ILLINOIS POLLUTION CONTROL BOARD
August
8,
1991
IN THE MATTER OF:
)
R91—1
RCRA UPDATE, USEPA REGULATIONS
)
(Identical in Substance Rules)
(7—1—90 THROUGH 12—31—90)
)
ADOPTED RULES.
FINAL ORDER
ORDER OF THE BOARD
(by
3.
Anderson):
1Pu1~suantto Section 7.2 and 22.4(a)
of the Environmental
Protection Act (Act),
the Board is amending the RCRA hazardous
waste regulations.
The amendments involve 35 Ill.
Adm. Code 703,
720,
721,
722, 724 and 725.
Section 22.4 of the Act governs adoption of regulations
establishing the RCRA program in Illinois.
Section 22.4(a)
provides for quick adoption of regulations which are “identical
in substance” to federal regulations;
Section 22.4(a) provides
that Title VII of the Act and Section
5
of the Administrative
Procedure Act shall not apply.
Because this rulemaking is not
subject to Section 5 of the Administrative Procedure Act,
it is
not subject to first notice or to second notice review by the
Joint Committee on Administrative Rules
(JCAR).
The federal RCRA
regulations are found at 40 CFR 260 through 270.
This rulemaking
updates Illinois’ RCRA rules to correspond with federal
amendments during the period July
1 through December 31,
1990.
This Order is supported by an Opinion of this same date.
The Board will not file the rules until after September 9,
1991,
to allow time for post—adoption review and comments by the
agencies involved in the authorization process.
IT IS SO ORDERED.
B. Forcade concurred.
1The Board acknowledges the contributions of Morton Dorothy,
Mike McCambridge and Anne Manly in preparing the Opinion and Order.
125—173
2
I, Dorothy
M. Gunn, Clerk
of
the
Illinois
Pollution
Control
Board
do hereby certify that the above Order was adopted on the
_________day of
,
1991, by a vote of
7—c
Dorothy M.
~Unn,
Clerk
Illinois P~lutionControl Board
125—174
3
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER
I:
POLLUTION CONTROL BOARD
SUBCHAPTER b:
PERMITS
PART 703
RCRA PERMIT PROGRAM
SUBPART A:
GENERAL PROVISIONS
Section
703.100
703.101
703
.
110
Section
703.120
703.121
703.122
703.123
703.124
703.125
793.126
703.127
Scope and Relation to Other Parts
Purpose
References
SUBPART B:
PROHIBITIONS
Prohibitions in General
RCRA Permits
Specific Inclusions in Permit Program
Specific Exclusions from Permit Program
Discharges of Hazardous Waste
Reapplications
Initial Applications
Federal Permits (Repealed)
SUBPART C:
AUTHORIZATION BY RULE
AND
INTERIM STATUS
Purpose and Scope
Permits by Rule
Application by Existing
HWM
Facilities and Interim
Status Qualifications
Application by New HWM Facilities
Amended Part A Application
Qualifying for Interim Status
Prohibitions During Interim Status
Changes During Interim Status
Interim Status Standards
Grounds for Termination of Interim Status
Permits for Less Than an Entire Facility
Closure by Removal
Procedures for Closure Determination
SUBPART D:
APPLICATIONS
Section
703.180
703.181
703
.
182
703.183
703
.
184
703.185
703.186
703.187
Applications in General
Contents of Part A
Contents of Part B
General Information
Facility Location Information
Groundwater Protection Information
Exposure Information
Solid Waste Management Units
Section
703.140
703. 141
703.150
703.151
703.152
703.153
703.154
703.155
703
.
156
703.157
703.158
703.159
703. 160
125—175
4
703.188
703.200
703.201
.703.. 202
703.203
703.204
703.205
703.206
703.207
703.209
703.210
703.211
703.212
Section
703.221
703.222
703.223
703.224
703.225
703.230
703.231
Section
703.240
703.241
703.242
703.243
703.244
703.245
703.246
703.247
Section
703.260
703.270
703.271
703.272
703.273
703.280
703.281
703.282
703.283
Appendix A
Other Information
Specific Information
Containers
Tank Systems
Surface Impoundments.
Waste Piles
Incinerators
Land Treatment
Landfills
Miscellaneous Units
Process Vents
Equipment
Drip Pads
SUBPART E:
SHORT TERM AND PHASED PERMITS
Emergency Permits
Incinerator Conditions Prior to Trial Burn
Incinerator Conditions During Trial Burn
Incinerator Conditions After Trial Burn
Trial Burns for Existing Incinerators
Land Treatment Demonstration
Research, Development and Demonstration Permits
SUBPART F:
PERMIT CONDITIONS OR DENIAL
Permit Denial
Establishing Permit Conditions
Noncompliance Pursuant to Emergency Permit
Monitoring
Notice of Planned Changes
Twenty-four Hour Reporting
Reporting Requirements
Anticipated Noncompliance
SUBPART
G:
CHANGES TO PERMITS
Transfer
Modification
Causes for Modification
Causes for Modification or Reissuance
Facility Siting
Permit Modification at the Request of the Permittee
Class
1 Modifications
Class
2 Modifications
Class
3 Modifications
Classification of Permit Modifications
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111½,
pars.
1022.4 and 1027).
125—17 6
5
SOURCE:
Adopted in R82—19,
53 PCB 131,
at 7
Ill.
Reg.
14289,
effective October 12, 1983;
amended in R83—24 at 8
Ill.
Reg.
206,
effective December 27,
1983; amended in R84-9 at 9
Ill.
Reg.
11899, effective July 24,
1985; amended in R85—22 at 10 Ill.
Reg.
1110, effective January 2,
1987; amended in R85—23 at 10
Ill.
Reg.
13284, effective July 28,
1986; amended in R86—1 at 10 Ill.
Reg.
14093, effective August 12,
1986; amended in R86—19 at 10
Ill. Reg.
20702,
effective December 2,
1986; amended in R86-28 at
11 Ill.
Req.
6121, effective March 24,
1987; amended in R86—46 at
11 Ill. i~eg. 13543, effective August 4,
1987; amended in R87—5 at
11 Ill. Reg.
19383, effective November 12,
1987; amended in R87—
26 at 12
Ill.
Reg. 2584,
effective January 15,
1988; amended in
R87—39 at 12
Ill. Reg.
13069, effective July 29,
1988;
amended in
R88—16 at 13
Ill. Reg.
447, effective December 27,
1988; amended
in R89—1 at
13 Ill. Reg.
18477,
effective November 13,
1989;
amended in R89—9
at 14
Ill. Reg.
6278, effective April 16,
1990;
amended in R90-2 at 14
Ill. Req.
14492, effective August 22,
1990; amended in R90-ll at 15 Ill.
Req.
9616, effective June 17,
1991; amended in R91—1 at
15 Ill.
Reg.
,
effective
SUBPART D:
APPLICATIONS
Section 703.212
Drip Pads
Except as otherwise provided by 35 Ill.
Adm. Code 724.101,
owners
and operators of hazardous waste treatment,
storage or disposal
facilities that collect,
store or treat hazardous waste on drip
pads shall provide the following additional information:
~j
A list of hazardous wastes placed or to be placed on
each drip pad.
~j
If an exemption is sought to 35 Ill.
Adm. Code
724.Subpart F,
as provided by
35 Ill.
Adm. Code
724.190, detailed plans and an engineering report
describing how the requirements of 35
Ill.
