nonwastewaters are based on analysis of grab
    samples.
    4
    Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to
    be analyzed using Method 9010 or 9012, found in "Test Methods for
    Evaluating Solid Waste, Physical/Chemical Methods", USEPA Publication
    SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111, with a
    sample size of 10 grams and a distillation time of one hour and 15
    491
    minutes.
    5 Vanadium and zinc
    These constituents
    are not "underlying hazardous
    constituents" in characteristic wastes, according to the definition at
    Section 728.102(i).
    6
    This footnote corresponds with note 6 to the table to 40 CFR 268.48(a),
    which has already expired by its own terms. This statement maintains
    structural consistency with the federal regulations.
    Note: NA means not applicable.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 733
    STANDARDS FOR UNIVERSAL WASTE MANAGEMENT
    SUBPART A: GENERAL
    Section
    733.101
    Scope
    733.102
    Applicability--Batteries
    733.103
    Applicability--Pesticides
    733.104
    Applicability--Mercury Thermostats
    733.105
    Applicability--Household and Conditionally Exempt Small Quantity
    Generator Waste
    733.106
    Definitions
    SUBPART B: STANDARDS FOR SMALL QUANTITY HANDLERS
    Section
    733.110
    Applicability
    733.111
    Prohibitions
    733.112
    Notification
    733.113
    Waste Management
    733.114
    Labeling and Marking
    733.115
    Accumulation Time Limits
    733.116
    Employee Training
    733.117
    Response to Releases
    733.118
    Off-Site Shipments
    733.119
    Tracking Universal Waste Shipments
    733.120
    Exports
    SUBPART C: STANDARDS FOR LARGE QUANTITY HANDLERS
    Section
    733.130
    Applicability
    733.131
    Prohibitions
    733.132
    Notification
    733.133
    Waste Management
    733.134
    Labeling and Marking
    733.135
    Accumulation Time Limits
    733.136
    Employee Training
    733.137
    Response to Releases
    733.138
    Off-Site Shipments
    733.139
    Tracking Universal Waste Shipments
    733.140
    Exports
    492
    SUBPART D: STANDARDS FOR UNIVERSAL WASTE TRANSPORTERS
    Section
    733.150
    Applicability
    733.151
    Prohibitions
    733.152
    Waste Management
    733.153
    Accumulation Time Limits
    733.154
    Response to Releases
    733.155
    Off-site Shipments
    733.156
    Exports
    SUBPART E: STA NDARDS FOR DESTINATION FACILITIES
    Section
    733.160
    Applicability
    733.161
    Off-Site Shipments
    733.162
    Tracking Universal Waste Shipments
    SUBPART F: IMPORT REQUIREMENTS
    Section
    733.170
    Imports
    SUBPART G: PETITIONS TO INCLUDE OTHER WASTES
    Section
    733.180
    General
    733.181
    Factors for Petitions to Include Other Wastes
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R95-20 at 20 Ill. Reg. 11291, effective August 1, 1996
    ;
    amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
    ____________________
    .
    SUBPART B: STANDARDS FOR SMALL QUANTITY HANDLERS
    Section 733.120
    Exports
    A small quantity handler of universal waste that sends universal waste to a
    foreign destination
    other than to those OECD countries specified in 35 Ill.
    Adm. Code 722.158(a)(1) (in which case the handler is subject to the
    requirements of 35 Ill. Adm. Code 722.Subpart H)
    shall:
    a)
    Comply with the requirements applicable to
    a primary exporter in
    35 Ill. Adm. Code 722.153; 722.156(a)(1) through (a)(4), (a)(6),
    and (b); and 722.157;
    b)
    Export such universal waste only upon consent of the receiving
    country and in conformance with the USEPA Acknowledgement of
    Consent, as defined in 35 Ill. Adm. Code 722.Subpart E; and
    c)
    Provide a copy of the USEPA Acknowledgment of Consent for the
    shipment to the transporter transporting the shipment for export.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART C: STANDARDS FOR LARGE QUANTITY HANDLERS
    Section 733.140
    Exports
    A large quantity handler of universal waste that sends universal waste to a
    493
    foreign destination
    other than to those OECD countries specified in 35 Ill.
