ILLINOIS POLLUTION CONTROL BOARD
    February 6, 1997
    IN THE MATTER OF:
    )
    )
    15% ROP PLAN: CLEAN-UP
    )
    R96-13
    PART II: AMENDMENTS TO
    )
    (Rulemaking-Air)
    35 ILL. ADM. CODE PARTS
    )
    218 AND 219
    )
    Adopted Rule. Final Order. Expedited Correction.
    OPINION AND ORDER OF THE BOARD (by J. Theodore Meyer):
    On October 17, 1996 the Board adopted a final opinion and order in this matter.
    The adopted rules were published in 20 Illinois Register 14462, on November 8, 1996.
    At the request of the Joint Committee on Administrative Rules to correct an omission in
    the Table of Contents, the Board hereby adopts a corrected order in this matter.
    Specifically, the October 17, 1996 final order omitted an amendment’s citation
    and effective date in the Source Note of the Table of Contents for Organic Material
    Emission Standards and Limitations for the Metro East Area (35 Ill. Adm. Code 219).
    Today’s order corrects the error by adding the missing citation and effective date. The
    Board’s final opinion of October 17, 1996 has not been altered.
    ORDER
    The Board directs that the following correction be submitted to the Joint
    Committee on Administrative Rules for final notice pursuant to Section 5-85 of the
    Illinois Administrative Procedure Act.
    TITLE 35: ENVIRONMENTAL PROTECTION
    SUBTITLE B: AIR POLLUTION
    CHAPTER I: POLLUTION CONTROL BOARD
    SUBCHAPTER c: EMISSIONS STANDARDS AND
    LIMITATIONS FOR STATIONARY SOURCES
    PART 219
    ORGANIC MATERIAL EMISSION STANDARDS AND
    LIMITATIONS FOR THE METRO EAST AREA
    SUBPART A: GENERAL PROVISIONS
    Section
    219.100
    Introduction

    2
    219.101
    Savings Clause
    219.102
    Abbreviations and Conversion Factors
    219.103
    Applicability
    219.104
    Definitions
    219.105
    Test Methods and Procedures
    219.106
    Compliance Dates
    219.107
    Operation of Afterburners
    219.108
    Exemptions, Variations, and Alternative Means of Control or Compliance
    Determinations
    219.109
    Vapor Pressure of Volatile Organic Liquids
    219.110
    Vapor Pressure of Organic Material or Solvents
    219.111
    Vapor Pressure of Volatile Organic Material
    219.112
    Incorporations by Reference
    219.113
    Monitoring for Negligibly-Reactive Compounds
    SUBPART B: ORGANIC EMISSIONS FROM STORAGE
    AND LOADING OPERATIONS
    Section
    219.119
    Applicability for VOL
    219.120
    Control Requirements for Storage Containers of VOL
    219.121
    Storage Containers of VPL
    219.122
    Loading Operations
    219.123
    Petroleum Liquid Storage Tanks
    219.124
    External Floating Roofs
    219.125
    Compliance Dates
    219.126
    Compliance Plan (Repealed)
    219.127
    Testing VOL Operations
    219.128
    Monitoring VOL Operations
    219.129
    Recordkeeping and Reporting for VOL Operations
    SUBPART C: ORGANIC EMISSIONS FROM
    MISCELLANEOUS EQUIPMENT
    Section
    219.141
    Separation Operations
    219.142
    Pumps and Compressors
    219.143
    Vapor Blowdown
    219.144
    Safety Relief Valves
    SUBPART E: SOLVENT CLEANING
    Section
    219.181
    Solvent Cleaning in General
    219.182
    Cold Cleaning

    3
    219.183
    Open Top Vapor Degreasing
    219.184
    Conveyorized Degreasing
    219.185
    Compliance Schedule (Repealed)
    219.186
    Test Methods
    SUBPART F: COATING OPERATIONS
    Section
    219.204
    Emission Limitations
    219.205
    Daily-Weighted Average Limitations
    219.206
    Solids Basis Calculation
    219.207
    Alternative Emission Limitations
    219.208
    Exemptions From Emission Limitations
    219.209
    Exemption From General Rule on Use of Organic Material
    219.210
    Compliance Schedule
    219.211
    Recordkeeping and Reporting
    219.212
    Cross-Line Averaging to Establish Compliance for Coating Lines
    219.213
    Recordkeeping and Reporting for Cross-Line Averaging Participating
    Coating Lines
    219.214
    Changing Compliance Methods
    SUBPART G: USE OF ORGANIC MATERIAL
    Section
    219.301
    Use of Organic Material
    219.302
    Alternative Standard
    219.303
    Fuel Combustion Emission Units
    219.304
    Operations with Compliance Program
    SUBPART H: PRINTING AND PUBLISHING
    Section
    219.401
    Flexographic and Rotogravure Printing
    219.402
    Applicability
    219.403
    Compliance Schedule
    219.404
    Recordkeeping and Reporting
    219.405
    Lithographic Printing: Applicability
    219.406
    Provisions Applying to Heatset Web Offset Lithographic Printing Prior to
    March 15, 1996
    219.407
    Emission Limitations and Control Requirements for Lithographic Printing
    Lines On and After March 15, 1996
    219.408
    Compliance Schedule for Lithographic Printing on and After March 15,
    1996
    219.409
    Testing for Lithographic Printing On and After March 15, 1996
    219.410
    Monitoring Requirements for Lithographic Printing

    4
    219.411
    Recordkeeping and Reporting for Lithographic Printing
    SUBPART Q: SYNTHETIC ORGANIC CHEMICAL
    AND POLYMER MANUFACTURING PLANT
    Section
    219.421
    General Requirements
    219.422
    Inspection Program Plan for Leaks
    219.423
    Inspection Program for Leaks
    219.424
    Repairing Leaks
    219.425
    Recordkeeping for Leaks
    219.426
    Report for Leaks
    219.427
    Alternative Program for Leaks
    219.428
    Open-Ended Valves
    219.429
    Standards for Control Devices
    219.430
    Compliance Date (Repealed)
    219.431
    Applicability
    219.432
    Control Requirements
    219.433
    Performance and Testing Requirements
    219.434
    Monitoring Requirements
    219.435
    Recordkeeping and Reporting Requirements
    219.436
    Compliance Date
    SUBPART R: PETROLEUM REFINING AND
    RELATED INDUSTRIES; ASPHALT MATERIALS
    Section
    219.441
    Petroleum Refinery Waste Gas Disposal
    219.442
    Vacuum Producing Systems
    219.443
    Wastewater (Oil/Water) Separator
    219.444
    Process Unit Turnarounds
    219.445
    Leaks: General Requirements
    219.446
    Monitoring Program Plan for Leaks
    219.447
    Monitoring Program for Leaks
    219.448
    Recordkeeping for Leaks
    219.449
    Reporting for Leaks
    219.450
    Alternative Program for Leaks
    219.451
    Sealing Device Requirements
    219.452
    Compliance Schedule for Leaks
    219.453
    Compliance Dates (Repealed)
    SUBPART S: RUBBER AND MISCELLANEOUS
    PLASTIC PRODUCTS

