ILLINOIS POLLUTION CONTROL BOARD
April
11,
1991
IN THE MATTER OF:
)
R90—ll
RCRA UPDATE, USEPA REGULATIONS
)
(Identical in Substance Rules)
(4—1—90 THROUGH 6—30—90)
)
ADOPTED RULE.
FINAL ORDER.
ORDER OF THE BOARD
(By J. Anderson):
Pursuant to Sections 22.4(a)
of the Environmental Protection
Act
(Act), the Board is amending RCRA hazardous waste
regulations.
The amendments involve 35 Iii.
Adin.
Code 703,
720,
721,
722,
724,
725,
726 and 728.
Section 22.4(a) provides for quick adoption of regulations
which are “identical
in substance” to federal regulations;
it
also provides that Title VII of the Act and Section 5 of the
Administrative Procedure Act
(APA) shall not apply.
Because this
rulemaking is not subject to Section
5 of the APA,
it is not
subject to first notice or to second notice review by the Joint
Committee on Administrative Rules
(JCAR).
The federal RCRA
regulations are found at 40 CFR 260 through 270.
This rulemaking
updates RCRA rules to correspond with federal amendments more
fully outlined in the accompanying Opinion.
This Order is supported by an Opinion adopted on the same
day.
The Board will allow 30 days for post—adoption
comment by
the agencies’involved in the authorization process before filing
the adopted rules.
IT IS SO ORDERED.
I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control
Board, hereby certify that
~he
above Order was adopted on the
//~
day of
______________________,
1991, by a vote of
7-0
.
Dorothy N. ,G~mn, Clerk
Illinois ~bl~ution Control Board
/
121—149
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE
G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER b:
PERMITS
PART 703
RCRA PERMIT PROGRAM
Section
703. 100
703.101
703
.
110
Section
703.120
703.121
703.122
703
.
123
703
.
124
703.125
703.126
703.127
Section
703.140
703.141
703. 150
703.151
703. 152
703.153
703
.
154
703.155
703.156
703.157
703. 158
703.159
703.160
Section
703.180
703.181
703.182
703.183
703.184
703.185
703.186
703.187
703.188
703.200
SUBPART A:
GENERAL PROVISIONS
Scope and Relation to Other Parts
Purpose
References
SUBPART B:
PROHIBITIONS
Prohibitions in General
RCRA Permits
Specific Inclusions in Permit Program
Specific Exclusions from Permit Program
Discharges of Hazardous Waste
Reappiications
Initial Applications
Federal Permits
(Repealed)
SUBPART C:
AUTHORIZATION BY RULE AND INTERIM STATUS
Purpose and Scope
Permits by Rule
Application by Existing HWM Facilities and Interim
Status Qualifications
Application by New HWN Facilities
Amended Part A Application
Qualifying for Interim Status
Prohibitions During Interim Status
Changes During Interim Status
Interim Status Standards
Grounds for Termination of Interim Status
Permits for Less Than an Entire Facility
Closure by Removal
Procedures for Closure Determination
SUBPART D:
APPLICATIONS
Applications
in General
Contents of Part A
Contents of Part B
General Information
Facility Location Information
Groundwater Protection Information
Exposure Information
Solid Waste Management Units
Other Information
Specific Information
12
1—150
2
703.201
703.202
703.203
703.204
703.205
703.206
703.207
703.209
Section
703.221
703.222
703.223
703.224
703.225
703.230
703.231
Section
703.240
703.241
703 .242
703.243
703.244
703.245
703.246
703.247
Section
703.260
703.270
703.271
703.272
703.273
703
.
280
703.281
703.282
703.283
Appendix A
Containers
Tank Systems
Surface Impoundments
Waste Piles
Incinerators
Land Treatment
Landfills
Miscellaneous Units
SUBPART E:
SHORT TERM AND PHASED PERMITS
Emergency Permits
Incinerator Conditions Prior to Trial Burn
Incinerator Conditions During Trial Burn
Incinerator Conditions After Trial Burn
Trial Burns for Existing Incinerators
Land Treatment Demonstration
Research,
Development and Demonstration Permits
SUBPART F:
PERMIT CONDITIONS OR DENIAL
Permit Denial
Establishing Permit Conditions
Noncompliance Pursuant to Emergency Permit
Monitoring
Notice of Planned Changes
Twenty-four Hour Reporting
Reporting Requirements
Anticipated Noncompliance
SUBPART C:
CHANGES TO PERMITS
Transfer
Modification
Causes for Modification
Causes for Modification or Reissuance
Facility Siting
Permit Modification at the Request of the Permittee
Class
1 Modifications
Class
2 Modifications
Class
3 Modifications
Classification of Permit Modifications
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act (Ill. Rev.
Stat.
1989,
ch.
111 1/2, pars. 1022.4 and 1027).
SOURCE:
Adopted
in R82-l9,
53 PCB 131,
at 7 Ill.
Reg.
14289,
effective October 12,
1983;
amended in R83-24 at
8 Ill.
Reg. 206,
effective December 27,
1983; amended in R84—9
at 9 Ill. Reg.
11899, effective July 24,
1985; amended in R85—22 at 10 Ill.
Reg.
12 1—151
3
1110,
effective January
2,
1987; amended in R85—23 at
10 Ill.
Reg.
13284, effective July 28,
1986; amended in R86—l at 10
Ill.
Reg.
14093, effective August 12,
1986; amended in R86-l9 at 10
Ill. Reg.
20702, effective December 2,
1986; amended in R86—28 at
11 Ill. Reg.
6121, effective March 24,
1987; amended in R86—46 at
11 Ill. Reg.
13543, effective August
4,
1987; amended in R87-5 at
11 Ill. Reg.
19383, effective November 12,
1987; amended in R87-
26 at 12 Ill. Reg.
2584,
effective January 15,
1988;
amended in
R87—39 at 12 Ill. Reg.
13069, effective July 29,
1988; amended in
R88—16 at 13
Ill. Reg.
447, effective December 27,
1988;
amended
in R89—l at
13 Ill. Reg.
18477, effective November 13,
1989;
amended in R89—9 at
14
Ill. Reg. 6278, effective April
16,
1990;
amended in R90—2 at 14
Ill. Reg. 14492,
effective August 22,
1990; amended in R90-ll at 15 Ill. Reg.
,
effective
SUBPART
D:
APPLICATIONS
Section 703.183
General Information
The following information is required in the Part B application
for all HWM facilities, except as 35 Ill. Adm. Code 724.lOi
provides otherwise:
a)
A general description of the facility;
b)
Chemical and physical analyses of the hazardous wastes
to be handled at the facility.
At a minimum, these
analyses must contain all the information which must be
known to treat, store or dispose of the wastes properly
in accordance with 35 Ill.
Adm.
Code 724;
c)
A copy of the waste analysis plan required by 35 Ill.
Adm.
Code 724.113(b)
and,
if applicable,
35 Ill.
Adm.
Code 724.113(c);
d)
A description of the security procedures and equipment
required by 35
Ill. Adm.
Code 724.114, or a
justification demonstrating the reasons for requesting
a waiver of this requirement;
e)
A copy of the general inspection schedule required by
35
Ill. Adm.
Code 724.115(b).
Include where
applicable, as part of the inspection schedule,
specific requirements in 35 Ill. Adm. Code 724.274,
724.293(i),
724.295, 724.326,
724.354, 724.373,
724.403~&n4724.702, 724.933,
724.952, 924.953 and
724.958
f)
A justification of any request for a waiver of the
preparedness and prevention requirements of
35 Ill.
Adin.
Code 724.Subpart C;
121—152
4
g)
A copy of the contingency plan required by 35 Ill.
Adm.
Code 724.Subpart D;
BOARD NOTE:
Include, where applicable,
as part of the
contingency plan,
specific requirements in 35 Ill.
Adm.
Code 724.327 and 724.355.
35 Ill. Adm. Code 724.355
has not yet been adopted.
h)
A description of procedures, structures or equipment
used at the facility to:
1)
Prevent hazards in unloading operations (for
example, ramps, special forklifts);
2)
Prevent runoff from hazardous waste handling areas
to other areas of the facility or environment, or
to prevent flooding
(for example, berms,
dikes,
trenches);
3)
Prevent contamination of water supplies;
4)
Mitigate effects of equipment failure and power
outages;
e-nd
5)
Prevent undue exposure of personnel to hazardous
waste
(for example, protective clothing);
~
.~j
Prevent releases to the atmosphere.
i)
A description of precautions to prevent accidental
ignition or reaction of ignitable, reactive or
incompatible wastes as required to demonstrate
compliance with 35 Ill. Adm. Code 724.117 including
documentation demonstrating compliance with 35 Ill.
Adm. Code 724.117(c);
j)
Traffic pattern, estimated volume
(number, types of
vehicles) and control
(for example, show turns across
traffic lanes and stacking lanes
(if appropriate);
describe access road surfacing and load bearing
capacity; show traffic control signals);
k)
Facility location information as required by Section
703.184;
1)
An outline of both the introductory and continuing
training programs by owners or operators to prepare
persons to operate or maintain the
HWM
facility in a
safe manner as required to demonstrate compliance with
35 Ill. Adm. Code 724.116.
A brief description of how
training will be designed to meet actual job tasks
in
121—153
5
accordance with requirements in 35 Ill.
Adm. Code
724.116(a) (3);
m)
A copy of the closure plan and, where applicable, the
post-closure
plan
required
by
35
Ill.
Adm.
Code
724.212, 724.218 and 724.297.
Include where
applicable,
as part of the plans, specific requirements
in 35 Ill. Adm. Code 724.278,
724.297, 724.328,
724.358,
724.380,
724.410, 724.451, 724.701 and
724.703;
n)
For hazardous waste disposal units that have been
closed, documentation that notices required under 35
Ill.
Adin Code 724.219 have been filed;
0)
The most recent closure cost estimate for the facility
prepared in accordance with 35 Ill.
Adm. Code 724.242
and a copy of the documentation required to demonstrate
financial assurance under 35 Ill.
Adm. Code 724.243.
For a new facility,
a copy of the required
documentation may be submitted 60 days prior to the
intitial receipt of hazardous wastes,
if it
is later
than the submission of the Part B;
p)
Where applicable, the most recent post—closure cost
estimate for the facility prepared in-accordance with
35
Ill.
Adm. Code 724.244 plus a copy of the
documentation required to demonstrate financial
assurance under 35 Ill. Adm. Code 724.245; For a new
facility,
a copy of the required documentation may be
submitted 60 days prior to the intitial receipt of
hazardous wastes,
if
it is later than the submission of
the Part B;
q)
Where applicable,
a copy of the insurance policy or
other documentation which comprises compliance with the
requirements of 35
Ill. Adm. Code 724.247.
For a new
facility, documentation showing the amount of insurance
meeting the specification of 35 Ill. Adm. Code
724.247(a)
and,
if applicable,
35 Ill.
Adin.
Code
724.247(b),
that the owner or operator plans to have in
effect before initial receipt of hazardous waste for
treatment, storage or disposal.
A request for an
alternative level of required coverage, for a new or
existing facility, may be submitted as specified in 35
Ill.
Adm. Code 724.247(c);
s)
A topographic map showing a distance
of~
1000 feet
around the facility at a scale of 2.5 centimeters
(1
inch)
equal to not more than 61.0 meters
(200 feet).
Contours must be shown on the map.
The contour
interval must be sufficient to clearly show the pattern
121—154
6
of surface water flow in the vicinity of and from each
operational unit of the facility.
For example,
contours with an interval of 1.5 meters
(5 feet),
if
relief is greater than 6.1 meters
(20 feet), or an
interval of 0.6 meters
(2 feet),
if relief
is less than
6.1 meters
(20 feet).
Ownersand operators of HWM
•facilities located in mountainous areas shall use
larger contour intervals to adequately show topographic
profiles of facilities.
The map must clearly show the
following:
1)
Map scale and date;
2)
100—year floodplain area;
3)
Surface waters including intermittent streams;
4)
Surrounding land uses (residential, commercial,
agricultural, recreational);
5)
A wind rose
(i.e., prevailing windspeed and
direction);
6)
Orientation of the map (north arrow);
7)
Legal boundaries of the
HWM
facility site;
8)
Access control
(fences, gates);
9)
Injection and withdrawal wells both on-site and
off—site;
10)
Buildings; treatment, storage or disposal
operations;
or other structures (recreation areas,
runoff control systems, access and internal roads,
storm,
sanitary and process sewage systems,
loading and unloading areas,
fire control
facilities,
etc.);
11)
Barriers for drainage or flood control;
12)
Location of operational units within the HWM
facility site, where hazardous waste is
(or will
be)
treated,
stored or disposed (include equipment
cleanup areas);
BOARD NOTE:
For large HWM facilities,
the Agency
shall allow the use of other scal&s on a case by
case basis.
t)
Applicants shall submit such information as the Agency
determines is necessary for it to determine whether to
121—155
7
issue a permit and what conditions to impose in any
permit
issued.
u)
For land disposal facilities,
if a case—by—case
extension has been approved under 35 Ill. Adm. Code
728.105, or if
a petition has been approved under 35
Ill. Adm. Code 728.106, a copy of the notice of
approval of the extension or of approval of the
petition is required.
BOARD NOTE:
Derived from 40 CFR 270.14(b)
(1988),
as
amended at 54 Fed. Reg.
617, January
9, 1989.
Source:
Amended at 15 Ill. Reg.
,
effective
Section 703.210
Process Vents
Except as otherwise provided in 35 Ill. Adm. Code 724.101,
owners
and operators of facilities which have process vents to which 35
Ill. Adm. Code 724.Subpart AA applies shall provide the following
additional information:
~j
For facilities which cannot install a closed-vent
system and control device to comply with 35 Ill. Mm.
Code 724.Subpart AA, on the effective date on which the
facility becomes sublect to that Subpart or 35 Ill.
Adm. Code 725.Subpart AA. an implementation schedule as
specified in 35 Ill. Adm. Code 724.933(a) (2).
~j
Documentation of compliance with the process vent
standards in 35 Ill.
Adm. Code 724.932,
including:
fl
Information and data identifying all affected
process vents, annual throughput and operating
hours of each affected unit, estimated emission
rates for the affected vent and for the overall
facility
(i.e.. the total emissions for all
affected vents at the facility) and the
approximate location within the facility of each
affected unit (e.g.,
identify the hazardous waste
management units on a facility plot plan).
21
Information and data supporting estimates of vent
emissions and emission reduction achieved by add—
on control devices based on engineering
calculations or source tests.
For the purpose of
determining compliance, estimates of vent
emissions and emission reductions must be made
using operating parameter values
(e.g.,
temperatures, flow rates or concentrations) which
represent the conditions which exist when the
121—156
8
waste management unit is operating at the highest
load or capacity level reasonably expected to
occur.
fl
Information and data used to determine whether or
not a process vent is sublect to 35
Ill. Adm. Code
724.932.
~
Where an owner or operator applies for permission to
use a control device other than a thermal vapor
incinerator, catalytic vapor incinerator,
flare,
boiler, process heater, condenser or carbon adsorption
sYstem to comply with 35 Ill.
Adiu.
Code 724.932, and
chooses to use test data to determine the organic
removal efficiency or the total organic compound
concentration achieved by the control device,
a
performance test plan as specified in 35 Ill.
Adm. Code
724.935(b) (3).
~j.
Documentation of compliance with 35 Ill. Adm. Code
724.933, including:
fl
A list of all information references and sources
used in preparing the documentation.
21.
Records including the dates of each compliance
test recruired by 35 Ill. Adm. Code 724.933(k).
~j
A design analysis, specifications, drawings,
schematics, and piping and instrumentation
diagrams based on the appropriate sections of APTI
Course 415,
incorporated by reference in 35 Ill.
Adm. Code 720.111, or other engineering texts
approved bY the Agency which present basic control
device design
information.
The design analysis
must address the vent stream characteristics and
control device parameters as specified in 35
Ill.
Adm. Code 724.935(b) (4) (C).
j)
A statement signed and dated by the owner or
operator certifyincr that the operating parameters
used in the design analysis reasonably represent
the conditions which exist when the hazardous
waste management unit is or would be operating at
the highest load or capacity level reasonably
exPected to occur.
~j
A statement signed and dated by the owner or
operator certifying that the control device is
designed to operate at an efficiency of 95 weight
percent or crreater unless the total organic
emission limits of
35
Ill. Adm. Code 724.932(a)
121—157
9
for affected process vents at the facility can be
attained by a control device involving vapor
recovery at an efficiency less than 95 weight
percent.
Source:
Added at 15 Ill. Reg.
,
effective
Section 703.211
Equipment
Except as otherwise provided in 35 Ill.
Adni.
Code 724.101, owners
and operators of facilities which have equipment to which 35 Ill.
Adm. Code 724.Subpart BB applies shall provide the following
additional information:
~J
For each piece of equipment to which 35
Ill.
Adm. Code
724.Subpart BB applies:
fl.
Eguipment identification number and hazardous
waste management unit identification.
21
Approximate locations within the facility
(e.g.,
identify the hazardous waste management unit on a
facility plot plan).
~J.
Type of eciui~ment(e.g.,
a pump or pipeline
valve).
4j
Percent by weight total organics in the hazardous
wastestream at the equipment.
~j
Hazardous waste state at the equipment (e.g.,
gas/vapor or
liquid).
~J
Method of compliance with the standard (e.g.,
“monthly leak detection and repair” or “equipped
with dual mechanical seals”).
~j.
For facilities which cannot install a closed—vent
system and control device to comply with 35
Ill.
Adin.
Code 724.Subpart BB on the effective date that facility
becomes sublect to this Subpart or 35
111.
Adm. Code
724.Subpart BB,
an implementation schedule as specified
in 35 Ill.
Adm. Code 724.933(a) (2).
~
Where an owner or operator applies for permission to
use
a control device other than a thermal vapor
incinerator, catalytic vapor incinerato’r,
flare,
boiler, process heater, condenser or carbon adsorption
system and chooses to use test data to determine the
organic removal efficiency or the total organic
compound concentration achieved by the control device,
12 1—158
10
a performance test plan as specified in 35 Ill.
Adm.
Code 724.935(b) (3)
~j.
Documentation which demonstrates compliance with the
equipment standards
in 35 Ill. Adm. Code 724.952 or
724.959.
This documentation must contain the records
required under 35 Ill. Adm. Code 724.964.
The Agency
shall request further documentation if necessary to
demonstrate compliance.
Documentation to demonstrate
compliance with 35 Ill. Adm. Code 724.960 must include
the following information:
jj
A list of all information references and sources
used in preparing the documentation.
21
Records including the dates of each compliance
test required by 35 Ill. Adm. Code 724.933(1).
fl
A design analysis, specifications,
drawings,
schematics,
and piping and instrumentation.
diagrams based on the appropriate sections of APTI
Course 415, incorporated by reference in 35
Ill.
Mm. Code 720.111, or other engineering texts
appproved by the Agency which present basic
control device design information.
The design
analysis must address the vent stream
characteristics and control device parameters as
specified in 35
Ill.
Adni.
Code 724.935(b) (4) (C).
iL
A statement signed and dated by the owner or
operator certifying that the operating parameters
used
in the design analysis reasonably represent
the conditions which exist when the hazardous
waste management unit is or would be operating at
the highest load or capacity level reasonably
expected to occur.
~j
A statement signed and dated by the owner or
operator certifying that the control device is
designed to operate at an efficiency of 95 weight
percent or greater.
Source:
Added at 15 Ill. Reg.
,
effective
12 1—159
11
Section 703.Appendix A
Classification of Permit Modifications
Class
Modifications
A.
General Permit Provisions
1
1.
Administrative and informational changes.
1
2.
Correction of typographical errors.
1
3.
Equipment replacement or upgrading with
functionally equivalent components
(e.g., pipes,
valves, pumps, conveyors, controls).
4.
Changes in the frequency of or procedures for
monitoring,
reporting,
sampling or maintenance
activities by the permittee:
1
a.
To provide for more frequent monitoring,
reporting or maintenance.
2
b.
Other changes.
5.
Schedule of compliance:
1*
a.
Changes in interim compliance dates, with
prior approval of the Agency.
BOARD NOTE:
~
indicates that prior Agency
approval is required.
3
b.
Extension of final compliance date.
1*
6.
Changes
in expiration date of permit to allow
earlier permit termination, with prior approval of
the Agency.
1*
7.
Changes in ownership or operational control of a
facility, provided the procedures of Section
703.260(b)
are followed.
B.
General Facility Standards
1.
Changes to waste sampling or analysis methods:
1
a.
To conform with Agency guidance or Board
regulations.
~
To incorporate changes associated with F039
(multi—source leachate) sampling or analysis
methods.
12 1—160
12
2
~.
Other changes.
2.
Changes to analytical quality assurance/control
plan:
1
a.
To conform with agency guidance or
regulations.
2
b.
Other changes.
1
3.
Changes in procedures for maintaining the
operating record.
2
4.
Changes in frequency or content of inspection
schedules.
5.
Changes in the training plan:
2
a.
That affect the type or decrease the amount
of training given to employees.
1
b.
Other changes.
6.
Contingency plan:
2
a.
Changes in emergency procedures
(i.e.,
spill
or release response procedures).
1
b.
Replacement with functionally equivalent
equipment,
upgrade or relocate emergency
equipment listed.
2
c.
Removal of equipment from emergency equipment
list.
1
d.
Changes in name,
address or phone number of
coordinators or other persons or agencies
identified in the plan.
Note:
When a permit modification (such as
introduction of a new unit)
requires a change
in facility plans or other general facility
standards, that change must be reviewed under
the same procedures as the permit
modification.
C.
Groundwater Protection
1.
Changes to wells:
2
a.
Changes in the number,
location, depth or
design of upgradient or downgradient wells of
121—161
13
permitted groundwater monitoring system.
I
b.
Replacement of an existing well that has been
damaged or rendered inoperable, without
change to location, design or depth of the
well.
1*
2.
Changes in groundwater sampling or analysis
procedures or monitoring schedule, with prior
approval of the Agency.
1*
3.
Changes in statistical procedure for determining
whether a statistically significant change in
groundwater quality between upgradient and
downgradient wells has occurred, with prior
approval of the Agency.
2*
4.
Changes in point of compliance.
5.
Changes in indicator parameters, hazardous
constituents or concentration limits
(including
ACLs (Alternate Concentration Limits)):
3
a.
As specified in the groundwater protection
standard.
2
b.
As specified in the detection monitoring
program.
2
6.
Changes to a detection monitoring program as
required by 35 Ill.
Adm. Code 724.198(j),
unless
otherwise specified in this Appendix.
7.
Compliance monitoring program:
3
a.
Addition of compliance monitoring program as
required by 35 Ill.
Adm. Code 724.198(h) (4)
and 724.199.
2
b.
Changes to a compliance monitoring program as
required by 35 Ill.
Adm. Code 724.199(k),
unless otherwise specified in this Appendix.
8.
Corrective action program:
3
a.
Addition of
a corrective action program as
required by 35
Ill. Adm. Code 724.199(i) (2)
and 724.200.
2
b.
Changes to a corrective action program as
required by 35 Ill. Adm. Code 724.200(h),
unless otherwise specified in this Appendix.
12 1—162
14
D.
Closure
1.
Changes to the closure plan:
1*
a.
Changes in estimate of maximum extent of
operations •or maximum inventory of waste on—
site at any time during the active life of
the facility, with prior approval of the
Agency.
1*
b.
Changes in the closure schedule for any unit,
changes in the final closure schedule for the
facility or extension of the closure period,
with prior approval of the Agency.
1*
c.
Changes in the expected year of final
closure, where other permit conditions are
not changed, with prior approval of the
Agency.
1*
d.
Changes in procedures for decontamination of
facility equipment or structures, with prior
approval of the Agency.
2
e.
Changes in approved closure plan resulting
from unexpected events occurring during
partial or final closure, unless otherwise
specified in this Appendix.
2
f.
Extension of the closure period to allow a
landfill, surface impoundment or land
treatment unit to receive non—hazardous
wastes after final receipt of hazardous
wastes under 35 Ill. Adm. Code 724.213(d)
or
(e).
3
2.
Creation of a new landfill unit as part of
closure.
3.
Addition of the following new units to be used
temporarily for closure activities:
3
a.
Surface impoundments.
3
b.
Incinerators.
3
c.
Waste piles that do not comply with 35 Ill.
Adm. Code 724.350(c).
2
d.
Waste piles that comply with 35 Ill.
Adm.
Code 724.350(c).
12 1—163
15
2
e.
Tanks or containers (other than specified
below).
1*
f.
Tanks used for neutralization,
dewatering,
phase separation or component separation,
with prior approval of the Agency.
E.
Post—Closure
1.
Changes in name,
address or phone number of
contact in post—closure plan.
2
2.
Extension of post—closure care period.
3
3.
Reduction in the post—closure care period.
4.
Changes to the expected year of final closure,
where other permit conditions are not changed.
2
5.
Changes in post—closure plan necessitated by
events occurring during the active life of the
facility, including partial and final closure.
F.
Containers
1.
Modification or addition of container units:
3
a.
Resulting in greater than 25
increase in the
facility’s container storage capacity, except
as provided in F(l) (c) and F(4) (a).
2
b.
Resulting in up to 25
increase in the
facility’s container storage capacity, except
as provided in F(l) (c) and F(4) (a).
c.
Or treatment processes necessary to treat
wastes that are restricted from land disposal
to meet some or all of the applicable
treatment standards or to treat wastes to
satisfy (in whole or in part)
the standard of
“use of practically available technology that
yields the greatest environmental benefit”
contained in 40 CFR 268.8(a) (2) (ii),
incorporated by reference in 35 Ill. Adm.
Code 728.108, with prior approval of the
Agency.
This modification may also involve
the addition of new waste codes or narrative
description of wastes.
It is not applicable
to dioxin-containing wastes
(F020, F02l,
F022,
F023,
F026,
F027 and F028).
121—164
16
2.
2
a.
Modification of a container unit without
increasing the capacity of the unit.
b.
Addition of a roof to a container unit
without alteration of the containment system.
3.
Storage of different wastes in containers, except
as provided in F(4):
3
a.
That require additional or different
management practices from those authorized in
the permit.
2
b.
That do not require additional or different
management practices from those authorized in
the permit.
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
4.
Storage or treatment of different wastes in
containers:
2
a.
That require addition of units or change in
treatment process or management standards,
provided that the wastes are restricted from
land disposal and are to be treated to meet
some or all of the applicable treatment
standards, or are to be treated to satisfy
(in whole or in part)
the standard of “use of
practically available technology that yields
the greatest environmental benefit” contained
in 40 CFR 268.8 (a) (2) (ii),
incorporated by
reference in
35 Ill. Adm.
Code 728.108.
It
is not applicable to dioxin-containing wastes
(F020,
F02l,
F022, F023,
F026,
F027 and
F028)
b.
That do not require the addition of unite or
a change in the treatment process or
management standards,
and provided that the
units have previously received wastes of the
same type
(e.g.,
incinerator scrubber water).
This modification is not appl’icable to
dioxin-containing wastes
(F020, F021,
F022,
F023,
F026,
F027 and F028).
G.
Tanks
12
1—165
17
1.
3
a.
Modification or addition of tank units
resulting in greater than 25
increase in the
facility’s tank capacity, except as provided
in paragraphs G(l) (c),
G(l) (d) and G(1) (e).
2
b.
Modification or addition of tank units
resulting in up to 25
increase in the
facility’s tank capacity, except as provided
in paragraphs G(1) (d) and G(l) (e).
2
c.
Addition of a new tank that will operate for
more than 90 days using any of the following
physical or chemical treatment technologies:
neutralization,
dewatering, phase separation
or component separation.
1*
d.
After prior approval of the Agency, addition
of a new tank that will operate for up to 90
days using any of the following physical or
chemical treatment technologies:
neutralization, dewatering, phase separation
or component separation.
e.
Modification or addition of tank units or
treatment processes that are necessary to
treat wastes that are restricted from land
disposal to meet some or all of the
applicable treatment standards or to treat
wastes to satisfy (in whole or in part)
the
standard of “use of practically available
technology that yields the greatest
environmental benefit” contained in 40 CFR
268.8(a) (2) (ii),
incorporated by reference in
35
Ill. Adm. Code 728.108, with prior
approval of the Agency.
This modification
may also involve the addition of new waste
codes.
It is not applicable to dioxin—
containing wastes
(F020,
F021,
F022,
F023,
F026,
F027 and F028).
2
2.
Modification of a tank unit or secondary
containment system without increasing the capacity
of the unit.
3.
Replacement of a tank with a tank that meets the
same design standards and has a capacity within
+1-
10
of the replaced tank provided:
a.
The capacity difference is no more than 1500
12 1—166
18
gallons,
b.
The facility’s permitted tank capacity is not
increased and
c.
The replacement tank meets the same
conditions in the permit.
2
4.
Modification of a tank management practice.
5.
Management of different wastes in tanks:
3
a.
That require additional or different
management practices, tank design, different
fire protection specifications or
significantly different tank treatment
process from that authorized in the permit,
except as provided in paragraph G(5) (c).
2
b.
That do not require additional or different
management practices, tank design, different
fire protection specification or
significantly different tank treatment
process than authorized in the permit, except
as provided in paragraph G(5) (d).
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
c.
That require addition of units or change in
treatment processes or management standards,
provided that the wastes are restricted from
land disposal and are to be treated to meet
some or all of the applicable treatment
standards,
or that are to be treated to
satisfy
(in whole or in part)
the standard of
“use of practically available technology that
yields the greatest environmental benefit”
contained in 40 CFR 268.8(a) (2) (ii),
incorporated by reference in 35 Ill. Adm.
Code 728.108.
The modification is not
applicable to dioxin-containing wastes
(F020,
F02l,
F022, F023,
F026,
F027 and F028).
a.
d.
That do not require the addition of units or
a change in the treatment prcfcess or
management standards,
and provided that the
units have previously received wastes of the
same type
(e.g.,
incinerator scrubber water).
This modification is not applicable to
12
1—167
19
dioxin-containing wastes
(F020,
F021,
F022,
F023,
F026, F027 and F028).
H.
Surface Impoundments
3
1.
Modification or addition of surface impoundment
units that result in increasing the facility’s
surface impoundment storage or treatment capacity.
3
2.
Replacement of a surface impoundment unit.
2
3.
Modification of a surface impoundment unit without
increasing the facility’s surface impoundment
storage or treatment capacity and without
modifying the unit’s liner, leak detection system
or leachate collection system.
2
4.
Modification of a surface impoundment management
practice.
5.
Treatment,
storage or disposal of different wastes
in surface impoundments:
3
a.
That require additional or different
management practices or different design of
the liner or leak detection system than
authorized in the permit.
2
b.
That do not require additional or different
management practices or different design of
the liner or leak detection system than
authcrized in the permit.
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
C.
That are wastes restricted from land disposal
that meet the applicable treatment standards
or that are treated to satisfy the standard
of “use of practically available technology
that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a) (2) (ii),
incorporated by reference in 35 Ill. Adm.
Code 728.108, and provided that the unit
meets the minimum technological reguireinents
stated in 40 CFR 268.5(h) (2)
,‘
incorporated by
reference in 35 Ill. Adm. Code 728.105.
This
modification is not applicable to dioxin-
containing wastes
(F020,
F021,
F022,
F023,
F026, F027 and F028).
12 1—168
20
d.
That are residues from wastewater treatment
or incineration, provided the disposal occurs
in a unit that meets the minimum
technological reguirements stated in 40 CFR
268.5(h) (2), incorporated by reference in 35
Ill. Adm. Code 728.105, and provided further
that the surface impoundment has previously
received wastes of the same type
(for
example,
incinerator scrubber water).
This
modification is not applicable to dioxin-
containing wastes (F020, F02l,
F022,
F023,
F026,
F027 and F028).
I.
Enclosed Waste Piles.
For all waste piles,
except
those complying with 35
Ill. Mm.
Code 724.350(c),
modifications are treated the same as for a landfill.
The following modifications are applicable only to
waste piles complying with 35 Ill.
Adin.
Code
724.350(c).
1.
Modification or addition of waste pile units:
3
a.
Resulting in greater than 25
increase in the
facility’s waste pile storage or treatment
capacity.
2
b.
Resulting in up to 25
increase in the
facility’s waste pile storage or treatment
capacity.
2
2.
Modification of waste pile unit without increasing
the capacity of the unit.
3.
Replacement of a waste pile unit with another
waste pile unit of the same design and capacity
and meeting all waste pile conditions in the
permit.
2
4.
Modification of a waste pile management practice.
5.
Storage or treatment of different wastes in waste
piles:
3
a.
That require additional or different
management practices or different design of
the unit.
2
b.
That do not require additional or different
management practices or different design of
the unit.
12
1—169
19
dioxin-containing wastes
(F020,
F021,
F022,
F023,
F026, F027 and F028).
H.
Surface Impoundments
3
1.
Modification or addition of surface impoundment
units that result in increasing the facility’s
surface impoundment storage or treatment capacity.
3
2.
Replacement of
a surface impoundment unit.
2
3.
Modification of a surface impoundment unit without
increasing the facility’s surface impoundment
storage or treatment capacity and without
modifying the unit’s liner, leak detection system
or leachate collection system.
2
4.
Modification of a surface impoundment management
practice.
5.
Treatment, storage or disposal of different wastes
in surface impoundments:
3
a.
That require additional or different
management practices or different design of
the liner or leak detection system than
authorized in the permit.
2
b.
That do not require additional or different
management practices or different design of
the liner or leak detection system than
authorized in the permit.
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
c.
That are wastes restricted from land disposal
that meet the applicable treatment standards
or that are treated to satisfy the standard
of “use of practically available technology
that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a) (2) (ii),
incorporated by reference in 35 Ill. Adm.
Code 728.108,
and provided that the unit
meets the minimum technological reguirements
stated in 40 CFR 268.5(h) (2)
,
incorporated by
reference in 35
Ill. Adm. Code 728.105.
This
modification is not applicable to dioxin-
containing wastes
(F020,
F02l, F022,
F023,
F026,
F027 and F028).
12
1—168
20
d.
That are residues from wastewater treatment
or incineration, provided the disposal occurs
in a unit that meets the minimum
technological reguirements stated in 40 CFR
268.5(h) (2), incorporated by reference in 35
Ill. Adm. Code 728. 105, and provided further
that the surface impoundment has previously
received wastes of the same
type
(for
example, incinerator scrubber water).
This
modification is not applicable to dioxin-
containing wastes
(F020, F021, F022,
F023,
F026, F027 and F028).
I.
Enclosed Waste Piles.
For all waste piles, except
those complying with 35 Ill.
Adm. Code 724.350(c),
modifications are treated the same as for a landfill.
The following modifications are applicable only to
waste piles complying with 35 Ill. Adm.
Code
724.350(c).
1.
Modification or addition of waste pile units:
3
a.
Resulting in greater than 25
increase in the
facility’s waste pile storage or treatment
capacity.
2
b.
Resulting in up to 25
increase in the
facility’s waste pile storage or treatment
capacity.
2
2.
Modification of waste pile unit without increasing
the capacity of the unit.
3.
Replacement of a waste pile unit with another
waste pile unit of the same design and capacity
and meeting all waste pile conditions in the
permit.
2
4.
Modification of a waste pile management practice.
5.
Storage or treatment of different wastes in waste
piles:
3
a.
That require additional or different
management practices or different design of
the unit.
2
b.
That do not require additional or different
management practices or different design of
the unit.
121—169
21
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
3.
Landfills and Unenclosed Waste Piles
3
1.
Modification or addition of landfill units that
result in increasing the facility’s disposal
capacity.
3
2.
Replacement of a landfill.
3
3.
Addition or modification of a liner,
leachate
collection system,
leachate detection system, run-
off control or final cover system.
2
4.
Modification of a landfill unit without changing a
liner,
leachate collection system, leachate
detection system, run—off control or final cover
system.
2
5.
Modification of a landfill management practice.
6.
Landfill different wastes:
3
a.
That require additional or different
management practices, different design of the
liner, leachate collection system or leachate
detection system.
2
b.
That do not require additional or different
management practices, different design of the
liner,
leachate collection system or leachate
detection system.
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
c.
That are wastes restricted from land disposal
that meet the applicable treatment standards
or that are treated to satisfy the standard
of “use of practically available technology
that yields the greatest environmental
benefit” contained in 40 CFR 268.8(a) (2) (ii),
incorporated by reference in 35 Ill. Adm.
Code 728.108, and provided that the landfill
unit meets the minimum technological
reguirements stated in 40 CFR 268.5(h) (2),
incorporated by reference in 35 Ill. Adm.
121—170
22
Code 728.105.
This modification is not
applicable to dioxin-containing wastes
(F020,
F02l, F022,
F023,
F026,
F027 and F028).
d.
That are residues from wastewater treatment
or incineration, provided the disposal occurs
in a landfill unit that meets the minimum
technological reguirements stated in 40 CFR
268.5(h) (2), incorporated by reference in 35
Ill. Adm. Code 728.105, and provided further
that the landfill has previously received
wastes of the same type
(for example,
incinerator ash).
This modification is not
applicable to dioxin—containing wastes
(F020,
F02l,
F022,
F023,
F026,
F027 and F028).
K.
Land Treatment
3
1.
Lateral expansion of or other modification of a
land treatment unit to increase area extent.
2
2.
Modification of run—on control system.
3
3.
Modify run-off control system.
2
4.
Other modification of land treatment unit
component specifications or standards required in
permit.
5.
Management of different wastes in land treatment
units:
3
a.
That require a change in permit operating
conditions or unit design specifications.
2
b.
That do not require a change in permit
operating conditions or unit design
specifications.
Note:
See Section 703.280(g)
for
modification procedures to be used for the
management of newly listed or identified
wastes.
6.
Modification of a land treatment unit management
practice to:
3
a.
Increase rate or change methd’d of waste
application.
b.
Decrease rate of waste application.
121—171
23
2
7.
Modification of a land treatment unit management
practice to change measures of pH or moisture
content or to enhance microbial or chemical
reactions.
3
8.
Modification of a land treatment unit management
practice to grow food chain crops, to add to or
replace existing permitted crops with different
food chain crops or to modify operating plans for
distribution of animal feeds resulting from such
crops.
3
9.
Modification of operating practice due to
detection of releases from the land treatment unit
pursuant to 35 Ill. Adm. Code 724.378(g) (2).
3
10.
Changes in the unsaturated zone monitoring system
resulting in a change to the location, depth,
number of sampling points or replace unsaturated
zone monitoring devices or components of devices
with devices or components that have
specifications different from permit requirements.
2
11.
Changes in the unsaturated zone monitoring system
that do not result in a change to the location,
depth, number of sampling points, or that replace
unsaturated zone monitoring devices or components
of devices with devices or components having
specifications different from permit requirements.
2
12.
Changes in background values for hazardous
constituents in soil and soil-pore liquid.
2
13.
Changes in sampling, analysis or statistical
procedure.
2
14.
Changes in land treatment demonstration program
prior to or during the demonstration.
1*
15.
Changes in any condition specified in the permit
for a land treatment unit to reflect results of
the land treatment demonstration, provided
performance standards are met, and the Agency’s
prior approval has been received.
1*
16.
Changes to allow a second land treatment
demonstration to be conducted when the results of
the first demonstration have not shown the
conditions under which the wastes can be treated
completely, provided the conditions for the second
demonstration are substantially the same as the
conditions for the first demonstration and have
121—172
24
received the prior approval of the Agency.
3
17.
Changes to allow a second land treatment
demonstration to be conducted when the results of
the first demonstration have not shown the
conditions under which the wastes can be treated
completely, where the conditions for the second
demonstration are not substantially the same as
the conditions for the first demonstration.
2
18.
Changes in vegetative cover requirements for
closure.
L.
Incinerators
3
1.
Changes to increase by more than 25
any of the
following limits authorized in the permit: A
thermal feed rate limit,
a waste feed rate limit
or an organic chlorine feed rate limit.
The
Agency shall require a new trial burn to
substantiate compliance with the regulatory
performance standards unless this demonstration
can be made through other means.
2
2.
Changes to increase by up to 25
any of the
following limits authorized in the permit: A
thermal feed rate limit,
a waste feed limit or an
organic chlorine feed rate limit.
The Agency
shall require a new trial burn to substantiate
compliance with the regulatory performance
standards unless this demonstration can be made
through other means.
3
3.
Modification of an incinerator unit by changing
the internal size or geometry of the primary or
secondary combustion units,
by adding a primary or
secondary combustion unit, by substantially
changing the design of any component used to
remove HCI or particulates from the combustion
gases or by changing other features of the
incinerator that could affect its capability to
meet the regulatory performance standards.
The
Agency shall require a new trial burn to
substantiate compliance with the regulatory
performance standards, unless this demonstration
can be made through other means.
2
4.
Modification of an incinerator unit in a manner
that will not likely affect the capability of the
unit to meet the regulatory performance standards
but which will change the operating conditions or
monitoring requirements specified in the permit.
121—173
25
The Agency may require a new trial burn to
demonstrate compliance with the regulatory
performance standards.
5.
Operating requirements:
3
a.
Modification of the limits specified in the
permit for minimum combustion gas
temperature, minimum combustion gas residence
time or oxygen concentration in the secondary
combustion chamber.
The Agency shall require
a new trial burn to substantiate compliance
with the regulatory performance standards
unless this demonstration can be made through
other means.
3
b.
Modification of any stack gas emission limits
specified in the permit, or modification of
any conditions
in the permit concerning
emergency shutdown or automatic waste feed
cutoff procedures or controls.
2
c.
Modification of any other operating condition
or any inspection or recordkeeping
requirement specified in the permit.
6.
Incineration of different wastes:
3
a.
If the waste contains a POHC that is more
difficult to incinerate than authorized by
the permit or if incineration of the waste
requires compliance with different regulatory
performance standards than specified in the
permit, the Agency shall require a new trial
burn to substantiate compliance with the
regulatory performance standards,
unless this
demonstration can be made through other
means.
b.
If the waste does not contain a POHC that is
more difficult to incinerate than authorized
by the permit and if incineration of the
waste does not require compliance with
different regulatory performance standards
than specified in the permit.
BOARD NOTE:
See Section 703.280(g)
for
modification procedures to
be~
used for the
management of newly listed or identified
wastes.
7.
Shakedown and trial burn:
12 1—174
26
2
a.
Modification of the trial burn plan or any of
the permit conditions applicable during the
shakedown period for determining operational
readiness after construction, the trial burn
period or the period immediately following
the trial burn.
1*
b.
Authorization of up to an additional 720
hours of waste incineration during the
shakedown period for determining operational
readiness after construction, with the prior
approval of the Agency.
1*
c.
Changes in the operating requirements set in
the permit for conducting a trial burn,
provided the change
is minor and has received
the prior approval of the Agency.
1*
d.
Changes in the ranges of the operating
requirements set in the permit to reflect the
results of the trial burn, provided the
change is minor and has received the prior
approval of the Agency.
8.
Substitution of an alternate type of fuel that is
not specified in the permit.
BOARD NOTE:
Derived from 40 CFR 270.42, Appendix
I,
as adopted at 53 Fed.
fleg.
37934,
Scptcmber 28,
1988
(1990)
(Source:
Amended at 15 Ill.
Reg.
,
effective
121—175
27
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE
C:
WASTE DISPOSAL
CHAPTER
I:
POLLUTION CONTROL BOARD
SUBCHAPTER
C:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 720
HAZARDOUS WASTE MANAGEMENT SYSTEM:
GENERAL
SUBPART A:
GENERAL PROVISIONS
Section
720.101
720.102
720.103
Section
720.110
720.111
Purpose, Scope and Applicability
Availability of Information; Confidentiality of
Information
Use of Number and Gender
SUBPART B:
DEFINITIONS
Definitions
References
SUBPART
C:
RULEMAKING PETITIONS AND OTHER PROCEDURES
Section
720.120
720.121
720. 122
720.130
720.131
720.132
720.133
720.140
720.141
Appendix A
Rulemaking
Alternative Equivalent Testing Methods
Waste Delisting
Procedures for Solid Waste Determinations
Solid Waste Determinations
Boiler Determinations
Procedures for Determinations
Additional regulation of certain hazardous waste
Recycling Activities on a case—by—case Basis
Procedures for case—by—case regulation of
hazardous waste Recycling Activities
Overview of 40 CFR, Subtitle C Regulations
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act (Ill.
Rev. Stat.
1989,
ch.
111
1/2, pars.
1022.4 and 1027).
SOURCE:
Adopted in R8l-22,
43 PCB 427,
at
5 Ill. Reg.
9781,
effective as noted in 35
111. Adm. Code 700.106; amended and
codified in R81—22,
45 PCB 317,
at 6 Ill. Reg.
4828,
effective as
noted in
35 Ill.
Adm. Code
700.106; amended in R82-19 at
7
Ill.
Reg.
14015, effective Oct.
12,
1983;
amended in R84-9,
53 PCB 131
at 9
Ill. Reg.
11819, effective July 24,
1985;
amended in R85—
22 at 10 Ill.
Reg.
968, effective January
2,
1986; amended in
R86—1 at 10 Ill. Reg.
13998, effective August 12,
1986;
amended
in R86—l9 at 10 Ill.
Reg.
20630, effective December 2,
1986;
amended in R86-28 at 11
Ill. Reg.
6017,
effective March 24,
1987;
amended in R86-46 at 11
Iii.
Reg.
13435, effective August
4,
1987;
amended in R87—5 at 11 Ill.
Reg.
19280, effective November
12,
1987;
amended in R87—26 at 12
Ill.
Reg.
2450, effective
January 15,
1988;
amended in R87—39 at 12 Ill. Reg.
12999,
12
1—176
28
effective July 29,
1988;
amended in R88—l6 at 13
Ill.
Reg. 362,
effective December 27,
1988;
amended in R89—l at 13
Ill. Reg.
18278, effective November 13,
1989;
amended in R89—2
at
14
Ill.
Reg.
3075,
effective February 20,
1990;
amended in R89—9 at 14
Ill.
Reg.
6225,
effective April
16,
1990;
amended in R90-10 at
14 Ill. Reg.
16450,
effective September 25,
1990;
amended in
R90—l7 at 15 Iii. Reg.
,
effective
amended in R90-ll at 15 Ill. Reg.
,
effective
SUBPART
B:
DEFINITIONS
Section 720.lllReferences
a)
The following publications are incorporated by
reference:
ANSI.
Available from the American National
Standards Institute,
1430 Broadway, New York, New
York
10018,
(212)
354—3300:
ANSI B3l.3 and B3l.4.
See ASME/ANSI B3l.3
and B3l.4
API.
Available from the American Petroleum
Institute,
1220 L Street, N.W.,
Washington,
D.C.
20005,
(202)
682—8000:
“Guide for Inspection of Refinery Equipment,
Chapter XIII, Atmospheric and Low Pressure
Storage Tanks,” 4th Edition,
1981, reaffirmed
December,
1987.
“Cathodic Protection of Underground Petroleum
Storage Tanks and Piping Systems,” API
Recommended Practice 1632, Second Edition,
December,
1987.
“Installation of Underground Petroleum
Storage Systems,” API Recommended Practice
1615,
Fourth Edition, November,
1987.
APTI.
Available from the Air and Waste Management
Association,
Box 2861, Pittsburgh,
PA
15230,
(412)
232—3444:
APTI Course
415:
Control of Gaseous
Emissions, EPA Publication EPA—450/2-8l-005,
December,
1981.
ASME.
Available from the American Society of
Mechanical Engineers,
345 East 47th Street, New
12 1—17 7
29
York, NY
10017,
(212)
705—7722:
“Chemical Plant and Petroleum Refinery
Piping”, ASME/ANSI B31.3—1987,
as
supplemented by B3l.3a-1988 and B31.3b-l988.
Also available from ANSI.
“Liquid Transportation Systems for
Hydrocarbons, Liquid Petroleum Gas, Anhydrous
Ammonia, and Alcohols”, ASME/ANSI B31.4—
1986, as supplemented by B31.4a—1987.
Also
available from ANSI.
ASTM.
Available from American Society for Testing
and Materials,
1916 Race Street, Philadelphia, PA
19103,
(215)
299—5400:
“ACTM Standard Test Methods for Flash Point
of Liquids by Cetaflash Closed Tester,” ACTh
Standard D 3823 87.
ASTN D93-85,”ASTM Standard Test Methods for
Flash Point ~yPensky-Martens
Closed Tester-,-”
ASTM Standard D 93
79 or D-93-Boapproved
October 25,
1985.
ASTM D1946-90, Standard Practice for Analysis
of Reformed Gas by Gas Chromatography,
Approved March 30,
1990.
ASTM D2267-88, Standard Test Method for
Aroinatics in Light Naphthas and Aviation
Gasolines by Gas Chromatography,
approved
November 17,
1988.
ASTM D2382-88, Standard Test Method for Heat
of Combustion of Hydrocarbon Fuels by Bomb
Calorimeter
(High Precision Method), approved
October 31,
1988.
ASTM D2879-86,
Standard Test Method for Vapor
Pressure—Temperature Relationship and Initial
Decomposition Temperature of Liquids by
Isoteniscope, approved October
31,
1986.
ASTN D3828-87, Standard Test Methods for
Flash Point of Liquids by Setaflash Closed
Tester, approved December 14,~1988.
ASTM El68—88, Standard Practices for General
Techniques of Infrared Quantitative Analysis,
approved May 27,
1988.
12 1—178
30
ASTM El69—87, Standard Practices for General
Techniques of Ultraviolet-Visible
Quantitative Analysis, approved February
1,
1987.
ASTM E260-85, Standard Practice for Packed
Column Gas Chromatography, approved June 28,
1985.
GPO.
Available from the Superintendent of
Documents,
U.S. Government Printing Office,
Washington,
D.C.
20401,
(202)
783—3238:
Standard Industrial Classification Manual
(1972), and 1977 Supplement,
republished in
1983
NACE.
Available from the National Association of
Corrosion Engineers,
1400 South Creek Dr.,
Houston, TX
77084,
(713)
492—0535:
“Control of External Corrosion on Metallic
Buried, Partially Buried, or
Submerged Liquid
Storage Systems”, NACE Recommended Practice
RP0285—85,
approved March,
1985.
NFPA.
Available from the National Fire Protection
Association, Batterymarch Park,
Boston, MA
02269,
(617)
770—3000 or
(800)
344—3555:
“Flammable and Combustible Liquids Code” NFPA
30, issued July 17,
1987.
Also available
from ANSI.
NTIS.
Available from the National Technical
Information Service,
5285 Port Royal Road,
Springfield, VA
22161,
(703)
487—4600:
“Generic Quality Assurance Project Plan for
Land Disposal Restrictions Program”, EPA/530-
SW-87—Oll, March 15,
1987.
(Document number
PB 88—l70766.j
“Methods for Chemical Analysis of Water and
Wastes”, Third Edition, March,
1983.
(Document number PB 84—128677)
“Petitions to Delist Hazardous Wastes
--
A
Guidance Manual”, EPA/530—SW—85-003,
April,
1985.
(Document Number PB 85—194488
121.—179
31
“Procedures Manual for Ground Water
Monitoring at Solid Waste Disposal
Facilities”, EPA—530/SW—6ll,
1977.
(Document
number PB 84-174820)
“Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods,” EPA Publication
number SW-846
(Second Edition,
1982 as
amended by Update
I
(April,
1984)
and Update
II
(April, 1985))
(Document number PB 87-
120291)
STI.
Available from the Steel Tank Institute,
728
Anthony Trail,
Northbrook,
IL
60062,
(312) 498—
1980:
“Standard for Dual Wall Underground Steel
Storage Tanks”
(1986).
USEPA.
Available from United States Environmental
Protection Agency,
Office of Drinking Water, State
Programs Division, WH 550 E, Washington,
D.C.
20460:
“Technical Assistance Document:
Corrosion,
Its Detection and Control in Injection
Wells”, EPA 570/9—87—002, August,
1987.
b)
Code of Federal Regulations.
Available from the
Superintendent of Documents,
U.S. Government Printing
Office, Washington,
D.C.
20401,
(202)
783—3238:
10 CFR 20, Appendix B
(1939) (1990)
40 CFR 60
(1990)
40 CFR 61, Subpart V
(1990)
40 CFR 136 (1089) (1990)
40 CFR 142
(1939) (1990)
40 CFR 220
(1039) (1990)
40 CFR 260.20
(1089) (1990)
40 CFR 264
(1089) (1990)
40 CFR 302.4,
302.5 and 302.6
(1089) (1990)
40 CFR 761
(1039) (1990)
121—180
32
c)
Federal Statutes
Section 3004 of the Resource Conservation and Recovery
Act
(42 U.S.C.
6901 et seq.), as amended through
December 31,
1987.
d)
This Section incorporates no later editions or
amendments.
(Source:
Amended at 15 Ill. Reg.
,
effective
12 1—181
33
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE
G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER
C:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 721
IDENTIFICATION
AND
LISTING OF HAZARDOUS WASTE
SUBPART A:
GENERAL PROVISIONS
Section
721.101
721.102
721.103
721.104
721.105
721. 106
721.107
721.108
Purpose of Scope
Definition of Solid Waste
Definition of Hazardous Waste
Exclusions
Special Requirements for Hazardous Waste Generated
by Small Quantity Generators
Requirements for Recyclable Materials
Residues of Hazardous Waste in Empty Containers
PCB Wastes Regulated under TSCA
SUPBART
B:
CRITERIA FOR IDENTIFYING
THE CHARACTERISTICS
OF HAZARDOUS WASTE AND FOR LISTING HAZARDOUS WASTES
Section
721.110
721.111
Section
721.120
721.121
721.122
721.123
721.124
Criteria for Identifying the Characteristics of
Hazardous Waste
Criteria for Listing Hazardous Waste
SUBPART C:
CHARACTERISTICS OF HAZARDOUS WASTE
General
Characteristic of Ignitability
Characteristic of Corrosivity
Characteristic of Reactivity
Toxicity Characteristic
Section
721.130
721.131
721.132
721. 133
Appendix A
Appendix B
Appendix
Table A
Table B
Table C
SUBPART D:
LISTS OF HAZARDOUS WASTE
General
Hazardous Wastes From Nonspecific Sources
Hazardous Waste from Specific Sources
Discarded Commercial Chemical Products, Off-
Specification
Species,
Container Residues and
Spill Residues Thereof
Representative Sampling Methods
Method 1311 Toxicity Characteristic Leaching
Procedure
(TCLP)
C
Chemical Analysis Test Methods
Analytical Characteristics of Organic Chemicals
(Repealed)
Analytical Characteristics of Inorganic Species
(Repealed)
Sample Preparation/Sample Introduction Techniques
(Repealed)
121—182
34
Appendix C
Basis for Listing Hazardous Wastes
Appendix H
Hazardous Constituents
Appendix
I
Wastes Excluded under Section 720.120 and 720.122
Table A
Wastes Excluded from Non—Specific Sources
Table B
Wastes Excluded from Specific Sources
Table C
Wastes Excluded From Commercial Chemical Products,
Off-Specification Species, Container Residues, and
Soil Residues Thereof
Appendix J
Method of Analysis for Chlorinated Dibenzo-p-
Dioxins and Dibenzofurans
Appendix
Z
Table to Section 721.102
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111 1/2, pars.
1022.4 and 1027).
SOURCE:
Adopted in R8l-22,
43 PCB 427, at
5 Ill.
Reg. 9781,
effective as noted in 35 Ill. Adm. Code 700.106;
amended and
codified in R81-22,
45 PCB 317,
at
6 Ill.
Reg. 4828, effective as
noted in 35
Ill. Adm. Code 700.106; amended in R82—18,
51 PCB 31,
at
7 Ill. Reg. 2518,
effective February 22,
1983.; amended in R82—
19,
53 PCB 131, at 7
Ill.
Reg.
13999,
effective October 12,
1983;
amended in R84-34,
61 PCB 247, at 8
Ill. Reg.
24562,
effective
December 11,
1984; amended in R84-9, at
9 Ill.
Reg.
11834,
effective July 24,
1985;
amended in R85-22 at 10 Ill. Reg.
998,
effective January
2,
1986; amended in R85-2 at 10 Ill.
Reg.
8112,
effective May 2,
1986; amended in R86—l at 10 Ill. Reg.
14002,
effective August 12,
1986;
amended in R86-19 at 10
Ill. Reg.
20647, effective December
2,
1986; amended in R86—28 at Il
Ill.
Reg.
6035, effective March 24,
1987; amended in R86-46 at 11 Ill.
Reg.
13466, effective August
4,
1987; amended in R87—32 at
11
Ill.
Reg.
16698, effective September 30,
1987; amended in R87-5
at 11 Ill. Reg.
19303, effective November 12,
1987; amended in
R87-26 at 12
Ill.
Reg.
2456,
effective January 15,
1988;
amended
in R87—30 at
12
Ill. Reg.
12070, effective July 12,
1988; amended
in R87—39 at
12 Ill.
Reg.
13006, effective July 29,
1988; amended
in R88—l6 at
13
Ill.
Reg.
382, effective December 27,
1988;
amended in R89-1 at 13 Ill. Reg.
18300, effective November 13,
1989; amended in R90-2 at 14
Ill.
Reg. 14401, effective
August
22,
1990; amended in R90—10 at
14 Ill.
Reg.
16472, effective
September 25,
1990; amended in R90—l7 at
15 Ill.
Reg.
effective
; amended in R90-1l at 15 Ill. Reg.
effective
SUBPART A:
GENERAL PROVISIONS
Section 721.104
Exclusions
a)
Materials which are not solid wastes.
The following
materials are not solid wastes for the purpose of this
Part:
12 1—183
35
1)
Sewage:
A)
Domestic sewage; and
B)
Any mixture of domestic sewage and other
waste that passes through a sewer system to
publicly—owned treatment works for treatment.
“Domestic sewage” means untreated sanitary
wastes that pass through a sewer system.
2)
Industrial wastewater discharges that are point
source discharges with NPDES permits issued by the
Agency pursuant to Section 12(f) of the
Environmental Protection Act and 35 Ill. Mm.
Code
309.
BOARD NOTE:
This exclusion applies only to the
actual point source discharge.
It does not
exclude industrial wastewaters while they are
being collected,
stored or treated before
discharge, nor does
it exclude sludges that are
generated by industrial wastewater treatment.
3)
Irrigation return flows.
4)
Source, special nuclear or by—product material as
defined by the Atomic Energy Act of 1954,
as
amended
(42
U.S.C.
2011 et seq.)
5)
Materials subjected to in-situ mining techniques
which are not removed from the ground as part of
the extraotion process.
6)
Pulping liquors
(i.e., black liquor) that are
reclaimed in a pulping liquor recovery furnace and
then reused in the pulping process, unless
accumulated speculatively as defined in Section
721.101(c)
;
7)
Spent sulfuric acid used to produce virgin
sulfuric acid, unless
it is accumulated
speculatively as defined in Section 721.101(c).
8)
Secondary materials that are reclaimed and
returned
to
the original process or processes in
which they were generated where they are reused
in
the production process, provided:
A)
Only tank storage
is involved, and the entire
process through completion of reclamation is
closed by being entirely connected with pipes
or other comparable enclosed means of
12 1—184
36
conveyance;
B)
Reclamation does not involve controlled flame
combustion (such as occurs in boilers,
industrial furnaces or incinerators);
C)
The secondary materials are never accumulated
in such tanks for over twelve months without
being reclaimed; and
D)
The reclaimed material is not used to produce
a fuel,
or used to produce products that are
used in a manner constituting disposal.
b)
Solid wastes which are not hazardous wastes.
The
following solid wastes are not hazardous wastes:
1)
Household waste,
including household waste that
has been collected,
transported, stored, treated,
disposed, recovered
(e.g.,
refuse—derived fuel) or
reused.
“Household waste” means any waste
material
(including garbage, trash and sanitary
wastes in septic tanks)
derived from households
(including single and multiple residences, hotels
and motels,
bunkhouses, ranger stations, crew
quarters, campgrounds, picnic grounds and day—use
recreation areas).
A resource recovery facility
managing municipal solid waste shall not be deemed
to be treating, storing, disposing of or otherwise
managing hazardous wastes for the purposes of
regulation under this Part,
if such facility:
A)
Receives and burns only:
i)
Household waste
(from single and
multiple dwellings, hotels, motels and
other residential sources) and
ii)
Solid waste from commercial or
industrial sources that does not contain
hazardous waste; and
B)
Such facility does not accept hazardous waste
and the owner or operator of such facility
has established contractural requirements or
other appropriate notification or inspection
procedures to assure that hazardous wastes
are not received at or burned in such
facility.
2)
Solid wastes generated by any of the following and
which are returned to the soil as fertilizers:
12 1—185
37
A)
The growing and harvesting of agricultural
crops.
B)
The raising of animals,
including animal
manures.
3)
Mining overburden returned to the mine site.
4)
Fly ash waste,
bottom ash waste, slag waste, and
flue gas emission control waste generated
primarily from the combustion of coal or other
fossil fuels.
5)
Drilling fluids, produced waters, and other wastes
associated with the exploration, development, or
production of crude oil, natural gas or geothermal
energy.
6)
Chromium wastes:
A)
Wastes which fail the test for the toxicity
characteristic (Section 721.124 and Appendix
B) because chromium is present or are listed
in Subpart D due to the presence of chromium,
which do not fail the test for the toxicity
characteristic for any other constituent or
are not listed due to the presence of any
other constituent, and which do not fail the
test for any other characteristic,
if it is
shown by a waste generator or by waste
generators that:
i)
The chromium in the waste is exclusively
(or nearly exclusively) trivalent
chromium; and
ii)
The waste is generated from an
industrial process which uses trivalent
chromium exclusively
(or nearly
exclusively) and the process does not
generate hexavalent chromium; and
iii) The waste is typically and frequently
managed in non—oxidizing environments.
B)
Specific wastes which meet the standard in
subsections
(b) (6) (A) (i),
(ii) and
(iii)
(so
long as they do not fail the test for the
characteristic of EP toxicity, and do not
fail the test for any other characteristic)
are
121—186
38
1)
Chrome
(blue)
trimmings generated by the
following subcategories of the leather
tanning and finishing industry; hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
ii)
Chrome
(blue)
shavings generated by the
following subcategories of the leather
tanning and finishing industry; hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beairthouse; through-
the-blue; and shearling.
iii) Buffing dust generated by the following
subcategories of the leather tanning and
finishing industry:
hair pulp/chrome
tan/retan/wet finish; hair save/chrome
tan/retan/wet finish; retan/wet finish;
no beamhouse; through—the—blue.
iv)
Sewer screenings generated by the
following subcategories of the leather
tanning and finishing industry:
hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
v)
Wastewater treatment sludges generated
by the following subcategories of the
leather tanning and finishing industry:
hair pulp/chrome tan/retan/wet finish;
hair save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
vi)
Wastewater treatment sludges generated
by the following subcategories of the
leather tanning and finishing industry:
hair pulp/chrome tan/retan/wet finish;
hair save/chrome tan/retan/wet finish;
and through-the-blue.
vii) Waste scrap leather fronr the leather
tanning industry, the shoe manufacturing
industry, and other leather product
manufacturing industries.
12 1—187
39
viii)
Wastewater treatment sludges from
the production of titanium dioxide
pigment using chromium—bearing ores
by the chloride process.
7)
Solid waste from the extraction, beneficiation and
processing of ores and minerals (including coal),
including phosphate rock and overburden from the
mining of uranium ore.
For purposes of this
subsection,
beneficiation of ores and minerals is
restricted to the following activities:
crushing,
grinding, washing,
dissolution, crystallization,
filtration,
sorting,
sizing,
drying, sintering,
pelletizing, briquetting, calcining to remove
water or carbon dioxide,
roasting, autoclaving or
chlorination in preparation for leaching
(except
where the roasting or autoclaving or
chlorination)/leaching sequence produces a final
or intermediate product that does not undergo
further beneficiation or processing), gravity
concentration, magnetic separation,
electrostatic
separation,
floatation,
ion exchange, solvent
extraction,
electrowinning, precipitation,
amalgamation, and heap, dump, vat tank and in situ
leaching.
For the purposes of this subsection,
solid waste from the processing of ores and
minerals will include only the following wastes:
A)
Slag from primary copper processing;
B)
Slag from primary lead processing;
C)
Red and brown muds from bauxite refining;
D)
Phosphogypsum from phosphoric acid
production;
E)
Slag from elemental phosphorus production;
F)
Gasifier ash from coal gasification;
G)
Process wastewater from coal gasification;
H)
Calcium sulfate wastewater treatment plant
sludge from primary copper processing;
I)
Slag tailings from primary copper processing;
J)
Fluorogypsum from hydrofluoric acid
production;
K)
Process wastewater from hydrofluoric acid
12 1—188
40
production;
L)
Air pollution control dust/sludge from iron
blast furnaces;
M)
Iron blast furnace slag;
N)
Treated residue from roasting/leaching of
chrome ore;
0)
Process wastewater from primary magnesium
processing by the anhydrous process;
P)
Process wastewater from phosphoric acid
production;
Q)
Basic oxygen furnace and open hearth furnace
air pollution control dust/sludge from carbon
steel production;
R)
Basic oxygen furnace and open hearth furnace
slag from carbon steel production;
5)
Chloride processing waste solids from
titanium tetrachioride production;
T)
Slag from primary zinc smelting; and,
U)
Until June 30,
1991, process wastewater,
acid
plant blowdown and wastewater treatment plant
solids from primary zinc smelting and
refining, except for wastewater treatment
plant solids which are hazardous by
characteristic and which are not processed.
8)
Cement kiln dust waste.
9)
Solid waste which consists of discarded wood or
wood products which fails the test for the
toxicity characteristic solely for arsenic and
which is not a hazardous waste for any other
reason or reasons if the waste
is generated by
persons who utilize the arsenical—treated wood and
wood products for these materials’ intended end
use.
10)
Petroleum-contaminated media and debris that fail
the test for the toxicity characte~isticof
Section 721.124
(hazardous waste codes D0l8
through D043 only)
and are subject to corrective
action regulations under 35 Ill. Adm. Code 731.
12 1—189
41
C)
Hazardous wastes which are exempted from certain
regulations.
A hazardous waste which is generated in a
product or raw material storage tank,
a product or raw
material transport vehicle or vessel, a product or raw
material pipeline, or in a manufacturing process unit
or an associated non—waste—treatment manufacturing
unit,
is not subject to regulation under 35 Ill. Adm.
Code 702,
703, 705 and 722 through 725 and 728 or to
the notification requirements of Section 3010 of RCRA
until
it exits the unit in which it was generated,
unless the unit is a surface impoundment, or unless the
hazardous waste remains in the unit more than 90 days
after the unit ceases to be operated for manufacturing,
or for storage or transportation of product or raw
materials.
d)
Samples
1)
Except as provided in subsection
(d) (2), a sample
of solid waste or a sample of water, soil or air,
which is collected for the sole purpose of testing
to determine its characteristics or composition,
is not subject to any requirements of this Part or
35
Ill. Adm. Code 702, 703,705 and 722 through
728.
The sample qualifies when:
A)
The sample is being transported to a
laboratory for the purpose of testing; or
B)
The sample is being transported back to the
sample collector after testing; or
C)
The sample is being stored by the sample
collector before transport to a laboratory
for testing; or
D)
The sample is being stored in a laboratory
before testing; or
E)
The sample
is being stored in a laboratory
for testing but before it is returned to the
sample collector; or
F)
The sample
is being stored temporarily in the
laboratory after testing for a specific
purpose
(for example,
until conclusion of a
court case or enforcement action where
further testing of the sampl~may be
necessary).
2)
In order to qualify for the exemption in
subsection
(d) (1) (A) and
(B),
a sample collector
121—190
42
shipping samples to a laboratory and a laboratory
returning samples to a sample collector must:
A)
Comply with U.S. Department of Transportation
(DOT),
U.S. Postal Service
(USPS)
or any
other applicable shipping requirements; or
B)
Comply with the following requirements if the
sample collector determines that DOT, USPS or
other shipping requirements do not apply to
the shipment of the sample:
i)
Assure that the following information
accompanies the sample:
The sample
collector’s name, mailing address and
telephone number; the laboratory’s name,
mailing address and telephone number;
the quantity of the sample; the date of
the shipment; and a description of the
sample.
ii)
Package the sample so that it does not
leak,
spill or vaporize from its
packaging.
3)
This exemption does not apply if the laboratory
determines that the waste is hazardous but the
laboratory is no longer meeting any of the
conditions stated in subsection
(d) (1).
e)
Treatability study samples.
1)
Except as
is provided in subsection
(e) (2),
persons who generate or collect samples for the
purpose of conducting treatability studies,
as
defined in 35 Ill.
Adm. Code 720.110, are not
subject to any requirement of 35 Ill. Adm. Code
721 through 723 or to the notification
requirements of Section 3010 of the Resource
Conservation and Recovery Act.
Nor are such
samples included in the quantity determinations of
Section 721.105 and 35 Ill. Adm. Code 722.134(d)
when:
A)
The sample
is being collected and prepared
for transportation by the generator or sample
collector;
or,
B)
The sample is being accumulated or stored by
the generator or sample collector prior to
transportation to a laboratory or testing
facility; or
121—191
43
C)
The sample is being transported to the
laboratory or testing facility for the
purpose of conducting a treatability study.
2)
The exemption in subsection
(e) (1)
is applicable
to samples of hazardous waste being collected and
shipped for the purpose of conducting treatability
studies provided that:
A)
The generator or sample collector uses
(in
“treatability studies”) no more than 1000 kg
of any non—acute hazardous waste,
1 kg of
acute hazardous waste or 250 kg of soils,
water or debris contaminated with acute
hazardous waste for each process being
evaluated for each generated wastestream; and
B)
The mass of each shipment does not exceed
1000 kg of non—acute hazardous waste,
1 kg of
acute hazardous waste or 250 kg of soils,
water or debris contaminated with acute
hazardous waste;
and
C)
The sample must be packaged so that it does
not leak,
spill or vaporize from its
packaging during shipment and the
requirements of subsections
(i) or
(ii) are
met.
i)
The transportation of each sample
shipment complies with U.S. Department
of Transportation (DOT), U.S. Postal
Service
(USPS)
or any other applicable
shipping requirements; or
ii)
If the DOT, USPS or other shipping
requirements do not apply to the
shipment of the sample,
the following
information must accompany the sample:
The name, mailing address and telephone
number of the originator of the sample;
the name,
address and telephone number
of the facility that will perform the
treatability study; the quantity of the
sample; the date of the shipment; and, a
description of the sample, including its
USEPA hazardous waste ninaber.
D)
The sample is shipped to a laboratory or
testing facility which is exempt under
subsection
(f) or has an appropriate RCRA
12 1—192
44
permit or interim status.
E)
The generator or sample collector maintains
the following records for a period ending
3
years after completion of the treatability
study:
i)
Copies of the shipping documents;
ii)
A copy of the contract with the facility
conducting the treatability study;
iii) Documentation showing:
The amount of
waste shipped under this exemption; the
name, address and USEPA identification
number of the laboratory or testing
facility that received the waste; the
date the shipment was made;
and, whether
or not unused samples and residues were
returned to the generator.
F)
The generator reports the information
required in subsection
(e) (2) (E) (iii)
in its
report under 35 Ill. Adm. Code 722.141.
3)
The Agency may grant requests, on a case—by—case
basis,
for quantity limits in excess of those
specified in subsection
(e) (2) (A), for up to an
additional 500 kg of any non-acute hazardous
waste,
1 kg of acute hazardous waste and 250 kg of
soils, water or debris contaminated with acute
hazardous waste, to conduct further treatability
study evaluation when:
There has been an
equipment or mechanical failure during the conduct
of the treatability study; there is need to verify
the results of a previously conducted treatability
study; there is a need to study and analyze
alternative techniques within a previously
evaluated treatment process;
or, there is a need
to do further evaluation of an ongoing
treatability study to determine final
specifications for treatment.
The additional
quantities allowed are subject to all the
provisions in subsections
(e) (1) and
(e) (2) (B)
through
(F).
The generator or sample collector
must apply to the Agency and provide in writing
the following information:
A)
The reason why the generator or sample
collector requires additional quantity of
sample for the treatability study evaluation
and the additional quantity needed;
12 1—193
45
B)
Documentation accounting for all samples of
hazardous waste from the wastestream which
have been sent for or undergone treatability
studies, including the date each previous
sample was shipped, the quantity of each
previous shipment, the laboratory or testing
facility to which it was shipped, what
treatability study processes were conducted
on each sample shipped, and the available
results of each treatability study;
C)
A description of the technical modifications
or change in specifications which will be
evaluated and the expected results;
D)
If such further study is being required due
to equipment or mechanical failure, the
applicant must include information regarding
the reason for the failure or breakdown and
also include what procedures or equipment
have been made to protect against further
breakdowns;
and,
E)
Such other information as the Agency
determines is necessary.
4)
Final Agency determinations pursuant to this
subsection may be appealed to the Board.
f)
Samples undergoing treatability studies at laboratories
or testing facilities.
Samples undergoing treatability
studies and the laboratory or testing facility
conducting such treatability studies (to the extent
such facilities are not otherwise subject to RCRA
requirements) are not subject to any requirement of
this Part,
or of 35 Ill.
Adm. Code 702,
703,
705,
722
through 726, and 728,
or to the notification
requirements of Section 3010 of the Resource
Conservation and Recovery Act, provided that the
requirements of subsections
(f) (1) through
(f) (11) are
met.
A mobile treatment unit may qualify as a testing
facility subject to subsections
(f) (1) through
(f) (11).
Where a group of mobile treatment units are located at
the same site, the limitations specified in subsections
(f) (1) through
(f) (11) apply to the entire group of
mobile treatment units collectively as if the group
were one mobile treatment unit.
1)
No less than 45 days before conducting
treatability studies, the facility notifies the
Agency in writing that it intends to conduct
12 1—194
46
treatability studies under this subsection.
2)
The laboratory or testing facility conducting the
treatability study has a USEPA identification
number.
3)
No more than a total of 250 kg of “as received”
hazardous waste is subjected to initiation of
treatability studies in any single day.
“As
received” waste refers to the waste as received in
the shipment from the generator or sample
collector.
4)
The quantity of “as received” hazardous waste
stored at the facility for the purpose of
evaluation in treatability studies does not exceed
1000 kg, the total of which can include 500 kg of
soils, water or debris contaminated with acute
hazardous waste or
1 kg of acute hazardous waste.
This quantity limitation does not include:.
A)
Treatability study residues; and,
B)
Treatment materials (including nonhazardous
solid waste)
added to “as received” hazardous
waste.
5).
No more than 90 days have elapsed since the
treatability study for the sample was completed,
or no more than one year has elapsed since the
generator or sample collector shipped the sample
to the laboratory or testing facility, whichever
date first occurs.
6)
The treatability study does not involve the
placement of hazardous waste on the land or open
burning of hazardous waste.
7)
The facility maintains records for 3 years
following completion of each study that show
compliance with the treatment rate limits and the
storage time and quantity limits.
The following
specific information must be included for each
treatability study conducted:
A)
The name, address and USEPA identification
number of the generator or sample collector
of each waste sample;
B)
The date the shipment was received;
C)
The quantity of waste accepted;
12
1—195
47
D)
The quantity of “as received” waste in
storage each day;
E)
The date the treatment study was initiated
and the amount of “as received” waste
introduced to treatment each day;
F)
The date the treatability study was
concluded;
G)
The date any unused sample or residues
generated from the treatability study were
returned to the generator or sample collector
or,
if sent to a designated facility, the
name of the facility and the USEPA
identification number.
8)
The facility keeps,
on-site,
a copy of the
treatability study contract and all shipping
papers associated with the transport of
treatability study samples to and from the
facility for a period ending
3 years from the
completion date of each treatability study.
9)
The facility prepares and submits a report to the
Agency by March 15 of each year that estimates the
number of studies and the amount of waste expected
to be used in treatability studies during the
current year, and includes the following
information for the previous calendar year:
A)
The name, address and USEPA identification
number of the facility conducting the
treatability studies;
B)
The types
(by process) of treatability
studies conducted;
C)
The names and addresses of persons for whom
studies have been conducted (including their
USEPA identification numbers);
D)
The total quantity of waste in storage each
day;
E)
The quantity and types of waste subjected to
treatability studies;
F)
When each treatability study was conducted;
G)
The final disposition of residues and unused
12 1—196
48
sample from each treatability study;
10)
The facility determines whether any unused sample
or residues generated by the treatability study
are hazardous waste under Section 721.103 and, if
so, are subject to 35
Ill. Adm. Code 702, 703 and
721 through 728, unless the residues and unused
samples are returned to the sample originator
under the subsection
(e)
exemption.
11)
The facility notifies the Agency by letter when
the facility is no longer planning to conduct any
treatability studies at the site.
(Source:
Amended at 15 Ill. Reg.
,
effective
Section 721.106
Requirements for Recyclable Materials
a)
Recyclable materials:
1)
Hazardous wastes that are recycled are subject to
the requirements for generators, transporters and
storage facilities of subsections
(b) and
(c),
except for the materials listed in subsections
(a) (2) and
(a) (3).
Hazardous wastes that are
recycled will be known as “recyclable materials”.
2)
The following recyclable materials are not subject
to the requirements of this Section but are
regulated under 35 Ill. Adm. Code 726.Subparts C
through C and all applicable provisions in 35 Ill.
Adm. Code 702, 703 and 705.
A)
Recyclable materials used in a manner
constituting disposal
(35 Ill. Adm. Code
726.Subpart C);
B)
Hazardous wastes burned for energy recovery
in boilers and industrial furnaces that are
not regulated under 35 Ill. Adm. Code 724 or
725.Subpart 0
(35 Ill.
Adm. Code 726.Subpart
D.)
C)
Used oil that exhibits one or more of the
characteristics of hazardous waste and is
burned for energy recovery in boilers or
industrial furnaces that are ‘not regulated
under 35 Ill. Mm. Code 724 or 725.Subpart
0.
(35 Ill. Adm. Code 726.Subpart E);
D)
Recyclable materials from which precious
12 1—197
49
metals are reclaimed (35 Ill.
Adm. Code
726.Subpart F);
E)
Spent lead-acid batteries that are being
reclaimed
(35 Ill. Adm. Code 726.Subpart G).
3)
The following recyclable materials are not subject
to regulation under 35 Ill. Adm. Code 722 through
726,
728, or 702,
703 or 705 and are not subject
to the notification requirements of Section 3010
of the Resource Conservation and Recovery Act:
A)
Industrial ethyl alcohol that is reclaimed
except that, unless provided otherwise in an
international agreement as specified in 35
Ill.
Adm. Code 722.158:
i)
A person initiating a shipment for
reclamation in a foreign country, and
any intermediary arranging for the
shipment, shall comply with the
requirements applicable to a primary
exporter in 35 Ill. Adm. Code 722.153,
722.156(a)(1) through
(a)(4),
(a)(6)
and
(b), and 722.157, shall export such
materials only upon consent of the
receiving country and in conformance
with the USEPA Acknowledgement of
Consent as defined in 35 Ill. Mm.
Code
722.Subpart
E, and shall provide a copy
of the USEPA Acknowledgement of Consent
to the shipment to the transporter
transporting the shipment for export;
ii)
Transporters transporting a shipment for
export shall not accept a shipment if
the transporter knows the shipment does
not conform to the USEPA Acknowledgement
of Consent,
shall ensure that a copy of
the USEPA Acknowledgement of Consent
accompanies the shipment and shall
ensure that it is delivered to the
facility designated by the person
initiating the shipment.
B)
Used batteries
(or used battery cells)
returned to a battery manufacturer for
regeneration;
C)
Used oil that exhibits one or more of the
characteristics of hazardous waste but is
recycled in some other manner than being
12 1—198
50
burned for energy recovery;
D)
Scrap metal;
E)
Fuels produced from the refining of oil—
bearing hazardous wastes along with normal
process streams at a petroleum refining
facility if such wastes result from normal
petroleum refining, production and
transportation practices;
F)
.
Oil reclaimed from hazardous waste resulting
from normal petrolueiu refining, production
and transportation practices, which oil is to
be refined along with normal process streams
at a petroleum refining facility;
G)
Coke and coal tar from the iron and steel
industry that contains USEPA hazardous waste
number K087
(decanter tank tar sludgefrom
coking operations)
(Section 721.132)
from the
iron and steel production process;
H)
Petroleum refining wastes.
i)
Hazardous waste fuel produced from oil—
bearing hazardous wastes from petroleum
refining, production or transportation
practices,
or produced from oil
reclaimed from such hazardous wastes,
where such hazardous wastes are
reintroduced into a process that does
not use distillation or does not produce
products from crude oil so long as the
resulting fuel meets the used oil
specification under 35 Ill. Adm. Code
726.140(e)
and so long as no other
hazardous wastes are used to produce the
hazardous waste fuel;
ii)
Hazardous waste fuel produced from oil—
bearing hazardous waste from petroleum
refining production and transportation
practices, where such hazardous wastes
are reintroduced into a refining process
after a point at which contaminants are
removed,
so long as the fuel meets the
used oil fuel specifica?ion under 35
Ill. Adm. Code 726.140(e);
and
iii)
Oil reclaimed from oil-bearing hazardous
wastes from petroleum refining,
121—199
51
production and transportation practices,
which reclaimed oil is burned as a fuel
without reintroduction to a refining
process,
so long as the reclaimed oil
meets the used oil fuel specification
under 35
Ill.
Adin. Code 726.140(e); and
I)
Petroleum coke produced from petroleum
refinery hazardous wastes containing oil at
the same facility at which such wastes were
generated, unless the resulting coke product
exceeds one or more of the characteristics of
hazardous waste in Subpart C.
b)
Generators and transporters of recyclable materials are
subject to the applicable requirements of 35 Ill. Adm.
Code 722 and 723 and the notification requirements
under Section 3010 of the Resource Conservation and
Recovery Act, except as provided in subsection
(a).
c)
Storage and recycling:
1)
Owners or operators of facilities that store
recyclable materials before they are recycled are
regulated under all applicable provisions of 35
Ill. Adm. Code 724.Subparts A through
L, AA and BB
and 725.Subparts A through L, AA and BB,
726,
728,
702, 703 and 705 and the notification requirement
under Section 3010 of the Resource Conservation
and Recovery Act, except as provided in subsection
(a).