    Adm. Code 722.158(a)(1) (in which case the handler is subject to the
    requirements of 35 Ill. Adm. Code 722.Subpart H)
    shall:
    a)
    Comply with the requirements applicable to a primary exporter in
    35 Ill. Adm. Code 722.153; 722.156(a)(1) through (a)(4), (a)(6),
    and (b); and 722.157;
    b)
    Export such universal waste only upon consent of the receiving
    country and in conformance with the USEPA Acknowledgement of
    Consent as defined in 35 Ill. Adm. Code 722.Subpart E; and
    c)
    Provide a copy of the USEPA Acknowledgement of Consent for the
    shipment to the transporter transporting the shipment for export.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART D: STANDARDS FOR UNIVERSAL WASTE TRANSPORTERS
    Section 733.156
    Exports
    A universal waste transporter transporting a shipment of universal waste to a
    foreign destination
    other than to those OECD countries specified in 35 Ill.
    Adm. Code 722.158(a)(1) (in which case the transporter is subject to the
    requirements of 35 Ill. Adm. Code 722.Subpart H)
    may not accept a shipment if
    the transporter knows the shipment does not conform to the USEPA
    Acknowledgment of Consent. In addition the transporter shall ensure the
    following:
    a)
    A copy of the USEPA Acknowledgment of Consent accompanies the
    shipment; and
    b)
    The shipment is delivered to the facility designated by the person
    initiating the shipment.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART F: IMPORT REQUIREMENTS
    Section 733.170
    Imports
    Persons managing universal waste that is imported from a foreign country into
    the United States are subject to the applicable requirements of this Part
    immediately after the waste enters the United States, as
    follows indicated in
    subsections (a) through (c) below
    :
    a)
    A universal w aste transporter is subject to the universal waste
    transporter requirements of 733.Subpart D.
    b)
    A universal waste handler is subject to the small or large
    quantity handler of universal waste requirements of 733.Subpart B
    or C, as applicable.
    c)
    An owner or operator of a destination facility is subject to the
    destination facility requirements of 733.Subpart E.
    d)
    Persons managing universal waste that is imported from an OECD
    country as specified in 35 Ill. Adm. Code 722.158(a)(1) are
    subject to subsections (a) through (c) above, in addition to the
    494
    requirements of 35 Ill. Adm. Code 722.Subpart H.
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER d: UNDERGROUND INJECTION CONTROL AND UNDERGROUND
    STORAGE TANK PROGRAMS
    PART 738
    HAZARDOUS WASTE INJECTION RESTRICTIONS
    SUBPART A: GENERAL
    Section
    738.101
    Purpose Scope and Applicability
    738.102
    Definitions
    738.103
    Dilution Prohibited as a Substitute
    for Treatment
    738.104
    Case-by-Case Extensions of an Effective Date
    738.105
    Waste Analysis
    SUBPART B: PROHIBITIONS ON INJECTION
    Section
    738.110
    Waste Specific Prohibitions - Solvent Wastes
    738.111
    Waste Specific Prohibitions - Dioxin-Containing Wastes
    738.112
    Waste Specific Prohibitions - California List Wastes
    738.114
    Waste Specific Prohibitions - First Third Wastes
    738.115
    Waste Specific Prohibitions - Second Third Wastes
    738.116
    Waste Specific Prohibitions - Third Third Wastes
    738.117
    Waste Specific Pr
    ohibitions - Newly-Listed Wastes
    738.118
    Waste specific prohibitions
    --Newly Identified Wastes
    SUBPART C: PETITION STANDARDS AND PROCEDURES
    Section
    738.120
    Petitions to Allow Injection of a Prohibited Waste
    738.121
    Required Information to Support Petitions
    738.122
    Submission, Review and Approval or Denial of Petitions
    738.123
    Review of Adjusted Standards
    738.124
    Termination of Adjusted Standards
    AUTHORITY: Implementing Section 13 and 22.4 and authorized by Section 27 of
    the Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
    SOURCE: Adopted in R89-2 at 14 Ill. Reg. 3059, effective February 20, 1990;
    amended in R89-11 at 14 Ill. Reg. 11948, effective July 9, 1990; amended in
    R90-14 at 15 Ill. Reg. 11425, effective July 24, 1991; amended in R92-13 at 17
    Ill. Reg. 6190, effective April 5, 1993; amended in R93-6 at 17 Ill. Reg.
    15641, effective September 14, 1993; amended in R95-4 at 19 Ill. Reg. 9501,
    effective June 27, 1995
    ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
    ________, effective ____________________
    .