    5
    Section
    219.461
    Manufacture of Pneumatic Rubber Tires
    219.462
    Green Tire Spraying Operations
    219.463
    Alternative Emission Reduction Systems
    219.464
    Emission Testing
    219.465
    Compliance Dates (Repealed)
    219.466
    Compliance Plan (Repealed)
    SUBPART T: PHARMACEUTICAL MANUFACTURING
    Section
    219.480
    Applicability
    219.481
    Control of Reactors, Distillation Units, Crystallizers, Centrifuges and
    Vacuum Dryers
    219.482
    Control of Air Dryers, Production Equipment Exhaust Systems and Filters
    219.483
    Material Storage and Transfer
    219.484
    In-Process Tanks
    219.485
    Leaks
    219.486
    Other Emission Units
    219.487
    Testing
    219.488
    Monitoring for Air Pollution Control Equipment
    219.489
    Recordkeeping for Air Pollution Control Equipment
    SUBPART V: BATCH OPERATIONS AND AIR OXIDATION PROCESSES
    Section
    219.500
    Applicability for Batch Operations
    219.501
    Control Requirements for Batch Operations
    219.502
    Determination of Uncontrolled Total Annual Mass Emissions and Actual
    Weighted Average Flow Rate Values for Batch Operations
    219.503
    Performance and Testing Requirements for Batch Operations
    219.504
    Monitoring Requirements for Batch Operations
    219.505
    Reporting and Recordkeeping for Batch Operations
    219.506
    Compliance Date
    219.520
    Emission Limitations for Air Oxidation Processes
    219.521
    Definitions (Repealed)
    219.522
    Savings Clause
    219.523
    Compliance
    219.524
    Determination of Applicability
    219.525
    Emission Limitations for Air Oxidation Processes (Renumbered)
    219.526
    Testing and Monitoring
    219.527
    Compliance Date (Repealed)
    SUBPART W: AGRICULTURE

    6
    Section
    219.541
    Pesticide Exception
    SUBPART X: CONSTRUCTION
    Section
    219.561
    Architectural Coatings
    219.562
    Paving Operations
    219.563
    Cutback Asphalt
    SUBPART Y: GASOLINE DISTRIBUTION
    Section
    219.581
    Bulk Gasoline Plants
    219.582
    Bulk Gasoline Terminals
    219.583
    Gasoline Dispensing Operations - Storage Tank Filling Operations
    219.584
    Gasoline Delivery Vessels
    219.585
    Gasoline Volatility Standards
    219.586
    Gasoline Dispensing Operations - Motor Vehicle Fueling Operations
    (Repealed)
    SUBPART Z: DRY CLEANERS
    Section
    219.601
    Perchloroethylene Dry Cleaners
    219.602
    Exemptions
    219.603
    Leaks
    219.604
    Compliance Dates (Repealed)
    219.605
    Compliance Plan (Repealed)
    219.606
    Exception to Compliance Plan (Repealed)
    219.607
    Standards for Petroleum Solvent Dry Cleaners
    219.608
    Operating Practices for Petroleum Solvent Dry Cleaners
    219.609
    Program for Inspection and Repair of Leaks
    219.610
    Testing and Monitoring
    219.611
    Exemption for Petroleum Solvent Dry Cleaners
    219.612
    Compliance Dates (Repealed)
    219.613
    Compliance Plan (Repealed)
    SUBPART AA: PAINT AND INK MANUFACTURING
    Section
    219.620
    Applicability
    219.621
    Exemption for Waterbase Material and Heatset-Offset Ink
    219.623
    Permit Conditions
    219.624
    Open-Top Mills, Tanks, Vats or Vessels

    7
    219.625
    Grinding Mills
    219.626
    Storage Tanks
    219.628
    Leaks
    219.630
    Clean Up
    219.636
    Compliance Schedule
    219.637
    Recordkeeping and Reporting
    SUBPART BB: POLYSTYRENE PLANTS
    Section
    219.640
    Applicability
    219.642
    Emissions Limitation at Polystyrene Plants
    219.644
    Emissions Testing
    SUBPART FF: BAKERY OVENS (Repealed)
    Section
    219.720
    Applicability (Repealed)
    219.722
    Control Requirements (Repealed)
    219.726
    Testing (Repealed)
    219.727
    Monitoring (Repealed)
    219.728
    Recordkeeping and Reporting (Repealed)
    219.729
    Compliance Date (Repealed)
    219.730
    Certification (Repealed)
    SUBPART GG: MARINE TERMINALS
    Section
    219.760
    Applicability
    219.762
    Control Requirements
    219.764
    Compliance Certification
    219.766
    Leaks
    219.768
    Testing and Monitoring
    219.770
    Recordkeeping and Reporting
    SUBPART HH: MOTOR VEHICLE REFINISHING
    Section
    219.780
    Emission Limitations
    219.782
    Alternative Control Requirements
    219.784
    Equipment Specifications
    219.786
    Surface Preparation Materials
    219.787
    Work Practices
    219.788
    Testing
    219.789
    Monitoring and Recordkeeping for Control Devices

    8
    219.790
    General Recordkeeping and Reporting
    219.791
    Compliance Date
    219.792
    Registration
    219.875
    Applicability of Subpart BB (Renumbered)
    219.877
    Emissions Limitation at Polystyrene Plants (Renumbered)
    219.879
    Compliance Date (Repealed)
    219.881
    Compliance Plan (Repealed)
    219.883
    Special Requirements for Compliance Plan (Repealed)
    219.886
    Emissions Testing (Renumbered)
    SUBPART PP: MISCELLANEOUS FABRICATED
    PRODUCT MANUFACTURING PROCESSES
    Section
    219.920
    Applicability
    219.923
    Permit Conditions
    219.926
    Control Requirements
    219.927
    Compliance Schedule
    219.928
    Testing
    SUBPART QQ: MISCELLANEOUS FORMULATION
    MANUFACTURING PROCESSES
    Section
    219.940
    Applicability
    219.943
    Permit Conditions
    219.946
    Control Requirements
    219.947
    Compliance Schedule
    219.948
    Testing
    SUBPART RR: MISCELLANEOUS ORGANIC
    CHEMICAL MANUFACTURING PROCESSES
    Section
    219.960
    Applicability
    219.963
    Permit Conditions
    219.966
    Control Requirements
    219.967
    Compliance Schedule
    219.968
    Testing
    SUBPART TT: OTHER EMISSION UNITS
    Section
    219.980
    Applicability
    219.983
    Permit Conditions

    9
    219.986
    Control Requirements
    219.987
    Compliance Schedule
    219.988
    Testing
    SUBPART UU: RECORDKEEPING AND REPORTING
    Section
    219.990
    Exempt Emission Units
    219.991
    Subject Emission Units
    Section 219.Appendix A:
    List of Chemicals Defining Synthetic Organic Chemical and
    Polymer Manufacturing
    Section 219.Appendix B:
    VOM Measurement Techniques for Capture Efficiency
    Section 219.Appendix C:
    Reference Methods And Procedures
    Section 219.Appendix D:
    Coefficients for the Total Resource Effectiveness Index
    (TRE) Equation
    Section 219.Appendix E:
    List of Affected Marine Terminals
    Section 219.Appendix G:
    TRE Index Measurements for SOCMI Reactors and
    Distillation Units
    Section 219.Appendix H:
    Baseline VOM Content Limitations for Subpart F, Section
    219.212 Cross-Line Averaging
    AUTHORITY: Implementing Section 10 and authorized by Section 28.5 of the
    Environmental Protection Act [415 ILCS 5/10 and 28.5].
    SOURCE: Adopted at R91-8 at 15 Ill. Reg. 12491, effective August 16, 1991; amended in
    R91-24 at 16 Ill. Reg. 13597, effective August 24, 1992; amended in R91-30 at 16 Ill.
    Reg. 13883, effective August 24, 1992; emergency amendment in R93-12 at 17 Ill. Reg.
    8295, effective May 24, 1993, for a maximum of 150 days, amended in R93-9 at 17 Ill.
    Reg. 16918, effective September 27, 1993 and October 21, 1993; amended in R93-28 at 18
    Ill. Reg. 4242, effective March 3, 1994; amended in R94-12 at 18 Ill. Reg. 14987,
    effective September 21, 1994; amended in R94-15 at 18 Ill. Reg. 16415, effective October
    25, 1994; amended in R94-16 at 18 Ill. Reg. 16980, effective November 15, 1994;
    emergency amendment in R95-10 at 19 Ill. Reg. 3059, effective February 28, 1995, for a
    maximum of 150 days; amended in R94-21, R94-31 and R94-32 at 19 Ill. Reg. 6958,
    effective May 9, 1995; amended in R94-33 at 19 Ill. Reg. 7385, effective May 22, 1995;
    amended in R96-13 at 20 Ill. Reg. 14462, effective October 28, 1996; expedited correction
    at 21 Ill. Reg. ________, effective _______________________.
    BOARD NOTE: This Part implements the Illinois Environmental Protection Act as of July
    1, 1994.
    NOTE: In this Part, superscript numbers or letters are denoted by parentheses, subscript
    are denoted by brackets, and SUM means the summation series or sigma function as used
    in mathematics.