(The recycling process itself is exempt from
regulation, except as provided in subsection
(d).)
2)
Owners or operators of facilities that recycle
recyclable materials without storing them before
they are recycled are subject to the following
requirements, except as provided in subsection
(a).
A)
Notification requirements under Section 3010
of the Resource Conservation and Recovery
Act.
B)
35 Ill. Adm. Code 725.171 and 725.172
(dealing with the use of the manifest and
manifest discrepancies)
~j
Subsection
(d).
~j
Owners or operators of facilities required to have a
RCRA permit Pursuant to 35
Ill. Adm. Code 703 with
hazardous waste management units which recycle
121—200
52
hazardous wastes are sublect to 35
Ill. Adm. Code
724.Subpart AA and BB and 725.Subpart AA and BB.
(Source:
Amended at
15 Ill. Reg.
,
effective
SUBPART C:
CHARACTERISTICS OF
HAZARDOUS
WASTE
Section 721.120
General
a)
A solid waste, as defined in Section 721.102, which is
not excluded from regulation as a hazardous waste under
Section 721.104(b),
is a hazardous waste if it exhibits
any of the characteristics identified in this Subpart.
-(-Board Note:BOARD NOTE:
35 Ill. Adm. Code 722.111 sets
forth the generator’s responsibility to determine
whether the generator’s waste exhibits one or more
characteristics identified in this Subpart4-
b)
A hazardous waste which is identified by ~
characteristic in this Subpart, but is not listed as
a
hazardous waste
in Subpart
D,
is assigned t~eevery
USEPA Hazardous Waste Number which is applicable as set
forth in the respective characteristic in this Subpart.
This number must be used in complying with the
notification requirements of Section 3010 of the
Resource Conservation and Recovery Act and
~a-i~nall
applicable recordkeeping and reporting requirements
under 35
Ill. Adm. Code 702,
703,
722 through 725 and
728.
c)
For purposes of this Subpart,
a sample obtained using
any of the applicable sampling methods specified in
Appendix A is a representative sample within the
meaning of 35
Ill. Adm. Code 720.
-(-Board NOte:BOARD NOTE:
Since the Appendix A sampling
methods are not being formally adopted,
a person who
desires to employ an alternative sampling method is not
required to demonstrate the equivalency of the person’s
method under the procedures set forth in 35 Ill. Adm.
Code 720.121.-)-
(Source:
Amended at 15 Ill.
Reg.
,
effective
Section 721.121
Characteristic of Ignitability
a)
A solid waste exhibits the characteristic of
ignitability
if a representative sample of the waste
has any of the following properties:
121—201
53
1)
It is a liquid,
other than an aqueous solution
containing less than 24 percent alcohol by volume,
and has a flash point less than 60°C(140°F),as
determined by a Pensky-Martens Closed Cup Tester,
using the test method specified in the American
Cocicty of Testing Materials
(ACTI4)
Standard D-
93-79 or D-93 CO (incorporated by reference, see
§720.l11)ASTM D-93,
incorporated by reference in
35 Ill. Adm. Code 720.111, or a Setaflash Closed
Cup Tester,
using the test method specified in
ASTN Standard D-32283270-78 (incorporated by
reference,
see §720.111),
incorporated by
reference in 35 Ill. Adm. Code 720.111, or as
determined by an equivalent test method approved
by the Board
(*35 Ill.
Adm. Code 720.120).
2)
It is not a liquid and is capable, under standard
temperature and pressure, of causing fire through
friction, absorption of moisture or spontaneous
chemical changes and, when ignited, burns so
vigorously and persistently that it creates a
hazard.
3)
It is an ignitable compressed gas as defined in 49
CFR 173.300, incorporated by reference in 35
Ill.
Adm. Code 720.111, and as determined by the test
methods described in that regulation or equivalent
test methods approved by the Board
(*35 Ill. Adm.
Code 720.120).
4)
It is an c~idizeras defined in 49 CFR 173.15l~
incorporated by reference in 35 Ill. Adm. Code
720.111.
b)
A solid waste that exhibits the characteristic of
ignitability, but is not listed as a hazardous waste in
Subpart
D,
has the~EPA Hazardous Waste Number of DOOl.
(Source:
Amended at
15 Ill. Reg.
,
effective
Section 721.122
Characteristic of Corrosivity
a)
A solid waste exhibits the characteristic of
corrosivity if a representative sample of the waste has
either of the following properties:
1)
It is aqueous and has a pH less than or equal to 2
or greater than or equal to 12.5,
as determined by
a pH meter using either an EPA test method or an
equivalent test method
(*35 Ill.
Adm. Code
121—202
54
720.121).
The EPA test method for pH is specified
as Method 5.2 in “Test Methods for the Evaluation
of Solid Waste, Physical/Chemical Methods”
(incorporated by reference,
see §720.1I1)~
incorporated by reference in 35
Ill. Adm. Code
720.111.
2)
It
is a liquid and corrodes steel
(SAE 1020)
at a
rate greater than 6.35
nun (0.250 inch) per year at
a test temperature of 55°C(130°F)as determined
by the test method specified in NACE (National
Association of Corrosion Engineers)
Standard TM—
01-69
as standardized in “Test Methods for the
Evaluation of Solid Waste, Physical/Chemical
Methods”
(incorporated by reference,
see
§720.111),
incorporated by reference in 35 Ill.
Adm. Code 720.111, or an equivalent test method
(*35 Ill.
Adm. Code 720.121).
b)
A solid waste that exhibits the characteristic of
corrosivity
,
but is not listed as
a hazardous waste in
Subpart
D, has the EPA Hazardous Waste Number of DOO2.
(Source:
Amended at 15 Ill.
Reg.
,
effective
Section 721.123
Characteristic of Reactivity
a)
A solid waste exhibits the characteristic of reactivity
if a representative sample of the waste has any of the
following properties:
1)
It is normally unstable and readily undergoes
violent change without detonating.
2)
It reacts violently with water.
3)
It forms potentially explosive mixtures with
water.
4)
When
mixed with water,
it generates toxic gases,
vapors or fumes in a quantity sufficient to
present a danger to human health or the
environment.
5)
It
is a cyanide or sulfide bearing waste which,
when exposed to pH conditions between
2 and 12.5
can generate toxic gases, vapors or fumes in a
quantity sufficient to present a danger to human
health or the environment.
6)
It is capable of detonation or explosive reaction
121—203
55
if it is subjected to a strong initiating source
or if heated under confinement.
7)
It is readily capable of detonation or explosive
decomposition or reaction at standard temperature
and pressure.
8)
It is a forbidden explosive as defined in 49 CFR
173.51, or a Class A explosive as defined in 49
CFR 173.53 or a Class B explosive as defined in 49
CFR 173.88, incorporated by reference in 35 Ill.
Adm. Code 720.111.
b)
A solid waste that exhibits the characteristic of
reactivity
,
but is not listed as a hazardous waste in
Subpart D, has the EPA Hazardous Waste Number of D003.
(Source:
Amended at 15
Ill. Reg.
,
effective
Section 721.124
Toxicity Characteristic
a)
A solid waste exhibits the characteristic of toxicity
if, using the test methods described in Appendix B or
equivalent methods approved by the Agency under the
procedures set forth in Sections 720.120 and 720.121,
the extract from
a representative sample of the waste
contains any of the contaminants listed in the table in
subsection
(b) at a concentration equal to or greater
than the respective value given
in that table.
Where
the waste contains less than 0.5 percent filterable
solids, the waste
itself, after filtering using the
methodology outlined in Appendix B,
is considered to be
the extract for the purpose of this Section.
BOARD NOTE:
Generators are required to use the TCLP
test for the hazardous waste determination under 35
Ill. Adm. Code 722.120 as of September 25,
1990.
Provided, however, that,
as specified at 55 Fed.
Reg.
11850, March 29,
1990,
small quantity generators of 100
to 1000 kg/ month, as defined in 35 Ill. Adm. Code
721.105, may continue to use the EP toxicity test until
March 29, 1991.
The EP toxicity test is Method 1310
in
SW 846,
“Test Methods for Evaluating Solid Wastes,
Physical/Chemical Methods”, incorporated by reference
in 35 Ill. Adm. Code 720.111.
The reference to the “EP
toxicity test”
in 35 Ill. Adm. Code 808.410(b) (4)
is to
be understood as referencing the test required by this
Section.
b)
A solid waste that exhibits the characteristic of
toxicity, but
is not listed as
a hazardous waste in
121—204
56
Subpart
D,
has the USEPA Hazardous Waste Number
specified in the following table which corresponds to
the toxic contaminant causing it to be hazardous.
MAXIMUM
CONCENTRATION
OF
CONTAMINANTS
FOR
THE TOXICITY CHARACTERISTIC
USEPA
Hazardous
CAB
Regulatory
Waste No. Contaminant
Number
Note
Level(mg/L)
D004
Arsenic
7440—38—2
5.0
D005
Barium
7440—39—3
100.0
D018
Benzene
71—43—2
0.5
D006
Cadmium
7440—43—9
1.0
D019
Carbon
tetra-
56-23—5
0.5
chloride
D020
Chlordane
57—74—9
0.03
D021
Chlorobenzene
108—90—7
100.0
D022
Chloroform
67—66—3
6.0
D007
Chromium
7440—47—3
5.0
D023
o—Cresol
95—48—7
4
200.0
D024
m—Cresol
108—39—4
4
200.0
D025
p—Cresol
106—44—5
4
200.0
D026
Cresol
4
200.0
D016
2,4—D
94—75—7
10.0
D027
1,4—Dichloro—
106—46—7
7.5
benzene
D028
l,2—Dichloro—
107—06—2
0.5
ethane
D029
l,l—Dichloro—
75—35—4
0.7
ethylene
D030
2,4—Dinitro—
121—14—2
3
0.13
toluene
D0l2
Endrin
72—20—8
0.02
D031
Heptachlor (and
76—44—8
0.008
its epoxide)
D032
Hexachloro—
118—74—1
3
0.13
benzene
D033
Hexachlorobuta-
87-68—3
0.5
diene
D034
Hexachloroethane
67-72—1
3.0
D008
Lead
7439—92—1
5.0
D013
Lindane
58—89—9
0.4
D009
Mercury
7439—97—6
0.2
D014
Methoxychlor
72—43-5
10.0
D035
Methyl ethyl
78—93—3
200.0
ketone
D036
Nitrobenzene
98—95—3
2.0
D037
Pentachloro—
87—86—5
100.0
phenol
D038
Pyridine
110—86—1
3
5.0
12 1—205
57
DOlO
Selenium
7782—49—2
1.0
DOll
Silver
7440—22—4
5.0
D039
Tetrachloro—
127-18-4
0.7
ethylene
DO15
Toxaphene
8001—35-2
0.5
D040
Trichloro—
79—01—6
0.5
ethylene
D041
2,4,5—Trichloro—
95—95—4
400.0
phenol
D042
2,4,6—Trichloro—
88—06—2
2.0
phenol
D017
2,4,5—TP
93—72—1
1.0
(Silvex)
D043
Vinyl chloride
75—01—4
0.2
Notes to Table:
3
Quantitation
limit
is
greater
than
the
calculated
regulatory
level.
The
quantitation
limit
therefore
becomes
the
regulatory
level.
4
If
0—,
m—,
p—cresol
concentrations
cannot be
differentiated,
the
total
cresol
(D026)
concentration
is
used.
The
regulatory level of
total cresol
is
200.0
mg/L.
(Source:
Amended at 15 Ill.
Reg.
,
effective
SUBPART
D:
LISTS OF HAZARDOUS WASTE
Section 721.131
Hazardous Wastes From Nonspecific Sources
The following solid wastes are listed hazardous wastes from non-
specific sources unless they are excluded under 35 Ill. Adm. Code
720.120 and 720.122 and listed in Appendix I.
12 1—206
58
EPA
Hazardous
Hazard
Waste
No.
Industry
and
Hazardous
Waste
Code
FOOl
The
following
spent
halogenated
solvents
(T)
used
in
degreasing:
tetrachloroethylene,
trichloroethylene,
methylene
chloride,
1,1,
1—trichloroethane,
carbon
tetrachloride
and chlorinated fluorocarbons; all spent
solvent mixtures and blends used in
degreasing containing, before use, a total
of
ten
percent
or
more
(by
volume)
of
one
or
more
of
the
above
halogenated
solvents
or
those
solvents
listed
in
FOO2,
FOO4
or
FOO5;
and
still
bottoms
from
the
recovery
of
these
spent
solvents
and
spent
solvent
mixtures.
FOO2
The
following
spent
halogenated
solvents:
(T)
tetrachloroethylene,
methylene
chloride,
trichloroethylene,
1,1, l-trichloroethane,
chlorobenzene,
1,1,
2—trichloro—1,2,2—tri—
fluoroethane,
orthodichlorobenzene,
tn—
chlorofluoromethane
and
1,1,
2—tnichloro—
ethane; all spent solvent mixtures and
blends containing, before use, a total of
ten percent or more
(by volume)
of one or
more of the above halogenated solvents or
those solvents listed in FOOl, FOO4 or FOOS;
and still bottoms from the recovery of these
spent solvents and spent solvent mixtures.
F003
The following spent non-halogenated
(I)
solvents:
xylene,
acetone, ethyl acetate,
ethyl benzene, ethyl ether, methyl isobutyl
ketone, n-butyl alcohol, cyclohexanone and
methanol; all spent solvent mixtures and
blends containing, before use, only the
above spent non—halogenated solvents; and
all spent solvent mixtures and blends
containing, before use, one or more of the
above non—halogenated solvents and a total
of ten percent or more
(by volume)
of one or
more of those solvents listed in FOOl,
F002,
FOO4 or F005; and still bottoms from the
recovery of these spent solvents and spent
solvent mixtures.
12 1—207
59
F004
The
following
spent
non-halogenated
(T)
solvents:
cresols
and
cresylic
acid and
nitrobenzene;
all
spent
solvent
mixtures
and
blends
containing,
before
use,
a
total
of
ten percent or more
(by volume) of one or
more of the above non—halogenated solvents
or those solvents listed in FOOl,
F002 or
FOO5; and still bottoms from the recovery of
these spent solvents and spent solvent
mixtures.
F005
The following spent non-halogenated
(I,
T)
solvents:
toluene, methyl ethyl ketone,
carbon disulfide,
isobutanol, pynidine,
benzene, 2—ethoxyethanol and 2—nitropropane;
all spent solvent mixtures and blends,
containing,
before use,
a total of ten
percent or more (by volume) of one or more
of
the
above
non—halogenated
solvents
or
those
solvents
listed
in
FOOl,
FOO2
or
FOO4;
and
still
bottoms
from
the
recovery
of
these
spent
solvents
and
spent solvent mixtures.
F006
Wastewater
treatment
sludges
from
(T)
electroplating
operations
except
from
the
following
processes:
(1)
sulfuric
acid
anodizing
of
aluminum;
(2)
tin
plating
on
carbon
steel;
(3) zinc plating (segregated
basis)
on
carbon steel;
(4)
aluminum
or
zinc—aluminum plating on carbon steel;
(5)
cleaning/stripping associated with tin,
zinc
and aluminum plating on carbon steel; and
(6)
chemical etching and milling of
aluminum.
FO19
See Below
F007
Spent cyanide plating bath solutions from
(R,
T)
electroplating operations.
F008
Plating bath residues from the bottom of
(R,
T)
plating baths from electroplating operations
where cyanides are used in the process.
F009
Spent stripping and cleaning bath solutions
(R,
T)
from electroplating operations where
cyanides are used in the process.
FO1O
Quenching bath residues from oil baths from
(R,
T)
metal heat treating operations where
cyanides are used in the process.
121—208
•60
FOll
Spent
cyanide
solutions
from
salt
bath
pot
(R,
T)
cleaning
from
metal
heat
treating
operations.
FO12
Quenching wastewater treatment sludges from
(T)
metal heat treating operations where
cyanides are used in the process.
FO19
Wastewater treatment sludges from the
(T)
chemical conversion coating of aluminum
except from zirconium phosphating in
aluminum can washing when such phosphating
is an exclusive conversion coating process.
F020
Wastes
(except wastewater and spent carbon
(H)
from hydrogen chloride purification)
from
the production or manufacturing use
(as a
reactant, chemical intermediate or component
ma
formulating process)
of tn— or tetra—
chlorophenol, or of intermediates used to
produce their pesticide derivatives.
(This
listing does not include wastes from the
production of hexachlorophene from highly
purified 2,4,5-trichlorophenol.)
F021
Wastes
(except wastewater and spent carbon
(H)
from hydrogen chloride purification)
from
the production or manufacturing use
(as a
reactant, chemical intermediate or component
in a formulating process) of pentachloro—
phenol, or of intermediates used to produce
its derivatives.
F022
Wastes
(except wastewater and spent carbon
(H)
from hydrogen chloride purification) from
the manufacturing use
(as a reactant,
chemical intermediate or component in a
formulating process)
of tetra—, penta— or
hexachlorobenzenes
under
alkaline
conditions.
F023
Wastes
(except wastewater and spent carbon
(H)
from hydrogen chloride purification)
from
the production of materials on equipment
previously used for the production or
manufacturing use
(as a reactant, chemical
intermediate or component in
a formulating
process)
of tn— and tetrachlorophenols.
(This listing does not include wastes from
equipment used only for the production or
use of hexachlorophene from highly purified
2,4,5- trichlorophenol.
121—209
61
F024
Process wastes including but not limited to,
(T)
distillation residues, heavy ends,
tars, and
reactor cleanout wastes, from the production
of certain chlorinated aliphatic
hydrocarbons by free radical catalyzed
processes.
These chlorinated aliphatic
hydrocarbons are those having carbon chain
lengths ranging from one to and including
five, with varying amounts and positions of
chlorine substitution.
(This listing does
not include wastewaters, wastewater
treatment sludges, spent catalysts and
wastes listed in this Section or Section
721.132.)
FO25
Condensed light ends, spent filters and
(T)
filter aids, and spent dessicant wastes from
the production of certain chlorinated
aliphatic hydrocarbons by free radical
catalyzed processes.
These chlorinated
aliphatic hydrocarbons are those having
carbon chain lengths ranging from one to and
including five, with varying amounts and
positions of chlorine substitution.
F026
Wastes (except wastewater and spent carbon
(H)
from hydrogen chloride purification)
from
the production of materials on equipment
previously used for the manufacturing use
(as a reactant, chemical intermediate or
component in a formulating process) of
tetra—, penta— or hexachlorobenzene under
alkaline conditions.
FO27
Discarded unused formulations containing
(H)
tn—, tetra— or pentachlorophenol or
discarded unused formulations containing
compounds derived from these chlorophenols.
(This listing does not include formulations
containing hexachlorophene synthesized from
prepurified 2,4,5-trichlorophenol as the
sole component).
FO28
Residues resulting from the incineration or
(T)
thermal treatment of soil contaminated with
hazardous waste numbers FO2O,
FO21,
FO22,
FO23,
F026 and F027.
121—210
62
FO39
Leachate resulting from the treatment,
storage or disposal of wastes classified by
more than one waste code under Subpart D,
or
from a mixture of wastes classified under
Subparts C and D.
(Leachate resulting from
the management of one or more of the
following USEPA hazardous wastes and no
other hazardous wastes retains its hazardous
waste code(s):
FO2O, FO21,
F022, FO23,
F026, F027 or FO28.)
(Board Note:BOARD NOTE:
The primary hazardous properties of
these materials have been indicated by the letters T (Toxicity),
R (Reactivity),
I
(Ignitability),
and C (Corrosivity).
The
letter H indicates Acute Hazardous Waste.)-
(Source:
Amended at 15
Ill. Reg.
,
effective
Section 721.132
Hazardous Waste from Specific Sources
The following solid wastes are listed hazardous wastes from
specific sources unless they are excluded under 35 Ill. Adm. Code
720.120 and 720.122 and listed in Appendix I.
EPA
Hazardous
Hazard
Waste No.
Industry and Hazardous Waste
Code
Wood Preservation:
KOOl
Bottom sediment sludge from the treatment of
(T)
wastewaters from wood preserving processes
that use creosote and/or pentachlorophenol.
Inorganic Pigments:
K002
Wastewater treatment sludge from the
(T)
production of chrome yellow and orange
pigments.
KOO3
Wastewater treatment sludge from the
(T)
production of molybdate orange pigments.
KOO4
Wastewater treatment sludge from the
(T)
production of zinc yellow pigments.
K005
Wastewater treatment sludge from the
(T)
production of chrome green pigments.
121—211
63
K006
Wastewater
treatment
sludge
from
the
(T)
production of chrome oxide green pigments
(anhydrous
and
hydrated).
K007
Wastewater
treatment
sludge
from
the
(T)
production
of
iron
blue
pigments.
K008
Oven
residue
from
the
production
of
chrome
(T)
oxide
green
pigments.
Organic
Chemicals:
KOO9
Distillation
bottoms
from
the
production
of
(T)
acetaldehyde
from
ethylene.
KO1O
Distillation side cuts from the production
CT)
of
acetaldehyde
from
ethylene.
KOll
Bottom
stream
from
the
wastewater
stripper
(R,T)
in
the
production
of
acrylonitnile.
KO13
Bottom stream from the acetronitnile column
(T)
in the production of acrylonitnile.
K0l4
Bottoms from the acetontnile purification
(T)
column in the production of acrylonitnile.
KOlS
Still bottoms from the distillation of
(T)
benzyl chloride.
KO16
Heavy ends or distillation residues from the
(T)
production of carbon tetrachlonide.
KO17
Heavy ends
(still bottoms) from the
(T)
purification column in the production of
epichlorohydrin.
K018
Heavy ends from the fractionation column in
(T)
ethyl chloride production.
K0l9
Heavy ends from the distillation of ethylene
(T)
dichlonide in ethylene dichlonide
production.
KO2O
Heavy ends from the distillation of vinyl
(T)
chloride in vinyl chloride monomer
production.
K02l
Aqueous spent antimony catalyst waste from
(T)
fluoromethanes production.
121—121
64
K022
Distillation
bottom
tars
from
the
production
(T)
of phenol/acetone from cumene.
K023
Distillation light ends from the production
(T)
of
phthalic
anhydnide
from
naphthalene.
KO24
Distillation bottoms from the production of
(T)
phthalic anhydnide from naphthalene.
KO93
Distillation light ends from the production
(T)
of phthalic anhydnide from ortho-xylene.
K094
Distillation bottoms from the production of
(T)
phthalic anhydride from ortho-xylene.
K025
Distillation bottoms from the production of
(T)
nitrobenzene by the nitration of benzene.
KO26
Stripping still tails from the production of
(T)
methyl ethyl pynidines.
KO27
Centrifuge and distillation residues from
(R,T)
toluene diisocyanate production.
KO28
Spent catalyst from the hydrochloninator
(T)
reactor in the production of 1,1,1-tn-
chloroethane.
KO29
Waste from the product stream stripper in
(T)
the production of 1,1,l-tnichloroethane.
KO95
Distillation bottoms from the production of
(T)
1,1,l-tnichloroethane.
K096
Heavy ends from the heavy ends column from
(T)
the production of 1,1,l-tnichloroethane.
K030
Column bottoms or heavy ends from the
(T)
combined production of trichloroethylene and
perchloroethylene.
KO83
Distillation bottoms from aniline
(T)
production.
K103
Process residues from aniline extraction
(T)
from the production of aniline.
K104
Combined wastewater streams generated ‘from
(T)
nitrobenzene/aniline production.
KOB5
Distillation or fractionation column bottoms
(T)
from the production of chlorobenzenes.
12 1—213
65
K1O5
Separated aqueous stream from the reactor
(T)
product washing step in the production of
chlorobenzenes.
Kl07
Column bottoms from product separation from
(C,T)
the production of 1,1-dimethylhydrazine
(UDMH)
from carboxilic acid hydrazides.
K108
Condensed column overheads from product
(I,T)
separation and condensed reactor vent gases
from the production of i,i-dimethvlhydrazine
(UDMH)
from carboxilic acid hydrazides.
K1O9
Spent filter cartridges from the product
fl~j
purification from the production of 1,1-di-
methylhydrazine
(UDMH)
from carboxilic acid
hydrazides.
KllO
Condensed column overheads from intermediate
jfl
separation from the production of 1,1-di-
methylhydrazine
(UDMH)
from carboxilic acid
hydraz ides.
Kill
Product wastewaters from the production of
(C,T)
dinitrotoluene via nitration of toluene.
Kll2
Reaction by-product water from the drying
(T)
column in the production of toluenediamine
via hydrogenation of dinitrotoluene.
K113
Condensed
liqu,td
light ends from the
(T)
purification
of
toluenediamine
in
the
production of toluenediamine via
hydrogenation of dinitroluene.
1(114
Vicinals from the purification of toluene-
(T)
diamine in the production of toluenediamine
via hydrogenation of dinitrotolune.
Kl15
Heavy ends from the purification of
(T)
toluenediamine in the production of
toluenediamine via hydrogenation of di—
nitrotoluene.
Kl16
Organic condensate from the solvent recovery
(T)
column in the production of toluene di—
isocyanate via phosgenation of toluene’di—
amine.
121—214
66
K117
Wastewater from the reactor vent gas
(T)
scrubber
in
the
production
of
ethylene
di-
bromide via bromination of ethene.
K118
Spent adsorbent solids from purification of
(T)
ethylene
dibnomide
in
the
production
of
ethylene
dibromide
via
bromination
of
ethene.
K136
Still
bottoms
from
the
purification
of
(T)
ethylene dibromide in the production of
ethylene dibromide via broinination of
ethene
*
Inorganic Chemicals:
KO71
Brine
purification
muds
from
the
mercury
(T)
cell process in chlorine production, where
separately prepunified brine is not used.
K073
Chlorinated hydrocarbon waste from the
(T)
purification step of the diaphragm cell
process using graphite anodes in chlorine
production.
K1O6
Wastewater
treatment
sludge
from
the
mercury
(T)
cell process in chlorine production.
Pesticides:
1(031
By-product salts generated in the production
(T)
of
MSMA
and cacodylic acid.
1(032
Wastewater treatment sludge from the
(T)
production of chlordane.
1(033
Wastewater
and
scrub
water
from
the
(T)
chlorination of cyclopentadiene in the
production of chlordane.
K034
Filter solids from the filtration of hexa-
(T)
chlorocyclopentadiene in the production of
chlordane.
K097
Vacuum stripper discharge from the chiordane
(T)
chlorinator in the production of chlordane.
K035
Wastewater treatment sludges generated in
(T)
the production of creosote.
12 1—2 15
67
KO36
Still bottoms from toluene reclamation
(T)
distillation in the production of di-
sulfoton.
1(037
Wastewater treatment sludges from the
(T)
production of disulfoton.
1(038
Wastewater from the washing and stripping of
(T)
phorate production.
1(039
Filter cake from the filtration of diethyl-
(T)
phosphorodithioic acid in the production of
phorate.
1(040
Wastewater
treatment
sludge
from
the
(T)
production
of
phorate.
1(041
Wastewater
treatment
sludge
from
the
(T)
production
of
toxaphene.
1(098
Untreated
process
wastewater from the
(T)
production
of
toxaphene.
1(042
Heavy
ends
or
distillation residues from the
(T)
distillation of tetrachlorobenzene in the
production of 2,4,5-T.
KO43
2,6-Dichlorophenol waste from the production
(T)
of 2,4—D.
1(099
Untreated wastewater from the production of
(T)
2,
4—D.
1(123
Process wastewater (including supernates,
(T)
filtrates and washwaters)
from the
production of ethylenebisdithiocarbamic acid
and
its
salts.
1(124
Reactor
vent
scrubber
water
from
the
(C,T)
production
of
ethylenebisdithiocarbamic
acid
and
its
salts.
K125
Filtration,
evaporation
and
centnifugation
(T)
solids from the production of ethylenebis-
dithiocarbamic acid and its salts.
K126
Baghouse dust and floor sweepings in milling
(T)
and packaging operations from the production
or formulation of ethylenebisdithiocarbamic
acid and its salts.
121—2 16
68
K13l
Wastewater from the reactor and spent
(C,T)
sulfuric acid from the acid dryer from the
production
of methyl bromide.
1(132
Spent
absorbent
and
wastewater
separator
(T)
solids
from
the
production
of
methyl
bromide.
Explosives:
1(044
Wastewater
treatment
sludges
from
the
(R)
manufacturing
and
processing
of
explosives.
1(045
Spent
carbon
from
the
treatment
of
(R)
wastewaten
containing
explosives.
K046
Wastewater treatment sludges from the
(T)
manufacturing, formulation and loading of
lead-based initiating compounds.
1(047
Pink/red
water
from
TNT
operations.
(R)
Petroleum
Refining:
1(048
Dissolved
air
flotation
(DAF)
float
from
the
(T)
petroleum
refining
industry.
KO49
Slop
oil
emulsion
solids from the petroleum
(T)
refining industry.
1(050
Heat exchanger bundle cleaning sludge from
(T)
the petroleum refining industry.
1(051
API separator sludge from the petroleum
(T)
refining industry.
KO52
Tank bottoms (leaded)
from the petroleum
(T)
refining industry.
Iron and Steel:
K06l
Emission control dust/sludge from the
(T)
primary production of steel
in electric
furnaces.
1(062
Spent pickle liquor generated by steel
(C,T)
finishing operations of facilities within
the iron and steel industry (SIC Codes~331
and 332)
(as defined in 35 Ill. Adm. Code
720.110).
12 1—217
69
Primary
Copper:
1(064
Acid
plant
blowdown
slurry
or
sludge
(T)
resulting
from
the
thickening
of
blowdown
slurry
from
primary
copper
production.
Primary
Lead:
1(065
Surface
impoundment
solids
contained
in
and
(T)
dredged
from
surface
impoundments
at
primary
lead
smelting
facilities.
Primary
Zinc:
K066
After
June
30,
1990,
sludge
from
treatment
(T)
of
process
wastewater
or
acid
plant
blowdown
from
primary
zinc
production.
Primary
Aluminum:
KO88
Spent
potliners
from
primary
aluminum
(T)
reduction.
Ferroalloys:
1(090
Emission
control
dust
or
sludge
from
(T)
ferrochromiumsil
icon
production.
KO91
Emission
control
dust
or
sludge
from
(T)
ferrochromium production.
Secondary Lead:
1(069
Emission control dust/sludge from secondary
(T)
lead
smelting.
1(100
Waste leaching solution from acid leaching
(T)
of
emission
control
dust/sludge
from
secondary lead smelting.
Veterinary Pharmaceuticals:
1(084
Wastewater
treatment
sludges
generated
(T)
during the production of veterinary
pharmaceuticals from arsenic or organo—
arsenic compounds.
1(101
Distillation tar residues from the
(T)
distillation of aniline-based compounds in
the production of veterinary pharmaceuticals
from
arsenic
or organoansenic compounds.
12 1—218
70
1(102
Residue from use of activated carbon for
(T)
decolonization in the production of
veterinary pharmaceuticals from arsenic or
organo—arsenic
compounds.
Ink
Formulation:
1(086
Solvent washes and sludges, caustic washes
CT)
and sludges, or water washes and sludges
from cleaning tubs and equipment used in the
formulation of ink from pigments, driers,
soaps and stabilizers containing chromium
and lead.
Coking:
KO6O.
Ammonia still lime sludge from coking
(T)
operations.
1(087
Decanter tank tar sludge from coking
(T)
operations.
(Source:
Amended at 15 Ill.
Reg.
,
effective
Section 721.133
Discarded Commercial Chemical Products, Off-
Specification Species, Container Residues and
Spill Residues Thereof
The
following
materials
or
items
are
hazardous
wastes
if
and
when
they are discarded or intended to be discarded as described in
Section 721.102(a) (2) (A), when they are mixed with waste oil or
used
oil
on
other
material
and
applied
to
the
land
for
dust
suppression
or
road
treatment,
when
they
are
otherwise
applied
to
the
land
in
lieu
of
their
original
intended
use
or
when
they
are
contained in products that are applied to land in lieu of their
original intended use,
or when,
in lieu of their original
intended use, they are produced for use as
(or as a component of)
a
fuel,
distributed
for
use
as
a
fuel,
or
burned
as
a
fuel.
a)
Any commercial chemical product, or manufacturing
chemical intermediate having the generic name listed in
subsections
(e)
or
(f).
b)
Any off-specification commercial chemical product or
manufacturing chemical intermediate which,
if it met
specifications,
would
have
the
generic
‘name
listed
in
subsections
(e)
on
(f).
c)
Any
residue
remaining
in
a
container
or
inner
liner
removed
from
a
container
that
has
held
any
commercial
121—219
71
chemical product or manufacturing chemical intermediate
having the generic name listed in subsection (e)~
jfl,
unless the container is empty as defined in
Section 721.107(b) (3).
BOARD NOTE:
Unless the residue is being beneficially
used or reused, or legitimately recycled or reclaimed,
or being accumulated, stored, transported or treated
prior to such use,
reuse, recycling or reclamation, the
Board considers the residue to be intended for discard,
and thus a hazardous waste.
An example of a legitimate
reuse of the residue would be where the residue remains
in the container and the container is used to hold the
same commercial chemical product or manufacturing
chemical intermediate it previously held.
An example
of the discard of the residue would be where the drum
is sent to a drum reconditioner who reconditions the
drum but discards the residue.
d)
Any residue or contaminated soil, water or other debris
resulting from the cleanup of a spill,
into or on any
land
or
water
of
any
commercial
chemical
product
or
manufacturing
chemical
intermediate
having
the
generic
name
listed
in
subsection
(e)
or.
(f),
or
any
residue
or
contaminated
soil,
water
or
other
debris
resulting
from
the
cleanup
of
a
spill,
into
or
on
any
land
on
water,
of
any
off—specification
chemical
product
or
manufacturing
chemical
intermediate
which,
if
it
met
specifications,
would
have
the
generic
name
listed
in
subsection
(e)
or
(f).
BOARD
NOTE:
Th~_
phrase
“commercial
chemical
product
or
manufacturing
chemical
intermediate
having the generic
name
listed
in
...“
refers
to
a
chemical
substance
which
is
manufactured
or
formulated
for
commercial
or
manufacturing
use
which
consists
of
the
commercially
pure
grade
of
the
chemical,
any
technical
grades of the
chemical
that
are
produced
or
marketed,
and
all
formulations
in
which
the
chemical
is
the
sole
active
ingredient.
It
does
not
refer
to
a
material,
such
as
a
manufacturing
process
waste,
that
contains
any
of
the
substances listed in subsections
(e) or
(f).
Where
a
manufacturing process waste is deemed to be a hazardous
waste because it contains a substance listed in
subsections
(e) or
(f), such waste will be listed in
either Sections 721.131 or 721.132 or will be
identified as a hazardous waste by the characteristics
set forth in Subpart C.
e)
The commercial chemical products, manufacturing
chemical intermediates or off—specification commercial
chemical products or manufacturing chemical
12 1—220
72
intermediates referred to in subsections
(a) through
(d), are identified as acute hazardous waste
(H) and
are
subject
to
the
small
quantity
exclusion
defined
in
Section 721.105(e).
These wastes and their
corresponding EPA Hazardous Waste Numbers are:
BOARD NOTE:
For the convenience of the regulated
community the primary hazardous properties of these
materials have been indicated by the letters T
(Toxicity), and R (Reactivity).
Absence of a letter
indicates that the compound only is listed for acute
toxicity.
Chemical
Hazardous Abstracts
Waste No. No.
Substance
P023
107-20-0
Acetaldehyde, chloro-
P002
591-08-2
Acetamide, N-(aminothioxomethyl)
P057
640-19-7
Acetamide,
2—fluoro-
P058
62-74—8
Acetic acid,
fluoro—, sodium salt
P002
591-08-2
1-Acetyl—2-thiourea
P003
107—02—8
Acrolein
P070
116—06—3
Aldicarb
P004
309—00—2
Aldnin
P005
107—18—6
Allyl alcohol
P006
20859—73-8
Aluminum
phosphide
(R,T)
P007
2763—96—4
5—(Aminomethyl)—3—isoxazolol
P008
504—24-5
4—Aminopynidine
P009
131-74-8
Ammonium picnate
(R)
P119
7803-55-6
Ammoniuin vanadate
P099
506-61-6
Angentate(l-), bis(cyano-C)-,
potassium
POlO
7778—39—4
Arsenic acid H3A5O4
P012
1327—53—3
Arsenic oxide As2O3
P011
1303—28—2
Arsenic oxide A52O5
POll
1303-28—2
Arsenic pentoxide
P012
1327—53—3
Arsenic
tnioxide
P038
692-42—2
Arsine, diethyl—
P036
696-28-6
Ansonous dichlonide,
phenyl—
P054
151—56—4
Azinidine
P067
75—55—8
Azinidine,
2—methyl
P013
542-62—1
Barium
cyanide
P024
106—47-8
Benzenamine,
4-chloro-
P077
100—01-6
Benzenamine, 4—nitro-
P028
100—44-7
Benzene,
(chloromethyl)—
P042
51—43—4
1,2—Benzenediol,
4—1—hydroxy—2—
(methylamino)
ethyl
-,
(R)
-
P046
122-09-8
Benzeneethanamine,
alpha,
alpha—
dimethyl-
P014
108—98—5
Benzenethiol
121—221
73
P001
P81-81-2
2H-l-Benzopyran-2-one,
4-hydroxy-
3-(3-oxo-1-phenylbutyl)-,
and
salts,
when
present
at
concentrations
greater
than
0.3
P028
100—44-7
Benzyl
chloride
P015
7440—41—7
Beryllium
P017
598—31-2
Bromoacetone
P018
357—57—3
Brucine
P045
3 9196—18—6
2—Butanone, 3, 3—dimethyl—1—
(methylthio)
-,
O-methylamino)
-
carbonyl
oxime
P021
592—01-8
Calcium
cyanide
P021
592-01-8
Calcium
cyanide
Ca(CN)2
P022
75-15-0
Carbon
disulfide
P095
75-44-5
Carbonic
dichloride
P023
107-20-0
Chloroacetaldehyde
P024
106—47—8
p—Chloroaniline
P026
5344-82-1
1-(o-Chlorophenyl)thiourea
P027
542-76-7
3-Chloropropionitnile
P029
544-92-3
Copper
cyanide
P029
544-92-3
Copper
cyanide
CuCN
P030
.
Cyanides
(soluble
cyanide
salts),
not
otherwise
specified
P031
460—19—5
Cyanogen
P033
506—77—4
Cyanogen
chloride
P033
506-77—4
Cyanogen
chloride
CNC1
P034
13 1-89—5
2—Cyclohexyl-4,
6-dinitnophenol
P016
542-88-1
Dichlonomethyl ether
P036
696-28—6
Dichlorophenylarsine
P037
60—57—1
Dieldnin
P038
692—42—2
Diethylarsine
P041
311-45-5
Diethyl-p-nitrophenyl phosphate
P040
297-97—2
0,0-Diethyl
0—pyrazinyl
phosphorothioate
P043
55-91-4
Diisopropylfluorophosphate
(DFP)
P004
309-00-2
1,4,5,8-Diinethanonaphthalene,
l,2,3,4,lO,10—hexachloro—
1,4,4a,
5,8,8a-hexahydro-,
(lalpha,
4alpha,
4abeta,
Salpha,
8alpha,
8abeta)-
P060
465—73—6
1,4,5,8-Di-methanonaphthalene,
1,2,3,4,10,
1O—hexachlono—
1, 4,4a,
5,8,8a—hexahydro—,
(lalpha,
4alpha,
4abeta,
Sbeta,
8beta,
8abeta)—
P037
60—57—1
2,7:3,6—Dimethanonaphth2,3—b—
oxirene,
3,4,5,6,9,9—hexachloro—
1a,2,2a,3,6,6a,7,-7a—octahydro—,
(laalpha,
2beta, 2aalpha,
3beta,
6beta,
6aalpha, 7beta, 7aalpha)-
121—222
P051
P72—20—8
2,7:3,6—Dimethanonaphth2,3—b—
oxirene,
3,4,5,6,9,9—hexachloro—
la,
2, 2a, 3,6,
6a, 7, 7a—octahydro—,
(laalpha,
2beta,
2abeta,
3alpha,
6alpha,
6abeta,
7beta,
laalpha)-
and
metabolites
P044
60-51-5
Dimethoate
P046
122-09-8
alpha,
alpha-Dimethylphenethyl-
amine
P047
534-52—1
4,6—Dinitro—o—cresol
and
salts
P048
51-28-5
2,4—Dinitrophenol
P020
88—85—7
Dinoseb
P085
152-16-9
Diphosphoramide,
octamethyl-
P111
107-49-3
Diphosphonic
acid,
tetraethyl
ester
P039
298—04—4
Disulfoton
P049
541-53-7
Dithiobiuret
P050
115—29—7
Endosulfan
P088
145-73-3
Endothall
P051
72—20-8
Endnin
P051
72-20-8
Endnin,
and
metabolites
P042
51-43-4
Epinephnine
P031
460-19-5
Ethanedinitnile
P066
16752-77—5
Ethanimidothioic
acid,
N-
((methylamino)carbonyl)oxy—,
methyl ester
P101
107-12-0
Ethyl cyanide
P054
151-56-4
Ethylenimine
P097
52-85—7
Famphur
P056
7782—41—4
Fluorine
P057
640-19—7
Fluoroacetamide
P058
62-74-8
Fluoroacetic acid,
sodium salt
P065
628-86—4
Fulminic acid,
mercury
(2+) salt
(R,T)
P059
76-44-8
Heptachlor
P062
757-58-4
Hexaethyl
tetraphosphate
P116
79-19-6
Hydrazinecarbothioamide
P068
60-34-4
Hydrazine, methyl—
P063
74-90-8
Hydrocyanic acid
P063
74-90-8
Hydrogen
cyanide
P096
7803-51-2
Hydrogen phosphide
P060
465—73—6
Isodnin
P007
2763—96—4
3(2H)—Isoxazolone,
5—(amino—
methyl)
-
P092
62-38-4
Mercury,
(acetato-O)phenyl-
P065
628-86-4
Mencury
fulminate
(R,T)
P082
62-75-9
Methanamine,
N-methyl-N-nitroso—
P064
624-83-9
Methane,
isocyan&to-
P016
542-88—1
Methane, oxybischlono-
P112
509-14-8
Methane,
tetranitro-
(R)
P118
75—70-7
Methanethiol,
tnichloro-
121—223
75
P050
115—29—7
6, 9—Methano—2
,
4,3—benzodi—
oxathiepen,
6,7,8,9,10,10-hexa—
chloro-l,
5, 5a, 6,9, 9a-hexahydro—,
3-oxide
P059
7 6—44—8
4, 7—Methano-1H—indene,
1,4,
5, 6, 7,8,
8—heptachloro—
3a, 4,7,
7a-tetrahydro-
P066
16752—77—5
Methomyl
P068
60-34-4
Methyl
hydrazine
P064
624-83-9
Methyl
isocyanate
P069
75—86-5
2—Methyllactonitrile
P071
298-00-0
Methyl
parathion
P072
86—88-4
alpha-Naphthylthiourea
P073
13463—39—3
Nickel
carbonyl
P073
13463—39—3
Nickel
carbonyl
Ni(CO)4,
(T—4)—
P074
557-19-7
Nickel
cyanide
P074
557—19—7
Nickel
cyanide
Ni(CN)2
P075
54-11—5
Nicotine,
and
salts
P076
10102—43—9
Nitric
oxide
P077
100-01-6
p—Nitroaniline
P078
10102—44—0
Nitrogen
dioxide
P076
10102-43-9
Nitrogen
oxide
NO
P078
10102—44—0
Nitrogen
oxide
NO2
P081
55-63—0
Nitroglycerine
(R)
P082
62-75-9
N-Nitrosodimethylamine
P084
4549-40-0
N-Nitrosomethylvinylamine
P085
152 -16-9
Octamethylpyrophosphonamide
P087
20816—12—0
Osmium
oxide
0s04,
(T—4)—
P087
20816-12-0
Osmium
tetroxide
P088
145—73—3
7—Oxabicyclo2.2.lheptane—2,3—
dicarboxylic
acid
P089
56-38-2
Parathion
P034
131-89-5
Phenol,
2-cyclohexyl-4,
6—dinitro-
P048
51—28—5
Phenol, 2,4—dinitro—
P047
P534—52-1
Phenol,
2-inethyl—4,
6-dinitro—,
and
salts
P020
88—85—7
Phenol,
2—(1—methylpropyl)-4,6—
dinitro-
P009
131-74-8
Phenol, 2,4,6—trinitro—, ammonium
salt
(R)
P092
62-38-4
Phenylmercury acetate
P093
103-85-5
Phenylthiourea
P094
298—02-2
Phorate
P095
75-44—5
Phosgene
P096
7803—51—2
Phosphine
P041
311-45-5
Phosphoric
acid,
diethyl
4-
nitrophenyl
ester
P039
298-04-4
Phosphorodithioic
acid,
O,O-di-
ethyl
S-2-
(ethylthio)
ethyl
ester
P094
298-02-2
Phosphorodithioic
acid,
O,O-di—
ethyl
S-(ethylthio)methyl)
ester
121—224
76
P044
60-51—5
Phosphorodithioic
acid,
0,0-di--
methyl
S-(2-(methylamirio)
-2-
oxoethyl
)
ester
P043
55-91-4
Phosphonofluonidic
acid,
bis(1-
methylethyl)
ester
P089
56-38-2
Phosphorothioic
acid,
O,O-diethyl
O-(4-nitrophenyl)
ester
P040
297-97-2
Phosphorothioic
acid,
0,0-diethyl
O-pyrazinyl
ester
P097
52-85-7
Phosphorothioic
acid,
O-4-(di-
methylamino)
sulfonyl)
)phenyl)
0, 0-dimethyl
ester
P071
298-00-0
Phosphorothioic
acid,
0,0—di-
methyl
O-(4-nitrophenyl)
ester
P110
78-00-2
Plumbane,
tetraethyl-
P098
151-50-8
Potassium
cyanide
P098
151-50-8
Potassium
cyanide
KCN
P099
506-61-6
Potassium
silver
cyanide
P070
116-06—3
Propanal,
2—methyl—2—(methyl—
thio)-, O-~(methylamino)-
carbonyl
oxime
P101
107—12—0
Propanenitnile
P027
542—76—7
Propanenitrile,
3—chloro-
P069
75-86-5
Propanenitnile,
2-hydroxy-2-
methyl
-
P081
55-63-0
1, 2,3—Propanetniol,
tninitrate-
(R)
P017
598-31-2
2-Propanone,
1—bromo—
P102
107-19-7
Propargyl
alcohol
P003
107-02-8
2—Propenal
P005
107—18—6
2—Propen—1—ol
P067
75—55—8
1,2—Propylenimine
P102
107—19—7
2—Propyn—1—ol
P008
504—24-5
4—Pynidinamine
P075
P54—11—S
Pynidine, 3—(1—methyl-2—
pyrrolidinyl)—,
(5)- and salts
P114
12039—52—0
Selenious
acid,
dithallium
(1+)
salt
P103
630-10-4
Selenourea
P104
506-64-9
Silver cyanide
P104
506-64-9
Silver cyanide AgCN
P105
26628—22—8
Sodium azide
P106
143-33-9
Sodium
cyanide
P106
143-33-9
Sodium
cyanide
NaCN
P108
P57-24-9
Strychnidin-lO-one,
and
salts
P018
357—57—3
Strychnidin—lO—one, 2,3—di—
methoxy-
P108
P57—24-9
Strychnine and salts
P115
7446—18—6
Sulfuric acid, dithallium (1+)
salt
P109
3689-24-5
Tetraethyldithiopyrophosphate
P110
78-00-2
Tetraethyl lead
12 1—225
77
P111
107-49-3
Tetraethylpyrophosphate
P112
509-14—8
Tetranitromethane
(R)
P062
757-58—4
Tetraphosphonic
acid,
hexaethyl
ester
P113
1314—32—5
Thallic
oxide
P113
1314—32—5
Thallium
oxide
Tl203
P114
12039—52—0
Thallium
(I)
selenite
P115
7446—18—6
Thallium
(I)
sulfate
P109
3689-24-5
Thiodiphosphonic
acid,
tetraethyl
ester
P045
39196—18—4
Thiofanox
P049
541-53—7
Thioimidodicarbonic
diamide
(H~N)C(S)
32
P014
108-98-5
Thiophenol
P116
79-19-6
Thiosemicarbazide
P026
5344-82-1
Thiourea,
(2-chiorophenyl)-
P072
86-88-4
Thiourea,
1-naphthalenyl-
P093
103-85-5
Thiourea,
phenyl—
P123
8001-35—2
Toxaphene
P118
75-70-7
Tnichloromethanethiol
P119
7803-55—6
Vanadic
acid,
animonium
salt
P120
1314-62-1
Vanadium
oxide
V205
P120
1314-62-1
Vanadium
pentoxide
P084
4549-40-0
Vinylamine, N—methyl—N—nitroso-
POOl
P81-81-2
Warfarin,
and
salts,
when
present
at
concentrations
greater
than
0.3.
P121
557-21—1
Zinc
cyanide
P121
557—21—1
Zinc
cyanide
Zn(CN)2
P122
1314—84—7
Zinc
phosphide
Zn3P2,
when
present
at
concentrations
greater
than
10
(R,T)
f)
The
commercial
chemical
products,
manufacturing
chemical
intermediates
or
off—specification
commercial
chemical
products
referred
to
in
subsections
(a)
through
(d),
are
identified as toxic wastes
(T)
unless
otherwise
designated
and
are
subject
to
the
small
quantity
exclusion
defined
in
Section
721.105(a)
and
(g).
These
wastes
and
their
corresponding
EPA
Hazardous
Waste
Numbers
are:
BOARD
NOTE:
For
the
convenience of the regulated
community,
the
primary
hazardous
properties
of
these
materials
have
been
indicated
by
the
letters
T
(Toxicity),
R
(Reactivity),
I
(Ignitability)
and
C
(Corrosivity).
Absence of a letter indicates that the
compound is only listed for toxicity.
12 1—226
78
Chemical
Hazardous
Abstracts
Waste
No.
No.
Substance
UO01
75—07-0
Acetaldehyde
(I)
U034
75—87-6
Acetaldehyde,
trichloro-
U187
62-44-2
Acetamide,
N-(4-ethoxyphenyl)-
U005
53-96-3
Acetamide,
N-9H-fluoren-2-yl-
U240
P
94-75-7
Acetic
acid,
(2,4—dichloro-
phenoxy)—,
salts
and
esters
U112
141-78-6
Acetic
acid,
ethyl
ester
(I)
U144
301-04-2
Acetic
acid,
lead
(2+)
salt
U2l4
563—68-8
Acetic
acid,
thallium
(1+)
salt
See
F027
93—76—5
Acetic
acid,
(2,4,5-tnichlono—
phenoxy)
-
U002
67—64-1
Acetone
(I)
U003
75—05—8
Acetonitnile
(I,T)
U004
98-86-2
Acetophenone
UOO5
53-96-3
2-Acetylaminofluorene
U006
75-36—5
Acetyl
chloride
(C,R,T)
U007
79-06-1
Acrylamide
U008
79—10—7
Acrylic
acid
(I)
U009
107—13-1
Acrylonitnile
U011
61—82—5
Amitrole
U0l2
62—S3—3
Aniline
(I,T)
U136
75—60—S
Arsinic
acid,
dimethyl—
U014
492—80—8
Auramine
UO15
115—02—6
Azasenine
UO1O
50—07—7
Azirino2’
,3’ :3,4pyrrolo1,2—
a
indole-4
,
7-dione,
6—amino—8-
(aminocanbonyl)
oxymethyl
-
1, la, 2,8,
8a,8b-hexahydro-8a-
methoxy-5-methyl-,
1a-S-
(laalpha,
8beta,
8aalpha,
8balpha)
3-
Ul57
56—49—5
Benzjaceanthrylene,
1,2-di—
hydro-3-methyl
-
U016
225-51—4
Benz(c)acnidine
U017
98—87—3
Benzal chloride
Ul92
23950—58—5
Benzamide,
3,5—dichloro—N—(1, 1—
dimethyl-2-propynyl)
-
U0l8
56—55-3
Benzaanthnacene
U094
57—97-6
BenzaJanthracene,
7, l2—dimethyl-
U012
62—53—3
Benzenamine
(I,T)
U014
492—80-8
Benzenamine,
4,4’-carbonimidoyl-
bisN,N-diniethyl-
U049
3165-93-3
Benzenamine, 4—chloro—2-methyl—,
hydrochloride
U093
60-11-7
Benzenamine, N,N—dimethyl-4-
(phenylazo)
-
U328
95—53-4
Benzenamine,
2—methyl-
U353
106-49-0
Benzenamine, 4—methyl—
12 1—227
79
Ul58
101-14—4
Benzenamine, 4,4’—methylenebis—
2
-chloro-
U222
636-21-5
Benzenamine,
2-methyl-,
hydrochloride
U181
99-55-8
Benzenamine,
2-methyl-5-nitro-
U019
71—43—2
Benzene
(I,T)
U038
510-1S-6
Benzeneacetic
acid,
4-chloro-
alpha-
(4—chlorophenyl)
-alpha-
hydroxy-,
ethyl
ester
U030
101-55-3
Benzene,
1-bromo—4-phenoxy-
U035
305-03-3
Benzenebutanoic
acid,
4-bis(2-
chloroethyl)
amino)
-
U037
108-90-7
Benzene,
chloro-
U22l
25376-45-8
Benzenediamine,
ar-methyl—
U028
117—81-7
1,2—Benzenedicarboxylic
acid,
bis(2-ethylhexyl)
ester
UO69
84—74—2
1,2—Benzenedicarboxylic
acid,
di—
butyl
ester
U088
84—66—2
1,2—Benzenedicarboxylic
acid,
di-
ethyl
ester
U1O2
131-11-3
1,2-Benzenedicarboxylic
acid,
di-
methyl
ester
U107
117-84—0
l,2—Benzenedicarboxylic
acid,
di—
octyl
ester
U070
95—50-1
Benzene,
1,2—dichloro-
U071
541—73—1
Benzene,
1,3—dichloro-
U072
106-46-7
Benzene,
1,4—dichloro-
U060
72—54—8
Benzene,
1,1 ‘—(2, 2—dichloroethyl—
idene) bis 4-chloro-
U017
98—87—3
Benzene,
(dichloromethyl)—
U223
26471-62—5
Benzene,
1,3—diisocyanatomethyl-
(R,T)
U239
1330—20—7
Benzene,
dimethyl—
(I,T)
U201
108—46—3
1,3—Benzenediol
U127
118-74-1
Benzene,
hexachloro—
U056
110-82—7
Benzene,
hexahydro—
(I)
U220
108—88—3
Benzene,
methyl—
Ul05
121-14—2
Benzene,
1—methyl-2,4-dinitro-
U106
606-20-2
Benzene,
2-methyl-1,3-dinitro-
U055
98-82-8
Benzene,
(1-methylethyl)-
(I)
U169
98-95-3
Benzene,
nitro-
U183
608-93-S
Benzene,
pentachloro-
U185
82-68-8
Benzene,
pentachloronitro-
U020
98-09—9
Benzenesulfonic
acid
chloride
(C,R)
U020
98-09-9
Benzenesulfonyl
chloride
(C,R)
U207
95-94-3
Benzene,
1,2,4,5—tetrachloro—
UO61
S0—29—3
Benzene,
1,1’—(2,’2,2—tnichlono—
ethylidene)bis4-chlono-
U247
72—43—S
Benzene,
l,1’—(2,2,2—trichlono—
ethylidene)
bis 4-methoxy-
U023
98—07-7
Benzene,
(trichloromethyl)—
12 1—228
80
U234
99—35—4
Benzene, 1,3,5—tninitro—
U021
92—87—5
Benzidene
U202
P
81—07—2
1,2—Benzisothiazol—3(2H)—one,
1,1—dioxide,
and
salts
U203
94—59—7
1,3—Benzodioxole,
5—(2—propenyl)—
U141
120—58—1
1,3—Benzodioxole,
5—(1—propenyl)—
U090
94-58—6
1,3-Benzodioxole,
5-propyl-
U064
189-SS-9
Benzorst)pentaphene
U248
P
81-81-2
2H-1-Benzopyran-2-one,
4-hydroxy-
3- (3-oxo-1-phenylbutyl)
-,
and
salts,
when
present
at
concentrations
of
0.3
or
less
U022
50-32-8
Benzoapyrene
Ul97
106-51-4
p-Benzoquinone
U023
98—07-7
Benzotnichlonide
(C,R,T)
U085
1464—S3—S
2,2’—Bioxirane
U021
92—87—S
1,l’—Biphenyl—4,4’—diamine
UO73
91—94—1
1,1’—Biphenyl—4,4’—diamine,
3,3’-dichloro-
U09l
119—90—4
1, 1’—Biphenyl—4,4
‘—diamine,
3,3’ -dimethoxy-
U095
119—93—7
1,1’—Biphenyl—4,4’—diamine,
3,3’ -dimethyl—
U225
75-25—2
Bromoform
U030
101-55-3
4-Bromophenyl
phenyl
ether
U128
87—68—3
1,3—Butadiene,
1,1,2,3,4,4—hexa—
chloro—
U172
924-16-3
1-Butanamine, N-butyl-N-nitroso-
U031
71—36—3
1—Butanol
(I)
TJl59
78—93—3
2—Butanone
(I,T)
U160
1338-23-4
2-Butanone, peroxide
(R,T)
U053
4170—30—3
2—Butenal
tJ074
764—41—0
2—Butene, 1,4—dichloro—
(I,T)
U143
303-34—4
2-Butenoic
acid,
2—methyl—,
7-
2,
3—dihydroxy-2-(1—
methoxyethyl)—3-methyl-1-oxo-
butoxy)methyl
—2,3,5, 7a—tetra-
hydno-1H-pyrrolizin-1-yl
ester,
1S—lalpha(Z),
7(2S*,3R*),
7aalpha
—
U031
71—36—3
n-Butyl
alcohol
(I)
U136
75—60-5
Cacodylic
acid
U032
13765-19-0
Calcium
chromate
U238
51-79—6
Carbamic
acid,
ethyl
ester
U178
615—53-2
Carbamic
acid,
methylnitroso-,
ethyl
ester
U097
79-44-7
Canbamic
chloride,
dimethyl-
U1l4
P
111-54-6
Carbamodithioic a~cid, 1,2—
ethanediylbis—,
salts and esters
U062
2303-16—4
Carbamothioic acid, bis(1—methyl—
ethyl)-, S—(2,3—dichloro-2-
propenyl) ester
12 1—229
81
U2l5
6533-73-9
Carbonic
acid,
dithallium
(1+)
salt
U033
353-50-4
Carbonic
difluonide
U156
79-22-1
Carbonochlonidic
acid,
methyl
ester
(I,T)
U033
353-50-4
Carbon
oxyfluonide
(R,T)
U2l1
56-23-S
Carbon
tetrachlonide
U034
75—87—6
Chloral
U035
305-03—3
Chlorambucil
U036
57—74-9
Chlordanealpha
and
gamma
isomers
U026
494-03-1
Chlornaphazin
1JO37
108-90-7
Chlorobenzene
U038
510-15-6
Chlorobenzilate
U039
59-50-7
p-Chloro-m-cresol
U042
110-75-8
2-Chloroethyl
vinyl
ether
U044
67—66-3
Chloroform
U046
107-30-2
Chloromethyl
methyl
ether
U04 7
91-58-7
beta—Chloronaphthalene
U048
95-57-8
o-Chlorophenol
U049
3165—93-3
4—Chlono—o-toluidine,
hydrochloride
U032
13765-19-0
Chromic
acid
H2CrO4,
calcium
salt
U050
218-01-9
Chrysene
UOS1
Creosote
U052
1319—77-3
Cresol
(Cresylic
acid)
U053
4170—30-3
Crotonaldehyde
U055
98—82—8
Cumeme
(I)
U246
506-68-3
Cyanogen
bromide
CNBr
U197
106—51-4
2, 5-Cyclohexadiene-l,
4-dione
U056
110—82—7
Cyclohexane
(I)
U129
58—89—9
Cyclohexane, 1,2,3,4,5,6—hexa—.
chloro—,
(lalpha,
2alpha,
3beta,
4alpha,
Salph
a,6beta)-
U057
108-94-1
Cyclohexanone
(I)
U130
77—47—4
l,3—Cyclopentadiene,
1,2,3,4,5,5—
hexachi
oro—
U058
50-18-0
Cyclophosphamide
U240
P
94—75—7
2,4—D,
salts
and
esters
U059
20830—81—3
Daunomycin
U060
72—54—8
DDD
U061
50—29—3
DDT
U062
2303—16—4
Diallate
U063
53-70-3
Dibenz a,hanthracene
U064
189—55—9
Dibenzoa,i3pyrene
U066
96-12-8
1,2-Dibromo-3-chloropnopane
U069
84-74-2
Dibutyl phthalate
U070
95-50-1
o-Dichlorobenzene
U071
541-73-1
m-Dichlorobenzene
U072
106-46-7
p-Dichlorobenzene
U073
91—94—1
3,3‘—Dichlonobenzidine
U074
764—41-0
1,4-Dichlono-2—butene
(I,T)
12 1—230
82
IJO7S
75-71-8
Dichlorodifluoromethane
U078
75-35—4
1,1-Dichlonoethylene
U079
156-60-5
1, 2-Dichlonoethylene
UO25
111-44-4
Dichloroethyl ether
U027
108-60-1
Dichloroisopropyl
ether
U024
111-91-1
Dichloromethoxy
ethane
UO81
120-83—2
2,4-Dichlonophenol
U082
87-65—0
2,6-Dichiorophenol
U084
542-75—6
1,3-Dichloropropene
U085
1464—53—S
1,2:3,4—Diepoxybutane
(I,T)
U108
123-91—1
1,4-Diethyleneoxide
UO28
117-81-7
Diethylhexyl
phthalate
U086
1615-80-1
N,N’ -Diethylhydrazine
U087
3288—58—2
0,O-Diethyl
S-methyl
di-
thiophosphate
U088
84-66-2
Diethyl
phthalate
U089
S6—53—1
Diethylstilbestrol
U090
94—58—6
Dihydrosafrole
U091
119-90-4
3,3 ‘-Dimethoxybenzidine
U092
124—40—3
Dimethylamine
(I)
U093
60-11-7
p-Dimethylaminoazobenzene
U094
57—97—6
7, 12-Dimethylbenza)anthracene
U095
119—93-7
3,3‘-Dimethylbenzidine
U096
80—15—9
alpha, alpha—Dimethyl—
benzylhydroperoxide
(R)
U097
79-44-7
Dimethylcarbamoyl chloride
U098
57-14—7
1, l-Dimethylhydnazine
UO99
540—73-8
1, 2-Dimethylhydnazine
UlOl
105—67-9
2,4-Dimethylphenol
U1O2
131-11-3
Dimethyl phthalate
U103
77-78—1
Dimethyl sulfate
U1OS
121—14—2
2,4—Dinitrotoluene
U1O6
606-20—2
2,6-Dinitrotoluene
Ul07
117-84—0
Di—n-octyl phthalate
Ul08
123—91—1
1,4—Dioxane
Ul09
122—66—7
1, 2—Diphenyihydnazine
UllO
142—84—7
Dipnopylamine
(I)
U111
621—64—7
Di-n—propylnitnosamine
U04l
106-89-8
Epichlonohydnin
UOO1
75—07—0
Ethanal
(I)
Ul74
55-18-5
Ethanamine, N-ethyl—N-nitroso-
Ul55
91—80—S
1,2—Ethanediamine, N,N-dimethyl—
N’ -2-pynidinyl-N’
—
(2-thienyl-
methyl)
-
U067
106—93—4
Ethane,
l,2—dibromo—
U076
75-34—3
Ethane,
1,l-dichloro—
U077
107-06-2
Ethane, l,2-dichloro—
Ul31
67-72-1
Ethane, hexachloro-
U024
111-91-1
Ethane,
l,l’-methylenebis(oxy)—
bis2—chloro-
Ul17
60—29—7
Ethane, l,l’—oxybis—
(I)
UO2S
111-44-4
Ethane, l,1’-oxybis2—chlono-
12 1—231
83
U184
76-01-7
Ethane,
pentachloro-
U208
630—20—6
Ethane,
1,1,
1,2—tetrachlono-
U209
79—34-S
Ethane,
1,l,2,2—tetrachloro—
U218
62—55-S
Ethanethioamide
U226
71—S5-6
Ethane,
1,l,l—trichloro—
U227
79-00-S
Ethane,
1,1,2-tnichloro-
U359
110—80—5
Ethanol,
2—ethoxy—
U173
1116—S4—7
Ethanol,
2,2’—(nitrosoimino)bis—
1J004
98-86-2
Ethanone,
1—phenyl—
U043
75-01-4
Ethene,
chloro—
U042
110-75-8
Ethene,
(2-chloroethoxy)-
U078
75-35-4
Ethene,
1,l—dichloro-
U079
1S6—60—S
Ethene,
1,2—dichloro-,
(E)—
U210
127-18-4
Ethene,
tetrachloro—
13228
79-01-6
Ethene,
tnichloro-
U1l2
141-78-6
Ethyl
acetate
(I)
13113
140-88—5
Ethyl
acrylate
(I)
U238
S1-79-6
Ethyl
carbamate
(urethane)
Ul17
60-29-7
Ethyl
ether
U114
P
111-S4-6
Ethylenebisdithiocarbamic
acid,
salts
and
esters
U067
106-93-4
Ethylene
dibromide
U077
107-06-2
Ethylene
dichlonide
13359
110-80-S
Ethylene
glycol
inonoethyl
ether
Ul15
75—21-8
Ethylene
oxide
(I,T)
Ul16
96-45-7
Ethylenethiourea
U076
75-34-3
Ethylidene
dichionide
13118
97-63-2
Ethyl
methacrylate
Ul19
62-50-0
Ethyl
methanesulfonate
U120
206—44—0
Fluoranthene
U122
50—00-0
Formaldehyde
Ul23
64-18—6
Formic acid
(C,T)
U124
110—00—9
Furan
(I)
U125
98-01-1
2-Furancarboxaldehyde
(I)
13147
108-31-6
2,5-Furandione
U213
109-99-9
Furan, tetrahydro—
(I)
Ul25
98—01—1
Furfural
(I)
U124
110—00—9.
Furfuran
(I)
U206
18883-66-4
Glucopyranose,
2—deoxy—2—(3—
methyl-3—nitrosoureido)
-,
U206
18883-66—4
D-Glucose,
2—deoxy—2-
(methyl—
nitrosoamino)
—carbonyl
amino
—
13126
765—34-4
Glycidylaldehyde
U163
7 0-25-7
Guanidine,
N-methyl-N’
-nitro-N—
nitroso—
U127
118-74-1
Hexachlorobenzene
U128
87-68-3
Hexachlonobutadiene
13130
77—47—4
Hexachlorocyclope’ntadiene
U131
67—72-1
Hexachloroethane
13132
70-30-4
Hexachlorophene
U243
1888—71—7
Hexachloropropene
13133
302—01—2
Hydrazine
(R,T)
12 1—232
84
Hydnazine,
1, 2-diethyl-
Hydrazine,
1, 1-dimethyl-
Hydrazine,
1, 2-dimethyl—
Hydrazine,
1, 2-diphenyl-
Hydrofluonic
acid
(C,T)
Hydrogen
fluoride
(C,T)
Hydrogen
sulfide
Hydrogen
sulfide
H2S
Hydroperoxide, 1-methyl-l-phenyl-
ethyl-
(R)
2 -Imidazol
idinethiorie
Indeno1,
2, 3-cdpyrene
1, 3—Isobenzofurandione
Isobutyl
alcohol
(I,T)
Isosaf role
Kepone
Lasiocarpene
Lead
acetate
Lead,
bis (acetato-O)
tetra-
hydroxytni-
Lead phosphate
Lead subacetate
Lindane
MNNG
Maleic
anhydnide
Maleic
hydrazide
Malononitrile
Melphalan
Mercury
Methacnylonitrile
(I,T)
Methanamine, N-methyl-
(I)
Methane,
bromo—
Methane,
chloro-
(I,T)
Methane, chloromethoxy—
Methane, dibromo-
Methane, dichloro-
Methane,
dichlonodifluoro-
Methane,
iodo—
Methanesulfonic acid,
ethyl ester
Methane, tetrachlono—
Methanethiol
(I,T)
Methane, tnibromo—
Methane,
trichloro-
Methane, trichlorofluoro—
4, 7-Methano-1H-indene,
1,2,4,S,6,7,8,8—octachlono—
2,3,
3a, 4,7,
7a-hexahydno—
Methanol
(I)
Methapyrilene
13086
UO98
13099
13109
13134
U1 34
U135
U135
U096
13116
13137
13190
13140
U14 1
13142
U14 3
U144
Ul4 6
13145
13146
U129
U163
13147
U148
13149
13150
13151
U1S2
U092
U029
1104S
13046
UO68
13080
U075
13138
U119
U2 11
U153
13225
U044
13121
U03 6
13154
13155
1615—80—1
57—14—7
540—73—8
122—66—7
7664—39—3
7664—39—3
7783—06—4
7783—06—4
80—15—9
96—45—7
193—39—S
8S—44—9
78—83—1
120—58—1
143—50—0
303—34—4
301—04—2
1335—32—6
7446—27—7
1335—32—6
58—89—9
70—2S—7
108—31—6
123—33—1
109—77—3
148—82—3
74 39—97—6
12 6—98—7
124—40—3
74—83—9
74—87—3
107—30—2
74—95—3
75—09—2
75—71—8
74—88—4
62—50—0
56—23—S
74—93—1
75—25—2
67—66—3
75—69—4
57—74—9
67—56—1
91—80—5
121—233
85
U142
143—50-0
1,3,4—I4etheno-2H-cyclobutacd-
pentalen—2—one,
1, la,3,
3a, 4, 5, 5, Sa, 5b,
6—
decachl orooctahydro-
13247
72-43-5
Methoxychlor
U1S4
67—56-1
Methyl
alcohol
(I)
13029
74-83-9
Methyl bromide
13186
504-60-9
1-Methylbutadiene
(I)
UO4S
74—87—3
Methyl
chloride
(I,T)
13156
79-22-1
Methyl
chlorocarbonate
(I,T)
U226
71-S5-6
Methylchloroform
U1S7
56-49-5
3-Methylcholanthrene
U1S8
101—14-4
4,4‘—Nethylenebis(2-chloro—
aniline)
13068
74-95-3
Methylene
bromide
13080
7S-09-2
Methylene
chloride
U159
78-93-3
Methyl
ethyl
ketone
(MEK)
(I,T)
13160
1338-23-4
Methyl ethyl ketone peroxide
(R,T)
U138
74—88-4
Methyl
iodide
U161
108-10-1
Methyl
isobutyl
ketone
(I)
13162
80-62-6
Methyl methacrylate
(I,T)
Ul61
108—10-1
4—Methyl—2—pentanone
(I)
Ul64
56-04-2
Methylthiouracil
UOlO
50-07-7
Mitomycin C
UOS9
20830-81-3
S,12-Naphthacenedione,
8—acetyl-
10—
(3—amino-2,
3,
6-tnideoxy)
-
alpha-L-lyxo-hexapyranosyl) oxyl
-
7,8,9, 10—tetrahydro—6, 8,11—tn—
hydroxy—l-methoxy-,
(8S-cis)
-
13167
134—32-7
1—Naphthalenamine
Ul68
91-59-8
2-Naphthalenamine
U026
494-03-1
Naphthaleneamine, N,N’—bis(2-
chloroethyl)
—
Ul65
91—20-3
Naphthalene
U047
91—S8-7
Naphthalene, 2-chiono—
Ul66
130-15-4
1, 4-Naphthalenedione
U236
72-57-1
2,7-Naphthalenedisulfonic
acid,
3,3
t_(3,
3 ‘—dimethyl—l,
1’—
biphenyl)—4,4 ‘—diyl) bis (azo) bis—
S-amino-4 -hydroxy
-,
tetrasodium
salt
13166
130-15-4
l,4-Naphthoquinone
13167
134—32-7
alpha—Naphthylamine
U168
91-59-8
beta-Naphthylamine
U217
10102—45—1
Nitric
acid,
thallium
(1+)
salt
Ul69
98-9S-3
Nitrobenzene
(I,T)
13170
100-02-7
p-Nitrophenol
Ul7l
79—46-9
2—Nitropropane
(I,T)
13172
924-16-3
N-Nitrosodi-n-butylamine
13173
1116-54-7
N-Nitrosodiethanolamine
U174
5S—18—5
N-Nitrosodiethylamine
121—2 34
86
13176
759-73-9
N-Nitroso-N-ethylunea
13177
684-93-S
N-Nitroso-N-methylurea
13178
615-53-2
N-Nitroso-N-methylurethane
13179
100-75-4
N-Nitrosopipenidine
13180
930-55-2
N-Nitrosopyrrolidine
11181
99-55-8
S-Nitro-o—toluidine
U193
1120—71—4
1,2—Oxathiolane,
2,2—dioxide
UOS8
50-18—0
2H—1, 3,2—Oxazaphosphonin-2—amine,
N,N-bis (2-chloroethyl)
tetra—
hydro-,
2-oxide
U11S
75—21—8
Oxirane
(I,T)
13126
765-34-4
Oxiranecarboxyaldehyde
3041
106-89-8
Oxirane,
(chloromethyl)-
13182
123—63-7
Paraldehyde
13183
608—93—5
Pentachlorobenzene
13184
76—01—7
Pentachloroethane
13185
82-68-8
Pentachlononitrobenzene (PCNB)
See
F027
87—86-S
Pentachiorophenol
U16l
108-10-1
Pentanol, 4—methyl-
13186
504—60—9
1,3—Pentadiene
(I)
Ul87
62-44—2
Phenacetin
Ul88
108—9S—2
Phenol
UO48
95-57-8
Phenol, 2—chloro—
UO39
59—50-7
Phenol, 4—chlono—3-methyl-
U08l
120—83—2
Phenol, 2,4—dichloro—
U082
87—65—0
Phenol, 2,6—dichloro—
UO89
56—53—1
Phenol,
4,4’—(l,2—diethyl—l,2—
ethenediyl)bis-,
(E)
-
13101
105—67—9
Phenol, 2,4—dimethyl—
U052
1319-77-3
Phenol, methyl—
U132
70—30—4
Phenol, 2,2’—methylenebis3,4,6—
tnichloro-
U170
100-02—7
Phenol,
4-nitro—
See F027
87—86—S
Phenol, pentachloro-
See F027
58—90—2
Phenol, 2,3,4,6—tetrachloro—
See F027
95-95—4
Phenol, 2,4,S—tnichloro-
See F027
88-06—2
Phenol, 2,4,6—tnichloro-
U1SO
148—82—3
L—Phenylalanine,
4—bis(2—chloro—
ethyl) amino—
U14S
7446—27—7
Phosphoric acid,
lead (2+) salt
(2:3)
13087
3288—58-2
Phosphorodithioic
acid,
O,O-di-
ethyl
S-methyl
ester
U189
1314—80—3
Phosphorus
sulfide
(R)
13190
85-44-9
Phthalic
anhydnide
13191
109—06—8
2—Picoline
13179
100-75-4
Piperidine,
1—nitroso-
11192
23950—58—5
Pronamide
11194
107—10—8
1-Propanamine
(I,T)
Ulli
621-64-7
1-Propanamine, N-nitroso-N-
propyl—
13110
142-84-7
l-Propanamine, N-propyl—
(I)
121—235
87
U066
96—12—8
Propane, 1,2-dibromo—3—chloro—
U083
78-87—5
Propane,
1,2-dichloro—
13149
109-77-3
Propanedinitrile
13171
79—46—9
Propane,
2—nitro—
(I,T)
U027
108-60—1
Propane,
2,2 ‘—oxybis2-chloro—
See
F027
93—72—1
Propanoic
acid,
2—(2,4,5—tni—
chlorophenoxy)
-
U193
1120-71-4
1,3-Propane
sultone
13235
126—72-7
1-Propanol,
2,3—dibromo-,
phosphate
(3:1)
U140
78-83-1
1-Propanol,
2—methyl—
(I,T)
13002
67-64—1
2—Propanone
(I)
13007
79-06-G1
2-Propenamide
U084
542—75-6
1—Propene,
1,3—dichloro-
13243
1888—71—7
1—Propene,
1,1,2,3,3,3—hexa—
chl oro—
U009
107—13—1
2—Propenenitnile
U152
126-98-7
2-Propenenitnile,
2-methyl-
(I,T)
13008
79—10—7
2—Propenoic
acid
(I)
U113
140-88-S
2-Propenoic
acid,
ethyl
ester
(I)
13118
97-63-2
2-Propenoic
acid,
2-methyl-,
ethyl
ester
13162
80-62-6
2-Propenoic
acid,
2-methyl-,
methyl
ester
(I,T)
See
F027
93-72-1
Propionic
acid,
2—(2,4,5—tni—
chlorophenoxy)
—
-
13194
107—10—8
n—Propylamine
(I,T)
13083
78-87-S
Propylene dichlonide
13148
123-33-1
3,6—Pyridazinedione,
1,2—dihydro-
Ul96
110—86—1
Pyridine
Ul9l
109-06—8
Pynidine,
2—methyl—
U237
66—75—1
2,4—(1H,3H)—Pynimidinedione,
5—
bis(2-chloroethyl) amino—
13164
S8-04-2
4(1H)-Pynimidinone,
2 ,3-dihydro-
6-methyl-2-thioxo-
U180
930-SS-2
Pyrrolidine, 1-nitroso-
13200
50—55—S
Reserpine
13201
108—46—3
Resorcinol
13202
P
81-07—2
Saccharin
and
salts
U203
94—59—7
Safrole
13204
7783—00—8
Selenious
acid
U204
7783—00—8
Selenium
dioxide
13205
7488—56—4
Selenium
sulfide
U2OS
7488—56—4
Selenium
sulfide
SeS2
(R,T)
UO1S
11S-02—6
L—Senine,
diazoacetate
(ester)
See
F027
93—72—1
Silvex
(2,4,S—TP)
U2O6
18883—66-4
Streptozotocin
Ul03
77-78-1
Sulfuric
acid,
di-xnethyl
ester
U189
1314—80-3
Sulfur
phosphide
(R)
See
F027
93—76—S
2,4,5—T
13207
9S-94—3
1,2,4, 5—Tetrachlorobenzene
U2O8
630—20—6
1,1,1,2-Tetrachloroethane
12 1—236
88
13209
79—34—S
1, 1,2,2—Tetrachloroethane
U210
127-18-4
Tetnachloroethylene
See
F027
S8-90-2
2,3,4,6—Tetrachlorophenol
13213
109-99-9
Tetrahydrofuran
(I)
U214
563—68—8
Thallium
(I)
acetate
U215
6533—73—9
Thallium
(I)
carbonate
U216
7791—12—0
Thallium
(I)
chloride
U216
7791—12—0
Thallium
chloride
T1C1
13217
10102—4S—1
Thallium
(I)
nitrate
U218
62-55-S
Thioacetamide
13153
74—93—1
Thiomethanol
(I,T)
13244
137—26-8
Thioperoxydicarbonic
diamide
(H2N)C(S))2S2,
tetramethyl—
U219
62-56-6
Thiourea
U244
137—26—8
Thiram
13220
108-88-3
Toluene
U221
2S376—4S—8
Toluenediamine
U223
26471—62-5
Toluene diisocyanate
(R,T)
13328
95-53-4
o-Toluidine
U353
106—49—0
p—Toluidine
U222
636-21-5
o-Toluidine
hydrochloride
13011
61—82—S
111—1,2, 4—Tniazol—3—amine
13227
79—00—S
1, 1,2—Tnichloroethane
U228
79-01-6
Tnichloroethylene
U12
1
75-69-4
Tnichloromonofluonomethane
See
F027
95-95—4
2,4,S—Trichlorophenol
See
F027
88-06-2
2,4,6—Tnichlorophenol
11234
99-35-4
l,3,5—Tninitnobenzene
(R,T)
11182
123—63—7
1,3,5—Tnioxane,
2,4,6—tnimethyl—
U235
126-72-7
Tnis(2,
3-dibnomopropyl)
phosphate
U236
72-57-1
Trypan
blue
13237
66-75-1
Uracil
mustard
13176
759-73—9
Urea, N—ethyl-N—nitroso-
13177
684-93-5
Urea,
N-methyl-N-nitroso-
U043
7S—01—4
Vinyl
chloride
U248
P
81-81-2
Warfarin,
and
salts,
when
present
at
concentrations
of
0.3
or
less
U239
1330—20—7
Xylene
(I)
13200
50-55—5
Yohimban—16-carboxylic
acid,
11, 17—dimethoxy—18— (3,4,
5—tn—
methoxybenzoyl)
oxy
-,
methyl
ester,
(3beta,
l6beta,
l7alpha,
l8beta,
2Oal
pha)
-
U249
1314-84—7
Zinc
phosphide
Zn3P2,
when
present
at
concentrations
of
10
on
less
(Source:
Amended
at
15
Ill.
Reg.
,
effective
121—237
89
Section
721.Appendix
C
Chemical
Analysis
Test
Methods
The
Board
incorporates
by
reference
40
CFR
261,
Appendix
III
(1989),
as
amended
at
S4
Fed.
Reg.
41407,
October
6,
1989,
and
as
amended
at
55
Fed.
Reg.
8948,
March
9,
1990
and
at
55
Fed.
Req.
18496,
May
2,
1990.
This
Section
incorporates
no
future
editions
or
modifications.
(Source:
Amended
at
15
Ill.
Reg.
,
effective
12 1—238
90
Section 72l.Appendix G
Basis for Listing Hazardous Wastes
EPA
Hazardous
Constitutents
for
which
Listed
Hazardous
Waste
No.
FOOl
Tetrachlonoethylene,
methylene
chloride,
tnichloroethylene,
1,1,
l—tnichloroethane,
carbon
tetrachlonide,
chlorinated
fluorocarbons.