Adrn.
Code
724.190(b) (2) will be met.
~j
Detailed plans and an engineering report describing how
the drip ~ad is or will be designed. constructed.
operated and maintained to meet the reguireinents of 35
Ill. Adm. Code 724.673.
including the as-built drawings
and specifications.
This submission must address the
following items as specified in 35 Ill. Adm. Code
724.671
:
fl
The design characteristics of the drip pad
21
The liner system
125—17
7
6
fl
The leakage detection system,
including the leak
detection system and how it is designed to detect
the failure of the drip pad or the presence of any
releases of hazardous waste or accumulated liquid
at the earliest practicable time
~4j
Practices desic’ned to maintain drip pads
~j.
The associated collection system
QI
Control of run-on to the drip pad
~j.
Control of run-off from the drip pad
fi
The interval at which drippage and other materials
will be removed from the associated collection
system and a statement demonstrating that the
interval will be sufficient to prevent overflow
onto the drip pad
.21
Cleaning procedures and documentation.
~
Procedures for cleaning the drip pad at least
once every seven days to ensure the removal
of any accumulated residues of waste or other
materials,
including, but not limited to:
rinsing; washing with detergents or other
appropriate solvents; or,
steam cleaning.
And,
~j
Provisions for documenting the date, time and
cleaning procedure used each time the pad is
cleaned.
Operating
practices and procedures that will be
followed to ensure that tracking of hazardous
waste or waste constituents off the drip pad due
to activities by personnel or equipment is
minimized
JJJ.
Procedures for ensuring that,
after removal from
the treatment vessel, treated wood from pressure
and non—pressure processes
is held on the drip pad
until drippage has ceased,
including recordkeeping
practices
.3fl
Provisions for ensuring that collection and
holding units associated with the run-on and run-
off control systems are emptied or otherwise
managed as soon as possible after storms to
maintain design capacity of the system
125—178
7
If
treatment is carried out on the drip pad,
details of the process equipment used,
and the
nature and quality of the residuals.
141
A description of how each drip pad, including
appurtenances for control of run—on and run—off,
will be inspected in order to meet the
requirements of 35
Ill. Adm. Code 724.673.
This
information must be included in the inspection
plan submitted under Section 703.183(e).
j~j A certification signed by an independent
qualified, registered professional engineer,
stating that the drip pad design meets the
requirements of 35
Ill. Adm. Code 724.673(a)—(f).
~j
A description of how hazardous waste residues and
contaminated materials will be removed from the
drip pad at closure,
as required under 35
Ill.
Adm. Code 724.675(a).
For any waste not to be
removed from the drip pad upon closure, the owner
or operator shall submit detailed plans and an
engineering report describing how 35
Ill.
Adm.
Code 724.410(a)
and
(b) will be complied with.
This information must be included in the closure
plan and, where applicable,
the post—closure plan
submitted under Section 703.183(m).
BOARD NOTE:
Derived from 40 CFR 270.22,
adopted
at 55
Fed. Req.
50489, December 6,
1990;
renumbered to 270.26 and amended at 56 Fed.
Reg.
30192, July 1,
1991.
(Source:
Added at 15
Ill. Reg.
,
effective
125—179
8
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART
720
HAZARDOUS
WASTE
MANAGEMENT
SYSTEM:
GENERAL
SUBPART
A:
GENERAL
PROVISIONS
Section
720.101
‘
Purpose,
Scope and Applicability
720.102
Availability of Information; Confidentiality of
Information
720.103
Use of Number and Gender
SUBPART B:
DEFINITIONS
Section
720.110
Definitions
720.111
References
SUBPART C:
RULEMAKING PETITIONS
AND
OTHER PROCEDURES
Section
720.120
Rulemaking
720.121
Alternative Equivalent Testing Methods
720.122
Waste Delisting
720.130
Procedures for Solid Waste Determinations
720.131
Solid Waste Determinations
720.132
Boiler Determinations
720.133
Procedures for Determinations
720.140
Additional regulation of certain hazardous waste
Recycling Activities on a case—by—case Basis
720.141
Procedures for case—by—case regulation of hazardous
waste Recycling Activities
Appendix A
Overview of 40 CFR,
Subtitle C Regulations
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev. Stat.
1989,
ch.
111½, pars.
1022.4 and 1027).
SOURCE:
Adopted in R81—22,
43 PCB 427, at 5
Ill.
Req.
9781,
effective as noted in 35 Ill. Adm. Code 700.106; amended and
codified in R81-22, 45 PCB 317, at
6 Ill. Reg.
4828,
effective as
noted in 35 Ill.
Adm. Code 700.106;
amended in R82—19 at
7 Ill.
Req.
14015, effective Oct.
12, 1983;
amended in R84—9,
53 PCB 131
at
9
Ill. Req.
11819,
effective July 24,
1985;
amended in R85—
22 at 10 Iii.
Reg.
968, effective January
2,
1986;
amended in
R86—1
at 10 Ill. Reg.
13998,
effective August 12,
1986; amended
in R86-19 at 10 Ill. Reg.
20630, effective December 2,
1986;
amended in R86—28 at 11
Ill.
Reg.
6017, effective March 24,
1987;
amended in R86-46 at
1.
Ill. Reg.
13435, effective August
4,
1987; amended in R87—5 at
11
Ill. Req.
19280, effective November
125—180
9
L2,
1987;
amended in R87—26 at 12
Ill. Req. 2450,
effective
ranuary 15,
1988; amended in R87—39 at
12 Ill.
Reg.
12999,
~ffective July 29,
1988;
amended in R88—16 at 13
Ill.
Req.
362,
?ffective December 27,
1988; amended in R89—1 at 13 Ill.
Reg.
L8278, effective November 13,
1989; amended in R89—2 at
14
Ill.
~eg. 3075,
effective February 20,
1990; amended in R89—9 at
14
11.
Req.
6225, effective April 16,
1990; amended in R90—10 at 14
Cll. Reg.
16450,
effective September 25,
1990; amended in R90—li.
~t 15 Ill. Req.
9323,
effective June 17,
1991; amended in R91—1
~t 15 Ill. Req.
,
effective
-
SUBPART ,B:
DEFINITIONS
ection 720.110
Definitions
~hen used in 35 Ill.
Adin.
Code 720 through 725 and 728 only,
the
~o11owing terms have the meanings given below:
“Aboveground tank” means a device meeting the
definition of “tank” that is situated in such a way
that the entire surface area of the tank is completely
above the plane of the adjacent surrounding surface and
the entire surface area of the tank (including the tank
bottom)
is able to be visually inspected.
“Act” or “RCRA” means the Solid Waste Disposal Act,
as
amended by the Resource Conservation and Recovery Act
of 1976, as amended
(42 U.S.C.
6901 et seq.)
“Active life” of a facility means the period from the
initial receipt of hazardous waste at the facility
until the Agency receives certification of final
closure.
“Active portion” means that portion of a facility where
treatment,
storage or disposal operations are being or
have been conducted after May 19,
1980, and which is
not a closed portion.
(See also “closed portion” and
“inactive portion”.)
“Administrator” means the Administrator of the U.S.
Environmental Protection Agency or the Administrator’s
designee.
“Aqency” means the Illinois Environmental Protection
Agency.