    SUBPART A: GENERAL
    Section 738.101
    Purpose Scope and Applicability
    a)
    This Part identifies hazardous wastes that are restricted from
    disposal into Class I
    hazardous waste injection
    wells and defines
    those circumstances under which a waste, otherwise prohibited from
    injection, may be injected.
    495
    b)
    The requirements of this Part apply to owners or operators of
    the
    following Class I wells:
    1)
    hHazardous waste injection wells
    that are used to inject
    hazardous waste ; and
    2)
    Injection wells that are used to inject wastes which once
    exhibited a prohibited characteristic of hazardous waste
    identified in 35 Ill. Adm. Code 721.Subpart C, at the point
    of generation, and which no longer exhibit the
    characteristic at the point of injection
    .
    c)
    Wastes otherwise prohibited from injection may continue to be
    injected:
    1)
    If an extension from the effective date of a prohibition has
    been granted pursuant to Section 738.104; or
    2)
    If an adjusted standard has been granted in response to a
    petition filed under Section 738.120; or
    3)
    If the waste is generated by a conditionally exempt small
    quantity generator, as defined in 35 Ill. Adm. Code 721.105.
    d) WA wastes that areis hazardous only because
    theyit exhibit s a
    hazardous characteristic , and which of hazardous waste and which
    areis otherwise prohibited from injection under this Part
    or 35
    Ill. Adm. Code 728
    , areis not prohibited from injection if
    the
    following is true of
    the waste s:
    1) AreIt is disposed into a
    Class I nonhazardous waste
    injection well or a Class I hazardous waste injection well
    that receives only non-prohibited hazardous wastes
    , as such
    are defined under 35 Ill. Adm. Code 730.106(a); and
    2) DoIt does not exhibit any prohibited characteristic of
    hazardous waste identified in 35 Ill. Adm. Code 721.Subpart
    C at the point of injection.
    BOARD NOTE: The exemption for injection of diluted
    hazardous waste in this subsection was the subject of
    litigation in Chemical Waste Management et al. v. USEPA, 976
    F.2d 2 (D.C. Cir. 1992). The USEPA response to the mandate
    in this litigation may result in the repeal or modification
    of 40 CFR 148.1(d), from which this subsection is derived.
    USEPA responded to the remand by issuing an interim final
    rule on May 24, 1993, at 58 Fed. Reg. 29860, but that action
    did not directly affect 40 CFR 148.1. The Board views any
    federal court decision on the effectiveness or
    enforceability of the USEPA rule as binding on this
    subsection.
    BOARD NOTE: Derived from 40 CFR 148.1 (199
    26), as amended
    at 57 Fed. Reg. 31963 (July 20, 1992)
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 738.103
    Dilution Prohibited as a Substitute for
    Treatment
    The prohibition of 35 Ill. Adm. Code 728.103 shall apply to owners or
    496
    operators of Class I hazardous waste injection wells.
    a)
    The provisions of 35 Ill. Adm. Code 728.103 shall apply to owners
    or operators of Class I wells used to inject a waste that is
    hazardous at the point of generation whether or not the waste is
    hazardous at the point of injection.
    b)
    Owners or operators of Class I nonhazardous waste injection wells
    that inject waste formerly exhibiting a hazardous characteristic
    which has been removed by dilution may address underlying
    hazardous constituents by treating the hazardous waste, obtaining
    an exemption pursuant to a petition filed under Section 738.120,
    or complying with the provisions set forth in 35 Ill. Adm. Code
    728.109.
    BOARD NOTE: Derived from 40 CFR 148.3 (19
    8896), as added at 53 Fed. Reg.
    28155, July 26, 1988
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 738.104
    Case-by-Case Extensions of an Effective Date
    The owner or operator of a Class I hazardous
    or nonhazardous waste injection
    well may submit an application to
    USEPA for an extension of the effective date
    of any applicable prohibition established under Subpart B. (See 35 Ill. Adm.
    Code 728.105.)
    BOARD NOTE: Derived from 40 CFR 148.4 (19
    8896), as added at 53 Fed. Reg.