    10
    SUBPART A: GENERAL PROVISIONS
    Section 219.108 Exemptions, Variations, and Alternative Means of Control or
    Compliance Determinations
    Notwithstanding the provisions of any other Sections of this Part:
    a) Any exemptions, variations or alternatives to the control requirements,
    emission limitations, or test methods set forth in this Part shall be
    effective only when approved by the Agency and approved by the
    USEPA as a SIP revision.
     
    b) Any equivalent alternative control plans, equivalent device, or other
    equivalent practice authorized by the Agency where this Part provides
    for such alternative or equivalent practice or equivalent variations or
    alterations to test methods approved by the Agency shall be effective
    only when included in a federally enforceable permit or approved as a
    SIP revision.
    (Source: Amended at ____ Ill. Reg. _______, effective _____________)
    Section 219.110 Vapor Pressure of Organic Material or Solvent
    a) If the organic material or solvent consists of only a single compound, the
    vapor pressure shall be determined by ASTM Method D2879-86
    (incorporated by reference in Section 219.112 of this Part) or the vapor
    pressure may be obtained from a publication such as: Boublik, T., V.
    Fried and E. Hala, "The Vapor Pressure of Pure Substances," Elsevier
    Scientific Publishing Co., New York (1973); Perry's Chemical
    Engineer's Handbook, McGraw-Hill Book Company (1984); CRC
    Handbook of Chemistry and Physics, Chemical Rubber Publishing
    Company (1986-87); and Lange's Handbook of Chemistry, John A.
    Dean, editor, McGraw-Hill Book Company (1985).
     
    b) If the organic material or solvent is in a mixture made up of both organic
    material compounds and compounds which are not organic material, the
    vapor pressure shall be determined by the following equation:
    n
    Σ
    P
    i
    X
    i
    P
    om
    = i=1____________
    n
    Σ
    X
    i
    i=1

    11
    where:
    P
    om
    =
    Total vapor pressure of the portion of the mixture which is
    composed of organic material;
    n =
    Number of organic material components in the mixture;
    i =
    Subscript denoting an individual component;
    P
    i
    =
    Vapor pressure of an organic material component determined in
    accordance with subsection (a) of this Section;
    X
    i
    =
    Mole fraction of the organic material component of the total
    organic mixture.
     
    c) If the organic material or solvent is in a mixture made up of only organic
    material compounds, the vapor pressure shall be determined by ASTM Method
    D2879-86 (incorporated by reference in Section 219.112 of this Part) or by the
    above equation.
     
    (Source: Amended at ___ Ill. Reg. __________, effective _____________)
    Section 219.111 Vapor Pressure of Volatile Organic Material
    a) If the VOM consists of only a single compound, the vapor pressure
    shall be determined by ASTM Method D2879-86 (incorporated by
    reference in Section 219.112 of this Part) or the vapor pressure may be
    obtained from a publication such as: Boublik, T., V. Fried and E. Hala,
    "The Vapor Pressure of Pure Substances," Elsevier Scientific Publishing
    Co., New York (1973); Perry's Chemical Engineer's Handbook,
    McGraw-Hill Book Company (1984); CRC Handbook of Chemistry and
    Physics, Chemical Rubber Publishing Company (1986-87); and Lange's
    Handbook of Chemistry, John A. Dean, editor, McGraw-Hill Book
    Company (1985).
     
    b) If the VOM is in a mixture made up of both VOM compounds and
    compounds which are not VOM, the vapor pressure shall be determined
    by the following equation:
    n
    Σ
    P
    i
    X
    i
    P
    vom
    = __i=1________
    n
    Σ
    Xi

    12
    i=1
    where:
    P
    vom
    = Total vapor pressure of the portion of the mixture which is composed
    of VOM;
    n = Number of VOM components in the mixture;
    I = Subscript denoting an individual component;
    P
    i
    = Vapor pressure of a VOM component determined in accordance with
    subsection (a) of this Section;
    X
    i
    = Mole fraction of the VOM component of the total organic mixture.
    c) If the VOM is in a mixture made up of only VOM compounds, the
    vapor pressure shall be determined by ASTM Method D2879-86
    (incorporated by reference in Section 219.112 of this Part) or by the
    above equation.
     
    (Source: Amended at ___ Ill. Reg. ________, effective ____________)
    SUBPART F: COATING OPERATIONS
    Section 219.208 Exemptions From Emission Limitations
    a) Exemptions for all coating categories except wood furniture coating.
    The limitations of this Subpart shall not apply to coating lines within a
    source, that otherwise would be subject to the same subsection of Section
    219.204 (because they belong to the same coating category, e.g. can
    coating), provided that combined actual emissions of VOM from all lines
    at the source subject to that subsection never exceed 6.8 kg/day (15
    lbs/day) before the application of capture systems and control devices.
    (For example, can coating lines within a source would not be subject to
    the limitations of Section 219.204(b) of this Subpart if the combined
    actual emissions of VOM from the can coating lines never exceed 6.8
    kg/day (15 lbs/day) before the application of capture systems and control
    devices.) Volatile organic material emissions from heavy off-highway
    vehicle products coating lines must be combined with VOM emissions
    from miscellaneous metal parts and products coating lines to determine
    applicability. Any owner or operator of a coating source shall comply
    with the applicable coating analysis test methods and procedures
    specified in Section 219.105(a) of this Part and the recordkeeping and

    13
    reporting requirements specified in Section 219.211(a) of this Subpart if
    total VOM emissions from the subject coating lines are always less than
    or equal to 6.8 kg/day (15 lbs/day) before the application of capture
    systems and control devices and, therefore, are not subject to the
    limitations of Section 219.204 of this Subpart. Once a category of
    coating lines at a source is subject to the limitations in Section 219.204
    of this Subpart the coating lines are always subject to the limitations in
    Section 219.204 of this Subpart.
     
    b) Applicability for wood furniture coating
     
    1) The limitations of this Subpart shall apply to a source's wood
    furniture coating lines if the source contains process emission
    units, not regulated by Subparts B, E, F (excluding Section
    219.204(l) of this Subpart), H (excluding Section 219.405 of this
    Part), Q, R, S, T (excluding Section 219.486 of this Part), V, X,
    Y, Z or BB of this Part, which as a group both:
     
    A) Have a maximum theoretical emissions of 91 Mg (100
    tons) or more per calendar year of VOM if no air
    pollution control equipment were used, and
     
    B) Are not limited to less than 91 Mg (100 tons) of VOM per
    calendar year if no air pollution control equipment were
    used, through production or capacity limitations contained
    in a federally enforceable permit or SIP revision.
     