“Ancillary equipment” means any device including,
but
not limited to, such devices as piping,
fittings,
flanges, valves and pumps, that is used to distribute,
meter or control the flow of hazardous waste from its
point of generation to storage or treatment tank(s),
125—181
10
between hazardous waste storage and treatment tanks to
a point of disposal onsite, or to a point of shipment
for disposal off-site.
“Aquifer” means a geologic formation, group of
formations or part of a formation capable of yielding a
significant amount of groundwater to wells or springs.
“Authorized representative” means the person
responsible for the overall operation of a facility or
an operational unit
(i.e., part of
a facility),
e.g.,
the plant manager,
superintendent or person of
equivalent responsibility.
“Board” means the Illinois Pollution Control Board.
“Boiler” means an enclosed device using controlled
flame combustion and having the following
characteristics:
The unit must have physical provisions for
recovering and exporting thermal energy in the
form of steam,
heated fluids or heated gases; and
the unit’s combustion chamber and primary energy
recovery section(s) must be of integral design.
To be of integral design, the combustion chamber
and the primary energy recovery section(s)
(such
as waterwalls and superheaters) must be physically
formed into one manufactured or assembled unit.
A
unit in which the combustion chamber and the
primary energy recovery section(s)
are joined only
by ducts or connections carrying flue gas is not
integrally designed; however, secondary energy
recovery equipment (such as economizers or air
preheaters) need not be physically formed into the
same unit as the combustion chamber and the
primary energy recovery section.
The following
units are not precluded from being boilers solely
because they are not of integral design:
process
heaters
(units that transfer energy directly to a
process stream), and fluidized bed combustion
units; and
While in operation, the unit must maintain a
thermal energy recovery efficiency of at least 60
percent, calculated in terms of the recovered
energy compared with the thermal value of the
fuel;
and
The unit must export and utilize at least 75
percent of the recovered energy, calculated on an
annual basis.
In this calculation, no credit
125—182
11
shall be given for recovered heat used internally
in the same unit.
(Examples of internal use are
the preheating of fuel or combustion air, and the
driving of induced or forced draft fans or
feedwater pumps); or
The unit is one which the Board has determined,
on
a case—by—case basis, to be a boiler, after
considering the standards in Section 720.132.
“Certification” means a statement of professional
opinion based upon knowledge and belief.
“Closed Portion” means that portion of a facility which
an owner or operator has closed in accordance with the
approved facility closure plan and all applicable
closure requirements.
(See also “active portion” and
“inactive portion”.)
“Component” means either the tank or ancillary
equipment of a tank system.
“Confined aquifer” means an aquifer bounded above and
below by impermeable beds or by beds of distinctly
lower permeability than that of the aquifer itself; an
aquifer containing confined groundwater.
“Container” means any portable device in which a
material
is stored, transported, treated, disposed of
or otherwise handled.
“Contingency plan” means
a document setting out an
organized, planned and coordinated course of action to
be followed in case of a fire, explosion or release of
hazardous waste or hazardous waste constituents which
could threaten human health or the environment.
“Corrosion expert” means a person who, by reason of
knowledge of the physical sciences and the principles
of engineering and mathematics, acquired by a
professional education and related practical
experience,
is qualified to engage in the practice of
corrosion control on buried or submerged metal piping
systems and metal tanks.
Such
a person must be
certified as being qualified by the National
Association of Corrosion Engineers
(NACE)
or be a
registered professional engineer who has certification
or licensing that includes education and experience in
corrosion control on buried or submerged metal piping
systems and metal tanks.
“Designated facility”.
125—183
12
“Designated facility” means a hazardous waste
treatment,
storage or disposal facility,
Which:
Has received a RCRA permit
(or interim
status) pursuant to 35 Ill.
Adin.
Code 702,
703 and 705;
Has received a RCRA permit from USEPA
pursuant to 40 CFR 124 and 270
(1989);
Has received a RCRA permit from a state
authorized by USEPA pursuant to 40 CFR 271
(1989); or
Is regulated under 35 Ill.
Adm. Code
721.106(c) (2)
or 266.Subpart F; and
Which has been designated on the manifest by the
generator pursuant to 35
111. Adm. Code 722.120.
If a waste
is destined to a facility in a state,
other than Illinois, which has been authorized by
USEPA pursuant to 40 CFR 271, but which has not
yet obtained authorization to regulate that waste
as hazardous, then the designated facility must be
a facility allowed by the receiving state to
accept such waste.
“Dike” means an embankment or ridge of either natural
or manmade materials used to prevent the movement of
liquids, sludges,
solids or other materials.
“Director” means the Director of the Illinois
Environmental Protection Agency.
“Discharge”
or “hazardous waste discharge” means the
accidental or intentional spilling, leaking, pumping,
pouring,
emitting, emptying or dumping of hazardous
waste into or on any land or water.
“Disposal” means the discharge, deposit,
injection,
dumping,
spilling, leaking or placing of any solid
waste or hazardous waste into or on any land or water
so that such solid waste or hazardous waste or any
constituent thereof may enter the environment or be
emitted into the air or discharged into any waters,
including groundwaters.
“Disposal facility” means a facility or part of a
125—184
13
facility at which hazardous waste is intentionally
placed into or on any land or water and at which waste
will remain after closure.
“Drip pad” means an engineered structure consisting of
a curbed, free—draining base, constructed of non—
earthen materials and designed to convey preservative
kick-back or drippage from treated wood, precipitation
and surface water run—on to an associated collection
system at wood preserving plants.
“Elementary neutralization unit” means a device which:
Is used for neutralizing wastes which are
hazardous only because they exhibit the
corrosivity characteristic defined in 35
Ill. Adm.
Code 721.122 or are listed in 35 Ill. Adm. Code
721.Subpart D only for this reason;
and
Meets the definition of tank, tank system,
container,
transport vehicle or vessel in this
Section.
“EPA” or “USEPA
“
means United States Environmental
Protection Agency.
“EPA hazardous waste number” or “USEPA hazardous waste
number” means the number assigned by EPA to each
hazardous waste listed in 35 111.
Adm. Code 721.Subpart
D and to each characteristic identified in 35 Ill. Adm.
Code 72l.Subpart C.
“EPA identification number” or “USEPA identification
number” means the number assigned by USEPA pursuant to
35 Ill.
Adm. Code 722 through 725 to each generator,
transporter and treatment, storage or disposal
facility.
“EPA region” means the states and territories found in
any one of the following ten regions:
Region I:
Maine, Vermont, New Hampshire,
Massachusetts, Connecticut and Rhode Island
Region II:
New York, New Jersey, Commonwealth of
Puerto Rico and the U.S. Virgin Islands
Region III:
Pennsylvania, Delaware, Maryland,
West Virginia, Virginia and the District of
Columbia
Region IV:
Kentucky, Tennessee, North Carolina,
125—185
14
Mississippi, Alabama, Georgia,
South Carolina and
Florida
Region V:
Minnesota,
Wisconsin, Illinois,
Michigan, Indiana and Ohio
Region VI:
New Mexico, Oklahoma, Arkansas,
Louisiana and Texas
Region VII:
Nebraska, Kansas, Missouri and Iowa
Region VIII:
•Montana, Wyoming, North Dakota,
South Dakota, Utah and Colorado
Region IX:
California,
Nevada, Arizona,
Hawaii,
Guam, American Samoa and Commonwealth of the
Northern Mariana Islands
Region
X:
Washington, Oregon,
Idaho and Alaska
“Equivalent method” means any testing or analytical
method approved by the Board pursuant to Section
720. 120.