F002
Tetrachloroethylene,
methylene
chloride,
tnichloroethylene,
1,1,l—trichloroethane,
1,1,2—tnichloroethane,
chlorobenzene,
1,1,2-tnichloro-1,2,2- tnifluoroethane, ortho-dichloro-
benzene, trichlonofluoromethane.
F003 N.A.
F004
Cresols
and
cresylic
acid,
nitrobenzene.
FOOS
Toluene,
methyl
ethyl
ketone,
carbon
disulfide,
isobutanol,
pynidine,
2—ethoxyethanol,
benzene,
2—nitropropane
F006
Cadmium,
hexavalent
chromium,
nickel,
cyanide
(complexed).
F007
Cyanide
(salts).
F008
Cyanide
(salts).
F009
Cyanide
(salts).
FOlO
Cyanide
(salts).
FOil
Cyanide
(salts).
F012
Cyanide
(complexed).
F019 Hexavalent chromium, cyanide
(coniplexed).
F020
Tetra-
and
pentachlorodibenzo-p-dioxins;
tetra—
and
penta—
chlorodibenzofunans;
tn-
and
tetrachlorophenols and their
chlorophenoxy
derivative
acids,
esters,
ethers,
ainines
and
other
salts.
F02l
Penta-
and
hexachlonodibenzo-p-dioxins;
penta-
and
hexa-
chlorodibenzofurans; pentachlorophenol and its derivatives.
F022
Tetra-,
penta-
and
hexachlorodibenzo-p-dioxins;
tetra-,
penta—
and
hexachlonodibenzofurans.
F023
Tetna-
and
pentachlorodibenzo-p-dioxins;
tetra-
and
penta-
chlorodibenzofurans;
tn-
and
tetra—
chlonophenols and them
chlonophenoxy
derivative
acids,
esters,
ethers,
amines
and
12 1—239
91
other salts.
FO24 Chloromethane, dichioromethane, tnichloromethane,
carbon
tetrachlonide,
chloroethylene,
1, 1-dichloroethane,
1, 2-di-
chloroethane,
trans-i,
2-dichloroethylene,
1, 1—dichloro-
ethylene,
1,1, 1-trichloroethane,
1,1,
2—tnichloroethane,
tn-
chloroethylene,
1,1,1,
2—tetrachloroethane,
1,1,2,
2—tetra—
chloroethane,
tetrachloroethylene,
pentachloroethane,
hexa-
chloroethane,
allyl
chloride
(3-chloropropene),
dichloro-
propane,
dichloropropene,
2—chloro—1, 3—butadiene,
hexa—
chloro—l, 3—butadiene,
hexachlorocyclopentadiene,
hexa-
chlorocyclohexane,
benzene,
chlorobenzene,
dichlorobenzenes,
1,2, 4—tnichlonobenzene,
tetrachlorobenzenes,
pentachioro—
benzene,
hexachlorobenzene,
toluene,
naphthalene.
F025 Chloromethane, dichloromethane, tnichloromethane; carbon
tetrachlonide;
chloroethylene;
1, 1-dichloroethane;
1, 2—di-
chloroethane;
trans-i,
2-dichioroethylene;
1, 1-dichloro-
ethylene;
1,1,
1-tnichloroethane;
1,1,
2—tnichloroethane;
tn-
chloroethylene;
1,1,1,
2-tetnachloroethane;
1,1,2,
2—tetna—
chloroethane;
tetrachloroethylene;
pentachloroethane;
hexa—
chloroethane;
allyl
chloride
(3-chloropnopene);
dichlono-
propane; dichloropnopene;
2-chloro-1, 3-butadiene; hexa-
chloro—1,3—butadiene; hexachlonocyclopentadiene; benzene;
chlorobenzene;
dichlonobenzene;
1,2, 4—tnichlonobenzene;
tetrachlorobenzene; pentachlorobenzene; hexachlonobenzene;
toluene; naphthalene.
F026 Tetna-, penta-, and hexachlorodibenzo-p-dioxins;
tetna-,
penta-,
and hexachlorodibenzofurans.
F027 Tetra-, penta-, and hexachlorodibenzo-p-dioxins;
tetna-,
penta—, and hexachlonodibenzofurans; tn—,
tetra—, and
pentachlorophenols and their chlorophenoxy derivative acids,
esters, ethers,
amine and other salts.
F028 Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetna-,
penta—, and hexachlorodibenzofurans; tn-,
tetra—, and
pentachlorophenols and their chlonophenoxy derivative acids,
esters, ethers, amine and other salts.
F039 All constituents for which treatment standards are specified
for multi—source leachate (wastewaters and non—wastewaters)
under 35
Ill. Adm. Code 728.Table B
(Constituent
Concentrations in Waste)
1(001 Pentachlorophenol, phenol,
2-chlorophenol, p-chloro-m-
cresol,
2, 4-dimethylphenol,
2, 4-dinitrophenol, tnichloro-
phenols, tetrachlorophenols,
2,4—dinitrophenol,
cresosote,
chrysene, naphthalene, fluoranthene, benzo (b) fluoranthene,
benzo(a)pynene,
indeno(1,2,3—cd)pyrene, benz(a)anthracene,
dibenz (a) anthracene, acenaphthalene.
121—240
92
KOO2 Hexavalent chromium, lead.
K003
Hexavalent
chromium,
lead.
1(004
Hexavalent
chromuim.
K005
Hexavalent
chromium,
lead.
K006
Hexavalent
chromium.
K007
Cyanide
(complexed),
hexavalent
chromium.
K008
Hexavalent
chromium.
K009
Chloroform,
formaldehyde,
methylene
chloride,
methyl
chloride, paraldehyde,
formic acid.
KO1O Chloroform,
formaldehyde, methylene chloride, methyl
chloride, paraldehyde,
formic acid, chioroacetaldehyde.
KOll Acrylonitnile, acetonitnile, hydrocyanic acid.
K013
Hydro
cyanic
acid,
acrylonitnile,
acetonitnile.
K014
Acetonitnile,
acrylamide.
1(015
Benzyl
chloride,
chlorobenzene,
toluene,
benzotnichloride.
1(016 Hexachlorobenzene, hexachlorobutadiene, carbon tetra—
chloride, hexachloroethane,
perchloroethylene.
1(017 Epichlorohydrin,
chloroethers bis(chloromethyl)
ether and
bis—(2-chloroethyl)
ethers,
tnichlonopropane, dichlono-
propanols.
1(018
1, 2-dichloroethane, tnichloroethylene,
hexachlorobutadiene,
hexachlorobenzene.
K0l9 Ethylene dichlonide,
1,1,l-tnichlonoethane,
1,1,2—tn-
chloroethane,
tetrachloroethanes
(1,1,2,
2—tetrachloroethane
and
1,1,1,
2—tetnachioroethane),
trichlonoethylene,
tetna-
chloroethylene,
carbon tetnachloride, chloroform, vinyl
chloride, vinylidene chloride.
1(020 Ethylene dichlonide,
1,1,1-tnichioroethane,
1,1,2-tn-
chloroethane, tetrachioro-ethanes (1,1,2,2—tetrachlono—
ethane and 1,1,1, 2-tetrachlonoethane),
tnich’loroethylene,
tetnachloroethylene, carbon tetnachionide, chloroform, vinyl
chloride, vinylidene chloride.
1(021 Antimony, carbon tetrachlonide, chloroform.
12 1—241
93
KO22 Phenol, tars (polycyclic aromatic hydrocarbons).
1(023 Phthalic anhydnide, maleic anhydnide.
1(024 Phthalic anhydnide,
l,4-naphthoguinone.
1(025 Meta-dinitrobenzene,
2, 4-dinitrotoluene.
K026 Panaldehyde, pynidines,
2—picoline.
1(027 Toluene diisocyanate, toluene—2,
4—diamine.
1(028 l,1,l—tnichlonoethane, vinyl chloride.
K029
1, 2-dichloroethane,
1,1,1-tnichloroethane, vinyl chloride,
vinylidene chloride, chloroform.
1(030 Hexachlorobenzene, hexachlorobutadiene, hexachlonoethane,
1,1,1, 2-tetnachlonoethane,
1,1,2, 2—tetrachlonoethane, ethyl-
ene dichionide.
K031
Arsenic.
K032
Hexachlonocyclopentadiene.
K033
Hexachlorocyclopentadiene.
K034
Hexachlorocyclopentadiene.
KO3S Creosote, chrysene, naphthalene, fluonanthene,
benzo(b)
fluoranthene,
benzo(a)
-pynene,
indeno(l, 2,3—cd)
pyrene,
benzo (a) anthracene,
dibenzo
(a) anthnacene,
acenaphthalene.
1(036
Toluene,
phosphorodithioic
and
phosphorothioic acid esters.
K037
Toluene,
phosphorodithioic
and
phosphorothioic
acid
esters.
KO38
Phorate,
formaldehyde, phosphonodithioic and phosphoro-
thioic acid esters.
K039
Phosphonodithioic
and
phosphonothioic acid esters.
KO4O Phonate, formaldehyde, phosphorodithioic and phosphono-
thioic
acid
esters.
1(041
Toxaphene.
1(042
Hexachlorobenzene,
ortho—dichlonobenzene.
1(043 2,4-dichlorophenol,
2, 6—dichionophenol,
2 ,4,6—tnichloro—
phenol.
121—242
94
KO44 N.A.
K04S N.A.
1(046 Lead
1(047 N.A.
K048 Hexavalent chromium, lead.
K049 Hexavalent chromium,
lead.
KOSO Hexavalent chromium.
K05l
Hexavalent
chromium,
lead.
K0S2
Lead
KO6O
Cyanide,
naphthalene,
phenolic
compounds,
arsenic.
1(061
Hexavalent
chromium,
lead,
cadmium.
KO62
Hexavalent
chromium,
lead.
1(064
Lead,
cadmium
K065
Lead,
cadmium
K066
Lead,
cadmium
1(069
Hexavalent
chromium,
lead,
cadmium.
1(071
Mercury.
K073
Chloroform,
carbon
tetrachlonide,
hexachloroethane,
tn—
chlonoethane,
tetnachloroethylene,
dichioroethylene,
1,1,2,
2—tetnachloroethane.
KO83
Aniline,
diphenylamine,
nitrobenzene,
phenylenediamine.
1(084
Arsenic.
K08S
Benzene,
dichlonobenzenes,
tnichlorobenzenes,
tetnachloro—
benzenes,
pentachlonobenzene,
hexachlonobenzene,
benzyl
chloride.
1(086
Lead,
hexavalent
chromium.
1(087
Phenol,
naphthalene.
K088
Cyanide
(complexes)
12 1—243
95
1(090
Chromium
1(091
Chromium
K093
Phthalic
anhydnide
maleic
anhydnide.
1(094
Phthalic
anhydnide.
1(095
1, 1,2—tnichloroethane,
1,1,
1,2—tetrachlonoethane,
1,1,2,2—
tetrachloroethane.
K096
1,2—dichionoethane,
1,1, 1,—tnichloroethane,
1, 1,2—tn—
chloroethane.
1(097
Chlordane,
heptachlon.
K098
Toxaphene.
1(099
2, 4—dichlorophenol,
2,4,
6—tnichlorophenol.
KlOO
Hexavalent
chromium,
lead,
cadmium.
1(101
Arsenic.
1(102
Arsenic.
1(103
Aniline,
nitrobenzene,
phenylenediamine.
1(104
Aniline,
benzene,
diphenylamine,
nitnobenzene, phynylenedi-
amine.
1(105 ~Benzene,
..monochlorobenzene,
dichlonobenzenes,
2,4,
6—tn—
chlorophenol.
1(106 Mercury.
1(107 l,i-Dimethylhydrazine
(UDMH)
K1O8 1,1-Dimethylhydrazine
(UDMH)
1(109 l,i-Dimethylhydrazine
(UDMH)
KilO 1.l-Dimethylhydrazine
(UDMH)
1(111
2, 4—Dinitnotoluene.
1(112
2,4-Toluenediamine,
o-toluidine,
p—toluidine’,
aniline.
Kll3 2,4-Toluenediamine, o-toluidine, p—toluidine, aniline.
Kl14 2,4-Toluenediamine, o-toluidine, p—toluidine.
121—244
96
1(115
2, 4—Toluenediamine.
K116 Carbon tetnachlonide, tetnachloroethylene,
chloroform,
phosgene.
1(117 Ethylene dibnomide
K118 Ethylene dibromide
1(123
Ethylene
thiourea
1(124 Ethylene thiounea
K12S Ethylene thiourea
K126 Ethylene thiounea
1(131
Dimethyl
sulfate,
methyl
bromide
1(132
Methyl
bromide
K136
Ethylene
dibromide
N.A.——Waste
is
hazardous
because
it
fails
the
test
for
the
characteristic of ignitability, conrosivity on reactivity.
(Source:
Amended at
15 Ill.
Reg.
,
effective
12 1—245
97
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART
722
STANDARDS
APPLICABLE
TO
GENERATORS
OF
HAZARDOUS
WASTE
SUBPART
A:
GENERAL
Section
722.110
722.111
722.112
Section
722.130
722.
131
722.132
722.
133
722.134
Section
722.140
722
.
141
722.142
722.143
722 .144
Section
722.150
722.151
722. 152
722.
153
722.
154
722.155
722.156
722.
157
Purpose,
Scope
and
Applicability
Hazardous
Waste
Determination
USEPA Identification Numbers
SUBPART B:
THE
MANIFEST
General Requirements
Acquisition .of Manifests
Number of Copies
Use of the Manifest
SUBPART
C:
PRE-TRANSPORT
REQUIREMENTS
Packaging
Labeling
Marking
Placanding
Accumulation Time
SUBPART
D:
RECORDKEEPING
AND
REPORTING
Recordkeeping
Annual Reporting
Exception Reporting
Additional Reporting
Special Requirements for Generators of between 100 and
1000 kilograms per month
SUBPART E:
EXPORTS OF HAZARDOUS WASTE
Applicability
Definitions
General Requirements
Notification
of
Intent
to
Export
Special
Manifest
Requirements
Exception
Report
Annual
Reports
Recondkeeping
SUBPART
F:
IMPORTS
OF
HAZARDOUS
WASTE
Section
722.160
Imports of Hazardous Waste
Section
722.120
722.121
722.122
722.123
12 1—246
98
SUBPART
G:
FARMERS
Section
722.170
Farmers
Appendix A
Hazardous Waste Manifest
AUTHORITY.:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111 1/2, pans.
1022.4
and
1027).
SOURCE:
Adopted
in
R8l-22,
43 PCB 427, at
5
Ill.
Reg.
9781,
effective as noted in 35
Ill. Adm. Code 700.106; amended and
codified in R81—22,
45 PCB 317, at
6 Ill.
Reg.
4828, effective as
noted in 35
Ill. Adm. Code 700.106; amended in R82—l8,
51 PCB 31,
at
7
Ill. Reg.
2518,
effective February 22,
1983; amended in R84-
9 at
9
Ill. Reg.
11950, effective July 24,
l98S; amended in R85—
22 at 10
Ill. Reg.
1131,
effective
January
2,
1986;
amended in
R86—1 at 10
Ill. Reg.
14112,
effective August 12,
1986;
amended
in R86—19 at 10 Ill. Reg.
20709, effective December 2,
1986;
amended in R86-46 at 11 Ill.
Reg.
13SSS, effective August.4,
1987;
amended in R87—5 at 11
Ill.
Reg.
19392,
effective
November
12,
1987; amended in R87—39 at 12
Ill. Reg.
13129, effective July
29,
1988; amended in R88—16 at 13
Ill. Reg.
452, effective
December 27,
1988; amended in R89—1 at 13 Ill. Reg.
18523,
effective November 13,
1989; amended in R90—10 at 14
Ill.
Reg.
,
effective September 25,
1990; amended in R90-ll at 15
Ill. Reg.
,
effective
SUBPART A:
GENERAL
Section 722.111
Hazardous Waste Determination
A person who generates a solid waste,
as defined in 35 Ill.
Adm.
Code 721.102, shall determine if that waste is a hazardous waste
using the following method:
a)
The person should first determine if the waste is
excluded from regulation under 3S Ill. Adm. Code
721.104.
b)
The person should then determine if the waste is listed
as a hazardous waste in 35 Ill. Adm. Code 72l.Subpart
D.
(Board Note:
Even if a waste is listed, the generator
still has an opportunity under 3S Ill. Adm. Code
720.122 and 40 CFR 260.22
(1986) to demonstrate that
the waste from the generator’s panticul’~anfacility or
operation is not a hazardous waste.
c)
For purposes of compliance with 35 Ill. Adm. Code 728,
on
if14
the waste is not listed as
a hazardous waste
in
12 1—247
99
35 Ill. Adm. Code 721.Subpart D, the generator
shouldshall then determine whether the waste is
identified in 35 Ill.
Adm. Code 721.Subpart C by
either:
1)
Testing the waste according to the methods set
forth in 35 Ill. Adm. Code 721.Subpart
C, or
according to an equivalent method approved by the
Board
under
35
Ill.
Adm.
Code
720.120;
or
2)
Applying
knowledge
of
the
hazard
characteristic
of
the
waste
in light of the materials
or
processes
used.
d)
If the generator determines that the waste is
hazardous, the generator shall refer to 35
Ill. Adm.
Code
724,
725
and
728 for possible exclusions on
restrictions
pertaining
to the management of the
specific
waste.
(Source:
Amended
at
15
Ill.
Reg.
,
effective
SUBPART
C:
PRE-TRANSPORT
REQUIREMENTS
Section
722.134
Accumulation Time
a)
Except
as
provided
in
subsections
(d), (e) or
(f),
a
generator
may
accumulate
hazardous
waste on—site for 90
days
or
less without a permit on without having interim
status provided that:
1)
The waste is placed in containers and the
generator complies with 35 Ill. Adm. Code
725.Subpart
I or the waste is placed in tanks and
the generator complies with 35 Ill.
Adin.
Code
725.Subpant J except 35
Ill.
Adm.
Code
725.297(c)
and 725.300..
In addition, such a generator is
exempt from all the requirements in 35 Ill.
Adm.
Code 72S.Subpants G and H, except for 35 Ill. Adm.
Code 72S.2l1 and 725.214;
2)
The
date
upon
which
each
period
of accumulation
begins is clearly marked and visible for
inspection on each container;
3)
While being accumulated on—site, each container
and tank is labeled or marked cleaTly with the
words,
“Hazardous Waste”,
and
4)
The generator complies with the requirements for
owners or operators in 35 Ill. Adm. Code
12 1—248
100
725.Subpants C and D~and with 3S Ill. Adm. Code
725.116 and 728.107(a) (4).
b)
A generator who accumulates hazardous waste for more
than 90 days is an operator of a
storage
facility
and
is
subject
to
the
requirements
of
35 Ill. Adm. Code 724
and
725 and the permit requirements of 35 Ill. Adm.
Code
702,
703
and
70S
unless
the
generator
has
been
granted
an
extension
of
the
90-day
period.
If
hazardous
wastes
must
remain
on—site
for
longer
than
90
days
due
to
unforeseen,
temporary,
and
uncontrollable
circumstances,
the
generator
may
seek
an
extension
of
up
to
30
days by means of a variance or provisional
variance,
pursuant
to
Section
37
of
the
Environmental
Protection Act.
c)
Accumulation near point of generation.
1)
A generator may accumulate as much as 55 gallons
of hazardous waste on
one
quart
of acutely
hazardous waste listed in
35
Ill. Adm. Code
721.133(e)
in containers at on near any point of
generation where wastes initially accumulate,
which is under the control of the operator of the
process generating the waste, without a permit on
interim status and without complying with
paragraph
(a) provided the generator:
A)
Complies with 35 Ill. Adm. Code 725.271,
725.272 and 725.273(a); and
B)
marks the generator’s containers either with
the words
“Hazardous Waste” or with other
words that identify the contents of the
containers.
2)
A generator who accumulates either hazardous waste
or acutely hazardous waste listed in 3S Ill. Adm.
Code 721.133(e)
in excess of the amounts listed in
subsection
(c) (1) at or near any point of
generation must, with respect to that amount of
excess waste,
comply within three days with
subsection
(a)
on
other
applicable
provisions
of
this
chapter.
During the three day period the
generator
must
continue to comply with subsection
(c)
(1).
The
generator
must
mark the container
holding the excess accumulation of hazardous waste
with the date the excess amount began
accumulating.
d)
A generator who generates greater than 100 kilograms
but less than 1000 kilograms of hazardous waste in a
121—249
101
calendar month may accumulate hazardous waste on—site
for
180
days
or
less
without a permit on without having
interim
status
provided
that:
1)
The
quantity
of
waste
accumulated
on—site
never
exceeds
6000
kilograms;
2)
The
generator
complies
with
the
requirements
of 35
Ill.
Adm.
Code
725.Subpart
I,
except
the
genenator
need
not
comply
with
35
111.
Adm.
Code
725.276;
3)
The generator complies with the requirements of 35
Ill.
Adin.
Code 72S.301;
4)
The
generator
complies
with the requirements of
subsections
(a) (2) and
(a) (3) and the requirements
of 35
Ill. Adm. Code 72S.Subpart C; and
5)
The
generator complies with the following
requirements:
A)
At all times there must be at least one
employee
either
on the premises or on call
(i.e.,
available
to
respond
to
an
emergency
by reaching the facility within
a short
period of time) with the responsibility for
coordinating all emergency response measures
specified in subsection
(d) (4) (D).
The
employee is the emergency coordinator.
B)
The generator shall post the following
information next to the telephone:
i)
The name and telephone number of the
emergency coordinator:
ii)
Location of fine extinguishers and spill
control
material,
and
if present,
fire
alarm:
and
iii)
The telephone number of the fine
department,
unless
the facility has a
direct
alarm.
C)
The generator shall ensure that all employees
are thoroughly familiar with properwaste
handling and emergency procedures, relevant
to their responsibilities during normal
facility operations and emergencies:
D)
The emergency coordinator or designee shall
respond to any emergencies that arise.
The
121—250
102
applicable responses are as follows:
i)
In
the
event
of
a
fire, call the fine
department
or
attempt to extinguish it
using a fire extinguisher:
ii)
In the event
of
a spill, contain the
flow of hazardous waste to the extent
possible,
and
as
soon
as
is
practicable,
clean
up
the
hazardous
waste
and
any
contaminated
materials
or
soil:
iii)
In the event of a fire, explosion or
other
release
which
could
threaten
human
health outside the facility on when the
generaton has knowledge that a spill has
reached surface water,
the generator
shall immediately notify the National
Response Center
(using its 24—hour toll
free number
800/424—8802).
The
report
must include the following information:
the name, address and USEPA
identification number
(35 Ill.
Adm. Code
722.112) of the generator;
date, time
and type of incident (e.g.,
spill or
fine); quantity and type of hazardous
waste
involved
in
the
incident;
extent
of injuries,
if any; and, estimated
quantity and disposition of recoverable
materials,
if
any.
e)
A
generator
who
generates
greater
than 100
kilograms
but
less than 1000 kilograms of hazardous waste
in a
calendar
month
and who must transport the waste, or
offer the waste for transportation,
over a distance of
200 miles on more for off—site treatment,
storage on
disposal may accumulate hazardous waste on—site for 270
days or less without a permit or without having interim
status provided that the generator complies with the
requirements of subsection
(d).
f)
A generator who generates greaten than 100 kilograms
but
less
than
1000
kilograms of hazardous waste in
a
calendar
month
and
who accumulates hazardous waste in
quantities exceeding 6000 kg or accumulates hazardous
waste for more than 180 days (or for more than 270 days
if the generator must transport the waste, or offer the
waste for transportation, over a distan~ceof 200 miles
on more)
is an operator of a storage facility and is
subject to the requirements of 3S
Ill. Adm. Code 724
and 725 and the permit requirements of 35
Ill. Adm.
Code 703 unless the generator has been granted an
12 1—251
103
extension to the 180-day (or
270—day
if
applicable)
period.
If hazardous wastes must remain on—site for
longer
than
180
days
(on
270
days
if applicable)
due to
unforeseen,
temporary
and
uncontrollable
circumstances,
the
generator
may
seek
an
extension
of
up
to
30 days by
means
of
variance
on
provisional
variance
pursuant
to
Section
37
of
the
Environmental
Protection
Act.
(Source:
Amended
at
15
Ill.
Reg.
,
effective
12 1—252
104
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER
c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 724
STANDARDS FOR OWNERS
AND
OPERATORS
OF
HAZARDOUS
WASTE
TREATMENT, STORAGE
AND
DISPOSAL FACILITIES
SUBPART A:
GENERAL PROVISIONS
Purpose, Scope and Applicability
Relationship to Interim Status Standards
SUBPART
B:
GENERAL
FACILITY STANDARDS
Applicability
Identification Number
Required Notices
General Waste Analysis
Security
General Inspection Requirements
Personnel Training
General Requirements for Ignitable, Reactive or
Incompatible Wastes
724.118
Location Standards
SUBPART C:
PREPAREDNESS
AND
PREVENTION
Applicability
Design and Operation of Facility
Required Equipment
Testing and Maintenance of Equipment
Access to Communications or Alarm System
Required Aisle Space
Arrangements with Local Authorities
SUBPART
D: CONTINGENCY
PLAN
AND EMERGENCY PROCEDURES
Section
724.150
Applicability
724.151
Purpose and Implementation of Contingency Plan
724.1S2
Content of Contingency Plan
724.153
Copies
of
Contingency
Plan
724.154
Amendment of Contingency Plan
724.155
Emergency Coordinator
724.156
Emergency Procedures
SUBPART
E:
MANIFEST SYSTEM, RECORDKEEPING
AND REPORTING
Section
Applicability
Use of Manifest System
Manifest Discrepancies
Operating Record
Availability, Retention and Disposition of Reconds
Section
724
.
101
724. 103
Section
724.110
724.111
724. 112
724. 113
724. 114
724.115
724.116
724.117
Section
724.130
724.131
724.132
724.133
724.134
724.135
724.137
724.170
724.171
724.172
724.173
724.174
12 1—253
105
724.
175
724.176
724.
177
Section
724.
190
724.191
724.
192
724.
193
724.194
724.195
724.196
724.197
724.198
724.199
724 .200
724.201
Annual
Report
Unmanifested Waste Report
Additional
Reports
SUBPART
F:
RELEASES FROM SOLID WASTE MANAGEMENT UNITS
Applicability
Required
Programs
Groundwater
Protection
Standard
Hazardous
Constituents
Concentration
Limits
Point
of
Compliance
Compliance Period
General Groundwater Monitoring Requirements
Detection Monitoring Program
Compliance Monitoring Program
Corrective Action Program
Corrective Action for Solid Waste Management Units
SUBPART G:
CLOSURE AND POST-CLOSURE
Applicability
Closure
Performance
Standard
Closure
Plan;
Amendment
of
Plan
Closure;
Time
Allowed For Closure
Disposal or Decontamination of Equipment,
Structures
and Soils
Certification of Closure
Survey Plat
Post—closure Care and Use of Property
Post—closure Plan; Amendment of Plan
Post—closure Notices
Certification of Completion of Post—closure Care
SUBPART H:
FINANCIAL REQUIREMENTS
Applicability
Definitions of Terms As Used In This Subpart
Cost Estimate for Closure
Financial Assurance for Closure
Cost Estimate for Post—closure Care
Financial
Assurance
for
Post—closure
Care
Use of a Mechanism for Financial Assurance of Both
Closure
and
Post—closure
Cane
Liability Requirements
Incapacity of Owners or Operators, Guanantors. or
Financial
Institutions
724.251
Wording of the Instruments
SUBPART
I:
USE AND MANAGEMENT OF CONTAINERS
Section
724.270
Applicability
Section
724 .210
724.211
724 .212
724.
2 13
724.
2 14
724.215
724.216
724.
217
724.218
724.219
724.220
Section
724.240
724.241
724.242
724.243
724.244
724.245
724.246
724. 247
724.248
121—254
106
Condition
of
Containers
Compatibility
of
Waste
With
Container
Management of Containers
Inspections
Containment
Special
Requirements
for
Ignitable
on
Reactive
Waste
Special
Requirements
for
Incompatible
Wastes
Closure
SUBPART
J:
TANK
SYSTEMS
Applicability
Assessment of Existing Tank System’s Integrity
Design
and
Installation
of
New
Tank
Systems
or
Components
Containment and Detection of Releases
General
Operating
Requirements
Inspect
ions
Response
to
Leaks
or
Spills
and
Disposition
of
or
unfit—for—use
Tank
Systems
Closure
and
Post—Closure
Care
Special
Requirements
for
Ignitable
or
Reactive
Waste
Special Requirements for Incompatible Wastes
Special Requirements for Hazardous Wastes FO2O,
FO21,
F022,
F023,
F026
and
F027
SUBPART
K:
SURFACE
IMPOUNDMENTS
Applicability
Design and Operating Requirements
Double—lined
Surface
Impoundments:
Exemption
from
Subpart F: Ground—water Protection Requirements
(Repealed)
Monitoring
and
Inspection
Emergency
Repairs;
Contingency
Plans
Closure and Post—closune Care
Special
Requirements
for
Ignitable
or
Reactive
Waste
Special
Requirements
for
Incompatible
Wastes
Special Requirements for Hazardous Wastes F020,
F021,
F022,
FO23, FO26 and FO27
SUBPART
L:
WASTE
PILES
Section
724.3S0
Applicability
724.3S1
Design
and
Operating
Requirements
724.352
Double-lined
Piles:
Exemption
from
Subpart
F:
water Protection Requirements (Repealed)
724.353
Inspection
of
Liners:
Exemption
from
Subpart
F:
Ground—water Protection Requirements
(Repealed)
Monitoring
and
Inspection
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
724 .271
724.272
724.273
724.274
724 .275
724.276
724.277
724.278
Section
724.290
724.291
724.292
724.293
724.294
724 .295
724.296
724.297
724
.
298
724. 299
724.300
Section
724.320
724.321
724.322
724.326
724
.
327
724.328
724.329
724. 330
724.331
Leaking
724
.
3S4
724.356
724.357
Ground
—
121—255
107
724.358
724.359
Section
724.370
724.371
724.372
724.373
724.376
724.378
724.379
724.380
724.381
724. 382
724. 383
Section
724.400
724.401
724.402
724.403
724.409
724.410
724.412
724.413
724.414
724.415
724.416
724.417
Section
724.440
724.441
724.442
724.443
724.444
724.44S
724.447
724.451
Section
724.
701
724.701
Closure
and
Post—closure
Care
Special Requirements for Hazardous Wastes F020,
FO21,
F022,
FO23, F026 and F027
SUBPART M:
LAND
TREATMENT
Applicability
Treatment
Program
Treatment
Demonstration
Design
and
Operating
Requirements
Food—chain
Crops
Unsaturated
Zone
Monitoring
Recondkeep ing
Closure
and
Post—closure
Care
Special
Requirements
for
Ignitable
on
Reactive
Waste
Special Requirements for Incompatible
Wastes
Special Requirements for Hazardous Wastes F020,
F02l,
F022, F023,
F026 and FO27
SUBPART N:
LANDFILLS
Applicability
Design
and
Operating
Requirements
Double-lined Landfills:
Exemption from Subpart F:
Ground—water Protection Requirements
(Repealed)
Monitoring and Inspection
Surveying and Recondkeeping
Closure and Post—closure Cane
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Special Requirements for Bulk and Containerized Liquids
Special Require:nents for Containers
Disposal of Small Containers of Hazardous Waste in
Overpacked Drums
(Lab Packs)
Special Requirements for Hazardous Wastes FO2O,
F02l,
FO22, FO23,
FO26 and F027
SUBPART .0:
INCINERATORS
Applicability
Waste Analysis
Principal Organic Hazardous Constituents (POHC5)
Performance Standards
Hazardous Waste Incinerator Permits
Operating Requirements
Monitoring and Inspections
Closure
SUBPART X:
MISCELLANEOUS UNITS
Applicability
Environmental Performance Standards
12 1—246
108
724.702
Monitoring, Analysis, Inspection, Response, Reporting
and
Connective
Action
724.703
Post—closure
Care
Section
724.930
724.931
724.932
724.933
724.934
724.935
724.936
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS VENTS
Applicability
Definitions
Standards:
Process Vents
Closed—vent Systems and Control Devices
Test methods and procedures
Recondkeepinci requirements
Reporting Rrequirements
SUBPART BB:
AIR EMISSION STANDARDS FOR EOUIPMENT LEAKS
Applicability
Pumps in Light Liquid Service
Compressors
Standards:
Pressure Relief Devices in Gas/Vapor
Service
Standards:
Sampling Connecting Systems
Standards:
Open-ended Valves on Lines
Standards:
Valves in Gas/Vapor or Light Liquid Service
Standards:
Pumps, Valves, Pressure Relief Devices and
Other Connectors
Standards:
Delay of Repair
Standards:
Closed—vent Systems and Control Devices
Alternative Percentage Standard for Valves
Skip Period Alternative for Valves
Test Methods and Procedures
Recordkeeping Requirements
Reporting Requirements
Appendix A
Appendix
B
Appendix
D
Appendix
E
Appendix
I
Recordkeeping Instructions
EPA Report Form and Instructions (Repealed)
Cochran’s Approximation to the Behrens—Fisher
Student’s T-Test
Examples of Potentially Incompatible Waste
Groundwater Monitoring List
AUTHORITY:
Implementing Section
22.4
and authorized by Section
27 of the Environmental Protection Act
(Ill.
Rev.
Stat.
1989,
ch.
111 1/2, pars.
1022.4 and 1027).
SOURCE:
Adopted in R82-l9,
53
PCB
131,
at
7
Ill.
Reg.
14059,
effective October 12,
1983; amended in R84-9 at 91ll.
Reg.
11964, effective July 24,
1985; amended in R85—22 at 10
Ill.
Reg.
1136, effective January
2,
1986; amended
in R86—l
at 10
Ill.
Reg.
14119, effective August
12,
1986; amended in R86—28 at 11 Ill.
Reg.
6138, effective March 24,
1987; amended in R86—28 at 11 Ill.
Definitions
Standards:
Section
724.9S0
724.951
724.952
724 .953
724 .954
724.9SS
724.956
724.957
724.958
724.959
724.960
724.961
724.962
724.963
724.964
724.965
121—257
109
Reg. 8684,
effective April 21,
1987; amended in R86—46 at 11
Ill.
Reg.
13577,
effective
August
4,
1987;
amended
in
R87—5
at
11
Ill.
Reg.
19397, effective November. 12,
1987; amended in R87-39 at
12
Ill.
Reg.
13135,
effective
July
29,
1988; amended in R88—16 at 13
Ill.
Reg.
458,
effective
December
28,
1988;
amended
in R89—1 at
13 Ill. Reg.
18527, effective November 13,
1989; amended in R90-
2
at
14
Ill.
Reg.
14S11,
effective
August
22,
1990;
amended in
R90—1O at 14 Ill.
Reg.
16658, effective September 25,
1990;
amended in R90-11 at 15 Ill. Reg.
effective
SUBPART
B:
GENERAL
FACILITY
STANDARDS
Section
724.113
General
Waste
Analysis
a)
Analysis:
1)
Before an owner or operator treats,
stones on
disposes of any hazardous waste, or non—hazardous
waste if applicable under Section 724.213(d), the
owner
on
operator
shall
obtain
a
detailed
chemical
and
physical
analysis
of
a
representative
sample
of the waste.
At a minimum, this analysis must
contain
all
the
information
which must be known to
treat, store or dispose of
the
waste in accordance
with the requirements of this Part or
35
Ill.
Adm.
Code
728,
or with the conditions of a permit
issued under 35 Ill.
Adm. Code 702, 703 and 705.
2)
The analysis may include data developed under 35
Ill. Adm. Code 721,
and
existing published or
documented data on the hazardous waste on on
hazardous waste generated from similar processes.
BOARD NOTE:
For example, the facility’s records
of analyses performed on the waste before the
effective date of these regulations, or studies
conducted on hazardous waste generated from
processes similar to that which generated the
waste to be managed at the facility, may be
included in the data base required to comply with
subsection
(a) (1).
The owner on operator of an
off-site facility may arrange for the generator of
the hazardous waste to supply part or all of the
information required by subsection
(a)(1), except
as otherwise specified in 35 Ill.
Adm. Code
728.107(b)
and
(c).
If
the
generator
does not
supply the information, and the owner on operator
chooses to accept a hazardous waste, the owner or
operator is responsible for obtaining the
information required to comply with this Section.
121—248
110
3)
The analysis must be repeated as necessary to
ensure that it is accurate and up to date.
At a
minimum, the analysis must be repeated:
A)
When the owner or operator is
notified,
or
has reason to believe, that the process or
operation generating the hazardous waste, or
non—hazardous waste if applicable under
Section
724.213(d),
has
changed;
and
B)
For off-site facilities, when the results of
the inspection required in subsection
(a) (4)
indicate
that
the
hazardous
waste
received
at
the facility does not match the waste
designated on the accompanying manifest or
shipping paper.
4)
The
owner
or operator of an off-site facility
shall
inspect and,
if necessary,
analyze each
hazardous waste movement received at the facility
to determine whether it matches the identity of
the
waste specified on the accompanying manifest
on shipping paper.
b)
The owner or operator shall develop and follow a
written waste analysis plan which describes the
procedures which it will carry out to comply with
subsection
(a).
The owner or operator shall keep this
plan at the facility.
At a minimum, the plan must
specify:
1)
The parameters for which each hazardous waste, or
non-hazardous waste if applicable under Section
724.213(d), will be analyzed and the rationale for
the
selection
of these parameters
(i.e., how
analysis for these parameters will provide
sufficient information on the waste’s properties
to comply with subsection
(a)).
2)
The test methods which will be used to test for
these parameters.
3)
The sampling method which will be used to obtain
a
representative sample of the waste to be analyzed.
A representative sample may be obtained using
either:
A)
One of the sampling methods described in 3S
Ill.
Adm. Code 721.Appendix A;
on
B)
An equivalent sampling method.
121—259
il~
BOARD NOTE:
See 35
Ill. Adm. Code 720.121
for
related
discussion.
4)
The
frequency
with
which
the
initial
analysis
of
the
waste
will
be
reviewed
or
repeated to ensure
that
the
analysis is accurate and up to date.
5)
For
off-site
facilities,
the
waste
analyses
that
hazardous
waste
generators
have
agreed
to
supply.
6)
Where
applicable,
the
methods
which
will
be
used
to meet the additional waste analysis requirements
for specific waste management methods as specified
in Sections 724.117, 724.414~and 724.441~
724.934(d) and 724.963(d), and 35 Ill.
Adm. Code
728.107.
And,
7)
For
surface
impoundments
exempted
from
land
disposal restrictions under 35 Ill. Adm. Code
728.104(a),
the
procedures and schedules for:
A)
The
sampling
of
impoundment
contents;
B)
The
analysis
of test data; and,
C)
The annual removal of residues which are not
delisted under 35 Ill. Adm. Code 720.122 or
which exhibit a characteristic of hazardous
waste, and either:
i)
Do not meet applicable treatment
standards of 3S Ill.
Adm. Code
728.Subpart D; or
ii)
Where no treatment standards have been
established:
Such residues are
prohibited
from
land
disposal
under
35
Ill.
Adm.
Code
728.132
on
728.139;
or
such residues are prohibited from land
disposal under 35
Ill. Adm. Code
728.133(f).
c)
For off—site facilities,
the waste analysis plan
required in subsection
(b) must also specify the
procedures which will be used to inspect and,, if
necessary,
analyze each movement of hazardous waste
received at the facility to ensure
that’S it matches the
identity of the waste designated on the accompanying
manifest or shipping paper.
At a minimum, the plan
must describe:
12 1—260
112
1)
The procedures which will be used to determine the
identity of each movement of waste managed at the
facility;
and
2)
The sampling method which will be used to obtain a
representative
sample
of
the
waste
to
be
identified,
if
the
identification
method
includes
sampling.
BOARD NOTE:
35
Ill.
Adm.
Code
703,
requires
that
the waste analysis plan be submitted with Part B
of the permit application.
(Source:
Amended at 15 Ill.
Reg.
,
effective
Section 724.115
General Inspection Requirements
a)
The owner or operator shall conduct inspections often
enough to identify problems in time to connect them
before they harm human health on the environment.
The
owner on operator shall inspect the facility for
malfunctions and deterioration, operator errors and
discharges which may be causing, on may lead to:
1)
Release of hazardous waste constituents to the
environment; on
2)
A threat to human health.
b)
Inspection schedule.
1)
The owner on operator shall develop and follow
a
written schedule fon inspecting monitoring
equipment, safety and emergency equipment,
security devices and operating and structural
equipment (such as dikes and suinp pumps)
that are
important to preventing, detecting or responding
to environmental on human health hazards.
2)
The owner on operator shall keep this schedule at
the facility.
3)
The
schedule
must
identify
the
types of problems
(e.g., malfunctions or deterioration) which are to
be looked for during the inspection
(e.g.,
inoperative sump pump,
leaking fitting, eroding
dike, etc.).
4)
The frequency of inspection may vary for the items
on the schedule.
However,
it should be based on
the
nate
of
possible
deterioration
of
the
121—261
113
equipment
and
the
probability
of
an
environmental
on
human
health
incident
if
the
deterioration,
malfunction
on
any
operator
error
goes
undetected
between
inspections.
Areas
subject
to
spills,
such
as
loading’
and
unloading
areas,
must
be
inspected
daily
when
in
use.
At
a
minimum,
the
inspection
schedule
must
include
the
terms
and
frequencies called for in Sections 724.274,
724.294,
724.326,
724.353,
724.354,
724.403,
724.447~ and
724.702,
724.933.
724.952,
724.953
and
724.958,
where
applicable.
BOARD
NOTE:
35
Ill.
Adm.
Code
703
requires
the
inspection
schedule
to
be
submitted
with
Part
B
of
the
permit
application.
The
Agency
will
evaluate
the
schedule
along
with
the
nest
of
the
application
to
ensure
that
it
adequately
protects
human
health
and
the
environment.
As
part
of
this
review,
the
Agency
may
modify
or
amend
the
schedule as may be necessary.
c)
The
owner
or
operator
shall
remedy
any
deterioration
or
malfunction
of
equipment
on
structures
which
the
inspection
reveals
on
a
schedule
which
ensures
that
the
problem
does
not
lead
to
an
environmental
or
human
health
hazard.
Where
a
hazard
is
imminent
or
has
already
occurred,
remedial
action
must
be
taken
immediately.
d)
The
owner
or
operator
shall
record
inspections
in
an
inspection
log
or
summary.
The
owner
or
operator
shall
keep
these
recc~-ds for
at
least
three
years
from
the
date of inspection.
At a minimum, these records must
include
the
date
and
time
of
the
inspection,
the
name
of
the
inspector,
a
notation
of
the
observations
made
and
the
date
and
nature
of
any
repairs
or
other
remedial actions.
(Source:
Amended
at
15
Ill.
Reg.
effective
SUBPART E:
MANIFEST
SYSTEM, RECORDKEEPING AND REPORTING
Section 724.173
Operating Record
a)
The owner on operator shall keep a written operating
record at the facility.
b)
The following information must be recorded,
as
it
becomes available,
and maintained in the operating
record until closure of the facility:
12 1—262
114
1)
A
description
and
the
quantity
of
each
hazardous
waste received, and the methodon methods and date
or dates of its treatment,
storage on disposal at
the facility as required by Appendix A;
2)
The location of each hazardous waste within the
facility and the quantity at each location.
For
disposal facilities, the location and quantity of
each hazardous waste must be recorded on a map or
diagram of each cell or disposal area.
For all
facilities, this information must include cross—
references to specific manifest document numbers,
if the waste was accompanied by
a manifest;
BOARD NOTE:
See Section 724.219 for related
requirements.
3)
Records and results of waste analyses performed as
specified in Sections 724.113, 724.117, 724.4l4~
and 724.441,
724.934, 724.963, and in 35 Ill.
Adm.
Code 728.104(a)
and 728.107;
4)
Summary reports and details of all incidents that
require implementing the contingency plan as
specified in Section 724.156(j);
5)
Records and results of inspections as required by
Section 724.115(d)
(except these data need to be
kept only three years);
6)
Monitoring, testing or analytical data and
corrective action where required by Subpart F on
Sections 724.326, 724.353,
724.354, 724.376,
724.378,
724.380, 724.403,
724.409, 724.447~e~
724.702.
724.934(c)
through
(f), 724.935.
724.963(d) through (U
on 724.964.
7)
For off—site facilities, notices to generators as
specified in Section 724.112(b);
8)
All closure cost estimates under Section 724.242
and, for disposal facilities,
all post—closure
cost estimates under Section 724.244;
9)
A certification by the permittee, no less often
than annually: that the penmittee has a program in
place to reduce the volume and toxicity of
hazardous waste that the penmittee generates, to
the degree the penmittee determines to be
economically practicable; and that the proposed
method of treatment, storage or disposal
is that
12 1—263
115
practicable
method
currently
available
to
the
penmittee
which
minimizes
the
poraentpresent
and
future
threat
to
human
health
and
the
environment;
10)
Records
of
the
quantities
(and
date
of
placement)
for
each
shipment
of
hazardous
waste
placed
in
land
disposal
units
under
an
extension
of
the
effective
date
of
any
land
disposal
restriction
granted
pursuant
to
35
Ill.
Adm.
Code
728.105,
a
petition
pursuant
to
35
Ill..
Adm.
Code
728.106
or
a
certification
under
35
Ill.
Adin.
Code
728.108,
and
the
applicable
notice
required
of
a
generator
under
35
Ill.
Adin.
Code
728.107(a);
11)
For
an
off-site
treatment
facility,
a
copy
of
the
notice,.
and
the
certification
and
demonstration,
if
applicable,
required
of
the
generator
or
the
owner
or
operator
under
35
Ill.
Adm.
Code
728.107
or
728.108;
12)
For
an
on-site
treatment
facility,
the
information
contained in the notice
(except the manifest
number),
and
the
certification
and
demonstration,
if
applicable,
required
of
the
generator
on
the
owner or operator under 35 Ill. Adm. Code 728.107
or
728.108;
13)
For
an
off—site
land
disposal
facility,
a
copy
of
the
notice,
and
the
certification
and
demonstration,
if
applicable,
required
of
the
generator
or
the
owner
on
operator
of
a
treatment
facility
under
35
Ill.
Adm.
Code
728.107
or
728.108,
whichever
is
applicable;
and
14)
For
an
on-site
land
disposal
facility,
the
information
contained
in
the
notice
required
of
the generator or owner or operator of a treatment
facility
under
35
Ill.
Adm.
Code
728.107,
except
for
the
manifest
number,
and
the
certification
and
demonstration if applicable,
required under 35
Ill.
Adm.
Code
728.108,
whichever
is
applicable.
15)
For
an
off-site
storage
facility,
a
copy
of
the
notice,
and
the
certification
and
demonstration
if
applicable,
required
of
the
generator
on
the
owner
on
operator
under
35
Ill.
Adm.
Code
728.107
or
728.108;
and,
16)
For
an
on-site
storage
facility,
the
information
contained in the notice
(except the manifest
number),
and the certification and demonstration
if applicable, required of the generator or the
121—264
116
owner on operator under 35 Ill. Adm. Code 728.107
or 728.108.
(Source:
Amended at 15 Ill.
Reg.
,
effective
Section 724.177
Additional Reports
In addition to submitting the annual report and unmanifested
waste
reports
described
in
Sections
724.175
and
724.176,
the
owner or operator mu3tshall also report to the Agency:
a)
Releases,
fires and explosions as specified in Section
724.1S6(j);
b)
Facility closures specified in Section 724.21S; and
c)
As otherwise required by Subparts
F and K
NF,
K through
N, AA and BB.
(Source:
Amended at 15 Ill. Reg.
effective
SUBPART
K:
SURFACE IMPOUNDMENTS
Section 724.321
Design and Operating Requirements
a)
Any sS-urface impoundment that it not covered by
subsection
(c)
or 35 Ill. Adm.
Code 72S.321 must have a
liner for all portions of the impoundment
(except for
existing portions of such impoundment).
The linen must
be designed, constructed and installed to prevent any
migration of wastes out of the impoundment to the
adjacent subsurface soil or
g-r-eu
rounthater or
surface water at any time during the active life
(including the closure period) of the impoundment.
The
liner may be constructed of materials that may allow
wastes to migrate into the linen
(but not into the
adjacent subsurface soil or g ou 4—wa
nou~,ç~ater
or
surface water) during the active life of the facility,
provided that the impoundment is closed in accordance
with Section 724.328(a)(l).
For impoundments that will
be closed in accordance with Section 724.328(a)(2). the
liner must be constructed of materials that can prevent
wastes from migrating into the liner during the active
life of the facility.
The liner must be:
1)
Constructed of materials that have~appropriate
chemical properties and sufficient strength and
thickness to prevent failure due to pressure
gradients (including static head and external
hydrogeologic forces), physical contact with the
12 1—265
117
waste or leachate to which they are exposed,
climatic conditions, the stress of installation
and
the
stress
of
daily
operation;
2)
Placed
upon
a
foundation
or
base
capable
of
providing
support
to
the
liner
and
resistance
to
pressure
gradients
above
and
below
the
linen
to
prevent
failure
of
the
liner
due
to
settlement,
compression
or
uplift;
and
3)
Installed
to
cover
all
surrounding
earth
likely
to
be
in
contact
with
the
waste
or
leachate.
b)
The
owner
or
operator
will
be
exempted
from
the
requirements
of
subsection
(a)
if
the
Board
finds,
based on a demonstration by the owner or operator,
in a
variance
and/on
site—specific
rulemaking,
that
alternate
design
and
operating
practices, together with
location
characteristics,
will
prevent
the
migration
of
any
hazardous
constituents
(see
Section
724.193)
into
the
~
on surface water at any
future
time.
In
deciding
whether
to
grant
an
exemption,
the
Board
will
consider:
1)
The
nature
and
quantity
of
the
wastes;
2)
The
proposed
alternate
design
and
operation;
3)
The
hydrogeologic
setting
of
the
facility,
including
the
attenuative
capacity
and
thickness
of
the
linens
and
soils
present
between
the
impoundment
and
g±~e8—wa
eroundwae~
or
surface
water;
and
4)
All
other
factors
which
would
influence
the
quality
and
mobility
of
the
leachate
produced
and
the potential for it to migrate to ground-
wat-e~groundwat~r
or
surface
water.
c)
The
owner
on
operator
of
each
new
surface
impoundment,
each
new
surface
impoundment
unit
at
an
existing
facility,
each
replacement
of
an
existing
surface
impoundment unit and each lateral expansion of an
existing
surface
impoundment
unit,
must
install
two
on
more
liners
and
a
leachate
collection
system
between
such
linens.
The
liners
and
leachate
collection
system
must
protect
human
health
and
the
environment.
The
requirements of this subsection shall apply with
respect to all waste received after the issuance of the
permit
for
units
where
Pant
B
of
the
permit
ap~1ication
is received by the Agency on USEPA after November 8,
1984.
The requirement for the installation of two or
121—266
118
more
liners
in
this
subsection
may
be
satisfied
by
the
installation
of
a
top
liner
designed~
operated
and
constructed
of
materials
to
prevent
the
migration
of
any
constituent
into
such
liner
during
the
period
such
facility
remains
in
operation
(including
any
post-
closure
monitoring
period),
and
a
lower
liner
designed,
operated
and
constructed
to
prevent
the migration of
any constituent through such linen during
such
period.
For
the
purpose
of
the
preceding
sentence,
a
lower
liner shall be deemed to satisfy such requirement if it
is
constructed
of
at
least
a
3-foot
thick
layer
of
recompacted clay or other natural material with a
permeability of no more than 1
x 10~’centimeter pen
second.
d)
Subsection
(c) will not apply if
the
owner
or
operator
demonstrates to the Agency and the Agency
finds
for
such surface impoundment, that alternative design and
operating
practices,
together with location
characteristics, will prevent the migration of any
hazardous
constituent
into
the
g-~eun8—wate~gro3,n~,w.~ç,
or
surface
water
at
least
as
effectively
as
such
liners
and leachate collection systems.
e)
The
double
linen requirement set forth in subsection
(c) may be waived by the Agency
for
any
monofill,
if:
1)
The monofill contains only hazardous wastes from
foundry furnace emission controls or metal casting
molding sand, and such wastes do
not
contain
constituents which would
render
the
wastes
hazardous for reasons other than the E~P—toxicity
charactenistic~in 3S
Ill. Adm. Code 721.124; ~
2)
Design and location.
A)
Liner,
location and groundwater monitoring.
i)
The monofill has at
least
one
linen
for
which there is no evidence that such
linen is leaking.
For
the
purposes
of
this
subsection,
the
term
“linen”
means
a linen designed, constructed,
installed
and operated to prevent hazardous waste
from passing into the liner at any time
during the active life of the facility,
or a liner designed, constructed,
installed and operated to
prevent
hazardous waste from migrating beyond
the liner to adjacent subsurface
soil,
groundwater or surface water at any time
during the active life of the facility.
121—267
119
In the case of any surface impoundment
which has been exempted from the
requirements of subsection
(c) on the
basis of a linen designed, constructed,
installed and operated to prevent
hazardous waste from passing beyond the
liner, at the closure of such
impoundment, the owner or operator must
remove or decontaminate all waste
residues, all contaminated liner
material and contaminated soil to the
extent practicable.
If all contaminated
soil is not removed or decontaminated,
the owner or operator of such
impoundment will comply with appropriate
post—closure requirements,
including but
not limited to groundwater monitoring
and corrective action;
ii)
The monofill is located more than one-
quarter mile from an underground source
of drinking water
(as that term is
defined in 35
Ill. Adm. Code 702.110 and
iii)
The monofill is in compliance with
generally applicable ground
wg~ur~~~
monitoring requirements
for facilities with permits or
B)
RCRA
The owner or operator demonstrates to the
Board that the monofill is located, designed
and operated so as to assure that there will
be no migration of any hazardous constituent
into g~eun8—w
e~g,çiç,,~te~-
on surface water
at any future time.
f)
A surface impoundment must be designed, constructed,
maintained and operated to prevent overtopping
resulting from normal or abnormal operations;
ovenfilling; wind and wave action; rainfall; run-on;
malfunctions of level controllers, alarms and other
equipment; and human error.
g)
A surface impoundment must have dikes that are
designed, constructed and maintained with sufficient
structural integrity to prevent massive’ failure of the
dikes.
In ensuring structural integrity,
it must not
be presumed that the liner system will function without
leakage during the active life of the unit.
121—268
120
h)
The Agency will specify in the permit all design and
operating practices that are necessary to ensure that
the requirements of this Section are satisfied.
(Source:
Amended at 15
Ill. Reg.
effective
Section 724.329
Special Requirements for Ignitable or
Reactive Waste
Ignitable or reactive waste must not be placed in a surface
impoundment, unless the waste and impoundment satisfy all
applicable requirements of
35 Ill. Adm. Code 728,
and:
a)
The waste is treated, rendered on mixed before or
immediately after placement in the impoundment so that:
1)
The resulting waste, mixture on dissolution of
material no longer meets the definition of
ignitable or reactive waste under 35 Ill.
Adin.
Code 721.121 or 721.123; and
2)’
Section 724.117(b)
is complied with; or
b)
The waste is managed in such a way that it is protected
from any material or conditions which may cause
it to
ignite on react;
or
c)
The surface impoundment is used solely for emergencies.
(Source~: Amended at 15
Ill.
Reg.
effective
SUBPART L:
WASTE PILES
Section 724.3S6
Special Requirements for Ignitable or
Reactive Waste
Ignitable or reactive waste must not be placed in a waste pile,
unless the waste and waste pile satisfy all applicable
requirements of 35
Ill.
Adrn. Code 728,
and:
a)
The waste is treated,
rendered on mixed before or
immediately after placement in the pile so that:
1)
The resulting waste, mixture or dissolution of
material no longer meets the definition of
ignitable or reactive waste under ~35Ill. Adm.
Code 721.121 on 721.123; and
2)
Section 724.117(b)
is complied with; or
121—269
121
b)
The waste is managed in such a way that it is protected
from any material on conditions which may cause it to
ignite or react.
(Source:
Amended at 15 Ill. Reg.
,
effective
SUBPART
N:
LAND
TREATMENT
Section 724.381
Special Requirements for Ignitable or
Reactive Waste
The owner or operator must not apply ignitable or reactive waste
to the treatment zone, unless the waste and and the treatment
zone satisfy all applicable requirements of 35 Ill. Adm. Code
728,
and:
a)
The waste is immediately incorporated into the soil so
that:
1)
The resulting waste, mixture or dissolution of
material no longer meets the definition of
ignitable on reactive waste under 35 Ill.
Adm.
Code 721.121 on 721.123; and
2)
Section 724.117(b)
is complied with; or
b)
The waste is managed in such a way that it is protected
from any material on conditions which may cause it to
ignite on react.
(Source:
Amended at 15 Ill. Reg.
,
effective
SUBPART N:
LANDFILLS
Section 724.401
Design and Operating Requirements
a)
Any landfill that is not covered by subsection
(c) or
35 Ill.
Adm. Code 725.401(a) must have a liner system
for all portions of the landfill
(except for existing
portions of such landfill).
The linen system must
have:
1)
A linen that is designed, constructed and
installed to prevent any migration of wastes out
of the landfill to the adjacent subsurface soil on
groundwater or surface water at any time during
the active life (including the closure period) of
the landfill.
The liner must be constructed of
materials that prevent wastes from passing into
the liner during the active life of the facility.
12 1—270
122
The liner must be:
A)
Constructed of materials that have
appropriate chemical properties and
sufficient strength and thickness to prevent
failure due to pressure gradients (including
static head and external hydrogeologic
forces), physical contact with the waste or
leachate to which they are exposed, climatic
conditions, the stress of installation and
the stress of daily operation;
B)
Placed upon a foundation on base capable of
providing support to the liner and resistance
to pressure gradients above and below the
liner to prevent failure of the liner due to
settlement,
compression or uplift; and
C)
Installed to cover all surrounding earth
likely to be
in contact
with the .waGte or
leachate; and
2)
A leachate collection and removal system
immediately above the liner that is designed,
constructed, maintained and operated to collect
and remove leachate from the landfill.
The Agency
will specify design and operatThg conditions in
the permit to ensure that the leachate depth over
the liner does not exceed 30 cm (one foot).
The
leachate collectic~n
and
removal system must be:
A)
Constructed of materials that are:
i)
Chemically resistant to the waste
managed in the landfill and the leachate
expected to be generated; and
ii)
Of sufficient strength and thickness to
prevent collapse under the pressures
exer~iedby overlying wastes, waste cover
materials and by any equipment used at
the landfill; and
B)
Designed and operated to function without.
clogging through the scheduled closure of the
landfill.
b)
The owner or operator will be exempted from the
requirements of subsection
(a)
if the Board finds,
based on a demonstration by the owner or operator,
in a
variance and/or site—specific rulemaking,
that alter-
native design and operating practices, together with
12 1—27 1
123
location characteristics, will prevent the migration of
any hazardous constituents
(see Section 724.193) into
the groundwater on surface water at any future time.
In deciding whether to grant an exemption,
the Board
will consider:
1)
The nature and quantity of the wastes;
2)
The proposed alternate design and operation;
3)
The hydnogeologic setting of the facility,
including the attenuative capacity and thickness
of the linens and soils present between the
landfill and groundwater or surface water; and
4)
All other factors which would influence the
quality and mobility of the leachate produced and
the potential ‘for it to migrate to groundwater on
surface water.
c)
The owner or oprator of each new landfill, each new
landfill unit at an existing facility, each replacement
of an existing landfill unit and each lateral expansion
of an existing landfill unit, must install two on more
linens and a leachate collection system above and
between the liners.
The liners and leachate collectipn
systems must protect human health and the environment.
This subsection applies with respect to all waste
received after issuance of the permit for units where
Part B of the permit application is received by the
Agency on USEPA after November 8,
1984.
The
requirement for the installation of two or more linens
in this subsection may be satisfied by the installation
of a top linen designed, operated and constructed of
materials to prevent the migration of any constituent
into such liner during the period such facility remains
in operation (including any post—closure monitoring
period), and a lower liner designed, operated and
constructed to prevent the migration of any constituent
through such linen during such period.
For the
purpose
of the preceding sentence, a lower liner shall be
deemed to satisfy such requirement
if it is constructed
of at least a 3—foot thick layer of recompacted clay or
other natural material with a permeability of no more
than
1 x 10~centimeter per second.
d)
Subsection
(c) will not apply if the owner on operator
demonstrates to the Agency, and the Agency finds for
such landfill, that alternative design and operating
practices, together with location characteristics,
will
prevent the migration of any hazardous constituent into
the groundwater or surface water at least as
121—272
124
effectively as such liners and leachate collection
systems.
e)
The double liner requirement set forth in subsection
(c) be waived by the Agency for any monofill,
if:
1)
The monofill contains only hazardous wastes from
foundry furnace emission controls or metal casting
molding sand, and such wastes do not contain
constituents which would render the wastes
hazardous for reasons other than the toxicity
characteristic in 35 Ill.
Adju.
Code 721.124, with
USEPA hazardous waste numbers D004 through DOll;
and
2)
No migration demonstration.
A)
Design and location requirements.
i)
The nionofill has at least one linen for
which there is no evidence that such
liner is leaking.
ii)
The monofill
is located more than one-
quarter mile from an underground source
of drinking water
(as that term is
defined in 35 Ill. Adm. Code 702.110.
iii) The monofill is in compliance with
generally applicable groundwater
monitoring requirements for facilities
with
RCRA
permits; on
B)
The owner or operator demonstrates to the
Board that the monofill is located, designed
and operated so as to assure that there will
be no migration of any hazardous constituent
into groundwater on surface water at any
future time.
f)
The owner on operator must design,
construct,
operate
and maintain a run—on control system capable of
preventing flow onto the active portion of the landfill
during peak discharge from at least a 25—year storm.
g)
The owner or operator must design, construct,
operate
and maintain a run—off management system to collect and
control at least the water volume resulting from a 24
hour,
25—year storm.
h)
Collection and holding facilities
(e.g., tanks on
basins)
associated with run—on and nun—off control
121—273
125
systems must be emptied or otherwise managed
expeditiously after storms to maintain design capacity
of the system.
1)
If the landfill contains any particulate matter which
may be subject to wind dispersal,
the owner or operator
must cover on otherwise manage the landfill to control
wind dispersal.
j)
The Agency will specify in the permit all design and
operating practices that are necessary to ensure that
the requirements of this Section are satisfied.
a)
b)
,
effective
Special Requirements for Ignitable on
Reactive Waste
(Source:
Amended at 15
Ill. Reg.
,
effective
(Source:
Amended at 15 Ill. Reg.
Section 724.412
Except as provided in paragraphsubsection
(b) and in
Section 724.416,
ignitable or reactive waste must not
be placed in a landfill, unless the waste and landfill
meet all applicable requirements of 35 Ill.
Adm. Code
728, and the waste is treated, rendered on mixed before
or immediately after placement in a landfill so that:
1)
The resulting waste, mixture on dissolution of
material no longer meets the definition of
ignitable or reactive waste under 35 Ill. Adm.
Code 721.121 or 721.123; and
2)
Section 724.117(b)
is complied with.
-lExcept for prohibited wastes which remain subiect to
treatment standards in 35 Ill. Mm. Code.Sub~artD,
jgnitable waste in containers may be landfilled without
meeting the requirements of paragraphsubsection
(a)
provided that the wastes are disposed of in such a way
that they are protected from any material or conditions
which may cause them to ignite.
At a minimum,
ignitable wastes must be disposed of in non-leaking
containers which are carefully handled and placed so as
to avoid heat,
sparks, rupture on any other condition
that might cause ignition of the wastes; must be
covered daily with soil or other non—combustible
material to minimize the potential for ignition of the
wastes; and must not be disposed of in cells that
contain on will contain other wastes which may generate
heat sufficient to cause ignition of the waste.
121—274
126
Section 724.416
Disposal of Small Containers of Hazardous
Waste in Overpacked Drums
(Lab Packs)
Small containers of hazardous waste in overpacked drums
(lab
packs) may be placed in a landfill if the following requirements
are met:
a)
Hazardous waste must be packaged in non—leaking inside
containers.
The inside containers must be of a design
and constructed of a material that will not react
dangerously with, be decomposed by or be ignited by the
contained waste.
The inside containers must be tightly
and securely sealed.
The inside containers must be of
the size and type specified in the Department of
Transportation
(DOT) hazardous materials regulations
(49 CFR 173,
178 and 179),
if those regulations specify
a particular inside container for the waste.
b)
The inside containers must be overpacked in an open
head DOT-specification metal shipping container (49 CFR
178 and 179)
of no more than 416 liter
(110 gallon)
capacity and surrounded by, at a minimum,
a sufficient
quantity of absorbent
material to completely absorb all
of the liquid contents of the inside containers.
The
metal outer container must be full after packing with
inside containers and absorbent material.
c)
In accordance with Section 724.117(b), the absorbent
material used must not be capable of reacting
dangerously with, being decomposed by or being ignited
by the contents of the inside containers.
d)
Incompatible waste,
as defined in 35
Ill.
Adm. Code
720.110, must not be placed in the same outside
container.
e)
Reactive wastes, other than cyanide— on sulfide—bearing
waste as defined in 35 Ill. Mm.
Code 721.123(a) (5),
must be treated or rendered non—reactive prior to
packaging in accordance with paragraphsubsections
(a)
through
(d).
Cyanide- and sulfide-beaning reacitve
waste may be packed in accordance with
paragraphsubsections
(a) through
(d) without first
being treated or rendered non—reactive.
fl
Such disposal is in compliance with 35
Ill.
Adm. Code
728.
Persons who incinerate lab packs’according to 35
Ill.
Adni.
Code 728.142(c) (1) may use fiber drums in
place of metal outer containers.
Such fiber drums must
meet the DOT specifications in 49 CFR 173.12 and be
overpacked according to the requirements of subsection
121—275
127
(b).
g)
Pursuant to 35 Ill.
Adin.
Code 729.312, the use of
labpacks for disposal of liquid wastes or wastes
containing free liquids allowed under this Section is
restricted to labwaste and non—periodic waste, as those
terms are defined in that Part.
(Source:
Amended at 15 Ill. Reg.
,
effective
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 724.930
Applicability
a)
This Subpart applies to owners and operators of
facilities that treat,
store on dispose of hazardous
wastes
(except as provided in Section 724.101).
b)
Except for Sections 724.934(d) and 724.935(e),
this
Subpart applies to process vents associated with
distillation, fractionation, thin-film evaporation,
solvent extraction,
or air or steam stripping
operations that manage hazardous wastes with organic
concentrations of at least
10 ppmw (parts per million
by weight),
if these operations are conducted in:
1)
Units that are subject to the permitting
requirements of 35
Ill. Adm. Code 703; on
2)
Hazardous waste recycling units that are located
on hazardous waste management facilities otherwise
subject to the permitting requirements of 35 Ill.
Adm. Code 703.
c)
If the owner or operator of process vents subject to
the requirements of Sections 724.932 through 724.936
has received a RCRA permit prior to December 21, 1990,
the requirements of Sections 724.932 through 724.936
must be incorporated when the permit is reissued under
35 Ill. Adm. Code 705.201 or reviewed under 35 Ill.
Adm. Code 702.161.
BOARD NOTE:
The requirements of Sections 724.932
through 724.936 apply to process vents on hazardous
waste recycling units previously exempt under 35 Ill.
Adm. Code 721.106(c) (1).
Other exempti’ons under 35
Ill. Adm. Code 721.104, 722.134 and 724.101(g)
are not
affected by these requirements.
(Source:
Added at 15
Ill. Reg.
,
effective
121—276
128
Section 724.931
Definitions
As used in this Subpart, all terms not defined in the Subpart
have the meaning given them in the Resource Conservation and
Recovery Act and 35 Ill. Adm. Code 720 through 726.
Air stripping operation is a desorption operation
employed to transfer one or more volatile components
from a liquid mixture into a gas
(air)
either with or
without the application of heat to the liquid.
Packed
towers, spray towers and bubble—cap,
sieve, or valve—
type plate towers are among the process configurations
used for contacting the air and a liquid.
Bottoms receiver means a container or tank used to
receive and collect the heavier bottoms fractions of
the distillation feed stream that remain in the liquid
phase.
BTU means British thermal unit.
Closed—vent system means a system that is not open to
the atmosphere and that is composed of piping,
connections,
and,
if necessary, flow—inducing devices
that transport gas or vapor from a piece on pieces of
equipment to a control
device.
Condenser means a heat—transfer device that reduces a
thermodynamic fluid from its vapor phase to its liquid
phase.
Connector means flanged,
screwed, welded or other
joined fittings used to connect two pipelines or a
pipeline and a piece of equipment.
For the purposes of
reporting and recordkeeping, connector means flanged
fittings that are not covered by insulation or other
materials that prevent location of the fittings.
Continuous recorder means a data—recording device
recording an instantaneous data value at least once
every 15 minutes.
Control device means an enclosed combustion device,
vapor recovery system, or flare.
Any device the
primary function of which is the recovery on capture of
solvents or other organics for use,
reuse,
on sale
(e.g.,
a primary condenser on a solvent recovery unit)
is not a control device.
Control device shutdown means the cessation of
121—277
129
operation of a control device for any purpose.
Distillate receiver means a container or tank used to
receive and collect liquid material
(condensed)
from
the overhead condenser of a distillation unit and from
which the condensed liquid is pumped to larger storage
tanks or other process units.
Distillation operation means an operation,
either batch
or continuous, separating one or more feed stream(s)
into two or more exit streams, each exit stream having
component concentrations different from those in the
feed stream(s).
The separation is achieved by the
redistribution of the components between the liquid and
vapor phase as they approach equilibrium within the
distillation unit.
Double block and bleed system means two block valves
connected in series with a bleed valve on line that can
vent the line between the two block valves.
Equipment
means each valve,
pump, compresson,’pressure
relief device, sampling connection system, open—ended
valve on line, or flange, and any control devices on
systems required by this Subpart.
Flame zone means the portion of the combustion chamber
in a boiler occupied by the flame envelope.
Flow indicator means a device that indicates whether
gas flow is present in a vent stream.
First attempt at repair means to take rapid action for
the purpose of stopping or reducing leakage of organic
material to the atmosphere using best practices.
Fractionation operation means a distillation operation
on method used to separate a mixture of several
volatile components of different boiling points in
successive stages, each stage removing from the mixture
some proportion of one of the components.
ft means
foot.
h means hour.
Hazardous waste management unit shutdown means a work
practice or operational procedure that ‘stops operation
of a hazardous waste management unit on part of a
hazardous waste management unit.
An unscheduled work
practice or operational procedure that stops operation
of a hazardous waste management unit on part of a
121—278
130
hazardous waste management unit for less than 24 hours
is not a hazardous waste management unit shutdown.
The
use of spare equipment and technically feasible
bypassing of equipment without stopping operation are
not hazardous waste management unit shutdowns.
Hot well means a container for collecting condensate as
in a steam condenser serving a vacuum—jet or steam—jet
ejector.
In gas—vapor service means that the piece of equipment
contains or contacts a hazardous waste stream that is
in the gaseous state at operating conditions.
In heavy liquid service means that the piece of
equipment is not in gas—vapor service or in light
liquid service.
In light liquid service means that the piece of
equipment contains or contacts a waste stream where the
vapor pressure of one on more of the components in the
stream is greaten than 0.3 kilopascals
(kPa)
at 20 C,
the total concentration of the pure components having a
vapor pressure greaten than 0.3 kPa at 20 C is equal to
or greaten than 20 percent by weight, and the fluid is
a liquid at operating conditions.
In situ sampling systems means nonextractive samplers
on in—line samplers.
In vacuum service means that equipment is operating at
an internal pressure that is at least
5 kPa below
ambient pressure.
Kg means kilogram.
kPa means kilopascals.
lb means pound.
m means meter.
Mg means Megagrams,
or metric tonnes.
MJ means Megajoules,
on ten to the sixth Joules.
MW means Megawatts.
Malfunction means any sudden failure of a control
device on a hazardous waste management unit or failure
of a hazardous waste management unit to operate in a
normal on usual manner, so that organic emissions are
12 1—279
131
increased.
Open—ended valve on line means any valve,
except
pressure relief valves, having one side of the valve
seat in contact with process fluid and one side open to
the atmosphere, either directly or through open piping.
ppmv means pants per million by volume.
ppmw meant parts pen million by weight.
Pressure release means the emission of materials
resulting from the system pressure being greater than
the set pressure of the pressure relief device.
Process heater means a device that transfers heat
liberated by burning fuel to fluids contained in tubes,
including all fluids except water that are heated to
produce steam.
Process vent means any open—ended pipe or stack that is
vented to the atmosphere either directly, through a
vacuum—producing system, or through a tank (e.g.,
distillate receiver,
condenser,
bottoms receiver, surge
control tank, separator tank,
or hot well)
associated,.
with hazardous waste distillation, fractionation, thin-
film evaporation, solvent extraction, or air or steam
stripping operations.
Repaired means that equipment is adjusted, or otherwise
altered, to eliminate a leak.
s means second.
scm means standard cubic meter.
scft meant standard cubic foot.
Sensor means a device that measures a physical quantity
or the change in a physical quantity, such as
temperature, pressure, flow rate,
pH, or liquid level.
Separator tank means a device used for separation of
two immiscible liquids.
Solvent extraction operation means an operation on
method of separation
in which a solid or solution is
contracted with a liquid solvent (the t~obeing
mutually insoluble)
to preferentially dissolve and
transfer one or more components into the solvent.
Startup means the setting in operation of a hazardous
12 1—280
132
waste management unit or control device for any
purpose.
Steam stripping operation means a distillation
operation in which vaporization of the volatile
constituents of a liquid mixture takes place by the
introduction of steam directly in to the charge.
Surge control tank means a large—sized pipe on storage
reservoir sufficient to contain the surging liquid
discharge of the process tank to which it is connected.
Thin-f
ilm
evaporation operation means a distillation
operation that employs a heating surface consisting or
a large diameter tube that may be either straight on
tapered, horizontal on vertical.
Liquid is spread on
the tube wall by
a rotating assembly of blades that
maintain a close clearance from the wall or actually
ride on the film of liquid on the wall.
Vapor incinerator means any enclosed combustion device
that is used for destroying organic compounds and does
not extract energy in the form of steam or process
heat.
Vented means discharged through an opening, typically
an open—ended pipe or stack, allowing the passage of a
stream of liquids, gases, on fumes into the atmosphere.
The passage of liquids,
gases, or fumes
is caused by
mechanical means such as compressors or vacuum—
producing systems or by process—related means such as
evaporation produced by heating and not caused by tank
loading and unloading (working losses) or by natural
means such as diurnal temperature changes.
yr means year.
(Source:
Added at 15
Ill. Reg.
,
effective
Section 724.932
Standards:
Process Vents
a)
The owner on operator of a facility with process vents
associated with distillation,
fractionation, thin-film
evaporation, solvent extraction,
or air on steam
stripping operations managing hazardous wastes with
organic concentrations of at least 10 ppmw shall
either:
1)
Reduce total organic emissions from all affected
process vents at the facility below 1.4 kg/h
(3
lb/h)
and 2.8 Mg/yr
(3.1 tons/yr); or
121—281
133
2)
Reduce, by use of a control device, total organic
emissions from all affected process vents at the
facility by 95 weight percent.
b)
If the owner or operator installs a closed—vent system
and control device to comply with the provisions of
subsection
(a), the closed—vent system and control
device must meet the requirements of Section 724.933.
C)
Determinations of vent emissions and emission
reductions or total organic compound concentrations
achieved by add—on control devices must be either based
on engineering calculations or performance tests.
If
performance tests are used to determine vent emissions,
emission reductions,
or total organic compound
concentrations achieved by add—on control devices,
the
performance tests must conform with the requirements of
Section 724.934(c).
d)
When
an owner on operator and the Agency do not agree
on determinations of vent emissions on emission
reductions on total organic compound concentrations
achieved by add—on control devices based on engineering
calculations, the procedures in Section 724.934(c)
must
be used to resolve the disagreement.
Source:
Added at
15 Ill.
Req.
,
effective
Section 724.933
Standards:
Closed-vent Systems and Control
Devices
a)
Compliance Required.
1)
Owners or operators of closed—vent systems and
control devices used to comply with provisions of
this Part shall comply with the provisions of this
Section.
2)
‘The owner or operator of an existing facility who
cannot install
a closed—vent system and control
device to comply with the provisions of this
Subpart on the effective date that the facility
becomes subject to the provisions of this Subpart
shall prepare an implementation schedule that
includes dates by which the closed—vent system and
control device will be installed ahd in operation.
The controls must be installed as soon as
possible, but the implementation schedule may
allow up to 18 months after the effective date
that the facility becomes subject to this Subpart
121—282
134
for installation and startup.
All units that
begin operation after December 21,
1990, must
comply with the rules immediately
(i.e., must have
control devices installed and operating on startup
of the affected unit); the 2—year implementation
schedule does not apply to these units.
b)
A control device involving vapor recovery (e.g.,
a
condenser or adsorben) must be designed and operated to
recover the organic vapors vented to it with an
efficiency of 95 weight percent or greaten unless the
total organic emission limits of Section 724.932(a) (1)
for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device
(e.g.,
a vapor
incinerator, boiler or process heater) must be designed
and operated to reduce the organic emissions vented to
it by 95 weight percent or greaten; to achieve a total
organic compound concentration of 20 ppmv,
expressed as
the sum of the actual compounds,
not carbon
equivalents, on a dry basis connected to 3 percent
oxygen; or to provide a minimum residence time of 0.50
seconds at a minimum temperature of 760
C.
If a boiler
or process heater is used as the control device, then
the vent stream must be introduced into the flame zone
of*the boiler on process heater.
d)
Flares
1)
A flare must be designed for and operated with no
visible emissions as determined by the methods
specified in subsection
(e) (1)
except for periods
not to exceed a total of
5 minutes during any 2
consecutive hours.
2)
A flare must be operated with a flame present at
all times,
as determined by the methods specified
in subsection
(f) (2) (c).
3)
A flare must be used only if the net heating valu’~
of the gas being combusted is 11.2
NJ/scm
(300
Btu/scf)
on greaten if the flare is steam—assisted
on air—assisted; on if the net heating value of
the gas being combusted is 7.45 NJ/scm (200
Btu/scf)
or greaten if the flare is nonassisted.
The net heating value of the gas being combusted
must be determined by the methods bpecified in
subsection
(e) (2).
4)
Exit Velocity.
121—283
135
A)
A steam—assisted or nonassisted flare must be
designed for an operated with an exit
velocity, as determined by the methods
specified in subsection
(e)(3),.less than
18.3
ni/s
(‘60 ft/s), except as provided in
subsections
(d) (4) (B) and
(C).
B)
A steam-assisted or nonassisted flare
designed for and operated with an exit
velocity, as determined by the methods
specified in subsection
(e)(3), equal to on
greaten than 18.3
ni/s
(60 ft/s) but less than
122 ni/s
(400 ft/s)
is allowed if the net
heating value of the gas being combusted is
greaten than 37.3
NJ/scm
(1000 Btu/scf).
C)
A steam—assisted on nonassisted flare
designed for and operated with an exit
velocity,
as determined by the methods
specified in subsection
(e) (3), less than the
velocity, V as determined by the method
specified in subsection
(e) (4) and less than
122
in/s
(400 ft/s)
is allowed.
5)
An air-assisted flare must be designed and
operated with an exit velocity less than the
velocity, V as determined by the method specified
in subsection
(e) (5).
6)
A flare used to comply with this Section must be
steam—assisted, air—assisted on nonassisted.
e)
1)
Reference Method 22 in 40 CFR 60,
incorporated by
reference in 35 Ill.
Adm. Code 720.111, must be
used to determine the compliance of a flare with
the visible emission provisions of this Subpart.
The observation period is
2 hours and must be used
according to Method 22.
2)
The net heating value of the gas being combusted
in a flare must be calculated using the following
equation:
H
=
K
*
SUM(Ci
*
Hi)
Where:
H is the net heating value of the sample in
MJ/scm; where the net enthalpy pen mole of
offgas is based on combustion at 25 C and 760
mm Hg, but the standard temperature for
determining the volume corrersponding to
1
121—284
136
mole is 20 C.
K
=
1.74 E -7
(1/ppm) (g mol/scm)
(MJ/kcal)
where standard temperature for
(g mol/scm)
20
C.
SUM(Xi) means the sum of the values of X for
each component i,
from i=1 to n.
Ci is the concentration of sample component
i
in ppm on a wet basis,
as measured for
organics by Reference Method 18 in 40 CFR 60,
and for carbon monoxide, by ASTM D1946,
incorporated by reference in 35 Ill. Adm.
Code 720.111.
Hi is the net heat of combustion of sample
component i, kcal/gmol at 25 C and 760 mm Hg.
The heats of combustion must be determined
using ASTM D2382,
incorporated by reference
in 35 Ill. Adm. Code 720.111,
if published
values are not available on cannot be
calculated.
3)
The actual exit velocity of a flare must be
determined by dividing the volumetric flow rate
(in units of standard temperature and pressure),
as determined by Reference Methods
2,
2A,
2C, or
2D in 40 CFR 60, incorporated by reference in 35
Ill.
Adm. Code 720.111,
as appropriate, by the
unobstructed
(free)
cross—sectional area of the
flare tip.
4)
The maximum allowed velocity in m/s, V for a flare
complying with subsection
(d) (4) (C) must be
determined by the following equation:
LOG(V)
=
(H
+
28.8)
/
31.7
Where:
LOG
means logarithm to the base 10
H is the net heating value as determined in
subsection
(e) (2).
5)
The maximum allowed velocity in m/s, V for an air—
assisted flare must be determined’by the following
equation:
V
=
8.706
+
O.7084H
121—285
137
Where:
H is the net heating value as determined in
subsection
(e) (2)
f)
The owner or operator shall monitor and inspect each
control device required to comply with this Section to
ensure proper operation and maintenance of the control
device by implementing the following requirements:
1)
Install, calibrate, maintain and operate according
to the manufacturer’s specifications a flow
indicator that provides a record of stream flow
from each affected process vent to the control
device at least once every hour.