    2) The limitations of this Subpart shall apply to a source's wood
    furniture coating lines, on and after March 15, 1996, if the
    source contains process emission units, which as a group have a
    potential to emit 22.7 Mg (25 tons) or more of VOM per
    calendar year and have not limited emissions to less than 22.7
    Mg (25 tons) of VOM per calendar year through production or
    capacity limitations contained in a federally enforceable operating
    permit or SIP revision, and which:
     
    A) Are not regulated by Subparts B, E, F (excluding Section
    219.204(l) of this Subpart), H, Q, R, S, T (excluding
    Section 219.486 of this Part), V, X, Y, Z or BB of this
    Part; and
     
    B) Are not included in any of the following categories:
    synthetic organic chemical manufacturing industry
    (SOCMI) distillation, SOCMI reactors, plastic parts
    coating (business machines), plastic parts coating (other),

    14
    offset lithography, industrial wastewater, autobody
    refinishing, SOCMI batch processing, volatile organic
    liquid storage tanks and clean-up solvents operations.
     
    3) If a source ceases to fulfill the criteria of subsection (b)(1) or
    (b)(2) of this Section, the limitations of Section 219.204(l) of this
    Subpart shall continue to apply to any wood furniture coating line
    which was ever subject to the limitations of Section 219.204(l) of
    this Subpart.
     
    4) For the purposes of subsection (b) of this Section, an emission
    unit shall be considered to be regulated by a Subpart if it is
    subject to the limitations of that Subpart. An emission unit is not
    considered regulated by a Subpart if it is not subject to the limits
    of that Subpart, e.g., the emission unit is covered by an
    exemption in the Subpart or the applicability criteria of the
    Subpart are not met.
     
    5) Any owner or operator of a wood furniture coating line to which
    the limitations of this Subpart are not applicable due to the
    criteria in subsection (b) of this Section shall, upon request by the
    Agency or the USEPA, submit records to the Agency and the
    USEPA within 30 calendar days from the date of the request that
    document that the coating line is exempt from the limitations of
    this Subpart.
     
    c) On and after March 15, 1996, the limitations of this Subpart shall not
    apply to touch-up and repair coatings used by a coating source described
    by subsections 219.204(b), (d), (f), (g), (i), (j), (m) and (n) of this
    Subpart; provided that the source-wide volume of such coatings used
    does not exceed 0.95 l (1 quart) per eight- hour period or exceed 209
    l/yr (55 gal/yr) for any rolling twelve month period. Recordkeeping and
    reporting for touch-up and repair coatings shall be consistent with
    subsection (d) of this Section.
     
    d) On and after March 15, 1996, the owner or operator of a coating line or
    a group of coating lines using touch-up and repair coatings that are
    exempted from the limitations of Section 219.204(b), (d), (f), (g), (i),
    (j), (m) and (n) of this Subpart because of the provisions of Section
    219.208(c) of this Subpart shall:
     
    1) Collect and record the name, identification number, and volume
    used of each touch-up and repair coating, as applied on each
    coating line, per eight- hour period and per month;
     

    15
    2) Perform calculations on a daily basis, and maintain at the source
    records of such calculations of the combined volume of touch-up
    and repair coatings used source-wide for each eight-hour period;
     
    3) Perform calculations on a monthly basis, and maintain at the
    source records of such calculations of the combined volume of
    touch-up and repair coatings used source-wide for the month and
    the rolling twelve month period;
     
    4) Prepare and maintain at the source an annual summary of the
    information required to be compiled pursuant to subsections
    (d)(1) and (d)(2) of this Section on or before January 31 of the
    following year;
     
    5) Maintain at the source for a minimum period of three years all
    records required to be kept under this subsection and make such
    records available to the Agency upon request;
     
    6) Notify the Agency in writing if the use of touch-up and repair
    coatings at the source ever exceeds a volume of 0.95 l (1 quart)
    per eight-hour period or exceeds 209 l/yr (55 gal/yr) for any
    rolling twelve month period within 30 days after any such
    exceedance. Such notification shall include a copy of any records
    of such exceedance; and
     
    7) "Touch-up and repair coatings" means, for purposes of 35 Ill.
    Adm. Code 219.208, any coating used to cover minor scratches
    and nicks that occur during manufacturing and assembly
    processes.
    (Source: Amended at _____ Ill. Reg. _________, effective _______________)
    SUBPART Q: SYNTHETIC ORGANIC CHEMICAL
    AND POLYMER MANUFACTURING PLANT
    Section 219.431 Applicability
    a) The provisions of Sections 219.431 through 219.436 of this Subpart
    shall apply to every owner or operator of any chemical manufacturing
    process unit that manufactures, as a primary product, one or more of the
    chemicals listed in Appendix A of this Part and that chemical
    manufacturing process unit causes or allows any reactor or distillation
    unit, either individually or in tandem, to discharge one or more process
    vent streams either directly to the atmosphere or to a recovery system.

    16
     
    b) Notwithstanding subsection (a) of this Section, the control requirements
    set forth within Section 219.432 of this Subpart shall not apply to the
    following:
     
    1) Any process vent stream with a total resource effectiveness
    (TRE) index value greater than 1.0. However, such process vent
    stream remains subject to the performance testing requirements
    contained in Section 219.433 of this Subpart and the reporting
    and recordkeeping requirements contained in Section 219.435 of
    this Subpart;
     
    2) Any reactor or distillation unit that is designed and operated as a
    batch operation;
     
    3) Any reactor or distillation unit that is part of a polymer
    manufacturing operation;
     
    4) Any reactor or distillation unit that is part of the chemical
    manufacturing process unit with a total design capacity of less
    than 1 gigagram (1,100 tons) per year for all chemicals produced,
    as a primary product, within that process unit. However, such
    operations remain subject to the reporting and recordkeeping
    requirements contained in Section 219.435(d) of this Subpart;
     
    5) Any vent stream with a flow rate less than 0.0085 scm/min or a
    total VOM concentration of less than 500 ppmv, less methane
    and ethane, as measured by Method 18, or a concentration of
    VOM of less than 250 ppmv as measured by Method 25A.
    However, such operations remain subject to the performance
    testing requirement listed in Section 219.433 of this Subpart, as
    well as the reporting and recordkeeping requirements contained in
    Section 219.435 of this Subpart; or
     
    6) Any reactor or distillation unit included within an Early
    Reduction Program, as specified in 40 CFR 63, and published in
    57 Fed. Reg. 61970 (December 29, 1992), evidenced by a timely
    enforceable commitment approved by USEPA.
    (Source: Amended at _____ Ill. Reg. ________, effective _______________)
    Section 219.434 Monitoring Requirements
    a) The owner or operator of a source subject to the control requirements in
    Section 219.432 of this Subpart that uses an incinerator to comply with

    17
    the VOM emission limitation specified in Section 219.432(a)(1) shall
    install, calibrate, maintain, and operate, according to manufacturer's
    specifications, a temperature monitoring device equipped with a
    continuous recorder and having an accuracy of
    ±
    1 percent of the
    temperature measured expressed in degress Celsius, or
    ±
    0.5
    ø
    C,
    whichever is greater.
     
    1) Where an incinerator other than a catalytic incinerator is used, a
    temperature monitoring device shall be installed in the firebox.
     
    2) Where a catalytic incinerator is used, temperature monitoring
    devices shall be installed in the gas stream immediately before
    and after the catalyst bed.
     
    b) The owner or operator of a source that uses a flare to comply with
    Section 219.432(a)(2) of this Subpart shall install, calibrate, maintain
    and operate, according to manufacturer's specifications, a heat-sensing
    device, such as an ultraviolet beam sensor or thermocouple, at the pilot
    light to indicate continuous presence of a flame.
     
    c) The owner or operator of a source that uses a boiler or process heater
    with a design heat input capacity less than 44 megawatts to comply with
    Section 219.432(a)(1) of this Subpart shall install, calibrate, maintain
    and operate, according to the manufacturer's specifications, a
    temperature monitoring device in the firebox. The monitoring device
    shall be equipped with a continuous recorder with an accuracy of
    ±
    1
    percent of the temperature being measured expressed in degrees Celsius
    or
    ±
    0.5
    ø
    C, whichever is greater. Any boiler or process heater in which
    all vent streams are introduced with primary fuel is exempt from this
    requirement.
     
    d) The owner or operator of a process vent with a TRE index value of 4.0
    or less that uses one or more product recovery devices shall install either
    an organic monitoring device equipped with a continuous recorder or the
    monitoring equipment specified in subsection (d)(1), (d)(2), (d)(3) or
    (d)(4) of this Section, depending on the type of recovery device used.
    All monitoring equipment shall be installed, calibrated and maintained
    according to the manufacturer's specifications.
     