“Existing hazardous waste management
(HWM)
facility” or
“existing facility” means a facility which was in
operation or for which construction commenced on or
before November 19,
1980.
A facility had commenced
construction if the owner or operator had obtained the
federal,
state and local approvals or permits necessary
to begin physical construction and either
A continuous on—site, physical construction program had
begun or the owner or operator had entered into
contractual obligations
——
which could not be cancelled
or modified without substantial loss
--
for physical
construction of the facility to be completed within a
reasonable time.”Existing portion” means that land
surface area of an existing waste management unit,
included in the original Part A permit application, on
which wastes have been placed prior to the issuance of
a permit.
“Existing tank system” or “existing component” means a
tank system or component that is used for the storage
or treatment of hazardous waste and that is in
operation,
or for which installation has commenced on
or prior to July 14,
1986.
Installation will be
considered to have commenced if the owner or operator
has obtained all federal, State and local approvals or
permits necessary.to begin physical construction of the
site or installation of the tank system and if either
125—186
15
A continuous on—site physical construction or
installation program has begun; or
The owner or áperator has entered into contractual
obligations
——
which cannot be canceled or
modified without substantial loss
--
for physical
construction of the site or installation of the
tank system to be completed within a reasonable
time.
~Facility~ means all contiguous land and structures,
other appurtenances and improvements on the land used
for treating, storing or disposing of hazardous waste.
A facility may consist of several treatment,
storage or
disposal operational units
(e.g.,
one or more
landfills,
surface impoundments or combinations of
them).
“Final closure” means the closure of all hazardous
waste management units at the facility in accordance
with all applicable closure requirements so that
hazardous waste management activities under 35
Ill.
Adm. Code 724 and 725 are no longer conducted at the
facility unless subject to the provisions of
35
Ill.
Adm. Code 722.134.
“Federal agency” means any department, agency or other
instrumentality of the federal government,
any
independent agency or establishment of the federal
government including any government corporation and the
Government Printing Office.
“Federal, state and local approvals or permits
necessary to begin physical construction” means permits
and approvals required under federal, state or local
hazardous waste control statutes, regulations or
ordinances.
“Food—chain crops” means tobacco,
crops grown for human
consumption and crops grown for feed for animals whose
products are consumed by humans.
“Freeboard” means the vertical distance between the top
of a tank or surface impoundment dike and the surface
of the waste contained therein.
“Free liquids” means liquids which readily separate
from the solid portion of a waste under ambient
temperature and pressure.
“Generator” means any person, by site, whose act or
125—187
16
process produce hazardous waste identified or listed in
35 Ill.
Adxn.
Code 721 or whose act first causes a
hazardous waste to become subject to regulation.
“Groundwater” means water below the land surface
in a
zone of saturation.
“Hazardous waste” means a hazardous waste as defined in
35
Iii. Adm. Code 721.103.
“Hazardous waste constituent” means a constituent which
caused the hazardous waste to be listed in 35 Ill.
Adin.
Code 721.Subpart D, or a constituent listed in of 35
Ill. Adm. Code 721.124.
“Hazardous waste management unit”
is a contiguous area
of land on or in which hazardous waste is placed, or
the largest area in which there is significant
likelihood of mixing hazardous waste constituents in
the same area.
Examples of hazardous waste management
units include a surface impoundment,
a waste pile,
a
land treatment area,
a landfill cell,
an incinerator,
a
tank and its associated piping and underlying
containment system and a container storage area.
A
container alone does not constitute a unit; the unit
includes containers and the land or pad upon which they
are placed.
“Inactive portion” means that portion of a facility
which is not operated after November 19,
1980.
(See
also “active portion” and “closed portion”.)
“Incinerator” means any enclosed device using
controlled flame combustion which is neither a “boiler”
nor an “industrial furnace”.
“Incompatible waste” means a hazardous waste which
is
suitable for:
Placement in a particular device or facility
because it may cause corrosion or decay of
containment materials (e.g.,
container inner
liners or tank walls); or
Commingling with another waste or material under
uncontrolled conditions because the commingling
might produce heat or pressure,
fire or explosion,
violent reaction, toxic dusts, mists,
fumes or
gases or flammable fumes or gases.
(See 35 Ill.
Adm. Code 725.Appendix E for
examples.)
125—188
17
“Industrial furnace” means any of the following
enclosed devices that are integral components of
manufacturing processes and that use controlled flame
devices to accomplish recovery of materials or energy:
Cement kilns
Lime kilns
Aggregate kilns
Phosphate kilns
Coke ovens
Blast furnaces
Smelting, melting and refining furnaces
(including
pyrometallurgical devices such as cupolas,
reverberator furnaces, sintering machines,
roasters and foundry furnaces)
Titanium dioxide chloride process oxidation
reactors
Methane reforming furnaces
Pulping liquor recovery furnaces
Combustion devices used in the recovery of sulfur
values from spent sulfuric acid
Any other such device as the Agency determines to
be an “Industrial Furnace” on the basis of one or
more of the following factors:
The design and use of the device primarily to
accomplish recovery of material products;
The use of the device to burn or reduce raw
materials to make a material product;
The use of the device to burn or reduce
secondary materials as effective substitutes
for raw materials,
in processes using raw
materials as principal feedstocks;
The use of the device to burn or reduce
secondary materials as ingredients
in an
industrial process to make a material
product;
125— 189
18
The use of the device in common industrial
practice to produce a material product; and
Other relevant factors.
“Individual generation site” means the contiguous site
at or on which one or more hazardous wastes are
generated.
An individual generation site,
such as a
large manufacturing plant, may have one or more sources
of hazardous waste but is considered a single or
individual generation site if the site or property is
contiguous.
“Inground tank” means a device meeting the definition
of “tank” whereby a portion of the tank wall is
situated to any degree within the ground, thereby
preventing visual inspection of that external surface
area of the tank that is in the ground.
“In operation” refers to a facility which
is treating,
storing or disposing of hazardous waste.
“Injection well” means a well into which fluids are
being injected.
(See also “underground injection”.)
“Inner liner” means a continuous layer of material
placed inside a tank or container which protects the
construction materials of the tank or container from
the contained waste or reagents used to treat the
waste.
“Installation inspector” means a person who,
by reason
of knowledge of the physical sciences and the
principles of engineering, acquired by a professional
education and related practical experience,
is
qualified to supervise the installation of tank
systems.
“International shipment” means the transportation of
hazardous waste into or out of the jurisdiction of the
United States.
“Land treatment facility” means a facility or part of a
facility at which hazardous waste is applied onto or
incorporated into the soil surface; such facilities are
disposal facilities if the waste will remain after
closure.
“Landfill” means a disposal facility or part of a
facility where hazardous waste is placed in or on land
and which is not a pile,
a land treatment facility,
a
125—190
19
surface impoundment, an underground injection well,
a
salt dome formation, an underground mine or a cave.
“Landfill cell” means a discrete volume of a hazardous
waste landfill which uses a liner to provide isolation
of wastes from adjacent cells or wastes.
Examples of
landfill cells are trenches and pits.
“Leachate” means any liquid,
including any suspended
components in the liquid, that has percolated through
or drained from hazardous waste.