The flow
indicator sensor must be installed in the vent
stream at the nearest feasible point to the
control device inlet but before the point at which
the vent streams are combined.
2)
Install, calibrate, maintain and operate according
to the manufacturer’s specifications a devic’e to
continuously monitor control device operation as
specified below:
A)
For a thermal vapor incinerator,
a
temperature monitoring device equipped with
a
continuous recorder.
The device must have
accuracy of ±1 percent of the temperature
being monitored in C or±C, whichever is
greater.
the temperature sensor must be
installed at a location in the combustion
chamber downstream of the combustion zone.
B)
For a catalytic vapor incinerator,
a
temperature monitoring device equipped with a
continuous recorder.
The device must be
capable of monitoring temperature at two
locations and have an accuracy of ±1 percent
of the temperature being monitored in C or±
0.5 C, whichever is greaten.
One temperature
sensor must be installed in the vent stream
at the nearest feasible point to the catalyst
bed inlet and a second temperature sensor
must be installed in the vent stream at the
nearest feasible point to the catalyst bed
outlet.
C)
For a flare,
a heat sensing monitoring device
equipped with a continuous recorder that
indicates the continuous ignition of the
pilot
flame.
12 1—286
138
D)
For a boiler or process heater having a
design heat input capacity less than 44 MW,
a
temperature monitoring device equipped with a
continuous recorder.
The ‘device must have an
accuracy of ±1 percent of the temperature
being monitored in C or ±0.5 C, whichever is
greater.
The temperature sensor must be
installed at a location in the furnace
downstream of the combustion zone.
E)
For a boiler or process heater having a
design heat input capacity greater than or
equal to 44 NW,
a monitoring device equipped
with a continuous recorder to measure a
parameter(s) that indicates good combustion
operating practices are being used.
F)
For a condenser,
either:
i)
A monitoring device equipped with a
continuous recorder to measure the
concentration level of the organic
compounds in the exhaust vent stream
from the condenser; or
ii)
A temperature monitoring device equipped
with a continuous recorder.
The device
must be capable of monitoring
temperature at two locations and have an
accuracy of±1 percent of the
temperature being monitored in C on ±
0.5 C, whichever is greaten.
One
temperature sensor must be installed at
a location in the exhaust vent stream
from the condenser,
and a second
temperature sensor must be installed at
a location in the coolant fluid exiting
the condenser.
G)
For a carbon adsorption system that
regenerates the carbon bed directly in the
control device such as a fixed—bed carbon
adsorber, either:
1)
A monitoring device equipped with a
continuous recorder to measure the
concentration level of the organic
compounds in the exhaust vent stream
from the carbon bed, on
ii)
A monitoring device equipped with a
121—287
139
continuous recorder to measure a
parameter that indicates the carbon bed
is regenerated on a regular,
predetermined time cycle.
3)
Inspect the readings from each monitoring device
required by subsection
(f) (1) and
(2)
at least
once each operating day to check control device
operation and,
if necessary,
immediately implement
the corrective measures necessary to ensure the
control device operates in compliance with the
requirements of this Section.
g)
An owner or operator using a carbon adsorption system
such as a fixed—bed carbon adsonber that regenerates
the carbon bed directly onsite in the control device
shall replace the existing carbon in the control device
with fresh carbon at
a regular, predetermined time
interval that is no longer than the carbon service life
established as
a requirement of Section
724.935(b) (4) (C) (vi).
h)
An owner on operator using a carbon adsorption system
such as a carbon canister that does not regenerate the
carbon bed directly onsite in the control device shall
replace the existing carbon in the control device with
fresh carbon on a regular basis by using one of the
following procedures:
1)
Monitor the concentration level of the organic
compounds in the exhaust vent stream from the
carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon
immediately when carbon breakthrough is indicated.
The monitoring frequency must be daily or at an
interval no greaten than 20 percent of the time
required to consume the total carbon working
capacity established as a requirement of Section
724.935(b) (4) (C) (vii), whichever is longer.
2)
Replace the existing carbon with fresh carbon at a
regular, predetermined time interval that is less
than the design carbon replacement interval
established as a requirement of Section
724.935(b) (4) (C(vii)
i)
An alternative operational on process parameter may be
monitored if the operator demonstrates ‘that the
parameter will ensure that the control device is
operated in conformance with these standards and the
control device’s design specifications.
121—288
140
j)
An owner or operator of an affected facility seeking to
comply with the provisions of this Part by using a
control device other than a thermal vapor incinerator,
catalytic vapor incinerator,
flare, boiler, process
heater, condenser or carbon adsorption system is
required to develop documentation including sufficient
information to describe the control device operation
and identify the process parameter or parameters that
indicate proper operation and maintenance of the
control device.
k)
Closed vent systems.
1)
Closed—vent systems must be designed for and
operated with no detectable emissions,
as
indicated by an instrument reading of less than
500 ppm above background and by visual
inspections,
as determined by the methods
specified at Section 724.934(b).
2)
Closed—vent systems must be monitored to determine
compliance with this Section during the initial
leak detection monitoring, which must be conducted
by the date that the facility becomes subject to
the provisions of this Section annually, and at
other times as specified in the RCRA permit.
3).
Detectable emissions,
as indicated by an
instrument reading greater than 500 ppm and visual
inspections, must be controlled as soon as
practicable, but not later than 15 calendar days
after the emission is detected.
4)
A first attempt at repair must be made no later
than
5 calendar days after the emission
is
detected..
1)
Closed—vent systems and control devices used to comply
with provisions of this Subpart must be operated at all
times when emissions may be vented to them.
Source:
Added at 15
Ill.
Reg.
,
effective
Section 724.934
Test methods and procedures
a)
Each owner on operator subject to the provisions of
this Subpart shall comply with the tests methods and
procedures requirements provided in this Section
b)
When a closed-vent system is tested for compliance with
no detectable emissions,
as required in Section
12 1—289
141
724.933(k),
the test must comply with the following
requirements:
1)
Monitoring must comply with Reference Method 21 in
40 CFR 60,
incorporated by reference in 35 Ill.
Adm. Code 720.111.
2)
The detection instrument must meet the performance
criteria of Reference Method 21.
3)
The instrument must be calibrated before use on
each day of its use by the procedures specified in
Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in
air).
B)
A mixture of methane or n—hexane and air at a
concentration of approximately, but less
than,
10,000 ppm methane or n—hexane.
5)
The background level must be determined as set
forth in Reference Method 21.
6)
The instrument probe must be traversed around all
potential leak interfaces as close to the
interface as possible as described in Reference
Method 21.
7)
The anith~eticdifference between the maximum
concentration indicated by the instrument and the
background level
is compared with 500 ppm for
determining compliance.
c)
Performance tests to determine compliance with Section
724.932(a)
and with the total organic compound
concentration limit of Section 724.933(c)
must comply
with the following:
1)
Performance tests to determine total organic
compound concentrations and mass flow rates
entering and exiting control devices must be
conducted and data reduced in accordance with the
following reference methods and calculation
procedures:
A)
Method
2 in 40 CFR 60 for velocity and
volumetric flow rate.
B)
Method 18 in 40 CFR 60 for organic content.
121—290
142
C)
Each performance test must consist of three
separate runs, each run conducted for at
least 1 hour under the conditions that exist
when the hazardous waste management unit is
operating at the highest load on capacity
level reasonably expected to occur.
For the
purpose of determining total organic compound
concentrations and mass flow rates, the
average of results of all runs applies.
The
average must be computed on a time—weighed
basis.
D)
Total organic mass flow rates must be
determined by the following equation:
F
=
K
*
Q
*
SUN(Ci
*
MWi)
Where:
F is the total organic mass flow rate,
kg/h.
K
=
4.16 E —8, conversion factor for
molar volume, kg-mol/cubic m, at 293 K
and 760 mm Hg.
Q
=
volumetric flow rate of gases
entering or exiting control device,
dscm/h, as determined by Method
2 in 40
CFR 60, incorporated by reference in 35
Ill. Adm. Code 720.111.
SUM(Xi) means the sum of the values of X
for each component i, from i=1 to n.
n
=
number of organic compounds in the
vent gas.
Ci is the organic concentration in ppm,
dry basis,
of compound
i in the vent
gas, as determined by Method 18
in 40
CFR 60.
MWi
is the molecular weight of organic
compound
i in the vent gas, kg/kg-mol.
E)
The annual total organic emi~ssionrate must
be determined by the following equation:
A
=
F
*
HOURS
12 1—29
1
143
‘Where:
A is total organic emission rate, kg/y.
F is the total organic mass flow nate,
kg/h, as calculated in subsection
(c) (1) (D)
HOURS is the total annual hours of
operation for the affected unit.
F)
Total organic emissions from all affected
process vents at the facility must be
determined by summing the hourly total
organic mass emissions rates
(F as determined
in. subsection
(c) (1) (D))
and by summing the
annual total organic mass emission rates
(A
as determined in subsection
(c) (1) (E))
for
all affected process vents at the facility.
2)
The owner on operator shall record such process
information as is necessary to determine the
conditions of the performance tests.
Operations
during periods of startup, shutdown and
malfunction do not constitute representative
conditions for the purpose of a performance test.
3)
The owner on operator of an affected facility
shall provide, or cause to be provided,
performance testing facilities as follows:
A)
Sampling ports adequate for the test methods
specified in subsection
(c) (1).
B)
Safe sampling platform(s).
C)
Safe access to sampling platform(s).
D)
Utilities for sampling and testing equipment..
4)
For the purpose of making compliance
determinations, the time-weighted average of the
results of the three runs must apply.
In the
event that a sample is accidentally lost or
conditions occur in which one of the three nuns
must be discontinued because of forced shutdown,
failure of an irreplaceable portion of the sample
train, extreme meteorological conditions or other
circumstances beyond the owner or operator’s
control,
compliance may, upon the Agency’s
approval, be determined using the average of the
results of the two other runs.
12
1—292
144
d)
To show that a process vent associated with a hazardous
waste distillation, fractionation, thin-film
evaporation, solvent extraction,
on air or steam
stripping operation is not subject to the requirements
of this Subpart, the owner or operator shall make an
initial determination that the time-weighted, annual
average total organic concentration of the waste
managed by the waste management unit is less than 10
ppmw using one of the following two methods:
1)
Direct measurement of the organic concentration of
the waste using the following procedures:
A)
The owner or operator shall take a minimum of
four grab samples of waste for each
wastestneam managed in the affected unit
under process conditions expected to cause
the maximum waste organic concentration.
B)
For waste generated onsite, the grab samples
must be collected at a point before the waste
is exposed to the atmosphere such as in an
enclosed pipe on other closed system that is
used to transfer the waste after generation
to the first affected distillation,
fractionation, thin—film evaporation,
solvent
extraction,
or air on steam stripping
operation.
For waste generated offsite, the
grab samples must be collected at the inlet
to the first waste management unit that
receives the waste provided the waste has
been transferred to the facility in a closed
system such as a tank truck and the waste is
not diluted on mixed with other waste.
C)
Each sample must be analyzed and the total
organic concentration of the sample must be
computed using Method 9060 or 8240 of SW-846
(incorporated by reference under 35 Ill.
Adm.
Code 720.111.
D)
The arithmetic mean of the results of the
analyses of the four samples apply for each
wastestream managed in the unit in
determining the time—weighted, annual average
total organic concentration of the waste.
The time-weighted average is to be calculated
using the annual quantity of each waste
stream processed and the mean organic
concentration of each wastestream managed in
the unit.
12 1—293
145
2)
Using knowledge of the waste to determine that its
total organic concentration is less that 10 ppmw.
Documentation of the waste determination is
required.
Examples of documentation that must be
used to support
a determination under this
subsection include:
A)
Production process information documenting
that no organic compounds are used.
B)
Information that the waste is generated by a
process that is identical to a process at the
same on another facility that has previously
been demonstrated by direct measurement to
generate a wastestream having a total organic
content less than 10 ppmw,
or
C)
Prior speciation analysis results on the same
wastestream where it is also documented that
no process changes have occurred since that
analysis that could affect the waste total
organic concentration.
e)
The determination that distillation, fractionation,
thin—film evaporation, solvent extraction,
or air on
steam stripping operations which manage hazardous
wastes with time-weighted, annual average total organic
concentrations less than 10 ppmw must be made as
follows:
1)
By the effective date that the facility becomes
subject to the provisions of this Subpart or by
the date when the waste is first managed in a
waste management unit, whichever is later; and
2)
For continuously generated waste,
annually; or
3)
Whenever there is a change in the waste being
managed or a change in the process that generates
or treats the waste.
f)
When
an owner or operator and the Agency do not agree
on whether a distillation, fractionation, thin-film
evaporation, solvent extraction,
or air or steam
stripping operation manages a hazardous waste, with
organic concentrations of at least
10 ppmw based on
knowledge of the waste,
the procedures in Method 8240
in SW-846,
incorporated by reference in 35 Ill. Adm.
Code 720.111, must be used to resolve the dispute.
(Source:
Added at 15 Ill.
Reg.
effective
121—294
146
Section 724.935
Recondkeeping requirements
a)
Compliance Required.
1)
Each owner or operator subject to the provisions
of this Subpart shall comply with the
recordkeeping requirements of this Section.
2)
An owner or operator of more than one hazardous
waste management unit subject to the provisions of
this Subpart may comply with the recordkeeping
requirements for these hazardous waste management
units in one recordkeeping system if the system
identifies each record by each hazardous waste
management unit.
b)
Owners and operators shall record the following
information in the facility operating record:
1)
For facilities that comply with the provisions of~
Section 724.933 (a) (2), an implementation schedule
that includes dates by which the closed-vent
system and control device will be installed and in
operation.
The schedule must also include a
rationale of why the installation cannot be
completed at an earlier date.
The implementation
schedule must be in the facility operating record
by the effective date that the facility becomes
subject to the provisions of this Subpart.
2)
Up-to-date documentation of compliance with the
process vent standards in Section 724.932,
including:
A)
Information and data identifyin’g all affected
process vents, annual throughput and
operating hours of each affected unit,
estimated emission rates for each affected
vent and for the overall facility (i.e.,
the
total emissions for all affected vents at the
facility), and the approximate location
within the facility of each affected unit
(e.g.,
identify the hazardous waste
management units on a facility plot plan).
B)
Information and data supporting determination
of vent emissions and emission reductions
achieved by add—on control devices based on
engineering calculations on source tests.
For the purpose of determining compliance,
121—295
147
determinations of vent emissions and emission
reductions must be made using operating
parameter values
(e.g.,
temperatures, flow
rates,
or vent stream organic compounds and
concentrations)
that represent the conditions
that result in maximum organic emissions,
such as when the waste management unit is
operating at the highest load or capacity
level reasonably expected to occur.
If the
owner or operator takes any action (e.g.,
managing a waste of different composition or
increasing operating hours of affected waste
management units)
that would result in an
increase in total organic emissions from
affected process vents at the facility, then
a new determination is required.
3)
Where an owner on operator chooses to use test
data to determine the organic removal efficiency
or total organic compound concentration achieved
by the control device,
a performance test plan.
The test plan must include:
A)
A description of how it is determined that
the planned test is going to be conducted
when the hazardous waste management unit is
operating at the highest load or capacity
level reasonably expected to occur.
This
must include the estimated or design flow
rate and organic content of each vent stream
and define the acceptable operating ranges of
key process and control device parameters
during the test program.
B)
A detailed engineering description of the
closed-vent system and control device
including:
i)
Manufacturer’s name and model number of
control device.
ii)
Type of control device.
iii) Dimensions of the control device.
iv)
Capacity.
v)
Construction materials.
C)
A detailed description of sampling and
monitoring procedures,
including sampling and
monitoring locations in the system, the
121—296
248
equipment to be used,
sampling and monitoring
frequency, and planned analytical procedures
for sample analysis.
4)
Documentation of compliance with Section 724.933
must include the following information:
A)
A list of all information references and
sources used in preparing the documentation.
B)
Records including the dates of each
compliance test required by Section
724.933 (k).
C)
If engineering calculations are used,
a
design analysis,
specifications,
drawings,
schematics, and piping and instrumentation
diagrams based on the appropriate sections of
APTI Course 415 (incorporated by reference in
35 Ill.
Adm. Code 720.111) on other
engineering texts, approved by the Agency,
that present basic control device design
information.
Documentation provided by the
control device manufacturer or vendor that
describes the control device design in
accordance with subsections
(b) (4) (C) (1)
through
(vii) may be used to comply with this
requirement.
The design analysis must
address the vent stream characteristics and
control device operation parameters as
specified below.
i)
For a thermal vapor incinerator, the
design analysis must consider the vent
stream composition, constituent
concentrations and flow rate.
The
design analysis must also establish the
design minimum and average temperature
in the combustion zone and the
combustion zone residence time.
ii)
For a catalytic vapor incinerator, the
design analysis must consider the vent
stream composition, constituent
concentrations,
and flow rate.
The
design analysis must also establish the
design minimum and average temperatures
across the catalyst bed ‘inlet and
outlet.
iii) For a boiler or process heater, the
design analysis must consider the vent
121—297
149
stream composition, constituent
concentrations and flow rate.
The
design analysis must also establish the
design minimum and average flame zone
temperatures, combustion zone residence
time and description of method and
location where the vent stream is
introduced into the combustion zone.
iv)
For a flare, the design analysis must
consider the vent stream composition,
constituent concentrations,
and flow
rate.
The design analysis must also
consider the requirements specified in
Section 724.933(d).
v)
For a condenser, the design analysis
must consider the vent stream
composition, constituent concentrations,
flow rate, relative humidity and
temperature.
The design analysis must
also establish the design outlet organic
compound concentration level, design
average temperature of the condenser
exhaust vent stream and design average
temperatures of the coolant fluid at the
condenser inlet and outlet.
vi)
For a carbon adsorption system such as a
fixed—bed adsorber that regenerates the
carbon bed directly onsite in the
control device, the design analysis must
consider the vent stream composition,
constituent concentrations,
flow rate,
relative humidity and temperature.
The
design analysis must also establish the
design exhaust vent stream organic
compound concentration level, number and
capacity of carbon beds, type and
working capacity of activated carbon
used for carbon beds,
design total steam
flow over the period of each complete
carbon bed regeneration cycle,
duration
of the carbon bed steaming and
cooling/drying cycles, design carbon bed
temperature after regeneration, design
carbon bed regeneration time and design
service life of carbon.
vii)
For a carbon adsorption system such as a
carbon canister that does not regenerate
the carbon bed directly onsite in the
12 1—298
150
control device, the design analysis must
consider the vent stream composition,
constituent concentrations,
flow rate,
relative humidity and temperature.
The
design analysis must also establish the
design outlet organic concentration
level, capacity of carbon bed, type and
working capacity of activated carbon
used for carbon bed and design carbon
replacement interval based on the total
carbon working capacity of the control
device and source operating schedule.
D)
A statement signed and dated by the owner or
operator certifying that the operating
parameters used in the design analysis
reasonably represent the conditions that
exist when the hazardous waste management
unit is or would be operating at the highest
load or capacity level reasonably expected to
occur.
E)
A statement signed and dated by the owner or
operator certifying that the control device
is designed to operate at an efficiency of 95
percent or greater unless the total organic
concentration limit of Section 724.932(a)
is
achieved at an efficiency less than 95 weight
percent or the total organic emission limits
of Section 724.932(a)
for affected process
vents at the facility are attained by a
control device involving vapor recovery at an
efficiency less than 95 weight percent.
A
statement provided by the control device
manufacturer on vendor certifying that the
control equipment meets the design
specifications may be used to comply with
this requirement.
F)
If performance tests are used to demonstrate
compliance,
all test results.
c)
Design documentation and monitoring operating and
inspection information for each closed-vent system and
control device required to comply with the provisions
of this Part must be recorded and kept up-to-date in
the facility operating record.
The information must
include:
1)
Description and date of each modification that is
made to the closed—vent system on control device
design.
12 1—2
99
151
2)
Identification of operating parameter,
description
of monitoring device, and diagram of monitoring
sensor location or locations used to comply with
Section 724.933(f) (1) and
(2).
3)
Monitoring, operating and inspection information
required by Section 724.933(f)
through
(k).
4)
Date, time and duration of each period that occurs
while the control device is operating when any
monitored parameter exceeds the value established
in the control device design analysis as specified
below:
A)
For a thermal vapor incinerator designed to
operate with a minimum residence time of 0.50
second at a minimum temperature of 760 C, any
period when the combustion temperature is
below 760 C.
B)
For a thermal vapor incinerator designed to
operate with an organic emission reduction
efficiency of 95 weight percent or greater,
any period when the combustion zone
temperature is more than 28 .C below the
design average combustion zone temperature
established as a requirement of subsection
(b) (4) (C) (i)
C)
For a catalytic vapor incinerator, any period
when:
i)
Temperature of the vent stream at the
catalyst bed inlet is more than 28 C
below the average temperature
of’ the
inlet vent stream established as a
requirement of subsection
(b) (4) (C) (ii);
or
ii)
Temperature difference across the
catalyst bed
is less than 80 percent of
the design average temperature
difference established as a requirement
of subsection
(b) (4) (C) (ii).
D)
For a boiler or process heater, any period
when:
i)
Flame zone temperature
is more than 28 C
below the design average flame zone
temperature established as a requirement
121—300
1~2
of subsection
(b) (4) (C) (iii); or
ii)
Position changes where the vent stream
is introduced to the combustion zone
from the location established as a
requirement of subsection
(b) (4) (C) (iii).
E)
For a flare, period when the pilot flame is
not ignited.
F)
For a condenser that complies with Section
724.933 (f) (2) (F) (1), any period when the
organic compound concentration level or
readings of organic compounds in the exhaust
vent stream from the condenser are more than
20 percent greaten than the design outlet
organic compound concentration level
established as a requirement of subsection
(b)
(4)
(C) (v).
G)
For a condenser that complies with Section
724.933(f) (2) (F) (ii),
any period when:
i)
Temperature of the exhaust vent stream
from the condenser is more than 6 C
above the design average exhaust vent
stream temperature established as a
requirement of subsection (b)(4)(C)(v).
ii)
Temperature of the coolant fluid exiting
the condenser is more than 6
C above the
design average coolant fluid temperature
at the condenser outlet established as a
requirement of subsection
(b)
(4)
(C) (v).
H)
For a carbon adsorption system ‘such as a
fixed—bed carbon adsonber that regenerates
the carbon bed directly onsite in the control
device and complies with Section
724.933(f)(2QG)(i), any period when the
organic compound concentration level or
readings of organic compounds in the exhaust
vent stream from the carbon bed are more than
20 percent greater than the design exhaust
vent stream organic compound concentration
level established as a requirement of
subsection
(b) (4) (C) (vi).
I)
For a carbon adsorption
system such
as a
fixed—bed carbon adsorber that regenerates
the carbon bed directly onsite in the control
121—301
.153
device
and
complies
with
Section
724.933(f)
(2) (G) (ii),
any
period
when
the
vent
stream
continues
to
flow
through
the
control
device
beyond
the
predetermined
carbon
bed’
regeneration
time
established
as
a
requirement
of
subsection
(b) (4)
(C) (vi).
5)
Explanation for each period recorded under
subsection
(C)
(4)
of
the
cause
for
control
device
operating
parameter
exceeding
the
design
value
and
the
measures
implemented
to
correct
the
control
device
operation.
6)
For a carbon adsorption system operated subject to
requirements specified in Section 724.933(g)
or
(h) (2), any date when existing carbon in the
control device is replaced with fresh carbon.
7)
For a carbon adsorption system operated subject to
requirements specified in Section 724.933(h) (1), a
log that records:
A)
Date and time when control device is
monitored for carbon breakthrough and the
monitoring device reading.
B)
Date when existing carbon in the control
device
is replaced with fresh carbon.
8)
Date of each control device startup and shutdown.
d)
Records of the monitoning, operating and inspection
information required by subsections
(c) (3) through
(8)
need be kept only 3 years.
e)
For a control device other than a thermal vapor
incinerator, catalytic vapor incinerator,
flare,
boiler, process heater, condenser or carbon adsorption
system, the Agency shall specify the appropriate
recordkeeping requirements.
f)
Up-to-date
information
and
data
used
to
determine
whether
on
not
a
process
vent
is
subject
to
the
requirements
in
Section
724.932,
including
supporting
documentation as required by Section 724.934(d) (2),
when application of the knowledge of the nature of the
hazardous wastestream or the process by which it was
produced is used, must be recorded in
a- log that is
kept
in
the
facility
operating
record.
Source: Added at 15 Ill. Reg.
,
effective
121—302
154
Section 724.936
Reporting Requirements
a)
A semiannual report must be submitted by owners and
operators
subject
to
the
requirements
of this Subpart
to
the
Agency
by
dates
specified
in
the
RCRA
permit.
The report must include the following information:
1)
The USEPA identification number
(35 Ill. Adm. Code
722.112),
name, and address of the facility.
2)
For each month during the semiannual reporting
period:
a)
Dates when the control device:
i)
Exceeded or operated outside of the
design specifications as defined in
Section 724.935(c) (4) and
ii)
Such exceedances were not corrected
within 24 hours,
or that a flare
operated with visible emissions as
defined by Method 22 monitoring
B)
The duration and cause of each exceedance on
visible emissions, and
C)
Any corrective measures taken.
b)
If during the semiannual reporting period, the control
device does not exceed or operate outside of the design
specifications as defined in Section 724.935(c) (4) for
more than 24 hours or a flare does not operate with
visible emissions as defined in Section 724.933(d),
a
report to the Agency is not required.
Source:
Added at 15 Ill.
Reg.
,
effective
SUBPART BB:
AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 724.950
Applicability
~j
The regulations in this Subpart apply to owners and
operators of facilities that treat, store,
or dispose
of hazardous wastes (except as provided’ in Section
724.101).
~2J
Except as provided
in Section 724.964(k)1 this Subpart
applies to equipment that contains or contacts
12 1—303
155
hazardous wastes with organic concentrations of at
least
10 percent by weight that are managed in:
fl.
Units that are subject to the RCRA permitting
requirements of 35 Ill. Adm. Code 703, on
Z1.
Hazardous waste recycling units that are located
on hazardous waste management facilities otherwise
subject to the permitting requirements of 35 Ill.
Adm. Code 703.
gj
If the owner or o~enatonof equipment subject to the
requirements of Sections 724.952 through 724.965 has
received a RCRA permit prior to December 21,
1990.
the
requirements of Sections 724.952 through 724.965 must
be incorporated when the permit is reissued under
35
Ill. Adm. Code 705.201 or reviewed under 35 Ill. Adm.
Code 702.161.
~j
Each piece of equipment to which this Subpart applies
must be marked in such a manner that it can be
distinguished readily from other pieces of equipment.
~j.
Equipment that is in vacuum service is excluded from
the requirements of Sections 724.952 to 724.960,
if it
is identified as required in Section 724.964(g) (5).
BOARD NOTE:
The requirements
of
Sections
724.952
through 724.965 apply to equipment associated with
hazardous waste recycling units previously exempt under
35 Ill. Adm. Code 721.106(c)(1).
Other exemptions
under 35 Ill. Mm.
Code 721.104,
722.134 and 724.101(g)
are not affected by these requirements.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.951
Definitions
As used in this Subpart,
all terms have the meaning given them in
Section 724.931,
the Resource Conservation and Recovery Act and
35
Ill. Adm. Code 720 through 726.
Source:
Added at
15 Ill.
Reg.
,
effective
Section 724.952
Standards:
Pumps in Light Liquid Service
~j
Monitoring
3j
Each pump in light liquid service must be
monitored monthly to detect leaks by the methods
12 1—304
156
specified in Section 724.963(b),
except as
provided in subsections
(d).
(e)
and
(f).
~j
Each pump in light liquid service must be checked
by visual inspection each calendar week for
indications of liquids dripping from the pump
seal.
~
Leaks
fl
If an instrument reading of 10,000 ppm or greater
is measured,
a leak is detected.
21
If there are indications of liquids dni~pingfrom
the pump seal,
a leak is detected.
~
Repairs
fl
When a leak is detected,
it must be repaired as
soon as practicable. but not later than 15.
calendar days after it is detected, except as
provided in Section
724.959.
21
A first attempt at repair
(e.g., tightening the
packing gland) must be made no later than
5
calendar days after each leak is detected.
~j.
Each pump equipped with
a dual mechanical seal system
that includes a barrier fluid system is exempt from the
requirements of subsection
(a). provided the following
requirements are met:
31
Each dual mechanical seal system must be:
~J
Operated with the barrier fluid at
a pressure
that is at all times greater than the pump
stuffing
box
pressures;
or
~j
Equipped
with
a
barrier fluid degassing
reservoir
that
is
connected by a closed—vent
system
to
a
control device that complies with
the
requirements
of
Section
724.960;
on
~j
Equipped
with
a
system
that
purges the
barrier
fluid
into
a
hazardous
wastestream
with
no
detectable
emissions
to
the
atmosphere.
21
The
barrier
fluid
system
must
not
be
a
hazardous
waste
with
organic
concentrations
10
percent
or
greater
by
weight.
12 1—305
157
fl
Each barrier fluid system must be equipped with a
sensor
that
will
detect
failure
of
the
seal
system,
the
barrier fluid system,
or
both.
~j.. Each pump must be checked by visual inspection.
each
calendar
week,
for
indications
of
liquids
dripping from the rump seals.
~j.
Alarms
~
Each sensor as described in subsection
(d) (3)
must be checked daily on be equipped with an
audible alarm that must be checked monthly to
ensure that it is functioning properly.
~j.
The owner or operator shall determine, based
on design considerations and operating
experience,
a criterion that indicates
failure of the seal system, the barrier fluid
system, or both.
~
Leaks
~j
If there are indications of liquids dripping
from the pump seal or the sensor indicates
failure of the seal system. •the barrier fluid
system, on both based on the criterion
determined in subsection
(d) (5) (B),
a leak is
detected.
~j
When a leak is detected,
it must be repaired
as soon as practicable, but not later than 15
calendar days after it
is detected, except as
provided in Section 724.959.
Qj
A
first
attempt
at
repair
(e.g.,
relapping
the seal)
must be made no later than
5
calendar days after each leak is detected.
~j
Any pump that is designated,
as described in Section
724.964(g) (2), for no detectable emissions,
as
indicated by an instrument reading of less than 500 ppm
above background,
is exempt from the requirements cf
subsections
(a),
(c) and
(d).
if the pump meets the
following requirements:
31
Must have no externally actuated shaft penetrating
the pump housing.
~
Must operate with no detectable emissions as
indicated by an instrument reading of less than
500 ppm above background as measured by the
121—306
158
methods specified in Section 724.963(c)’.
~j.
Must be tested for compliance with subsection
(e) (2)
initially upon designation, annually and at
other times as specified in the RCRA permit.
ZI
If any pump is equipped with a closed-vent system
capable of capturing and transporting any leakage from
the seal on seals to a control device that complies
with the requirements of Section 724.960,
it
is exempt
from the requirements of subsections
(a) through
(e).
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.953
Standards:
Compressors
~j
Each compressor must be equipped with a seal system
that includes
a barrier fluid system and that prevents
leakage of total organic emissions to the atmosphere,
except as provided in subsections
(h) and
(i).
~
Each compressor seal system as required in subsection
(a)
must
be:
31
Operated with the barrier fluid at a pressure that
is at all times greater than the compressor
stuffing box pressure; or
21.
Equipped with a barrier fluid system that is
connected by a closed—vent system to a control
device that complies with the requirements of
Section 724.960; or
~j.
Equipped with a system that purges the
barrier
fluid into a hazardous wastestneam with no
detectable emissions to atmosphere.
çj
The barrier fluid must not be
a hazardous waste with
organic concentrations 10 percent or greater by weight.
~.j
Each barrier fluid system as described in subsections
(a) through
(c) must be equipped with a sensor that
will detect failure of the seal system, barrier fluid
system, on both.
31
Each sensor as required in subsection
(d) must be
checked daily or must be equipped with an audible
alarm that must be checked monthly to ensure that
it is functioning properly unless the compressor
is
located
within
the
boundary
of
an
unmanned
plant site,
in which case the sensor must be
121—307
159
checked daily.
21
The owner or operator shall determine, based on
design
considerations
and
operating
experience,
a,
criterion
that
indicates
failure
of
the
seal
system, the barrier fluid system. or both.
fj
If
the
sensor
indicates
failure
of
the
seal
system,
the
barrier
fluid
system,
or
both
based
on
the
criterion
determined
under
subsection
(e)
(2),
a
leak
is
detected.
gj
Repairs
31
When a
leak
is
detected,
it
must
be
repaired
as
soon as practicable,
but
not
later
than
15
calendar
days
after
it
is
detected,
except
as
provided
in
Section
724.959.
21
A first attempt at repair
(e.g., tightening the
packing
gland)
must
be
made
no
later
than
5
calendar
days
after
each
leak
is
detected.
~j
A compressor is exempt from the requirements of
subsections
(a)
and
(b)
if it is equipped with a
closed—vent system capable of capturing and
transporting any leakage from the seal to a control
device that complies with the requirements of Section
724.960, except as provided in subsection
(i).
j)
Any compressor that
is designated.
as described in
Section 724.964(g) (2). for no detectable emission as
indicated by
art. instrument reading of less than 500 ~pm
above background,
is exemPt from the requirements of
subsections
(a) through
(h)
if the compressor:
31
Isdetermined
to be
operating with no detectable
emissions,
as indicated by an instrument reading
of less than 500 ppm above background,
as measured
by the method specified in Section 724.963(c).
21
Is
tested
for compliance with subsection
(i) (1)
initially upon designation, annually and other
times
as
specified
in
the
RCRA
permit.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.954
Standards:
Pressure Relief Devices in Gas—
Vapor Service
~j
Except during pressure releases, each pressure relief
device in gas—vapor service must be operated with no
121—308
160
detectable emissions. as indicated by an instrument
reading
of
less
than
500
p~mabove
background
as
measured by the method specified in Section 724.963(c).
~
Actions
following
pressure
release.
31
After each pressure
release,
the pressure relief
device_must
be
returned
to
a
condition
of
no
detectable emissions, as indicated by an
instrument reading of less than 500 ppm above
background,
as
soon
as
practicable.
but
no
later
than
5
calendar
days
after
each
pressure
release.
except
as
provided
in
Section
724.959.
21
No later than
5 calendar days after the pressure
release, the pressure relief device must be
monitored to confirm the condition of no
detectable emissions, as indicated by an
instrument reading of less than 500 ppm above
background,
as measured by the method specified in
Section 724.963 (c).
~j
Any
pressure
relief
device
that
is
eaui~ped
with
a
closed—vent system capable of capturing and
transporting leakage from the pressure relief device to
a
control
device
as
described
in
Section
724.960
is
exemPt
from
the
requirements
of
subsections
(a)
and
(b).
Source:
Added at 15 Ill. Reg.
,
effective
Section 724.955
Standards:
Sampling Connecting Systems
~j
Each sampling connection system must be equipped with a
closed Purge sYstem or closed—vent system.
~kj
Each closed—purge system on closed—vent system as
required in subsection
(a) must:
31
Return the purged hazardous waste stream directly
to
the
hazardous
waste
management
process
line
with no detectable emissions to atmosphere; or
21
Collect and recycle the purged hazardous waste
stream with no detectable emissions to atmosphere
or
~
Be designed and operated to capture and transport
all the purged hazardous wastestream to
a control
device that complies with the requirements of
Section 724.960.
12 1—309
161
gj
In situ sampling systems are exempt from the
requirements of subsections
(a)
and
(b).
Source:
Added
at
15
Ill.
Reg.
,
effective
Section 724.956
Standards:
Open—ended Valves on Lines
~j
Equipment.
31
Each open—ended valve or line must be equipped
with a cap, blind flange. plug or a second valve.
21
The cap, blind flange, plug or second valve must
seal the open end at all times except during
operations requiring hazardous wastestream flow
through the open—ended valve or line.
~
Each open—ended valve or line equipped with a second
valve must be operated in a manner such that the valve
on the hazardous wastestream end is closed before the
second valve is closed.
~j
When
a
double
block
and
bleed
system
is being used, the
bleed valve or line
may
remain
open
during
operations
that require venting the line between the block valves
but must comply with subsection
(a) at all other times.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.957
Standards:
Valves in Gas-vapor or Light
Liquid
Service
~j
Each valve in gas-vapor or light liquid service must be
monitored monthly to detect leaks by the methods
specified
in
Section
724.963(b)
and
must comply with
subsections
(b) through
(e), except as provided in
subsections
(f),
(g)
and
(h), and in Section 724.961
and 724.962.
~j
If an instrument reading of 10.000 ppm or greaten is
measured,
a leak is detected.
Monitoring Frequency
31
Any
valve
for which a leak is not ~ietectedfor two
successive months must be monitored the first
month of
every
succeeding quarter, beginning with
the next quarter, until
a leak is detected.
121—310
162
21
If a leak is detected, the valve must be monitored
monthly until a leak is not detected for two
successive
months,
31
When a
leak
is
detected.
it must be repaired as
soon as practicable, but no later than 15 calendar
days after the leak is detected, except as
provided
in
Section
724,959.
21
A first attempt at repair must be made no later
than
5 calendar days after each leak is detected.
~j
First attempts at repair include, but are not limited
to the following best practices where practicable:
31
Tightening of bonnet bolts.
21
Replacement of bonnet bolts.
31
Tightening of packing gland nuts.
j)~.
Injection of lubricant into lubricated packing.
fi
Any
valve
that
is
designated,
as
described
in
Section
724.964(g) (2), for no detectable emissions,
as
indicated by an instrument reading of less than 500 ppm
above background,
is exempt from the requirements of
subsection
(a)
if the valve:
31
Has no external actuating mechanism in contact
with the hazardous wastestream.
21
Is operated with emissions less than 500 ppm above
background as determined by the method specified
in Section 724.963(c).
31
Is tested for compliance with subsection
(f) (2)
initially upon designation, annually, and at other
times as specified in the RCRA permit.
gI
Any valve that is designated,
as described in Section
724.964(h) (1), as an unsafe-to—monitor valve is exempt
from the requirements of subsection
(a),
if:
31
The owner or operator of the valve determines that
the_valve is unsafe to monitor because monitoring
personnel would be exposed to an immediate danger
as a consequence of complying with’ subsection
(a).
21
The owner or operator of the valve adheres to a
written plan that requires monitoring of the valve
as
frequently
as
practicable
during
safe—to—
121—311
163
monitor times.
~J
AnY valve that is designated, as described in Section
724.964(h)
(2),
as
a
difficult—to—monitor
valve
is
exempt from the requirements of subsection
(a).
if:
31
The owner or operator of the valve determines that
the
valve
cannot
be
monitored
without
elevating
the
monitoring
personnel
more
than
2
meters
above
a
support
surface
21
The
hazardous
waste
management
unit
within
which
the valve is located was in operation before June
21,
1990;
and
31
The owner or operator of the valve follows a
written plan that requires monitoring of the valye
at least once per calendar year.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.958
Standards:
Pumps, Valves, Pressure Relief
Devices and Other Connectors
~j
Pumps
and valves in heavy liquid service, pressure
relief
devices
in
light
liquid
or heavy liquid service
and flanges and other connectors must be monitored
within
5 days by the method specified in Section
724.963(b),
if evidence of a potential leak is found by
visual,
audible, olfactory,
on any other detection
method.
ki
If an instrument reading of 10,000 ppm on greater is
measured,
a
leak
is
detected.
gj
Repairs
31
When a
leak
is
detected,
it
must
be
repaired
as
soon_as practicable. but not later than 15
calendar days after
it
is
detected,
except
as
provided in Section 724.959.
21
The first attempt at repair must be made no
later
than
5 calendar days after each leak is detected.
~j
First attempts at repair include, but are not limited
to, the best practices described under Section
724.957(e)
Source:
Added at 15 Ill.
Reg.
,
effective
121—312
164
Section 724.959
Standards:
Delay of Repair
~j
Delay
of
repair
of equipment for which leaks have been
detected
is
allowed
if the repair is technically
infeasible without a hazardous waste management unit
shutdown.
In such a case,
repair of this equipment
must occur before the end of the next hazardous waste
management unit shutdown.
kI
Delay of repair of equipment for which leaks have been
detected
is allowed for equipment that is isolated from
the hazardous waste management unit and that does not
continue to contain or contact hazardous waste with
organic concentrations at least
10 percent by weight.
gI
Delay of repair for valves is allowed if:
31
The owner or operator determines that emissions of
purged material resulting from immediate repair
are greater than the emissions likely to result
from delay of repair.
21
When repair procedures are effected, the purged
material
is collected and destroyed or recovered
in a control device complying with Section
724.960.
~j.
Delay
of
repair
for
pumps
is
allowed
if:
31
Repair requires the use of a dual mechanical seal
system that includes a barrier fluid system.
21
Repair is completed as soon as practicable, but
not later than
6 months after the leak was
detected.
~j
Delay
of
repair
beyond
a hazardous waste management
unit shutdown is allowed for a valve if valve assembly
replacement is necessary during the hazardous waste
management unit shutdown, valve assembly supplies have
been depleted, and valve assembly supplies had been
sufficiently stocked before the supplies were depleted.
Delay of repair beyond the next hazardous waste
management unit shutdown is not allowed unless the next
hazardous waste management unit shutdown occurs sooner
than 6 months after the first hazardous waste
management unit shutdown.
Source:
Added at 15 Ill.
Reg.
,
effective
121—313
165
Section 724.960
Standards:
Closed-vent Systems and Control
Devices
Owners on operators of closed—vent systems and control devices
shall comply with the ~novisions of Section 724.933.
‘Source:
Added at 15 Ill. Reg.
,
effective
Section
724.961
Alternative
Percentage
Standard
for
Valves
~j
An
owner
on
operator
subiect
to
the
requirements
of
Section
724.957
may
elect
to
have
all
valves
within
a
hazardous
waste
management
unit
comply
with
an
alternative
standard
which
allows
no
greater
than
2
percent of the valves to leak.
ki
The following requirements must be met
if
an
owner
or
operator decides to comply with the alternative
standard of allowing 2 percent of valves to leak:
31
An owner or operator shall notify the Agency that
the owner or operator has elected to comply with
the requirements of this Section.
21
A
performance test as specified in subsection
(c)
must be conducted initially upon designation,
annually and other times specified in the RCRA
permit.
31
If a valve leak is detected it must be repaired in
accordance:with Section 724.957(d)
and
(e).
~
Performance tests must be conducted in the following
manner:
31
All valves subject to the requirements in Section
724.957 within the hazardous waste management unit
must be monitored within
1 week by the methods
specified in Section 724.963(b).
21
If an instrument reading of 10,000 ppm or greaten
is
measured,
a
leak
is
detected.
31
The leak percentage must be determined by dividing
the number of valves subject to the requirements
in Section 724.957 for which leaks are detected by
the total number of valves subject-to the
requirements in Section 724.957 within the
hazardous waste management unit.
~J
If an owner or operator decides to comply with this
121—314
166
Section no longer, the owner or operator shall notify
the Agency in writing that the work practice standard
described
in
Section
724.957(a)
through
(e)
will
be
followed.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.962
Skip Period Alternative for Valves
~j
Election
31
An
owner
or
operator
subject
to
the
requirements
of Section 724.957 may electfor all valves within
a hazardous waste management unit to comply with
one of the alternative work practices specified in
subsections
(b)(2)
and
(3).
21
An owner or operator shall notify the Agency
before implementing one of the alternative .work
practices.
~j
Reduced Monitoring
31
An owner or operator shall comply with the
requirements for valves,
as described in Section
724.957,
except as described in subsection
(b)(2)
and
(3).
21
After two consecutive quarterly leak detection
periods with the percentage of valves leaking
equal to on less than 2 percent,
an
owner
or
operator
may
begin
to
skip one of the quarterly
leak detection periods for the valves subject to
the requirements in Section 724.957.
31
After five consecutive quarterly leak detection
periods with the percentage of valves leaking
equal to on less than
2 percent, an owner on
operator may begin to skip three of the quarterly
leak detection periods for the valves subject to
the requirements in Section 724.957.
41
If the percentage of valves leaking is greater
than
2 percent,
the owner or operator shall
monitor monthly in compliance with the
requirements in Section 724.957, but may again
elect to use this Section after me’eting the
requirements of Section 724.957(c) (1).
Source:
Added at
15 Ill.
Reg.
,
effective
12 1—315
167
Section 724.963
Test
Methods
and
Procedures
~j
Each owner or operator subject to the provisions of
this
Subpart
shall
comply
with
the
test
methods
and
procedures
requirements
provided
in
this
Section.
ki
Leak
detection
monitoring,
as
required
in
Sections
724.952
through
724.962,
must
comply
with
the
following
requirements:
31
Monitoring
must comply with Reference Method 21 in
40
CFR
60,
incorporated
by
reference
in
35
Ill.
Adm.
Code
720.111.
21
The detection instrument must meet the performance
criteria
of
Reference
Method
21.
31
41
_____________
~j
When equipment is tested for compliance with no
detectable emissions,
as required in Sections
724.952(e), 724.953(i).
724.954 and 724.957(f), the
test must comply with the following requirements:
31
The requirements of subsections
(b) (1) through
(4).
apply.
21
The
background
level must be determined as set
forth in Reference Method 21.
31
The instrument probe must be trave~rsedaround all
potential leak interfaces as close to the
interface as possible as described in Reference
Method 21.
The instrument must be calibrated before use on
each day of its use by the procedures specified in
Reference
Method
21.
Calibration gases must be:
~j
Zero air (less than 10 ppm of hydrocarbon in
air).
~J
A mixture of methane or n—hexane and air at a
concentration of approximately, but less than
10,000 ppm methane or n—hexane.
The instrument probe must be traversed around all
potential leak interfaces as close to the
interface as possible as described in Reference
Method 21.
121—316
168
41
This arithmetic difference between the maximum
concentration indicated by the instrument and the
background level
is compared with 500 ppm for
determining compliance.
~,j
In accordance with the waste analysis plan required by
Section
724.113(b),
an
owner
or
operator
of a facility
shall determine,
for each piece of equipment, whether
the equipment contains on contacts
a
hazardous
waste
with organic concentration that equals or exceeds 10
percent by weight using the following:
31
Methods described in
ASTN
Methods
D
2267,
E
169,
E
168,
E 260 incorporated by reference in 35
Ill.
Adm. Code 720.111
21
Method 9060 or 8240 of SW-846, incorporated by
reference in 35
Ill. Adm. Code 720.111; on
31
Application of the knowledge of the nature of the
hazardous wastestream on the process by which it
was produced.
Documentation of a waste
determination by knowledge is required.
Examples
of documentation that must be used to support a
determination under this provision include
production process information documenting that no
organic compounds are used,
information that the
waste
is generated by a process that is identical
to
a
process
at
the
same
or
another
facility
that
has previously been demonstrated by direct
measurement to have a total organic content less
than 10 percent.
or
prior
speciation
analysis
results on the same wastestream where
it
is also
documented that no process changes have occurred
since that analysis that could affect the waste
total organic concentration.
g~
If an owner or operator determines that a piece of
equipment
contains on contacts a hazardous waste with
organic concentrations at least 10 percent by weight,
the determination can be revised only after following
the procedures in subsection
(d) (1) or
(2).
fl
When
an
owner on operator and the Agency do not agree
on whether a piece of equipment contains on contacts a
hazardous waste with organic concentrations at least 10
percent by weight, the procedures in subsection
(d) (U
or
(2) must be used to resolve the dispute.
gi
Samples used in determining the percent organic content
must be representative of the highest total organic
content hazardous waste that is expected to be
121—317
169
contained
in
or
contact
the
equipment.
~
To determine if pumps or valves are in light liquid
service. the vapor pressures of constituents must
either
be
obtained
from
standard
reference
texts
or
be
determined
by
ASTM
D-2879
incorporated
by
reference
in
35
Ill.
Adm.
Code
720.111.
31
Performance
tests
to
determine
if
a
control
device
achieves
95
weight
percent
organic
emission
reduction
must
comply
with
the
procedures
of
Section
724.934(c)(1)
through
(4).
Source:
Added
at
15
Ill.
Reg.
,
effective
Section 724.964
Recordkeeping Requirements
~j.
Lumping
Units
31
Each owner or operator subject to the provisions
of this Subpart shall comply with the
recordkeeping
requirements
of
this
Section.
2.1
An
owner
or operator of more than one hazardous
waste
management unit subject to -the provisions of
this Subpart may comply with the recordkeeping
requirements
for these hazardous waste management
units
in one recordkeeping system if the system
identifies each record by each hazardous waste
management unit.
kI
Owners
and
operators
shall
record
the
following
information in the facility operating record:
31
For each piece of equipment to which this Subpart’
applies:
~j.
~quipinentidentification number and hazardous
waste management unit identification.
~1
Approximate locations within the facility
(e.g.,
identify the hazardous waste
management unit on a facility clot plan).
~
Type of equipment
(e.g.,
a pump on pipeline
valve)
P1
Percent-by-weight total organics in the
hazardous wastestream at the equipment.
Hazardous waste state at the equipment (e.g
12 1—318
170
gas—vapor
or
liquid).
fi
Method of compliance with the standard (e.g..
“monthly leak detection and repair” or
“equipped with dual mechanical seals”).
21
for facilities than comely with the provisions of
Section
724 .933 (a) (2).
an
implementation
schedule
as specified in that Section.
31
Where
an
owner
or
operator
chooses
to
use
test
data
to
demonstrate
the
organic
removal
efficiency
or
total
organic
compound
concentration
achieved
by the control device,
a performance test plan as
specified in Section 724.935(b) (3).
41
Documentation of compliance with Section 724.960,
including the detailed design documentation or
performance test results specified in Section
724.935(b) (4).
gi
When each leak is detected as specified in Sections
724.952.
724.953, 724.957 or 724.958, the following
requirements apply:
31
A weatherproof and readily visible identification.
marked with the equipment identification number,
the date evidence of a potential leak was found
in
accordance with Section 724.958(a),
and the date
the leak was detected, must be attached to the
leaking equipment.
21
The identification on equipment except on a valve,
may be removed after it has been repaired.
31
The identification on a valve may be removed after
it has been monitored for 2 successive months as
specified in Section 724.957(c)
and no leak has
been detected during those
2 months.
~J.
When each leak is detected as specified in Sections
724.952,
724.953, 724.957 or 724.958, the following
information must be recorded in an inspection lo~and
must be kent in the facility operating record:
31
The instrument and operator identification numbers
and the equipment identification number.
21
The date evidence of a potential leak was found in
accordance with Section 724.958(a).
31
The date the leak was detected and the dates of
12 1—319
171
each attempt to reiair the leak.
41
Repair
methods
a~p1ied in
each
attempt
to
regain
the
leak.
~
“Above
10,000”,
if
the
maximum
instrument
reading
measured
by
the
methods
specified
in
Section
724.963(b)
after each repair attempt is equal to
or
~neaten
than
10.000
ppm.
j)
“Repair
delayed”
and
the
reason
for
the
delay
if
a
leak
is
not
repaired
within
15
calendar
days
after
discovery of the leak.
21
Documentation supporting the delay of repair of a
valve
in
compliance with Section 724.959(c).
~1
The signature of the owner or oPerator
(or
designate) whose decision it was that repair could
not
be
effected
without
a
hazardous
waste
management unit shutdown.
QJ..
The
expected
date of successful repair of the leak
if a leak is not repaired within 15 calendar days.
.lQ1
The date of successful repair of the leak.
~j
Design documentation and monitoring, operating and
inspection information for each closed—vent system and
control device required to com~lvwith the provisions
of Section 724.960 must be recorded and kept up-to-
date in the facility operating record as specified in
Section 724.935(c) (1) and
(2). and monitoring,
operating and inspection information in Section
724.935(c)(3)
through
(8).
.fj
For a control device other than a thermal vapor
incinerator,
catalytic
vapor
incinerator,
flare,
boiler, process heater, condenser, or carbon adsorption
system, the Agency shall specify the appropriate
necordkeeping requirements, indicating proper operation
and maintenance of the control device, in the RCRA
permit.
gj
The following information pertaining to all equipment
subject to the requirements in Sections 724.952 through
724.960 must be recorded in
a log that is kept in the
facility operating record:
31
A list of identification numbers for equipment
(except welded fittings)
subject to the
requirements of this Subpart.
12 1—320
172
21
List of Equipment
~j
A
list
of
identification
numbers
for
equipment that the owner on operator elects
to
designate
for
no
detectable
emissions,
as
indicated by an instrument reading of less
than 500 ppm above background, under the
provisions
of
Sections
724.952(e).
724.953(i)
and_724.957(f).
~j
The designation of this equipment as subject
to
the requirements of Sections 724.952(e),
724.953(i)
or
724.957(f)
must
be
signed
by
the owner or operator.
31
A list of equipment identification numbers for
pressure relief devices required to comply with
Section 724.954 (a).
41
Compliance tests.
~j
The dates of each compliance test required in
Sections 724.952(e),
724.953(i),
724.954 and
724.957(f).
~
The background level measured during each
compliance test.
~j
The maximum instrument reading measured at
the equipment during each compliance test.
,~j
A list of identification numbers for equipment in
vacuum service.
bi
The following information pertaining to all valves
subject to the requirements of Section 724.957(g)
and.
(h) must be recorded in a log that is kent in the
facility operating record:
31
A list of identification numbers for valves that
are_designated as unsafe to monitor,
an
explanation
for
each
valve stating why the valve
is
unsafe
to
monitor, and the plan for monitoring
each valve.
21
A list of identification numbers for valves that
are designated as difficult to monitor, an
explanation for each valve stating why the valve
is difficult to monitor,
and the planned schedule
for monitoring each valve.
121—321
173
31
The following information must be recorded in the
facility
operating
record
for
valves
complying
with
Section
724.962:
31
A schedule of monitoring.
21
The
percent
of
valves
found
leaking
during
each
monitoring
period.
jJ.
The following information must be recorded in a log
that
is
kent
in
the facility operating record:
31
Criteria
required
in
Section
724.952(d)
(5) (B) and
724.953(e)
(2)
and
an
explanation
of
the
design
criteria.
21
Any changes to these criteria and the reasons for
the changes.
çJ..
The following information must be recorded in a -log
that is kept in the facility operating record for use
in determining exemptions as provided in Section
724.950 and other specific Subparts:
31
An
analysis determining the design capacity of the
hazardous waste management unit.
21
A statement listing the hazardous waste influent
to and effluent from each hazardous waste
management unit subject to the requirements in
Sections 724.960 and an analysis determining
whether these hazardous wastes are heavy liquids.
31
An
up-to-date
analysis and the supporting
information and data used to determine whether on
not equipment is subject to the requirements in
Sections 724.952 through 724.960.
The record must
include
supporting
documentation
as
required
by
Section 724.963(d) (3) when application of the
knowledge of the nature of the hazardous
wastestream or the process by which it was
produced is used.
If the owner or operator takes
any action
(e.g.. changing the process that
produced the waste)
that could result in an
increase in the total organic content of the waste
contained in on contacted by equipment determined
not to be subject to the requirements in Sections
724.952 through 724.960, then a ne’~idetermination
is required.
31
Records of the equipment leak information required by
subsection
(d) and the operating information required
12 1—322
174
by subsection
(e) need be kept only 3 years.
~
The owner on operator of any facility that is subject
to this Subpart and to regulations at 40 CFR 60,
Subpart
VV,
or
40
CFR
61,
Subpart V. incorporated by
reference
in
35 Ill. Adm. Code
720.111,
may
elect
to
determine
compliance
with this Subpart by documentation
either pursuant to Section 724.964. or pursuant to
those provisions of 40 CFR 60 on 61. to the extent that
the documentation under the regulation at 40 CFR 60 or
61
duplicates
the
documentation
required
under
this
Subpart.
The
documentation
under
the
regulation
at
40
CFR
60
or
61
must
be
kept
with
or
made
readily
available with the facility operating record.
Source:
Added at 15 Ill. Reg.
effective
Section 724.965
Reporting Requirements
~j.
A semiannual report must be submitted by owners and
operators subject to the requirements of this Subpart
to the Agency by dates specified in the RCRA permit.
The report must include the following information:
31
The USEPA identification number
(35 Ill.
Adm. Code
722.112).
name, and address of the facility.
21
For each month during the semiannual reporting
period:
~j
The equipment identification number of each
valve for which a leak was not repaired as
required in Section 724.957(d).
~
The equipment identification number of each
pump for which a leak was not repaired as
required
in
Sections
724.952(c)
and
(d)(6).
çj
The equipment identification number of each
compressor for which a leak was not repaired
as required in Section 724.953(g).
31
Dates of hazardous waste management unit shutdowns
that occurred within the semiannual reporting
period.
41
For each month during the semiannual reporting
period,
dates when the control device installed as
required by Sections 724.952, 724.953, 724.954 or
724.955, exceeded or operated outside of the
design specifications as defined in Section
12
1—323
175
724.964(e) and as indicated by the control device
monitoring required by Section 724.960 and was not
corrected
within
24
hours.
the duration and cause
of
each
exceedance,
and
any
corrective
measures
taken.
ki
If. during the semiannual retorting period, leaks from
valves.
pumps and compressors are repaired as required
in
Sections
724.957(d).
724.952(c)
and
(d)(6).
and
724.953(g),
respectively,
and
the
control
device
does
not
exceed
or
oPerate
outside
of
the
design
specifications
as
defined
in
Section
724.964(e)
for
more
than
24
hours,
a
report to the Agency is not
required.
Source:
Added
at
15
Ill.
Reg.
,
effective
12 1—324
176
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE
G:
WASTE DISPOSAL
CHAPTER
I:
POLLUTION CONTROL BOARD
SUBCHAPTER
c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART
725
INTERIM
STATUS
STANDARDS
FOR
OWNERS
AND
OPERATORS
OF
HAZARDOUS
WASTE
TREATMENT,
STORAGE
AND
DISPOSAL FACILITIES
SUBPART A:
GENERAL PROVISIONS
Purpose,
Scope
and
Applicability
Imminent
Hazard
Action
SUBPART
B:
GENERAL
FACILITY
STANDARDS
Applicability
USEPA Identification Number
Required
Notices
General
Waste
Analysis
Security
General Inspection Requirements
Personnel Training
General Requirements for Ignitable, Reactive or
Incompatible Wastes
725.118
Location Standards
SUBPART C:
PREPAREDNESS
AND
PREVENTION
Section
725.130
Applicability
725.131
Maintenance and Operation of Facility
725.132
Required Equipment
725.133
Testing and Maintenance of Equipment
725.134
Access to Communications or Alarm System
725.135
Required Aisle Space
725.137
Arrangements with Local Authorities
SUBPART D:
CONTINGENCY
PLAN AND
EMERGENCY PROCEDURES
Applicability
Purpose and Implementation of Contingency Plan
Content of Contingency Plan
Copies of Contingency Plan
Amendment of Contingency Plan
Emergency Coordinator
Emergency Procedures
SUBPART E:
MANIFEST SYSTEM, RECORDKEEPING
AND
REPORTING
Applicability
Use of Manifest System
Manifest Discrepancies
Operating Record
Availability, Retention and Disposition of Records
Section
725.101
725.104
Section
725.110
725.111
725.112
725.113
725.114
725.115
725.116
725.117
Section
725. 150
725. 151
725.152
725. 153
725.154
725.155
725.156
Section
725.170
725.171
725. 172
725.173
725.174
121—325
177
725.175
725.176
725.
177
Section
725.190
725.
191
725.192
725.
193
725.194
Section
725.210
725.211
725.212
725.213
725.
2 14
725.215
725. 216
725.
2 17
725.218
725.219
725.220
Section
725.240
725.241
725.242
725.243
725.244
725.245
725.246
725.247
725.248
725.251
Section
725.270
725.271
725.272
725.273
725.274
725.276
725.277
Annual
Report
Unmanifested
Waste
Report
Additional Reports
SUBPART
F:
GROUNDWATER
MONITORING
Applicability
Groundwater
Monitoring
System
Sampling
and
Analysis
Preparation,
Evaluation
and
Response
Recordkeeping
and
Reporting
SUBPART
G:
CLOSURE
AND
POST-CLOSURE
Applicability
Closure Performance Standard
Closure
Plan;
Amendment
of
Plan
Closure; Time Allowed for Closure
Disposal or Decontamination of Equipment,
Structures
and
Soils
Certification of Closure
Survey Plat
Post—closure
Care and Use of Property
Post—closure
Plan;
Amendment
of
Plan
Post—Closure Notices
Certification of Completion of Post-Closure Care
SUBPART H:
FINANCIAL REQUIREMENTS
Applicability
Definitions of Terms as Used in this Subpart
Cost Estimate for Closure
Financial
Assurance
for Closure
Cost
Estimate for Post—closure Cane
Financial Assurance for Post—closure Monitoring and
Maintenance
Use of a Mechanism for Financial Assurance of Both
Closure and Post—closure Care
Liability
Requirements
Incapacity of Owners or Operators,
Guarantors
or
Financial Institutions
Promulgation of Forms
(Repealed)
SUBPART I:
USE AND MANAGEMENT OF CONTAINERS
Applicability
Condition of Containers
Compatibility of Waste with Container
Management
of
Containers
Inspections
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
121—326
178
SUBPART
J:
TANK
SYSTEMS
Section
725.290
725.291
725. 292
725.293
725.294
725.295
725.296
725.297
725. 298
725.299
725.300
725. 301
Section
725.320
725.321
725. 322
725. 323
725.325
725.326
725.328
725.329
725.330
Applicability
Assessment of Existing Tank System’s Integrity
Design and Installation
of
New
Tank
Systems on
Components
Containment
and
Detection
of
Releases
General
Operating
Requirements
Inspections
Response
to
leaks
on spills and disposition of Tank
Systems
Closure
and
Post—Closure
Care
Special Requirements for Ignitable on Reactive Waste
Special Requirements for Incompatible Wastes
Waste Analysis and Trial Tests
Generators of 100 to 1000
kg/mo.
SUBPART K:
SURFACE IMPOUNDMENTS
Applicability
Design Requirements
General Operating Requirements
Containment System
Waste Analysis and Trial Tests
Inspections
Closure and Post—Closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART L:
WASTE PILES
Section
725.350
725.351
725.352
725.353
725.354
725.356
725.357
725. 358
Applicability
Protection from Wind
Waste Analysis
Containment
Design Requirements
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Closure and Post—Closure Care
SUBPART M:
LAND TREATMENT
Applicability
General Operating Requirements
Waste Analysis
Food Chain Crops
Unsaturated Zone (Zone of Aeration) Norfitoring
Recordkeeping
Closure and Post—closure
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Section
725. 370
725. 372
725. 373
725.376
725. 378
725. 379
725.380
725.381
725. 382
121—327
179
SUBPART N:
LANDFILLS
Applicability
Design
Requirements
General
Operating
Requirements
Surveying and Recordkeeping
Closure
and
Post—Closure
Special
Requirements
for
Ignitable
or
Reactive
Waste
Special
Requirements
for
Incompatible
Wastes
Special
Requirements
for
Liquid
Wastes
Special
Requirements
for
Containers
Disposal
of
Small
Containers
of
Hazardous
Waste
in
Overpacked
Drums
(Lab
Packs)
SUBPART 0:
INCINERATORS
Applicability
Waste Analysis
General Operating Requirements
Monitoring and Inspection
Closure
Interim Status Incinerators Burning Particular
Hazardous Wastes
SUBPART P:
THERMAL TREATMENT
Other Thermal Treatment
General Operating Requirements
Waste Analysis
Monitoring and Inspections
Closure
Open Burning; Waste Explosives
Interim Status Thermal Treatment Devices Burning
Particular Hazardous Waste
SUBPART
Q:
CHEMICAL, PHYSICAL
AND BIOLOGICAL TREATMENT
Applicability
General Operating Requirements
Waste Analysis and Trial Tests
Inspections
Closure
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART R:
UNDERGROUND INJECTION
Section
725.530
Applicability
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
Section
725.400
725.401
725. 402
725.409
725.
4 10
725. 4
12
725. 413
725.
4 14
725.
4 15
725.416
Section
725.440
725.441
725.445
725.447
725.451
725.452
Section
725.470
725. 473
725.475
725.477
725.481
725.482
725.483
Section
725.500
725.501
725.502
725. 503
725.504
725.505
725.506
12 1—328
180
725.930
725.931
725.932
725.933
725.934
725.935
AP~1icability
Definitions
Standards:
Process Vents
Standards:
Closed—vent Systems and Control Devices
Test methods and procedures
Recordkeeping Requirements
SUBPART BB;
AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
725.950
725.951
725. 952
725.953
725. 954
725.955
725.956
725.957
725.958
725.959
725. 960
725.961
725.962
725.963
725.964
AP~licability
Definitions
Standards:
Pumps
in
Light
Liquid
Service
Standards:
Compressors
Standards:
Pressure Relief Devices in Gas/Vapor
Service
Standards:
Sampling Connecting Systems
Standards:
Open—ended Valves or Lines
Standards:
Valves in Gas/Vapor on Light Liquid Service
Standards:
Pumps, Valves, Pressure Relief Devices,
Flanges and Other Connectors
Standards:
Delay of Repair
Standards:
Closed—vent Systems and Control Devices
Percent Leakage Alternative for Valves
Skip Period Alternative for Valves
Test Methods and Procedures
Recordkeeping Requirements
Appendix A
Appendix B
Appendix
C
Appendix
D
Appendix E
Recordkeeping Instructions
EPA Report Form and Instructions
(Repealed)
EPA Interim Primary Drinking Water Standards
Tests for Significance
Examples of Potentially Incompatible Waste
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111—1/2,
pars.
1022.4 and 1027).
SOURCE:
Adopted in R8l-22,
43 PCB 427, at
5 Ill.
Reg.
9781,
effective as noted in 35 Ill.
Adm. Code~700.106; amended and
codified in R81—22,
45 PCB 317,
at 6 Ill. Reg. 4828,
effective as
noted in 35 Ill.
Adm. Code 700.106; amended in R82—18,
51 PCB
831,
at
7 Ill.
Reg.
2518, effective February 22,
1983;
amended
iii
R82—19,
53 PCB 131,
at
7
Ill.
Reg.
14034, effective October 12,
1983; amended in R84—9,
at
9 Ill.
Reg.
11869, effective July 24,
1985; amended in R85—22 at
10
Ill. Reg.
1085, effective January
2,
1986; amended in R86-l at 10 Ill. Reg.
14069, effective August
12,
1986;
amended in R86—28 at 11 Ill. Reg.
6044, effective March
24,
1987; amended in R86—46 at 11 Ill.
Reg.
13489, effective
August
4, 1987;
amended in R87—5 at 11
Ill. Reg.
19338,
effective
November 10,
1987; amended in R87—26 at
12 Ill. Reg.
2485,
effective January
15,
1988; amended in R87—39 at 12
Ill.
Reg.
13027, effective July 29,
1988;
amended in R88—l6 at 13
Ill.
Reg.
121—329
181
437, effective December 28,
1988; amended
in
R89—1
at
13
Ill.
Reg.
18354,
effective
November
13,
1989;
amended
in
R90—2
at
14
Ill.
Reg.
14447,
effective
August
22,
1990; amended in R90-10 at
14
Ill.
Reg.
16498,
effective
September
25,
1990;
amended in R90-
11 at 15 Ill. Reg.
,
effective
SUBPART
A:
GENERAL
PROVISIONS
Section
725.101
Purpose,
Scope
and
Applicability
a)
The
purpose
of
this
Part
is
to
establish
minimum
standards
which
define
the
acceptable
management
of
hazardous
waste
during
the
period
of
interim status and
until
certification
of
final
closure
or,
if the
facility is subject to post—closure requirements, until
post—closure responsibilities are fulfilled.
b)
The standards in this Part apply to owners and
operators of facilities which treat,
stone on dispose
of
hazardous waste who have fully complied with the
requirements for interim status under Section 3005(e)
of
the
Resource
Conservation and Recovery Act (RCRA)
(42 U.S.C.
6901 et seq.) and 35 Ill. Adm. Code 703,
until either a permit is issued under Section 3005
of
the Resource Conservation and Recovery. Act or Section
21(f)
of the Environmental Protection Act, on until
applicable closure and post—closure responsibilities
under this Part are fulfilled, and to those owners and
operators of facilities in existence on November 19,
1980, who have failed to provide timely notification as
required by Section
3010(a)
of
RCRA,
on failed to file
Part
A
of
the Permit Application as required by 40 CFR
270.10(e)
and
(g)
or 35 Ill. Adm. Code 703.150 and
703.152.
These standards apply to all treatment,
storage on disposal of hazardous waste at these
facilities after November 19,
1980, except as
specifically provided otherwise in this Pant on 35 Ill.
Adm.
Code
721;
BOARD NOTE:
As stated in Section 3005(a)
of RCRA,
after the effective date of regulations under that
Section,
i.e.,
40 CFR 270 and 124, the treatment,
storage on disposal of hazardous waste is prohibited
except in accordance with a permit.
Section 3005(e) of
RCRA
provides for the continued operation of an
existing facility which meets certain conditions until
final administrative disposition of the-owner’s and
operator’s permit application is made.
35
Ill. Adm.
Code 703.140 et seq. provide that a permit is deemed
issued under Section 21(f) (1) of the Environmental
Protection Act under conditions similar to federal
12 1—230
182
interim
status.
c)
The
requirements
of
this
Part
do
not
apply
to:
1)
A
person
disposing
of
hazardous
waste
by
means
of
ocean
disposal
subject
to
a
permit
issued
under
the
Marine
Protection,
Research
and
Sanctuaries
Act
(16
U.S.C.
1431—1434;
33
U.S.C.
1401);
BOARD
NOTE:
This
Part
applies
to
the
treatment
or
storage
of
hazardous
waste
before
it
is
loaded
into
an
ocean
vessel
for
incineration
or
disposal
at
sea,
as
provided
in
subsection
(b).
3)
The
owner
or
operator
of
a
POTW
(publicly
owned
treatment works) which treats,
stones on disposes
of hazardous waste;
BOARD NOTE:
The owner or operator of a facility
under subsections
(c) (1) through
(c) (3)
is -subject
to the requirements of 35 Ill. Adm. Code 724 to
the extent they are included in a permit by rule
granted to such a person under 35 Ill. Adm. Code
702 and 703 or are required by 35 Ill. Adm. Code
704.Subpart
F.
5)
The owner or operator of a facility permitted,
licensed on registered by Illinois to manage
municipal or industrial solid waste,
if the only
hazardous waste the facility treats, stones or
disposes of is excluded from regulation under this
Part by 35 Ill. Adm. Code 721.105;
6)
The owner or operator of
a facility managing
recyclable materials described in 35 Ill.
Adm.
Code 721.106(a) (2) and
(3)
(except to the extent
that requirements of this Pant are referred to in
35 Ill.
Adm. Code 726.Subparts
C,
D,
F or G;
7)
A generator accumulating waste on—site in
compliance with 35 Ill. Adm. Code 722.134, except
to the extent the requirements are included in 35
Ill. Adm. Code 722.134;
8)
A farmer disposing of waste pesticides from the
farmer’s own use in compliance with 35 Ill. Adm.
Code 722.170;
9)
The owner on operator of a totally enclosed
treatment facility,
as defined in 35 Ill.
Adm.
Code 720.110;
12 1—231
183
10)
The
owner
or
operator
of
an
elementary
neutralization
unit
or
a
wastewater
treatment
unit
as
defined
in
35
Ill.
Adm.
Code
720.110;
11)
Immediate
response:
A)
Except
as
provided
in
subsection
(C)
(11) (B),
a
person
engaged
in
treatment
or
containment
activities
during
immediate
response
to
any
of
the
following
situations:
i)
A
discharge
of
a
hazardous
waste;
ii)
An imminent and
substantial
threat
of
a
discharge
of
a
hazardous
waste;
iii) A discharge of a material which, when
discharged,
becomes
a
hazardous
waste.
B)
An
owner
or
operator
of
a
facility
otherwise
regulated by this Pant must comply with all
applicable requirements of Subparts C and D.
C)
Any person who is covered by subsection
(c) (11) (A) and who continues on initiates
hazardous waste treatment or containment
activities
after
the
immediate
response
is
oven
is
subject
to
all
applicable
requirements of this Part and 35 Ill.
Adm.
Code
702,
703
and
705 for those activities.
12)
A transporter storing manifested shipments of
hazardous waste in containers meeting the
requirements of 35 Ill. Adm. Code 722.130 at a
transfer facility for a period of ten days or
less.
13)
The
addition
of
absorbent
material
to
waste
in
a
container (as defined in 35 Ill. Adm. Code
720.110), or the addition of waste to the
absorbent material in a container,
provided that
these
actions
occur
at
the
time
waste
is
first
placed
in
the
containers;
and
Sections
725.117(b),
725.271
and
725.272
are
complied
with.
d)
The following hazardous wastes must not be managed at
facilities subject to regulation under this Part:
hazardous waste numbers F020,
F02l,
F022,
F023,
F026 or
F027 unless:
1)
The wastewater treatment sludge is generated in a
surface impoundment as part of the plant’s
12 1—332
184
wastewater treatment system;
2)
The waste is stored in tanks or containers;
3)
The waste is stored on treated in waste piles that
meet the requirements of 35 Ill.
Adin. Code
724.350(c) as well as all other applicable
requirements
of
Subpart
L;
4)
The waste is burned in incinerators that are
certified
pursuant
to
the
standards
and
procedures
in
Section
725.452;
or
5)
The waste is burned in facilities that thermally
treat
the
waste
in
a
device
other
than
an
incinerator and that are certified pursuant to the
standards and procedures in Section 725.483.
e)
This
Part
applies
to
owners
and operators of facilities
which
treat,
stone
on
dispose
of
hazardous
wastes
referred
to
in
35
Ill. Adm. Code 728, and the 35 Ill.
Adm. Code 728 standards are considered material
conditions or requirements of the interim status
standards of this Part.
f)
35 Ill. Adm. Code 700 contains rules concerning
application of other Board regulations.
‘Source:
Amended at 15 Ill.
Reg.
,
effective
SUBPART B:
GENERAL FACILITY STANDARDS
Section 725.113
General Waste Analysis
a)
Waste analysis:
1)
Before an owner or operator treats,
stores or
disposes of any hazardous waste,
or non—hazardous
waste if applicable under Section 725.213(d),
the
owner or operator shall obtain a detailed chemical
and physical analysis of a representative sample
of the waste.
At a minimum,
this analysis must
contain all the information which must be known to
treat, store or dispose of the waste in accordance
with the requirements of this Part and 35 Ill.
Adm. Code 728.
2)
The analysis may include data developed under 35
Ill.
Adm. Code 721 and existing published or
documented data on the hazardous waste or on waste
121—333
185
generated
from
similar
processes.
BOARD NOTE:
For example, the facility’s record of
analyses performed on the waste before the
effective
date
of
these
regulations
or
studies
conducted
on
hazardous
waste
generated
from
processes
similar
to
that
which
generated
the
waste
to
be
managed
at
the
facility
may
be
included
in
the
data
base
required
to
comply
with
subsection
(a)
(1).
except
as
otherwise
s~ecifled
in 35 Ill.
Adm. Code 728.107(b) and
(c).
The
owner
or
operator
of
an
off—site
facility
may
arrange
for
the
generator
of
the
hazardous
waste
to
supply
part
or
all
of
the
information
required
by subsection
(a) (1).
If the generator does not
supply the information and the owner or operator
chooses to accept a hazardous waste, the owner on
operator
is
responsible
for
obtaining
the
information required to comply with this Section.
3)
The analysis must be repeated as necessary to
ensure that
it
is
accurate
and
up
to
date.
•At
a
minimum,
the
analysis
must
be
repeated:
A)
When the owner or
operator
is
notified,
or
has reason to believe, that the process or
operation generating the hazardous waste, or
non—hazardous waste if applicable under
Section 725.213(d), has changed; and
B)
For off-site facilities, when the results of
the
inspection
required
in
subsection,
(a)
(4)
indicate that the hazardous waste received at
the facility does not match the waste
designated on the accompanying manifest or
shipping paper.
4)
The
owner
on
operator
of
an
off—site
facility
shall inspect and,
if
necessary,
analyze
each
hazardous
waste
movement
received
at
the
facility
to
determine
whether
it matches the identity of
the waste specified on the accompanying manifest
or
shipping
paper.
b)
The owner or operator shall
develop
and
follow
a
written
waste
analysis
plan
which
describes
the
procedures
which
the
owner
or
operator
will carry out
to
comply
with
subsection
(a).
The
owner
or
operator
shall
keep
this
plan
at
the
facility.
At
a
minimum,
the plan must specify:
1)
The
parameters
for
which
each
hazardous
waste,
on
12 1—334
186
non—hazardous
waste
if
applicable
under
Section
725.213(d), will be analyzed and the rationale for
the
selection
of
these
parameters
(i.e.,
how
analysis
for
these
parameters
will
provide
sufficient information on the waste’s properties
to comply with subsection
(a).
2)
The test methods which will be used to test for
these
parameters.
3)
The
sampling
method
which
will
be
used
to
obtain
a
representative
sample
of
the
waste
to
be
analyzed.
A
representative
sample
may
be
obtained
using
either:
A)
One of the sampling methods described in 35
Ill.
Adm.
Code
721.Appendix
A
or
B)
An equivalent sampling method.
BOARD NOTE:
See 35
Ill. Adm. Code 720.120(c)
for related discussion.
4)
The frequency with which the initial analysis of
the waste will be reviewed or repeated to ensure
that the analysis is accurate and up—to—date.
5)
For off-site facilities,
the waste analyses that
hazardous waste generators have agreed to supply.
6)
Where
applicable,
the
methods
which
will
be
used
to
meet
the
additional
waste
analysis
requirements
for specific waste management methods as specified
in Sections 725.293, 725.325,
725.352,
725.373,
725.414, 725.441, 725.475~and 725.502,
725.934(d)
and 725.963(d),
and 35 Ill.
Adm.
Code
728.107.
And,
7)
For surface impoundments exempted from land
disposal
restrictions
under
35
Ill.
Adm.
Code
728.104(a), the procedures and schedules for:
A)
The sampling of impoundment contents;
B)
The analysis of test data;
and,
C)
The annual removal of residues which are not
delisted under 35 Ill. Adm. Cbde 720.122 or
which exhibit a characteristic of hazardous
waste, and either:
I)
Do not meet applicable treatment
121—335
187
standards
of
35 Ill. Adm. Code
723.Subpart
D;
or
ii)
Where
no
treatment
standards
have
been
established:
Such
residues
are
prohibited
from
land
disposal
under
35
Ill.
Adin.
Code
728.132
or
728.139;
or
such
residues
are
prohibited
from
land
disposal
under
35
Ill.
Adm.
Code
728.133(f).
c)
For off-site facilities, the waste analysis plan
required
in
subsection
(b)
must
also
specify
the
procedures
which
will
be
used
to
inspect
and,
if
necessary,
analyze
each
movement
of
hazardous
waste
received at the facility to ensure that it matches the
identity of the waste designated on the accompanying
manifest
on
shipping
paper.
At
a
minimum,
the
plan
must
describe:
1)
The
procedures
which
will
be
used
to
determine
the
identity
of
each
movement
of
waste
managed
at
the
facility; and
2)
The sampling method which will be used to obtain a
representative
sample
of the waste to be
identified,
if the identification method includes
sampling.
Source:
Amended at 15 Ill. Reg.
,
effective
Section 725.115
General Inspection Requirements
a)
The owner or operator shall inspect the facility for
malfunctions and deterioration, operator errors and
discharges which may be causing
——
or may lead to
——
the conditions listed below.
The owner or operator
shall conduct these inspections often enough to
identify problems in time to correct them before they
harm human health or the environment.
1)
Release of hazardous waste constituents to the
environment or
2)
A threat to human health.
b)
1)
The owner or operator shall develop and follow a
written schedule for inspecting all monitoring
equipment,
safety and emergency equipment,
security devices and operating and structural
equipment (such as dikes and sump pumps)
that are
12 1—336
188
important to preventing, detecting or responding
to environmental or human health hazards.
2)
The owner or operator shall keep this schedule at
the facility.
3)
The schedule must identify the
types
of
problems
(e.g.,
malfunctions
or
deterioration)
which
are
to
be
looked
for
during
the
inspection
(e.g.,
inoperative
sump
pump,
leaking
fitting,
eroding
dike,
etc.).
4)
The frequency of inspection may vary for the items
on the schedule.
However,
it
should
be
based
on
the rate of possible deterioration of the
equipment and the probability of an environmental
or
human
health
incident
if
the
deterioration
on
malfunction on any operator error goes undetected
between
inspections.
Areas
subject
to
spills,
such as loading and unloading areas, must be
inspected
daily
when
in
use.
At
a
minimum,
the
inspection schedule must include the items and
frequencies called for in Sections 725.274,
725.293,
725.295, 725.326, 725.447, 725.477~end
725.503.
725.933, 725.952,
725.953 and 725.958.
c)
The
owner
or
operator
shall remedy any deterioration or
malfunction of equipment or structure which the
inspection reveals on a schedule which ensures that the
problem does not lead to an environmental or human
health hazard.
Where a hazard is imminent or has
already occurred, remedial action must be taken
immediately.
d)
The owner or operator shall record inspections in an
inspection log or summary.
The owner on operator shall
keep these records for at least three years from the
date of inspection.
At a minimum, these records must
include the date and time of the inspection,
the name
of the inspector,
a notation of the observations made
and the date and nature of any repairs or other
remedial actions.
Source:
Amended at 15
Ill.
Reg.
,
effective
SUBPART E:
MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 725.173
Operating Record
a)
The owner or operator shall keep a written operating
record at the facility.
12 1—337
189
b)
The following information must be recorded as it
becomes
available
and
maintained
in
the
operating
record
until
closure
of
the
facility.
1)
A
description
and
the
quantity
of
each
hazardous
waste received and the method or methods and date
or dates of its treatment, storage or disposal at
the facility as required by Appendix A;
2)
The location of each hazardous waste within the
facility and the quantity at each location.
For
disposal facilities the location and quantity of
each hazardous waste must be recorded on a map or
diagram of each cell or disposal area.