    1) Where an absorber is the final recovery device in the recovery
    system, a scrubbing liquid temperature monitoring device and a
    specific gravity monitoring device, each equipped with a
    continuous recorder, shall be used.
     

    18
    2) Where a condenser is the final recovery device in the recovery
    system, a condenser exit (product side) temperature monitoring
    device equipped with a continuous recorder and having an
    accuracy of
    ±
    1 percent of the temperature being monitored
    expressed in degrees Celsius or
    ±
    0.5
    ø
    C, whichever is greater.
     
    3) Where a carbon adsorber is the final recovery device in the
    recovery system, an integrating regeneration steam flow
    monitoring device having an accuracy of
    ±
    10 percent, capable of
    recording the total regeneration steam mass flow for each
    regeneration cycle; and a carbon bed temperature monitoring
    device having an accuracy of
    ±
    1 percent of the temperature being
    monitored expressed in degrees Celsius of
    ±
    0.5
    ø
    C, capable of
    recording the carbon bed temperature after each regeneration and
    within 15 minutes of completing any cooling cycle.
     
    4) Where a scrubber is used with an incinerator, boiler, or, in the
    case of halogenated vent streams, a process heater, the following
    monitoring equipment is required for the scrubber:
     
    A) A pH monitoring device equipped with a continuous
    recorder to monitor the pH of the scrubber effluent; and
     
    B) Flow meters equipped with a continuous recorder at the
    scrubber influent for liquid flow and the scrubber inlet for
    gas stream flow.
     
    e) The owner or operator of a process vent using a vent system that
    contains bypass lines capable of diverting a vent stream away from the
    control device associated with a process vent shall comply with either
    (e)(1) or (e)(2) of this Section. Equipment needed for safety purposes,
    including, but not limited to, pressure relief devices, are not subject to
    this subsection.
     
    1) The owner or operator shall install, calibrate, maintain and
    operate a flow indicator that provides a record of vent stream
    flow at least once every 15 minutes. The flow indicator shall be
    installed at the entrance to any bypass line that could divert the
    vent stream away from the control device to the atmosphere.
     
    2) The owner or operator shall secure the bypass line valve in the
    closed position with a car-seal or a lock-and-key type
    configuration. A visual inspection of the seal or closure
    mechanism shall be performed at least once every month to

    19
    ensure that the valve is maintained in the closed position and the
    vent stream is not diverted through the bypass line.
     
    f) The owner or operator of a process vent may monitor by an equivalent
    alternative means or parameters other than those listed in subsections (a)
    through (d) of this Section. Any equivalent alternative shall be approved
    by the Agency and USEPA, and contained in the source's operating
    permit as federally enforceable permit conditions.
    (Source: Amended at _____ Ill. Reg. _________, effective _______________)
    Section 219.435 Recordkeeping and Reporting Requirements
    a) Every owner or operator of a reactor or distillation unit with a TRE index value of
    4.0 or less shall keep records, for a minimum of 3 years, of the following
    parameters measured during a performance test or TRE determination required
    under Section 219.433 of this Subpart, and required to be monitored under Section
    219.434 of this Subpart.
    1) Every owner or operator of a source that seeks to demonstrate
    compliance with Section 219.432(a)(1) of this Subpart through
    the use of either a thermal or catalytic incinerator shall maintain
    records of the following:
     
    A) The average firebox temperature of the incinerator (or the
    average temperature upstream and downstream of the
    catalyst bed for a catalytic incinerator), measured at least
    every 15 minutes and averaged over the same time period
    of the performance testing; and
     
    B) The percent reduction of VOM determined as specified in
    Section 219.433(c) of this Subpart achieved by the
    incinerator, or the concentration of VOM (ppmv, by
    compound) determined as specified in Section 219.433(c)
    of this Subpart at the outlet of the control device, on a dry
    basis, corrected to 3 percent oxygen.
     
    2) Every owner or operator of a source that seeks to demonstrate
    compliance with Section 219.432(a)(1) of this Subpart through
    the use of a boiler or process heater shall maintain the records
    described below. Any boiler or process heater in which all vent
    streams are introduced with primary fuel are exempt from these
    requirements.
     

    20
    A) A description of the location at which the vent stream is
    introduced into the boiler or process heater; and
     
    B) The average combustion temperature of the boiler or
    process heater with a design heat input capacity of less
    than 44 megawatt measured at least every 15 minutes and
    averaged over the same time period of the performance
    testing.
     
    3) Every owner or operator of a source that seeks to demonstrate
    compliance with Section 219.432(a)(2) of this Subpart through
    use of a smokeless flare, or flare design (i.e., steam-assisted, air-
    assisted, or nonassisted shall maintain records of all visible
    emission readings, heat content determinations, flow rate
    measurements, and exit velocity determinations made during the
    performance test, continuous records of the flare pilot flame
    monitoring, and records of all periods of operations during which
    the pilot flame is absent.
     
    4) Every owner or operator of a source that seeks to demonstrate
    compliance with Section 219.432(b) of this Subpart shall
    maintain records of the following:
     
    A) Where an absorber is the final recovery device in the
    recovery system, the exit specific gravity (or alternative
    parameter) which is a measure of the degree of absorbing
    liquid saturation, if approved by the Agency and USEPA,
    and average exit temperature of the absorbing liquid
    measured at least every 15 minutes and averaged over the
    same time period as the performance testing (both
    measured while the vent stream is normally routed and
    constituted);
     
    B) Where a condenser is the final recovery device in the
    recovery system, the average exit (product side)
    temperature measured at least every 15 minutes and
    averaged over the same time period as the performance
    testing while the vent stream is normally routed and
    constituted;
     
    C) Where a carbon absorber is the final recovery device in
    the recovery system, the total steam mass or volumetric
    flow measured at least every 15 minutes and averaged
    over the same time period as the performance testing (full
    carbon bed cycle), the temperature of the carbon bed after

    21
    regeneration (and within 15 minutes of completion of any
    cooling cycle(s)), and duration of the carbon bed steaming
    cycle (all measured while the vent stream is normally
    routed and constituted);
     
    D) As an alternative to subsection (a)(4)(A), (a)(4)(B) or
    (a)(4)(C) of this Section, the concentration level or
    reading indicated by the organic monitoring device at the
    outlet of the absorber, condenser, or carbon absorber,
    measured at least every 15 minutes and averaged over the
    same time period as the performance testing (measured
    while the vent stream is normally routed and constituted);
    or
     
    E) All measurements and calculations performed to
    determine the flow rate, VOM concentration, heating
    value, and TRE index value of the vent stream.
     
    b) Every owner or operator of a reactor or distillation unit with a TRE
    index value of less than 4.0 shall be subject to the exceedance reporting
    requirements of the draft Enhanced Monitoring Guidelines as published
    at 58 Fed. Reg. 54648 (October 22, 1993).
     
    c) Every owner or operator of a source seeking to comply with Section
    219.432(b) of this Subpart shall maintain records of the following:
     
    1) Any changes in production capacity, feedstock type, catalyst
    type, or of any replacement, removal, or addition of recovery
    equipment or reactors and distillation units; and
     
    2) Any recalculation of the flow rate, VOM concentration, or TRE
    index value calculated according to subsection (c) of Appendix G
    of this Part.
     
    d) Every owner or operator of a source claiming a design capacity of less
    than 1 gigagram (1,100 tons) per year, as contained in Section
    219.431(b) of this Subpart, shall maintain records of the design capacity
    or any changes in equipment or operations that may affect the design
    capacity.
     
    e) Every owner or operator of a source claiming a vent stream flow rate or
    vent stream concentration exemption level, as contained in Section
    219.431(b)(5) of this Subpart, shall maintain records to indicate that the
    stream flow rate is less than 0.0085 scm/min or the vent stream
    concentration is less than 500 ppmv.