“Liner” means a continuous layer of natural or manmade
materials beneath or on the sides of a surface
impoundment, landfill or landfill cell, which restricts
the downward or lateral escape of hazardous waste,
hazardous waste constituents or leachate.
“Leak—detection system” means
a system capable of
detecting the failure of either the primary or
secondary containment structure or the presence of a
release of hazardous waste or accumulated liquid in the
secondary containment structure.
Such a system must
employ operational controls
(e.g., daily visual
inspections for releases into the secondary containment
system of aboveground tanks)
or consist of an
interstitial monitoring device designed to detect
continuously and automatically the failure of the
primary or secondary containment structure or the
presence of a release of hazardous waste into the
secondary containment structure.
“Management” or “hazardous waste management” means the
systematic control of the collection,
source
separation, storage, transportation,
processing,
treatment,
recovery and disposal of hazardous waste.
“Manifest” means the shipping document originated and
signed by the generator which contains the information
required by 35 Ill.
Adm. Code.722.Subpart B.
“Manifest document number” means the USEPA twelve digit
identification number assigned to the generator plus a
unique five digit document number assigned to the
manifest by the generator for recording and reporting
purposes.
“Mining overburden returned to the mine site” means any
material overlying an economic mineral deposit which is
removed to gain access to that deposit and is then used
for reclamation of a surface mine.
125—19 1
20
“Miscellaneous unit” means a hazardous waste management
unit where hazardous waste is treated,
stored or
disposed of and which is not a container, tank,
tank
system, surface impoundment, pile,
land treatment unit,
landfill,
incinerator, boiler,
industrial furnace,
underground injection well with appropriate technical
standards under 35 Ill. Adm. Code 730, or a unit
eligible for a research, development and demonstration
permit under 35 Ill. Adm. Code 703.231.
“Movement” means that hazardous waste transported to a
facility in an individual vehicle.
“New hazardous waste management facility” or “new
facility” means
a facility which began operation,
or
for which construction commenced, after November 19,
1980.
(See also “Existing hazardous waste management
facility”.)
“New tank system” or “new tank component” means a tank
system or component that will be used for the storage
or treatment of hazardous waste and for which
installation commenced after July 14,
1986; except,
however,
for purposes of
35 Ill. Adm.
Code
724.293(g) (2) and 725.293(g) (2), a new tank system is
one for which construction commences after July 14,
1986.
(See also “existing tank system.”)
“Onground tank” means a device meeting the definition
of “tank” that is situated in such a way that the
bottom of the tank is on the same level as the adjacent
surrounding surfaces so that the external tank bottom
cannot be visually inspected.
“On—site” means the same or geographically contiguous
property which may be divided by public or private
right—of—way, provided the entrance and exit between
the properties is at a crossroads intersection and
access is by crossing as opposed to going along the
right-of-way.
Noncontiguous properties owned by the
same person but connected by
a right—of-way which he
controls and to which the public does not have access
is also considered on—site property.
“Open burning” means the combustion of any material
without the following characteristics:
Control of combustion air to maintain adequate
temperature for efficient combustion;
Containment of the combustion reaction in an
enclosed device to provide sufficient residence
125— 192
21
time and mixing for complete combustion;
and
Control of emission of the gaseous combustion
products.
(See also “incineration” and “thermal treatment”.)
“Operator” means the person responsible for the overall
operation of a facility.
“Owner” means the person who owns a facility or part of
a
facility.
“Partial closure” means the closure of a hazardous
waste management unit in accordance with the applicable
closure requirements of 35 Ill. Adm. Code 724 or 725 at
a facility which contains other active hazardous waste
management units.
For example, partial closure may
include the closure of a tank (including its associated
piping and underlying containment systems), landfill
cell,
surface impoundment,
waste pile or other
hazardous waste management unit, while other units of
the same facility continue to operate.
“Person” means an individual,
trust,
firm,
joint stock
company,
federal agency, corporation (including a
government corporation), partnership, association,
state, municipality, commission, political subdivision
of
a state or any interstate body.
“Personnel” or “facility personnel” means all persons
who work at or oversee the operations of a hazardous
waste facility and whose actions or failure to act may
result in noncompliance with the requirements of 35
Ill. Adm. Code 724 or 725.
“Pile” means any noncontainerized accumulation of
solid, non—flowing hazardous waste that is used for
treatment or storage.
“Point source” means any discernible, confined and
discrete conveyance including, but not limited to, any
pipe, ditch, channel, tunnel, conduit, well,
discrete
fissure, container, rolling stock, concentrated animal
feeding operation or vessel or other floating craft
from which pollutants are or may be discharged.
This
term does not include return flows from irrigated
agriculture.
“Publicly owned treatment works” or “POTW” is as
defined in 35 Ill. Adm. Code 310.110.
125—193
22
“Regional Administrator” means the Regional
Administrator for the EPA Region in which the facility
is located or the Regional Administrator’s designee.
“Representative sample” means a sample of a universe or
whole
(e.g., waste pile,
lagoon, groundwater) which can
be expected to exhibit the average properties of the
universe or whole.
“Runoff” means any rainwater,
leachate or other liquid
that drains over land from any part of a facility.
“Runon” means any rainwater,
leachate or other liquid
that drains over land onto any part of a facility.
“Saturated
zone”
or
“zone
of
saturation”
means
that
part
of
the
earth’s
crust
in
which
all voids are filled
with
water.
“SIC
Code”
means
Standard
Industrial
Code
as
defined in
Standard Industrial Classification Manual, incorporated
by reference in Section 720.111.
“Sludge” means any solid,
semi—solid or liquid waste
generated from a municipal,
commercial or industrial
wastewater treatment plant, water supply treatment
plant or air pollution control facility exclusive of
the treated effluent from a wastewater treatment plant.
“Small Quantity Generator” means a generator which
generates less than 1000 kg of hazardous waste in a
calendar month.
“Solid waste” means a solid waste as defined
in
35 Ill.
Adm.
Code
721.102.
“Sump”
means
any
pit
or
reservoir
that
meets
the
definition
of
tank and those troughs or trenches
connected
to
it
that
serve
to
collect
hazardous
waste
for
transport
to
hazardous
waste
storage,
treatment
or
disposal facilities.
“State” means any of the several states, the District
of Columbia, the Commonwealth of Puerto Rico, the
Virgin Islands, Guam, American Samoa and the
Commonwealth of the Northern Mariana Islands.
“Storage” means the holding of hazardous waste for a
temporary period, at the end of which the hazardous
waste is treated, disposed of or stored elsewhere.
“Surface impoundment” or “impoundment” means a facility
125—194
23
or part of a facility which is a natural topographic
depression, manmade excavation or diked area formed
primarily of earthen materials (although it may be
lined with manmade materials) which is designed to hold
an accumulation of liquid wastes or wastes containing
free liquids and which is not an injection well.
Examples of surface impoundments are holding, storage,
settling and aeration pits,
ponds and lagoons.
“Tank” means a stationary device, designed to contain
an accumulation of hazardous waste which is constructed
primarily of nonearthen materials (e.g.,
wood,
concrete, steel, plastic) which provide structural
support.
“Tank system” means a hazardous waste storage or
treatment tank and
its
associated
ancillary
equipment
and containment system.
“Thermal treatment” means the treatment of hazardous
waste in a device which uses elevated temperatures as
the primary means to change the chemical, physical or
biological character or composition of the hazardous
waste.