    28155, July 26, 1988
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    SUBPART B: PROHIBITIONS ON INJECTION
    Section 738.117
    Waste Specific Prohibitions - Newly-Listed Wastes
    a)
    The wastes specified in 35 Ill. Adm. Code 721.Subpart D by the
    following U .S. EPA hazardous waste numbers are prohibited from
    underground injection:
    F037
    F038
    K107
    K108
    K109
    K110
    K111
    K112
    K117
    K118
    K123
    K124
    K125
    K126
    K131
    K136
    U328
    U353
    U359
    497
    b)
    The wa stes specified in 35 Ill. Adm. Code 721.Subpart D by the
    following U .S. EPA hazardous waste numbers are prohibited from
    underground injection:
    K141
    K142
    K143
    K144
    K145
    K147
    K148
    K149
    K150
    K151
    c) Effective September 19, 1995, the wastes specified in 35 Ill. Adm.
    Code 721.Subpart C by the following U.S. EPA hazardous waste
    numbers are prohibited from underground injection:
    D001 (high TOC subcategory, as specified at 35 Ill.
    Adm. Code 728.140)
    D012
    D013
    D014
    D015
    D016
    D017
    c)
    This subsection corresponds with 40 CFR 148.17(c), removed and
    marked "reserved" by USEPA at 61 Fed. Reg. 15662 (Apr. 8, 1996).
    This statement maintains structural consistency with USEPA rules.
    d)
    Effective June 30, 1995, the wastes specified in 35 Ill. Adm. Code
    721.Subpart D by the following U
    .S. EPA hazardous waste numbers
    are prohibited from underground injection:
    K117
    K118
    K131
    K132
    e)
    The requirements of subsections (a) and (b) above do no
    t apply:
    1)
    If the wastes meet or are treated to meet the applicable
    standards specified in 35 Ill. Adm. Code 728.Subpart D; or
    2)
    If an adjusted standard has been granted in response to a
    petition under 738.Subpart C; or
    3)
    During the period of extension of the applicable effective
    date, if an extension is granted under Section 738.104.
    BOARD NOTE: Derived from 40 CFR 148.17
    , as added at 57 Fed.
    Reg. 37263 (Aug. 18, 1992)
    (1996) .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    Section 738.118
    Waste specific prohibitions
    --Newly Identified Wastes
    a)
    The wastes specified in 35 Ill. Adm. Code 721.132 as having the
    following USEPA hazardous waste numbers are prohibited from
    498
    underground injection:
    K156
    K157
    K158
    K159
    K160
    K161
    P127
    P128
    P185
    P188
    P189
    P190
    P191
    P192
    P194
    P196
    P197
    P198
    P199
    P201
    P202
    P203
    P204
    P205
    U271
    U277
    U278
    U279
    U280
    U364
    U365
    U366
    U367
    U372
    U373
    U375
    U376
    U377
    U378
    U379
    U381
    U382
    U383
    U384
    U385
    U386
    U387
    U389
    U390
    U391
    U392
    U393
    U394
    U395
    U396
    U400
    U401
    U402
    U403
    499
    U404
    U407
    U409
    U410
    U411
    b)
    The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA
    Hazardous waste number K088 is prohibited from underground
    injection.
    c)
    On April 8, 1998, the wastes specified in 35 Ill. Adm. Code 721 as
    having the following USEPA Hazardous waste numbers and Mixed
    TC/Radioactive wastes are prohibited from underground injection:
    D018
    D019
    D020
    D021
    D022
    D023
    D024
    D025
    D026
    D027
    D028
    D029
    D030
    D031
    D032
    D033
    D034
    D035
    D036
    D037
    D038
    D039
    D040
    D041
    D042
    D043
    d)
    On April 8, 1998, the wastes specified in 35 Ill. Adm. Code 721 as
    having the following USEPA Hazardous waste numbers are prohibited
    from underground injection:
    D001
    D002
    D003
    (Source: Added at 21 Ill. Reg. ________, effective ______________________)
    SUBPART C: PETITION STANDARDS AND PROCEDURES
    Section 738.120
    Petitions to Allow Injection of a Prohibited Waste
    a)
    Any person seeking an exemption from a prohibition under Subpart B
    for the injection of a restricted hazardous waste
    into an
    injection well or wells
    , including a hazardous waste that exhibits
    a characteristic of hazardous waste and which contains underlying
    hazardous constituents at the point of generation, but which no
    500
    longer exhibits a characteristic of hazardous waste when injected
    into a Class I injection well or wells,
    shall submit a petition
    for an adjusted standard to the Board, pursuant to 35 Ill. Adm.