For all
facilities this information must include cross—
references to specific manifest document numbers
if the waste was accompanied by a manifest;
BOARD NOTE:
See Sections 725.219, 725.379 .and
725.409 for related requirements.
3)
Records and results of waste analysis and trial
tests performed as specified in Sections 725.113,
725.293, 725.325, 725.352,
725.373, 725.414,
725.441, 725.475~end
725.502,
725.934 and 725.963
and 35 Ill. Adm. Code 728.104(a)
and 728.107;
4)
Summary reports and details of all incidents that
require implementing the contingency plan as
specified in Section 725.156(j);
5)
Records and results of inspections as required by
Sections 725.115(d)
(except these data need be
kept
only
three
years);
6)
Monitoring,
testing
on
analytical
data
where
required by Sections 725.190,
725.194,
725.291,
725.293,
725.295,
725.376,
725.378,
725.380(d)(1),
725.447~~a-nd725.477. 725.934(c) throu~h (f),
725.935,
725.963(d) through
(i) and 725.964
BOARD NOTE:
As required by Section 725.194,
monitoring data at disposal facilities must be
kept throughout the post-closure period.
7)
All closure cost estimates under Section 725.242
and, for disposal facilities, all post—closure
cost estimates under Section 725.244;
8)
Records of the quantities
(and date of placement)
for each shipment of hazardous waste placed in
121—33
8
190
land disposal units under an extension of the
effective date of any land disposal restriction
granted pursuant to 35 Ill. Adm. Code 728.105, a
petition
pursuant
to
35 Ill. Adm. Code 728.106 on
a
certification
under
35
Ill.
Adin.
Code
728.108,
and the applicable notice required of a generator
under 35 Ill.
Adm. Code 728.107(a);
9)
For
an
off-site
treatment
facility,
a
copy
of
the
notice, and the certification and demonstration,
if
applicable,
required
of
the
generator
on
the
owner or operator under 35 Ill.
Adm. Code 728.107
or 728.108;
10)
For an on-site treatment facility, the information
contained
in
the
notice
(except
the
manifest
number), and the certification and demonstration,
if applicable,
required of the generator on the
owner on operator under 35
Ill. Adm. Code 728.107
or 728.108;
11)
For an off—site land disposal
facility,
a copy of
the notice, and the certification and
demonstration,
if
applicable,
required
of
the
generator
or
the
owner
on
operator
of
a
treatment
facility under 35 Ill. Adm. Code 728.107 or
728.108, whichever is applicable; and
12)
For an on-site land disposal facility, the
information contained in the notice required of
the
generator
or
owner
on
operator
of
a
treatment
facility under 35 Ill.
Adm. Code 728.107, except
for the manifest number, and the certification and
demonstration,
if applicable,
required under 35
Ill. Adm. Code 728.108, whichever is applicable.
13)
For
an
off-site
storage facility,
a copy of the
notice, and the certification and demonstration if
applicable,
required of the generator on the owner
or operator under 35 Ill.
Adm. Code 728.107 on
728.108; and,
14)
For an on-site storage facility, the information
contained in the notice (except the manifest
number), and the certification and demonstration
if applicable, required of the generator on the
owner on operator under 35 Ill. Adm. Code 728.107
or 728.108.
Source:
Amended
at
15
Ill.
Reg.
,
effective
121—339
191
Section 725.177
Additional Reports
In addition
to
submitting
the
annual
report
and
unmanifested
waste reports described in
ffSections
725.175
and
725.176,
the
owner or operator muatshall also report to the DirectorAgency:
a)
Releases,
fires and explosions as specified in -s-Section
725.156(j)
;
b)
Groundwater contamination and monitoring data
as
specified in ffSection 725.193 and 725.194; end
c)
Facility closure as specified in *Section 725.2l5-r; and
~
As
otherwise required by Subparts AA and BB.
Source:
Amended at 15 Ill. Reg.
,
effective
SUBPART K:
SURFACE IMPOUNDMENTS
Section 725.329
Special Requirements for Ignitable or
Reactive Waste
Ignitable or reactive waste must not be placed in a surface
impoundment, unless the waste and impoundment satisfy all
applicable requirements of 35 Ill.
Adm. Code 728,
and:
a)
The waste is treated, rendered or mixed before on
immediately after placement in the impoundment so that
1)
The resulting waste, mixture on dissolution of
material no longer meets the definition of
ignitable on reactive waste under 35 Ill. Adm.
Code 721.121 on 721.123; and
2)
Section
725.117(b)
is
complied
with;
or
b)
Management conditions.
1)
The waste is managed in such a way that it
is
protected from any material or conditions which
may
cause
it
to
ignite
on
react;
and
2)
The
owner
or
operator
obtains
a
certification
from
a qualified chemist on engineer that,
to the best
of
the
chemist
or
engineer’s knowledge and
opinion, the design features on operating plans of
the facility will prevent ignition or reaction;
and
3)
The certification and the basis for it are
12 1—340
192
maintained
at
the
facility;
or
c)
The
surface
impoundment
is
used
solely
for
emergencies.
Source:
Amended at 15 Ill.
Reg.
,
effective
SUBPART
L:
WASTE PILES
Section 725.356
Special Requirements for Ignitable or
Reactive Waste
Ignitable or reactive wastes must not be placed in a pile unless
the waste and pile meet all applicable requirements of 35 Ill.
Adm. Code 728,
and:
a)
Addition of the waste to an existing pile~
1)
Results in the waste or mixture no longer meeting
the definjtion of ignitable or reactive waste
under ff35 Ill.
Adm. Code 721.121 on 72l.123j. and
2)
Complies with *Section 725.117(b); or
b)
The waste is managed in such a way that it is protected
from any material or conditions which may cause it to
ignite or react.
Source:
Amended at 15
Ill. Reg.
,
effective
SUBPART M:
LAND
TREATMENT
Section 725.381
Special Requirements for Ignitable or
Reactive Waste
Ignitable on rcactive wa3tes must not bc land treatcd un1ess:I~
owner or operator shall not apply ignitable or reactive waste to
the treatment zone unless unless the waste and treatment zone
meet all applicable requirements of
35 Ill.
Adm. Code 728.
and:
a)
The waste is immediately incorporated into the soil so
that:
1)
The resulting waste, mixture on dissolution of
material no longer meets the definition of
ignitable or reactive waste under section 725.121
e~35
Ill. Adm. Code 721.121 or 721.123; and
2)
Section ~-2-&724.ll7(b)is complied with;
or
12 1—341
193
b)
The
waste
is
managed
in
such
a
way
that
it is protected
from
any
material
or
conditions
which
may
cause
it
to
ignite
or
react.
Source:
Amended
at
15
Ill.
Reg.
•
effective
SUBPART
N:
LANDFILLS
Section
725.412
a)
b)
Special
Requirements
for
Ignitable
or
Reactive
Waste
effective
Disposal of Small Containers ~f Hazardous
Waste in Overpacked Drums
(Lab Packs)
Small
containers
of
hazardous
waste
in
overpacked
drums
(lab
packs)
may
be
placed
in
a
landfill
if
the
following
requirements
Except
as
provided
in
panagraphsubsection
(b)
and
in
Sec’tion 725.416,
ignitable or reactive waste must not
be placed in a landfill, unless the waste and landfill
meets all applicable requirements
of
35
Ill. Adm.
Code
728, and the waste is treated, rendered or
mixed
befor~
or immediately after placement
in
a
landfill
so
that:
1)
The resulting waste, mixture or dissolution
of
material no longer meets the definition of
ignitable or reactive waste under 35 Ill.
Adiu.
Code 721.121 on 721.123; and
2)
Section 725.117(b)
is complied with.
~Except
for prohibited wastes which remain subject t~
treatment standards in
35 Ill.
Adm. Code 728.Subpart
D,
jgnitable waste in containers may be landfilled without
meeting the requirements of paragnaphsubsection
(a),
provided that the wastes are disposed of in such a way
that they are protected from any material or conditions
which may cause them to ignite.
At a minimum,
ignitable wastes must be disposed of in non-leaking
containers which are carefully handled and placed so as
to avoid heat,
sparks, rupture on any o’ther condition
that might cause ignition of the wastes; must be
covered daily with soil or other non—combustible
material to minimize the potential for ignition of the
wastes; and must not be disposed in cells that contain
or will contain other wastes which may generate heat
sufficient to cause ignition of the waste.
Source:
Amended
at
15
Ill.
Reg.
Section 725.416
121—342
194
are met:
a)
Hazardous
waste
must
be
packaged
in
non—leaking
inside
containers.
The
inside
containers
must
be
of a design
and constructed of a material that will not react
dangerously with, be decomposed by or be ignited by the
contained waste.
The inside containers must be tightly
and securely sealed.
The inside containers must be of
the size and type specified in the Department of
Transportation (DOT) hazardous materials regulations
(49 CFR 173,
178 and 179, incorporated by reference in
35 Ill. Adm. Code 720.111),
if those regulations
specify a particular inside container for the waste.
b)
The inside containers must be overpacked in an open
head DOT-specification metal shipping container (49 CFR
178 and 179) of no more than 416 liter
(110 gallon)
capacity and surrounded by, at a minimum,
a sufficient
quantity of absorbent material to completely absorb all
of the liquid contents of the inside containers.
The
metal outer container must be full after packing with
inside containers and absorbent material.
c)
In accordance with Section 725.117(b),
the absorbent
material used must not be capable of reacting
dangerously with,
being decomposed by or being ignited
by
the contents of the inside containers.
d)
Incompatible
waste,
as
defined
in
35
Ill.
Adm.
Code
720.110,
must
not
be
placed
in
the
same
outside
container.
e)
Reactive wastes,
other than cyanide— or sulfide—beaning
waste as defined in 35 Ill. Adm. Code 721.123(a) (5),
must be treated or rendered non—reactive prior to
packaging in accordance with paragraphsubsections
(a)
through
(d).
Cyanide- and sulfide-bearing neacitve
waste
may
be
packed
in
accordance
with
panagraphsubsections
(a) through
(d) without first
being
treated
or
rendered
non—reactive.
fi
Such disposal
is
in compliance with the requirements
of..
35
Ill.
Adm.
Code
728.
Persons
who
incinerate
lab
packs according to the requirements of 35 Ill. Adm.
Code
728.142(c)
(1)
may
use
fiber
drums
in
place
of
metal outer containers.
Such fiber drums must meet the
DOT
specifications in 49 CFR 171.12 and be overpacked
according to subsection
(b).
g)
Pursuant to 35
Ill. Adm. Code 729.312, the use of
labpacks for disposal of liquid wastes or wastes
containing free liquids allowed under this Section is
12 1—343
195
restricted
to
labwaste
and
non—periodic
waste,
as
those
terms
are
defined
in
that
Part.
Source:
Amended
at
15
Ill.
Reg.
,
effective
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS
VENTS
Section
725.930
Applicability
a)
This
Subpart
applies
to
owners
and
operators
of
facilities
that
treat,
store
or
dispose
of
hazardous
wastes
(except
as
provided
in
Section
725.101).
b)
Except
for
Sections
725.934(d)
and
725.935(e),
this
Subpart applies to process vents associated with
distillation, fractionation, thin-film evaporation,
solvent
extraction,
on
air
or
steam
stripping
operations that manage hazardous wastes with organic
concentrations
of
at
least
10
ppmw
(parts
per
million
by
weight),
if
these
operations
are
conducted
in:
1)
Units
that
are
subject
to
the
permitting
requirements
of
35
Ill.
Adm.
Code
703;
or
2)
Hazardous waste recycling units that are located
on
hazardous
waste
management
facilities
otherwise
subject to the permitting requirements of 35
Ill.
Adm.
Code
703.
BOARD
NOTE’:
The
requirements
of
Sections
725.932
through
725.936
apply
to
process
vents
on
hazardous waste recycling units previously exempt
under
35
Ill.
Adm.
Code
72l.106(c)(l).
Other
exemptions
under
35
Ill.
Adm.
Code
721.104,
722.134
and
725.101(c)
are
not
affected
by
these
requirements.
C)
Agency
decisions
pursuant
to
this
Part
must
be
made
in
writing,
are
in
the
nature
of
permit
decisions
pursuant
to Section 39 of the Environmental Protection Act and
may be appealed to the Board pursuant to 35 Ill. Adm.
Code 105.
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.931
Definitions
As used in this Subpart,
all terms not defined in the Subpart
have the meaning given them in 35
Ill. Adm.
Code 724.931, the
121—344
196
Resource Conservation and Recovery Act and 35
Ill.
Adm. Code 720
through 726.
BTU
means British thermal unit.
ft
means
foot.
h
means
hour.
kg means kilogram.
kPa means kilopascals.
lb
means
pound.
m means meter.
Mg means Megagrams,
or
metric tonnes.
NJ means Megajoules,
or ten to the sixth Joules.
NW means Megawatts.
ppmv means parts per million by volume.
ppmw meant parts per million by weight.
s means second.
scm means standard cubic meter.
scft meant standard cubic foot.
yr
means
year.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 725.932
Standards: Process Vents
a)
The owner or operator
of
a facility with process vents
associated with distillation, fractionation, thin—film
evaporation, solvent extraction,
or air or steam
stripping operations managing hazardous wastes with
organic concentrations of at least
10 ppmw shall
either:
1)
Reduce total organic emissions from all affected
process vents at the facility below 1.4 kg/h
(3
lb/h)
and 2.8 Mg/yr (3.1 tons/yr); on
2)
Reduce, by use of a control device, total organic
121—345
197
emissions
from
all
affected
process
vents
at
the
facility by 9~weight percent.
b)
If the owner on operator installs a closed-vent system
and
control
device
to
comply
with
the
provisions
of
subsection
(a),
the
closed—vent
system
and
control
device must meet the requirements of Section 725.933.
c)
Determinations
of
vent
emissions
and
emission
reductions
on
total
organic
compound
concentrations
achieved
by
add-on
control
devices
must
be
based
on
either
engineering
calculations
or
performance
tests.
If
performance
tests
are
used
to
determine
vent
emissions,
emission
reductions,
or
total
organic
compound concentrations achieved by add—on control
devices, the performance tests must conform with the
requirements of Section 725.934(c).
d)
When
an
owner
or
operator
and
the
Agency
do
not
agree
on
determinations
of
vent
emissions
on
emission
reductions
or
total
organic
compound
concentrations
achieved
by
add—on
control
devices
based
on
engineering
calculations,
the
test
methods
in
Section
725.934(c)
must
be
used
to
resolve
the
disagreement.
Source:
Added
at
15
Ill.
Reg.
,
effective
Section 725.933
Standards:
Closed-vent Systems and Control
Devices
a)
Compliance Required.
1)
Owners on operators of closed—vent systems and
control devices used to comply with provisions of
this
Part
shall
comply
with
the
provisions
of
this
Section.
2)
The owner
on
operator
of
an
existing
facility
who
cannot install a closed—vent system and control
device to comply with the provisions of this
Subpart on the effective date that the facility
becomes subject to the provisions of this Subpart
shall prepare an implementation schedule that
includes dates by which the closed—vent system and
control device will be installed and in operation.
The controls must be installed as soon as
possible, but the implementation sthedule may
allow up to 18 months after the effective date
that the facility becomes subject to this Subpart
for installation and startup.
All units that
begin operation after December 21,
1990, must
12 1—346
198
comply
with
the
rules
immediately
(i.e.,
must
have
control devices installed and operating on startup
of
the
affected
unit);
the
2-year
implementation
schedule does not apply to these units.
b)
A control device involving vapor recovery (e.g.,
a
condenser
or
adsonber)
must
be
designed
and
operated
to
recover
the
organic
vapors
vented
to
it
with
an
efficiency
of
95
weight
percent
or
greater
unless
the
total
organic
emission
limits
of
Section
725.932(a)
(1)
for
all
affected
process
vents
is
attained
at
an
efficiency
less
than
95
weight
percent.
c)
An
enclosed
combustion
device
(e.g.,
a
vapor
incinerator, boiler on process heater)
must
be
designed
and operated to reduce the organic emissions vented to
it by 95 weight percent or greater; to achieve a total
organic compound concentration of 20 ppmv, expressed as
the sum of the actual compounds, not carbon
equivalents, on a dry basis corrected to
3 percent
oxygen; on to provide a minimum residence time of 0.50
seconds at
a minimum temperature of 760 C.
If a boiler
or process heater is used as the control device, then
the vent stream must be introduced into the flame
combustion zone of the boiler or process heater.
d)
Flares
1)
A flare must be designed for and operated with no
visible emissions as determined by the methods
specified in subsection
(e) (1) except for periods
not to exceed a total of 5 minutes during any
2
consecutive hours.
2)
A flare must be operated with a flame present at
all times,
as determined by the methods specified
in subsection
(f) (2) (c).
3)
A flare must be used only. if the net heating value
of the gas being combusted is 11.2 NJ/scm (300
Btu/scf)
or greater if the flare is steam—assisted
or air-assisted; on if the net heating value of
the gas being combusted is 7.45 NJ/scm (200
Btu/scf) or greaten if the flare is nonassisted.
The net heating value of the gas being combusted
must be determined by the methods specified in
subsection
(e) (2).
4)
Exit Velocity.
A)
A steam—assisted or nonassisted flare must be
designed for an operated with an exit
121—347
199
velocity, as determined by the methods
specified
in
subsection
(e)(3),
less
than
18.3
m/s
(60
ft/s),
except
as
provided
in
subsections
(d) (4)
(B)
and
(C).
B)
A
steam—assisted
or
nonassisted
flare
designed
for
and
operated
with
an
exit
velocity,
as
determined
by
the
methods
specified
in
subsection
(e)(3),
equal
to
or
greater
than
18.3
rn/s
(60
ft/s)
but
less
than
122
m/s
(400
ft/s)
is
allowed
if
the
net
heating
value
of
the
gas
being
combusted
is
greater
than
37
•
3
NJ/scm
(1000
Btu/scf).
C)
A
steam-assisted
or
nonassisted
flare
designed for and operated with an exit
velocity,
as
determined
by
the
methods
specified
in
subsection
(e) (3),
less
than
the
velocity,
V
as
determined
by
the
method
specified
in
subsection
(e)
(4)
and
less
than
122 m/s
(400 ft/s)
is allowed.
5)
An
air-assisted
flare
must
be
designed
and
operated
with
an
exit
velocity
less
than
the
velocity,
V
as
determined
by
the
method
specified
in
subsection
(e)
(5).
6)
A flare used to comply with this Section must be
steam—assisted, air—assisted or nonassisted.
e)
1)
Reference Method
22
in
40
CFR
60,
incorporated
by
reference in 35 Ill.
Adm. Code 720.111, must be
used to determine the compliance of a flare with
the
visible
emission
provisions
of
this
Subpart.
The observation period is
2 hours and must be used
according to Method 22.
2)
The net heating value of the gas being combusted
in a flare must be calculated using the following
equation:
H
=
K
*
SUM(C1
*
Hi)
Where:
H is the net heating value of the sample in
NJ/scm; where the net enthalpy per mole of
offgas is based on combustion- at 25 C and 760
mm Hg, but the standard temperature for
determining the volume cornensponding to 1
mole is 20
C.
12 1—348
200
K
=
1.74 E —7 (1/ppm) (g mol/scm) (MJ/kcal)
where
standard
temperature
for
(g
mol/scm)
20
C.
SUM(Xi)
means
the
sum
of
the
values
of
X
for
each
component
i,
from i=1 to n.
Ci
is
the
concentration
of
sample
component
i
in
ppm
on
a
wet
basis,
as
measured
for
organics
by
Reference
Method
18
in
40
CFR
60,
and for carbon monoxide, by
ASTM
D1946,
incorporated
by
reference
in
35
Ill.
Adm.
Code
720.111.
Hi
is
the
net
heat
of
combustion
of
sample
component i, kcal/gmol at 25 C and 760 mm
Hg.
The heats of combustion must be determined
using ASTM D2382,
incorporated by reference
in 35 Ill. Adm. Code 720.111,
if published
values are not available or cannot be
calculated.
3)
The actual exit velocity of a flare must be
determined by dividing the volumetric flow rate
(in units of standard temperature and pressure),
as determined by Reference Methods
2,
2A,
2C, or
2D in 40 CFR 60, incorporated by reference in 35
Ill. Adm. Code 720.111, as appropriate, by the
unobstructed
(free)
cross—sectional area of the
flare tip.
4)
The maximum allowed velocity in m/s, V for a flare
complying with subsection
(d) (4) (C) must be
determined by the following equation:
LOG(V)
=
(H
+ 28.8)
/
31.7
Where:
LOG
means logarithm to the base 10
H is the net heating value as determined in
subsection
(e) (2).
5)
The maximum allowed velocity in m/s, V for an air—
assisted flare must be determined by the following
equation:
V
=
8.706
+
0.7084H
Where:
121—349
201
H is the net heating value as determined in
subsection
(e) (2)
f)
The owner or operator shall monitor and inspect each
control
device
required
to
comply
with
this
Section
to
ensure
proper
operation
and
maintenance
of
the
control
device
by
implementing
the
following
requirements:
1)
Install,
calibrate,
maintain
and
operate
according
to the manufacturer’s specifications a flow
indicator
that
provides
a
record
of
vent
stream
flow
from
each
affected
process
vent
to
the
control
device
at
least
once
every
hour.
The
flow
indicator
sensor
must
be
installed
in
the
vent
stream
at
the
nearest
feasible
point
to
the
control device inlet but before being combined
with
other
vent
streams.
2)
Install,
calibrate,
maintain
and
operate
according
to
the
manufacturer’s
specifications a device to
continuously monitor control device operation as
specified below:
A)
For
a
thermal
vapor
incinerator,
a
temperature monitoring device equipped with a
continuous recorder.
The device
must
have
accuracy of ±1 percent of the temperature
being monitored in C or±C, whichever is
greater.
the temperature sensor must be
installed at a location in the combustion
chamber
downstream
of
the
combustion
zone.
B)
For a catalytic vapor incinerator,
a
temperature
monitoring
device
equipped
with
a
continuous
recorder.
The
device
must
be
capable
of
monitoring
temperature
at
two
locations
and
have
an
accuracy
of
±1 percent
of
the
temperature
being
monitored
in
C
or ±
0.5
C,
whichever
is
greater.
One
temperature
sensor
must
be
installed
in
the
vent
stream
at
the
nearest
feasible
point
to
the
catalyst
bed
inlet
and
a
second
temperature
sensor
must
be
installed
in
the
vent
stream
at
the
nearest feasible point to the catalyst bed
outlet.
C)
For a flare,
a heat sensing monitoring device
equipped with a continuous rebonden that
indicates the continuous ignition of the
pilot flame.
D)
For a boiler or process heater having a
12 1—350
202
design heat input capacity less than 44 MW,
a
temperature monitoring device equipped with a
continuous recorder.
The device must have an
accuracy of±1 percent of the temperature
being monitored in C or±0.5 C, whichever is
greater.
The temperature sensor must be
installed at a location in the furnace
downstream of the combustion zone.
E)
For a boiler or process heater having a
design heat input capacity greaten than or
equal
to
44
MW,
a monitoring device equipped
with a continuous recorder to measure a
parameter(s) that indicates good combustion
operating practices are being used.
F)
For a condenser,
either:
i)
A monitoring device equipped with a
continuous recorder to measure the
concentration level of the organic
compounds in the exhaust vent stream
from
the
condenser;
on
ii)
A temperature monitoring device equipped
with
a
continuous
recorder.
The
device
must
be
capable
of
monitoring
temperature at two locations and have an
accuracy of ±1 percent of the
temperature being monitored in C on±
0.5 C, whichever is greaten.
One
temperature
sensor
must
be
installed
at
a
location
in
the exhaust vent stream
from the condenser,
and a second
temperature sensor must be installed at
a location in the coolant fluid exiting
the condenser.
G)
For a carbon adsorption system such as a
fixed—bed carbon adsonber that regenerates
the carbon bed directly in the control
device,
either:
i)
A monitoring device equipped with a
continuous recorder to measure the
concentration level of the organic
compounds in the exhaust vent stream
from the carbon bed; or
ii)
A monitoring device equipped with a
continuous recorder to measure a
parameter that indicates the carbon bed
121—351
203
is regenerated on a regular,
predetermined time cycle.
3)
Inspect the readings from each monitoring device
required by subsection
(f) (1) and
(2) at least
once each operating day to check control device
operation and, if necessary,
immediately implement
the corrective measures necessary to ensure the
control device operates in compliance with the
requirements of this Section.
g)
An owner or operator using a carbon adsorption system
such as a fixed—bed carbon adsorber that regenerates
the carbon bed directly onsite in the control device
shall replace the existing carbon in the control device
with fresh carbon at a regular, predetermined time
interval that is no longer than the carbon service life
established as a requirement of Section
725.935(b) (4) (C) (vi).
h)
An owner on operator using a carbon adsorption system
such as a carbon canister that does not regenerate the
carbon bed directly onsite in the control device shall
replace the existing carbon in the control device with
fresh carbon on a regular basis by using one of the
following procedures:
1)
Monitor the concentration level of the organic
compounds in the exhaust vent stream from the
carbon adsorption system on a regular schedule,
and replace the existing carbon with fresh carbon
immediately when carbon breakthrough is indicated.
The monitoring frequency must be daily or at an
interval no greaten than 20 percent of the time
required to consume the total carbon working
capacity established as a requirement of Section
725.935(b) (4) (C) (vii), whichever is longer.
2)
Replace the existing carbon with fresh carbon at a
regular, predetermined time interval that is less
than the design carbon replacement interval
established as a requirement of Section
725.935(b) (4) (C) (vii)
i)
An owner or operator of an affected facility seeking to
comply with the provisions of this Part by using a
control device other than
a thermal vapor incinerator,
catalytic vapor incinerator,
flare, boiler, process
heater, condenser or carbon adsorption system is
required to develop documentation including sufficient
information to describe the control device operation
and identify the process parameter or parameters that
121—352
204
indicate proper operation and maintenance
of
the
control device.
j)
Closed vent systems.
1)
Closed-vent systems must be designed for and
operated with no detectable emissions,
as
indicated by an instrument reading of less than
500 ppm above background and by visual
inspections,
as determined by the methods
specified
at
Section
725.934(b).
2)
Closed—vent systems must be monitored to determine
compliance with this Section during the initial
leak detection monitoring, which must be conducted
by the date that the facility becomes subject to
the provisions of this Section annually, and at
other times as specified by the Agency pursuant to
Section 725.930(c).
3)
Detectable emissions,
as indicated by an
instrument reading greaten than 500
ppm
and
visual
inspections,
must be controlled as soon as
practicable, but not later than 15 calendar days
after the emission is detected.
4)
A first attempt at repair must be made no later
than
5 calendar days after the emission is
detected..
k)
Closed—vent systems and control devices used to comply
with provisions of this Subpart must be operated at all
times
when
emissions
may
be
vented
to
them.
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.934
Test Methods and Procedures
a)
Each owner or operator subject to the provisions of
this Subpart shall comply with the test methods and
procedures requirements provided in this Section
b)
When a closed—vent system is tested for compliance with
no
detectable
emissions,
as
required
in
Section
725.933(j), the test must comply with the following
requirements:
1)
Monitoring
must
comply
with
Reference
Method
21
in
40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111.
12 1—353
205
2)
The detection instrument must meet the performance
criteria of Reference Method 21.
3)
The instrument must be calibrated before use on
each day of its use by the procedures specified in
Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10 ppm of hydrocarbon in
air).
B)
A mixture of methane or n—hexane and air at a
concentration of approximately, but less
than,
10,000 ppm methane or n—hexane.
5)
The background level must be determined as set
forth in Reference Method 21.
6)
The instrument probe must be traversed around all
potential leak interfaces as close to the
interface as possible as described in Reference
Method
21.
7)
The arithmetic difference between the maximum
concentration indicated by the instrument and the
background level
is compared with 500 ppm for
determining compliance.
c)
Performance tests to determine compliance with Section
725.932(a) and with the total organic compound
concentration limit of Section 725.933(c) must comply
with the following:
1)
Performance tests to determine total organic
compound concentrations and mass flow rates
entering and exiting control devices must be
conducted and data reduced in accordance with the
following reference methods and calculation
procedures:
A)
Method
2
in
40
CFR
60
for
velocity
and
volumetric flow rate.
B)
Method
18
in
40
CFR
60
for organic content.
C)
Each
performance
test
must
consist
of
three
separate
runs,
each
run conducted for at
least
1 hour under the conditions that exist
when the hazardous waste management unit is
operating at the highest load on capacity
level reasonably expected to occur.
For the
121—354
206
purpose of determining total organic compound
concentrations
and
mass
flow
rates,
the
average of results of all runs applies.
The
average must be computed on
a time—weighed
basis.
D)
Total organic mass flow rates must be
determined by the following equation:
F
=
K
*
Q
*
StJN(Ci
*
MWi)
Where:
F is the total organic mass flow rate,
kg/h.
K
=
4.16 E —8, conversion factor for
molar
volume,
kg-mol/cubic
m,
at
293
K
and 760 mm Hg.
Q
=
volumetric flow nate of gases
entering or exiting control device,
dscm/h,
as determined by Method
2 in 40
CFR 60, incorporated by reference in 35
Ill. Adm. Code 720.111.
SUN(Xi)
means the sum of the values of X
for each component i, from i=1 to n.
n
=
number of organic compounds in the
vent gas.
Ci is the organic concentration in ppm,
dry basis, of compound
i in the vent
gas,
as determined by Method
18 in 40
CFR 60.
MWi
is the molecular weight of organic
compound
i in the vent gas, kg/kg-mol.
E)
The annual total organic emission rate must
be determined by the following equation:
A= F
*
HOURS
Where:
A is total organic emission rate, kg/y.
F
is the total organic mass flow rate,
kg/h,
as calculated in subsection
(c) (1) (D).
121—355
207
HOURS
IE
the
total
annual
hours
of
operation
for
the
affected
unit.
F)
Total organic emissions from all affected
process
vents
at
the
facility
must
be
determined by
summing
the hourly total
organic mass emissions rates
(F as determined
in subsection
(c) (1) (D)) and by summing the
annual total organic mass emission rates
(A
as determined in subsection
(c) (1) (E))
for
all affected process vents at the facility.
2)
The owner or operator shall record such process
information
as
is
necessary
to
determine
the
conditions of the performance tests.
Operations
during periods of startup, shutdown and
malfunction do not constitute representative
conditions for the purpose of a performance test.
3)
The owner or operator of an affected facility
shall provide, on cause to be provided,
performance testing facilities as follows:
A)
Sampling ports adequate for the test methods
specified in subsection
(C)
(1).
B)
Safe sampling platform(s).
C)
Safe
access
to
sampling
platform(s).
D)
Utilities
for
sampling
and testing equipment.
4)
For the purpose of making compliance
determinations, the time-weighted average of the
results of the three runs must apply.
In the
event that a sample is accidentally lost on
conditions occur in which one of the three runs
must be discontinued because of forced shutdown,
failure of an irreplaceable portion of the sample
train, extreme meteorological conditions or other
circumstances beyond the owner or operator’s
control, compliance may, upon the Agency’s
approval, be determined using the average of the
results of the two other nuns.
d)
To show that a process vent associated with a hazardous
waste distillation, fractionation, thin-film
evaporation, solvent extraction, or air or steam
stripping operation is not subject to the requirements
of this Subpart, the owner or operator shall make an
initial determination that the time-weighted, annual
121—356
208
average total organic concentration of the waste
managed
by
the
waste management unit is less than 10
ppmw
using
one
of
the
following
two
methods:
1)
Direct
measurement
of
the
organic
concentration
of
the waste using the following procedures:
A)
The
owner
or
operator
shall
take
a minimum of
four
grab
samples
of
waste
for
each
wastestream managed
in
the
affected
unit
under process conditions expected to cause
the maximum waste organic concentration.
B)
For waste generated onsite, the grab samples
must be collected at a point before the waste
is exposed to the atmosphere such as in an
enclosed pipe on other closed system that is
used to transfer the waste after generation
to the first affected distillation,
fractionation, thin—film evaporation, solvent
extraction, or air or steam stripping
operation.
For waste generated offsite, the
grab
samples
must
be
collected
at
the
inlet
to
the first waste management unit that
receives the waste provided the waste has
been transferred to the facility in a closed
system such as a tank truck and the waste is
not diluted or mixed with other waste.
C)
Each sample must be analyzed and the total
organic concentration of the sample must be
computed using Method 9060 or 8240 of SW—846
(incorporated by reference under 35 Ill.
Adm.
Code 720.111.
D)
The arithmetic mean of the results of the
analyses of the four samples apply for each
wastestream managed in the unit in
determining the time—weighted, annual average
total organic concentration of the waste.
The time-weighted average is to be calculated
using the annual quantity of each waste
stream processed and the mean organic
concentration of each wastestream managed in
the unit.
2)
Using knowledge of the waste to determine that its
total organic concentration is less that 10 ppmw.
Documentation of the waste determination is
required.
Examples of documentation that must be
used to support a determination under this
subsection include:
121—357
209
A)
Production
process
information
documenting
that
no
organic
compounds
are
used.
B)
Information
that
the
waste
is
generated
by
a
process
that
is
identical
to
a
process
at
the
same
or
another
facility
that
has
previously
been
demonstrated
by
direct
measurement
to
generate
a
wastestream
having
a
total
organic
content
less
than
10
ppmw,
or
C)
Prior
speciation
analysis
results
on
the
same
wastestream
where
it
is
documented
that
no
process
changes
have
occurred
since
that
analysis
that
could
affect
the
waste
total
organic concentration.
e)
‘The
determination
that
distillation,
fractionation,
thin—film
evaporation,
solvent
extraction,
or
air
on
steam
stripping
operations
which
manage
hazardous
wastes with time-weighted, annual average total organic
concentrations
less
than
10
ppinw
must
be
made
as
follows:
1)
By
the
effective
date
that
the
facility
becomes
subject
to
the
provisions
of
this
Subpart
on
by
the
date
when
the
waste
is
first
managed
in
a
waste management unit, whichever is later; and
2)
For
continuously
generated
waste,
annually;
or
3)
Whenever
there
is
a
change
in
the
waste
being
managed
or
a
change
in
the
process
that
generates
on treats the waste.
f)
When
an
owner
or
operator
and
the
Agency
do
not
agree
on
whether
a
distillation,
fractionation, thin-film
evaporation, solvent extraction,
or air or steam
stripping
operation
manages
a
hazardous
waste
with
organic
concentrations
of
at
least
10
ppmw
based
on
knowledge
of
the
waste,
the
procedures
in
Method
8240
in
SW-846,
incorporated
by
reference
in
35
Ill.
Adm.
Code
720.111,
must
be
used
to
resolve
the
dispute.
Source:
Added
at
15
Ill.
Reg.
,
effective
Section 725.935
Recordkeeping Requirements
a)
Compliance
Required.
1)
Each owner or operator subject to the provisions
121—358
210
of
this Subpart shall comply with the
necordkeeping
requirements
of
this
Section.
2)
An
owner
or
operator
of
more
than
one
hazardous
waste
management
unit
subject
to
the
provisions
of
this Subpart may comply with the recordkeeping
requirements for these hazardous waste management
units
in
one
recondkeeping
system
if
the
system
identifies each record by each hazardous waste
management
unit.
b)
Owners and operators shall record the following
information
in
the
facility
operating
record:
1)
For facilities that comply with the provisions of
Section 725.933(a) (2), an implementation schedule
that includes dates by which the closed-vent
system and control device will be installed and ih
operation.
The
schedule
must
also
include
a
rationale
of
why
the
installation
cannot
be
completed
at
an
earlier
date.
The
implementation
schedule must be in the facility operating record
by the effective date that the facility becomes
subject
to
the
provisions
of
this
Subpart.
2)
Up-to-date
documentation
of
compliance
with
the
process vent standards in Section 725.932,
including:
A)
Information and data identifying all affected
process vents,
annual throughput and
operating hours of each affected unit,
estimated emission rates for each affected
vent and for the overall facility
(i.e.,
the
total emissions for all affected vents at the
facility),
and the approximate location
within the facility of each affected unit
(e.g.,
identify the hazardous waste
management
units
on
a
facility
plot
plan).
B)
Information and data supporting determination
of
vent
emissions
and
emission
reductions
achieved by add—on control devices based on
engineering calculations or source tests.
For the purpose of determining compliance,
determinations of vent emissions and emission
reductions must be made using operating
parameter values
(e.g.,
tempeIatunes,
flow
rates,
or vent stream organic compounds and
concentrations) that represent the conditions
that result in maximum organic emissions,
such as when the waste management unit is
121—359
211
operating
at
the
highest
load
or
capacity
level
reasonably
expected
to
occur.
If
the
owner
or
operator
takes
any
action
(e.g.,
managing
a
waste
of
different
composition
or
increasing
operating
hours
of
affected
waste
management
units)
that
would
result
in
an
increase
in
total
organic
emissions
from
affected
process
vents
at
the
facility,
then
a
new
determination
is
required.
3)
Where
an
owner
or
operator
chooses
to
use
test
date
to
determine
the
organic
removal
efficiency
on
total
organic
compound
concentration
achieved
by
the
control
device,
a
performance
test
plan.
The
test
plan
must
include:
A)
A
description
of
how
it
is
determined
that
the
planned
test
is
going
to
be
conducted
when
the
hazardous
waste
management
unit
is
operating
at
the
highest
load
or
capacity
level reasonably expected to occur.
This
must include the estimated
or
design
flow
rate
and
organic
content
of
each
vent
stream
and define the acceptable operating ranges of
key process and control device parameters
during the test program.
B)
A detailed engineering description of the
closed—vent system and control device
including:
i)
Manufacturer’s
name
and
model
number
of
control device.
ii)
Type
of
control
device.
iii) Dimensions of the control device.
iv)
Capacity.
v)
Construction
materials.
C)
A detailed
description
of
sampling
and
monitoring procedures,
including sampling and
monitoring locations in the system, the
equipment
to
be
used,
sampling
and
monitoring
frequency,
and planned analytical procedures
for sample analysis.
4)
Documentation of compliance with Section 725.933•
must include the following information:
121—360
212
A)
A list of all information references and
sources
used
in
preparing
the
documentation.
B)
Records
including
the
dates
of
each
compliance
test
required
by
Section
725.933(j).
C)
If
engineering
calculations
are
used,
a
design analysis, specifications,
drawings,
schematics,
and
piping
and
instrumentation
diagrams based on the appropriate sections of
APTI
Course
415
(incorporated by reference in
35
Ill.
Adm.
Code
720.111)
or
other
engineering texts, approved by the Agency,
that present basic control device design
information.
Documentation provided by the
control device manufacturer
or
vendor
that
describes the control device design in
accordance with subsections
(b) (4) (C) (i)
through
(vii)
may
be
used
to
comply
with
this
requirement.
The design analysis must
address the vent stream characteristics and
control device operation parameters as
specified below.
i)
For
a thermal vapor incinerator, the
design analysis must consider the vent
stream composition, constituent
concentrations and flow rate.
The
design analysis must also establish the
design minimum and average temperature
in the combustion zone and the
combustion zone residence time.
ii)
For a catalytic vapor incinerator, the
design analysis must consider the vent
stream composition, constituent
concentrations,
and flow rate.
The
design analysis must also establish the
design minimum and average temperatures
across the catalyst bed inlet and
outlet.
iii) For a boiler on process heater, the
design analysis must consider the vent
stream composition, constituent
concentrations and flow rate.
The
design analysis must also establish the
design
minimum
and
average
flame
zone
temperatures, combustion zone residence
time and description of method and
location where the vent stream is
12 1—361
213
introduced
into
the
combustion
zone.
iv)
For
a
flare,
the
design
analysis
must
consider
the
vent
stream
composition,
constituent
concentrations,
and
flow
rate.
The
design
analysis
must
also
consider
the
requirements
specified
in
Section
725.933(d).
v)
For
a
condenser,
the
design
analysis
must
consider
the
vent
stream
composition,
constituent
concentrations,
flow
rate,
relative
humidity
and
temperature.
The
design
analysis
must
also establish the design outlet organic
compound
concentration
level,
design
average
temperature
of
the
condenser
exhaust
vent
stream
and
design
average
temperatures
of
the
coolant
fluid
at
the
condenser
inlet
and
outlet.
vi)
For
a
carbon
adsorption
system
such
as
a
fixed—bed adsorben that regenerates the
carbon bed directly onsite in the
control device, the design analysis must
consider
the
vent
stream
composition,
constituent
concentrations,
flow
rate,
relative
humidity
and
temperature.
The
design analysis must also establish the
design
exhaust
vent
stream
organic
compound concentration level, number and
capacity
of
carbon
beds,
type
and
working
capacity
of
activated
carbon
used
for
carbon
beds,
design
total
steam
flow
over
the
period
of
each
complete
carbon bed regeneration cycle, duration
of
the
carbon
bed
steaming
and
cooling/drying cycles, design carbon bed
temperature after regeneration, design
carbon
bed
regeneration
time
and
design
service
life
of
carbon.
vii)
For
a
carbon
adsorption
system
such
as
a
carbon
canister
that
does
not
regenerate
the carbon bed directly onsite in the
control device, the design analysis must
consider the vent stream composition,
constituent concentrations,
flow nate,
relative humidity and temperature.
The
design analysis must also establish the
design outlet organic concentration
level, capacity of carbon bed, type and
121—362
214
working capacity of activated carbon
used
for
carbon
bed
and
design
carbon
replacement
interval
based
on
the
total
carbon
working
capacity
of
the
control
device
and
source
operating
schedule.
D)
A
statement
signed
and
dated
by
the
owner
or
operator
certifying
that
the
operating
parameters used in the design analysis
reasonably
represent
the
conditions
that
exist when the hazardous waste management
unit
is
on
would
be
operating
at
the
highest
load
on
capacity
level
reasonably
expected
to
occur.
E)
A
statement
signed
and
dated
by
the
owner
or
operator certifying that the control device
is designed to operate at an efficiency of 95
percent or greaten unless the total organic
concentration limit of Section 725.932(a)
is
achieved at an efficiency less than 95 weight
percent on the total organic emission limits
of Section 725.932(a)
for affected process
vents at the facility are attained by a
control
device
involving
vapor recovery at an
efficiency less than 95 weight percent.
A
statement provided by the control device
manufacturer
on
vendor
certifying
that
the
control equipment meets the design
specifications may be used to comply with
this requirement.
F)
If
performance
tests
are
used
to
demonstrate
compliance, all test results.
c)
Design documentation and monitoring operating and’
inspection
information
for
each
closed—vent
system
and
control
device
required
to
comply
with
the
provisions
of
this
Part
must
be
recorded
and
kept
up—to-date
in
the facility operating record.
The information must
include:
1)
Description and date of each modification that is
made
to
the
closed—vent
system
or
control
device
design.
2)
Identification
of
operating
parameter,
description
of monitoring device, and diagram of monitoring
sensor location or locations used to comply with
Section 725.933(f) (1) and
(2).
3)
Monitoring, operating and inspection information
12 1—363
215
required
by
Section
725.933(f)
through
(k).
4)
Date,
time
and
duration
of
each
period
that
occurs
while the control device is operating when any
monitored parameter exceeds the value established
in
the
control
device
design
analysis
as
specified
below:
A)
For
a
thermal
vapor
incinerator
designed
to
operate
with
a
minimum
residence
time
of
0.50
second
at
a
minimum
temperature
of
760
C,
any
period
when
the
combustion
temperature
is
below 760 C.
B)
For a thermal vapor incinerator
designed
to
operate with an organic emission reduction
efficiency of 95 percent on greaten, any
period when the combustion zone temperature
is
more
than
28
C
below
the
design
average
combustion zone temperature established as a
requirement
of
subsection
(b) (4)
(C) (i).
C)
For
a
catalytic
vapor
incinerator,
any
period
when:
i)
Temperature
of
the
vent
stream
at
the
catalyst bed inlet is more than 28 C
below the average temperature of the
inlet
vent
stream
established
as
a
requirement
of
subsection
(b) (4)
(C) (ii);
or
ii)
Temperature difference across the
catalyst bed is less than 80 percent of
the design average temperature
difference established as a requirement
of subsection
(b) (4) (C) (ii).
D)
For
a
boiler
on
process
heater,
any
period
when:
i)
Flame
zone
temperature
is
more
than
28
C
below
the
design
average
flame
zone
temperature
established
as
a
requirement
of
subsection
(b) (4)
(C) (iii);
or
ii)
Position changes where the vent stream
is introduced to the combustion zone
from
the
location
established
as
a
requirement of subsection
(b) (4) (C) (iii).
E)
For a flare, period when the pilot flame is
121—364
216
not ignited.
F)
For
a
condenser
that
complies
with
Section
725.933(f)
(2)
(F) (i),
any
period
when
the
organic compound concentration level on
readings
of
organic
compounds
in
the
exhaust
vent
stream
from
the
condenser
are
more
than
20
percent
greater
than
the
design
outlet
organic compound concentration level
established
as
a
requirement
of
subsection
(b) (4)
(C) (v)
G)
For a condenser that complies with Section
725.933(f)
(2) (F) (ii),
any
period
when:
i)
Temperature of the exhaust vent stream
from
the
condenser
is
more
than
6
C
above the design average exhaust vent
stream temperature established as a
requirement of subsection
(b) (4) (C) (v).
ii)
Temperature
of
the
coolant
fluid
exiting
the condenser is more than 6 C above the
design average coolant fluid temperature
at
the
condenser
outlet
established
as
a
requirement of subsection
(b) (4) (C) (v).
H)
For a carbon adsorption system such as a
fixed-bed carbon adsorber that regenerates
the carbon bed directly onsite in the control
device and complies with Section
725.933(f)(2)(G)(i), any period when the
organic compound concentration level or
readings of organic compounds in the exhaust
vent stream from the carbon bed are more than
20 percent greater than the design exhaust
vent
stream
organic compound concentration
level
established
as
a
requirement
of
subsection
(b) (4) (C).(vi).
I)
For a carbon adsorption system such as a
fixed—bed carbon adsorber that regenerates
the carbon bed directly onsite in the control
device and complies with Section
725.933(f) (2) (G) (ii),
any period when the
vent
stream
continues
to
flow through the
control device beyond the predetermined
carbon bed regeneration time established as a
requirement of subsection
(b) (4) (C) (vi).
5)
Explanation for each period recorded under
subsection
(c) (4)
of the cause for control device
12 1—365
217
operating
parameter
exceeding
the
design
value
and
the
measures
implemented
to
correct
the
control
device operation.
6)
For
carbon
adsorption
systems
operated
subject
to
requirements
specified
in
Section
725.933(g)
on
(h) (2),
any
date
when
existing
carbon
in
the
control
device
is
replaced
with
fresh
carbon.
7)
For
carbon
adsorption
systems
operated
subject
to
requirements
specified
in
Section
725.933(h)
(1),
a
log
that
records:
A)
Date
and
time
when
control
device
is
monitored for carbon breakthrough and the
monitoring device reading.
B)
Date when existing carbon in the control
device is replaced with fresh carbon.
8)
Date
of
each
control
device startup and shutdown.
d)
Records of the monitoring, operating and inspection
information
required
by
subsections
(c)
(3)
through
(8)
need be kept only
3 years.
e)
For
a
control
device
other
than
a
thermal
vapor
incinerator,
catalytic
vapor
incinerator,
flare,
boiler,
process
heater,
condenser
or
carbon
adsorption
system, monitoring and inspection information
indicating proper
operation
and
maintenance
of
the
control device must be recorded in the facility
operating record.
f)
Up-to—date information and data
used
to
determine
whether on not a process vent is subject to the
requirements in Section 725.932,
including supporting
documentation as required by Section 725.934(d) (2),
when application of the knowledge of the nature of the
hazardous wastestream or the process by which it was
produced is used, must be recorded in a log that is
kept in the facility operating record.
Source:
Added
at
15
Ill.
Reg.
,
effective
SUBPART BB:
AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 725.950
Applicability
~j
The regulations in this Subpart apply to owners and
121—366
218
operators of facilities that treat,
stone,
on dispose
of
hazardous
wastes
(except
as
provided
in
Section
725.101)
~j
Except
as
provided
in
Section
725.964(1),
this
Subpart
applies to equipment that contains or contacts
hazardous wastes with organic concentrations of at
least
10 percent by weight that are mana~edin:
fl
Units that are subject to the
RCRA
permitting
requirements
of
35
Ill.
Adm.
Code
703,
or
21
Hazardous waste recycling units that are located
on
hazardous
waste
management
facilities
otherwise
subiect to the permitting requirements of 35
Ill.
Adm. Code 703.
gj..
Each
piece
of
equipment
to
which
this
Subpart
applies
must
be
marked
in
such
a
manner
that
it
can
be
distinguished readily from other pieces of equipment.
~j
Equipment that is in vacuum service
is excluded from
the requirements of Sections
725.952
to
725.960.
if
it
is identified as required in Section 725.964(g) (5).
BOARD NOTE:
The requirements of Sections 725.952
through 725.964 apply to equipment associated with
hazardous waste recycling units previously exempt under
35111. Adm. Code 721.106(c)(l).
Other exemøtions
under 35
111.
Adm. Code 721.104, 722.134 and 725.101(e)
are
not
affected
by
these
requirements.
~j
Agency decisions pursuant to this Part must be made in
writing,
are in the nature of permit decisions pursuant
to Section
39 of the Environmental Protection Act and
may be appealed to the Board pursuant to 35
Ill.
Adm.
Code 105.
Source:
Added
at
15 Ill.
Reg.
,
effective
Section 725.951
Definitions
As used in this Subpart, all terms have the meaning given them in
Section 725.931,
the Resource Conservation and Recovery Act and
35 Ill. Adm. Code 720 through 726.
Source:
Added
at
15
Ill.
Reg.
,
effective
121—367
219
c~r.Fton 725.952
Standards:
Pumps
in
Light
Liquid
Service
~j
Monitoring
fl~.
Each
pump
in
light
liquid
service
must
be
monitored
monthly
to
detect
leaks
by
the
methods
specified
in
Section
725.963(b),
except
as
provided
in
subsections
(d),
(e)
and
(f).
21
Each
pump
in
light
liquid
service
must
be
checked
by
visual
inspection
each
calendar
week
for
indications
of
liquids
dripping
from
the
pump
seal.
~j
Leaks
fl
If an
instrument
reading
of
10,000
ppm or greater
is measured,
a leak is detected.
21
If there are indications
of liquids dripping from
the
pump
seal,
a
leak
is
detected.
~j
Repairs
fl
When a
leak is detected,
it
must
be
repaired
as
soon
as
practicable,
but
not
later
than
15
calendar
days
after
it
is
detected,
except
as
provided in Section 725.959.
21
A first
attempt
at
repair
(e.g.,
tightening
the
packing gland) must be made no later than 5
calendar days after each leak is detected.
~j
Each
pump
equipped
with
a
dual
mechanical
seal
system
that
includes
a
barrier
fluid
system
is
exempt
from
the
requirements of subsection
(a), provided the following’
requirements are met:
fl
Eaci dual mechanical seal system must be:
~j.
Operated with the barrier fluid at a pressure
that
is
at
all
times
greater
than
the
pump
stuffing box pressures;
on
~j
Equipped with a barrier fluid degassing
reservoir that is connected by a closed—vent
system to a control device that complies with
the
requirements
of
Section
725.960;
or
~j
Equipped with a system that purges the
barrier fluid into a hazardous wastestream
with no detectable emissions to the
12 1—368
220
atmosphere.
21
The barrier fluid system must not be a hazardous
waste with organic concentrations 10 percent or
greaten
by
weight.
fl
Each barrier fluid system must be equipped with a
sensor_that will detect failure of the seal
system,
the barrier fluid system, or
both.
iL
Each
pump
must
be
checked
by
visual
inspection.
each calendar week,
for indications of liquids
dripping from the pump seals.
~
Alarms
~j
Each
sensor
as
described
in
subsection
(dl
(3)
must be checked daily or be equipped with an
audible alarm that must be checked monthly to
ensure
that
it
is
functioning
properly.
~j
The owner or operator shall determine, based
on design considerations and operating
experience,
a criterion that indicates
failure of the seal system, the barrier fluid
system.
or both.
.~j
Leaks
~j
If
there
are
indications
of
liquids
dripping
from the pump seal or the sensor indicates
failure of the seal system, the barrier fluid
system,
or
both
based
on
the
criterion
determined in subsection
(d) (5) (B),
a leak is
detected.
~j
When a leak
is detected,
it must be repaired
as
soon
as
practicable,
but
not
later
than
15
calendar
days
after
it
is
detected,
except
as
provided in Section 725.959.
Q1
A
first
attempt
at
repair
(e.g.,
relapping
the
seal)
must
be
made
no
later
than
5
calendar days after each leak is detected.
~j
Any pump that is designated,
as described in Section
725.964(g) (2), for no detectable emissions,
as
indicated by an instrument reading of less than 500 ppm
above
background,
is
exempt
from
the
requirements
of
subsections
(a),
(C)
and
(d),
if the pump meets the
following requirements:
12 1—369
221
fl
Must have no externally actuated shaft penetrating
the pump housing.
21
Must
operate
with
no
detectable emissions as
indicated
by
an
instrument
reading
of
less than
500 ppm above background as measured by the
methods specified in Section 725.963(c).
fl
Must be tested for compliance with subsection
(a)
(2)
initially
upon
designation,
annually
and
at
other
times
as
specified
by
the
Agency
pursuant
to
Section
725.950(e).
fl
If any pump is equipped with
a
closed-vent
system
capable
of
capturing
and
transporting
any
leakage
from
the
seal
or
seals
to
a control device that complj.~
with
the
requirements
of
Section
725.960.
it
is
exempt
from
the
requirements
of
subsections
(a)
through
(e).
‘Source:
Added at 15 Ill. Reg.
,
effective
Section 725.953
Standards:
Compressors
~j
Each
compressor
must
be
equipped
with
a
seal
system
that
includes
a
barrier
fluid
system
and
that
prevents
leakage of total organic emissions to the atmosphere,
except
as
provided
in
subsections
(h)
and
(1).
~j
Each compressor seal system as required in subsection
(a) must be:
fl
Operated with the barrier fluid at a pressure that
is at all times greaten than the compressor
stuffing
box
pressure;
or
21
Equipped with a barrier fluid system that is
connected by a closed—vent system to a control
device that complies with the requirements of
Section
725.960;
on
~j
Equipped with a system that purges the barrier
fluid into a hazardous wastestream with no
detectable emissions to atmosphere.
~j
The barrier fluid must not be a hazardous waste with
organic concentrations 10 percent or greaten by weight.
~j
Each
barrier
fluid
system
as
described
in
subsections
(a)
through
(c)
must
be
equipped
with
a
sensor
that
will detect failure of the seal system, barrier fluid
system,
or both.
12 1—370
222
~j
~
Each sensor as required in subsection
(dl must be
checked daily or must be equipped with an audible
alarm that must be checked monthly to ensure that
it is functioning properly unless the compressor
is located within the boundary of an unmanned
plant site,
in which case the sensor must be
checked daily.
21
The owner or operator shall determine, based on
design considerations and operating experience,
a
criterion that indicates failure of the seal
~
the barrier fluid system,
or both.
~fj
If the sensor indicates failure of the seal system, the
barrier fluid system,
or both based on the criterion
determined under subsection
(e) (2), a leak is detected.
gj
Repairs
fl
When a leak is detected,
it must be repaired as
soon as practicable, but not later than 15
calendar days after it is detected, except as
provided in Section 725.959.
21
A first attempt at repair
(e.g.,
tightening the
packing gland) must be made no later than
5
calendar days after each leak is detected.
~
A compressor is exempt from the requirements of
subsections
(a)
and
(b)
if it is equipped with a
closed-vent system capable of capturing and
transporting any leakage from the seal to
a control
device that complies with the requirements of Section
725.960,
except as provided in subsection
(i).
j).
Any compressor that is designated,
as described in
Section 725.964(g) (2).
for no detectable emission as
indicated by an instrument reading of less than 500 ppm
above background,
is exempt from the requirements of
subsections
(a) through
(h)
if the compressor:
fl
Is determined to be opera
g.
with
no detectable
~issions,
as indicated by an instrument reading
of less than 500 ppm above background,
as measured
by the method specified in Section 725.963(c).
~
Is tested for compliance with subsection
(i) (1)
j~tia1~yupon designation,
annually and other
times as specified by the Agency pursuant to
Section 725.950(~j~
121—37 1
223
Source:
Added at 15
Ill. Reg.
,
effective
Section 725.954
Standards:
Pressure Relief Devices in
Gas/Vapor Service
~j
Except during pressure releases, each pressure relief
device
in
gas/vapor
service
must
be
operated
with
no
detectable emissions,
as indicated by an instrument
reading of less than 500 ppm above background as
measured by the method specified in Section 725.963(c).
~j
Actions following pressure release.
fl
After each pressure release,
the pressure relief
device must be returned to a condition of no
detectable emissions,
as indicated by an
instrument reading of less than 500 ppm above
background,
as soon as practicable. but no later
than S calendar days after each pressure release,
except as provided in Section 725.959.
21
No later than 5 calendar days after the pressure
release, the pressure relief device must be
monitored to confirm the condition of no
detectable
emissions,
as
indicated by an
instrument reading of less than 500 ppm above
background,
as measured by the method specified in
Section 725.963(c)
gj
Any pressure relief device that is equipped with a
closed-vent system capable of capturing and
transporting leakage from the pressure relief device to
a control device as described in Section 725.960
is
exempt from the requirements of subsections
(a) and
(b).
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.955
Standards:
Sampling Connecting Systems
~j
Each sampling connection system must be equipped with a
closed purge system or closed—vent system.
~j
Each closed—purge system or closed—vent system as
required in subsection
(a) must:
fl
Return the pur~edhazardous waste stream directly
to the hazardous waste management process line
with no detectable emissions to atmosphere; or
121—372
224
21
Collect and recycle the purged hazardous waste
stream with no detectable emissions to atmosphere
on
~j
Be designed and operated to capture and transport
all_the purged hazardous wastestream to a control
device that complies with the requirements of
Section 725.960.
~J..
In situ sampling systems are exempt from the
requirements of subsections
(a)
and
(b).
Source:
Added at 15 Ill.
Reg.
,
effective
Section 725.956
Standards:
Open-ended Valves or Lines
~
Equipment.
jj.
Each op~n-endedvalve or line must be equipped
with a cap, blind flange, plug or a second valve.
21
The cap, blind flange, plug or second valve must
seal the open end at all times except during
operations requiring hazardous wastestreani flow
through the open—ended valve on line.
~j
Each open—ended valve or line equipped with
a second
yalve must be operated in a manner such that the valve
on the hazardous wastestream end
is closed before the
second valve is closed.
çj
When a double block and bleed system is being used,
the
bleed valve or line may~emainopen during operations
that require venting the line between the block valves
but must comply with subsection
(a) at all other times.
Source:
Added at
15 Ill.
Reg.
,
effective
Section 725.957
Standards:
Valves in Gas/Vapor or Light
Liquid Service
~j
Each valve iflgas/vapor on light liquid service must be
monitored mc
dtleaks
b~ythe methods
~p~cifled in Section 725.963(b) and must comply with
subsections
(hI through
(e), except as provided in
subsections
(f),
(ci) and
(h), and in Section 725.961
and 725.962.
~j
If an instrument reading
flo,000ppm
or greater is
measure~a leak is detected.
12 1—373
225
.çj
Monitoring Frequency
j
Any valve for which a leak is not detected for two
successive months must be monitored the first
month of every succeeding quarter, beginning with
the next quarter. until
a leak
is detected.
21
If a leak
is detected, the valve must be monitored
monthly until
a leak is not detected for two
successive months,
j~
When a leak is detected,
it must be repaired as
soon
as
practicable,
but no later than 15 calendar
days after the leak is detected,
except as
provided in Section 725.959.
21
A first attempt at repair must be made no later
than
5 calendar days after each leak is detected.
~j
First attempts at repair include, but are not limited
to the following best practices where practicable:
fl
Tightening of bonnet bolts.
21
Replacement
of
bonnet
bolts.
~j
Tightening of packing gland nuts.
41
Injection of lubricant into lubricated packing.
fl
Any valve that
is designated,
as described in Section
725.964(g) (2),
for no detectable emissions, as
indicated by an instrument reading of less than 500 ppm
above background,
is exempt from the reciuirements of
subsection
(a)
if the valve:
,3j~.
Has no external actuating mechanism in contact
with the hazardous wastestream.
21
Is
operated
with emissions less than 500 ppm above
background
as
determined by the method specified
in Section 725.963(c).
fl
Is tested for compliance with subsection
(f) (2)
initially upon designation, annually, and at other
times as specified by the Agency pursuant to
Section 725.950(e).
gj
~knyvalve that is designated,
as described in Section
725.964(h) (1), as an unsafe—to—monitor valve
is exempt
from the requirements of subsection
(a).
if:
121—374
226
fl
The owner or operator of the valve determines that
the valve is unsafe to monitor because monitoring
personnel would be exposed to an immediate danger
as a consequence of complying with subsection
(a).
21
The owner or operator of the valve adheres to a
written plan that requires monitoring of the valve
as frequently as practicable during safe—to-
monitor times.
~j
Any valve that is designated,
as described in Section
725.964(h) (2), as a difficult-to-monitor valve is
exempt from the requirements of subsection
(a), if:
~j
The owner or operator of the valve determines that
the valve cannot be monitored without elevating
the monitoring personnel more than
2 meters above
a support surface
21
The hazardous waste management unit within which
the valve is located was
in operation before June
21,
1990; and
~j
The owner or operator of the valve follows a
written plan that requires monitoring of the valve
at least once per calendar year.
Source:
Added at
15 Ill.
Reg.
,
effective
Section 725.958
Standards:
Pumps. Valves, Pressure Relief
Devices,
Flanges and other Connectors
~j
Pumps and valves in heavy liquid service, pressure
relief
devices in light liquid or heavy liquid service
and flanges and other connectors must be monitored
within
5 days by the method specified in Section
725.963(b),
if evidence of a potential leak is found by
visual,
audible, olfactory,
or any other detection
method.
~j
If an instrument reading of 10,000 ppm or cireater is
measured,
a leak is detected.
~j
Repairs
fl
When a leak
is detected,
it must be repaired ~
soon as practicable, but not later than 15
calendar days after ~
provided in Section 725.959.
12 1—375
227
21
Tue first attempt at repair must
be
made no later
than 5 calendar days after each leak is detected.
~J
First attempts at repair include, but are not limited
to, the best practices described under Section
725.957(e).
Source:
Added
at
15
Ill.
Reg.
,
effective
Section
725.959
Standards:
Delay
of
Repair
~j.
Delay of repair of equipment for which leaks have been
detected
is allowed if the repair is technically
infeasible without a hazardous waste management unit
shutdown.
In such a case,
repair of this equipment
must occur before the end of the next hazardous waste
management unit shutdown.
~j
Delay of repair of equipment for which leaks have been
detected is allowed for equipment that is isolated from
the hazardous waste management unit and that does not
continue to contain on contact hazardous waste with
organic concentrations at least 10 percent by weight.
~j
Delay of repair for valves is allowed if:
fl
The owner or operator determines that emissions of
purged material resulting from immediate repair
are greater than the emissions likely to result
from delay of repair.
21
When repair procedures are effected, the purged
material is collected and destroyed or recovered
in a control device complying with Section
725. 960.
~
Delay of repair for pumps is allowed if:
fl
Repair requires the use of a dual mechanical seal
system that includes a barrier fluid system.
21
Repair is completed as soon as practicable, but
not later than
6 months after the leak was
detected.
~j
Delay of repair beyond
a hazardous waste management
unit shutdown is allowed for a valve if valve assembly
replacement
is necessary during the hazardous waste
management unit shutdown, valve assembly supplies have
been depleted, and valve assembly supplies had been
sufficiently stocked before the supplies were depleted.
12 1—376
228
Delay of repair beyond the next hazardous waste
manaqç~mentunit shutdown
is not allowed unless the next
hazardous waste management unit shutdown occurs sooner
than
6 months after the first hazardous waste
management unit shutdown.
Source:
Added at
15 Ill. Reg.
,
effective
Section 725.960
Standards:
Closed-vent Systems and Control
Devices
Owners on operators of closed—vent systems and control devices
shall comply with the provisions of Section 725.933.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 725.961
Percent Leakage Alternative for Valves
~j
~~owner
or operator subject to the requirements of
Section 725.957 may elect to have all valves within a
hazardous waste management unit comply with an
alternative standard which allows no greater than
2
p~rcentof the valves to leak.
ki
The following requirements must be met if an owner or
operator decides to comply with the alternative
standard of allowing
2 percent of valves to leak:
~
An owner or operator shall notify the Agency that
the owner or operator has elected to comply with
the requirements of this Section.
21
A performance test as specified in subsection
(c)
must be conducted initially upon designation,
annually and other times as specified by the
Agency pursuant to Section 725.950(e).
fl
If a valve leak is detected
it must be repaired in
accordance with Section 725.957(d)
and
(e).
~
Performance tests must be conducted in the following
manner:
fl
All valves subject to the requirements in Section
725.957 within the hazardous waste management unit
must
be monitored within
1 week by the methods
~pecified
in Section 725.963(b).
21
If an instrument reading of 10,000 ppm or greater
is
measured,
a leak is detected.
12
1—377
229
fl
The leak percentage must be determined by dividing
the number of valves subject to the requirements
in Section 725.957 for which leaks are detected by
the total number of valves subject to the
requirements in Section 725.957 within the
hazardous waste management unit.
~j
If an owner or operator decides no longer to comply
with this Section, the owner or operator shall notify
the Agency in writing that the work practice standard
described in Section 725.957(a) through
(e) will be
followed.
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.962
Skip Period Alternative for Valves
~j.
Election
fl
An owner on operator subject to the requirements
of Section 725.957 may elect for all valves within
a hazardous waste management unit to comply with
one of the alternative work practices specified in
subsections
(b) (2)
and
(3).
21
An owner or operator shall notify the Agency
before implementing one of the alternative work
practices.
~j
Reduced Monitoring
fl
An owner or operator shall comply with the
requirements for valves,
as described in Section
725.957, except as described in subsection
(b) (2)
and
(3).
21
After two consecutive quarterly leak detection
periods with the percentage of valves leaking
~qual to on less than
2 percent,
an owner or
operator
may
begin
to
skip
one
of
the
quarterly
leak detection periods for the valves subject to
the requirements
in Section 725.957.
fl
After five consecutive quarterly leak detection
periods with the percentage of valves leaking
equal to on less than
2 percent,
an owner or
operator may begin to skip three of the quarterly
leak det~ectio~periodsfor the valves subject to
the requirements in Section 725.957.
121—3
78
230
41
If the percentage of valves leaking is greater
than
2 percent. the owner on operator shall
monitor monthly in compliance with the
requirements
in Section 725.957. but may again
elect
to use this Section after meeting the
requirements of Section 725.957(c) (1).
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.963
Test Methods and Procedures
~j
Each
owner
or
operator subject to the provisions of
this Subpart shall comply with the test methods and
p~ocedunesrequirements provided
in this Section.
ki
Leak detection monitoring,
as required in Sections
725.952 through 725.962, must comply with the following
requirements:
fl
Mc~nitoringmust comply with Reference Method 21 in
40 CFR 60, incorporated by reference in 35 Ill.
Adm. Code 720.111.
21
The detection instrument must meet the performance
criteria of Reference Method 21.
fl
The instrument must be calibrated before use on
each day of its use by the procedures specified in
Reference Method 21.
41
Calibration gases must be:
~j
Zero air
(less than 10 ppm of hydrocarbon
in
air).
~j
A mixture of methane or n—hexane and air at a
concentration of approximately, but less than
10,000 ppm methane or
n-hexane.
~
The instrument probe must be traversed around all
potential leak interfaces as close to the
interf~ce
as possible as described in Reference
Method 21.
~j
When equipment is tested for compliance with no
detectable emissions,
as required in Sections
725.952(e), 725.953(i),
725.954
and 725.957(f),
the
test must comply with the following requirements:
fl
Phe requirements of subsections (bUll
through
(4)
apply.
12 1—379
231
21
The background level must be determined as set
forth
in
Reference
Method
21.
21
The instrument probe
must
be
traversed
around
all
potential leak interfaces as close to the
interface as possible as described in Reference
Method
21.
41
This arithmetic difference between the maximum
concentration
indicated
by
the
instrument and the
background level is com~anedwith 500 ppm for
determining compliance.
~j
In accordance with the waste analysis plan required by
Section 725.113(b). an owner on operator of a facility
shall determine,
for each piece of equipment,
whether
the equipment contains or contacts a hazardous waste
with organic concentration that equals or exceeds 10
percent by weight using the following:
fl
Methods described in ASTM Methods
D 2267,
E 169,
E
168.
E 260 incorporated by reference in 35 Ill.
Adm. Code 720.111
21
Method 9060 or 8240 of SW-846.
incorporated by
reference in
35 Ill. Adm. Code 720.111; or
IL
Application of the knowledge of the nature of the
hazardous wastestream or the process by which it
was produced.
Documentation of a waste
determination by knowledge is required.
Examples
of documentation that must be used to support a
determination under this provision include
production process information documenting that no
organic compounds are used,
information that the
waste
is generated by a process that is identical
to a process at the same or another facility that
has previously been demonstrated by direct
measurement to have a total organic content less
than 10 percent,
or prior speciation analysis
results on the same wastestream where it
is
also
documented that no process changes have occurred
since that analysis that could affect the waste
total organic concentration.
~j
If an owner or operator determines that a piece of
equipment contains or contacts a hazardous waste with
organic concentrations at least 10 percent by weight,
the determination can be revised only after following
the procedures
in subsection
(d)(l)
or
(2).
121—380
232
fj.
When an owner or operator and the Agency do not agree
on whether a piece of equipment contains or contacts a
hazardous waste with organic concentrations at least 10
percent by weight, the procedures in subsection
(dl (1)
or
(2) must be used to resolve the dispute.
gj
Samples used in determining the percent organic content
must be representative of the highest total organic
content hazardous waste that
is expected to be
contained in or contact the equipment.
hi
To determine if pumps on valves are in light liquid
service,
the vapor pressures of constituents must
either be obtained from standard reference texts or be
determined by ASTM D-2879 incorporated by reference in
35 Ill.
Adni.
Code 720.111.
jj
Performance tests to determine if a control device
achieves
95 weight percent organic emission reduction
must comply with the procedures of Section
725.934(c)(1) through
(4).
Source:
Added at 15 Ill. Reg.
,
effective
Section 725.964
Recordkeeping Requirements
~J.
Lumping Units
fl
Each owner or operator subject to the provisions
QLthis Subpart shall comply with the
recordkeeping requirements of this Section.
21
An
owner
or operator of more than one hazardous
waste management unit subject to the provisions of
this Subpart may comply with the recondkeeping
requirements for these hazardous w~~~flag~ment
units
in one recordkeeping system
if the system
identifies each record by each hazardous waste
management unit.
hi
pwners and operators shall record the followin~g
information in the facility operatjng record:
~j
For each piece of equipment to which this Subpart
applies:
~j
Equipment identification number and h~zardous
waste management unit identification.
~j
approximate locations within the f~ci1ity
(e.g.,
identify the hazardous waste
121—381
233
management unit on a facility plot plan).
çj
Type
of equipment (e.g.,
a pump or pipeline
valve).
~j
Percent-by-weight total organics in the
hazardous wastestream at the equipment.
~j
Hazardous waste state at the equipment (e.g.
gas/vapor
on
liquid).
fi
Method of compliance with the standard
(e.g.
“monthly leak detection and repair” or
“equipped with dual mechanical seals”).
21
for facilities than comply with the provisions of
Section 725.933 (a) (2).
an implementation schedule
as specified in that Section.
IL
Where an owner or operator chooses to use test
data to demonstrate the organic removal efficiency
on total organic compound concentration achieved.
by the control device,
a performance test plan as
specified in Section 725.93S(b) (3).
41
Documentation of compliance with Section 725.960,
including the detailed design documentation or
performance test results specified in Section
725.935(b) (4).
gj
When each leak is detected as specified in Sections
725.952. 725.953, 725.957 or 725.958. the following
requirements apply:
fl
A weatherproof and readily visible identification,
marked with the equipment identification number,
the date evidence of a potential leak was found in
accordance with Section 725.958(a),
and the date
the leak was detected, must be attached to the
leaking equipment.
21
The identification on equipment except on a valve,
may be removed after it has been repaired.
IL
The identification on a valve may be removed after
it has been monitored for
2 successive months as
specified in Section 725.957(c)
and no leak has
been detected during those
2 months.
.ç~j
When each leak is detected as specified in Sections
725.952,
725.953, 725.957 or 725.958, the following
information must be recorded in an inspection log and
12
1—3 82
234
must be kept in the facility operating record:
LJ.
The instrument and operator identification numbers
and the equipment identification number.
21
The date evidence of a potential leak was found in
accordance with Section 725.958(a).
IL
The date the leak was detected and the dates of
each attempt to repair the leak.
41
Repair methods applied in each attempt to repair
the leak.
~J.
“Above 10,000”,
if the maximum instrument reading
measured by the methods specified in Section
725.963(b)
after each repair attempt
is equal to
or greater than 10,000 ppm.
~j.
“Repair delayed” and the reason for the delay if a
leak is not repaired within 15 calendar days after
discovery of the leak.
fl
Documentation supporting the delay of repair of a
valve in compliance with Section 725.959(c).
fi
The signature of the owner or operator
(or
designate)
whose decision it was that repair could
not be effected without a hazardous waste
management unit shutdown.
2J
The expected date of successful repair of the leak
if a leak is not repaired within 15 calendar days.
j~Q)
The date of successful repair of the leak.
~j
Design documentation ard monitoring,
operating and
inspection information for each closed—vent system and
control device required to comply with the provisions
of Section 725.960 must be recorded and kept up-to—
date in the facility operating record as specified in
~çtion
725.935(c) (1)
and
(2),
and monitoring,
operating and inspection information in Section
725.935(c)(3)
through
(8).
fi
For a control device other than a thermal va~p~
incinerator, catalytic vapor incinerator,
flare,
boiler, process heater,
condenser,
or carbon adsorption
system, monitoring and inspection information
incating proper operation and maintenance of the
g~~ntroldevice must be recorded in the facility
gp~~tingrecord.
12 1—383
235
gj
The following information pertaining to all equipment
subject to the requirements in Sections 725.952 through
725.960 must be recorded in a log that is kept in the
facility operating record:
fl
A list of identification numbers for equipment
(except
welded fittings) subject to the
requirements of this Subpart.
21
List
of
Equipment
~j
A list of identification numbers for
equipment that the owner or operator elects
to designate for no detectable emissions,
as
indicated by an instrument reading of less
than 500 ppm above background,
under the
provisions of Sections 725.952(e),
725.953(i)
and 725.957(f).
~
The designation of this equipment as subject
to the requirements of Sections 725.952(e),
725.953(i) or 725.957(f) must be signed by
the owner or operator.
IL
A list of equipment identification numbers for
pressure relief devices required to comply with
Section 725.954 (a).
41
Compliance tests.
j~j
The dates of each compliance test required in
Sections 725.952(e),
725.953(i),
72S.954 and
725.957(f).
~
The background level measured during each
compliance test.
QJ
The maximum instrument reading measured at
the equipment during each compliance test.
~j
A list of identification numbers for equipment in
vacuum
service.
hi
The following information pertaining to all valves
sublect to the requirements of Section 725.957(g)
and
(hI must be recorded in a log that is kept in the
facility operating record:
fl
A list of identification numbers for valves that
are designated as unsafe to monitor,
an
explanation for each valve stating why the va~
121—384
236
is unsafe to monitor, and the plan for monitoring
each valve.
21
A list of identification numbers for valves that
are designated as difficult to monitor,
an
explanation for each valve stating why the valve
is difficult to monitor, and the planned schedule
for monitoring each valve.
j)
The following information must be recorded in the
facility operating record for valves complying with
Section 725.962:
flU.
A schedule of monitoring.
21
The percent of valves found leaking during each
monitoring period.
jJ
The following information must be recorded in a log
that is kept in the facility operating record:
fl
Criteria required in Section 725.952(d) (5) (B)
and
725.953(e) (2) and an explanation of the criteria.
21
Any changes to these criteria and the reasons for
the changes.
~
The following inforipation must be recorded in a
lo~g
that is kept in the facility operating record for use
in determining exemptions as provided in Section
725.9S0 and other specific Subparts:
j)
An analysis determining the design capacity of the
hazardous waste management unit.
21
A statement listing the hazardous waste influent
to and effluent from each hazardous waste
management unit subject to the requirements in
Sections 725.960 and an analysis determining
whether these hazardous wastes are heavy liquids.
IL
An up-to-date analysis and the supporting
information and data used to determine whether or
not e~ipmentis subject to the requirements in
Sections 725.952 through 725.960.
The record must
include supporting documentation as required by
Section 725.963(d) (3) when application of the
j~~eofthe nature of the hazardous
wastestream or the process by which
it
was
produced is used.
If the owner or operator takes
a~yaction je.g., changing the process that
~ç~d
the waste)
that could result in~
121—385
237
increase in the total organic content of the waste
contained in or contacted by equipment determined
not to be subject to the requirements in Sections
725.952 through 725.960, then
a new determination
is
required.
fl
Records of the equipment leak information required by
subsection
(d)
and the operating information required
by subsection
(e) need be kept only 3 years.
~
The owner or operator of any facility that is subject
to this Subpart and to reg~1ationsat
40 CFR 60,
Subpart VV, or 40 CFR 61, Subpart V. incorporated by
reference in
35 Ill. Adm. Code 720.111, may elect to
determine compliance with this Subpart by documentation
either pursuant to Section 725.964,
or pursuant to
those provisions of 40 CFR 60 or 61, to the extent that
the documentation under the regulation at 40 CFR 60 or
61 duplicates the documentation required under this
Subpart.
The documentation under the regulation at 40
CFR 60 or
61 must be kept with or made readily
available with the facility operating record.
Source:
Added at 15 Ill.
Reg.
,
effective
12 1—3 86
238
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER
I:
POLLUTION CONTROL BOARD
SUBCHAPTER c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 726
STANDARDS FOR THE MANAGEMENT OF SPECIFIC HAZARDOUS WASTE
AND SPECIFIC TYPES OF HAZARDOUS WASTE
MANAGEMENT FACILITIES
SUBPART
C:
RECYCLABLE MATERIALS
USED IN A MANNER
CONSTITUTING DISPOSAL
Section
726.120
Applicability
726.121
Standards applicable to generators and transporters of
materials used in a manner that constitutes disposal
726.122
Standards applicable to storers, who are not the
ultimate users,
of materials that are to be used in
a
manner that constitutes disposal
726.123
Standards applicable to users of materials that are
used in a manner that constitutes disposal
SUBPART
D:
HAZARDOUS WASTE BURNED FOR ENERGY RECOVERY
Section
726.130
Applicability
726. 131
Prohibitions
726.132
Standards applicable to generators of hazardous waste
fuel
726.133
Standards applicable to transporters of hazardous waste
fuel
726.134
Standards applicable to marketers of hazardous waste
fuel
726.135
Standards applicable to burners of hazardous waste
fuel
726.136
Conditional exemption for spent materials and by-
products exhibiting a characteristic of hazardous waste
(Repealed)
SUBPART E:
USED OIL BURNED FOR ENERGY RECOVERY
Section
726.140
Applicability
726.141
Prohibitions
726.142
Sta~~dardsapplicable to generators of used oil burned
for energy recovery
726.143
Standards applicable to marketers of used oil burned
for energy recovery
726.144
Standards applicable to burners of used oil burned for
energy recovery
SUBPART
F:
RECYCLABLE
MATERIALS
UTILIZED
FOR
PRECIOUS
METAL
RECOVERY
Section
726.170
Applicability and requirements
121—387
239
SUBPART G:
SPENT LEAD-ACID BATTERIES BEING RECLAIMED
Section
726.180
Applicability and requirements
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111 1/2, pars.
1022.4 and 1027).
SOURCE:
Adopted
in
R85-22
at
10
Ill.
Reg.
1162,
effective
January
2,
1986;
amended
in
R86—l
at
10
Ill.
Reg.
14156,
effective
August
12,
1986;
amended
in
R87-26
at
12
Ill.
Reg.
2900, effective January 15,
1988; amended in R89—l
at 13
Ill.
Reg. 18606, effective November 13,
1989; amended in R90—2 at 14
Ill. Reg.
14533, effective August 22,
1990;
amended in R90—11 at
15 Ill. Reg.
,
effective
SUBPART D:
HAZARDOUS WASTE BURNED FOR ENERGY RECOVERY
Section 726.136
Conditional exemption for spent materials and
by—prodicts exhibiting a characteristic of
hazardous waste (Repealed)
e~
Except as provided in paragraph
(b), hazardous waste
fuels that are spent materials and by—products and that
are hazardous only because they exhibit a
characteristic of hazardous waste are not subject to
the
notification
requircmcnt3
of
Section 3010 of
the
Resource Conservation and Recovery Act, the generator,
transporter or storage requirements of 35 Ill.
Adm.
Code
722
through
725,
or
35
Ill. Adm.
Code 702,
703 or
705.
b~
This exemption does not apply when the spent mateni~
or by product is stored. in a surface
impe~ndmcnt
prior
Source:
Repealed at 15 Ill. Reg.