Examples of thermal treatment processes are
incineration, molten salt, pyrolysis,
calcination, wet
air oxidation and microwave discharge.
(See also
“incinerator” and “open burning”.)
“Totally enclosed treatment facility” means a facility
for the treatment of hazardous waste which is directly
connected to an industrial production process and which
is constructed and operated in a manner which prevents
the release of any hazardous waste or any constituent
thereof into the environment during treatment.
An
example is a pipe
in which waste acid is neutralized.
“Transfer
facility”
means
any
transportation
related
facility including loading docks, parking areas,
storage areas and other similar areas where shipments
of hazardous waste are held during the normal course of
transportation.
“Transport vehicle” means a motor vehicle or rail car
used for the transportation of cargo by any mode.
Each
cargo—carrying body (trailer, railroad freight car,
etc.)
is
a separate transport vehicle.
“Transportation” means the movement of hazardous waste
by air,
rail, highway or water.
“Transporter” means a person engaged in the off—site
transportation of hazardous waste by air,
rail,
highway
125—195
24
or water.
“Treatability study” means:
A study in which
a hazardous waste is subjected to
a treatment process to determine:
Whether the waste is amenable to the
treatment process.
What pretreatment
(if any)
is required.
The optimal process conditions needed to
achieve the desired treatment.
The efficiency of a treatment process for a
specific waste or wastes.
Or,
The characteristics and volumes of residuals
from a particular treatment process.
Also included in this definition for the purpose
of 35
Ill.
Adin.
Code 721.104(e)
and
(f) exemptions
are liner compatibility, corrosion and other
material compatibility studies and toxicological
and health effects studies.
A “treatability
study” is not a means to commercially treat or
dispose of hazardous waste.
“Treatment” means any method, technique or process,
including neutralization, designed to change the
physical, chemical or biological character or
composition of any hazardous waste so as to neutralize
such waste,
or so as to recover energy or material
resources from the waste or so as to render such waste
non—hazardous or less hazardous; safer to transport,
store or dispose of;
or amenable for recovery, amenable
for storage or reduced in volume.
“Treatment
zone” means a soil area of the unsaturated
zone of a land treatment unit within which hazardous
constituents are degraded, transformed or immobilized.
“Underground injection” means the subsurface
emplacement of fluids through a bored,
drilled or
driven well;
or through a dug well,
where the depth of
the dug well is greater than the largest surface
dimension.
(See also “injection well”.)
“Underground
tank”
means
a
device
meeting
the
definition of “tank” whose entire surface area is
totally below the surface of and covered by the ground.
125—196
25
“Unfit—for-use tank system” means
a tank system that
has been determined through an integrity assessment or
other inspection to be no longer capable of storing or
treating hazardous waste without posing a threat of
release of hazardous waste to the environment.
“Uppermost aquifer” means the geologic formation
nearest the natural ground surface that is an aquifer,
as well as lower aquifers that are hydraulically
interconnected with this aquifer within the facility’s
property boundary.
“United States” means the 50 States, the District of
Columbia, the Commonwealth of Puerto Rico, the U.S.
Virgin Islands, Guam, American Samoa and the
Commonwealth of the Northern Mariana Islands.
“Unsaturated zone” or “zone of aeration” means the zone
between the land surface and the water table.
“USEPA” means United States Environmental Protection
Agency.
“Vessel”
includes every description of watercraft, used
or capable of being used as a means of transportation
on the water.
“Wastewater treatment unit” means
a device which:
Is part of a wastewater treatment facility which
has an NPDES permit pursuant to 35
Ill.
Adm. Code
309 or a pretreatment permit or authorization to
discharge pursuant to 35
Ill. Adm. Code 310; and
Receives and treats or stores an influent
wastewater which is a hazardous waste as defined
in 35
Ill. Adm. Code 721.103, or generates and
accumulates a wastewater treatment sludge which is
a hazardous waste as defined in 35 Ill. Adm. Code
721.103, or treats or stores a wastewater
treatment sludge which is
a hazardous waste as
defined in 35
Ill. Adm. Code 721.103; and
Meets the definition of tank or tank system in
this Section.
“Water
(bulk shipment)” means the bulk transportation
of hazardous waste which is loaded or carried on board
a vessel without containers or labels.
“Well” means any shaft or pit dug or bored into the
125—197
26
earth,
generally of a cylindrical form, and often
walled with bricks or tubing to prevent the earth from
caving in.
“Well injection”
(See “underground injection”).
“Zone of engineering control” means an area under the
control of the owner or operator that, upon detection
of a hazardous waste release, can be readily cleaned up
prior to the release of hazardous waste or hazardous
constituents to groundwater or surface water.
(Source:
Amended at 15
Ill. Req.
,
effective
)
Section 720.111
References
a)
The following publications are incorporated by
reference:
ANSI.
Available from the American National
Standards Institute,
1430 Broadway, New York, New
York
10018,
(212)
354—3300:
ANSI B31.3 and B31.4.
See ASNE/ANSI B31.3
and B31.4
ACI.
Available from the American Concrete
Institute, Box 19150, Redford Station, Detroit,
Michigan
48219:
ACI 318-83:
“Building Code Requirements for
Reinforced Concrete”,
adopted September,
1983.
API.
Available from the American Petroleum
Institute, 1220 L Street,
N.W., Washington,
D.C.
20005,
(202)
682—8000:
“Guide for Inspection of Refinery Equipment,
Chapter XIII, Atmospheric and Low Pressure
Storage Tanks,” 4th Edition,
1981, reaffirmed
December,
1987.
“Cathodic Protection of Underground Petroleum
Storage Tanks and Piping Systems,” API
Recommended Practice 1632, Second Edition,
December,
1987.
“Installation of Underground Petroleum
Storage Systems,” API Recommended Practice
1615,
Fourth Edition, November,
1987.
125—198
27
APTI.
Available from the Air and Waste Management
Association, Box 2861, Pittsburgh,
PA
15230,
(412)
232—3444:
APTI Course 415:
Control of Gaseous
Emissions,
EPA Publication EPA—450/2-81-005,
December,
1981.
ASNE.
Available from the American Society of
Mechanical Engineers,
345 East 47th Street, New
York,
NY
10017,
(212)
705—7722:
“Chemical Plant and Petroleum Refinery
Piping”, ASME/ANSI B31.3—1987,
as
supplemented by B3l.3a—1988 and B31.3b—1988.
Also available from ANSI.
“Liquid Transportation Systems for
Hydrocarbons, Liquid Petroleum Gas, Anhydrous
Ammonia, and Alcohols”, ASME/ANSI B31.4—
1986,
as supplemented by B31.4a—1987.
Also
available from ANSI.
ASTM.
Available from American Society for Testing
and Materials,
1916 Race Street, Philadelphia, PA
19103,
(215)
299—5400:
ASTM C94-90, Standard
Specification
for
Ready-Mixed Concrete, approved March 30,
1990.
ASTM D93-85, Standard Test Methods for Flash
Point by Pensky-Martens Closed Testerapproved
October 25,
1985.
ASTM D1946—90, Standard Practice for Analysis
of Reformed Gas by Gas Chromatography,
Approved March
30,
1990.
ASTM D2267-88, Standard Test Method for
Aromatics in Light Naphthas and Aviation
Gasolines by Gas Chromatography, approved
November 17,
1988.