    Code 106.Subpart G, demonstrating that, to a reasonable degree of
    certainty, there will be no migration of hazardous constituents
    from the injection zone for as long as the waste remains
    hazardous. This demonstration requires a showing that:
    1)
    The hydrogeological and geochemical conditions at the
    site(s) and the physiochemical nature of the waste stream(s)
    are such that reliable predictions can be made that:
    A)
    Fluid movement conditions are such that the injected
    fluids will not migrate within 10,000 years:
    i)
    Vertically upward out of the injection zone; or
    ii)
    Laterally within the injection zone to a point
    of discharge or interface with an Underground
    Source of Drinking Water (USDW) as defined in 35
    Ill. Adm. Code 730; or
    B)
    Before the injected fluids migrate out of the
    injection zone or to a point of discharge or interface
    with USDW, the fluid will no longer be hazardous
    because of attenuation, transformation, or
    immobilization of hazardous constituents within the
    injection zone by hydrolysis, chemical interactions or
    other means; and
    2)
    For each well the petition has:
    A)
    Demonstrated that the injection well's area of review
    complies with the substantive requirements of 35 Ill.
    Adm. Code 730.163;
    B)
    Located, identified, and ascertained the condition of
    all wells within the injection well's area of review
    (as specified in 35 Ill. Adm. Code 730.163) that
    penetrate the injection zone or the confining zone by
    use of a protocol acceptable to the Board that meets
    the substantive requirements of 35 Ill. Adm. Code
    730.164;
    C)
    Submitted a corrective action plan that meets the
    substantive requirements of 35 Ill. Adm. Code 730.164,
    the implementation of which shall become a condition
    of any adjusted standard granted; and
    D)
    Submitted the results of pressure and radioactive
    tracer tests performed within one year prior to
    submission of the petition demonstrating the
    mechanical integrity of the well's long string casing,
    injection tube, annular seal, and bottom hole cement.
    In cases where the petition has not been approved or
    denied within one year after the initial demonstration
    of mechanical integrity, the Board may require the
    owner or operator to perform the tests again and
    submit the results of the new tests.
    BOARD NOTE: The requirements of subsection (a)(2)
    501
    need not be incorporated in a permit at the time the
    Board grants an adjusted standard.
    b)
    A demonstration under subsection (a)(1)(A) must identify the
    strata within the injection zone which will confine fluid movement
    above the injection interval and include a showing that this
    strata is free of known transmissive faults of fractures and that
    there is a confining zone above the injection zone.
    c)
    A demonstration under subsection (a)(1)(B) must identify the
    strata within the injection zone where waste transformation will
    be accomplished and include a showing that this strata is free of
    known transmissive faults or fractures and that there is a
    confining zone above the injection zone.
    d)
    A demonstration may include a showing that:
    1)
    Treatment methods that reduce the toxicity or mobility of
    the wastes, the implementation of which will become a
    condition of any adjusted standard, must be utilized; or
    2)
    A monitoring plan, the implementation of which will become a
    condition of any adjusted standard, must be utilized to
    enhance confidence in one or more aspects of the
    demonstration.
    e)
    Any person whothat has been granted an adjusted standard pursuant
    to this Section may submit a petition for reissuance of the
    adjusted standard to include an additional restricted waste or
    wastes or to modify any conditions placed on that adjusted
    standard by the Board. The Board will reissue the adjusted
    standard if the petitioner complies with subsections (a), (b) and
    (c).
    f)
    Any person whothat has been granted an adjusted standard pursuant
    to this Section may submit a petition to modify that adjusted
    standard to include an additional (hazardous) waste or wastes.
    The Board may grant the modification if it determines, to a
    reasonable degree of certainty, that the additional waste or
    wastes will behave hydraulically and chemically in a manner
    similar to previously included wastes and that it will not
    interfere with the containment capability of the injection zone.
    BOARD NOTE: Derived from 40 CFR 148.20 (19
    8896), as added at 53
    Fed. Reg. 28155, July 26, 1988
    .