,
effective
12 1—388
240
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER
c:
HAZARDOUS
WASTE
OPERATING
REQUIREMENTS
PART 728
LAND
DISPOSAL RESTRICTIONS
SUBPART A:
GENERAL
Section
728.101
Purpose, Scope and Applicability
728.102
Definitions
728.103
Dilution Prohibited as a Substitute for Treatment
728.104
Treatment Surface Impoundment Exemption
728.105
Procedures for case—by—case Extensions to an Effective
Date
728.106
Petitions to Allow Land Disposal of a Waste Prohibited
under Subpart C
728.107
Waste Analysis and Recordkeeping
728.108
Landfill and Surface Impoundment Disposal Restrictions
728.109
Special Rules for Characteristic Wastes
SUBPART
C:
PROHIBITION
ON
LAND
DISPOSAL
Section
728.130
728.131
728. 132
728.133
728.134
728.135
728. 139
Section
728.140
728.141
728.142
728.143
728. 144
Section
728.150
Appendix A
Appendix B
Appendix C
~pp~jj~jxD
~pp~n~jxE
Appendix F
Appendix G
Waste Specific Prohibitions
--
Solvent Wastes
Waste Specific Prohibitions
—-
Dioxin-Containing Wastes
Waste Specific Prohibitions
--
California List Wastes
Waste Specific Prohibitions
-—
First Third Wastes
Waste Specific Prohibitions
--
Second Third Wastes
Waste Specific Prohibitions
--
Third Third Wastes
Statutory Prohibitions
SUBPART
D:
TREATMENT STANDARDS
Applicability of Treatment Standards
Treatment Standards expressed as Concentrations in
Waste Extract
Treatment Standards expressed as Specified Technologies
Tr-~atmentStandards expressed as Waste Concentrations
Acijustinent of Treatment Standard
SUBPART E:
PROHIBITIONS ON
STORAGE
Prohibitions on Storage of Restricted Wastes
Toxicity Characteristic Leaching Procedure
(TCLP)
Treatment Standards (As concentrations in the
Treatment Residual Extract)
List of Halogenated Organic Compounds
Organometallic Lab Packs
Organic Lab Packs
Technologies
to
Achieve
Deactivation
of
Characteristics
Federal
Effective
Dates
12 1—389
241
Appendix H
National Capacity LDR Variances for UIC Wastes
Table A
Constituent Concentrations in Waste Extract (CCWE)
Table B
Constituent Concentrations in Wastes
(CCW)
Table C
Technology Codes and Description of Technology-Based
Standards
Table D
Technology-Based Standards by RCRA Waste Code
Table E
Standards for Radioactive Mixed Waste
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev. Stat.
1989,
ch.
111 1/2, pans.
1022.4 and 1027).
SOURCE:
Adopted in R87-5 at 11 Ill. Reg.
19354, effective
November 12,
1987; amended in R87—39 at
12
Ill.
Reg.
13046,
effective July 29,
1988;
amended in R89—l at
13
Ill. Reg.
18403,
effective November 13,
1989; amended in R89—9 at 14
Ill. Reg.
6232, effective April
16,
1990; amended in R90—2 at
14 Ill. Reg.
14470,
effective August 22,
1990; amended in R90—10 at
14 Ill.
Reg.
16508,
effective September 25,
1990;
amended in R90-l1 at
15
Ill.
Reg.
,
effective
SUBPART A:
GENERAL
Section 728.101
Purpose, Scope and Applicability
a)
This Pant identifies hazardous wastes that are
restricted from land disposal and defines those limited
circumstances under which an otherwise prohibited waste
may continue to be land disposed.
b)
Except as specifically provided otherwise in this Part
or 35 Ill. Adm. Code 721, the requirements of this Part
apply to persons who generate or transport hazardous
waste and to owners and operators of hazardous waste
treatment,
storage and disposal facilities.
c)
Restricted wastes may continue to be land disposed as
follows:
1)
Where persons have been granted an extension to
the effective date of a prohibition under Subpart
C or pursuant to Section 728.105, with respect to
those wastes covered by the extension;
2)
Where persons have been granted an exemption from
a prohibition punsuant.to a petition under Section
728.106, with respect to those wastes and units
covered by the petition;
IL
Wastes that are hazardous only because they
121—390
242
exhibit a hazardous characteristic,
and which are
otherwise prohibited from land disposal under this
Part, are not prohibited from land disposal
if the
wastes:
~j
Are disposed into a nonhazandous on hazardous
waste injection well as defined in 35 Ill.
Acim.
Code 704.106(a); and
~j
Do not exhibit any prohibited characteristic
of hazardous waste at the point of iniection.
5)
Prior to May
8,
1990,
in
a landfill or surface
-impoundment unit
where
all
~applicable
persons
are
-in
compliance with the requirements of Section
720.108. with respect
F~~~iFma~
to wastes which
r~t—
~
~
are—not
fr~i—+h
i
ri
subject to the
Subpart
D,
and which are not subject to the
prohibitions in Section 728.132 or 728.139.
d)
This Part doe~’not affect the availability of a waiver
under Section 121(d) (4) of the Comprehensive
Environmental Response, Compensation, and Liability Act
of 1980
(CERCLA)
(42 U.S.C.
9601 et seq).
e)
The following hazardous wastes are not subject to any
provision of this Part:
1)
Wastes generated by small quantity generators of
less than 100 kg of non—acute hazardous waste or
less than
1 kg of acute hazardous waste per month,
as defined in 35 Iii. Adm.
Code 721.105;
2)
Waste pesticides that a farmer disposes of
pursuant to 35 Ill.
Adm. Code 722.170;
3)
Wastes identified or listed as hazardous after
November 8,
1984,
for which USEPA has not
promulgated land disposal prohibitions or
treatment standards.
f)
This Part is cumulative with the land disposal
restrictions of 35
Ill. Adm. Code 729.
The
Environmental Protection Agency (Agency)
shall not
issue a wastestream authorization pursuant to 35
Ill.
Adm. Code 709 or Sections 22.6 or 39(h)
of the
Environmental Protection Act
(Ill. Rev.
Stat.
1987,
ch.
111 1/2, pars.
1022.6 or 1039(h)) unless the waste
meets the requirements of this Part as well as 35 Ill.
Adin. Code 729.
Source:
Amended at
15
Ill. Reg.
,
effective
121—391
243
Section 728.102
Definitions
a~
When used in this Part the following terms have the
meanings given
belowi-.
All other terms have the
meanings given under 35 Ill.
Adm. Code 702.l10~
720.110, 720.102 or 721.103.
“Agency” means the Illinois Environmental Protection
Agency.
“Board” means the Illinois Pollution Control Board.
“CERCLA” means the Comprehensive Environmental
Response, Compensation, and Liability Act of 1980
(42
U.S.C.
9601 et seq.)
“Halogenated organic compounds” or “HOCs” means those
compounds having a carbon—halogen bond which are listed
under Appendix C.
“Hazardous constituent or constituents” means those
constituents listed in 35 Ill.
Adm. Code 72l.Appendix
H.
Inorganic Solid Debris are nonfniable inorganic solids
that are incapable of passing through a 9.5 mm standard
sieve, and that require cutting, or crushing and
grinding,
in mechanical sizing equipment prior to
stabilization, limited to the following inorganic or
metal materials:
Metal slags
(either dross or sconia).
Glassified slag.
Glass.
Concrete (excluding cementitious or pozzolanic
stabilized hazardous wastes).
Masonry and refractory bricks.
Metal
cans,
containers, drums or tanks.
Metal nuts, bolts, pipes, pumps, valves,
appliances or industrial equipment.
Scrap metal
as defined in 35 Ill.
Adrn, Code
721.101(c) (6)
12 1—392
244
“Land disposal” means placement in or on the land and
includes, but is not limited to, placement in a
landfill, surface impoundment, waste pile,
injection
well,
land treatment facility,
salt dome formation,
salt bed formation, underground mine or cave,
or
placement in a concrete vault on bunker intended for
disposal purposes.
“Nonwastewaters” are wastes that do not meet the
criteria for “wastewaters” in this Section.
“Polychloninated biphenyls” or “PCBs” are halogenated
organic compounds defined in accordance with 40 CFR
761.3,
incorporated by reference in 35 Ill.
Adm. Code
720.111
“ppm” means parts per million.
“RCRA
corrective action” means corrective action taken
under 35 Ill.
Adm. Code 724.200 or 725.193,
40 CFR
264.100 on 265.93
(1987), or similar regulations in
other States with RCRA programs authorized by USEPA
pursuant to 40 CFR 271
(19862).
“USEPA” means the United States Environmental
Protection Agency.
“Wastewaters” are wastes that contain less than 1
by
weight total organic carbon
(TOC)
and less than 1
by
weight total suspended solids (TSS), with the following
exceptions:
FOOl,
F002, F003,
F004,
F005 solvent—water
mixtjires that contain less than 1
by weight TOC
or less than 1
by wejgiht total FOOl,
F002,
F003,
F004,
F005 solvent constituents listed in Table A.
KOll, K0l3,
K014 wastewaters
(as generated)
that
ontain less than 5
bY weight TOC and less than
1
by weight TSS.
1103
and 1104
w~ewaters that~gpntainless than
4
by weight TOC and less than 1
by weight TSS.
b-)--——-A-l-l----e-ther terms
have the meanings given under 35
Ill.
Adm-----Gode
702.110,
720.110,
720.102—or 721.103.
Source:
Amended at 15 Ill.
Reg.
,
effective
12 1—393
245
Section 728.103
Dilution Prohibited as
a Substitute for
Treatment
~j
Except as provided in subsection
(b), nNo generator,
transporter, handler or owner or
operator
of
a
treatment,
storage or
disposal
facility shall in any
way dilute a restricted waste or the residual from
treatment of a restricted waste as a substitute for
adequate treatment to achieve compliance with Subpart
D, to circumvent the effective date of a prohibition in
Subpart
C, to otherwise avoid
a prohibition in Subpart
C.
~j
Dilution
of wastes that are hazardous only because they
exhibit a characteristic in a treatment system which
treats wastes subsequently discharged to a water of the
State pursuant to an NPDES permit issued under 35 Ill.
Adm. Code 309 or which treats wastes for purposes of
pretreatment requirements under 35 Ill.
Adm. Code 310
is not impermissible dilution for purposes of this
Section unless
a method has been specified as the
treatment standard in Section 728.142.
Source:
Amended at 15 Ill. Reg.
,
effective
Section 728.105
Procedures for case—by—case Extensions to an
Effective Date
a)
The Board incorporates by reference 40 CFR 268.5
(1989),
as amended at 54
Fed. Reg 36970, September
6,
1989,
and at 55 Fed.
Reg.
23935, June 13,
1990.
This
Part incorporates no future editions or amendments.
b)
Persons may apply to IJSEPA for extensions of effective
dates pursuant to 40 CFR 268.5.
Extensions which are
granted by USEPA will be deemed extensions of dates
specified in the derivative Board rule.
Source:
Amended at 15 Ill. Reg.
,
effective
Section 728.107
Waste Analysis and Recordkeeping
a)
Except as specified in Section 728.132 or 728.143, the
-generator shall test the generator’s waste,
or test an
extract developed using the test method described in
Appendix A, on use knowledge of the waste,
to determine
if the waste
is restricted from land disposal under
this Part.
1)
If a generator determines that the generator is
12 1—394
246
managing a restricted waste under this Part and
determines that the waste does not meet the
applicable treatment standards set forth in
Subpart D on exceeds the applicable prohibition
levels set forth in Section 728.132 or 728.139,
with each shipment of waste the generator shall
notify the treatment or storage facility in
writing of the appropriate treatment standard set
forth in Subpart D and any applicable prohibition
levels set forth in Section 728.132 or 728.139.
The notice must include the following information:
A)
USEPA Hazardous Waste Number;
B)
The corresponding treatment standards for
wastes FOOl-F005,
F039 and wastes prohibited
pursuant to Section 728.132 or Section
3004(d) of the Resource Conservation and
Recovery Act, referenced in Section 728.139.
Treatment standards for all other restricted
wastes must either be referenced as above,
or
by including on the notification the
subcategory of the waste, the treatability
group(s)
of the waste(s), and the Section and
subsection where the treatment standards
~pp~ar.
Where the applicable treatment
standards are expressed as specified
technologies in Section 728.142. the
applicable five-letter treatment code found
in Table C (e.g.,
INCIN, WETOX)
also must be
listed on the notification.
and
all-
applicable ~tandards
~et forth in Section
C)
The manifest number associated with the
shipment of waste; and
D)
Waste analysis data, where available.
2)
If a generator determines that the generator is
managing a restricted waste under this Part,
and
determines that the waste can be land disposed
without further treatment, with each shipment of
waste the generator shall
submit, to the
treatment,
storage or land disposal facility, a
notice and a certification stating that the waste
meets the applicable treatment standards set forth
in Subpart D and the applicable prohibition levels
set forth in Section 728.132 or 728.139.
A)
The notice must include the following
information:
121—395
247
i)
USEPA Hazardous Waste Number;
ii)
The corresponding treatment standard~
for wastes F001—F005, F039 and wastes
p~phibitedpursuant to Section 728.132
or Section 3004(d) of the Resource
Conservation and Recovery Act,
referenced
in
Section
728.139.
Treatment standards for all other
restricted wastes must either be
referenced as above,
or by including on
the notification the subcategory of the
waste,
the treatability group(s)
of the
waste(s), and the Section and subsection
where the treatment standards appear.
Where the applicable treatment standards
are expressed as specified technologies
in Section 728.142,
the applicable
five—letter treatment code found in
Table C
(e.g.,
INCIN, WETOX)
also must
be listed on the notification.j~
iii) The manifest number associated with the
shipment of waste;
iv)
Waste analysis data, where available.
B)
The certification must be signed by an
authorized representative and must state the
following:
I certify under penalty of law that I
personally have examined and am familiar
with the waste through analysis and
testing or through knowledge of the
waste to support this certification that
the waste complies with the treatment
standards specified in 35 Ill. Adm. Code
728.Subpart D and all applicable
prohibitions set forth in 35 Ill. Adm.
Code 728.132, 728.139 on Section 3004(d)
of the Resource Conservation and
Recovery Act.
I believe that the
information
I submitted is true,
accurate and complete.
I am aware that
there are significant penalties for
submitting a false certification,
including the possibility of a fine and
imprisonment.
3)
If a generator’s waste
is subject to an exemption
121—396
248
from
a prohibition on the type of land disposal
method utilized for the waste
(such as, but not
limited to,
a case—by—case extension under Section
728.105, an exemption under Section 728.106, an
extension under Section 728.101(c) (3)
or a
nationwide capacity variance under 40 CFR
268.Subpart C (1989), with each shipment of waste,
the generator shall submit a notice with the waste
to the facility receiving the generator’s waste,
stating that the waste is not prohibited from land
disposal.
The notice must include the following
in
formation:
A)
EPA hazardous waste number:
B)
The corresponding treatment standards for
wastes FOOl-F005,
F039 and wastes prohibited
pursuant to Secti~on728.132 or Section
3004(d) of the Resource Conservation and
R~cQveryAct, referenced in Section 728.139.
Treatment standards for all other restricted
wastes must either be referenced as above, or
by including on the notification the
subcategory of the waste, the treatability
group(s)
of the waste(s), and the Section and
subsection where the treatment standards
appear.
Where the applicable treatment
standards are expressed as specified
technologies in Section 728.142, the
applicable five-letter treatment code found
in Table C
(e.g.,
INCIN, WETOX)~lsomust be
listed on the notification.
and all
applicable prohibitions set forth in Section
728.132 or 728.139-p
C)
The manifest number associated with the
shipment of waste;
D)
Waste analysis data, where available,
and
E)
The date the waste is subject to the
prohibitions.
4)
If
a
generator
~
managing a p~Qhihited_wastein t~~sor containers
regulated under 35
Ill.
Adm. Code 722.134~and is
treating such waste
in such tanks or containers to
~ee~
applicable treatment standards under Subpart
Q~the generator shall develop and follow a
written
waste analysis plan whi~Ldescnibesthe
procedures the generator will carry out to comply
with the treatment standards.
The plan must be
121—397
249
kept on—site in the generator’s records, and the
following requirements must be met: that is
subject to the prohibitions under Section
728.133(f)
(including wastes that are disposed of
in disposal units other than l-andfilla or surface
impoundments) and is not subject to the
prohibitions set forth in Section 728.132, with
each shipment of waste,
the generator shall notify
the
treatment
storage
or
disposal
facility,
in
writing,
of
any
applicable
prohibitions
set
forth
in
Section
728.133(f).
The
notice-must
include
the
roi
inc’
J.nLoriaation:
A-~
UCEPA
hazardous
waste
number
&~
The applicable proniDiLions set iortn in
Cection 728.133(f)r
C-)
The manifest number associated with the
shipment of waste; and
D~)
Waste analysis data where available.
~j
The waste analysis plan must be based on a
detailed chemical and physical analysis of a
representative sample of the prohibited
waste(s) being treated, and contain all
information necessary to treat the waste(s)
in accordance with the requirements of this
Part,
including the selected testing
frequency.
~j
Such
plan
must be filed with the Agency a
minimum of 30 days prior to the treatment
activity, with delivery verified.
çj
Wastes shipped off-site pursuant to this
subsection must comply with the notification
requirements of Section 728.107(a) (2).
5)
If a generator determines whether the waste is
restricted based solely on the generator’s
knowledge of the waste, the generator shall retain
all supporting data used to make this
determination on—site in the generator’s
files.
If a generator determines whether the waste is
restricted based on testing the waste or an
extract developed using the test method described
in Appendix A, the generator shall retain all
waste analysis data on site in the generator’s
files.
121—398
250
6)
Generators shall retain on—site a copy of all
notices, certifications, demonstrations,
waste
analysis data and other documentation produced
pursuant
to
this
Section
for
at
least
five
years
from the date that the waste that is the subject
of such documentation was last sent to on—site or
off—site treatment storage or disposal.
The five
year record retention period
is automatically
extended during the course of any unresolved
enforcement action regarding the regulated
activity or as requested by the Agency.
21
If a generator is managing a la~packthat
contains wastes identified in Appendix D and
wishes to use the alternative treatment standard
under Section 728.142, with each shipment of waste
the generator shall submit a notice to the
treatment facility in accordance with subsection
(a) (1).
The generator shall also comply with the
requirements in subsections
(a) (5)
and
(a) (6), and
shall submit the following certification, which
must be signed by an authorized representative:
I certify under penalty of law that
I
personally have examined and am familiar with
the waste and that
the
lab pack contains only
the wastes specified in 35
Ill. Adm. Code
728.Appendix D or solid wastes not subject to
regulation under 35
Ill.
Adm. Code 721.
I am
aware that there are significant penalties
for submitting a false certification.
•rncluding the possibility of fine or
imprisonment.
~j.
If a generator is managing a lab pack that
contains organic wastes specified in Appendix E
and wishes to use the alternate treatment
standards under Section 728.142, with each
shipment of waste the generator shall submit a
notice to the treatment facility in accordance
with subsection
(a)(l).
The generator also shall
comply with the requirements
in subsections
(a) (5)
and
(a) (6), and shall submit the followin2
certification which must be signed by an
authorized representative:
I certify under penalty of law that
I
personally have examined and am familiar with
the waste through analysis and testing or
~brough knowledge of the w~s~eand that the
lab pack contains only organic waste
specified in
35 Ill. Adm. Code 728.Appendix E
12
1—399
251
or solid wastes not subject to regulation
under 35 Ill.
Adm. Code 721.
I am aware that
there are significant penalties for
submitting a false certification, including
the possibility of fine or imprisonment.
~j.
Small auantity generators with tolling agreements
pursuant to 35
Ill. Adm. Code 722.120(e)
shall
comply with the applicable notification and
certification requirements of subsection
(a)
for
the initial shipment of the waste subject to the
agreement.
Such generators shall retain on—site a
copy of the notification and certification.
together with the tolling agreement,
for at least
three years after termination or expiration of the
agreement.
The three—year record retention period
is automatically extended following notification
pursuant to Section 31(d)
of the Environmental
Protection Act, until either any subsequent
enforcement action
is resolved, or the Agency
notifies the generator documents need no be
retained.
b)
Treatment facilities shall test their wastes according
to the frequency specified in their waste analysis
plans as required by 35 Ill.
Adm. Code 724.113 or
725.113.
Such testing must be performed as provided in
subsections
(b) (1),
(b) (2)
and
(b) (3).
1)
For wastes with treatment standards expressed as
concentrations in the waste extract
(Section
728.141), the owner or operator of the treatment
facility shall test the treatment residues on an
extract of such residues developed using the test
method described in Appendix A to assure that the
treatment residues or extract meet the applicable
treatment standards.
2)
For wastes prohibited under Section 728.132 or
728.139 which are not subject to any treatment
standards
under
Subpart
D,
the owner or operator
of the treatment facility shall test the treatment
residues according to the generator testing
requirements specified in Section 728.132 to
assure that the treatment residues comply with the
applicable prohibitions.
3)
For wastes with treatment standards expressed as
concentrations in the waste
(Section 728.143), the
owner or operator of the treatment facility shall.
test the treatment residues
(not an extract of
such residues) to assure that the treatment
12 1—400
252
residues meet the applicable treatment standards.
4)
A notice must be sent to the land disposal
facility which includes the following information:
A)
USEPA Hazardous Waste Number;
B)
The corresponding treatment standards ~
wastes FOO1-F005, F039 and wastes prohibited
pursuant to Section 728.132 or Section
3004(d)
of the Resource Conservation and
Recovery Act, referenced in Section 728.139.
Treatment standards for all other restricted
wastes must either be referenced as above, or
by including on the notification the
subcategory of the waste,
the treatability
group(s)
of the waste(sl, and the Section and
subsection where the treatment standards
appear.
Where the applicable treatment
~jdards
are expressed as specified
technologies in Section 728.142, the
applicable five-letter treatment code found
in Table C
(e.g.,
INCIN, WETOX)
also must he
listed on the notification,
and all
apeble—prohibitions
set
forth
in
Section
728.132 on 728.139.
C)
The manifest number associated with the
shipment of waste: and
D)
Waste analysis data,
where available.
5)
The treatment facility shall submit a
certification with each shipment of waste or
treatment residue of a restricted waste to the
land disposal facility stating that the waste or
treatment residue has been treated in compliance
with the treatment standards specified in Subpart,,
D and the applicable prohibitions set forth in
Section 728.132 on 728.139.
A)
For wastes with treatment standards expressed
as concentrations in the waste extract or in
the waste
(Sections 728.141 or 728.143), on
for wastes prohibited under Section 728.132
on 728.139 which are not subject to any
treatment standards under Subpart D, the
certification must be signed by an authorized
representative and must state the following:
I certify under penalty of law that
I
have personally examined and am familiar
121—40
1
253
with the treatment technology and
operation of the treatment process used
to
support
this
certification and that,
based on my inquiry of those individuals
immediately responsible for obtaining
this infonm.~tion, I believe that the
treatment process has been operated and
maintained properly so as to comply with
the performance levels specified in 35
Ill.
Adm. Code 728.Subpart D and all
applicable
prohibitions
set
forth in 35
Ill.
Adm. Code 728.13-2 or 728.139
or
section 3004(d)
of the Resource
Conservation and Recovery Act without
impermissible dilution of the prohibited
waste.
I am aware that there are
significant penalties for submitting a
false certification,
including the
possibility of fine and imprisonment.
B)
For wastes with treatment standards expressed
as technologies
(Section 728.142), the
certification must be signed by an authorized
representative and must state the following:
I certify under penalty of law that the
waste has been treated in accordance
with the requirements of 35 Ill.
Adm.
Code 728.142.
I am aware that there are
significant penalties for submitting a
false certification, including the
possibility of fine and imprisonment.
~J.
For wastes with treatment standards expressed
as concentrations in the waste pursuant to
Section 728.143,
if compliance with the
treatment standards in Subpart D is based in
pant or in whole on the analytical detection
limit alternative specified in Section
728.143(c), the certification also must state
the following:
I certify under penalty of law that
I
have personally examined and am familiar
with the treatment technology and
operation of the treatment process used
to support this certifi
ion and that,
based on my inquiry of those individuals
immediately responsible for obtaining
this information,
I believe that the
nonwastewater organic constituents have
been treated by incineration
in units
121—402
254
Qperated in accordance with 35
Ill. Adm.
Code 724.Subpant
0) on 35
Ill. Adm. Code
725.Subpart 0. or.by combustion in fuel
substitution units operating in
accordance with applicable technical
requirements, and I have been unable to
detect the nonwastewaten organic
constituents despite having used best
good faith efforts to analyze for such
constituents.
I am aware that there are
significant penalties for submitting a
false certification, including the
possibility of fine and imprisonment.
6)
If the waste or treatment residue will be further
managed at a different treatment on storage
facility, the treatment, storage or disposal
facility sending the waste on treatment residue
off-site must comply with the notice and
certification requirements applicable to
generators under this Section.
7)
wastes that are suoject co cne proh.~~ons
under
Section 728.133(f)
and are not subject
to
the prohibitions set forth in Section 720.132,
with each shipment of such waste the owner on
-eperator shall notify any subsequent treatment,
storage or disposal facility in writing,
of any
applicable prohibitions in writing, of any
,irn-~1icableiwohibitions set forth in Section
~28.133(f).
The notice must include the—following
information:
1~
B)-
The
applicable—prohibitions
set
forth
in
Section 728.133(f);
Ct
.—
-
‘~
-Phc
~
~
number
with
the
shipment of waste;
and
there available.
B-)-——---Waste
analysis data,
Z)
Where the wastes are recyclable materials used in
a manner constituting disposal subject to the
provisions of 35
Ill. Adm. Code 726.120(b),
regarding treatment standards and prohibition
levels, the owner on operator of a treatment
facility
(i.e. the recyclen)
is not required to
notify the receiving facility pursuant to
subsection
(b) (4).
With each shipment of such
wastes the owner or operator of the recycling
12 1—403
255
facility shall submit a certification described in
subsection
(b) (5), and a notice which includes the
information listed in subsection
(b) (4)
(except
the manifest number) to the Agency.
The recycling
facility also shall
keep
records
of
the
name
and
location of each entity receiving the hazardous
waste—derived product.
c)
Except where the owner or operator is disposing
of
any
waste that is a recyclable material used in a manner
constituting disposal pursuant to 35 Ill. Adm. Code
726.120(b).
the Pbe owner on operator of any land
disposal facility disposing any waste subject to
restrictions under this Part shall:
1)
Have copies of the notice and certification
specified in subsection
(a)
or
(b), and the
certification specified in Section 728.108 if
applicable.
2)
Test the waste, or an extract of the waste or
treatment residue developed using the test method
described in Appendix A on using any methods
required by generators under Section 728.132, to
assure that the wastes or treatment residues are
in compliance with the applicable treatment
standards set forth in Subpart D and all
applicable prohibitions set forth in Sections
728.132 or 728.139.
Such testing must be
performed according to the frequency specified in
the facility’s waste analysis plan as required by
35 Ill. Adm. Code 724.113 on 725.113.
3)
Where the owner or operator is disposing of any
waste that is subject to the prohibitions under
Section 728.133(f) but not subject to the
prohibitions set forth
in Section 728.132, the
owner or operator shall ensure that such waste is
the subject of a certification according to the
requirements of Section 728.108 prior to disposal
in a landfill or surface impoundment unit,
and
that such disposal is in accordance with the
requirements of Section 728.105(h)(2).
The same
requirement applies to any waste that is subject
to the prohibitions under Section 728.133(f)
and
also is subject to the statutory prohibitions in
the codified prohibitions in Section 728.139 or
Section 728.132
4)
Where the owner or operator is disposing of any
waste that is a recyclable material used in a
manner constituting disposal subject to the
121—404
256
provisions of 35
Ill. Adm. Code 726.120(b),
the
owner or operator is not subject to subsections
(c) (1)
through
(3) with respect to such waste.
Source:
Amended at 15
Ill. Reg.
,
effective
Section 728.108
Landfill and Surface Impoundment Disposal
Restrictions
(Repealed)
i-ne ~oura incorpora-ce3 ~y retenence 40
CFR
260.8
(1900j,
as
amended
at
54
Fed.
Reg.
36970,
September
6,
1900.
This
Section
incorporates
no
future
editions
on
amendments.
Prior
to
May
0,
1990, wastes which are otherwise prohibited from land disposal
under
Section
728.133(f)
may
be
disposed
in
a
landfill
or
surface
impoundment which is in compliance with the requirements of 40
CFR
2G8.5(h)
(2),
incorporated
by
reference
in
Section
728.105,
provided
the
requirements
of
40
CFR
260.8
are
met--
Source:
Repealed
at
15
Ill.
Reg.
,
effective
Section
728.109
Special Rules for Characteristic Wastes
~j
The
initial
generator
of
a
solid waste shall determine
each waste code applicable to the waste in order to
determine the applicable treatment standards under
Subpart D.
For purposes of pant 268, the waste will
carry a waste code designation for any applicable
listing under 35 Ill.
Adm. Code 721.Subpart
D.
and also
one or more waste code designations under 35
Ill. Adm.
Code 721.Subpart C where the waste exhibits the
relevant characteristic.
~j
Where
a prohibited waste is both listed under 35
Ill.
Adm. Code 721.Subpart D and exhibits a characteristic
under 35
Ill. Adm. Code 721.Subpart C, the treatment
standard for the waste code listed in 35
Ill.
Adm. Code
72l.Subpart D will operate in lieu of the standard for
the waste code under 35
Ill.
Adm. Code 721.Subpart
C,
provided that the treatment standard for the listed
waste includes
a treatment standard for the constituent
that causes the waste to exhibit the characteristic.
Otherwise, the waste must meet the treatment standards
for all applicable listed and characteristic waste
codes.
gj
In addition to any applicable standards determined
from
~he initial point of generation,
no prohibited waste
which exhibits
a characteristic under 35 Ill.
Adm. Code
721.Subpart C shall be land di~p
unjess
the waste
complies with the treatment standards under Subpart D.
121—405
257
~jJ
Wastes that exhibit a characteristic are also subject
to Section 728.107 requirements, except that once the
waste
is
no
longer
hazardous,
for
each
shipment
of
such
wastes to a non—hazardous waste facility, regulated
under 35 Ill. Adm. Code 807 or 811 through 815,
or
exempted under Section 21(d) (1) (i) of the Environmental
Protection Act, or similarly regulated in other States,-
the initial generator or the treatment facility need
not send a Section 728.107 notification to such
facility.
In such circumstances, a notification and
certification
must
be
sent
to
the
Agency,
or,
for
out-
of-State
shipments,
to
the
appropriate
USEPA
Regional
Administrator
or
State
authorized,
pursuant
to
40
CFR
271,
to
implement
40
CFR
268 requirements.
fl
The
notification
must
include
the
following
information:
~j
The name and address of the non—hazardous
waste facility receiving the waste shipment
~j
A description of the waste as initially
generated,
including the applicable USEPA
Hazardous Waste Number(s)
and treatability
group(s)
~j
The treatment standards applicable to the
waste at the initial point of generation.
21
The certification must be signed by an authorized
representative and must state the language found
in Section 728.107(b) (5) (A).
Source:
Added at 15 Ill.
Reg.
,
effective
SUBPART
C:
PROHIBITIONS ON
LAND
DISPOSAL
Section 728.135
Waste Specific Prohibitions-—Third Third
wastes.
~j
The following wastes are prohibited from land disposal.
~j
The
wastes
specified
in
35
Ill.
Adm.
Code
721.131
as
EPA
Hazardous
Waste
Numbers:
F006 (wastewaters).
FO19
F039 (wastewaters)
121—406
258
21
The wastes specified in
35 Ill.
Adm. Code 721.132
as EPA Hazardous Waste Numbers:
KO02
KO03
K004
(wastewaters)
1005
(wastewaters)
1006
1(008
(wastewatens)
1011
(wastewaters)
1013
(wastewaters)
1014
(wastewatens)
1(017
1021
(wastewaters)
K022
(wastewaters)
1025
(wastewaters)
1026
K029
(wastewaters)
1031
(wastewaters)
KO32
K033
K034
KO35
K041
K04 2
K046
(wastewaters)
1(048
(wastewaters)
K049
(wastewaters)
1050
(wastewaters)
1051
(wastewaters)
1052
(wastewaters)
1060
(wastewaters)
1061
(wastewaters)
1069
(wastewaters)
1073
1083
(wastewaters)
1084
(wastewaters)
K085
K095 (wastewaters)
K096 (wastewaters)
KO97
KO98
1100
(wastewaters)
1101
(wastewaters)
1102
(wastewaters)
1105
K106
(wastewaters)
fl
The
wastes
specified
in
35
Ill.
Adm.
Code
721.133(e)
as
EPA
Hazardous Waste Numbers:
P001
121—407
259
P002
P003
P004
P005
P006
P007
P008
P009
Polo
(wastewaters)
P011
(wastewatens)
P012
(wastewaters)
P014
P015
P016
P017
P018
(wastewaters)
P020
P022
P023
P024
P027
P028
P031
P033
P034
P036
(wastewaters)
P037
P038
(wastewaters)
P042
P045
P046
P047
P048
P049
P050
P051
P054
P056
P057
P058
P059
P060
P064
P065
(wastewaters)
P066
P067
P068
P069
P070
P072
P073
P075
121—408
260
41
P076
P077
P078
P081
P082
P084
P088
P092
P093
P095
P096
P101
P102
P103
P105
P108
P109
P110
P112
P113
P114
P115
P116
P118
P119
P120
P122
P123
The wastes specified in 35 Ill.
Adm. Code
721. 133 (f)
as EPA Hazardous Waste Numbers:
U0 01
U002
U003
U004
U005
U006
U007
U0 08
U009
U010
U011
U012
U014
U015
U016
U017
U018
U019
U020
U021
(wastewatens)~
12 1—409
261
U022
U023
U024
13025
U026
13027
13029
13030
U031
13032
13033
U034
U035
U036
U037
U038
U039
U04l
U042
13043
13044
13045
U046
U047
U048
U049
U050
U051
U052
U053
U055
U056
13057
13059
U060
13061
U062
U063
13064
U066
13067
13068
U070
13071
13072
U073
U074
U075
U076
U077
U078
U079
121—410
262
U080
U081
U0 82
13083
U084
U085
U086
U089
U090
U09l
U092
13093
U094
U095
13096
13097
U098
13099
UlOl
13103
U105
Ul 06
U108
U109
UllO
Ulll
Ull2
U1l3
U114
U115
Ui16
Ul17
U118
Ull9
U120
(wastewaters)
U121
U122
13123
Ul24
13125
13126
U127
13128
Ul2 9
13130
13131
Ul3 2
Ul33
13134
13135
13136
(wastewaters)
13137
121—411
263
U138
13140
13141
13142
13143
13144
13145
Ul46
13147
13148
13149
13150
Ul51
(wastewaters)
13152
13153
13154
Ul55
U156
Ul57
Ul58
U159
U160
U161
13162
Ul63
Ul64
U165
U16 6
13167
U168
Ul69
13170
13171
U172
U173
13174
U176
Ul77
U178
Ul79
Ul80
13181
13182
U183
U184
U185
13186
13187
U188
U189
U191
Ul92
121—412
264
U193
13194
13196
U197
13200
U201
U202
U203
13204
13205
U2 06
U207
U208
13209
U210
U2li
U213
13214
U215
U216
U2 17
U2i8
13219
13220
U2 22
U225
U226
13227
13228
13234
U2 36
13237
U2 38
U239
U240
13243
13244
13246
13247
13248
U2 49
41
The
following
wastes
identified
as
hazardous
based
on
a
characteristic
alone:
DO01
D002
DO03
DOO4
(wastewaters)
DO05
DO06
DO07
121—413
265
D008 (except for lead materials stored before
secondary smelting)
D009
(wastewatens)
DOlO
DOll
DO12
D013
DO14
DO15
DO16
DO 17
~j
The following wastes are prohibited from land disposal.
The wastes specified in 35 Ill.
Adm. Code 721.132 as
EPA Hazardous Waste Numbers:
1048
(nonwastewaters)
1049
(nonwastewaters)
KO5O (nonwastewaters)
1051
(nonwastewaters)
1052
(nonwastewaters)
Qj
Effective
May
8,
1992,
the
following
wastes
are
prohibited from land disposal:
fl
The wastes specified
in 35
Ill.
Adm. Code 721.131
as EPA Hazardous Waste Numbers:
F039
(nonwastewaters)
21
The wastes specified in 35
Ill. Adm.
Code 721.132
as EPA Hazardous Waste Numbers:
1031
(nonwastewaters)
KO84
(nonwastewaters)
KlOl (nonwastewaters)
1102
(nonwastewaters)
1106
(nonwastewaters)
fl
The
wastes
specified
in
35
Ill.
Adm.
Code
721.133(e)
as EPA Hazardous Waste Numbers:
P010
(nonwastewaters)
(nonwastewaters)
POll
P012 (nonwastewaters)
P036 (nonwastewaters)
P038 (nonwastewaters)
P065 (nonwastewaters)
P087
(nonwastewaters)
P092 (nonwastewaters)
41
The wastes specified in 35
Ill. Adm.
Code
12 1—414
266
721.133(f)
as
EPA
Hazardous
Waste
Numbers:
13136
(nonwastewaters)
13151
(nonwastewaters)
~j
The
following
wastes
identified
as
hazardous
based
on
a
characteristic
alone:
D004
(nonwastewatens)
DOO8
(lead materials stored before secondary
smelting)
D~O9(nonwastewaters)
~j
Inorganic solids debris as defined in
35 Ill.
Adm.
Code 728.102(a)(7)
(which also applies to chromium
refractory bricks carrying the EPA Hazardous Waste
Numbers K048-K052)
fl
RCRA
hazardous
wastes
that
contain
naturally
occurring
radioactive
materials.
~j
Effective Nay 8,
1992.
hazardous wastes listed in 40
CFR
268.12
that
are
mixed
radioactive/hazardous
wastes
are prohibited
from land disposal.
~j
Effective
Nay
8,
1992,
the
wastes
specified
in
this
Section
having
a
treatment
standard
in
Subpart
D
based
on
incineration,
mercury
retorting
or
vitrification,
and
which
are
contaminated
soil
or
debris,
are
prohibited
from
land dis~osa1.
~fl
Between
May
8,
1990,
and
May
8,
1992,
wastes
included
in
subsections
(c),
(d)
and
(e)
shall
be
disposed
of
in
a
landfill
or
surface
impoundment
only
if
such
unit
is
in
compliance
with
the
requirements
specified
in
Section
728,105(h)
(2).
il
The
requirements
of
subsections
(a),
(b).
(c),
(d)
and
(e)
do
not
apply
if:
fl
The
w~stes
meet
the
applicable
standards
specified
in
Subpart
D
21
Persons
have
been aranted an exemption from
a
prohibition
pursuant
to
a
petition
under
Section
728.106,
with
respect
to
those
wastes
and
units
covered
by
the
petition
~J
The
wastes
meet
the
applicable
alternate
standards
established
pursuant
to
a
petition
granted
under
Section
728.144
12 1—415
267
41
Persons
have
been
granted
an
extension
to
the
effective date of a prohibition pursuant to
Section 728.105. with respect to these wastes
covered by the extension.
jj
To
determine
whether
a
hazardous
waste
listed
in
40
CFR
268.10,
268.11 and 268.12 exceeds the applicable
treatment standards specified in Sections 728.141 and
728.143. the initial generator shall either test a
representative sample of the waste extract or the
entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste
extract or the waste,
on use knowledge of the waste.
If the waste contains constituents in excess of the
applicable Subpart D levels, the waste is prohibited
from land disposal, and all reguirements of this Part
are applicable,
except as otherwise specified.
SUBPART D:
TREATMENT STANDARDS
Section 728.140
Applicability of Treatment Standards
a)
A restricted waste identified in Section 728.141 may be
land disposed without further treatment only if an
extract of the waste or of the treatment residue of the
waste developed using the test method Appendix A does
not exceed the value shown in Table A for any hazardous
constituent listed in Table A for that waste, with the
following exceptions:
DOO4, DOO8, KO31,
1084,
1101,
K1021 POlO,
P011, P012,
P036, P038 and 13136.
Wastes
DOO4, DOO8,
1031,
K084,
1101,
1102,
POlO,
POll.
P012,
P036, P038 and 13136 may be land disposed~onlyif an
extract of the waste or of the treatment residue of the
waste developed using either the test method in 35
Ill.
Adin. ~Code 721.Appendix A or the test method in 35 Ill.
Adm. Code 728.Appendix B does not exceed the value
shown in Table B for any hazardous constituent listed
in Table A for that waste.
b)
A restricted waste for which a treatment technology is
specified under Section 728.142(a) may be land disposed
after it is treated using that specified technology or
an equivalent treatment method approved by the Agency
under the procedures set forth in Section 728.142(b).
c)
Except as otherwise specifies in Section 728.143(cL~aA
restricted waste identified in Section 728.143 may be
land disposed only if the constituent concentrations in
the waste on treatment residue of the waste do not
exceed the value shown in Table B for any hazardous
constituent listed in Table B for that waste.
12
1—4
16
268
Source:
Amended at 15 Ill. Reg.
,
effective
Section 728.141
Treatment Standards expressed as
Concentrations in Waste Extract
a)
Table A identifies the restricted wastes and the
concentrations of their associated hazardous
constituents which may not be exceeded by the extract
of a waste or waste treatment residual developed using
the test method in Appendix A for the allowable land
disposal of such waste, with the exception of wastes
DOO4,
D008, K031,
1084,
1101,
1102,
POlO,
POll,
P012.
P036,
P038 and Ul36.
Table A identifies the restricted
wastes D004,
DOOB, KO31,
1084,
KiOl, Kl02,
POlO.
POll,
P012,
P036, P038 and U136 and the concentrations of
their associated constituents which shall not be
exceeded by the extract of a waste or waste treatment
residual developed using the test method in 35
Ill.
Adm. Code 721~ppendixA or B for the allowable land
disposal of such wastes.
(Appendix B provides guidance
on treatment methods that have been shown to achieve
the Table A levels for the respective wastes.
Appendix
B is not a regulatory requirement but is provided to
assist generators and owners or operators in their
selection of appropriate treatment methods.)
Compliance
with these concentrations is required based on grab
samples.
b)
When wastes with differing treatment standards for a
constituent of concern are combined for purposes
of
treatment, the treatment residue must meet the lowest
treatment standard for the constituent of concern.
Section 728.142
Treatment Standards expressed as Specified
Technologies
a)
The following wastes in subsections
(a) (1) and
(2)
and
Table
D and E must be treated using the i-dentified
technology
on
technologies
~gJ~jed
in subsections
(a)Ll)
and
(2) and Table C.,
on an equivalent method
approved-under
subsection
(b).
1)
‘iquid hazardous wastes containing PCB5 at
concentrations greaten than or equal to 50 ppm but
less than 500 ppm must be incinerated in
accordance with technical requirements at 40 CFR
761.70, incorporated by reference in 35 Iii.
Adm.
Code 720.111, or burned in high efficiency boilers
in accordance with the technical requirements of
40 CFR 761.60.
Liquid hazardous wastes
121—417
269
containing
PCBs
at
concentrations
greaten
than
or
equal to 500 ppm must be incinerated in accordance
with the technical requirements of 40 CFR 761.70.
Thermal treatment in accordance with this Section
must be in compliance with applicable regulations
in 35
Ill. Adm. Code 724,
725 and 726.
2)
Nonliquid hazardous wastes containing halogenated
organic compounds (HOC5)
in total concentrations
greater than or equal to 1000 mg/kg and liquid
HOC-containing wastes that are prohibited under
Section 728.132(e) (1) must be incinerated in
accordance with the requirements of 35 Ill. Adm.
Code 724.Subpart 0 on 35 Ill.
Adm. Code
725.Subpart 0, or in boilers
-or
industrial
furnaces,
as defined in 35
Ill. Adm. Code 720,
bu-rning in accordance with
35-
Ill. Adm. Code 726.
These treatment standards do not apply where the
waste is subject to a Subpart C treatment standard
for a specific HOC (such as a hazardous waste
chlorinated solvent for which a treatment standard
is established under Section 728.141(a)).
-3-i
The nonwastewater form of the following ha-z-ardous
wastes -must be incinerated in accordance with the
requirements of
35 Ill.
Adm. -Code 724.Subpant 0,
on
35 Ill. Mm.
Code 725.Cubpart
0,
or
burned
in
boilers or industrial furnaces,
as defined in 35
Ill. Mm. Code-720,
in accordance with 35
Ill.
Mm..
Code
726:
1039
1113
1114
1115
1(116
P040
P041
P043
P044
r. r~
~
-~
J_ ,.J~_
P035
P109
Pill
U058
130137
TT—~~
U22-3-
4-)
The
wastewater
form
of—
the
following na~araous
-carbon--adsorption, or
121—418
270
incineration, or pretreatment followed by carbon
adsorption:
1027
1039
1113
1114
1115
1116
P040
P041
P043
P044
P062
P085
P109
Pill
U058
UO87
TT~~
._, L.~.
T1~~
¼)
~.
~.
.J
b)
Any person may submit an application to the Agency
demonstrating that an alternative treatment method can
achieve a level of performance equivalent to that
achievable by methods specified in subsection~(a),
(c)-
and
(d).
The applicant shall submit information
demonstrating that the applicant’s treatment method is
in compliance with federal and state requirements,
including this Part,
35
Ill. Mm.
Code 709, 724,
725,
726 and 729 and Sections 22.6 and 39(h)
of the
Environmental Protection Act
(Ill.
Rev.
Stat.
1987,
ch.
111 1/2, pars.
1022.6 and 1039(h)), and is protective
of human health or the environment.
On the basis of
such information and any other available information,
the Agency shall approve the use of the alternative
treatment method
if the Agency finds that the
alternative treatment method provides a measure of
performance equivalent to that achieved by methods
specified in subsection~(a)~(c)
and
(d).
Any
approval must be stated in writing and may contain such
provisions and conditions as the Agency determines to
be appropriate.
The person to whom such
approvaleertification is issued shall comply with all
limitations contained in such determination.
~
As an alternative to the otherwise applicable Subpart D
treatment standards,
lab p~cks
ai~e
eligible for land
disposal provided the following requirements are met:
~j
The labpacks comply with the applicable
provisions of 35 Ill.
Adm. Code 72416
and
121—419
271
725.416;
BOARD
NOTE:
35
Ill.
Adm.
Code 729.301 and 729.312
include additional restrictions on the use of lab
packs.
21
All hazardous wastes contained in such lab packs
are
specified
in
Appendix
D
or Appendix E
fl
The
lab packs are incinerated in accordance with
the
requirements
of
35
Ill. Mm.
Code 724.Subpart
0 or 35 Ill. Adm.
Code 725.Subpart 0; and
41
Any incinerator residues from lab packs containing
D004.
D005. D006,
DOO7,
DOOS,
DOlO and DOll are
treated in compliance with the applicable
treatment standards specified for such wastes in
Subpart
D.
~j.
Radioactive hazardous mixed wastes with treatment
standards specified in Table
E are n.pt subject to any
treatment standards specified in Section 728.141,
Section 728.143 or Table
D.
Radioactive hazardous
mixed wastes not subject to treatment standards in
Table
E remain subject to all applicable treatment
standards specified in Section 728.141, Section 728.143
and Table D.
Source:
Amended at
15 111. Reg.
,
effective
Section 728.143
Treatment Standards expressed as Waste
Concentrations
Table
B identifies the restricted wastes and
the
concentrations of their associated hazardous
constituents which must not be exceeded by the waste or
treatment residual
(not an extract of such waste or
treatment residual)
for the allowable land disposal of
such waste on residual.
Compliance with these
concentrations is required based upon arab samples,
unless otherwise noted in Table B.—Thc wastcwater and
nonwastewater treatment standards in Table B are based
analysis
of
grab
samp.Les
except
~Le
wastewat~.
treatment atandards that are based on analysis of
composite samples for wastes,
1009,
1010,
KO3G,
1038,
1040,
P039,
P071,
P089,
P094,
P097
and
U235.
b)
When w.astes with different treatment standards for a
constituent of concern are combined for purposes of
treatment,
the treatment residue must meet the lowest
treatment
standard
for
the
constituent
of
concern.
,
l.~
a)
121—420
272
g~
Notwithstanding
the
prohibitions
specified
in
subsection
(a)
and
Table
B, treatment and disposal
facilities
may
demonstrate
(and
certify
pursuant
to
Section 728.107(b) (5)) compliance with the treatment
standards
for organic constituents specified by a
footnote in Table
B, by satisfyin~the following
conditions:
fl
The treatment standards for the organic
constituents
were
established
based
on
incineration in units operated in accordance with
the technical requirements of 35 Ill. Adm. Code
724.Subpart
0
or
35
Ill.
Mm.
Code 725.Subpart OL
on based
on combustion in fuel substitution units
operating
in
accordance
with
applicable
technical
requirements
21
The treatment or disposal facility has used the
methods
referenced
in
subsection
(cl(1)
to
treat
the
organic
constituents;
and
~j
The
treatment
or
disposal
facility
has
been
unable
to
detect
the
organic
constituents
despite
using
its
best
good-faith
efforts
as
defined
by
applicable
standards.
Until
such
standards
are
developed,
the
treatment
or
disposal
facility
may
demonstrate
such
good-faith
efforts
by
achieving
detection
limits
for
the
regulated
for
the
regulated
organic
constituents
which
are
less
than
ten
times
the
treatment
standard
specified
in
this
Section.
Source:
Amended
at
15
Ill.
Reg.
,
effective
12 1—42
1
273
Section
728.Appendix
D
Organometallic
Lab
Packs
Hazardous
waste
with
the
following
EPA
waste
codes
may
be
placed
in
an
“organometallic”
or
“Appendix
D
lab
pack:”
POOl,
P002.
P003,
P004,
P005,
P006,
P007,
P008,
P009,
P013,
P014,
P015.
P016,
P017,
P018,
P020,
P022,
P023,
P024,
P025,
P0261
P027,
P028,
P031,
P034,
P036,
P037,
P038,
P039,
P040.
P041,
P042,
P043,
P044.
P045,
P047,
P048,
P049,
P050,
P051,
P054,
P056,
P057,
P058,
P059,
P060.
P062,
P063,
P064,
P065,
P066,
P067,
P068,
P069,
P070,
P071,
P072,
P073,
P074.
P075,
P077,
P081,
P082,
P084,
P0851
P087,
P088,
P089,
P092,
P093,
P094,
P095,
P096,
P097,
P098.
P099,
P101,
P102,
P103.
P104,
P105,
P108,
P109,
P110.
P112,
P113,
P114,
P115,
P116,
P118,
P119,
P120,
P122,
P123
UOOl,
UOO2,
UOO3,
13004,
U005,
13006,
U007,
13008,
13009,
13010,
U011,
13012,
UO14,
U015,
U0l6,
U0l7,
U018,
U0l9,
U020,
UO21,
UO22,
U023,
U024,
U025,
13026,
13027,
U028,
U029,
UO3O,
UO31,
U032,
UO33,
U034,
13035,
UO36,
13037.
13038,
U039,
U041,
U042,
U043,
U044,
U045,
U046,
13047,
U048,
U049,
U050,
UO51,
13052,
U053,
13055,
UO56,
U057,
U058.
13059,
U060,
U06l,
13062,
13063,
U064,
UO66,
13067,
13068,
U069,
13070,
13071,
U072,
U073,
U074,
13075,
U076,
U077,
UO78,
U079,
U080.
13081,
13082,
13083,
13084,
13085,
U086,
13087,
13088,
U089,
13090.
U091,
13092,
U093,
13094.
U095.
U096,
13097,
13098,
13099,
UlOl,
U102.
U103,
U1O5,
13106,
U107,
U108,
U1O9,
UllO,
UlIl,
U112,
Ul13,
Ul14,
13115,
Ul16,
U117,
Ui18,
13119,
13120,
Ul21.
U122,
13123,
U124,
13125,
Ul26,
Ul27,
Ul28,
U129,
Ul30,
13131,
13132,
U133,
13134,
U135,
13136,
U137,
U136,
Ul37,
13138,
Ul39,
13140,
13141,
13142,
Ul43,
13144.
13145,
13146,
U147,
Ul48,
13149,
U15O,
Ul52,
Ul54,
U153,
U154,
U155,
Ui56,
U157,
Ul58,
13159,
U160,
Ul61,
U162,
U164,
U165,
Ul66,
U167,
Ul68,
U169,
U170,
U171,
U172,
Ul73,
U174,
13176,
U177,
Ui78,
Ul79,
13180,
U181,
13182.
13183,
U184,
13185,
U186,
Ul87,
Ul88,
Ul89,
Ul90,
U19l,
13192,
13193,
U194,
U196,
13197,
U200,
U2O1,
U202,
U203,
U2O4,
U205,
U2O6,
U207,
U2O8,
U209.
13210,
13211,,
U213,
13214,
U2l5.
U2l6,
U217,
U2l8,
U2l9,
U220,
U22l,
U222,
U223,
13225,
U226,
U227,
U228,
13234,
U235,
U236,
13237,
U238,
U239,
U240.
U243,
U244,
13246,
U247,
U248.
13249,
13328.
13353,
13359
FOOl,
F002,
F003,
F004,
F005,
F006,
FOb,
FO2O,
F021,
F023,
F024,
F026,
FO27,
F028
1001,
1002,
1008,
K009,
1010,
1011,
1013,
K014,
1015,
1016,
1017,
1018,
1019,
1020.
1021.
1022,
1023,
K024.
1025,
K026,
1027,
K028,
1029,
1030,
1031,
K032.
1033,
1034,
1035,
1036,
1037,
1038,
K039,
1040,
1041,
K042,
1043,
1044.
1045,
K046,
K047,
1048,
1049,
1050,
K051,
1052.
1054,
1060,
K061,
1064,
1065.
1066,
1069,
1071,
K073,
1083,
1084,
1085,
1086,
1087,
1093,
1094.
K095.
1096.
1097,
KO98,
1099,
1101,
1102,
1103,
1104,
Kl05,
1111,
K1l2,
1113.
1114,
Kll5,
1116,
1117,
1118,
1123,
1124,
1125,
1126,
1136
DOOl,
D002,
DOO3,
D004,
D005,
DOO6,
D007,
DOO8,
DOlO,
DOll,
D012,
D013,
D014,
D0l5,
D016, D0i7
13032, Ul36,
U144,
13145. Ul46,
Ul63,
13214, U215,
13216, U217
12 1—422
274
BOARD
NOTE:
35
Ill.
Adm.
Code
729.301
and
729.312
include
additional
limitations
on
the
use
of
lab
packs.
Source:
Added at
15 Ill. Reg.
,
effective
Section 728.Appendix E
~ganic
Lab Packs
Hazardous wastes with the following EPA Hazardous Waste Code No.
may be ~1aced in an “organic” or “Appendix E”
lab pack:
POOl,
P002,
P003,
P004.
P005,
P006,
P007,
P008.
P009,
P013,
P014,
P015,
P016,
P017,
P018,
P020,
P022,
P023.
P025,
P024,
P026,
P027,
P028,
P031,
P034,
P036,
P037,
P038,
P039.
P040,
P041,
P042,
P043,
P044.
P045,
P046,
P047.
P048,
P049,
PO5O,
P051,
P054,
P057,
P058,
P059,
P060,
P062,
P063,
P064,
P064,
P065,
P066,
P067,
P068,
P069,
P070,
P071,
P072,
P073,
P074,
P075,
P077,
P081,
P082.
P084, PO85~
P087,
P088,
P089,
P092,
P093,
P094,
P095,
P096,
P097.
P098,
P099,
P101,
P102,
P103,
P104,
P105,
P108,
P109,
P110,
Pill,
P112,
P113,
P114,
P115,
P116.
P118,
P119,
P120,
P122,
P123
13001, UOO2,
U003,
13004,
13005, U006.
13007, U008. U009,
U010, UO11,
U012,
U014,
U015,
13016,
U017,
13018.,
U019,
13020,
U021,
U022,
13023,
U024,
U025,
U026,
U027,
U028,
U029,
13030,
U03l,
13033,
UO34,
U035.,
13036, U037,
U038, U039,
tJO4l,
13042,
13043,
U044,
U045,
U046,
U047,
13~Q48,U049,
13050,
U051,
UO52,
U053,
13055,
U056,
UO57,
UO58,
U059L
13060,
U061,
U062,
13063,
U064,
13066,
U067.
13068,
U069,
13070,13071,
13072, U073,
13074,
U075,
13076, U077, U078, UO79, U080,
UO81.,
13082,
U083,
U084.,
U085,
13086,
13087, U088,
UO89, UO9O,
U091,
13092,
13093,
13094,
U095,
U096,
U097,
13098,
U099,
UlOl,
U102,
U103,
0105,
U1O6.
13107,
U108.
U109,
13110,
Ulll.
U112,
Ul13,
U114,
U115,
13116,
U11~,
U118.
Ull9,
U120,
13121,
U122,
U123,
U124,
U125,
Ul26.
13127,
Ul28,
13129,
13130, U131, U132,
Ul33,
U135, U137,
Ul38,
13139,
13140, U141,
13142,
U143, U147, U148, U149, U150, U153, U154, U155,
U156, U157,
13158,
U159,
U160,
U161,
U162,
tJ163,
13164,
Ul65.
13166,
13167,
13168,
13169,
13170,
U171,
13172,
U173,
Ul74,
Ul76,
0177,
13178,
13179.
13180,
13181.
13182,
U183,
13184,
Ul85.
U186,
Ul87,
13188,
13189,
Ul90,
13191,
13192.
U193, Ul94,
U196,
U197,
U200, U2O1,
13202, U203.
U205,
U206,
U2O7,
U208,
U209,
U2l0,
U211,
13213,
U214,
0218,
13219,
U220,
13221,
13222,
13223, U225,
13226, U227,
13228, U234,
U235,
13236,
13237, U238,
12239,
U240, U243,
U244,
U246,
13247,
U248,
U249.
13328,
13353,
13359
FOOl,
F002,
F003, F004,
F005, FOb, F020,
FO21,
FO23,
FO24,
F026L
F027,
F028
~KO09,
1010,
1011,
1013,
K014,
1015,
1016,
1017,
1018,
101g.
1020.
1021,
1022,
1023,
1024,
1025,
1026,
1027,
K029,
1030,
1031,
iSQIZ~
1033,
1034,
1035,
K036,
1037,
1038,
1039,
1040,
1041,
1042,
1043,
1044,
1045,
K046,
1047,
1048,
1049.
1050,
K051,
1052,
1054,
K060,
1065,
1073,
1083,
K084,
1085,
1086,
1087.
1093,
1094,
1095.
1096,
1097,
1098,
1099,
1101.
1102,
1103,
1104,
K105,
KilL,
1112,
12 1—423
275
1113,
1114,
1115,
1116,
1117,
1118,
1123,
K124,
1125.
1126,
1136
DOO1, D0l2,
D0l3,
D0l4, D0l5,
D016,
DOll
BOARD
NOTE:
35
Ill.
Adm.
Code
729.301
and
729.312
include
additional
limitations
on
the
use
of
lab
packs.
Source:
Added at 15 Ill.
Reg.
,
effective
Section 728.Appendix F
Technologies to Achieve Deactivation of
Characteristics
The
treatment
standard
for
many
subcategories
of
DOOl,
D002
and
D003
wastes
as
well
as
for
1044,
1045
and
1047
wastes
is
listed
in
Section
728.142
simply
as
“Deactivation
to
remove
the
characteristics
of
ignitability,
corrosivity,
and
reactivity”.
USEPA
has
determined
that
many
technologies,
when
used
alone
on
in
combination,
can
achieve
this
standard.
The following
p~sents
a
partial
list
of
these
technologies,
utilizing
the
five
letter
technology
codes
established
in
Table
C.
Use
of
these
~pecific
technologies
is
not
mandatory
and
does
not
preclude
direct
reuse,
recovery
or
the
use
of
other
pretreatment
technologies
provided
deactivation
is
achieved and these
alternative
methods
are
not
performed
in
units
designated
as
land
disposal.
Waste
code/subcategory
Nonwastewaters
Wastewaters
DOOl
Ignitable
Liquids
based
on
35
RORGS
n.a.
Ill.
Adm.
Code
721.l21(a)(1)—-Low
WETOX
TOC
Nonwastewater
Subcateqory
INCIN
(containing
1
to
10
TOC)
CHOXD
BIODG
DOO1
Ignitable
Liquids
based
on
35
n.a.
WETOX
Ill.
Adin.
Code
721.121(a)
(1)——
RORGS
Ignitable
Wastewater
Subcategony
INCIN
(containing
1
TOC)
CHOXD
BIODG
D001
Compressed
Gases
based
on
35
RCGAS
n.a.
Ill.
Adm.
Code
721.121(a)
(3)
FSUBS
INCIN
ADGAS
fb.
INCIN
ADGAS
fb.
(CHOXD;
on
CHRED)
12 1—424
276
DOOl
Ignitable
R~actives
based
on
WTRRX
n.a.
35
Ill.
Adm.
Code
721.121(a)
(2)
CHOXD
CHRED
STABL
INCIN
DOOl
Ignitable
Oxidizers
based
on
CHRED
CHRED
35
Ill.
Mm.
Code
721.121(a)
(4)
INCIN
INCIN
D002
Acid
Subcategorv
based
on
35
RCORR
NEUTR
Ill.
Adm.
Code
721.122
(a)
(1)
with
NEUTR
INCIN
pH
less
than
or
e~a1
to
2
INCIN
DOO2
Alkaline
Subcategory
based
on
NEUTR
~EUTR
35
Ill.
Adm.
Code
721.122(a)
(1)
INCIN
INCIN
with
pH
greater
than
or
equal
to
12
.
5
D002
Other
Corrosives
based
on
35
CHOXD
CHOXD
Ill.
Adm.
Code
721.122(a)
(2)
CHRED
CHRED
INCIN
INCIN
STABL
D003
Water
Reactives
based
on
35
INCIN
n.a.
Ill.
Adm.
Code
72l.123(a)(2),
(3)
WTRRX
and
(4)
CHOXD
CHRED
D003
Reactive
Sulfides
based
on
35
CHOXD
CHOXD
Ill.
Adm.
Code
721.123
(a)
(5)
CHRED
CHRED
INCIN
BIODG
STABL
INCIN
DOO3
Explosives
based
on
35
Ill.
INCIN
INCIN
Adm.
Code
721.
123 (a)
(6),
(7)
and
CHOXD
CHOXD
CHRED
CHRED
BIODG
CARBN
D003
Other
Reactives
based
on
35
INCIN
INCIN
Ill.
Adm.
Code
721.
123 (a)
(1)
CHOXD
CHOXD
CHRED
CHRED
BIODG
CARBN
1044
Wastewater
treatment
sludges
CHOXD
CHOXD
from
the
manufacturing
and
CHRED
CHRED
processing
of
explosives
INCIN
BIODG
CARBN
INCIN
12 1—425
277
1045
Spent
carbon
from
the
CHOXD
CHOXD
treatment
of
wastewaters
containing
CHRED
CHRED
explosives
INCIN
BIODG
CARBN
INCIN
1047
Pink/red
water
from
TNT
CHOXD
CHOXD
operations
CHRED
CHRED
INCIN
BIODG
CARBN
INCIN
Note:”n.a.” stands for “not applicable”.
“fb.” stands for “followed by”.
Source:
Added at
15 Ill. Reg.
,
effective
121—426
278
Section
728.Appendix
G
Federal
Effective
Dates
The
following
are
the
effective
dates
for
the
USEPA
rules
in
40
CFR
268.
These
generally
became
effective
as
Illinois
rules
at
a
later
date.
Waste
Code
Waste
Cate~orv
Effective
date
California
list
Liquid
hazardous
wastes,
including
July
8.
1987
free
liquids
associated
with
solid
or
sludge,
containing
free
cyanides
at
concentrations
greater
than
or
equal
to
1,000
mg/i on certain
metals
on
compounds
of
these
metals
greater
than
or
equal
to
the
prohibition
levels
California
list
Liquid
(aqueous)
hazardous
wastes
having
a
pH
less
than
or
equal
to
2
July
8,
1987
California
list
Dilute
HOC
wastewaters,
defined
as
July
8,
1987
HOC—waste
mixtures
that
are
primarily
water
and
that
contain
greater
than
or
equal
to
1.000
mg/i
but
less
than
10,000
mg/l
California
list
Liquid
hazardous
waste
containing
PCBs
greater
than
or
equal
to
50
pPI~
July 8,
1987
California
list
California
list
California
list
DO01
DO02
DO03
Other liquid and non-liquid
hazardous wastes containing HOCs
in
total
concentration
greater
than
or
equal
to
1,000
ma
Soil
and
debris
HOCs
not
from
CERCLA/RCRA
corrective
actions
Soil
and
debris
HOCs
from
CERCLA/RCRA
corrective
actions
All
All
All
Nov.
8.
1988
July
8,
1989
Nov.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
DO04
Inorganic solid debris
May
8,
1992
DO04
Nonwastewater
May
8,
1992
12 1—427
279
DOO4
Wastewater
Aug.
8,
1990
D005
Inorganic solid debris
Nay 8,
1992
D005
All others
Aug.
8,
1990
D006
Inorganic solid debris
May 8.
1992
D006
All others
Aug.
8,
1990
DOO7
Inorganic solid debris
May 8.
1992
D007
All others
Aug.
8.
1990
DOO8
Inorganic solid debris
May 8.
1992
D008
Lead acid batteries
Nay 8,
1992
DOO8
All others
Aug.
8,
1990
D009
Inorganic solid debris
May 8,
1992
DOO9
High
mercury
nonwastewater
May
8,
1992
D009
Low
mercury
nonwastewater
May
8,
1992
DOO9
All
others
Aug.
8,
1990
DOlO
Inorganic
solid
debris
May
8,
1992
DO1O
All
others
Aug.
8,
1990
DOll
Inorganic
solid
debris
May
8,
1992
DOll
All
others
Aug.
8,
1990
D0l2
Aug.
8,
1990
D013
Aug.
8,
1990
DO14
Aug.
8,
1990
D0l5
~ug.
8,
1990
D016
Aug.
8,
1990
D017
Al.
Aug.
8,
1990
F001—FOO5
All,
except
in
next
listing
Nov.
8,
1986
121—428
280
FOOl—F005
F002 b
F005 c
FO 06
FO 06
FO 06
F007
F008
FO 09
FO10
FO1O
FOil
FO 12
FO19
FO20
FO2O
F021
FO21
F02 2
F022
FO 23
F023
Small
quantity
generators.
CERCLA/RCRA
corrective action,
initial generator’s solvent—water
mixtures,
solvent—containing
sludges
and
solids,
and
non
CERCLA/RCRA
corrective action soils
with less than
1 percent total
solvent constituents
Soil
and
debris
All
All
Wastewater
Nonwastewater
Nonwastewater
All
All
All
Soil
and
debris
All
others
All
All
All
Soil
and
debris
All
others
Soil and debris
All others
Soil
and
debris
All
others
Soil
and
debris
All
others
Nov.
8
Nov.
8..
Nov.
8,
Nov.
8.
1990
1990
1990
1990
1988
1989
198~
1989
1989
1991
1989
1989
1989
1990
_1990
1988
1990
1988
1990
1988
1990
1988
Nov._8._____
Nov._8,_____
~
F001—FOO5
Nov.
8,
1988
(cvanides)
Nov.
8,
Aug.
8.
Aug.
8,
Aug.
8,
Aug.
8.
July
8,
July
8,
July
8,
July
8,
June
8,
June
8.
July 8,
July
8,
Nr~v..
R.
12 1—429
281
F024
F024
(metals)
FO24
(dioxins/furans)
FO24
F025
FO26
F026
F027
FO27
F028
F028
F039
FO 39
KO 01
1001
(lead/onganics)
1001
1002
1003
KO 04
K005
d
1006
1007
d
1008
1009
KO09
Soil and debris
Nonwastewater
All
All others
All
Soil
and
debris
All
others
Soil and debris
All
others
Soil and debris
All others
Wastewater
Nonwastewater
Soil
and
debris
All
All
others
All
All
All
All
All
All
All
Soil and debris
All others
June
Aug.
Aua.
8,
1991
8,
1990
g~
1990
June 8.
Aug.
8,
£~
1989
1990
1990
1988
1990
1988
1990
1988
1990
1992
1990
1990
Nov.
Nov.
Nov.
Nov.
Nov.
Nov.
Aug.
May.
Aug.
Aua
-
8.
8
8
8
8
8
8
8
IL
Aug.
8,
1988
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
199Q
Aug.
8,
1990
Aug.
8.
1990
June 8,
1991
June
8,
1989
121—430
282
1010
__________________
1010
____________
1011
____________
1011
________________
1011
__________________
1013
_____________
KO 13
________________
1013
___________________
1014
Wastewater
K014
Nonwastewater
1014
Soil
and
debris
K015
Wastewater
K0l5
Nonwastewater
1016
Soil and debris
1016
All others
1017
All
1018
Soil
and
debris
1018
All others
1019
Soil
and
debris
KO19
All
others
1020
Soil
and
debris
1020
All
others
1021
e
All
1022
Wastewater
1022
Nonwastewater
1022
Soil and debris
Soil
and
debris
June
8,
1991
June
8,
1989
All
others
Wastewater
Nonwastewater
Aug.
8,
1990
June
8,
1989
June
8,
1991
Soil
and
debris
Aug.
8,
1990
Wastewater
Nonwastewater
June
8,
1989
June
8.
1991
Soil
and
debris
Aug.
8
June 8.
1990
1989
8,
1991
8,
1988
8,
1990
8,
1990
8,
1988
8,
1990
8,
1990
8,
1988
8,
1990
8,
1988
8,
1990
8.
1988
8,
1990
8,
1990
8,
1988
8.
1990
June
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Au
q•
12 1—431
283
1023
Soil and debris
June 8.
1991
K023
All others
June 8,
1989
K024
Soil
and debris
AUg.
8,
1990
1024
All others
aug.
8,
1988
1025
e
All
Aug.
8,
1990
1026
Aug.
8,
1990
1027
Soil and debris
June 8,
1991
KO27
All others
June 8,
1989
K028
Soil
and
debris
June
8,
1991
K028
(metals)
Nonwastewater
Aug.
8,
1990
K028
All others
June 8,
1989
K029
Wastewater
Aug.
8,
1990
1029
Nonwastewater
June
8,
1989
1029
Soil and debris
June 8,
1991
KO3O
Soil
and
debris
Aug.
8,
1990
1030
All others
Aug.
8.
1988
1031
Wastewater
Aug.
8,
1990
1031
Nonwastewater
May
8,
1992
1032
All
Aug.
8,
1990
1033
All
Aug.
8,
1990
K034
Aug.
8,
1990
K035
AU
Aug.
8,
1990
1036
e
All
Aug.
8,
1990
1037
Soil and debris
Aug.
8,
1990
1037
Wastewater
~kug.
2.
1990
037
All
others
Aug.
8,
1988
121—432
284
1038
1038
1039
KO 39
KO40
KO40
1041
1042
1043
1043
K044
1045
1046
K04 6
1047
1048
1048
1049
1049
KO50
K050
KO51
KO51
1052
1052
1060
e
Soil
and
debris
All
others
Soil
and
debris
All
others
Soil
and
debris
All others
All
All
Soil
and
debris
All others
All
All
Nonreactive
nonwastewater
All others
All
Wastewater
Nonwastewater
Wastewater
Nonwastewater
Wastewater
Nonwastewater
Wastewater
Nonwastewater
Wastewater
Nonwastewater
All
1991
1989
1991
1989
1991
1989
1990
8.
1990
8,
1991
1990
1990
1988
1990
1990
1990
1990
1990
1990
1990
1990
1990
1990
1990
1990
June
8,
June
8,
June 8,
June
8.
June
8,
June 8,
Aug.
8,
Aug.
June
June
Aug.
8
Aug.
8.
Aug.
8.
Aug.
8,
Aug.
8.
Aug.
8,
Nov.
8.
Aug.
8.
Nov.
8.
Aug.
8,
Nov.
8.
Nov.
8,
-
Aug._8,____
Aug.
8,
1990
121—433
285
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Aug.
Nay
Aug
Aug.
Aug.
Aug.
June
June
June
June
Aua
-
June
June
Aug.
Junc~
June
Aua.
L
8,
1990
8,
1988
8,
1988
8,
1990
8,
1990
8,
1990
8
1990
992
.a
1990
1
1990
I
199~
8,
1988
8.
1991
8,
1989
.~.
1991
1
1989
.a.
1990
.?~
1989
.~.
1991
.~.
1990
~
1989
IL.
1991
.L~
1990
1990
1988
1990
t—
~-
~-
8.
1061
Wastewaten
1061
Nonwastewaten
1062
All
1069
All
1073
~
1083
K084
Wastewater
1084
Nonwastewater
1085
~fl
KO86
1087
Soil
and
debris
K087
All others
KO93
Soil and debris
KO93
All others
1094
Soil
and
debris
1094
All
others
K095
Wastewater
1095
Noriwastewater
K095
Soil
and
debris
1096
Wastewater
1096
Nonwastewater
1096
Soil
and
debris
1097
1098
All
1099
All
1100
e
All
—
-
Aug.
8
Aug.
8.
Aug.
8
121—434
286
1101
Wastewater
K1O 1
Nonwastewater
1102
Wastewater
1102
Nonwastewater
1103
Soil
and
debris
Kl03
All
others
1104
Soil and debris
K104
All
others
K105
AU.
K?06
1106
1106
___________
1113
___________________
1113
All others
1114
Soil
and
debris
1114
All
others
1115
Soil
and
debris
1115
All
others
Kll6
Soil
and
debris
1116
All
others
POOl
P002
All
P003
All
P004
All
P005
All
P006
All
High
mercury
nonwastewater
Low
mercury
nonwastewater
All others
Soil
and
debris
Aug.
8.
1988
May 8.
1992
Aug.
8, 1988
Nay 8,
1992
Aug.
8.
1990
Aug.
8,
1988
Aug.
8,
1990
Aug.
8,
1988
Aug.
8,
1990
May 8,
1992’
May.
8.
1992
Aug.
8,
1990
June
8,
1991
June
8,
1989
June
8,
1989
June
8,
1991
June
8,
1989
June 8,
1991
June
8,
1989
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Auq~8,
1990
12 1—435
287
P007
Aug.
8,
1990
P008
All
Aug.
8,
1990
P009
A.U..
Aug.
8.
1990
POlO
Wastewater
Aug.
8,
1990
POlO
Nonwastewater
May
8.
1992
P011
Wastewater
Aug.
8.
1990
POll
Nonwastewater
Nay 8.
1992
P012
Wastewater
Aug.
8,
1990
P012
Nonwastewater
May
8,
1992
P013
Aug.
8,
1990
P014
AU
Aug.
8,
1990
P015
A.ll
Aug.
8,
1990
P016
Aug.
8,
1990
P017
~..U.
Aug.
8,
1990
P018
All
Aug.
8,
1990
P020
All
Aug.
8,
1990
P021
All
June
8,
1989
P022
Aug.
8,
1990
P023
~fl
Aug.
8,
1990
P024
Aug.
8,
1990
P026
All
Aug.
8.
1990
P027
AU
Aug.
8,
1990
P028
All
Aug.
8.
1990
P029
All
June 8,
1989
P030
All
June 8,
1989
P031
All
Aug.
8,
1990
121—436
288
P033
AU
Aug.
8, 1990
P034
All
Aug.
8,199.Q
P036
Wastewater
Aug.
8,
1990
P036
Nonwastewater
May
8.
1992
P037
All
Aug.
8,
1990
P038
Wastewater
Aug.
8,
1990
P038
Nonwastewater
Nay
8,
1992
P039
Soil
and
debris
June
8,
1991
P039
All
others
June
8.
1989
P040
Soil
and
debris
June
8,
1991
P040
All
others
June
8,
1989
P041
Soil
and
debris
June
8,
1991
P041
All
others
June
8,
1989
P042
AU.
Aug.
8,
1990
P043
Soil
and
debris
June
8,
1991
P043
All
others
June
8,
1989
P044
Soil
and
debris
June
8,
1991
P044
All
others
June
8,
1989
P045
AU
Aug.
8,
1990
P046
All
Aug.
8,
1990
P047
Aug.
~.
1990
P048
AU
~Aug.
8,
1990
All
~pg.
8
•
1990
P050
All
Aug.
8,
1990
P051
AU
Aug.
~
1990
P054
Aug.
8,
1990
121—437
289
P071
P071
P072
P073
P074
P075
P076
P077
P078
High
mercury
nonwastewater
Low
mercury
nonwastewater
All
others
All
All
All
All
All
Soil and debris
All others
All
All
P056
P057
P058
P059
P060
P062
P062
P063
P064
P065
P065
P065
P066
P067
P068
P069
P070
Aug.
8,
1990
Aug.
8.
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8.
1990
June 8,
1991
June
8,
1989
June
8,
1989
Aug.
8,
1990
May
8,
1992
May 8,
1992
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
June
8,
1991
June
8,
1989
Aug.
8.
1990
Aug.
8, 199~
June
8,
1989
Aug.
8,
1990
Aug.
8,
1990
~g~~990
Aug.
8,
1990
All
All
All
All
All
Soil
and
debris
All others
All
All
All
All
All
All
All
121—438
290
P081
P082
P084
P085
P085
P087
P088
P089
P089
P092
P092
P092
P093
P093
P094
P094
P095
P095
P096
P097
P097
P098
P099
(silver)
P099
(cyanides)
P099
jçy~de~/~Jlver
Soil and debris
All others
All
All
Soil
and
debris
All
others
High
mercury
nonwastewater
Low mercury nonwastewater
All
others
Soil
and
debris
All
others
Soil
and
debris
All
others
Soil
and
debris
All
others
All
Soil
and
debris
All
others
All
Wastewater
Wastewater
Nonwastewater
Aug.
8.
1990
Aug.
8,
1990
Aug.
8.
1990
June
8,
1991
June 8,
1989
May 8,
1992
Aug.
8.
1990
June
8,
1991
June 8,
1989
May
8,
1992
May
8,
1992
Aug.
8,
1990
Nay 8,
1992
Aug.
8.
1990
June
8.
1989
May
8,
1992
Aug.
8,
1990
Aug.
8,
1990
June
8,
1991
June
8,
1989
Aug.
8,
1990
June
8,
1989
June
8,
1989
All
All
All
12 1—439
291
P101
AU
Aug.
8,
1990
P102
AU
Aug.
8,
1990
P103
AU
Aug.
8,
1990
P104
(silver)
Wastewater
Aug.
8,
1990
P104
(cyanides)
Wastewater
June
8,
1989
‘P104
Nonwastewater
June
8,
1989
(cyanides/silver
P105
All
Aug.
8,
1990
P106
AU
June
8,
1989
P108
Soil and debris
Nay 8,
1992
P108
All
others
Aug.
8,
1990
P109
Soil
and
debris
June
8,
1991
P109
All
others
June
8,
1989
P110
AU
Aug.
8,
1990
P111
Soil
and
debris
June
8,
1991
P111
All
others
June
8,
1989
P112
AU
Aug.
8,
1990
P113
AU
Aug.
8,
1990
P114
AU
Aug.
8,
1990
P115
AU
Aug.
8,
1990
P116
Soil and debris
Nay 8,
1992
P116
All
others
Aug.
8,
1990
P118
Soil and debris
May 8,
1992
P118
All
others
Aug.
8,
1990
P119
AU
Aug.
8,
1990
P120
All
Aug.
8.
1990
12 1—440
292
P121
All
June
8,
1989
P122
All
Aug.
8,
1990
P123
All
Aug.
8,
1990
UOO1
AU
Aug.
8. 1990
13002
All
Aug.
8,
1990
U003
Soil
and
debris
Nay
8,
1992
U003
All
others
Aug.
8,
1990
UOO4
All
Aug.
8,
1990
UOO5
AU
Aug.
8,
19~0
U006
Soil
and
debris
May
8,
1992
13006
All,
others
Aug.
8,
1990
UOO7
Soil
and
debris
May
8.
1992
UOO7
All
others
Aug.
8,
1990
UOO8
AU
Aug.
8,
1990
13009
AU
Aug.
8,
1990
13010
Soil
and
debris
May
8,
1992
13010
All
others
Aug.
8,
1990
UOll
Soil
and
debris
~jay
8,
1992
13011
All
others
Aug.
8,
1990
13012
All
Aug.
8.
1990
U014
Soil
and
debris
May
8,
1992
13014
All
others
________
13015
Soil
and
debris
May
8,
1992
13015
All
others
Aug.
8,
1990
13016
AU
Aug.
8,
1990
13017
Soil
and
debris
May
8,
1992
12 1—44 1
293
UO17
13018
U019
13020
13020
13021
13021
U0 22
13023
13024
13025
UO2 6
13026
U027
U02 8
U028
U029
U0 30
U031
U0 32
U033
U0 33
U0 34
U034
U035
13035
All others
All
All
Soil and debris
All others
Soil and debris
All others
All
All
All
All
Soil and debris
All
others
All
Soil
and
debris
All
others
All
All
All
All
Soil
and
debris
All others
Soil and debris
All others
Soil and debris
All
others
Aug.
8,
1990
Aug.
8, 1990
Aug.
8,
1990
May 8,
1992
Aug.
8,
1990
Nay 8,
1992
Aug.
8.
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
May
8,
1992
Aug.
8,
1990
Aug.
8.
1990
June
8,
1991
June 8,
1989
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
May 8.
1992
Aug.
8,
1990
May 8,
1992
Aug.
8,
1990
May 8,
1992
Aug.
8,
1990
121—442
294
13036
13037
U038
U038
13039
UO4 1
UO4 1
UO42
13042
U043
13044
13045
U046
13046
U047
UO48
U0 49
U049
U050
U051
U052
13053
13055
UO56
U057
U058
All
All
Soil
and
debris
All others
All
Soil and debris
All others
Soil
and
debris
All
others
All
All
All
Soil
and
debris
All
others
All
All
Soil
and
debris
All
others
All
All
All
All
All
All
All
Soil
and
debris
Aug.
8,
1990
Aug.
8,
1990
May 8,
1992
Aug.
8,
1990
Aug.
8.
1990
May 8,
1992
Aug.
8.
1990
May
8.
1992
Aug.
8,
1990
Aug.
8.
1990
Aug.
8,
1990
Aug.
8,
1990
Nay
8,
1992
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
May
8,
1992
Aug.
8.
1990
Aug.
8,
1990
Aug.
8.
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8,
1990
Aug.
8.
1990
June
8,
1992
121
=
443
295
U058
All
others
June
8,
1989
U059
Soil
and
debris
Nay
8,
1992
13059
All others
Aug.
8,
1990
13060
Soil
and
debris
Nay
8.
1992
13060
All others
Aug.
8,
1990
13061
Soil and debris
Nay 8,
1992
13061
All others
Aug.