ASTN D2382-88, Standard Test Method for Heat
of Combustion of Hydrocarbon Fuels by Bomb
Calorimeter
(High Precision Method), approved
October 31,
1988.
ASTM D2879-86, Standard Test Method for Vapor
Pressure—Temperature Relationship and Initial
125—199
28
Decomposition Temperature of Liquids by
Isoteniscope, approved October 31,
1986.
ASTM D3828-87,
Standard Test Methods for
Flash Point of Liquids by Setaflash Closed
Tester, approved December 14,
1988.
ASTN E168-88, Standard Practices for General
Techniques of Infrared Quantitative Analysis,
approved Nay 27,
1988.
ASTN E169.-87, Standard Practices for General
Techniques of Ultraviolet-Visible
Quantitative Analysis, approved February 1,
1987.
ASTN E260-85, Standard Practice for Packed
Column Gas Chromatography, approved June 28,
1985.
GPO.
Available from the Superintendent of
Documents,
U.S. Government Printing Office,
Washington,
D.C.
20401,
(202)
783—3238:
Standard Industrial Classification Manual
(1972),
and 1977 Supplement,
republished in
1983
NACE.
Available from the National Association of
Corrosion Engineers,
1400 South Creek Dr.,
Houston, TX
77084,
(713)
492—0535:
“Control of External Corrosion on Metallic
Buried, Partially Buried,
or Submerged Liquid
Storage Systems”, NACE Recommended Practice
RP0285-85, approved March,
1985.
NFPA.
Available from the National Fire Protection
Association, Batterymarch Park,
Boston, MA
02269,
(617)
770—3000 or
(800)
344—3555:
“Flammable and Combustible Liquids Code” NFPA
30, issued July 17,
1987.
Also available
from ANSI.
NTIS.
Available from the National Technical
Information Service, 5285 Port Royal Road,
Springfield, VA
22161,
(703)
487—4600:
“Generic Quality Assurance Project Plan for
Land Disposal Restrictions Program”, EPA/530-
SW-87-011, March 15,
1987.
(Document number
125—200
29
PB 88—170766.)
“Methods for Chemical Analysis of Water and
Wastes”, Third Edition, March,
1983.
(Document number PB 84—128677)
“Petitions to Delist Hazardous Wastes
--
A
Guidance Manual”,
EPA/530—SW-85—003,
April,
1985.
(Document Number PB 85-194488
“Procedures Manual for Ground Water
Monitoring at Solid Waste Disposal
Facilities”, EPA—530/SW—611,
1977.
(Document
number PB 84—174820)
“Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods,” EPA Publication
number SW—846 (Second Edition,
1982 as
amended by Update
I
(April,
1984)
and Update
II
(April,
1985))
(Document number PB 87-
120291)
STI.
Available from the Steel Tank Institute,
728
Anthony Trail,
Northbrook,
IL
60062,
(312)
498—
1980:
“Standard for Dual Wall Underground Steel
Storage Tanks”
(1986).
USEPA.
Available from United States Environmental
Protection Agency,
Office of Drinking Water,
State
Programs Division, WH 550 E, Washington, D.C.
20460:
“Technical Assistance Document:
Corrosion,
Its Detection and Control in Injection
Wells”, EPA 570/9—87—002, August,
1987.
USEPA.
Available from tJSEPA, Room M2427,
401 N
Street SW, Washington,
D.C.
20460,
(202)
475—
9327:
Method 8290 proposed for inclusion in “Test
Methods for Evaluating Solid Waste,
Physical/Chemical Methods”, SW 846, Number F—
90—WPWF—FFFFF
b)
Code of Federal Regulations.
Available from the
Superintendent of Documents,
U.S. Government Printing
Office, Washington,
D.C.
20401,
(202)
783—3238:
125—20 1
30
10 CFR 20, Appendix B
(1990)
40 CFR 60
(1990)
40 CFR 61, Subpart V
(1990)
40 CFR 136 (1990)
40 CFR 142
(1990)
40 CFR 220
(1990)
40 CFR 260.20
(1990)
40 CFR 264
(1990)
40 CFR 302.4,
302.5 and 302.6
(1990)
40 CFR 761
(1990)
C)
Federal Statutes
Section 3004 of the Resource Conservation and Recovery
Act
(42 U.S.C.
6901 et seq.), as amended through
December 31,
1987.
d)
This Section incorporates no later editions or
amendments.
(Source:
Amended at
15 Ill. Req.
,
effective
125—202
31
Section
721.101
721. 102
721.103
721.104
721.105
721.106
721.107
721.108
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 721
IDENTIFICATION AND LISTING OF HAZARDOUS WASTE
SUBPART A:
GENERAL PROVISIONS
Purpose and Scope
Definition of Solid Waste
Definition of Hazardous Waste
Exclusions
Special Requirements for Hazardous Waste Generated by
Small Quantity Generators
Requirements for Recyclable Materials
Residues of Hazardous Waste
in Empty Containers
PCB Wastes Regulated under TSCA
CUPBARTSUBPART
B:
CRITERIA
FOR
IDENTIFYING
THE
CHARACTERISTICS
OF HAZARDOUS WASTE AND FOR LISTING HAZARDOUS WASTES
Section
721.110
Criteria for Identifying the Characteristics of
Hazardous Waste
721.111
Criteria for Listing Hazardous Waste
SUBPART
C:
CHARACTERISTICS
OF
HAZARDOUS
WASTE
General
Characteristic
of
Ignitability
Characteristic of Corrosivity
Characteristic of Reactivity
Toxicity
Characteristic
SUBPART
D:
LISTS
OF
HAZARDOUS
WASTE
General
Hazardous Wastes From Nonspecific Sources
Hazardous Waste from Specific Sources
Discarded Commercial Chemical Products, Off-
Specification Species, Container Residues and Spill
Residues Thereof
721.135
Wood Preserving Wastes
Appendix A
Appendix B
Appendix C
Table A
Table B
Representative Sampling Methods
Method 1311 Toxicity Characteristic Leaching
Procedure
(TCLP)
Chemical Analysis Test Methods
Analytical Characteristics of Organic Chemicals
(Repealed)
Analytical Characteristics of Inorganic Species
Section
721.120
721.121
721.122
721. 123
721.124
Section
721.130
721.131
721.132
721.133
125—203
32
(Repealed)
Table C
Sample Preparation/Sample Introduction Techniques
(Repealed)
Appendix G
Basis for Listing Hazardous Wastes
Appendix H
Hazardous Constituents
Appendix I
Wastes Excluded under Section 720.120 and 720.122
Table A
Wastes Excluded from Non—Specific Sources
Table B
Wastes Excluded from Specific Sources
Table C
Wastes Excluded From Commercial Chemical Products,
Off-Specification Species, Container Residues,
and
Soil Residues Thereof
Appendix J
Method of Analysis for Chlorinated Dibenzo—p-
Dioxins and Dibenzofurans
Appendix
Z
Table to Section 721.102
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev.
Stat.
1989,
ch.
111½, pars.
1022.4 and 1027).
SOURCE:
Adopted in R8l-22,
43 PCB 427, at
5 Ill.
Req.
9781,
effective as noted in 35 Ill.
Adm. Code 700.106; amended and
codified in R81—22, 45 PCB 317,
at
6 Ill.
Req. 4828,
effective as
noted in 35 Ill.