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE G: WASTE DISPOSAL
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
    PART 739
    STANDARDS FOR THE MANAGEMENT OF USED OIL
    SUBPART A: DEFINITIONS
    Section
    739.100
    Definitions
    502
    SUBPART B: APPLICABILITY
    Section
    739.110
    Applicability
    739.111
    Used oil specifications
    739.112
    Prohibitions
    SUBPART C: STANDARDS FOR USED OIL GENERATORS
    Section
    739.120
    Applicability
    739.121
    Hazardous waste mixing
    739.122
    Used oil storage
    739.123
    On-site burning in space heaters
    739.124
    Off-site shipments
    SUBPART D: STANDARDS FOR USED OIL COLLECTION CENTERS AND
    AGGREGATION POINTS
    Section
    739.130
    Do-it-yourselfer used oil collection centers
    739.131
    Used oil collection centers
    739.132
    Used oil aggregate points owned by the generator
    SUBPART E: STANDARDS FOR USED OIL TRANSPORTER AND TRANSFER
    FACILITIES
    Section
    739.140
    Applicability
    739.141
    Restrictions on transporters that are not als
    o processors
    739.142
    Notification
    739.143
    Used oil transportation
    739.144
    Rebuttable presumption for used oil
    739.145
    Used oil storage at transfer facilities
    739.146
    Tracking
    739.147
    Management of residues
    SUBPART F: STANDARDS FOR USED OIL PROCESSORS
    Section
    739.150
    Applicability
    739.151
    Notification
    739.152
    General facility standards
    739.153
    Rebuttable presumption for used oil
    739.154
    Used oil management
    739.155
    Analysis plan
    739.156
    Tracking
    739.157
    Operating record and reporting
    739.158
    Off-site shipm ents of used oil
    739.159
    Management of residues
    SUBPART G: STANDARDS FOR USED OIL BURNERS THAT BURN
    OFF-SPECIFICATION USED OIL FOR ENERGY RECOVERY
    Section
    739.160
    Applicability
    739.161
    Restriction on burning
    739.162
    Notification
    739.163
    Rebuttable presumption for used oil
    739.164
    Used oil storage
    739.165
    Tracking
    739.166
    Notices
    739.167
    Management of residues
    SUBPART H: STANDARDS FOR USED OIL FUEL MARKETERS
    Section
    739.170
    Applicability
    503
    739.171
    Prohibitions
    739.172
    On-specification used oil fuel
    739.173
    Notification
    739.174
    Tracking
    739.175
    Notices
    SUBPART I: STANDARDS FOR USE AS A DUST SUPPRESSANT DISPOSAL OF USED OIL
    Section
    739.180
    Applicability
    739.181
    Disposal
    739.182
    Use as a dust suppressant
    AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
    Environmental Protection Act [415 ILCS 5/22.4 and 27].
    SOURCE: Adopted in R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993;
    amended in R93-16 at 18 Ill. Reg. 6931, effective April 26, 1994; amended in
    R94-17 at 18 Ill. Reg. 17616, effective November 23, 1994; amended in R95-6 at
    19 Ill. Reg. 10036, effective June 27, 1995
    ; amended in R96-10/R97-3/R97-5 at
    21 Ill. Reg. ________, effective ____________________
    .
    SUBPART B: APPLICABILITY
    Section 739.110
    Applicability
    This Section identifies those materials which are subject to regulation as
    used oil under this Part. This Section also identifies some materials that
    are not subject to regulation as used oil under this Part, and indicates
    whether these materials may be subject to regulation as hazardous waste under
    Parts35 Ill. Adm. Code
    702, 703, 720 through 726, and 728.
    a)
    Used oil. U .S. EPA presumes that used oil is to be recycled
    unless a used oil handler disposes of used oil, or sends used oil
    for disposal. Except as provided in Section 739.111, the
    regulations of this Part apply to used oil, and to materials
    identified in this Section as being subject to regulation as used
    oil, whether or not the used oil or material exhibits any
    characteristics of hazardous waste identified in 35 Ill. Adm. Code
    721.Subpart C.
    b)
    Mixtures of used oil and hazardous waste.
    1)
    Listed hazardous waste.
    A)
    A mixture of used oil and hazardous waste that is
    listed in 35 Ill. Adm. Code 721.Subpart D is subject
    to regulation as hazardous waste under 35 Ill. Adm.
    Code 703, 720 through 726, and 728, rather than as
    used oil under this Part.