    22
    (Source: Amended at Ill. Reg. , effective )
    SUBPART FF: BAKERY OVENS (Repealed)
    Section 219.720 Applicability (Repealed)
    a) The provisions of this Subpart shall apply to every owner or operator of
    a source which operates a bakery oven, as defined at 35 Ill. Adm. Code
    211.680, unless the source bakes products only for on-site human
    consumption or on- site retail sale.
     
    b) Notwithstanding subsection (a) of this Section, a source is required to
    comply with the control requirements of this Subpart only if the source
    has the potential to emit 22.7 Mg (25 tons) or more of VOM per year, in
    the aggregate, from all emission units at the source, excluding:
     
    1) Emission units regulated by Subparts B, E, F, H, Q, R, S, T
    (excluding Section 219.486 of this Part), V, X, Y, Z or BB of
    this Part; and
     
    2) Emission units that are included in any of the following
    categories: synthetic organic chemical manufacturing industry
    (SOCMI) distillation, SOCMI reactors, wood furniture coating,
    plastic parts coating (business machines), plastic parts coating
    (other), offset lithography, industrial wastewater, autobody
    refinishing, SOCMI batch processing, volatile organic liquid
    storage tanks and clean-up solvents operations.
     
    c) Every owner or operator of a source which has limited its potential to
    emit below 22.7 Mg (25 tons) of VOM per year, as specified in
    subsection (b) of this Section, through federally enforceable permit
    conditions is not required to comply with this Subpart.
     
    d) Every owner or operator of a bakery oven which is exempt from the
    control requirements of this Subpart because of the criteria in subsection
    (b) of this Section remains subject to the recordkeeping and reporting
    requirements of Section 219.728(b) of this Subpart and the certification
    requirements in Section 219.730(d) of this Subpart.
    (Source: Repealed at ____ Ill. Reg. ________, effective ______________)
    Section 219.722 Control Requirements (Repealed)

    23
    a) Every owner or operator of a source subject to the control requirements
    of this Subpart shall comply with the requirements of subsection (a)(1)
    or (a)(2) of this Section for each bakery oven with a rated heat input
    capacity of at least 2 mmbtu/hr or at least 586 kW:
     
    1) Operate emissions capture and control equipment which achieves
    an overall reduction in uncontrolled VOM emissions of at least
    81 percent from each such bakery oven; or
     
    2) Provide an equivalent alternative control plan for such bakery
    ovens at the source which has been approved by the Agency and
    USEPA through federally enforceable permit conditions or as a
    SIP revision.
     
    b) An owner or operator of a source subject to the control requirements of
    this Subpart may elect to exempt from the control requirements in
    subsections (a)(1) or (a)(2) and (c)(1) or (c)(2) of this Section any bakery
    oven with actual VOM emissions less than or equal to 15 TPY; provided
    that the total actual VOM emissions from all such exempt bakery ovens
    never exceed 25 TPY.
     
    c) Notwithstanding the requirements in subsection (a) of this Section, until
    March 15, 1998, only, a source may elect to comply with the control
    requirements in subsection (c)(1) or (c)(2) of this Section, rather than the
    control requirements in subsection (a)(1) or (a)(2) of this Section, if all
    emission units at the source, in the aggregate, excluding emission units
    regulated by Subparts B, E, F, H (excluding Section 219.405 of this
    Subpart), Q, R, S, T (excluding Section 219.486 of this Subpart), V, X,
    Y, Z or BB of this Subpart, have maximum theoretical emissions of less
    than 90.7 Mg (100 tons) of VOM per year or are limited to less than
    90.7 Mg (100 tons) of VOM emissions per calendar year in the absence
    of air pollution control equipment through production or capacity
    limitations contained in federally enforceable permit conditions or in a
    SIP revision:
     
    1) Operate emissions capture and control equipment which achieves
    an overall reduction in uncontrolled VOM emissions of at least
    60 percent from each bakery oven with a rated heat input
    capacity of at least 2 mmbtu/hr or at least 586 KW; or
     
    2) Provide an equivalent alternative control plan for such bakery
    ovens at the source which has been approved by the Agency and
    USEPA through federally enforceable permit conditions or as a
    SIP revision.

    24
     
    d) Any bakery oven that becomes subject to the requirements of this
    Subpart at any time shall remain subject to the requirements of this
    Subpart at all times thereafter.
    (Source: Repealed at _____ Ill. Reg. _________, effective _______________)
    Section 219.726 Testing (Repealed)
     
    a) Upon request by the Agency, the owner or operator of a bakery oven
    shall, at its own expense, conduct such tests in accordance with the
    applicable test methods and procedures specified in Section 219.105(f) of
    this Part to demonstrate compliance with the control requirements of this
    Subpart and shall:
     
    1) Notify the Agency 30 days prior to conducting such tests; and
     
    2) Submit all test results to the Agency within 30 days of conducting
    such tests.
     
    b) Nothing in this Section shall limit the authority of USEPA pursuant to
    the Clean Air Act (CAA) to require testing, or shall affect the authority
    of USEPA under Section 114 of the CAA (42 U.S.C. 7414 (1990)).
     
    (Source: Repealed at _____ Ill. Reg. _________, effective _________________)
    Section 219.727 Monitoring (Repealed)
    a) Every owner or operator of a bakery oven subject to the control
    requirements of this Subpart shall install and operate at all times a device
    to continuously monitor the following parameters for each type of
    control device as follows:
     
    1) For catalytic oxidizers, the inlet and outlet temperatures of the
    oxidizer;
     
    2) For regenerative oxidizers, the temperature in the combustion
    chamber; or
     
    3) For thermal incinerators, the temperature in the combustion
    chamber.
     

    25
    b) The owner or operator may monitor with an alternative method or
    monitor other parameters if approved by the Agency and USEPA
    through federally enforceable permit conditions or as a SIP revision.
    (Source: Repealed at _____ Ill. Reg. ________, effective ___________________)
    Section 219.728 Recordkeeping and Reporting (Repealed)
    a) Every owner or operator of a bakery oven shall maintain the following
    records for the most recent consecutive 3 year period for all bakery
    ovens subject to the control requirements of this Subpart. Such records
    shall be made available to the Agency immediately upon request.
     