8,
1990
13062
Soil and debris
May 8,
1992
13062
All others
Aug.
8.
1990
11063
All
Aug.
8,
1990
13064
AU..
Aug.
8.
1990
13066
AU
Aug.
8,
1990
13067
AU
Aug.
8,
1990
13068
All
Aug.
8,
1990
U069
Soil
and
debris
June
8,
1991
13069
All others
June 8,
1989
13070
AU
Aug.
8,
1990
U07l
All
Aug.
8,
1990
U072
AU
Aug.
8,
1990
UO73
Soil and debris
May
8,
1992
U073
All others
Aug.
8,
1990
UO74
Soil and debris
May 8,
1992
UO74
All
others
Aug.
8,
1990
U075
All
Aug.
8,
1990
13076
AU
Aug.
8,
1990
13077
AU
Aug.
8,
1990
121—444
296
U078
AU
Aug.
8,
1990
UQ19.
AU
Aug~8,
1990
U080
AU
Aug.
8,
1990
13081
AU
Aug.
8,
1990
13082
AU
Aug.
8.,
1990
UO83
AU
Aug.
8.
1990
U084
AU
Aug.
8,
1990
13085
AU
Aug.
8,
1990
U086
All
Aug.
8,
1990
13087
Soil and debris
June
8,
1991
UO87
All
others
June
8,
1989
13088
Soil and debris
June
8.
1991
U088
All others
June 8,
1989
U089
AU
Aug.
8,
1990
13090
All
Aug.
8,
1990
U091
Soil
and
Debris
May
8,
1992
13091
All
others
Aug.
8,
1990
13092
Soil and debris
May 8.
1992
U092
All
others
Aug.
8,
1990
U093
Soil
and
debris
MaY
8,
1992
UO93
All others
Aug.
8,
1990
____
AU
Aug.
8,
1990
U095
Soil and debris
May
8,
1992
13095
All others
Aug.
8,
1990
UO96
All
_________
U097
Soil
and
debris
May
8,
1992
121—445
297
U097
All
others
Aug.
8,
1990
13098
All
Aug.
8,
1990
13099
AJJ..
Aug.
8,
1990
UlOl
All
Aug.
8,
1990
13102
Soil and debris
June
8,
1991
U102
All others
June
8.
1989
11103
AU
Aug.
8,
1990
11105
All
Aug.
8.
1990
13106
AU
Aug.
8,
1990
13107
Soil
and
debris
June
8,
1991
13107
All others
June
8,
1989
13108
AU
AUg.
8,
1990
U109
All
Aug.
8,
1990
13110
Soil and debris
Nay 8,
1992
UllO
All
others
Aug.
8,
1990
Ulll
AU
AIIQ.
8,
1990
U112
AU
Aug.
8,
1990
U1l3
AU
Aug.
8,
1990
Ul14
Soil
and
debris
May
8,
1992
U1l4
All
others
Aug.
8,
1990
13115
AU
Aug.
8,
1990
Ul16
Soil
and
debris
May
8,
1992
13116
All others
Aug.
8,
1990
U117
AU
Aug.
8,
1990
U118
All
Aug.
8,
1990
U119
Soil and debris
May 8,
1992
12 1—446
298
U119
All
others
Aug.
8,
1990
13120
Aug.
8,
1990
13121
All
Aug.
8,
1990
Ul22
AU
~..ug.8.
1990
U123
All
Aug.
8.
1990
U124
AU
Aug.
8.
1990
Ul25
All
Aug.
8,
1990
13126
AU
Aug.
8,
1990
13127
AU
Aug.
8,
1990
U128
AU
Aug.
8,
1990
U129
AU
Aug.
8.
1990
U130
Soil
and
debris
May
8,
1992
U13O
All others
Aug.
8,
1990
13131
All
Aug.
8,
1990
Ul32
Soil
and
debris
Nay
8,
1992
13132
All others
Aug.
8,
1990
Ul33
AU
Aug.
8,
1990
13134
All
Aug.
8,
1990
13135
AU
Aug.
8,
1990
U136
Wastewater
Aug.
8,
1990
____
Nonwastewater
May
8,
1992
13137
All
Apg.
8,
1990
Ul38
AU
Aug.
8,
1990
U140
AU
Aug.
8,
1990
Ul4l
AU
Aug.
8,
1990
U142
AU
Aug.
8,
1990
121—447
299
U143
Soil
and
debris
May
8,
1992
U143
All others
Aug.
8.
1990
11144
AU
Aug.
8,
1990
13145
AU
Aug.
8,
1990
U146
All
Aug.
8,
1990
13147
AU
Aug.
8,
1990
U148
Soil and debris
May 8, 1992
13148
All others
Aug.
8,
1990
13149
Soil and debris
May 8,
1992
13149
All
others
Aug.
8,
1990
U150
Soil and debris
May 8,
1992
13150
All
others
Aug.
8,
1990
13151
High mercury nonwastewater
May 8.
1992
Ul51
Low
mercury
nonwastewater
May
8,
1992
UlSl
Soil
and
debris
May
8.
1992
11151
All
others
Aug.
8,
1990
13152
AU
Aug.
8,
1990
U153
Soil
and
debris
May
8.
1992
13153
All others
Aug.
8,
1990
Ul54
All
Aug.
8,
1990
13155
AU
Aug.
8.
1990
13156
Soil and debris
May 8,
1992
U156
All
others
Aug.
8.
1990
13157
AU
Aug.
8,
1990
U158
All
Aug.
8,
1990
13159
AU
Aug.
8,
1990
121—448
300
11160
AU
Aug.
8,
1990
U161
All
Aug.
8,
1990
13162
All
Aug.
8,
1990
U163
Soil
and
debris
May
8,
1992
13163
ZIJJ others
Aug.
8,
1990
13164
Soil
and
debris
May
8,
1992
Ul64
All others
Aug.
8,
1990
13165
All
___________
13166
All
Aug.
8,
1990
13167
Soil and debris
May 8,
1992
U167
All
others
Aug.
8.
1990
U168
Soil
and
debris
May
8.
1992
13168
All
others
Aug.
8,
1990
Ui~
All
Aug.
8.
1990
13170
AU
Aug.
8,
1990
13171
Soil
and
debris
Nay
8,
1992
13171
All others
Aug.
8,
1990
U172
AU
Aug.
8,
1990
13173
Soil
and
debris
May
8,
1992
Ul73
All
others
Aug.
8,
1990
U12A
AU
Aug.
8,
1990
U176
Soil
and
debris
May
8,
1992
U176
All
others
Aug.
8,
1990
13177
Soil and debris
May 8,
1992
Ul77
All
others
Aug.
8,
1990
Ul78
Soil and debris
May 8,
1992
121—449
301
13178
All others
Aug.
8,
1990
13179
All
Aug.
8,
1990
U180
All
Aug.
8,
1990
13181
AU
Aug.
8,
1990
13182
All
Aug.
8,
1990
13183
All
Aug.
8,
1990
13184
Soil
and
debris
May
8,
1992
13184
All
others
Aug.
8,
1990
U185
AU
Aug.
8,
1990
13186
AU
Aug.
8,
1990
U187
AU
Aug.
8,
1990
Ul88
All
Aug.
8,
1990
11189
AU
Aug.
8,
1990
13190
Soil and debris
June 8,
1991
13190
All others
June 8,
1989
Ul91
Soil
and
debris
Nay
8,
1992
U19l
All others
Aug.
8,
1990
U192
All
Aug.
8.
1990
U193
Soil and debris
May 8,
1992
13193
All others
Aug.
8.
1990
Ul94
Soil and debris
May 8,
1992
Ul94
All others
Aug.
8,
1990
U196
AU
Aug.
8,
1990
U197
AU
Aug.
8,
1990
U200
Soil and debris
May 8,
1992
U200
All
others
Aug.
8,
1990
121—450
302
U201
AU
Aug.
8,
1990
U202
Soil
and
debris
May
8.
1992
11202
All
others
Aug.
8.
1990
13203
AU
Aug.
8,
1990
U204
AU
Aug.
8.
1990
13205
AU
Aug.
8,
1990
13206
Soil and debris
Nay 8,
1992
U2O6
All others
Aug.
8.
1990
13207
AU
Aug.
8.
199~O
13208
All
Aug.
8,
1990
13209
All
Aug.
8.
1990
U210
AU
Aug.
8,
1990
13211
AU
Aug.
8.
1990
13213
All
hug.
8,
1990
U214
AU
Aug.
8,
1990
U2l5
AU
Aug.
8.
1990
U216
All
Aug.
8,
1990
____
AU
Aug.
8,
1990
U218
Soil and debris
MaY 8,
1992
13218
All
others
Aug.
8,
1990
U219
Soil
and
debris
May
8,
1992
U219
All
others
Aug.
8,
1990
13220
AU
Aug.
8,
1990
13221
Soil
and
debris
June
8,
1991
U22l
All
others
June
8,
1989
U222
Soil
and
debris
May
8,
1992
12
1—45
1
303
U222
All
others
Aug.
8,
1990
13223
Soil and debris
June 8,
1991
13223
All
others
June
8,
1989
11225
AU
Aug.
8,
1990
U226
AU
Aug.
8,
1990
13227
All
Aug.
8,
1990
13228
All
Aug.
8,
1990
13234
Soil and debris
May 8,
1992
U234
All
others
Aug.
8,
1990
U235
Soil and debris
June 8,
1991
U235
All others
June 8,
1989
U236
Soil and debris
May 8,
1992
13236
All others
Aug.
8,
1990
U237
Soil and debris
May 8,
1992
13237
All others
Aug.
8,
1990
U238
Soil and debris
May 8,
1992
13238
All
others
Aug.
8,
1990
13239
AU
Aug.
8,
1990
U240
Soil and debris
May 8,
1992
13240
All others
Aug.
8,
1990
13243
AU
Aug.
8,
1990
13244
Soil and debris
M~~y
8,
1992
U244
All others
Aug.
8,
1990
13246
AU
Aug.
8,
1990
13247
AU
Aug.
8,
1990
13248
AU
Aug.
8,
1990
121—452
304
13249
AU
Aug.
8,
1990
a
This table does not include mixed radioactive wastes
(from
the
First~,
Second,
and
Third
Third
rules)
which
are
receiving
a
national
capacity
variance
until
May
8,
1992
for
all
applicable
treatment
technologies.
Standards
are
being
promulgated
for
l,1,2-trichloroethane
and
2—
nitropnopane
for
wastewaters
and
nonwastewaters.
C
Standards
are
being
pnomulgated
for
benzene
and
2—ethoxyethanol
for
wastewaters
and
nonwastewaters.
ci
Treatment
standards
for
nonwastewaters
disposed
of
after
June
8,
1989.
were
promulgated
June
8,
1989.
Treatment
standards
for
nonwastewaters
disposed
of
after
August
17,
1988,
were
promulgated
May
2.
1989.
BOARD
NOTE:
This
table
is
provided
for
the
convenience
of
the
reader.
Source:
Added
at
15
Ill.
Reg.
,
effective
12 1—453
305
Section 728.Appendix H
National Capacity LDR Variances for UIC
Wastes
Waste
Code
Waste
Category
Effective
date
FOOl-FOO5
All
spent
FOO1—FOO5
solvent
August
8,
containing less than
1 percent
1990.
total FOO1-FOO5 solvent
constituents
California
list
Liquid
hazardous
wastes,
including
August
8,
free liquids associated with any
1990
solid or sludge, containing free
cyanides at concentrations greater
than
or
equal
to 1,000 mg/l,
or
containing
certain
metals
or
compounds
of
these
metals
greater
than
or
equal
to
the
prohibition
levels
California
list
Liquid
hazardous
waste
having
a
pH
August
8.
less
than
or
equal
to
2
1990
California
list
Hazardous
wastes
containing
HOC5
in
August
8,
total
concentrations
less
than
1990
10,000
mg/i
but
greater
than
or
equal
to
1,000
m~/l
DOO2
b
All
MaY
8,
1992
DOO3
(cyanides)
AU
Nay
8.
1992
DOO3
(sulfides)
AU
~4ay
8.
1992
DOO3
AU
Nay
8,
1992
(explosives,
reactives)
D007
All
May 8,
1992
DO09
High Mercury Nonwastewater
May 8,
1992
DOO9
Low Mercury Nonwastewater
May 8,
1992
FOil
AU
June 8.
1991
F039
Wastewater
May 8,
1992
1009
Wastewater
June 8,
1991
1011
Nonwastewater
June
8.
1991
121—454
306
1011
Wastewater
Nay 8,
1992
1013
Nonwastewater
June
8,
1991
1013
Wastewater
May
8,
1992
KO14
All
MaY
8,
1992
1016
(duiutel
All
June
8,
1991
1048
AU
August
8,
1990
1049
AU
August
8,
1990
1050
AU
August
8,
1990
KO51
All
August
8.
1990
1052
AU
August
8,
1990
1062
AU
August
8,
1990
1071
All
August
8,
1990
1104
AU
August
8,
1990
Wastes
that
are
deep
well
disposed
on—site
receive
a
six—month
variance,
with
restrictions
effective
in
November
1990.
Deepwell
iniected
D002
liquids
with
a
pH
less
than
2
must
meet
the
California
List
treatment
standards
on
Aucust
8,
1990.
BOARD NOTE:
This table is provided for the convenience of the
reader.
Source:
Added
at
15
Ill.
Reg.
,
effective
12 1—455
307
Section 728.Table A Constituent Concentrations
in Waste Extract
(CCWE)
Concentration
(in mg/L)
FOOl
-
F005
Spent
Solvents
Wastewaters
All other
containing
spent
spent
solve-nt
solvents
wastes
Acetone
0.05
0.59
n-Butyl alcohol
5.0
5.0
Carbon disulfide
1.05
4.81
Carbon tetrachioride
0.05
0.96
Chlorobenzene
0.15
0.05
Cresols
(and
cr~csylic
acid)
2.82
0.75
Cyclohexanone
0.125
0.75
1,2 Dichlorobenzenc
0.65
0.125
Ethyl acetate
0.05
0.75
Ethy-lbenzene
0.05
0.053
Ethyl ether
0.05
0.75
Isobutanol
5.0
5.0
Methanol
0.25
0.75
Methylene chloride
0.20
0.96
Methyl ethyl ketone
0.05
0.75
Methyl isobutyl ketone
0.05
0.33
N-itrobenz-e-n-e
0.66
0.125
Pyridine
1.12
0.33
Tetrachloro~thy1ene
0.079
0.05
T-oluenc
1.12
0.33
1,1,1 Trichlorocthane
1.05
0.41
1,1,2 Trichloro-l, 2,2 trifluoroethanc
1.05
0.06
Trichloroethylenc
0.062
0.091
Trichlorofluoromethane
0.05
0.06
Xylene
0.05
0.15
F006 nonwastewaters
(see also Table
B)
Concentration
(in
rng/L)
0.066
Cathriium
Chromium
(Total)
5.2
Lead
0.51
Nickel
0.32
Silver
0.072
Cyanides
(Total)
fleserved
121—456
308
-F020-
-
F023 anu F026
F028
Con-centration
B-ioxin Containing Wastet~--
(Maximum)
HXCDD
-
All Hexachlorodibcnzo p dioxins
1 ppb
-H-x-CDF
All Hexachlorodibenzofurans
I ppb
PeCDD
All Pentachlorodibenzo-p-dioxins
1 ppb
PeCDF
All Pentachlorodibenzofurans
1 ppb
PGDD
-
All Tctrachlorodibenzo-p dioxins
1 ppb
TCDF
-
All Tetrachlorodibenzofurans
1 ppb
2,4,5 Trichlorophenol
0.05 ppm
2,4,6-Trichlorophenol
0.05 ppm
2
,
3,4,C-Tetrachlorophenol
0.10 ppm
Pentachlorophenol
0.01 ppm
1001
nonwastewatcrs
(see also Table B)
Concentration
(in mg/L)
0.51
Lead
1~O22 nonwastewaters
(see also Table B)
Concentration
(in mg/L)
chromium
~To?~i~
5.2
Nickel
0.32
1046
nonwastcwaters
(Nonreactive Cubcategory)
Concentration
-(in
mg/L)-
0.18
Lead
1048,
1040,
1050,
1051
and 1052
nonwastewaters
(see also Table
Cone-efitration
(in mg/L)
~rse-nic
0.004
Chromium (Total)
1.7
Nickel
0.04-8
Selenium
0.025
~6±—nonwastcwaters
-(Low Zinc Subcategory-less than 15
tot-u-I
mc)
Concentration
(in mg/L)
0.14
Cadmium
—
Chromium (Tota’)
5.2
Lead
0.24
Nickel
—
0.32-
121—457
309
1061
nonwastewater3
(High Zinc Subcategory
15
or greater total
zinc)
effecti;~euntil 8/8/00
Concentration
(in mg/L)
Cadmium
-
0.14
Chromium
(Total)
5.2
Lead
0.24
Nickel
0.32
1062
nonwastewaters
Concentration
(in mg/L)
Chromium
(Total)
0.094
Lead
0.37
1071
nonwastewaters
Concentration
(in
ing/L)
Mercury
0.025
1086
nonwastewaters (Solvent Washes Subcategory)
see
also Table
Concentration
(in mg/L)
B
Chromium
(Total)
0.004
Lead
0.37
1087
nonwastcwaters
(see also Table
B)
Concentration
(in mg/L)
Lead
0.51
1101
and 1102
nonwastewaters
(Low Arsenic Subcategory less than
1
Total Arsenic)
(see also Table B)
Concentration
(in mg/L)
Cadmium
0.066—
Chromium
(Total)
5.2
Lead
0.51
Nickel
0.32
D,
F and K Listed Wastes
CAS
No.
for
Concentration
(mg/i)
Wast See
Regulated
Regulated
Non-
e
Also
Hazardous Constituent
Hazardous Wastewateiv~stewaters
Code
Constitue
nt
D004 Table
Arsenic
7440—38—
5.0
#
121—458
310
D005 Table
Barium
B
D006 Table
Cadmium
B
D007 Table
Chromium (Total)
B
D008 Table
Lead
B
7440—39—
3
7440—43—
9
7440—47—
32
NA
D009
(Low Mercury Subcategory--less than 260 mg/kg Mercurvj.
Tables Mercury
7439—97-
NA
0.20
B&D
6
DOlO Table
Selenium
B
DOll Table
Silver
B
7782—49—
2
________
NA
100.
1.0
5.0
5.0
7439—92—
1
F001—F005 spent solvents
Tables Acetone
B&D
n-Butyl alcohol
Carbon disulfide
Carbon tetrachioride
_______
7440—22—
4
________
67—64—1
__________________
71—36—3
___________________
75—15—0
______________________
56—23—5
Chlorobenzene
108—90-7
Cresols
(and cresylic
acid)
-
Cyclohexanone
108—94—1
l,2—Dichlorobenzene
95-50-1
Ethyl acetate
141-78-6
Ethylbenzene
100-41-4
Ethyl ether
60-29-7
Isobutanol
78-83-1
Methanol
67—56—1
Methylene chloride
75—9—2
Methyl ethyl ketone
78—93-3
Methyl isobutyl ketone 108—10—1
Nitrobenzene
98-95-3
Pyridine
110—86—1
Tetrachioroethylene
127-18-4
Toluene
108-88—3
1,1, l—Trichloroethane
71—55—6
1,1,2—Trichloro—l,2,2— 76—13—1
5.7
5.0
O
.
59
5.0
4.81
0.96
O
.
05
0.75
0.75
0.125
0.75
0. 053
0.75
5.0
0.75
0.9
0.75
0.33
0.125
0.33
0.05
0.33
0.41
0.96
0.091
0.96
0.15
0.25
5.0
1
.
05
0.05
0.15
2.82
0.125
0.65
0.05
0.05
0.05
5.0
0.25
0.20
0.05
0.05
0.66
1. 12
0.079
1.12
1.05
1.05
0. 062
0.05
0.05
trifluoroethane
Trichioroethylene
19-01-6
Trichiorofluoroniethane 75-69-4
Xylene
12 1—459
311
Cadmium
Chromium
(Total)
F006 Table
B
F007 Table
B
F008 Table
B
F009 Table
B
FOil Table
B
Lead
Nickel
Silver
Cadmium
Chromium (Total)
Lead
Nickel
Silver
Cadmium
Chromium
(Total)
Lead
Nickel
Silver
Cadmium
Chromium
(Total)
Lead
Nickel
Silver
Cadmium
Chromium
(Total)
744 0—4 3—
9
7440—47—
32
7439—92—
1
744 0—02—
0
744 0—2 2—
4
7440—43—
9
7440—47—
32
74 39—92—
1
7440—02—
0
7440—22—
4
7440—43—
9
7440—47—
32
7439—92—
1
7440—02—
0
7440—22—
4
7440—43—
9
7440—47—
32
7439—92—
1
7440—02—
0
7440—22—
4
7440—43—
9
7440—47—
32
7439—92
—
1
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.066
5.2
0.51
0.32
0.072
0.066
5.2
0.51
0.32
0.072
0.066
5.2
0.51
0.32
0.072
0.066
5.2
0.51
0.32
0. 072
0.066
5.2
0.51
Lead
121—460
Nickel
7440—02—
NA
0.32
0
Silver
7440—22—
NA
0.072
4
F012 Table
Cadmium
7440—43—
NA
0.066
Chromium (Total)
7440-47-
~tA
5.2
32
Lead
7439—92—
NA
0.51
1
Nickel
7440—02—
NA
0.32
0
Silver
7440—22—
NA
0.072
4
F019 Table
Chromium
(Total)
7440-47—
NA
0.072
F020—FO23 and F026—F028 dioxin—containing wastes
*
HxCDD-A11 Hexachloro-
1.
p~b
1.
ppb
dibenzo-p-dioxins
HxCDF—A11 Hexachloro-
1.
ppb
1.
ppb
dibenzofurans
PeCDD-All Pentachloro-
1.
ppb
1.
ppb
dibenzo-p-dioxins
PeCDF-All Pentachloro-
1.
i~b
1.
ppb
dibenzofurans
TCDD-All Tetrachloro-
1.
PPb
1~. ppb
dibenzo-p-dioxins
TCDF-All Tetrachloro-
1.
PPb
1.
ppb
dibenzofurans
2,4,5—Trichlorophenol
95—95—
0.05
0.05
P1218
P1238
2,4,6—Trichiorophenol
88—06—
0.05
0.05
a
P1238
12238
2,3,4,6—Tetrachloro—
58—90—
0.05
0.05
phenol
a
1212111
121238
Pentachlorophenol
87—86—
0.05
0.05
1212111
PP-lU
F024 Table
Chromium
(Total)
7440—47—
NA
0.073
Lead
7439—92—
NA
0.021
1
Nickel
7440—02—
NA
0.088
0
F039 Table
Antimony
7440—36—
flA
0.23
Q
Arsenic
7440—38—
flA
2
12 1—46 1
313
Barium
7440—39—
NA
52.
3
Cadmium
7440—43—
NA
0.066
9
Chromium
(Total)
7440-47-
NA
5.2
32
Lead
7439—92—
NA
0.51
1
Mercury
7439—97-
flA
0.025
6
Nickel
7440—02—
NA
0.32
0
Selenium
7782—49—
2
Silver
7440—22—
NA
0.072
4
1001
Table
Lead
7439—92—
NA
0.51
1002
Table
Chromium (Total)
7440—47—
NA
0.094
Lead
7439—92—
NA
0.37
1
1003
Table
Chromium (Total)
7440-47—
NA
0.094
Lead
7439—92—
NA
0.37
1
1004
Table
Chromium (Total)
7440—47—
NA
0.094
Lead
7439—92—
NA
0.37
1
1005
Table
Chromium (Total)
7440-47—
NA
0.094
Ia
Lead
7439—92—
NA
0.37
1
1006
(anhydrous)
Table
Chromium
(Total)
7440—47-
NA
0.094
2?.
Lead
7439—92—
NA
0.37
1
K006
(hydrated)
Table
Chromium (Total)
7440-47-
flA
I?.
1007
Table
Chromium
(Total)
7440—47—
NA
0.094
Ia
121—462
314
Lead
7439—92—
NA
0.37
1
K008 Table
Chromium (Total)
7440-47-
NA
0.094
1?.
Lead
7439—92—
NA
0.37
1
1015
Table
Chromium (Total)
7440-47-
I?.
Lead
7439—92—
NA
0.2
1
1021
Table
Antimony
7440—36—
0.23
#
1022
Table
Chromium
(Total)
7440—47—
NA
5.2
P
2?.
Nickel
7440—02—
NA
0.32
2
K02~ Table
Chromium
(Total)
7440—47—
NA
0.073
P
2?.
Lead
7439—92—
NA
0.021
1
Nickel
7440—02—
NA
0.088
2
1031
Table
Arsenic
7440—38—
___
a
1046
Table
Lead
7439—92—
NA
0.18
P
i
K048 Table
Chromium (Total)
7440—47—
1.7
P
1?.
Nickel
7440—02—
fl~
0.20
2
Kpj~Table
Chromium
(Total)
7440-47-
NA
1.7
P
1?.
Nickel
7440—02—
NA
0.20
2
1050
Table
Chromium (Total)
7440—47-
P
Ia
Nickel
7440—02—
NA
0.20
2
K051 Table
Chromium
(Total)
7440—47—
NA
1.7
P
Ia
12 1—463
315
Nickel
7440—02—
NA
0.20
2
1052
Table
Chromium
(Total)
7440-47-
Li
P
Ia
Nickel
7440—02—
NA
0.20
2
1061
(Low Zinc Subcategory—-less than 15
Total
Zinc)
Table
Cadmium
7440—43—
NA
0.14
P
Chromium
(Total)
7440-47-
NA
5.2
32
L~d
7439—92—
NA
0.24
1
Nickel
7440—02—
NA
0.32
2
1062
Table
Chromium
(Total)
7440-47—
NA
0.094
P
Ia
Lead
7439—92—
NA
0.37
1
1069
(Calcium Sulfate Subcategory)
Tables Cadmium
7440—43—
NA
0.14
B&D
.2.
Lead
7439—92—
NA
0.24
1
K071
(Low Mercury Subcategory--less than
16 mg/kg Mercury)
Table
Mercury
7439—97—
0.025
P
1083
Table
Nickel
7440—02—
NA
0.088
P
a
1084
Table
Arsenic
7440—38—
NA
5.6
#
a
1086
Table
Chromium
(Total)
7440—47—
NA
0.094
P
Ia
Lead
7439—92—
NA
0.37
1
1087
Table
Lead
7439—92—
NA
0.51
P
.1
1100
Table
Cadmium
7440—43—
NA
0.066
P
.2.
Chromium (Total)
7440-47—
32
121—464
316
Leaä
7439—92—
NA
0.51
1
1101
Table
Arsenic
7440—38—
fl~
5.6
#
P
a
1102
Table
Arsenic
7440—38—
fl.~
5.6
#
P
a
1106
(Low Mercury Subcateqorv--less than 260 mg/kg Mercury--
residues from
RNERC)
Tables Mercury
7439-97-
fl~
0.20
B&D
6
1106
(Low Mercury Subcategory--less than 260 mg/kg Mercury--that
are not residues from
RNERC)
Tabi~
Mercury
7439-97-
A
0.20
B&D
6
1115
Table
Nickel
7440-02—
NA
0.32
a
#-—These treatment standards have been based on EP Leachate
analysis but
this does not preclude the use of TCLP analysis.
*——These waste codes are not subcategorized into wastewaters and
nonwastewaters.
NA--Not Applicable.
P and U Listed Wastes
CAS
No.
CommercialRegulated
~
Concentration
(mg/i)
Wast See
Chemical
Hazardous
Regulated
Non-
e
Also
Name
Constituent
Hazardous
Wastewater,~stewaters
Code
Constitue
nt
POlO Table
Arsenic
Arsenic
7440-38-
NA
5.6
B
acid
a
POll Table
Arsenic
Arsenic
7440—38—
NA
5.6
P
pentoxide
a
P012 Table
Arsenic
Arsenic
7440—38—
NA
5.6
P
trioxide
a
P013 Table
Barium
Barium
7440-39-
P
cyanide
I
12 1—465
317
P036 Table
Dichloro-
Arsenic
7440-38—
NA
5.6
phenyl-
a
arsine
P038 Table
Diethyl-
Arsenic
7440-38-
arsine
a
P065
(Low Mercury Subcategory--less than 260 rag/kg Mercury--
residues from RNERC)
Tables Mercury
Mercury
7439-97-
NA
0.20
B
&
D
fulminate
6
P065
(Low Mercury Subcategory--less than 260
mg/kg Mercury--
incinerator residues
(and are not residues from RNERC))
Tables Mercury
Mercury
7439-97-
0.025
B
& D
fulminate
P073 Table
Nickel
Nickel
7440—02—
NA
0.32
P
carbonyl
a
P074 Table
Nickel
Nickel
7440-02-
NA
0.32
B
cyanide
a
P092
(Low Mercury Subcategory
--
less
than
260
mg/kg
Mercury
residues from
RNERC)
Tables Phenyl
Mercury
7439—97-
0.20
B
& D
mercury
acetate
P092
(Low Mercury Subcategory--less than 260 mg/kg Mercury--
incinerator residues
(and are not residues from RNERC))
Tables Phenyl
Mercury
7439-97-
0.025
B
& D
mercury
6
acetate
P099 Table
Potassium
Silver
7440—22—
NA
0.072
B
silver
4
cyanide
P103 Table
Seleno-
Selenium
7782—49—
urea
2
P104 Table
Silver
Silver
7440—22—
NA
0.072
B
cy~nide
4
P110 Table
TetraethylLead
7439—92—
0.51
P
lead
.1
P114 Table
Thallium
Selenium
7782—49—
fl~
B
selenite
a
121—466
318
U032 Table
Calcium
Chromium
7440—47-
0.094
P
chromate
(Total)
Ia
U051 Table
Creosote
Lead
7439-92—
NA
0.51
P
.1
Ul36 Table
Cacodylic
Arsenic
7440-38-
flA
B
acid
a
U144 Table
Lead
Lead
7439—92—
0.51
B
acetate
1
U145 Table
Lead phos- Lead
7439-92—
NA
0.51
P
phate
1
U146 Table
Lead sub—
Lead
7439—92—
NA
0.51
P
acetate
1
U15l
(Low Mercury Subcategory—-less than 260 mg/kg Mercury--
residues from RMERC)
Tab1~ Mercury
Mercury
7439-97-
NA
0.20
B&D
6
U15i
(Low Mercury Subcategory--less than 260 mg/kg Mercury--that
are not residues from
RMERC)
Tables Mercury
~4ercury
7439-97—
0.025
B&D
6
U204 Table
Selenium
Selenium
7782—49—
NA
5.7
B
dioxide
a
U205 Table
Selenium
Selenium
7782-49—
NA
5.7
P
sulfide
a
-—These treatment standards have been based on
EP Leachate
analysis
but this
does not preclude the use of TCLP analysis.
*——These waste codes are not subcategorized into wastewaters and
nonwastewaters.
NA--Not Applicable.
Source:
Amended at 15
Ill. Reg.
,
effective
121—467
319
Section 728.Tabie B Constituent Concentrations
in Waste
(CCW)
F(~1
ron
Industry)
Concentration
(in mg/L)
Methylene chloride
0.44
F006 nonwastcwaters
(sec also Table A)
Cyanides
(Total)
Concentration
(in mg/kg)
Reserved
1001
nonwastewaters
(see also Table A)
Concentration
(in mg/kg)
0.0
Naphthalene
Pentachlorophenol
37.
Phenanthrene
0.0
-Pyrene
7.3
Toluenc
0.14
Xylenes
0.16
1001
wastewaters
Concentration
(inmg/L)
Naphthalene
0.15
Pentachlorophenol
0.88
Phenanthrene
0.15
Pyrene
0.14
Toluene
0.14
Xylenes
0.16
Lead
0.037
1015
wastewatcrs
Concentration
(in mg/L)
Anthracene
1.0
Benzal
chloride
0.28
Benzo
(b
or
k)
fluoranthene
Phenanthrene
Toluene
O-~-2-~
0.27
0.15
Chromium
(Total)
0.32
Nickel
0.44
12 1—468
320
-tim--mg/kg)-
f+exachlorobenzcnc
Hexachiorobutadiene
Hexachiorocyc-lopentadiene
Hexach-1-oroethane
T-etrachloroethene
20.
5--6---
5.6
28.
1016
wastewaters
Concentration
-(in
mg/Lj-
0.033
Hexachlorobenzcnc
Hexachiorobutadiene
0.007
Hexachlorocyclopentadiene
0. 007
Hexach-1-er-e-e-thanc
0.033
Tetrachioroethene
0.
oo~
I~018r.~nwaste~~atcrs
Concentration
-(in rag/kg)
6.0
Chioroethane
1, 1-Dichloroethane
1,2 Dichioroethane
c.
6.0
Hexachlorobenzene
20.
Hexachlorobutadiene
5. 6
Hexachioroethane
28.
Pe-a-e1~-1oroethane
5.6
1,1,
l-Trichloroe-thane
6.0
3018
wastewaters
Cpncentration
(inmg/L)
Chlcyr-eethanc
0.007
Chioromethanc
o.ooi
1, l—Dichlorocthane
1, 2-Dichloroethane
Hexachlorobenzenc
0.007
0.007
0.033
He-xi~ichlorobutadiene
0.007
Pentachloroethane
0. 007
0.007
12 1—469
Tf t~¶
321
(in mg/kg)
Bis (2—chloroethyl) ether
5.
Chlorobenzene
c.o
Chloroform
1, 2-Dichioroethane
Hexachloroethane
N-aphthalene
12-henanthrene
Tetrachl-oroethenc
6.0
6.0
23.
5.6
5.6
6.0
-17-2,4
Trichlorobcnzcne
1,1,
1-Trichloroethane
10.
6.0
3010
wastcwaters
Concentration
(in
mg/L)
Bis(2
chlorocthyl)cther
0.007
Chlorobenzene
0.006
Chloroform
0.007
p
Dichlorobenzenc
0.008
1,2
Dichioroethane
0.007
Fluorene
O.OO-~
Hexachloroethane
0. 033
Naphthalene
0.007
Phenanthrcnc
0.007
l,2,4,5-Tctrachlorobcnzenc
0.017
Tetrachloroethenc
0.007
1,2,4
Trichlorobcnzene
0.023
1,1,1
Trichloroethane
0.00~
3020
nonwastewaters
1, 2-Dichloroethane
1,1,2,2 Tetrachioroethane
Tetrachioroethene
Concentration
-(-in
mg/kg)
C.
0
5.6
6.0
14320
wastcwaters
Concentration
(in mg/L)
1, 2-Dichioroethane
0.007
1,1,2,2-Tctrachloroethane
0.007
Tetrachloroethene
0. 007
121—470
322
KO-2-2---n-enw-&s-tewaters (see also Table
A)-
C-cnc c-nt---~-~a
t-i c--n
(inmg/~g)
Acetophenone
10.
Oum of Diphenylamine and Diphenylnitr-osamine
13.
Phenol
12.
Toluenc
0.034
1024
nonwa-stewatcrs
Phthalic acid
3024-
wastewaters
Loncentration
(in mg/kg)
28.
Conccntrat-i-en
(in mg/L-)-
0.54
P-h-thalic
acid
10—~iewa-s-tewete~e—
Concentration
(in mg/kg)
Hexachiorobutadiene
5.6
Hexachloroethane
28.
He~a-ler-ep-repene
10.
Pentachlorobcnzene
Pentachloroethane
17-~±,
4, 5-Tetrachlorobenzene
Tetrachloroethene
28.
5.6
14.
1,2,4 Trichlorobenzene
10.
3030
wastewaters
Con-e-entrat
ion
-(in
nig/L~
o-Dichlorobenzene
0.008
p Dichlorobenzenc
0.008
Hex-e-ehiorobutadiene
0.007
+e~-achlorocthane
0.033
Pentachloroethane
0.007
1, 2,4, 5—Tetrachlorobcnzene
0. 017
Te-t-r-a-eh-loroethcne
1,2,4 Trichlorobenzene
0. 007
—o----&2-3-
1037
nonwastewaters
Concentration
-(--in mg/kg)
0.1
D4s-’~±1-foton
Tolucnc
-
28.
12 1—471
323
K037 wastewaters
Conbéntr
(in mg/L)
Disulfoton
Toluene
0.003
0.020
K048 nonwastewaters
(see also Table A)
Concentration
(in mg/kg)
9.5
Benzene
Benzo(a)pyrene
0.84
Bis (2-ethyihexyl)phthalate
37.
Chrysene
2.2
Di n butyl phthalatc
4.2
Ethylbenzenc
C7.
Reserved
Naphthalenc
Phenanthrenc
7.7
Phenol
2.7
Pyrene
2.0
T-e-luene
Xylenes
Cyanides
(Total)
1046
wastewaters
9.5
Reserved
1.8
Concentration
(in mg/L)
Benzene
0.011
Benzo(a)pyrene
0.047
Bis(2 ethylhexyl)phthalate
0.043
Chrysene
0.043
Di-n butyl phthalate
0.060
Ethylbenzene
0.011
Fluorcnc
0.050
Naphthalcne
0.033
Phenanthrenc
0.039
Phenol
0.047
Pyrene
0.045
Toluene
0.011
Xylcnes
0.011
Chromium (Tptal)
0.20
Lead
-
0.37
121—472
324
-
12 1—473
iS I UI
‘J
flU1Rc,J;1
~
F
~F~I
I
~
~I
I
~fl
‘I
Concentration
(in mg/kg)
Anthracenc
6.2
Benzenc
9.5
Benzo(a)pyrene
0.84
Bi-s (2-cthylhexyl) phthalate
37.
Chrysene
2.2
67.
Ethylbenzene
Naphthalenc
Phenanthrene
(Reserved)
7.7
Phenol
2.7
Pyrene
2.0
Toluenc
o..s
Xylenes
Reserved
Cyanidcs
(Total)
1.8
K0-4-9—-w-a-s-tewaters
Concentration
(in mg/L)
0.039
Anthracene
Benzenc
—-—
0.011
Benzo(a-)-pyrene
0.047
Bis(2 ethylhexyl)phthalate
0.043
Carbon disulfide
0.011
Chrysene
24—D4me-t~y1phcno1
0.043
-E-thylbenzene
0.011
Naphthalene
0.033
Ph-enanthrene
0.030
Phenol
0.047
Pyz-ene
0.045
Toluenc
0.011
Xv-Ienes
0.011
Chromium
(Total)
0.20
Lead
0-~-e-3~
1050
nonwastewaters
(sec also Table
A)-
Concentration
(in rag/kg)
0.84
Benzo(a)pyrene
Phenol
Cyanides (Total)
2.7
1.8
1050
wastewaters
(in mg/L)
Benzo(a)pyrene
Phenol
0.047
0.047
Chromium
(Total)
0.20
Lead
0.037
1051
nonwastewaters
(sec also Table
A)
Concentration
(in mg/kg)
Anthracene
6.2
Benzene
9.5
Benzo
(a) anthracene
1.4
Benzo(a)pyrene
Bis(2 ethylhexyl)phthalate
0.84
37.
Chrysene
2.2
Di n butyl phthalatc
4.2
Ethylbenzene
67.
Nciphthalcne
Reserved
Phenanthrene
7.7
Phenol
2.7
Pyrenc
2.0
Toluene
9.5
Xylenes
Reserved
Cyanides
(Total)
1.0
3051
wastcwaters
Concentration
(in mg/L)
Acenaphthenc
0.050
Anthraccne
0.030
Benzene
0.011
Benzo(a)anthracene
0.043
Benzo(a)pyrene
0.047
Bis(2 ethylhexyl)
phthalate
0.043
Chrysene
p•p43
Di-n butyl phthalate
0.060
Ethylbenzene
0.011
Fluorene
0.050
Naphthalene
0.033
Pherianthr-enc
0.039
Phenol
0.047
Pyrene
0.045
Toluene
0.011
Xylenes
Chromium (Total)
0.011
0.20
Lead
-
0.037
121—474
325
stewaters
.lso Table A)
326
‘... ¼1.LiL..
-
Si
¼..3 Li
L- S
LI
S
(inmg/)~g)
9.5
~-en
~
cn
~-
Benzo(a)pyrene
o Cresol
u.tsc~
2.2
p Cresol
Ethylbenzenc
0.90
67.
Naphth-a-Iene
Reserved
Phenanthrene
7.7
Phenol
2.7
Toluene
-
9.5
Xylenes
Reserved
1.8
Cyanides
(Total)
3052
wastewatcrs
Concentration
(in mg/L)
.
Benzcnc
0.011
Benzo(a)pyrene
-.
0.047
o Cresol
0.011
p Cresol
0.011
2,4 Dimethyiphenol
0.033
-E-thylbenzene
0.01-1
Naphthalenc
0.033
Phenanthrene
0.
Phenol
0.047
Toluene
0.011
~ylenes
0.011
Chromium
(Total)
0.20
Lead
-
0.037
1062
wastewaters
Concentration
(in mg/L)
0. 32
Chrornium—( Total)
Iead
0.04
Nickel
0.44
14371
wastcwaters
Concentration
(in mg/L)
0.030
Mercury
--
—
12 1—475
327
1066
nonwastcwatcrs-Solvcnt Washes Subcategory
(see also Table A)
Concentration
(in
rag/kg)
Acetone
0.37
bi3(2 ethylhcxyl) phthalate
0.49
n Butyl alcohol
0.37
Cyclohexanone
1,2 Dichlorobenzene
0.49
0.49
Ethyl acetate
0.37
Ethyl benzcnc
0.031
Methanol
0.37
Nethylene
chloride
0.037
Methyl ethyl ketone
0.37
Methyl isobutyl ketone
0.37
Naphthalene
-
-
0.40
Nitrobengene
0.40
Toluene
0.031
1,1,1, Trichloroethanc
0.044
Trichloroethylene
0.031
Xylcnes
0.015
1086
wastewaters-Solvent Washes Subcategory
(in mg/L)
bi3 (2 ethylhexyl)phthal
n Butyl alcohol
“-ii’-
Ethy
Mcthar5~...
Cl
LI
CYI~)
~
L.
‘oroben~ene
•
IWI
flfl~t1
!‘i
PiAA
0.031
1
r~~rir’
...
0.015
r~ r~
U
•
U_I
Met~y1ene
chloride
ketone
0.031
Methyl ethyl
Methyl isobutyl ketone
0.031
0.031
Naphthalene
Nitrobenzene
0.044
Toluene
0.044
0.029
1,1,1, Trichloroethane
0.031
Trichloroethylene
0. 029
Xylenes
0.015
Chromium (Total)
0.32
Lead
0.037
12 1—476
328
1,
r~
()
—7
s
(see
also
Table
A)
-(--i-n mg,’kg)
Acenaphthalen
Benzene
c
3.4
0.071
Chrysenc
3.4
Fluoranthene
3.4
Indeno(1,2,3
cd)pyrenc
3.4
Naphthalene
3.4
Phenanthrene
3.4
Toluene
0.65
Xylenes
0.070
1087
wastewaters
(inmg/L)
Accnaphthalenc
0.020
Benzene
0.014
Chrysenc
0.028
H-uer-onthene-—--—---———--
0 .--0 2-8
Indeno
(1,2,3
cd)
pyrene
0.028
Naphthalcne
p.o~-&
Phenanthrene
0.028
Tolucne
0.000
Xylenes
0.014
Lead
0.037
Si LILA
121—477
(in mg/L)
(in mg/kg~
2,4 Dichiorophenoxyacetic acid
1.0
Hexaehlorodibenzo p dioxins
0.001
Hexachlorodibcnzofurans
0.
001
Pentaehlorodibenzo p dioxins
0.001
Pentachlorodibenzofurans
0.001
Tetrachlorodibenzo p-dioxins
T-etrachlorodibenzofurans
0.00-1
0. 001
3099
wastewaters
2,4 Dichlorophenoxyacetic acid
1.0
Hexachlorodibcnzo-p dioxins
Hexachlorodibenzofurans
0.001
0.001
Pentachlorodibenzo p dioxins
0.001
Pentachlorodibenzofurans
0.001
Tetr-a-e~n1orodibenzop dioxins
0.001
Tetrachlorodibenzofurans
0.001
329
~.,ic)(seeaI~oTab1c
A)
ic Subcategory
1
12 1—478
4—1-.—..-.
1
O~
3—.-.4—--1
ortho Nitroaniline
3101
wastcwaters
Concentration
(in mg/kg)
14.
Concentration—
(in mg/L)
ortho Nitroanilinc
0.27
Arsenic
2.0
Cadmium
0.24
Lead
0.11
Mercury
0.027
3102
nonwastewaters
(Low Arsenic Subcategory less than 1
total
arsenic)
(see
also
Table
A)
Concentration
(in mg/kg)
13.
ortho Nitrophcnol
3102
wastewaters
Concentration
(in mg/L)
ortho Nitrophenol
0.028
Arsenic
2.0
Cadmium
0.24
Lead
0.11
Mercury
0.027
3103
nonwastewaters
Concentration
(in mg/kg)
Aniline
5.-C
Benzenc
6.0
2,4 Dinitrophenol
5.6
Nitrobenzene
5.6
Phenol
5.6
3103
wastewaters
Concentration
(in mg/L)
4.5
Aniline
-
Benzenc
0.15
2-i4
Dinitrophenol
0.61
Nitrobenzcne
0.073
Phenol
1.4
330
(in mg/kg)
Aniline
Benzene
5.6
6.0
2, 4—Dinitrophenol
Nitrobenzene
5.6
5.6
Phenol
5.6
eyanides
(Total)
1.8
1104
wastewaters
C-ee~a~en-
(ir~mg/L)
4.5
An-~iline
Benzene
0.15
2, 4-Dinitrophcnol
0. 61
Nitrobenzenc
0.073
Phenol
1.4
Cyanides
(Total)
2.7
No La-nd—Dsposal for:
1004
3008
Nonwastewaters
1015
Non~-&s-tewaters
34)21
Nonwastewaters
14)25
Nonwastewaters
3036
Nonwastewaters
K
30 4~
1060
Nonwast-ewaters
K06-l---Ne~-wa-etew-aters-HighZinc
&ubeat-egory
(greater -than or equal
to 15°~total zinc)
1069
Nonwastewaters Non Calcium
Sulfate Subcategory
143-8-3
Nonwastewaters-No Ash
~
/-1.--,-.,-.
4-1-..-..-.
Cl
ri1Q~
4—..4--.1
-(-Basod
0--n --No Goner-at-i-en-)-
-(-B-as-ed
on
--N
C--cnor—--a
(-Based on No Ash)
(-Based on No -Generation)
-NGene-t-i-ef~
(-Based on Reactivity)
(Based
on
Reactivity)
-(-~as-e4--a
-~c-a
e-t
i--vit -y
)—
-(-B-as-ed
on
No
Generation)
-(-Based
on
Recycling):
e-~f-eetive—8
/8/00
(Based on No Ash)
~~-SwLi-.stcw(oters
(Based on Recycling-)-
ener-at~en±
12 1—479
331
D,
F and K Listed Wastes
CAS No.
Concentration
(rag/i)
Wast See
Regulated
Regulated
Non-
e
Also
Hazardous Constituent
Hazardous Wastewater~stewaters
Code
Constitue
nt
D003
(Reactive
cyanides
subcategory--based
on
Cyanides
(Amenable)
35
Ill.
Adm.
Code
721.123(a)
(5))
Cyanides
(Totall
57—12—
Res.
#
590.
5
D004 Table
Arsenic
7440-38—
5.0
NA
a
D005 Table
Barium
7440—39—
100.
NA
A
D006 Table
Cadmium
7440—43—
1.0
NA
A
2
D007 Table
Chromium
(Total)
7440—47—
5.0
NA
A
Ia
D008 Table
Lead
7439—92—
5.0
NA
A
D009 Table
Mercury
7439-97—
0.20
NA
A
DOlO Table
Selenium
7782—49—
3~Q
NA
A
a
DOll Table
Silver
7440—22—
NA
A
D0l2 Table
Endrin
720—20—
NA
0.13
D013 Table
Lindane
58—89—
NA
0.066
P
2
D014 Table
Methoxychlor
72—43—
NA
0.18
P
D015 Table
Toxaphene
8001—35-
NA
P
12 1—480
332
0016 Table
2,4—D
94—75—
NA
10.0
P
2.
D017 Table
2,4,5—TP Silvex
93—76—
-
7.9
P
FOO1—F005 spent solvents
Tables l,1,2—Trichloroethane
71—55—6
0.030
a 7.6
A&D
Benzene
71—43—2
0.070
a 3.7
FO01-F005 spent solvents
(Pharmaceutical industry wastewater
Methylene chloride
______
____
____
_____
Cyanides
(Total)
F006 Table
A
F007 Table
A
FOOB Table
A
FOO9 Table
A
Cyanides
(Amenable)
Cadmium
Chromium
Lead
Nickel
Cyanides
(Total)
(Amenable)
Cyanides
Chromium (Total)
Lead
Nickel
Cyanides
(Total)
(Amenable)
Cyanides
Chromium
Lead
Nickel
çy~nides (Total)
75—09—
2
57—12—
5
57—12—5
7440—43—
9
7440—47—
32
7439—92—
1
7440—02—
2
57—12—
5
57—12—5
7440—47—
32
74 39—92—
1
7 44 0—02—
2
57—12—
5
57—12 —5
7440—47—
32
74 39—92—
1
744 0—02—
2
57—12—
5
57—12—5
744O—47—
32
0.44
1.2
0.86
1.6
0.32
0.040
0.44
1.9
0.1
0.32
0.04
0.44
1.9
0.13
0.32
0
.
04
0.44
1.95
0.1
0.32
NA
590.
30.
NA
NA
NA
NA
590.
30.
NA
NA
NA
590.
30.
NA
NA
NA
90.
30.
NA
Qy~nIde~
Chromium
(Amenable)
12 1—481
333
74 39—92—
1
7440—02—
2
0.04
NA
0.44
NA
çy~nides (Total)
Cyanides
LAmenable)
FOil Table
Cvanides
A
57—12—
5
57—12 —5
7440—47—
32
7439—92—
1
7440—02—
2
57—12
-~
5
57—12—5
7440—47—
32
7439—92
—
1
7440—02—
2
57—12—
5
57—12—
5
7440—47—
32
0,04
NA
0.44
NA
(R)
590.
0.86
(R)
30.
____
NA
107—0~—i
75—34—3
107—06—2
78—87—5
10061—
01—5
10061—
02—6
117—81—
7
~7—72—1
7440—47—
32
treated via
a
O~28
a
0.28
a
0.014
a
0.014
a
0.014
a
0.014
a
0.014
a
0.036
a
0.036
0.35
a
0.28
a
0.23
a
0.014
a
0.014
a
0.014
a
0.014
a
0.014
a
1.8
a
1.8
NA
Lead
Nickel
FO10
57—12—5
57—12—5
(Totafl
1.9
0.1
1.5
NA
1,9
110.
0.1
0.32
9.1
NA
Cyanides
(Amenable)
Chromium
(Total)
Lead
Nickel
Cyanides
(Total)
(Amenable)
Cyanides
Chromium (Total)
Lead
Nickel
Cyanides
(Total)
Cyanides
(Amenable)
0.04
NA
0.44
NA
1.9
110.
F012 Table
A
F019 Table
A
0.1
0.32
9.1
NA
Chromium (Total)
F024
(Note:
F024 organic standards must~~
incineration
(INCIN))
Tables 2—Chloro-L3—butadiene 126—99—
3-Ch1.oroprop-?ne
~1-Dichloroethane
1, 2-Dichloroethane
1, 2-Dichloropropane
cis—1,3—Dichloro—
p~opene
trans—1,
3—Dichloro-
pro~ene
Bis(2-ethylhexyl)
-
phthalate
Hexachloroethane
Chr oralu
m(T çtafl
12 1—482
334
7440—02—
2
67—63 —3
107—06—2
75—35—4
75—9—2
56—23—5
79—00—5
79—01—6
75—01—4
S
0.046
S
0.21
S
0.025
S
0.089
s
0.057
S
0.054
S
0.054
S
0.27
a
6.2
a
6.2
a
6.2
a 31.
a
6.2
a
6.2
5
5.6
a
33.
67—66—3
75—9—2
56—23—5
79—00—5
79—01—6
75—01—4
118—74—1
87—68—3
67—72—1
0.089
0.057
0.054
0.054
0.27
0. 055
0.055
0. 055
a
31.
a
6.2
a
6.2
s
5.6
a
33.
a
37.
a
28.
a
30.
Nickel
F025
(Light ends subcategorv)
Chloroform
1. 2-Dichloroethane
1, 1-Dichloroethylene
Methylene chloride
Carbon
tetrachloride
1
•
1. 2-Trichloroethane
Trichloroethylene
Vinyl chloride
0.47
NA
F025
(Spent filters/aids and desiccants subcategory)
Chloroform
Methylene chloride
Carbon tetrachloride
1, 1,2—Trichloroethane
Trichloroethylene
Vinyl chloride
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
s
0.046
a
6.2
F039
Table
A
S
S
S
S
S
S
S
S
Acetone
s
0.28
a160.
S
S
S
S
S
S
S
S
S
S
S
0.059
0.059
0.17
0.010
0. 059
0.24
0.021
0.13
0.81
0. 059
0.013
Acenaphthalene
Acenaphthene
Acetonitri le
Acetophenone
2 -Acetylaminofluorene
Acrylonitrile
Aldrin
4-Aminobiphenyl
Aniline
Anthracene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor
1242
Aroclor
1248
Aroclor 1254
AroclQr 1260
67—64—
1
208—96—8
83—32—9
75—05—8
96—86—2
53—96—3
107—13—1
309—00—2
92—67—1
62—53 —3
120—12—7
12674—
11—2
11104—
28—2
11141—
16—5
53469—
21—9
12672—
29—6
11097—
69—1
11096—
82—5
319—84—6
319—85—7
a
3.4
a
4.0
NA
a
9.7
a140.
a
84.
a
0.068
NA
a
14.
a
4.0
a
0.92
a
0.92
a
0.92
a
0.92
a
0.92
a
1.8
a
1.8
s
0.014
____
s
0.013
____
s
0.017
____
s
0.013
____
s
0.014
s
0.014
s
0.00O14~ 0.066
S
0.00014 a
0.066
~p~BHC
beta
-
BHC
121—483
335
bromide)
4-Bromophenyl phenyl
101-55-
ether
n-Butyl alcohol
71-36-3
Butyl benzyl phthalate 85-68-7
2—sec—Butyl—4,6—
88—85—7
dinitrophenol
Carbon tetrachloride
56—23—5
Carbon
disulfide
75—15-0
Chiordane
57—74—9
p—Chloroaniline
106—47—8
Chlorobenzene
108—90—7
Chlorobenzilate
510—15—6
Chiorodibroinomethane
124—48—1
Chloroethane
75—00-3
bis(2—Chloro—
111—91—
ethoxy) methane
bis(2—Chloroethyl)
111—44—
ether
4
2-Chioroethyl vinyl
ether
Chloroform
67-66-3
bis(2-Chloroisopropyl)
39638—
ether
32—9
p—Chloro—m—cresol
59-50—7
Chloromethane
(Methyl
74-87-3
chloride)
2-Chloronaphthalene
______
2-Chlorophenol
3—Chloropropene
__________
Chrysene
_________
o—Cresol
________
Cresol
(ra—
and
p—
isomers)
Cyclohexanone
1, 2-Dibromo-3-chloro-
________
propane
1, 2-Dibromoethane
________
(Ethylene dibroinide)
Dibromornethane
________
.a
0.36
NA
s
0.11
a 15.
s
0.028
a
15.
S
0.11
a
15.
delta-BHC
gamma-BHC
Benzerie
Benzo
(a) anthracene
Benzo
(b) fluoranthene
Benzo
(k) fluoranthene
Benzo(g,h,
i)perylene
Benzo(a)pyrene
Bromodichloromethane
Bromoform
Bromomethane
(methyl
319—86—8
58—89—9
71—43—2
56—55—3
205—99—2
207—08—9
191—24—2
50—32—8
75—27—4
75—25—2
74—63 —9
•~~_
0.023
~
0.0017
~
0.14
•~~_0.059
~
0.055
~
0.059
~
0.0055
~
0.061
.a..
0.35
~
0.63
~
0.11
a
0.066
a
0.066
a 36.
a
8.2
a
3.4
a
3.4
a
1.5
a
8.2
a 15.
a 15.
a
15.
0.055
a 15.
5
5.6
5
0.017
S
0.066
S
0.057
s
0.014
~
0.0033
S
0.46
S
0.057
S
0.10
s
0.057
S
0.27
S
0.036
a
2.6
a
7.9
a
2.5
a
5.6
NA
a
0.13
a 16.
a
5.7
NA
a
16.
a
6.0
a
7.2
S
0.033
a
7.2
~
0.057
NA
s
0.046
S
0.055
S
0.018
S
0.19
S
0.055
S
0.044
S
0.036
5
0.059
5
0.11
S
0.77
91—8—7
95—57—8
107—05—1
218—01—9
95—48—7
a
5.6
a
7.2
a 14.
a
33.
a
5.6
a
5.7
a 28.
a
8.2
a
5.6
a
3.2
108—94—1
96—12—8
106—93—4
74—95—3
12 1—484
336
2
,
4—Dichloro—
phenoxyacetic
acid
(2 ,4—D)
o,p’-ODD
p,p’-DDD
o,p‘-DDE
ra-Dichlorobenzene
o—Dichlorobenzene
p—Dichlorobenzene
Dichlorodifluoro-
methane
1, 1-Dichloroethane
1
.
2-Dichioroethane
1
,
l—Dichloroethylene
trans-l
.
2-Dichloro-
ethene
2, 4-Dichlorophenol
2, 6-Dichlorophenol
1, 2-Dichloropropane
cis-1
,
3—Dichioro—
propene
trans-l
,
3-Dichloro-
propene
Dieldrin
Diethyl phthalate
p-Dimethylaniinoazo-
benzene
2, 4-Dimethyl phenol
Dimethyl phthalate
Di-n-butyl phthalate
1, 4-Dinitrobenzene
4 ,6-Dinitro-o-cresol
2
,
4-Dinitrophenol
2, 4-D
i
nitrotoluene
2, 6-Dinitrotoluene
Di-n-octyl phthalate
Di-n-
propylnitrosoamine
~4 -Dioxane
Disulfoton
EndoSulfan
I
Endosulfan
II
Endosulfan Sulfate
94—75—
7
53—19—0
72—54—8
3424—82—
6
72—55—9
789—02—6
50—29—3
53—70—3
541—73—1
95—50—1
106—46—7
75—71—
8
75—34—3.
107—06—2
75—35—4
120—83—2
87—65—0
78—87—5
10061—
01—5
10061—
02—6
60—57—I
84—66—2
60—11—
3
105—67—9
131—11—3
84—74—2
100—25—4
534—52—1
51—28—5
121—14—2
60 6—2 0—2
117—84—0
621—64—
7
123—91—1
298—04 —4
939—98—8
33213—
6—
5
1031—07—
8
S
0.023
S
0.023
S
0.031
5
0.031
~
0.0039
S
0.0039
S
0.055
S
0.036
S
0.088
S
0.090
S
0.23
S
0.087
S
0.12
s
0.017
S
0.023
S
0.029
a
0.087
a
0.087
a
0.087
a
0.087
a
0.087
a
0.087
a
8.2
a
6.2
a
6.2
a
6.2
a
7.2
NA
a170.
a
6.2
a
0.066
a
0.13
S
0.72
a
10.
p,p‘-DDE
o.p’-DDT
p.p’ -DOT
Dibenzo(~i.h~
anthr~r~
s
0.059
a
7.2
s
0.21
a
7.2
S
0.025
a 33.
s
0.054
a 33.
S
0.044
a 14.
s
0.044
a 14.
S
0.85
a 18.
S
0.036
a 18.
s
0.036
a 18.
S
0.017
a
0.13
s
0.20
a 28.
s
0.13
NA
S
0.036
a
14.
s
0.047
a 28.
S
0.057
a 28.
s
0.32
a
2.3
S
0.28
a160.
S
0.12
a160.
s
0.32
al4O.
s
0.55
a 28.
s
0.017
a 28.
s
0.40
a
14.
1, 2-Diphenyl hydrazine
s
0.029
a
0.13
12 1—485
337
Endrin
Endrin aldehyde
Ethyl
acetate
Ethyl cyanide
Ethyl benzene
Ethyl ether
bis
(2-Ethylhexyl)
phthalate
Fthvi
m~thac~rv1at~
___________________
97—63—2
Ethylene
oxide
75—21—8
Famphur
52—85-7
Fluoranthene
206—44-0
Fluorene
86—73-7
Fluorotrichloromethane 75—69—4
-
Heptachlor
76—44—8
Heptachlor epoxide
1024-57-
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopenta—
diene
Hexachlorodibenzo-
furans
Hexachlorodibenzo-p-
dioxins
Hexachloroethane
Hexachloropropene
7—20—8
7421—93—
4
s
s
0.0028
0.025
a
0.13
a
0.13
141—78—6
100—41—4
60—29—7
s
~
S
5
0.34
0.24
0.057
0.12
a 33.
NA
a
6.0
al6O.
117—81—7
s
s
S
s
s
S
S
s
0.28
0.14
0.12
0.017
0.068
0.059
0.020
0.0012
a
28.
a160.
NA
a
15.
a
8.2
a
4.0
a
33.
a
0.066
3
S
0.016
~_
0.066
118—74—1
87—68—3
77—47—
4
~.
~.
s
S
0.
0.
0.055
0.055
0.057
000063
000063
a 37.
a 28.
a
3.6
~
0.001
a
0.001
67—72—1
1888—71—
7
s
s
0.055
0.035
a 28.
a 28.
193—39—
5
s
0.0055
a
8.2
74—88—4
0.019
a 65.
78—83—1
S
5.6
a170.
465—73—6
s
0.021
a
0.066
120—58—1
5
0.081
a
2.6
143—50—8
0.0011
a
0.13
126—98—7
Methapyrilene
91-80-5
Methoxychior
72—43-5
3—Methylcholanthrene
56—49-5
4,4—Methylene—bis—(2—
101—14—4
chloroaniline)
Methylene chloride
75—09-2
Methyl ethyl ketone
78-93-3
Methyl isobutyl ketonelo8—lO—1
5
s
S
s
5
~
5
S
~.
~
~
0.24
0.081
0.25
0.0055
0.50
0.089
0.28
0.14
0.14
0.018
0.014
0.059
a 84.
a
1.5
a
0.18
a 15.
a 35.
a 33.
a 36.
a 33.
a160.
NA
S
4.6
a
3.1
Methyl methacrylate
80—62—6
Methyl methansulfonate
Methyl parathion
298—00-1
Naphthalene
91—20—3
2-Naphtylamine
91—59—8
p—Nitroaniline
100—01—6
Nitrobenzene
98—95—3
S
0.52
0.028
0.068
NA
a
28.
a
14.
Indeno(l,2
,
3 ,—c,d)—
pyrene
Iodomethane
Isobutanol
Isodrin
Isosafrole
Kepone
Methacrylonitrile
12 1—486
338
5—Nitro—o—toluidine
99-55—8
4—Nitrophenol
100—02—7
N-Nitrosodiethylainine
55-18—5
N—Nitrosodimethylarnine 62—75—9
N-Nitroso-di-n-butyl
-_______
amine
N-Nitrosomethylethy1-
amine
N-Nitrosoinorpholme
N-Nitrosopiperidine
N-Nitrosopyrrol
idine
Parathion
Pentachlorobenzene
Pentachlorodibenzo—
furans
Pentachlorodibenzo-p-
dioxins
Pentachioro—
~acIi~,.
orgphenpj.
Phenol
Phorate
Propanenitrile
(ethyl
cyanide)
Pronamide
s
0.32
s
0.12
s
0.40
S
0.40
s
0.40
a 28.
a 29.
a 28.
NA
a
17.
924—16—
3
105—95—
6
5
0.40
a
2.3
59—89—2
100—75—4
930—55—2
56—38—2
s
0.40
S
0.013
S
0.013
s
0.017
a
2.3
a35.
a
35.
a
4.6
608—93—5
s
0.055
-~--
0.000035
a
0. 000063
a
37.
~
0.001
a
0.001
82—68—
~.
87—86—5
62—44—2
s
0.055
S
0.089
S
0.081
a
4.8
a
7.4
a
16.
nitrobenzene
Phenacetin
Phenanthrene
85—01-8
108—95—2
298—02—2
107—12—0
23950—
58—5
129—00—0
110—86—1
94—59—7
93—72—1
93—76—5
s
0.059
s
0.039
s
0.021
5
0.24
S
0.093
s
0.067
s
0.014
s
0.081
s
0.72
s
0.72
a
~
a
6.2
a
4.6
a360.
a
1.5
a
8.2
a
16.
a 22.
a
7.9
a
7.9
95—94—
3
s
0.055
0.000063
s
0.000063
a 19.
a
0.001
a
0.001
furans
Tetrachlorodibenzo-p-
dioxins
2,3,7,8—Tetrachioro—
630—20—
~
S
0. 000063
s
0.057
NA
a 42.
dibenzo-p-dioxin
1,l,1,2—Tetrachloro—
ethane
L~,2,2—Tetrach1oro-
79—34—
.~
s
0.057
a 42.
ethane
Tetrachloroethene
127-18-4
58—90—
a
S
0.056
s
0.030
a
~
a 37.
2,3,4,6—Tetrachloro—
phenol
Toluene
108—88—3
s
0.080
a 28.
Toxaphene
8001—35—
s
0.0095
a
1.3
1
~~4~Trich
lorobenzenel2o—82—l
s
0.055
a
19.
Pyrene
Pyridine
Safrole
Silvex
(2.4,5—TP)
2
,
4
,
5—T
1, 2
,
4,5-Tetrachloro—
benzene
Tetrachlorodibenzo—
121—487
339
1,1, 1-Trichloroethane
71-55-6
1, 1,2-Trichloroethane
79—00—5
Trichioroethylene
79—01-6
2,4,5—Trichlorophenol
95—95—4
2, 4, 6—Trichlorophenol
88—06—2
1,2, 3-Trichioropropane 96—18-4
1,1,2—Trichloro—1,2,2— 76—13—1
trifluoroethane
Vinyl chloride
75—01—4
Xylene(s)
Cyanides
(Total)
57—12—5
Cyanides
(Amenable)
57—12—5
Fluoride
16964-
48—8
Sulfide
8496—25—
8
Antimony
7440-36—
0
Arsenic
7440—38—
2
Barium
7440—39—
3
Beryllium
7440—41—
7
Cadmium
7440—43—
9
Chromium
(Total)
7440-47-
32
Copper
7440-50—
8
Lead
7439—92—
1
Mercury
7439—97—
6
Nickel
7440—02—
2
Selenium
7782—49—
2
Silver
7440—22—
4
Vanadium
7440—62—
2
Naphthalene
91-20-
3
Pentachlorophenol
87—86—5
Phenanthrene
85—01—8
Pyrene
129—00—0
Tol-uene
106—88-3
Xylenes
(Total)
Lead
7439—92—
1
5
0.054
S
0.054
S
0.054
S
0.18
s
0.035
5
0.85
S
0.057
5
0.27
S
0.32
S
1.2
S
0.86
S
35.
s
14.
S
1.9
5
5.0
S
1.2
S
0.82
S
0.20
S
0.37
S
1.3
S
0.28
5
0.15
S
0.55
S
0.82
5
0.29
S
0.042
~
0.031
a
0.031
a
0.031
a
0.028
a
0.028
a
0.032
a
0.037
a
5.6
a
5.6
a
5.6
a 37.
a 37.
a 28.
a
28.
a
33.
a
28.
a
1.8
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
a
1.5
a
1.5
a
1.5
a
1.5
a
28.
a 33.
NA
K001. Table
A
12 1—488
340
K002 Table
Chromium
(Total)
A
Lead
7440—47—
32
7439 —9 2—
1
7440—47—
32
7439—92—
1
7440—47—
32
7439—92—
1
7440—47—
32
7439—92—
1
57—12—5
7440—47—
32
74 39—92—
1
7440—47—
32
74 39—92—
1
57—12—5
7440—47—
32
74 39—92—
1
Chromium (Total)
Lead
1003
Table
A
1004
Table
A
1005
Table
A
1006
Table
A
1007
Table
A
1008
Table
A
Chromium
(Total)
Lead
Chromium (Total)
Lead
CyanideS
(Totall
Chromium
(Total)
Lead
Chromium
(Total)
Lead
Cyanides
(Total)
Chromium
(Total)
s
2.9
NA
~
3.4
NA
s
2.9
NA
s
3.4
NA
s
2.9
NA
S
3.4
NA
S
2.9
NA
S
3.4
NA
S
0.74
S
2.9
NA
s
3.4
NA
s
2.9
NA
.~—L~4~
(R) NA
5
0.74
S
2.9
NA
S
3.4
NA
a
6.0
Lead
1009
1010
1011
Chloroform
Chloroform
Acetonitrjle
,~y,lggitri~
Acrylamide
Benzene
67-66—3
67-66-3
75-05-8
107-13-1
79-06-1
71—43—2
0.1
QJ,.
Ia~
0.06
.l~
0.02
~Q
LA
~
ZL..
0.03
1013
Cyanide
(Total)
57—12—5
75—05—8
107—13—1
79-06—1
71—43—2
2L
Ia~
0.06
~
0.02
.~L..
i~
~
a
23.
a
0.03
Acetonitrile
Acrylonitrile
Acrylamide
Benzene
121—489
341
Cyar1ide
(Total)
~-Dichloropropane
1,2,3-Trichloropropane
Bis (2-chloroethyl)
-
ether
4
21.
1014
57.
38.
a
1.8
0.06
a
1.4
19.
a 23.
0.02
~.
0.03
21.
57.
1.Oa
3.4
57—12 —5
75—05—8
107—13—1
79-06-1
Acetonitrile
Acrylonitrile
Acrylamide
Benzene
71—43—2
1015
Table
Cyanide
(Total)
57—12—5
120—12—
Anthracene
A
Benzal chloride
Sum of Benzo(b)fluor-
anthene and Benzo(k)-
fluoranthene
Phenanthrene
Toluene
Chromium (Total)
Nickel
2
98—87—3
205—99-2
207-08-9
85—01-8
108—88—3
7440—47-
32
7440—02—
2
0.28
0.029
0.27
0.15
0.32
0.44
~.
~
3.4
a
3.4
a
6.0
NA
NA
1016
Hexachlorobenzene
118—74—1
87—68—3
77-47-
4
a
a
~
0.033
0.007
0.007
a
28.
a
~
a
~
Hexachlorobutadiene
Hexachlorocyclopenta-
diene
1017
1018
1019
Hexachloroethane
67—72-1
127-18—4
78—87—5
96—18—4
111—44—
75-00—3
75—34-3
107—06—2
87-68—3
67—72-1
76—01-7
71—55—6
111—44—
~
108-90-7
67-66-3
106—46—7
107—06—2
86—73-7
67—72—1
91—20—3
85-01—8
a
a
sa
sa
sa
a
a
a
a
a
a
~
a
a
a
a
a
a
a
a
a
0.033
0.007
0.85
0.85
0.033
0.007
0.007
0.007
0.033
0.007
0.007
0.007
0.007
0.006
0.006
0.008
0.008
0.007
0.033
0.007
0.007
a 28.
a
6.0
a 28.
a 28.
a
7.2
a
6.0
~
~
~
a
28.
a
5.6
~.
~Q
a
5.6
a
6.0
a
~
NA
NA
NA
a 28.
a
~
~
5.6
Tetrachloroethene
Chloroethane
l,1-Dichloroethane
1,2—Dichloroethane
Hexachlorobutadiene
Hexachloroethane
Pentachloroethane
1,1,l—Trichloroethane
Bis(2—chloroethyl)—
ether
Chlorobenzene
Chloroform
p-Dichlorobenzene
1,2—Dichloroethane
Fluorene
Hexachioroethane
Naphthalerie
Phenanthrene
12 1—490
342
1,2
•
4, 5—Tetrachloro—
95—94—
benzene
3
Tetrachloroethene
127-18-4
1,2
,
4—Trichlorobenzene 120—82—1
1, 1
,
1—Trichloroethane
7
1-55—6
1,2—Dichloroethane
1,1,2
,2—Tetrachloro—
ethane
Tetrachloroethene
Chloroform
Carbon tetrachloride
Antimony
Toluene
Acetophenone
Diphenylamine
Diphenylnitrosamine
Sum of Diphenylamine
and Diphenylnitros-
amine
Phenol
Chromium
(Total)
Nickel
107—06—2
79—34—
6
127— 18—4
67—66—
3
58—23—5
58—23—5
108—88—
3
96—86—2
22—39—4
86—30—6
108—95—2
7440—47—
32
744 0—02—
0
1023
Phthalic anhydride
L~asured as Phthalic
acid)
85—44—9
a
0.54
a 28.
1024
Phthalic anhydride
(measured as Phthalic
acid)
85—44—9
a
0.54
a
28.
1. 1-Dichloroethane
trpns-1
,
2-Dichloro-
ethene
Hexachlorobutad iene
Hexachloroethane
Pentachloroethane
1,1, 1, 2-Tetrachloro-
ethane
1,1,2, 2-Tetrachioro-
ethane
1, 1, l-Trichloroethane
1, 1, 2-Trichioroethane
Tetrachloroethylene
75—34—
~
0.007
3
87—68—3
______
67—72—1
______
76—01—7
______
63 0—2 0—
______
6
79—34—
______
6
71—55—6
______
29—00—5
127—18—4
______
0.017
NA
1020
K021 Table
A
K022 Table
A
a
0.007
a
0.023
a
0.007
a
0.007
a
0.007
a
0.007
S
0.046
S
0.057
S
0.057
S
0.060
0.010
S
0.52
S
0.40
NA
a
6.0
a 19.
a
6.0
a
6.0
a
5.6
a
6.0
a
6.2
a
6.2
a
6.2
a
0.034
a
19.
NA
NA
a 13.
0.039
a 12.
0.35
NA
0.47
NA
1028
Table
A
a
6.0
a
0.033
a
6.0
a
0.007
a
0.033
a
0.033
a
0.007
a
0.007
a
0.007
a
0.007
a
0.007
a
5.6
a
28.
a
5.6
a
5.6
a
5.6
a
6.0
a
6.0
a
6.0
12 1—49 1
343
a
a
a
a
0.008
0.006
0. 007
0.033
NA
NA
NA
a
5.6
a 28.
a 19.
a 28.
a
5.6
a 14.
a
6.0
a
19.
K033
Hexach lorocyc
lopenta—
diene
77—47—4
s
0.057
a
2.4
K034
Hexachlorocyclopenta
—
diene
77—47—4
S
0.057
a
2.4
NA
NA
S
0.59
NA
S
0.059
NA
S
0.068
NA
NA
a
3.4
a
3.4
a
3.4
a
3.4
a
3.4
a
3.4
a
3.4
a
3.4
a
3.4
6.4
0.35
0
.
037
0
.
47
0.46
0.21
0.025
0. 054
0.27
NA
NA
NA
NA
a
6.0
a
6.0
a
6.0
a
6.0
a
6.0
Cadmium
7440—43-
9
Chromium
(Total)
7440—47-
32
Lead
7439—92—
1
Nickel
7440—02—
2
Chloroform
67-66-3
1, 2-Dichloroethane
107-06—2
1, 1-Dichioroethylene
75-35-4
1, 1, 1—Trichloroethane
7 1-55—6
Vinyl
chloride
75-01—4
o—Dichlorobenzene
95—50—1
p—Dichlorobenzene
106-46—7
Hexachlorobutadiene
87-68-3
Hexachloroethane
67-72—1
Hexachloropropene
1888-71-
7
Pentachlorobenzene
608—93—5
Pentachloroethane
76—01—7
1,2,4,
5—Tetrachloro—
95—94—
benzene
Tetrachloroethane
127—18-4
1,2 ,4-Trichlorobenzene
120—82—1
1029
1030
1031
Table
A
1032
Arsenic
Hexachlorocyclopenta—
diene
Chlordane
Heptachlor
Heptachlor epoxide
NA
a
0.007
a
0.017
a
0.007
a
0.023
0.79
S
0.057
~
0.0033
S
0.012
5
0.016
7440—38—2
77—47—4
57—74—9
76—44—8
1024—57—3
NA
a 24.
a
0.26
a
0.066
a
0.066
1035
Acenaphthene
83—32-9
Anthracene
120—12-7
Benz (a) anthracene
56—55—3
Benzo(a)pyrene
50-32-8
Chrysene
-
218—01—9
D!benz
(a,h)anthracene
53-70-3
Fluoranthene
206-44-0
Fluorene
86—73—7
Indeno(1,2,3—cd)pyrene 193—39—5
121—492
344
Cresols
(m—
and
p—
isomers)
Naphthalene
o—Cresol
Phenanthrene
Phenol
Pyrene
K036
Disulfoton
29 8—04—4
5
0.025
a
0.1
1038
Phorate
298—02—2
0.025
a
0.1
1040
Phorate
298—02—2
0.025
a
0.1
1041
Toxaphene
8001—35—
1
0.0095
a
2.6
1,2
,
4
,
5—Tetrachloro—
95—94—
benzene
3
o—Dichlorobenzene
95-50—1
p-Dichlorobenzene
106-46-7
Pentachlorobenzene
808—93—5
1,2,4—Trichlorobenzene 120—82—1
1043
2~4-Dichlorophenol
~~pich1
prppiienQl
2
,
4
,
5-Trichlorophenol
2
,
4 ,6—Trichlorophenol
Tetrachlorophenols
(Total)
Pentachlorophenol
Tetrachloroethene
Hexachlorodibenzo—p—
dioxins
Hexachlorodibenzo—
furans
Pentachlorodibenzo-p-
dioxins
Pentachlorodibenzo—
furans
Tetrachlorodibenzo-p-
dioxins
Tetrachlorodibenzo-
furans
120—83—2
—65—0
95—95—4
88—06—2
87—86—5
79—01—6
a
0.049
a
0.013
a
0.016
a
0.039
a
0.018
a
0.22
a
0.006
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
a
0.38
a
0.3
a
8.2
a
7.8
a
0.68
a
1.9
a
1.7
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
Lead
7439—92—
1
0. 037
NA
s
0.77
NA
91—20—3
5
0.059
a
3.4
95—48—7
S
0.11
NA
85—01—8
5
0.059
a
3.4
108—95—2
0.039
NA
129—00—0
s
0.067
a
8.2
K037
Disulfoton
Toluene
298—04—4
s
0.025
a
0.1
108—88—3
~.
0.080
a 28.
1042
s
0.055
a
4.4
5
0.088
s
0.090
S
0.055
S
0.055
a
4.4
a
4.4
a
4.4
a
4.4
1046
Table
A
12 1—493
345
Benzo(a)pyrene
Phenol
Cyanides (Total)
Chromium
(Total)
50—32—
8
108—95—2
57—12 —5
7440—47—
32
7439—92
—
1
1048
Table
~
Benzene
Benzo(a)pyrene
Bis(2—ethylhexyl)—
71—43—
a
50—32—8
117—81—
2.
a
a
~
0.011
0.047
0.043
a 14.
a
12.
a
j~
phthalate
Chrysene
218—01—9
a
0.043
a
15.
Di-n-butyl
phthalate
84-74-2
100—41—4
86-73-7
a
a
a
0.06
0.011
0.05
a
3.6
a
14.
NA
Ethylbenzene
Fluorene
Naphthalene
91—20—3
a
0.033
a
42.
Phenanthrene
85—01-8
108-95-2
a
0.039
0.047
a
34.
a
~
Phenol
Pyrene
129—00—0
a
0.045
a
36.
Toluene
108—88—3
a
0.011
a
14.
Xylene(s)
a
0.011
a 22.
Cyanides
(Total)
57-12—5
7440-47-
32
a
0.028
0.2
a
LA
NA
Chromium
(Total)
Lead
7439—92—
0.037
NA
1
1049
Table
Anthracene
120—12—
a
0.039
a 28.
A
Benzene
Benzo(a)pyrene
Bis(2—ethylhexyl)—
phthalate
Carbon disulfide
Chrysene
2,4—Dimethylphenol
Ethylhenzene
Naphthalene
Phenanthrene
Phenol
Pyrene
Toluene
Xylene(s)
CyanideS
(Total)
Chromium
(Total)
Lead
2.
71—43—2
50-32—8
117—81—
2
75—15—0
218—01—9
105—67—9
100—41—4
91—20-3
85-01—8
108—95—2
129—00—0
108—88—3
57—12—5
7440-47—
32
7439—92—
a
a
a
a
a
a
a
~
a
a
a
a
a
~
0.011
0.047
-
0.043
0.011
0.043
0.033
0.011
0.033
0.039
0.047
0.045
0.011
0.011
0.028
Q~
0.037
a 14.
a 12.
~
NA
a
15.
NA
a
14.
a 42.
a 34.
a
3.6
a
36.
a
14.
a
22.
~
LA
NA
NA
1
1050
Table
A
a
0.047
a
12.
a
a
0.047
0.028
0.2
Lead
a
3.6
a
1.8
NA
0.037
NA
12 1—494
346
1060
Benzene
Benzo (a)pyrene
Naphthalene
Phenol
Cyanides
(Total)
71—43—2
50—32—8
91—20—3
108—95—2
57—12—5
S
0.17
S
0.035
S
0.028
S
0.042
1.9
a
0.071
a
3.6
a
3.4
a
3.4
1.2
7440—43—
9
1051
Table
A
Acenaphthene
83—32—
2
a
0.05
NA
Anthracene
120—12—7
a
0.039
a
28.
Benzene
71—43—2
a
0.011
a
14.
Benzo(a)anthracene
50—32—8
50—32—8
75—15—
.Q
a
a
a
0.043
0.047
0.043
a
20.
a
12.
a
L~
Benzo(a)pyrene
Bis(2—ethylhexyl)—
phthalate
Chrysene
218—01—9
a
0.043
a
15.
Di—n-butyl phthalate
105—67-9
100—41—4
86—73—7
a
a
a
0.06
0.011
0.05a
a
L~
a
14.