    B)
    Rebuttable presumption for used oil. Used oil
    containing more than 1,000 ppm total halogens is
    presumed to be a hazardous waste because it has been
    mixed with halogenated hazardous waste listed in 35
    Ill. Adm. Code 721.Subpart D. Persons may rebut this
    presumption by demonstrating that the used oil does
    not contain hazardous waste (for example, by using an
    analytical method from SW-846, Edition III, to show
    that the used oil does not contain significant
    concentrations of halogenated hazardous constituents
    504
    listed in 35 Ill. Adm. Code 721.Appendix H). U
    .S. EPA
    Publication SW-846, Third Edition, is available from
    the Government Printing Office, Superintendent of
    Documents, P.O. Box 371954, Pittsburgh, PA 15250-7954,
    (202) 783-3238 (document number 955-001-00000-1).
    i)
    The rebuttable presumption does not apply to
    metalworking oils or fluids containing
    chlorinated paraffins, if they are processed,
    through a tolling arrangement as described in
    Section 739.124(c), to reclaim metalworking oils
    or fluids. The presumption does apply to
    metalworking oils or fluids if such oils or
    fluids are recycled in any other manner, or
    disposed.
    ii)
    The reb uttable presumption does not apply to
    used oils contaminated with chlorofluorocarbons
    (CFCs) removed from refrigeration units where
    the CFCs are destined for reclamation. The
    rebuttable presumption does apply to used oils
    contaminated with CFCs that have been mixed with
    used oil from sources other than refrigeration
    units.
    2)
    Characteristic hazardous waste. A mixture of used oil and
    hazardous waste that exhibits a hazardous waste
    characteristic identified in 35 Ill. Adm. Code 721.Subpart C
    and a mixture of used oil and hazardous waste that is listed
    in Subpart D of this Part solely because it exhibits one or
    more of the characteristics of hazardous waste identified in
    35 Ill. Adm. Code 721.Subpart C is subject to:
    A)
    Except as provided in subsection (b)(2)(C) of this
    Section, regulation as hazardous waste under 35 Ill.
    Adm. Code 703, 720 through 726, and 728 rather than as
    used oil under this Part, if the resultant mixture
    exhibits any characteristics of hazardous waste
    identified in 35 Ill. Adm. Code 721.Subpart C; or
    B)
    Except as provided in subsection (b)(2)(C) of this
    Section, regulation as used oil under this Part, if
    the resultant mixture does not exhibit any
    characteristics of hazardous waste identified under 35
    Ill. Adm. Code 721.Subpart C.
    C)
    Regulation as used oil under this Part, if the mixture
    is of used oil and a waste which is hazardous solely
    because it exhibits the characteristic of ignitability
    (e.g., ignitable-only mineral spirits), provided that
    the resultant mixture does not exhibit the
    characteristic of ignitability under 35 Ill. Adm. Code
    721.121.
    3)
    Conditionally exempt small quantity generator hazardous
    waste. A mixture of used oil and conditionally exempt small
    quantity generator hazardous waste regulated under 35 Ill.
    Adm. Code 721.105 is subject to regulation as used oil under
    this Part.
    c)
    Materials containing or otherwise contaminated with used oil.
    505
    1)
    Except as provided in subsection (c)(2) of this Section, a
    material containing or otherwise contaminated with used oil
    from which the used oil has been properly drained or removed
    to the extent possible such that no visible signs of free-
    flowing oil remain in or on the material:
    A)
    Is not used oil, and thus, it is not subject to this
    Part, and
    B)
    If applicable, is subject to the hazardous waste
    regulations of 35 Ill. Adm. Code 703, 705, 720 through
    726, and 728.
    2)
    A material containing or otherwise contaminated with used
    oil that is burned for energy recovery is subject to
    regulation as used oil under this Part.
    3)
    Used oil drained or removed from materials containing or
    otherwise contaminated with used oil is subject to
    regulation as used oil under this Part.
    d)
    Mixtures of used oil with products.
    1)
    Except as provided in subsection (d)(2) below, mixtures of
    used oil and fuels or other fuel products are subject to
    regulation as used oil under this Part.
    2)
    Mixtures of used oil and diesel fuel mixed on-site by the
    generator of the used oil for use in the generator's own
    vehicles are not subject to this Part once the used oil and
    diesel fuel have been mixed. Prior to mixing, the used oil
    is subject to the requirements of Subpart C of this Part.
    e)
    Materials derived from used oil.