    1) Parameters for control devices as monitored pursuant to Section
    219.727 of this Subpart;
     
    2) Hrs/day of operation of each bakery oven;
     
    3) Factors necessary to calculate VOM emissions for all bakery
    ovens including, but not limited to, type of dough used for each
    yeast-leavened baked product, initial yeast percentage for each
    product, total fermentation time for each product, any additional
    percentage of yeast added, and the fermentation time of any
    additional yeast;
     
    4) Calculated daily VOM emissions of each bakery oven expressed
    as lbs/day;
     
    5) Total amount of each type of yeast-leavened bread product
    produced by each bakery oven expressed as lbs/day.
     
    b) Every owner or operator of a bakery oven which is exempt from the
    control requirements of this Subpart because of the criteria in Section
    219.720(b) of this Subpart shall maintain records necessary to
    demonstrate that its potential to emit is less than 22.7 Mg (25 tons) of
    VOM per year, as specified in Section 219.720(b). Such records shall
    be maintained for the most recent consecutive 3 year period and shall be
    made available to the Agency immediately upon request.
     
    c) Every owner or operator of a bakery oven which is exempt from the
    control requirements of this Subpart because of the criteria specified in
    Section 219.722(b) of this Subpart shall:
     

    26
    1) Maintain records necessary to demonstrate that the actual VOM
    emissions from exempt bakery ovens are less than or equal to 15
    TPY for each bakery oven and less than or equal to 25 TPY from
    all exempt bakery ovens combined. Such records shall be
    maintained for the most recent consecutive 3 year period and
    shall be made available to the Agency immediately upon request;
    and
     
    2) Notify the Agency in writing if the actual VOM emissions from
    an exempt bakery oven ever exceed 15 TPY or the actual VOM
    emissions from a combination of exempt bakery ovens ever
    exceed 25 TPY, within 30 days after the exceedance occurs.
    Such notice shall include a copy of all records of the exceedance.
     
    d) Every owner or operator of a bakery oven which is controlling emissions
    as provided in Section 219.722(c) of this Subpart until March 15, 1998,
    shall maintain records necessary to demonstrate that its maximum
    theoretical emissions as specified in Section 219.722(c) are less than
    90.7 Mg (100 tons) of VOM per year. Such records shall be maintaned
    for the most recent consecutive 3 year period and shall be made available
    to the Agency immediatley upon request.
    (Source: Repealed at _____ Ill. Reg. ________, effective _____________________)
    Section 219.729 Compliance Date (Repealed)
    On and after March 15, 1996, upon initial startup or upon modification, every owner
    or operator of a source subject to this Subpart shall comply with the requirements of
    this Subpart.
    (Source: Repealed at ____ Ill. Reg. _________, effective ________________)
    Section 219.730 Certification (Repealed)
    a) Every owner or operator of a source subject to the control requirements
    of this Subpart shall certify compliance with this Subpart on or before a
    date consistent with Section 219.729 of this Subpart.
     
    b) If an owner or operator of a bakery oven subject to the control
    requirements of this Subpart changes the method of compliance, the
    owner or operator shall certify compliance with the requirements of this
    Subpart for the alternative method upon changing the method of
    compliance.

    27
     
    c) All certifications of compliance with this Subpart shall include the results
    of all tests and the calculations performed to demonstrate that each oven
    at the source is in compliance with, or is exempt from, the control
    requirements of this Subpart. The certification shall include the
    following:
     
    1) The name and identification number of each oven and any
    associated capture and control device;
     
    2) The maximum rated heat input of each oven;
     
    3) A classification of each oven as either a "bakery oven" as defined
    in 35 Ill. Admin. Code 211.680 or an oven used exclusively to
    bake non-yeast-leavened products;
     
    4) The capture and control efficiency of each bakery oven control
    device;
     
    5) Test reports, calculations, and other data necessary to
    demonstrate that the capture and control efficiency of each bakery
    oven control device achieves an overall reduction in uncontrolled
    VOM emissions of at least 81 percent; and
     
    6) The date each bakery oven control device was installed and
    operating.
     
    d) On or before March 15, 1996, or upon initial startup, every owner or
    operator of a bakery oven which is exempt from the control requirements
    of this Subpart because of the criteria in Section 219.720(b) of this
    Subpart shall certify that its potential to emit is less than 22.7 Mg (25
    tons) of VOM per year, as specified in Section 219.720(b).
     
    e) On or before March 15, 1996, or upon initial startup, every owner or
    operator of a bakery oven which is exempt from the control requirements
    of this Subpart because of the criteria specified in Section 219.722(b) of
    this Subpart shall certify that actual VOM emissions from any individual
    exempt bakery oven never exceed 15 TPY and that VOM emissions
    from all exempt bakery ovens, in the aggregate, never exceed 25 TPY.
     
    f) On or before March 15, 1996, or upon initial startup if prior to March
    15, 1998, every owner or operator of a bakery oven which is controlling
    emissions as provided by Section 219.722(c) of this Subpart, shall
    certify that its maximum theoretical emissions as specified in Section
    219.722(c) are less than 90.7 Mg (100 tons) of VOM per year.

    28
    (Source: Repealed at _____ Ill. Reg. ___________, effective __________________)
    Section 219.Appendix G TRE Index Measurements for SOCMI Reactors and
    Distillation Units
    For purposes of Subpart Q, Sections 219.431 through 219.435, the following apply:
    a)
    The following test methods shall be used to determine compliance with the total
    resource effectiveness ("TRE") index value:
     
    1) Method 1 or 1A, incorporated by reference at Section 219.112 of this Part,
    as appropriate, for selection of the sampling site.
     
    A) The sampling site for the vent stream molar composition
    determination and flow rate prescribed in subsections (a)(2) and
    (a)(3) of this Appendix shall be, except for the situations outlined
    in subsection (a)(1)(B), after the final recovery device, if a
    recovery system is present, prior to the inlet of any control
    device, and prior to any post-reactor or post-distillation unit
    introduction of halogenated compounds into the vent stream. No
    traverse site selection method is needed for vents smaller than 10
    cm in diameter.
     
    B) If any gas stream other than the reactor or distillation unit vent
    stream is normally conducted through the final recovery device:
     
    i) The sampling site for vent stream flow rate and molar
    composition shall be prior to the final recovery device and
    prior to the point at which any nonreactor or
    nondistillation unit vent stream or stream from a
    nonaffected reactor or distillation unit is introduced.
    Method 18 incorporated by reference at Section 219.112
    of this Part, shall be used to measure organic compound
    concentrations at this site.
     
    ii. The efficiency of the final recovery device is determined
    by measuring the organic compound concentrations using
    Method 18, incorporated by reference at Section 219.112
    of this Part, at the inlet to the final recovery device after
    the introduction of all vent streams and at the outlet of the
    final recovery device.
     

    29
    iii. The efficiency of the final recovery device determined
    according to subsection (a)(1)(B)(ii) of this Appendix shall
    be applied to the organic compound concentrations
    measured according to subsection (a)(1)(B)(i) of this
    Appendix to determine the concentrations of organic
    compounds from the final recovery device attributable to
    the reactor or distillation unit vent stream. The resulting
    organic compound concentrations are then used to
    perform the calculations outlined in subsection (a)(4) of
    this Appendix.
     
    2) The molar composition of the vent stream shall be determined as follows:
     
    A) Method 18, incorporated by reference at Section 219.112 of this
    Part, to measure the concentration of organic compounds
    including those containing halogens;
     
    B) ASTM D1946-77, incorporated by reference at Section 219.112
    of this Part, to measure the concentration of carbon monoxide
    and hydrogen; and
     
    C) Method 4, incorporated by reference at Section 219.112 of this
    Part, to measure the content of water vapor.
     
    3) The volumetric flow rate shall be determined using Method 2, 2A, 2C,
    or 2D, incorporated by reference at Section 219.112 of this Part, as
    appropriate.
     
    4) The emission rate of VOM (minus methane and ethane) (EVOM) in the
    vent stream shall be calculated using the following formula:
     
    n
    E
    VOM
    = K
    2
     
    Σ
    C
    j
    M
    j
    Q
    s
    j=1
    where:
    E
    VOM
    = Emission rate of VOM (minus methane and ethane) in the sample,
    kg/hr.
    K
    2
    = Constant, 2.494 x 10-6 (l/ppmv)(g- mole/scm)(kg/g)(min/hr), where
    standard temperature for (g-mole/scm) is 20
    ø
    C.

    30
    C = Concentration of compound j, on a dry basis, in ppmv as measured
    by Method 18, incorporated by reference at Section 219.112 of this
    Part, as indicated in Section 219.433(c)(3) of this Part.
    M
    j
    = Molecular weight of sample j, g/g-mole.
    Q
    s
    = Vent stream flow rate (scm) at a temperature of 20
    ø
    C.
     