NA
Ethylbenzene
Fluorene
Naphthalene
91—20—3
0.033
a 42.
Phenanthrene
85—01—8
108—95-2
a
a
0.039
0.047
a
34.
a
3.6
Phenol
Pyrene
129—00—0
a
0.045
a
36.
Toluene
108—88—3
a
0.011
a 14.
~ylene(s)
a
0.011
a
22.
Cyanides
(Total)
57—12—5
7440-47-
32
a
0.028
~
LA
NA
Chromium
(Total)
Lead
7439—92—
0.037
NA
1
1052
Table
Benzene
71—43—
a
0.011
a
14.
A
~enzo(a)pyrene
o-Cresol
p~Cresol
2,4—Dimethylphenol
Ethylbenzene
Naphthalene
Phenanthrene
Phenol
Toluene
Xylene(s)
Cyanides
(Total)
Chromium
(Total)
a
50—32—8
95—48—7
106-44-5
105—67-9
100-41-4
91—20—3
85—01-8
108—95—2
108—88—3
57—12—5
7440-47-
32
7439—92—
1
a 12.
a
~
NA
a
14.
a 42.
a
34
a
3.6
a 14.
a 22.
a
LA
NA
Lead
a
a
a
a
a
a
a
a
a
a
a
0.047
0.011
0.011
0. 033a
0.011
0.033
0.039
0.047
0.011
0.011
0.028
0.2
0.037
NA
K061 Tables
A&D
Cadmium
1.61
NA
121—495
347
7440—47—
32
74 39—92—
1
7440—02—
2
7440—47—
32
7439—92—
1
74 40—02—
2
7440—43—
9
7439—92—
1
Chromium (Total)
Lead
Nickel
Chromium (Total)
0.32
NA
0.51
NA
0.44
NA
0.32
NA
0.04
NA
0.44
NA
1.6
NA
0.51
NA
0.030
NA
1062
Table
A
K069 Tables
A&D
1071
Table
A
1073
1083
Table
A
1084
1085
Lead
_________
Nickel
________
Cadmium
________
Lead
________
Mercury
7439-97—
6
Carbon tetrachloride
58-23-5
Chloroform
67-66-3
Hexachloroethane
67-72-1
Tetrachloroethene
127-18-4
1, 1, 1—Trichloroethane
7
1—55—6
Benzene
71—43—
2
Aniline
62—53—3
Diphenylainine
22-39-4
Diphenylnitrosamine
86-30-6
Sum of Diphenylamine.
and
Diphenylnitrosamine
Nitrobenzene
98-95-3
Phenol
108—95—2
Cyclohexanone
108-94-1
Nickel
7440—02—
2
Arsenic
7440—38—
2
Benzene
71—43—2
Chlorobenzene
108-90-7
o-D.ichlorobenzene
95—50-1
m-Dichlorobenzene
541-73—1
p-Dichlorobenzene
106-46-7
1, 2,4—Trichlorobenzene
120—82—1
S
0.057
S
0.046
S
0.055
S
0.056
5
0.054
S
0.14
S
0.81
S
0.52
S
0.40
NA
5
0.068
0.039
0.36
0.47
0.79
S
0.14
s
0.057
S
0.088
S
0.036
S
0.090
S
0.055
a
6.2
a
6.2
a
30.
a
6.2
a
6.2
a
6.6
a
14.
NA
NA
a
14.
a 14.
a
5.6
a 30.
NA
NA
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
121—496
348
__________________
_____
____
a
4.4
___________
3
___________________
608—93—5
0.055
a
4.4
_________________
118—74—1
s
0.055
a
4.4
____________
12674—
S
0.013
a
0.9
11—2
____________
11104—
0.014
a
0.92
28—2
____________
11141—
S
0.013
a
0.92
16—5
____________
53469—
~
0.017
a
0.92
21—9
____________
12672—
~
0.013
a
0.92
29—6
____________
11097—
s
0.014
a
1.8
69—1
____________
11096—
S
0.014
a
1.8
82—5
____
____
________
67—64—
_____
______
1
Acetophenone
96-86-2
_____
~is (2—ethylhexyl)
-
117—81—
____
_____
phthalate
2
n-Butyl alcohol
71-36-3
Butylbenzylphthalate
85—68-7
_____
cyclohexanone
108-94-1
____
1
,
2-Dichlorobenzene
95—50—1
_____
Diethyl phthalate
84—66—2
____
_____
Pimethyl phthalate
131-11-3
_____
_____
Di-n-butyl phthalate
84-74-2
_____
_____
Di-n-octyl phthalate
117-84-0
_____
_____
Ethyl acetate
141—78—6
____
_____
Ethylbenzene
100—41—4
_____
Methanol
67—56—1
Methyl isobutyl ketone 108—10-1
____
_____
Methyl ethyl keton
78—93—3
____
_____
Methylene chloride
75-09—2
_____
_____
Naphthalene
91—20-3
_____
Nitrobenzene
98—95—3
_____
_____
Toluene
108—88—3
____
_____
1,1, l—Trichloroethane
71—55—6
_____
Trichloroethylene
79—01—6
_____
Xylene(s)
(TotaJi
____
_____
Cyanides
(Total)
57—12—5
Chromium (Totalj
7440—47—
____
32
Lead
7439—92—
_____
1
1087
Table
Acenaphthalene
208—96-
a
0.028
3.4
A
95—94—
~
0.055
1,2,4
,
5—Tetrachloro—
benzene
Pentachlorobenzene
Hexachlorobenzene
Aroclor 1016
Aroclor
1221
Aroclor
1232
Aroclor
1242
Aroclor
1248
Aroclor
1254
Aroclor 1260
1086
Table
Acetone
A
0.28
a160.
0.010
a
9.7
s
0.28
a
28.
5.6
S
0.017
0.36
0.088
S
0.20
S
0.047
s
0.057
S
0.017
S
0.34
S
0.057
S
5.6
0.14
0.28
S
0.089
5
0.059
5
0.068
S
0.080
S
0.054
S
0.054
5
0.32
1.9
0.32
a
2.6
a
7.9
NA
a
6.0
a
28.
a 28.
a
28.
a 28.
a 33.
a
6.0
NA
a
33.
a
36.
a 33.
a
3.1
a 14.
a 28.
a
5.6
a
5.6
a 28.
1.5
NA
0.037
NA
12 1—497
349
K093
Phtha 1Ic anhydride
(measured as Phthalic
acid)
85—44—9
a
0.54
a
28.
1094
Phthalic anhydride
(measured as Phthalic
acid)
85—44—9
a
0.54
a
28.
Hexachlorocyclopenta-
77-47-
diene
Chlordane
57—74—9
Heptachior
76-44—8
Heptachlor
epoxide
1024-57-
1098
Toxaphene
8001—35—
1
0.0095
a
2.6
1099
2, 4-Dichloro—
phenoxyacetic acid
94—75—7
a
1.
a
1.
Ben~ene
ChrySene
Fluoranthene
Indeno(1,2,3—cd)pyrenel93—39—5
71—43—2
218-01-9
206—44—0
a
a
a
~
~
a
a
0.014
0.028
0.028
0.028
0.028
0.028
0.008
a
a
a
~
~
a
a
0.071
~j
3.4
~j
~
3.4
0.65
Naphthalene
Phenanthrene
91-20—3
85-01-8
108—88—3
Toluene
Xylene(s)
0.014
a
0.07
7439—92—
0.037
NA
1
1,1,1, 2—Tetrachioro-
ethane
1,1,2,
2—Tetrachloro-
ethane
Tetrach1oroethene
1,1, 2—Trichloroethane
Trichloroethylene
0.057
a
5.6
0.057
a
5.6
1095
1096
1097
0. 056
0. 054
0. 054
0
.
055
o
.
055
a
6.0
a
6.0
a
5.6
a
28.
a
5.6
Hexachloroethane
Pentach1oroethane
1,1,1,2-Tetrachloro—
ethane
1, 1 .2 ,2—Tetrachloro—
ethane
Tetrachioroethene
1,1,2-Trichloroethane
Trichloroethene
630—20—
6
79—34—
6
127—18—4
79—00—5
79—01—6
67—72—1
76—01—7
63 0—20—
6
79—34—
6
127—18—4
79—00—5
79—01—6
541—73—1
76—01—7
0.057
a
5.6
0.057
a
5.6
1, 3—Dichlorobenzene
Pentachioroethane
1,2,
4-Trichlorobenzene
12 0-82-1
0. 056
0. 054
0.054
0.036
0. 055
0. 055
a
6.0
a
6.0
a
5.6
a
5.6
a
5.6
a 19.
s
0.057
-
2.4
3
.a_
0.0033
S
0.0012
S
0.016
a
0.26
a
0.066
a
0.066
121—498
350
K100 Table
A
Hexachlorodibenzo—p—
dioxins
Hexachlorodibenzo—
furanS
Pentachlorodibenzo-p-
dioxins
Pentachlorodibenzo—
furans
Tetrachlorodibenzo-p-
dioxins
Tetrachlorodibenzo-
furans
Cadmium
Chromium
(Total)
Lead
7440—43—
9
7440—47—
32
7439—92—
1
a
a
a
a
a
a
0.001
0.001
0.001
0.001
0.001
0.001
1.6
0.32
0.51
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
a
0.001
NA
NA
NA
a
14.
NA
NA
NA
NA
a
13.
NA
NA
NA
NA
5.6
a
6.0
a
5.6
a
5.6
a
5.6
a
5.6
a
6.0
a
5.6
a
5.6
a
5.6
o-Nitroaniline
Arsenic
Cadmium
Lead
Mercury
o-Nitrophenol
Arsenic
Cadmium
Lead
Mercury
Aniline
Benzene
_______
eno1
Nitrobenzene
Phenol
Aniline
Benzene
2~4-Dinitrophenol
Nitrobenzene
Phenol
K102 Table
A
1103
1104
744 0—3 8—
2
744
0—4 3—
9
7439—92—
1
7439—97—
6
7440—38—
2
7440—43—
9
7439—92—
1
7439—97—
6
62—53—3
71—43—2
—28—5
98—95—3
108—95—2
62—53—3
71—43—2
51—28—5
98 —95—3
108 —9 5—2
a
0.27
0.79
0.24
0.17
0.082
a
0.028
0.79
0.24
0.17
0.082
a
4.5
a
0.15
a
0.61
a
0.073
a
1.4
a
4.5
a
0.15
a
0.61
a
0.073
a
1.4
12 1—4 99
351
2.7
Treatment standards for this organic constituent were
established based upon incineration
in units operated in
accordance with the technical requirements of 35
Ill.
Adm.
Code 724.Subpart 0 or 725.Subpart
0,
or based upon
combustion in fuel substitution units operating in
accordance with applicable technical requirements. A
facility may certify compliance with these treatment
standards according to provisions
in Section 728.107.
Based
on analysis of composite Samples.
j1~j
As
analyzed
using
SW—846
Method
9010;
sample
size:
0.5—10;
distillation time:
one hour to one hour and fifteen
minutes.
NA
Not
Applicable.
TABLE B
(CCW):
P
AND
U
LISTED
WASTES
Commercial
Wast Chemical
e
Name
Code
Regulated
See
Hazardous
Also
Constituent
CAS
No.
for
Concentration
(mg/l)
Regulated
Non-
Hazardous Wastewatei~stewaters
Const itue
nt
POll Arsenic
Table
pentoxide
A
1105
CyaniideS
(Total)
57—12—5
71—43—2
Benzene
Chlorobenzene
108—90-7
95-50-1
106-46—7
95—95—4
88—06—2
95-57-8
108—95—2
o-Dichlorobenzene
p—Dichlorobenzene
2 .4
,
5—Trichlorophenol
2
,
4
,
6—Trichlorophenol
2-Chlorophenol
Phenol
1106
Tables
A&D
Mercury
7439—97—
.~
1115
Table
A
Nickel
7440—02—
a
0.14
0. 057
0.088
0.090
0.18
0.035
0.044
0.039
0.030
0.47
a
1.8
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
a
4.4
NA
NA
P004 Aldrin
POlO Arsenic
acid
Table
A
Aldrin
309—00—
2
Arsenic
7440—38—
2
Arsenic
7440—38-
2
0.21
0.79
.066
NA
0.79
NA
12 1—500
352
P012 Arsenic
Table
Arsenic
7440-38-
0.79
NA
trioxide
A
a
P013 Barium
Table
Cyanides
57—12—5
110.
cyanide
A
(Totall
57—12—5
Q~J~
(Amenable)
P020 2—sec—
2—Sea—
88—~5~
0.066
*
~5
Butyl-4,6-
Butyl-4,6-
2.
dinitro-
dinitro-
phenol
phenol
(Dinoseb)
(DinoSeb)
P021 Calcium
çyanides
57—12—5
110.
cyanide
(Total)
Cyanides
57—12—5
.Q~j,.
lAmenable)
P022 Carbon di-Table
Carbon di-
75—15-0
0.014
NA
sulfide
D
sulfide
P024 p—Chloro—
p—Chloro—
106—47—8
0.46
*
16.
aniline
aniline
P029 Copper
Cyanides
57—12—5
LA
110.
cyanide
(Total)
Cyanides
57-12—5
(Amenable)
P030 çy~jdes
Cyanides
57—12-5
LA
ljQ~
(soluble
(Total)
salts and
complexes)
Cyanides
57—12-5
(Amenable)
P036 Dichloro—
Table
Arsenic
7440—38—
0.79
NA
phenyl-
A
a
ars me
P037 Dieldrin
Dieldrin
60—57—1
~
~
*
0.13
P038 Diethyl-
Table
Arsenic
7440-38—
0.79
~LA
arsine
A
a
P039 Disulfoton
Disulfoton
298-04~4
0.017
*
~.1
P047 j,6—Di—
4,6—Di—
534—52—
*
0.28
*160.
nitro—o—
nitro—o—
4
cresol
cresol
12 1—501
353
P048 2,4—Di—
2,4—Di—
51—28—
*
0.12
*160.
nitro-
nitrophenol 5
phenol
P050 Endosulfan
Endosulfan
939—98—
*
0.023
*
0.066
I
-~
Endosulfan
33213—
*
0.029
*
0.13
II
6—
5
Endosulfari
1031—07—
*
0.029
*
0.13
sulfate
B
P051 Endrin
Endrin
72—20—8
*
0.0028
*
0.13
Endrin
7421—93—
*
0.025
*
0.13
aldehyde
4
P056 Fluoride
Table
Fluoride
18694-
35.
NA
P
48—8
P059 Heptachior
Heptachlor
76—44—8
~
0.0012
~
0.066
Heptachlor
1024—57—
~
0.016
~
0.066
epoxide
3
P060 Isodrin
Isodrin
465—73—6
*
0.021
*
0.066
P063 Hydrogen
Cyanides
57—12—5
LA
110.
cyanide
(Total)
Cyanides
57—12—5
0.10
(Amenable)
P065 Mercury
Tables Mercury
7439-97-
0.030
NA
fulminate
A
&
D
6
P071 Methyl
Methyl
298—00—0
0.025
~
parathion
parathion
P073 Nickel
Table
Nickel
7440—02—
0.44
NA
carbonyl
A
a
P074 Nickel
Table
Cyanides
57—12—5
-
110.
cyanide
A
(Table)
Cyanides
57—12—5
0.10
(Amenable)
Nickel
7440—02—
0.44
NA
2
P077 p—Nitro—
p—Nitro—
100—01—6
*
0.028
*
28.
aniline
aniline
121—502
354
P082 N-Nitroso-fable
N—Nitroso-
62—75-
*
0.40
NA
dimethyl-
p
dimethyl-
2
amine
amine
P089 Parathion
Parathion
56—38-2
0.025
*
~
P092 Phenyl-
Tables Mercury
7439—97~
0.030
NA
mercury
A
& D
acetate
P094 Phorate
Phorate
298—02—2
0.025
*
0.1
P097 Famphur
Fainphur
52-85-7
0.025
*
0.1
P098 Potassium
Cyanides
57—12—5
LA
110.
cyanide
~Total)
Qyanides
57—12—5
0.10
9.1
(Amenable)
~
Potassium
Table
Cyanides
57—12-5
LA
110.
silver
A
(Total)
cyanide
Cyanides
57-12-5
(Amenable)
Silver
7440—22—
0.29
NA
4
P101 Ethyl
Ethyl
107—12—0
~.
0.24
*360.
cyanide
cyanide
IPropane—
(Propane-
nitrile)
nitrile)
P103 Seleno-
Table
Selenium
7782—49—
*
~
NA
urea
a
P104 Silver
Table
Cyanides
57—12—5
LA
110.
cyanide
A
(Total)
Cyanides
57—12—5
0.10
(Amenable)
Silver
7440—22—
0.29
NA
4
P106 Sodium
Cyanides
57—12—5
LA
110.
cyanide
(Total)
çy~njdes
57—12—5
0. 10
9.1
(Amenable)
P110 Tetraethyl Tables Lead
7439—92—
0.040
NA
lead
A&D
1
P113 Thallic
Table
Thallium
7440-28-
*
0.14
NA
oxide
P
0
121—503
355
P114 Thallium
Table
selenite
A
Selenium
7782—49-
a
LA
NA
P115 Thallium(ITable
)
sulfate
P
Thallium
7440—28—
0
*
0.14
NA
P119 Ammonia
Table
vanadate
P
Vanadium
7440—62-
a
*
28.
NA
P120 Vanadium
Table
pentoxide
P
Vanadium
7440—62—
a
*
28.
NA
P121 Zinc
cyanide
Cyanides
(Total)
Cyanides
I
Amenable)
57—12—5
57-12—5
LA
0.10
110.
P123 Toxaphene
Toxaphene
8001-35-
1
0.0095
LA
U002 Acetone
Acetone
67—64—1
0.28
*160.
U003 AcetonitriTable
P
Acetonitril
~
75-05-
~.
0.17
NA
U004 Acetopheno
n~
Acetophenon
~
98-86-
a
*
0.010
*
9.7
U005 2—Acetyl—
amino—
fluorene
2—Acetyl—
amino—
fluorene
53—96—3
*
0.059
*140.
U009 Acrylo—
nitrile
Acrylo—
nitrile
107—13—1
*
0.24
*
84.
U012 Aniline
Aniline
62—53—3
0.81
*
14.
U0l8
Benz(a)—
anthracene
Benz
(a)—
anthracene
56—55—3
*
0.059
*
3~
U019
Benzene
Benzene
71—43—2
*
0.14
*
36.
U022
Benzo(a)—
pyrene
Benzo(a)—
pyrene
50—32—8
*
0.061
*
5~
U024 Bis(2—
chloro—
ethoxy)-
methane
Bis(2—
chloro—
ethoxy)-
methane
111—91—1
0.036
*
7.2
12 1—504
356
U025 Bis(2—
Bis(2—
111—44—
0.033
~
chioro—
chloro—
4
ethyl)
-
ethyl)
-
ether
ether
U027 Bis(2—
Bis(2—
39638—
*
0.055
*
7~
chloro-
chloro-
32-9
isopropyl)
isopropyl)
ether
ether
U028 Bis(2—
Bis(2—
117—81—
*
0.54
*
28.
ethyl-
ethylhexyl)
2
hexyl)
pthalate
pthalate
U029 Bromometha
Bromomethan 74-83-9
*
~
*
15.
ne
(Methyl
e
(Methyl
bromide)
bromide)
U030 j~
4—
101—55—
*
0.055
*
Bromopheny
Efromophenyl
3
I phenyl
phenyl
ether
ether
U031 n-Butyl
n-Butyl
71-36-3
alcohol
alcohol
U032 Calcium
Table
Chromium
7440-47—
0.32
NA
chromate
A
(Total)
Ia
U036 Chlordane
Chlordane
57—74—9
*
0.00033*
0.13
(alpha and
(alpha and
gamma)
gamma)
U037 Chloro-
Chioro—
108—90—7
*
0.057
*
5~7
benzene
benzene
U038 Chioro-
Table
Chloro—
510-15-6
*
0.10
NA
benzilate
P
benzilate
U039 p—Chloro-
p—Chloro—
59—50—7
*
0.018
*
14.
m—cresol
m—cresol
U042
2-Chloro—
Table
2—Chioro-
110—75—
0.057
NA
ethyl
p
ethyl vinyl ~
vinyl
U043 Vinyl
Vinyl
75—01—4
*
0.27
*
33.
chloride
chloride
U044 Chloro-
Chloroform
67-66-
~
0.046
~
form
3
121—505
357
U045 Chloro-
methane
(Methyl
chloride)
Chloro-
methane
(Methyl
chloride)
74—87—3
*
0.19
*
33.~
U047 2—Chioro—
naphthalen
e
2-Chloro-
91-58—
naphthalene
2
*
0.055
*
5.6
U048 2—Chioro—
phenol
2 -Chloro-
~heno
1
95—57—8
*
0.044
*
5.7
U050 Chrysene
Chrysene
218—01—9
*
0.059
*
8.2
U052 Cresols
(Cresylic
acid)
o—Cresol
Cresols
(in—
and
p-
isomers)
95—48—7
108—94—1
*
0.11
*
0.77
*
5.6
*
3.2
0.36
NA
U060 DDD
p,p’-DDD
53—19—0
72—54—8
0.023
*
0.087
0.023
*
0.087
U06l DDT
o,p’ -DDT
p,p1-DDT
o,p’-DDD
p,p’-DDD
o,p’-DDE
p,p’-DDE
789—02 —6
50—29—3
53—19—0
72—54—8
3424—82—
6
72 —55—9
0.0039
±~~_
0.0039
0.023
0.023
*
0.031
*
0.031
*
0.087
*
0.087
*
0.087
*
0.087
*
0.087
*
0.087
U051 Creosote
Naphthalene 91—20—
3
Penta—
87—86—
chloro-
5
phenol
Phenanthren 85—01-
e
Pvrene
Toluene
Xv1ene
S
(Total)
Lead
*
0.031
*
0.18
*
0.031
*
0.028
*
0.028
*
0.032
*
0.037
Table
A
Table
D
*
1.5
*
7~4
*
1.5
*
28.
*
33.
NA
NA
8
129—00—0
108—88—3
7439—92—
1
U057 Cyclo-
hexanone
Cyclo-
hexanone
121—506
358
U063 Dibenzo-
Dibenzo—
53—70—3
*
0.055
*
(a,h)-
anthracene
anthracene
U066
l,2—Di—
1,2—Di—
96—12—
*
0.11
*
bromo-3-
broino-3-
chloro—
chloro—
p~c~p~n~
propane
U067 1,2—Di—
1,2—Di—
106—93—
*
0.028
*
15.
bromoethan
bromoethane
4
e
j~thy1ene
~~hylene
dibromide)
dibromide)
U068
Dibromo-
74-95-3
~
0.11
15.
ethan~
bromoethane
U069 Di-n-butyl
Di-n-butyl
84-74-2
~
0.54
*
28.
pi~t~
phthalate
U070 o-Di-
o-Dichloro- 95-50-
~
chlor~
benzen~
1
benzene
U071
m—Di—
m-Dichloro— 541—73—
0.036
chlor~
benzene
.1.
benzene
U072
p~J~iz
p-Dichloro- 104-46-
~
0.090
*
6.2
____
benzene
2
benzene
U075
Dichloro-
Dichloro-
75-71-8
*
0.23
*
7~
difluoro-
difluoro-
methane
methane
U076 1,1—Di—
1,1—Di—
75—34~
~
0.059
chloro-
chloro—
ethane
ethan~
U07
1, 2
-D.i~.
1,2-0 i
-
107
-~
~
0~2i
~
Li
chioro-
ch1or~
a
eth ane
eth~ri~.
U078
1,1—Di—
75—35—4
*
0.025
~
chioro-
chloro-
ethylene
U079 ~~Qj—
trans—1,2—
156—60—5
~
0.054
33.
X
chloro—
Dichloro—
~y~ne
~~ne
12 1—507
359
U080 Methylene
Nethylene
75—08—2
0.089
Y
33. X
chloride
chloride
U081
2,4—Di—
2,4—Di—
120—83—
0.044
Y
14.
X
chioro—
chloro—
a
phenol
phenol
U082 2,6—Di—
2,6—Di—
87—65—
0.044 Y
14.
X
chloro—
chioro—
0
phenol
phenol
U083 1,2—Di—
1,2—Di—
78—87—5
0.85 Y
18. X
chloro—
chioro—
propane
propane
U084 1,3—Di—
cis—1,3—
10061—
0.036
Y
18.
X
chloro-
Dichioro-
01-5
propene
propylene
trans—1,3—
10061—
0.036
Y
18.
X
Dichloro-
02-6
propylene
U088 Diethyl
Diethyl
84—86—2
0.54 X
28.
X
phthalate
phthalate
U093 p—Di—
Table
p-Dimethyl- 60—11—
0.13 Y
NA
methyl-
~
aminoazo-
2.
arninoazo—
benzene
benzene
U101
2,4—Di—
2,4—Di—
105—67—
0.036
Y
14.
X
methyl-
methyl-
2
phenol
phenol
Ul02 Dimethyl
Dimethyl
131-11-3
0.54 X
28.
X
phthalate
phthalate
U105 2,4—Di—
2,4—Di—
121—14—
0.32
Y
140.
X
nitro-
nitro-
a
toluene
toluene
U106 2,6—Di—
2,6—Di—
606—20—
0.55 Y
28.
X
nitro-
nitro-
a
toluene
toluene
U107 Di—n-octyl
Di—n—octyl
117—84-0
0.54 X
28.
X
phthalate
phthalate
U108 1,4—
l,4—Dioxane 123—91—
0.12 ~
170.
X
Dioxane
1
121—508
360
Ulli Di-n-
propyl-
nitroso—
amine
U1l2 Ethyl
acetate
acetate
141—78—6
0.34 Y
33.
X
U117 Ethyl
ether
Ul18
Ethyl
meth-
acrylate
U120 Fluoranthe
ne
Ul21 Trichloro-
inonofluoro
methane
U127 Hexa—
chloro-
benzene
U128 Hexa—
chloro—
butadiene
Ethyl ether 60—29-
7
Ethyl meth- 97-63-
acrylate
a
Fluoranthen 206—44-
P
Trichloro—
75—69—4
monofluoro-
methane
Hexachloro- 118-74-
benzene
I
Hexachioro— 87—68—
butadiene
.3
0.12 Y
160.
X
0.14 Y
160.
X
0.068 Y
0.02-0
‘1
0.055 Y
0.055 Y
8.2 ~
33.
X
37.
X
28.
X
U129 Lindane
alpha-BHC
beta-BHC
Delta—BHC
gamma
-
BHC
(Lindane)
319—84—6
319—85—7
319—86—8
58—89—9
Y
0.00014
0.00014
0.023
0.0017
0.066
X
0.066
1
0.066 X
0.066
1
U130 Hexa-
chloro-
cyclo-
pentadiene
Hexachloro—
77—47—
cyclopenta-
2
diene
0.057
Y
3.6 X
U13l
Hexa-
chloro—
ethane
E~~iiioro—
67—72—
ethane
0.055 Y
28.
X
U134 Hydrogen
fluorIde
Table
Fluoride
D
Ul36 Cacodylic
Table
acid
A
0.79
NA
Di—n—
621—64—
0.40
Y
14.
X
propyl-
I
nitroso—
amine
16964—
48—8
Arsenic
7440—38—
2
NA
12 1—509
361
U137 Indeno-
(1,2,3—
c,d)—
pyrene
Indeno—
(1, 2
,
3—
c
,
d) pyrene
0138 lodomethan
e
lodomethane 74-88-
4
0.19 Y
65.
X
Isobutyl
78—83—1
alcohol
U141 Isosafrole
Isosaf
role
120—58—1
0.081
2.6 X
U142 Kepone
Kepone
143—50-8
0.0011
0.13 X
U145 Lead
Table
phosphate
A
Lead
7439—92—
1
Lead
7439—92—
1
0.040
NA
0.040
NA
0146 Lead
Table
subacetate
A
Lead
7439—92—
1
0.040
NA
U15l Mercury
Tables Mercury
A&D
7439—97—
6
0.030
NA
U152 Meth-
acrylo-
nitrile
U155 M~j~pril
ene
Methacrylo- 126—98—
nitrile
2
Methapyrile 91-80-5
ne
0.24 Y
84.
X
0.081
L.5 X
U157 3-Methyl—
cholanthre
ne
3—Methyl—
56-49-
cholanthren
5
e
Y
0.0055
15.
X
U158 4,4’—
Methylene-
bis(2—
chloro—
4,—
aniline)
Methylene-
bis(2—
chloro—
aniline)
101—14—
4
0.50 Y
35.
X
0159 Methyl
ethyl
ketone
Ul61 Methyl
isobuty 1
ketone
Methyl
ethyl
ketone
78—93—
3
Methyl
108—10—1
isobutyl
ketone
193—39—
0.0055
-~
I
8.2 X
Ul40 Isobutyl
alcohol
170.
X
Ul44
Lead
acetate
Table
A
0.28
36.
X
0.14
33.
X
12 1—5
10
362
Ul62 Methyl
Methyl
80—62—
0.14
160.
X
methacryla
methacrylat
6
U165
Naphthalen
Naphthalene 91-20—
0.059
Y
3.1 X
U168 ~
Table
2-Naphthyl- 91—59—
0.52 Y
NA
~p~yi-D
amine
2
amine
0169 Nitro—
Nitro—
98—95—
0.068 Y
14. X
benzene
benzene
3
Ul70 4—NitrQ~
4—Nitro—
100—02—7
0.12 Y
29.
X
piiQflcl2.
phenpi
U172
N—Nitroso—
N—Nitroso-
924-16—
0.40
Y
17.
X
di-n-
di-n-butyl-
3
butylamine
amine
0174 N-Nitroso—
N-Nitroso-
55-18-
0.40
Y
28.
1
diethyl-
amine
amine
U179 N-Nitroso-
N-Nitroso-
100-75-4
0.013
Y
35.X
piperidine
piperidine
U180 N-Nitroso-
N-Nitroso-
930—55—
0.013
Y
35. X
pyrrolidin
pyrrolidine
a
e
0181 5—Nitro—
5—Nitro—
99—55—
0.32
Y
28. .X
2
toluidine
toluidine
U183 Penta—
Penta—
608—93—
0.055 Y
37. X
chlor.ip~
chloro-
5
benzene
benzene
U185 Penta—
Penta—
82—68—
0.055 Y
j~X
chloro-
chloro—
8
nitr
nitro-
benzen~
benzene
Ul87 Phenacetin
Phenacetin
62—44—2
0.081
16.
X
0188 Phenol
Phenol
108—95—2
0.039
6.2 X
121—511
363
Ul90 Phthalic
Phthalic
85—44-
0.54 X
28.
X
anhydride
anhydride
2
(measured
(measured
as
as Phthalic
Phthalic
acid)
acid)
0192
Pronainide
Pronamide
23950—
0.093
1.5 X
58—5
0196 Pyridine
Pyridine
110-86-1
0.014 Y
16.
X
0203 Safrole
Safrole
94—59—7
0.061
22.
X
0204 Selenium
Table
Selenium
7782—49—
1.0
NA
dioxide
A
a
U205 Selenium
Table
Selenium
7782—49-
LA
NA
sulfide
A
a
0207 1,2,4,5—
1,2,4,5—
95—94—
0.055 Y
19. X
Tetra-
Tetra-
3
chloro-
chloro-
benzene
benzene
0208
1,1,1,2—
1,1.1,2—
630—20—
0.057
42.
X
Tetra-
Tetra-
chloro—
chloro—
ethane
ethane
0209 1,1,2,2—
1,1,2,2—
79—34—
0.057 Y
42.
X
Tetra-
Tetra-
chloro—
chloro—
ethane
ethane
0210 Tetra—
Tetra—
127—18-
0.056 Y
5.6 X
chioro—
chloro—
4
ethylene
ethylene
0211 Carbon
Carbon
56—53—5
0.057
Y
5.6 X
tetra-
tetra—
chloride
chloride
0214
Tallium(I)
Table
Thallium
7440—28—
0.14
Y
NA
acetate
P
0
0215 Thallium(ITable
Thallium
7440—28—
0.14 Y
NA
I
p
p
carbonate
0216 Thallium(ITable
Thallium
7440—28—
0.14 Y
NA
-
)
chloride
p
p
121—512
364
U2l7 Thallium(ITable
Thallium
7440-28—
0.14 Y
NA
nitrate
P
0
U220 Toluene
Toluene
108—88—3
0.080 Y
28.
X
U225 Tribromo-
Tribromo-
75-25-
0.63 Y
15.
X
methane
methane
a
(Bromoform)
0226 Ll,~~~i—
1,1,1—Tn—
71—55—
0.054
Y
5.6
X
chloro—
chloro—
6
ethane
ethane
U227 Ll,2—Tri—
1,1,2—Tn—
79—00—
0.054 Y
5.6
1
chloro—
chloro—
5
ethane
ethane
0228 Tnichloro-
Tnichloro—
79—01—6
0.054
Y
5.6 X
ethylene
ethylene
U235 ~
tris—(2,3—
126—72—7
0.025
0.10 X
Dibromo—
Dibromo-
propyl)-
propyl)-
phosphate
phosphate
0239 Xylenes
Xylene
a
0.32 Y
28.
1
U240 ~,4—Di—
2,4—Di—
94—75—
0.72
10. X
chloro—
chloro—
2
phenoxy—
phenoxy—
acetic
acetic acid
acid
U243
Hexa—
Hexachloro- 1988—71—
0.095 Y
28.
chloro—
propene
2
propene
0247 Methoxy—
Methoxy—
72—43-
0.25
Y
0.18
X
chlor
chior
x
Treatment standards for this organic constituent were
established based ~~pon incineration in units operated in
accordance with the technical requirements of
35 Ill.
Adrn.
Code_724.Subpart
0 or 725.Subpart
0,
or based upon
combustion
in fuel substitution units operating
in
accordance with applicable technical requirements. A
facility may certify compliance with these treatment
standards according to provisions
in Section 728.107.
Y
Based on analysis of composite samples.
12 1—513
365
Z
As analyzed using SW—846 Method
9010.; sample size:
0.5—10;
distillation
time:
one
hour
to
one
hour
fifteen
minutes.
NA
Not
Applicable.
(Source:
Amended at 15
111.
Reg.
,
effective
121—5 14
366
Section 728.Tabie C Technology
Codes and Description
of
Technology-Based Standards
Technology
code Description of technology-based standard
ADGAS
Venting of compressed~ases into an absorbing
or
reacting media
(i.e., solid or liguid)——venting can be
accomplished through
physical release utilizing
values/piping; physical penetration
of the container;
and/or penetration through detonation.
AMLGM
Amalgamation
pf
liquid,
elemental mercury contaninated
with
radioactive materials utilizing inorganic
reagents such as
copper,
zinc,
nickel,
gold,
and
sulfur that result
in a
nonliquid,
semi-solid amalg.~
and thereby reducing potential
emissions
of elemental
mercury vapors to the air.
BIODG
Biodegradation of organics or non-metallic inorganics
(i.e.,
degradable inorganics that contain the elements
of phosphorus,
nitrogen,
and sulfur)
in
units
operated
under either aerobic or
anaerobic conditions such that
a surrogate compound or indicator
parameter has been
substantially reduced in concentration
in the
residuals
(e.g., Total Organic Carbon can often be used
as an
indicator parameter
for the biodegradation
of
many organic
constituents that cannot be directly
analyzed
in wastewater
residues).
CARBN
Carbon adsorption
(granulated or powdered)
of
non—metallic
inor~.g~.pics,organo—metallics,
and/or
organic constituents,
operated such that
a surrogate
compound or indicator parameter
has not undergone
breakthrough~(~e.g.,Total Organic Carbon can
often
he
used
as
an
indicator
parameter
for
the
adsorption
of
many organic constituents that cannot be directly
analyzed in
wastewater residues).
Breakthrough occurs
when the carbon has
become saturated with the
constituent
(or indicator parameter)
and substantial
change
in adsorption rate associated with that
constituent occurs.
CHOXD
Chemical or electrolytic oxidation u~~,1j,z
ing
following
oxidation reagents
(or waste reagents)
or
combinations or
reagents:
jj
Hypochlonite
(e.g.
bleach)
~j
chlorine
31
chlorine
dioxide
12 1—5 15
367
iL
ozone or UV (ultraviolet light) assisted ozone
~j
peroxides
~j
persulfates
31
perchlorate~j~
~j
permangantes; and/or
~j
othe-r
oxidizing
reagents
of
equivalent
efficiency1
performed
in
units
operated
such
that
a
Surrogate
compound
or
indicator
parameter
has
been
substantially
reduced
in
concentration
in
the
residuals
(e.g.,
Total
Organic Carbon
can often be used as an indicator
parameter
for
the
oxidation
of
many
organic
constituents
that
cannot
be
directly
analyzed
in
wastewater
residues).
Chemical
oxidation
specifically
includes
what
is
commonly
referred
to
as
alkaline
chlorination.
CHRED
Chemical reduction utilizing the following reducing
reagents
(or
waste reagents)
or combinations of
reagents:
fl
Sulfur dioxide
31
sodium, potassium,
or alkali salts of sulfites,
bisulfites,
metabisulfites,
and polyethylene glycols
(e.g.,
NaPEG and KPEG)
31
sodium hydrosulfide
il
ferrous
salts;
and/or
~J
other reducing reagents
of
equivalent
efficiency,
performed in units
operated such
that
a surrogate
compound
or
indicator
parameter
has been substantially
reduced
in
concentration
in
the
residuals
(e.g.,
Total
Organic
Halogens
can
often
be
used
as
an
indicator
parameter
for
the
reduction
of
many
halogenated
organic
constituents
that
cannot
be
directly
analyzed
in
wastewater
residues).
Chemical
reduction
is
commonl.y
used
for
the
reduction
of
hexavalent
chromium
to
the
trivalent
state.
DEACT
Deactivation to remove
the
hazardous
characteristics
of
a waste
due to
its ignitability, corrosivity,
and/or
reactivity.
FSUBS
Fuel substitution
in units operated
in accordance
with
applicable
technical operating requirements.
12 1—516
368
HLVIT
Vitrification of high level mixed radioactive wastes
in
units
in
compliance with all applicable radioactive
protection
requirements under control
of the Nuclear
Regulatory Commission.
IMERC
Incineration of wastes containing oraanics and mercury
in units
operated in accordance with the technical
operating requirements
of
35
Ill. Adm.
Code
724.Subpart 0 or 725.Subpart 0.
All wastewater and
nonwastewater residues derived from this
process must
then comply with the corresponding treatment
standards
per waste code with consideration of any applicable
subcategories
(e.g., High or Low Mercury
Subcategories).
INCIN
Incineration
in units operated in accordance with the
technical
operating requirements of 35
Ill.
Adin.
Code
724.Subpart 0 or 725.Subpart 0.
LLEXT
Liquid-liquid~extraction
(often referred toas
solvent
extraction)
of organics from liquid wastes into an
immiscible
solvent for which the hazardous
constituents have a greater
solvent affinity,
resulting
in an extract high in organics that
must
undergo either incineration, reuse as a fuel,
or other
recovery/reuse and a raffinate
(extracted liquid waste)
proportionately low in organics that must undergo
further
treatment as specified in the standard.
MACRO
Macroencapsulation with surface coating materials such
as
polymeric organics
(e.g.
resins a~dplastics)
or
with
a lacket
of inert inorganic materials to
substantially reduce surface
exposure to potential
leaching media. Macroencapsulation
specifically does
not include any material that would be
classified
as
a
tank or container according to 35
Ill.
Adm.
Code
720. 110.
NEUTR
Neutralization with the following reagents
(or waste
reagents)
or combinations of reagents:
fl
Acids
31
bases; or
31
water
(including wastewaters)
resulting
in
a pH
greater than
2 but
less than 12.5 as measured
in the
aqueous residuals.
NLDBR
No land disposal based on recycling.
121—5
17
369
PRECP
Chemical precipitation of metals and other inorganics
as
insoluble precipitates of oxides, hydroxides,
carbonates,
sulfides, sulfates, chlorides, flourides,
or phosphates. The
following reagents
(or waste
reagents) are typically used alone
or in combination:
fl
Lime
(i.e.,
containing oxides and/or
hydroxides of
calcium and/or magnesium
31
caustic
(i.e.,
sodium and/or potassium hydroxides
31
soda ash
(i.e., sodium
carbonate)
4j
sodium sulfide
~j
ferric sulfate or ferric
chloride
~j
alum;
or
31
sodium sulfate. Additional
floculating, coagulation,
or similar reagents/processes that
enhance sludge
dewatering characteristics are not precluded from
use.
RBERY
Thermal recovery of Beryllium.
RCGAS
Recovery/reuse of compressed gases including techniques
such as
reprocessing of the gases for reuse/resale;
filtering/adsorption
of impurities; remixing for
direct reuse of resale;
and use of
the gas as a fuel
source.
RCORR
Recovery of acids or bases utilizing one or more of the
following
recovery technologies:
Distillation
(i.e., thermal
concentration)
31
ion exchange
31
resin
or
solid
adsorption
j)
reverse osmosis; and/or
~j
incineration for the recovery of
acid-—Note:
this does
not preclude the use of other physical
phase
separation or concentration techniques such
as
decantation. filtration
(including ultrafiltration)~
and
centrifugation, when used in con-junction with the
above listed
recovery technologies.
RLEAD
Thermal recovery of lead in secondary lead smelters.
121—518
370
RI4ERC
Retorting or roasting in a thermal processing unit
capable of volatilizing mercury and
subsequently
condensing the volatilized mercury for recovery. The
retorting or roasting unit
(or facility) must be
sub-ject to one or more of the following:
~j
A
National Emissions Standard for Hazardous Air
Pollutants
(NESHAP)
for mercury
(40 CFR 61, Subpart E)
~j
A Best Available Control Technology
(BACT)
or a Lowest
Achievable Emission Rate
(LAER)
standard for mercury
imposed pursuant to a Prevention of Significant
Deterioration
(PSD) permit
(including
35
Ill.
Adm.
Code
201
through
203);
or
çj
A state permit that establishes emission limitations
(within meaning of Section 302 of the Clean Air Act)
for mercury, including a permit issued pursuant to
35
Ill. Adm.
Code 201. All wastewater and nonwastewater
residues derived from this process must then comply
with the corresponding treatment standards per waste
code with consideration of any applicable subcategories
(~g.,High or Low Mercury Subcategories).
RMETL
Recovery of metals or inorganics utilizing one or more
of the
following direct physical/removal technologies:
3j
Ion exchange
31
resin or solid
(i.e.,
zeolites)
adsorption
31
reverse osmosis
~
chelation/solvent extraction
~j
freeze
crystalization
~j
ultrafiltration;
and/or
6 simple
precipitation
(i.e.,
crystalization)
Note: this does not
preclude the use of other physical
p~se separation
or
concentration techniques such as
decantation,
filtration
(including ultrafiltration),~and
centrifucation,
when used
in
con-junction with the
above
listed recovery technologies.
RORGS
Recovery of organics utilizing one or more of the
following
technologies:
fl
Distillation
31
thin film evaporation
121—519
371
31
steam stripping
il
carbon adsorption
~j
critical
fluid
extraction
~j
liquid-liquid extraction
31
precipitationf crystallization
(including freeze
crystallization);
or
31
chemical phase separation techniques
(i.e., addition of
acids,
bases,
demulsifiers,
or
similar
chemicals)
;
Note:
This does not
preclude the use of other physical
phase separation techniques
such as decantation,
filtration
(including ultrafiltration), and centrifugation,
when used
in con-junction with the above listed
recovery technologies.
RTHRN
Thermal recovery of metals or inorganics from
nonwastewaters
in
units defined as cement kilns, blast
furnaces, smelting, melting and refining furnaces,
combustion
devices
used
to
recover
sulfur
values
from
spent
sulfuric
acid
and
“other
devices”
determined
by
the Agency pursuant to 35
Ill. Adm.
Code 720.110,
the
definition of “industrial furnaces”.
RZINC
Resmelting
in for the purpose of recovery of zinc high
temperature metal recovery units.
STABL
Stabilization with the following reagents
(or waste
reagents)
or
combinations of reagents:
31
Portland cement; or
31
lime!
pozzolans
(e.g.,
fly ash and cement kiln
dust) —-this does not
preclude the addition of reagents
(e.g.,
iron salts, silicates,
and clays)
designed to
enhance the set/cure time and/or
compressive strength,
or to overall reduce the leachability of
the metal or
inorganic.
SSTRP
Steam stripping of organics from liquid wastes
utilizing direct
application of steam to the waste~
operated such that liquid and
vapor flow rates,
as
well as, temperature and pressure ranges
have been
optimized, monitored,
and maintained. These operating
p~rametersare dependent upon the design parameters
of
the unit
such as,
the number of separation stages and
the internal column
design.
Thus, resulting in
a
condensed extract high in organics
that must under~Q
121—5 20
372
either incineration, reuse as a fuel,
or other
recovery/reuse and an extracted wastewater that must
undergo
further treatment as specified in the
standard.
WETOX
Wet air oxidation performed in units operated such that
a
surrogate compound or indicator parameter
has been
substantially
reduced
in- concentration
in the
residuals
(e.g., Total Organic
Carbon can often be
used as an indicator parameter for the
oxidation of
many organic constituents that cannot be directly
analyzed in wastewater residues).
WTP.RX
Controlled reaction
with water for highly reactive
inorganic or
organic chemicals with precautionary
controls for protection of
workers from potential
violent reactions as well as
precautionary controls
for potential emissions of toxic!
ignitable levels of
gases released during the reaction.
Note
1:
When
a combination of these technologies
(i.e.,
a
treatment train)
is
specified as
a single treatment
standard,
the order of application is
specified
in
Table D by indicating the five letter technology
code
that must be applied first, then the designation “fb.”
(an abbreviation
for “followed by”), then the five
letter technology code for the technology
that must be
applied next,
and so on.
Note
2:
When more than one technology
(or treatment train) are
specified as
alternative treatment standards,
the five
letter technology codes
(or the
treatment trains)
are
separated by
a semicolon
(;) with the last technology
preceded by the word “OR”. This indicates that any one
of these BDAT
technologies or treatment trains can be
used for compliance with the
standard.
(Source:
Added at 15
Ill.
Reg.
,
effective
121—521
373
Section 728.Tabe
0 Technology—Based Standards by RCRA Waste Code
WASTE
CODES SEE ALSO
CAS
NO.
TECHNOLOGY CODE
WASTEWATR~NWASTEWATERS
WASTE
DESCRIPTIONS
AND/OR
TREATMENT
SUBCATEGORY
FSUBS;
RORGS;
or
INCIN
Ignitable
Liquids
based on
35
Ill. Adm.
Code
721.121(a) (1
1=
wastewaters
Ignitable
Liquids
based on
35
Ill.
Adm.
Code
721.121(a) (1
)--Low
TOC
Ignitable
Liquids
Subcategory-
—Less than
10
total
organic
carbon
total
organic
carbon
DOOl
NA
DEACT
NA
DOOl
NA
NA
DEACT
0001
NA
NA
Ignitable
Liquids
based on
35
Ill. Adm.
Code
721.121(a) (1
)--High TOC
Ignitable
Liquids
Subcategor~
-Greater
than or
equal to 10
12 1—522
374
DOOl
NA
NA
DEACT**
Ignitable
compressed
gases based
on
35
Ill.
Adm.
Code
721.121(a) (3
DOOl
NA
NA
DEACT
Ignitable
reactives
35
Ill. Adm.
Code
721.121(a) (2
DOOl
NA
DEACT
DEACT
Oxidizers
based on
35
Ill. Adm.
Code
721.121(a) (4
D002
NA
DEACT
DEACT
Acid
subcategory
based
on 35
Ill.
Adm.
Code
721.122 (a) (1
D002
NA
DEACT
DEACT
Alkaline
subc ate gory
based on 35
Ill.
Adm.
Code
721.122(a)
(1
NA
DEACT
DEACT
Other
corrosives
based on
35
Ill. Mm.
Code
721.12~jjj.~
12 1—523
375
D003
NA
DEACT
DEACT
Reactive
sulfides
based
on 35
Ill. Adm.
Code
721.123 (a) (5
D003
NA
DEACT
DEACT
Explosives
based on 35
Ill. Adm.
Code
721. 123 (a) (6
),
(7)
and
131
D003
NA
NA
DEACT
Water
reactives
based on 35
Ill. Adm.
Code
721.123 (a) (2
),
(3)
and
141
D003
NA
DEACT
DEACT
Other
reactives
based on 35
Ill. Mm.
Code
721.123(a) (1
0006
7440—43—9
NA
RTHERM
Cadmium
containing
batteries
12 1—524
376
D008
7439-82-
NA
RLEAD
Lead acid
batteries
(Note:
This
standard
only applies
to lead acid
batteries
that are
identified
as
RCRA
hazardous
wastes and
that are not
excluded
elsewhere
from
regulation
under the
land
~pgsal
restrictions
of this Part
or exempted
under other
gulations
(see
35
Ill.
Adm.
Code
726. 180)
.)
D009
Tables A
& 7439—87—
NA
IMERC;
or
Mercury:
RMERC
(High
Subcategory-
—greater
than or
equal
to 260
mgj,k
g,,~ptal
Mercury——
contains
mercury and
organics
~enot
incinerator
~~jdues~
12 1—525
377
0009
Tables A
& 7439—87—
NA
RNERC
Mercury:
B
6
(High
Mercury
Subcategory-
—greater
than or
equal to 260
mg/kg total
Mercury—
-
inorganics
(including
incinerator
residues and
residues
from RMERC))
D0l2
Table B
72-20-8
BIODG; or
NA
Endrin
INCIN
0013
Table B
58—89—9
CARBN; or
NA
Lindane
INCIN
0014
Table B
72-43-6
WETOX;
or
NA
Methoxychlor
INCIN
D015
Table
B
8001-35—1
BIODG; or
NA
Toxaphene
INCIN
D0l6
Table
B
94—75—7
QJ~Q~Qi.
NA
2,4—D
BIODG; or
INCIN
0017
Table B
93-72-1
CHOXD; or
NA
2,4,5-TP
INCIM
F005
Tables A
& 79-46—9
(WETOX or
INCIN
2-
B
CHOXD)
fb
Nitropropane
CARBN;
or
INCIN
F005
Tables A
& 110-80-5
BIODG;
or
INCIN
INCIN
Ethoxyethano
1
F024
Tables A &
NA
INCIN
INCIN
B
12 1—526
378
1025
NA
LLEXT fb
INCIN
Distillation
SSTRIP fb
bottoms from
ç~jj~or
the
INCIN
production
of
nitrobenzene
by the
nitration of
benzene
1026
NA
INCIN
INCIN
Stripping
still tails
from the
production
of methyl
ethyl
pyridines
1027
NA
CARBN; or
FSUBS;
or
~ntrifuge
INCIN
INCIN
and
distillation
residues
from
toluene
diisocyanate
production
1039
NA
CARBN;
or
FSUBS;
or
Filter
cake
INCIN
INCIN
from the
filtration
of
d iethylphosp
horodithioc
acid in the
of phorate
1044
NA
DEACT
DEACT
Wastewater
treatment
sludges from
the
inanufacturin
g and
processing
of
explosives
1045
NA
DEACT
DEACT
Spent carbon
from the
treatment
of
wastewater
containing
explosives
12 1—527
379
1047
NA
DEACT
DEACT
Pink/red
water from
TNT
operations
1061
Table B
NA
NA
NLDBR
Emission
control
dust/sludge
from the
primary
production
of steel in
electric
furnaces
(High Zinc
Subcategory-
—greater
than or
equal to 15
total Zinc)
K069
Tables
A
&
NA
NA
PlEAD
Emission
B
control
dust/sludge
from
secondary
lead
smelting:
Non—Calcium
Sulfate
Subcategory
1106
Tables
A
&
NA
NA
RNERC
Wastewater
P
treatment
sludge from
the mercury
cell process
in chlorine
production:
(High
Subcategory
-
greater
than
or equal to
260 mg/kg
total
mercury)
12 1—528
380
1113
NA
CARBN; or
FSUBS;
or
Condensed
LNC1M
INCIN
liquid light
ends
from
the
purification
of
toluenediam!
ne in the
production
of
toluenedianii
ne via
hydrogenatlo
n of
dinitrotolue
ne
1114
NA
CARBN;
or
FSUBS;
or
Vicinals
INCIN
INCIN
from the
purification
of
toluenediame
in the
of
toluenediaini
ne via
hydrogenatio
n of
dinitrotolue
ne
1115
NA
CARBM;
or
FSUBS;
or
Heavy ends
INCIN
INCIN
from the
purification
of
toluenediame
in the
production
of
toluenediami
ne via
hydrogenatio
n of
dii. n
itrotoIue
ne
12 1—529
381
1116
NA
CARBN; or
FSUBS; or
Organic
INCIN
INCIN
condensate
from the
solvent
recovery
column
in
the
production
of toluene
diisocyanate
via
phosgenation
of
toluenediami
ne
POOl
81-81-2
(WETOX or
FSUBS; or
Warfarin
CHOXD)
fb
INCIM
(0.3)
CARBN; or
INCIN
P002
591-08—2
(WETOX or
INCIN
l—Acetyl-2-
CHOXD)
fb
thiourea
CARBN; or
INCIN
P003
107-02-8
(WETOX or
FSUBS; or
Acrolein
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
P005
107-18-6
(WETOX or
FSUBS; or
Allyl
CHOXD)
Lb
INCIN
alcohol
CARBM;
or
INCIN
P006
20859-73-8
CHOXD;
CHOXD;
Aluminum
CHRED; or
CHRED; or
phosphide
INCIN
INCIN
P007
2763-96-4
(WETOX or
INCIN
5-Aminoethyl
CHOXD)
Lb
3-isoxazolol
CARBN; or
INCIN
P008
504-24—5
(WETOX or
INCIN
4—
CEOXD)
Lb
Aminopyridin
CARBN;
or
e
INCIN
12 1—530
382
P009
131—74—8
FSUBS~
Ammonium
CHRED;
CHOXD;
picrate
CARBN;
CHRED;
or
BIODG; or
INCIN
INCIN
P014
108-95—5
(WETOX or
INCIN
Thiophenol
CHOXD)
fb
(Benzene
Q~jj~or
thiol)
INCIN
7440-41-7
NA
B~Lor
Beryllium
RTHRN
dust
P016
542—88-1
(WETOX or
INCIN
Bis(chloro-
CHOXD)
Lb
methyl)ether
CARBN; or
INCIN
P017
598-31-2
(WETOX
or
INCIN
Brornoacetone
CHOXD)
fb
CARBN; or
INCIN
P018
357—57-3
(WETOX or
INCIN
Brucine
CHOXD)
Lb
CARBN;
or
INCIN
P022
Table B
75—15-0
NA
INCIN
Carbon
disulfide
P023
107-20-0
(WETOX or
INCIN
Qhloroacetal
CHOXD)
Lb
dehyde
CARBN;
or
INCIN
P026
5344-82-1
(WETOX or
INCIN
1—(o—Chloro-
CHOXD)
Lb
phenyllthio-
CARBN;
or
urea
INCIN
P027
542-76-7
(WETOX or
INCIN
3-Chloro-
CHOXD)
Lb
pr~pio-
CARBN; or
nitrile
INCIN
P028
100—44—7
____
Q~pr
INCIN
____
CHOXD)
Lb
chloride
CARBN; or
INCIN
121—531
383
P031
460-19-5
CHOXD;
CHOXD;
~yanogen
WETOX; or
WETOX;
or
INCIN
INCIN
P033
506-77-4
CHOXD;
CHOXD;
Cyanogen
WETOX;
or
WETOX; or
chloride
INCIN
INCIN
P034
131-89-5
IWETOX
or
INCIN
2—Cyclo-
CHOXD)
Lb
hexyl-4,6-
CARBN;
or
dinitro-
INCIN
phenol
P040
297—97-2
CARBN;
or
FSUBS;
or
0,0-Diethyl
INCIN
INCIN
O-pyrazinyl
phosphoro-
thioate
P041
311-45-5
CARBN; or
rSUBS;
or
Diethyl-p—
INCIN
INCIN
nitrophenyl
phosphate
P042
51-43-4
(WETOX or
INCIN
Epinephrine
CHOXD)
Lb
CARBN;
or
INCIN
P043
55-91—4
CARBN;
or
FSUBS;
or
Diisopropyl-
INCIN
INCIN
Lluoro-
phosphate
(DFP)
P044
60-51-5
CARBN;
or
FSUBS;
or
Dimethoate
INCIN
INCIN
P045
39196-18—4
fWETOX or
INCIN
Thiofanox
.C1LOXD)
Lb
CARBN;
or
INCIN
P046
122—09—8
(WETOX
or
INCIN
alpha,alpha-
CHOXD)
fb
Dimethyl-
CARBN;
or
phenethyl-
INCIN
amine
P047
534—52—1
(WETOX or
INCIN
4,6-Dinitro-
CHOXD)
Lb
o-cresol
CARBN;
or
salts
INCIN
121—532
384
P049
541-53-7
(WETOX or
INCIN
2,4-Dithio-
CHOXD)
Lb
biuret
CARBN; or
INCIN
P054
151—56—4
(WETOX or
INCIN
Aziridine
CHOXD)
Lb
CARBN;
or
INCIN
P056
Table
B
7782—41—4
NA
ADGAS
Lb
Fluorine
NEUTR
P057
640-19-7
(WETOX or
INCIN
Fluoro—
CHOXD)
Lb
acetamide
CARBN; or
INCIN
P058
62—74-8
(WETOX or
INCIN
Fluoroacetic
CHOXD)
Lb
acid,
sodium
CARBN; or
salt
INCIN
P062
757-58-4
CARBN; or
FSUBS or
Hexaethyl-
INCIN
INCIN
tetra-
phosphate
P064
624-83-9
(WETOX or
INCIN
Isocyanic
CHOXD)
Lb
acid,
ethyl
CARBN; or
ester
INCIN
P065
Tables A
& 628-86-4
NA
RNERC
Mercury
P
fulminate:_
(High
Mercury
Subcategory-
—
greater
than or
e~~~260
mg/kg total
Mercury——
either
Inc
i
nerator
residues or
residues
from
RNERC)
12 1—533
385
P065
Tables A
& 628-86-4
NA
IMERC
Mercury
P
fulminate:
wastewaters
that
are not
incinerator
residues
from RNERC;
regardless
of Mercury
Content)
P066
16752-77—5
(WETOX
or
INCIN
Methomyl
CHOXD)
Lb
CARBN;
or
INCIN
P067
75-55-8
(WETOX
or
INCIN
2-Methyl-
CHOXD)
Lb
aziridine
CARBN; or
INCIN
P068
60—34—4
CHOXD;
FSUBS;
Methyl
CHRED;
CHOXD;
hydrazine
CAR3N;
CHRED; OR
BIODG; or
INCIN
INCIN
P069
75-86-5
(WETOX or
INCIN
Methyllacto-
CHOXD)
fb
nitrile
CARBN; or
INCIN
P070
116-06-3
(WETOX or
INCIN
Aldicarb
CHOXD)
Lb
CARBN;
or
INCIN
P072
86-88-4
(WETOX or
INCIN
1-Naphthyl-
CHOXD)
Lb
2-thiourea
CARBN;
or
INCIN
P075
54-11-5*
(WETOX or
INCIN
Nicotine and
CHOXD)
Lb
salts
CARBN;
or
INCIN
P076
10102—43-9
ADGAS
ADGAS
Nitric oxide
P078
10102-44-0
ADGAS
ADGAS
Nitrogen
dioxide
12 1—534
386
P081
55—63-0
FSUBS;
Nitro—
CHRED;
CHOXD;
glycerin
CARBN;
CHRED;
or
BIODG; or
INCIN
INCIN
P082
Table B
65—75—9
NA
INCIN
N—Nitroso-
dimethyl-
amine
P084
4549-40-0
(WETOX or
INCIN
N-Nitroso-
_______
inethylvinyl-
amine
INCIN
P085
152—16—9
~jjLor
FSUBS; or
Octamethyl—
INCIN
INCIN
pyro-
phosphor-
amide
P087
20816—12—0
NA
RNETL;
or
Osmium
RTHRM
tetroxide
P088
145-73-3
(WETOX or
FSUBS; or
Endothall
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
P092
Tables A
& 62-38-4
NA
RNERC
Phenyl
mercury
acetate:
(High
Mercury Sub-
category--
greater than
or equal to
260
mg/kg
total
Mercury—-
either
incinerator
residues or
residues
from RNERC)
121—535
387
P092
Tables
A
&
62—38—4
NA
IMERC; or
Phenyl
B
RNERC
mercury
acetate:
(All
nonwastewate
rs that are
not
incinerator
residues and
are
not
residues
from P1~ERC:
regardless
of Mercury
Content)
P093
103-85-5
(WETOX or
INCIN
Phenylthio-
CHOXD)
Lb
urea
CARBN;
or
INCIN
P095
75-44-5
(WETOX or
INCIN
Phosqene
CHOXD)
Lb
CARBN;
or
INCIN
P096
7803—51-2
CHOXD;
CHOXD;
Phosphine
CI-IRED; or
CHRED;
or
INCIN
INCIN
P102
107-19-7
(WETOX or
FSUBS;
or
Propargyl
CHOXD)
Lb
INCIN
alcohol
CARBN;
or
INCIN
P105
26628—22—
CHOXD;
FSUBS;
Sodium
azide
8
CHRED;
CHOXD;
CARBN
CHRED;
or
BIODG;
or
INCIN
INCIN
P108
57-24—9*
(WETOX
or
INCIN
Strychnine
CHOXD)
Lb
and salts
CARBN;
or
INCIN
P109
3689—24—5
CARBN; or
FSUBS;
or
Tetraethyl-
INCIN
INCIN
dithiopyro-
phosphate
12
1—536
388
P112
509—14-8
CHOXD;
FSUBS
________
CHRED;
CHOXD;
methane
CARBN;
CHRED;
or
BIODG; or
INCIN
INCIN
P113
Table
B
1314-32—5
NA
RTHRN; or
Thallic
STABL
oxide
P115
Table
B
7446—18-6
NA
RTHRN; or
Thallium
(I)
STABL
sulLate
P116
79-19-6
(WETOX or
INCIN
Thiosemi-
CHOXD)
Lb
carbazide
CARBN; or
INCIN
P118
75-70-7
jj~IQXç?~ INCIN
Trichioro-
CHOXD)
Lb
methanethiol
CARBN; or
INCIN
P119
Table B
7803-55-6
NA
STABL
ATnmonium
vanadate
P120
Table
B
1314—62-1
NA
STABL
Vanadium
pentoxide
P122
1314-84-7
CHOXD;
CHOXD;
Zinc
CHRED; or
CHRED;
or
Phosphide
INCIN
INCIN
(10)
U001
75—07—0
jQQ~
FSUBS;
or
Acetaldehyde
CHOXD)
fb
INCIN
CARBN; or
INCIN
U003
Table
B
75—05-8
NA
INCIN
Acetonitrile
U006
75-36-5
(WETOX or
INCIN
___
CHOXD)
Lb
chloride
CARBN; or
INCIN
U007
79-06-1
(WETOX or
INCIN
Acrylamide
CARBN;
or
INCIN
121—537
389
U008
79—10-7
(WETOX or
FSUBS; or
Acrylic acid
CHOXD)
Lb
INCIN
CARBN; or
INCIN
UOlO
50—07—7
(WETOX or
INCIN
Nitomycin C
CHOXD)
Lb
CARBN;
or
INCIN
UOll
61—82—5
(WETOX or
INCIN
Amitrole
CHOXD)
Lb
CARBN;
or
INCIN
U0l4
492—80—8
(WETOX
or
INCIN
Auramine
CHOXD)
Lb
CARBN;
or
INCIN
U0l5
115—02—6
(WETOX or
INCIN
Azaserine
CHOXD)
Lb
CARBN; or
INCIN
11016
225—51—4
(WETOX or
FSUBS; or
Benz(c)-
CHOXD)
Lb
INCIN
acridine
CARBN;
or
INCIN
13017
98—87—3
(WETOX or
INCIN
Benzal
CHOXD)
Lb
chloride
CARBN;
or
INCIN
11020
98-09-9
(WETOX or
INCIN
Benzene-
CHOXD)
Lb
sulfonyl
CARBN; or
chloride
INCIN
U021
92—87-5
(WETOX or
INCIN
Bënzidine
CHOXD)
fb
CARBN;
or
INCIN
11023
98-07-7
CHOXD;
FSUBS;
Benzotri-
CHRED;
CHOXD;
chloride
CARBN;
CHRED; or
BIODG; or
INCIN
INCIN
12 1—538
390
11026
494-03-1
(WETOX or
INCIN
Chlor-
CHOXD)
Lb
naphazin
CARBN;
or
INCIN
11033
353-50-4
(WETOX or
INCIN
Carbonyl
CHOXD)
Lb
fluoride
CARBN; or
INCIN
11034
75-87-6
(WETOX or
INCIN
Trichloro-
CHOXD)
Lb
acet-
CARBN; or
aldehyde
INCIN
(Chloral)
U035
305-03-3
(WETOX or
INCIN
Chlorambucil
CFJOXD)
Lb
CARBN;
or
INCIN
U038
Table B
510—15-6
NA
INCIN
Chloro-
benzilate
11041
106-89-8
(WETOX or
INCIN
1—Chloro-
CHOXD)
Lb
2,3-epoxy-
CARBN; or
p~çopane
INCIN
(Epichloro-
hydrin)
U042
Table B
110-75—8
NA
INCIN
2—Chloro—
ethyl vinyl
ether
11046
107-30-2
(WETOX or
INCIN
Chloromethyl
CHOXD)
Lb
CARBN; or
INCIN
11049
3165-93—3
jQ~~
INCIN
4-Chloro—o-
______
toluidine
_______
hydro-
INCIN
chloride
11053
4170-30-3
L~X~r
FSUBS; or
Croton-
CHOXD)
Lb
INCIN
aldehy~
CARBN;
or
INCIN
11055
98-82-8
(WETOX or
FSUBS;
or
Cuinene
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
12 1—539
391
U056
110—82-7
(WETOX or
FSUBS; or
Cyclohexane
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
11057
Table
B
108—94—1
NA
FSUBS;
or
Cyclo—
INCIN
hexanone
U058
50-18-0
CARBN;
or
FSUBS; or
Cyclophosph-
INCIN
INCIN
amide
U059
20830-81-3
(WETOX or
INCIN
Daunornycin
CHOXD)
Lb
CARBN;
or
INCIN
11062
2303-16—4
(WETOX or
INCIN
Diallate
CHOXD)
Lb
CARBN;
or
INCIN
11064
189—55—9
(WETOX or
~~~jor
1,2,7,8—Di—
CHOXD)
Lb
INCIN
benzopyrene
CARBN;
or
INCIN
11073
91—94—1
(WETOX or
INCIN
3,3’—Di—
CHOXD)
Lb
chlorobenz-
CARBN;
or
idine
INCIN
11074
1476—11—
(WETOX or
INCIN
cis—l,4—Di-
5
CHOXD)
Lb
chloro-2-
CARBN; or
butene;
INCIN
trans-1,4-
Dichloro-
2—
butene
11085
1464—53—5
(WETOX or
FSUBS; or
1,2:3,4-Di-
CHOXD)
Lb
INCIN
epoxybutane
CARBN;
or
INCIN
11086
1615-80-
CHOXD;
~p~j
N,N-Diethyl-
1
CHRED;
CHOXD;
hydrazine
CARBN
CHRED;
or
BIODG; or
INCIN
INCIN
12 1—540
392
11087
3288-58-
CARBN;
or
FSUBS;
or
0,0-Diethyl
2
INCIN
INCIN
S-methyl-
dithio-
phosphate
U089
56-53-1
(WETOX or
FSIJBS;
or
Diethyl
CHOXD)
Lb
INCIN
stilbestrol
CARBN;
or
INCIN
U090
94-58-6
(WETOX
or
FSUBS;
or
Dihydro-
CHOXD)
Lb
INCIN
safrole
CARBN; or
INCIN
11091
119—90—4
(WETOX
or
INCIN
3,3’—Di—
CHOXD)
Lb
methoxy-
CARBN; or
benzidine
INCIN
11092
124—Z~0—3
jIQXQr
INCIN
_______
amine
CARBN;
or
INCIN
11093
Table
B
621-90-9
NA
INCIN
p-Dimethyl-
aminoazo—
benzene
U094
57-97-6
(WETOX or
FSUBS;
or
7,12-
CHOXD)
Lb
INCIN
Dimethyl-
CARBN; or
benz (a)
-
INCIN
anthracene
U095
119—93—7
(WETOX or
INCIN
3,3’—
CHOXD)
Lb
Dirr~~y1-
CARBN; or
benzidine
INCIN
U096
80—15—9
Q~Q~
FSUBS;
alpha,alpha-
CHRED;
CHOXD;
Dilnethyl-
CARBN
CHRED; or
benzyl
BIODG; or
INCIN
hydro-
INCIN
peroxide
11097
79-44-7
(WETOX or
INCIN
Dimethyl-
_
~mol
CARBN;
or
chloride
INCIN
121—541
393
11098
57—14-7
CHOXD;
FSUBS;
1,1—
CHRED;
CHOXD
-
Dimethylhydr
CARBN;
CHRED;
or
azine
BIODG; or
INCIN
INCIN
U099
540—73—8
CHOXD;
FSUBS;
1,2—
CHRED;
CHOXD;
Dimethyl-
CARBN;
CHRED;
or
hydrazine
BIODG; or
INCIN
INCIN
U103
77—78-1
CHOXD;
FSUBS;
Dimethyl
CHRED;
CHOXD;
sulfate
CARBN;
CHRED; or
BIODG; or
INCIN
INCIN
11109
122—66—7
CHOXD;
FSUBS;
1,2—
CHRED;
CHOXD;
Diphenyl-
CARBN;
CHRED; or
hydrazine
BIODG; or
INCIN
INCIN
U110
142-84-7
(WETOX or
INCIN
Dipropyl-
CHOXD)
Lb
amine
CARBN; or
INCIN
U1l3
140-88-5
(WETOX or
FSUBS; or
Ethyl
CHOXD)
Lb
INCIN
acrylate
CARBN; or
INCIN
11114
111-54-6
(WETOX
or
INCIN
Ethylene-
CHOXD)
Lb
bisdithio-
CARBN; or
carbamic
INCIN
acid
0115
75-21-8
(WETOX or
CHOXD; or
Ethylene
CHOXD)
Lb
INCIN
oxide
CARBN; or
INCIN
11116
96-45-7
IWETOX or
INCIN
Ethylene
CHOXD)
Lb
thiourea
CARBN;
or
INCIN
12 1—542
394
11119
62-50-0
(WETOX or
INCIN
Ethyl
CHOXD)
Lb
methane-
CARBN; or
sulfonate
INCIN
11122
50-00-0
IWETOX or
FSUBS; or
Formaldehyde
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
11123
64-18-6
(WETOX or
FSUBS; or
Formic acid
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
11124
110-00-9
(WETOX or
FSUBS; or
Furan
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
U125
98-01-1
(WETOX or
FSUBS;
or
Furfural
CHOXD)
Lb
INCIN
CARBN; or
INCIN
U126
765-34-4
(WETOX or
FSUBS; or
Glycid-
HOXD)
Lb
INCIN
aldehyde
CARBN;
or
INCIN
11132
70—30-4
(WETOX or
INCIN
Hexachioro-
CHOXD)
Lb
phene
~~jjor
INCIN
11133
302—01—2
CHOXD
~UBS;
Hydrazine
CHRED;
CHOXD;
CARBN
CHRED;
or
BIODG; or
INCIN
INCIN
11134
Table
B
7664-39-3
NA
ADGAS Lb
Hydrogen
NEUTR;
or
Fluoride
NEUTR
11135
7783-06-4
CHOXD;
CHOXDi
Hydrogen
CHRED;
or
CHRED;
or
Sulfide
NCIN
INCIN
12 1—543
395
13143
303-34-4
(WETOX or
INCIN
Lasiocarpine
CHOXD)
Lb
CARBN;
or
INCIN
U147
108-31-6
(WETOX or
FSUBS; or
Maleic
CHOXD)
Lb
INCIN
anhydride
CARBN; or
INCIN
11148
123—33-1
(WETOX
or
INCIN
Maleic
CHOXD)
fb
hydrazide
CARBN;
or
INCIN
11149
109-77-3
(WETOX or
INCIN
Malono-
CHOXD)
Lb
nitrile
CARBN;
or
INCIN
U150
148—82—3
(WETOX or
INCIN
Melphalan
CHOXD)
Lb
CARBN;
or
INCIN
U151
Tables
A
~.
7439-97-
NA
RNERC
Mercury:
B
6
(High
Mercury Sub-
category——
greater than
or
equal
to
260
mg/kg
total
Mercury)
Ul53
74—93-1
(WETOX
or
INCIN
Methanethiol
CHOXD)
Lb
CARBN;
or
INCIN
11154
67-56-1
i~ETOX or
FSUBS;
or
Methanol
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
11156
79—22-1
(WETOX or
INCIN
Methyl
CHOXD)
Lb
chloro-
CARBN; or
carbonate
INCIN
121—544
396
Ul60
1338-23-
CHOXD;
FSUBS;
Methyl ethyl
CHRED;
ketone
CARBN
~~oI
peroxide
BIODG; or
INCIN
INCIN
U163
70-25-7
(WETOX or
INCIN
N-Methyl-
CHOXD)
Lb
N’-nitro-N-
CARBN;
or
Nitroso-
INCIN
guanidine
11164
56-04-2
(WETOX or
INCIN
Methylthio-
CHOXD)
Lb
uracil
CARBN; or
INCIN
11166
130-15—4
jQ~Qr
FSUBS;
or
1,4-Naphtho-
CHOXD)
Lb
INCIN
guinone
CARBN;
or
INCIN
11167
134-32-7
(WETOX or
INCIN
~~pj~h1~-
CHOXD)
Lb
amine
CARBN;
or
INCIN
11168
Table
B
91—59—8
NA
INCIN
2—Naphthyl-
amine
11171
79—46—9
(WETOX
or
INCIN
2-Nitro-
propane
CARBN; or
INCIN
U173
1116-54-7
(WETOX
or
INCIN
N-Nitroso-
CHOXD)
Lb
diethanol-
CARBN;
or
amine
INCIN
Ul76
759-73-9
(WETOX or
INCIN
N-Nitroso-
CHOXD)
Lb
~~~fly1u~a
CARBN; or
INCIN
11177
684-93—5
(WETOX or
INCIN
N—Nitroso-
CHOXD)
Lb
N-methyl-
CARBN;
or
urea
INCIN
12 1—545
397
11178
615-53-2
(WETOX
or
INCIN
N-Nitroso-
CHOXD)
Lb
N-methyl-
CARBN; or
urethane
INCIN
U182
123-63-7
~WETOX
or
FSUBS; or
Paraldehyde
CHOXD)
Lb
INCIN
CARBN;
or
INCIN
13184
76—01—7
(WETOX or
INCIN
Pentachloro-
CHOXD)
fb
ethane
CARBN;
or
INCIN
U186
504-60-9
(WETOX
or
FSUBS;
or
1,3-Penta-
CHOXD)
Lb
INCIN
diene
CARBN;
or
INCIN
13189
1314-80-3
CHOXD;
CHOXD;
Phosphorus
CHRED; or
CHRED; or
sulfide
INCIN
INCIN
11191
109—06—8
(WETOX or
INCIN
2—Picoline
CHOXD)
Lb
CARBN;
or
INCIN
U193
1120-71—4
(WETOX
or
INCIN
1,3-Propane
CHOXD)
Lb
sultone
CARBN;
or
INCIN
11194
107-10-8
(WETOX or
INCIN
n-Propyl-
CHOXD)
Lb
amine
CARBN;
or
INCIN
Ul97
106-51-4
(WETOX or
FSUBS; or
p-Benzo-
CHOXD)
Lb
INCIN
ciuinone
CARBN;
or
INCIN
11200
50-55-5
(WETOX or
INCIN
Reserpine
CHOXD)
Lb
CARBN;
or
INCIN
-
12 1—546
398
U201
108-46-3
(WETOX or
FSUBS;
or
Resorcinol
CHOXD)
fb
INCIN
CARBN; or
INCIN
U202
81—07—2*
(WETOX or
INCIN
Saccharin
CHOXD)
fb
and
salts
CARBN; or
INCIN
U206
18883-66-4
(WETOX or
INCIN
Strepto-
CHOXD)
Lb
zatocin
CARBN;
or
INCIN
11213
109—99—9
(WETOX or
FSUBS;~
Tetrahydro-
CHOXD)
Lb
INCIN
Luran
CARBN;
or
INCIN
11214
Table
B
563-~8—8
NA
RTHRN; or
Thallium
(I)
STABL
acetate
11215
Table
B
6533—73—9
NA
RTHPN;
or
Thallium
(I)
STABL
carbonate
13216
Table B
7791—12—0
NA
RTHRN;
or
Thallium
(I)
STABL
chloride
U217
Table
B
10102—45—1
NA
RTHRM;
or
Thallium
(I)
STABL
nitrate
11218
62-55-5
(WETOX or
INCIN
Thioacet-
CHOXD)
Lb
amide
CARBN; or
INCIN
11219
62-56-6
(WETOX or
INCIN
Thiourea
CHOXD)
fb
CARBN;
or
INCIN
U221
25376-45-8
CARBN; or
FSUBS; or
Toluenedi-
INCIN
INCIN
amine
11222
636-21-5
(WETOX or
INCIN
o-Toluidine
CHOXD)
Lb
hydro-
CARBN;
or
chloride
INCIN
U223
26471—62—5
CARBN; or
~
Toluene
INCIN
INCIN
diiso~y~j~~
12 1—547
399
U234
99-35-4
(WETOX or
INCIN
sym-Tri-
CHOXD)
Lb
nitrobenzene
CARBN;
or
INCIN
U236
72-57-1
(WETOX or
INCIN
Trypan Blue
CHOXD)
Lb
CARBN;
or
INCIN
11237
66-75-1
IWETOX or
INCIN
Uracil
CHOXD)
Lb
mustard
CARBN;
or
INCIN
11238
51-79—6
(WETOX or
INCIN
Ethyl
CHOXD)
Lb
carbamate
CARBN;
or
INCIN
13240
94_75_7*
(WETOX
or
INCIN
2,4—
CHOXD)
Lb
Dichloro-
CARBN;
or
phenoxy-
INCIN
acetic
acid
(salts and
esters)
11244
137-26-8
(WETOX or
INCIN
Thiram
CHOXD)
Lb
CARBN;
or
INCIN
11246
506-68-3
CHOXD;
CHOXD;
Cyanogen
WETOX; or
WETOX;
or
bromide
INCIN
INCIN
11248
81-81-2
(WETOX or
FSUBS;
or
Warfarin
CHOXD)
Lb
INCIN
(greater
CARBN; or
than or
INCIN
equal to
3)
11249
1314-84-7
CHOXD;
CHOXD;
Zinc
CHRED; or
CHRED; or
Phosphide
INCIN
INCIN
(10)
*
CAS Number given for parent compound only.
**
This waste code exists in gaseous form and
is not
categorized as wastewater or nonwastewater forms.
NA
Not Applicable.
12 1—548
400
BOARD NOTE:
When
a combination of these technologies
(i.e.,
a
t~~~menttrain)
is speciLied as a single treatment standard,
the
order of application is specified in this Table by indicating the
five
letter technology code that must be applied first,
then the
designation “fb”
(an abbreviation for “Followed by”),
then the
five letter technology code for the technology that must be
applied next,
and so on.
When more than one technology
(or
treatment
train)
are
specified a alternative treatment standards,
the five letter technology codes
(or the treatment trains)
are
separated by a semicolon
(;) with the last technology preceded by
the word
“or”.
This indicates that any oneof
these BDAT
technologies or treatment trains can be used for compliance with
the standard.
See Section 728.Table
C for a listing oL the
technology codes and technology—based treatment standards.
Derived from 40 CFR 268.42, Table
2,
‘as adopted at
54
Fed.
Rea.
22694, June
1,
1990.
(Source:
Added at
15 Ill.
Reg.
,
effective
12 1—549
401
Section 728.Table E
Standards for Radioactive Mixed Waste
TECHNOLOGY CODE
WASTE
NON-
WASTE DESCRIPTIONS
AND/OR
CODES
CAS NO.
WASTEWATERS
WI~EN~ERS
SUBCATEGORY
D002
NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing of Fuel Rods
Subcategory
D004
NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing of Fuel Rods
Subcategory
D005
NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing
of
Fuel
Rods
Subcategory
D006
NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing of Fuel Rods
Subcategory
D007 NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing of Fuel Rods
Subcategory
D008 7439—92-1
NA
MACRO
Radioactive Lead Solids
Subcategory
(Note: these lead
solids
include,
but are not
limited to, all forms of lead
shielding,
and
other
elemental
forms of
lead.
These lead
solids
do
not
include
treatment
residuals
such
as
hy~roxide
sludges,
other
wastewater treatment
residuals,
or
incinerator
ashes
that
can
undergo
conventional pozzolanic
stabilization,
nor do they
include organo—lead materials
that can be incinerated and
stabilized as ash.)
121—550
/
IV)
~t U ~
D008
NA
NA
HLVIT
Radioactive High Level Wastes
Generated Durinq the
Reprocessing of Fuel Rods
Subcateqory
DOO9 7439-97-6
NA
AMLGM
Elemental mercury contaminated
with
radioactive
materials
0009 7439-97-6
NA
INCIN
Hydraulic
oil
contaminated
with
MercurY
Radioactive
Materials Subcategory
D009
NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
Reprocessing of Fuel Rods
Subcategory
0010 NA
NA
HLVIT
Radioactive High Level Was~
Generated During the
Reprocessing oL Fuel Rods
Subcategory
DOll NA
NA
HLVIT
Radioactive High Level Wastes
Generated During the
~processing
of
Fuel
Rods
Subcategory
11151
7439-97-6
NA
AMLGM
Mercury: Elemental mercury
contaminated with radioactive
materials
NA-—Not Applicable.
(Source:
Added at 15
Ill.
Reg.
,
effective
12 1—551