    1)
    Materials that are reclaimed from used oil that are used
    beneficially and are not burned for energy recovery or used
    in a manner constituting disposal (e.g., re-refined
    lubricants) are:
    A)
    Not used oil and thus are not subject to this Part,
    and
    B)
    Not solid wastes and are thus not subject to the
    hazardous waste regulations of
    Parts 35 Ill. Adm. Code
    703, 720 through 726, and 728 as provided in 35 Ill.
    Adm. Code 721.103(e)(1).
    2)
    Materials produced from used oil that are burned for energy
    recovery (e.g., used oil fuels) are subject to regulation as
    used oil under this Part.
    3)
    Except as provided in subsection (e)(4) below, materials
    derived from used oil that are disposed of or used in a
    manner constituting disposal are:
    A)
    Not used oil and thus are not subject to this Part,
    and
    B)
    Are solid wastes and thus are subject to the hazardous
    506
    waste regulations of 35 Ill. Adm. Code 703, 720
    through 726, and 728 if the materials are listed or
    identified as hazardous waste.
    4)
    Used oil re-refining distillation bottoms that are used as
    feedstock to manufacture asphalt products are not subject to
    this Part.
    f)
    Wastewater. Wastewater, the discharge of which is subject to
    regulation under either Section 402 or Section 307(b) of the Clean
    Water Act (including wastewaters at facilities which have
    eliminated the discharge of wastewater), contaminated with de
    minimis quantities of used oil are not subject to the requirements
    of this Part. For purposes of this subsection, "de minimis"
    quantities of used oils are defined as small spills, leaks, or
    drippings from pumps, machinery, pipes, and other similar
    equipment during normal operations or small amounts of oil lost to
    the wastewater treatment system during washing or draining
    operations. This exception will not apply if the used oil is
    discarded as a result of abnormal manufacturing operations
    resulting in substantial leaks, spills, or other releases, or to
    used oil recovered from wastewaters.
    g)
    Used oil introduced into crude oil pipelines or a petroleum
    refining facility.
    1)
    Used oil mixed with crude oil or natural gas liquids (e.g.,
    in a production separator or crude oil stock tank) for
    insertion into a crude oil pipeline is exempt from the
    requirements of this Part. The used oil is subject to the
    requirements of this Part prior to the mixing of used oil
    with crude oil or natural gas liquids.
    2)
    Mixtures of used oil and crude oil or natural gas liquids
    containing less than 1% used oil that are being stored or
    transported to a crude oil pipeline or petroleum refining
    facility for insertion into the refining process at a point
    prior to crude distillation or catalytic cracking are exempt
    from the requirements of this Part.
    3)
    Used oil that is inserted into the petroleum refining
    process before crude distillation or catalytic cracking
    without prior mixing with crude oil is exempt from the
    requirements of this Part, provided that the used oil
    contains less than 1% of the crude oil feed to any petroleum
    refining facility process unit at any given time. Prior to
    insertion into the petroleum refining process, the used oil
    is subject to the requirements of this Part.
    4)
    Except as provided in subsection (g)(5) below, used oil that
    is introduced into a petroleum refining facility process
    after crude distillation or catalytic cracking is exempt
    from the requirements of this Part only if the used oil
    meets the specification of Section 739.111. Prior to
    insertion into the petroleum refining facility process, the
    used oil is subject to the requirements of this Part.
    5)
    Used oil that is incidentally captured by a hydrocarbon
    recovery system or wastewater treatment system as part of
    routine process operations at a petroleum refining facility
    and inserted into the petroleum refining facility process is
    507
    exempt from the requirements of this Part. This exemption
    does not extend to used oil that is intentionally introduced
    into a hydrocarbon recovery system (e.g., by pouring
    collected used oil into the wastewater treatment system).
    6)
    Tank bottoms from stock tanks containing exempt mixtures of
    used oil and crude oil or natural gas liquids are exempt
    from the requirements of this Part.
    h)
    Used oil on vessels. Used oil produced on vessels from normal
    shipboard operations is not subject to this Part until it is
    transported ashore.
    i)
    Used oil containing PCBs.
    In addition to the requirements of this
    Part, a marketer or burner of used oil that markets used oil
    containing any quantifiable level of PCBs is subject to the
    requirements of 40 CFR 761.20(e).
    (Source: Amended at 21 Ill. Reg. ________, effective ____________________)

    Back to top