    5) The total vent stream concentration (by volume) of compounds
    containing halogens (ppmv, by compound) shall be summed from the
    individual concentrations of compounds containing halogens which were
    measured by Method 18, incorporated by reference at Section 219.112
    of this Part.
     
    6) The net heating value of the vent stream shall be calculated using the
    following:
     
    n
    H
    T
    =
    K
    1
     
    Σ
    C
    j
    H
    j
    (1-B
    ws
    )
    j=1
    where:
    H
    T
    =
    Net heating value of the sample (MJ/scm), where the net
    enthaply
    per mole of vent stream is based on combustion of 25
    ø
    C
    and 760
    mmHG, but the standard temperature for determining the
    volume
    corresponding to one mole is 20
    ø
    C as in the definition of
    Qs (vent stream flow rate).
    K
    1
    =
    Constant, 1.740 x 10
    -7
    (ppmv)
    -1
    (g-mole/scm), (MJ/KCal),
    where standard temperature for (g-mole/scm) is 20
    ø
    C.
    B
    ws
    =
    Water vapor content of the vent stream, proportion by volume;
    except that if the vent stream passes through a final stream jet
    and is not condensed, it shall be assumed that B
    ws
    = 0.023 in
    order to correct to 2.3 percent moisture.
    Cj =
    Concentration on a dry basis of compound j in ppmv, as
    measured for all organic compounds by Method 18, incorporated
    by reference at Section 219.112 of this Part, and measured for
    hydrogen and carbon monoxide by using ASTM D1946-77,
    incorporated by reference at Section 219.112 of this Part.
    Hj =
    Net heat of combustion of compound j, kCal/g- mole, based on
    combustion at 25
    ø
    C and 760 mmHG. The heats of combustion

    31
    of vent stream components shall be determined using ASTM
    D2382-83, incorporated by reference at Section 219.112 of this
    Part, if published values are not available or cannot be
    calculated.
    b) 1) The TRE index value of the vent shall be calculated using the following:
    TRE =
    1 [a + b (Q
    s
    ) + c (H
    T
    ) + d (E
    VOM
    )]
    E
    VOM
    where:
    TRE =
    TRE index value.
    E
    VOM
    =
    Hourly emission rate of VOM (kg/hr) as calculated in subsection
    (a)(4) of this Appendix.
    Q
    s
    =
    Vent stream flow rate scm/min at a standard temperature of
    20
    ø
    C.
    H
    T
    =
    Vent stream net heating value (MJ/scm), as calculated in
    subsection (a)(6) of this Appendix.
    E
    VOM
    =
    Hourly emission rate of VOM (minus methane and ethane),
    (kg/hr) as calculated in subsection (a)(4) of this Appendix.
    a,b, =
    Value of coefficients presented below
    c,d
    are:
    Control Device
    Value of Coefficients
    Type of Stream Basis
    a
    b
    c
    d
    Nonhalogenated
    Flare
    2.129 0.183 -0.005 0.359
    Thermal incinerator 3.075 0.021 -0.037 0.018
    zero (0) Percent heat
    Recovery
    Thermal incinerator 3.803 0.032 -0.042 0.007
    70 Percent heat
    Recovery
    Halogenated
    Thermal incinerator 5.470 0.181 -0.040 0.004

    32
    and scrubber
    2) Every owner or operator of a vent stream shall use the applicable
    coefficients identified for values a, b, c and d in subsection (b)(1) of this
    Appendix to calculate the TRE index value based on a flare, a thermal
    incinerator with zero percent heat recovery, and a thermal incinerator
    with 70 percent heat recovery, and shall select the lowest TRE index
    value.
     
    3) Every owner or operator of a reactor or distillation unit with a
    halogenated vent stream, determined as any stream with a total
    concentration of halogen atoms contained in organic compounds of 200
    ppmv or greater, shall use the applicable coefficients identified for
    values a, b, c and d in subsection (b)(1) of this Appendix to calculate the
    TRE index value based on a thermal incinerator and scrubber.
     
    c) Every owner or operator of a source seeking to comply with Section 219.432(b)
    of this Part shall recalculate the flow rate and VOM concentration for each
    affected vent stream whenever process changes are made. Examples of process
    changes include, but are not limited to, changes in production capacity,
    feedstock type, or catalyst type, or whenever there is replacement, removal, or
    addition of recovery equipment. The flow rate and VOM concentration shall be
    recalculated based on test data, or on best engineering estimates of the effects of
    the change to the recovery system.
     
    d) Whenever a process change, as defined in Section 219.435(c) of this Subpart,
    yields a TRE index value of 1.0 or less, the owner or operator shall notify and
    submit a report to the Agency according to the requirements specified in Section
    219.435(c) of this Subpart, within 180 calendar days after the process change
    and shall conduct a performance test according to the methods and procedures
    required by Section 219.433 of this Part.
     
    e) For the purpose of demonstrating that a process vent stream has a VOM
    concentration below 500 ppmv, the following shall be used:
     
    1) The sampling site shall be selected as specified in Section 219.433(c)(1)
    of this Part.
     
    2) Method 18 or Method 25A of 40 CFR Part 60, Appendix A,
    incorporated by reference at Section 219.112 of this Part, shall be used
    to measure concentration; alternatively, any other method or data that
    has been validated according to the protocol in Method 301 of 40 CFR
    Part 63, Appendix A, incorporated by reference at Section 219.112 of
    this Part, may be used.
     

    33
    3) Where Method 18 is used, the following procedures shall be used to
    calculate ppmv concentration:
     
    i) The minimum sampling time for each run shall be 1 hour in
    which either an integrated sample or four grab samples shall be
    taken. If grab sampling is used, then the samples shall be taken
    at approximately equal intervals in time, such as 15 minute
    intervals during the run.
     
    ii) The concentration of VOM shall be calculated using Method 18
    according to Section 219.433(c)(4) of this Part.
     
    4) Where Method 25A is used, the following procedures shall be used to
    calculate ppmv VOM concentration:
    A) Method 25A shall be used only if a single VOM is greater than
    50 percent of total VOM, by volume, in the process vent stream.
     
    B) The vent stream composition may be determined by either
    process knowledge, test data collected using an appropriate
    Reference Method or a method of data collection validated
    according to the protocol in Method 301 of 40 CFR Part 63,
    Appendix A, incorporated by reference at Section 219.112 of
    this Part. Examples of information that constitute process
    knowledge include calculations based on material balances,
    process stoichiometry, or previous test results provided the results
    are still relevant to the current process vent stream conditions.
     
    C) The VOM used as the calibration gas for Method 25A shall be
    the single VOM present at greater than 50 percent of the total
    VOM by volume.
     
    D) The span value for Method 25A shall be 50 ppmv.
     
    E) Use of Method 25A is acceptable if the response from the high-
    level calibration gas is at least 20 times the standard deviation of
    the response from the zero calibration gas when the instrument is
    zeroed on the most sensitive scale.
     
    F) The concentration of VOM shall be corrected to 3 percent oxygen
    using the procedures and equation in Section 219.433(c)(3) of
    this Part.
     

    34
    The owner or operator shall demonstrate that the concentration of VOM,
    including methane and ethane, measured by Method 25A is below 250 ppmv to
    qualify for the low concentration exclusion in Section 219.431 of this Part.
    (Source: Amended at _____ Ill. Reg. ________, effective ________________)
    IT IS SO ORDERED.
    I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control Board, hereby
    certify that the above opinion and order was adopted on the ________ day of
    ____________, 1997 by a vote of ________________.
    ______________________________
    Dorothy M. Gunn
    Illinois Pollution Control Board

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