Adm. Code 700.106; amended in R82-18,
51 PCB 31,
at 7 Ill.
Req.
2518,
effective February 22,
1983; amended in R82—
19,
53 PCB 131,
at
7 Ill.
Reg.
13999, effective October
12,
1983;
amended in R84—34,
61 PCB 247, at
8 Ill. Req.
24562,
effective
December
11,
1984; amended in R84—9, at 9 Ill.
Req.
11834,
effective July 24,
1985; amended in R85—22 at 10
Ill. Reg.
998,
effective January 2,
1986;
amended in R85—2
at 10
Ill. Reg.
8112,
effective May 2,
1986; amended in R86—1 at 10 Ill. Reg.
14002,
effective August 12,
1986;
amended in R86—19 at 10 Ill. Req.
20647,
effective December 2,
1986; amended in R86—28 at
11
Ill.
Req. 6035,
effective March 24,
1987;
amended in R86—46 at 11 Ill.
Req.
13466, effective August
4,
1987; amended in R87—32 at 11
Ill. Reg.
16698,
effective September 30,
1987; amended in R87—5
at 11 Ill.
Reg.
19303, effective November 12,
1987; amended in
R87—26 at 12
Ill. Req.
2456,
effective January 15,
1988;
amended
in R87—30 at 12 Ill.
Reg.
12070, effective July 12,
1988; amended
in R87—39 at 12 Ill.
Reg.
13006, effective July 29,
1988;
amended
in R88—l6 at 13 Ill.
Req.
382, effective December 27,
1988;
amended in R89-1 at
13
Ill.
Req.
18300, effective November 13,
1989;
amended in R90-2
at 14
Ill.
Reg.
14401, effective August
22,
1990; amended in R90—1O at 14
Ill. Reg.
16472, effective
September 25, 1990;
amended in R90-1’7 at 15 Ill.
Req.
7950,
effective May
9,
1991; amended in R90—11 at
15 Ill.
Req.
9332,
effective June 17,
1991; amended in R91-1 at 15 Ill.
Req.
effective
SUBPART A:
GENERAL PROVISIONS
Section 721.104
Exclusions
125—204
33
a)
Materials which are not solid wastes.
The following
materials are not solid wastes for the purpose of this
Part:
1)
Sewage:
A)
‘Domestic sewage; and
B)
Any mixture of domestic sewage and other
waste that passes through a sewer system to
publicly—owned treatment works for treatment.
“Domestic sewage” means untreated sanitary
wastes that pass through a sewer system.
2)
Industrial wastewater discharges that are point
source discharges with NPDES permits issued by the
Agency pursuant to Section 12(f) of the
Environmental Protection Act and 35 Ill. Adm. Code
309.
BOARD NOTE:
This exclusion applies only to the
actual point source discharge.
It does not
exclude industrial wastewaters while they are
being collected,
stored or treated before
discharge,
nor does it exclude sludges that are
generated by industrial wastewater treatment.
3)
Irrigation return flows.
4)
Source,
special nuclear or by—product material as
defined by the Atomic Energy Act of 1954, as
amended
(42 U.S.C.
2011 et seq.)
5)
Materials subjected to in-situ mining techniques
which are not removed from the ground as part of
the extraction process.
6)
Pulping liquors
(i.e.,
black liquor) that are
reclaimed in a pulping liquor recovery furnace and
then reused
in the pulping process, unless
accumulated speculatively as defined in Section
721.101(c);
7)
Spent sulfuric acid used to produce virgin
sulfuric acid, unless it is accumulated
speculatively as defined in Section 721.101(c).
8)
Secondary materials that are reclaimed and
returned to the original process or processes in
which they were generated where they are reused in
the production process, provided:
125—205
34
A)
Only tank storage is involved, and the entire
process through completion of reclamation is
closed by being entirely connected with pipes
or other comparable enclosed means of
conveyance;
B)
Reclamation does not involve controlled flame
combustion
(such as occurs in boilers,
industrial furnaces or incinerators);
C)
The secondary materials are never accumulated
in such tanks for over twelve months without
being reclaimed; and
D)
The reclaimed material is not used to produce
‘a fuel, or used to produce products that are
used in a manner constituting disposal.
.21
Wood preserving wastes.
~j
Spent wood preserving solutions that have
been used and are reclaimed and reused for
their original intended purpose;
and
~
Wastewaters from the wood preserving process
that have been reclaimed and are reused to
treat wood.
b)
Solid wastes which are not hazardous wastes.
The
following solid wastes are not hazardous wastes:
1)
Household waste,
including household waste that
has been collected, transported, stored, treated,
disposed, recovered
(e.g., refuse—derived fuel) or
reused.
“Household waste” means any waste
material
(including garbage, trash and sanitary
wastes in septic tanks) derived from households
(including single and multiple residences, hotels
and motels, bunkhouses, ranger stations, crew
quarters, campgrounds, picnic grounds and day—use
recreation areas).
•A resource recovery facility
managing municipal solid waste shall not, be deemed
to be treating,
storing, disposing of or otherwise
managing hazardous wastes for the purposes of
regulation under this Part,
if such facility:
A)
Receives and burns only:
i)
Household waste (from single and
multiple dwellings, hotels, motels and
other residential sources) and
125—206
35
ii)
Solid waste from commercial or
industrial sources that does not contain
hazardous waste; and
B)
Such facility does not accept hazardous waste
and the owner or operator of such facility
has established contractual requirements or
other appropriate notification or inspectior1
procedures to assure that hazardous wastes
are not received at or burned in such
facility.
2)
Solid wastes generated by any of the following and
which are returned to the soil as fertilizers:
A)
The growing and harvesting of agricultural
crops.
B)
The raising of animals,
including animal
manures.
3)
Mining overburden returned to the mine site.
4)
Fly ash waste, bottom ash waste, slag waste, and
flue gas emission control waste generated
primarily from the combustion of coal or other
fossil fuels.
5)
Drilling fluids, produced waters, and other wastes
associated with the exploration, development, or
production of crude oil, natural gas or geothermal
energy.
6)
Chromium wastes:
A)
Wastes which fail the test for the toxicity
characteristic (Section 721.124 and Appendix
B)
because chromium is present or are listed
in Subpart D due to the presence of chromium,
which do not fail the test for the toxicity
characteristic for any other constituent or
are not listed due to the presence of any
other constituent, and which do not fail the
test for any other characteristic,
if it is
shown by a waste generator or by waste
generators that:
i)
The chromium in the waste is exclusively
(or nearly exclusively) trivalent
chromium; and
ii)
The waste
is generated from an
125—207
36
industrial process which uses trivalent
chromium exclusively
(or nearly
exclusively) and the process does not
generate hexavalent chromium; and
iii) The waste is typically and frequently
managed in non—oxidizing environments.
B)
Specific wastes which meet the standard in
subsections
(b) (6) (A) (i),
(ii) and
(iii)
(so
long as they do not fail the test for the
characteristic of EP toxicity, and do not
fail the test for any other characteristic)
are
i)
Chrome
(blue)
trimmings generated by the
following subcategories of the leather
tanning and finishing industry; hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
ii)
Chrome
(blue)
shavings generated by the
following subcategories of the leather
tanning and finishing industry; hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
iii) Buffing dust generated by the following
subcategories of the leather tanning and
finishing industry:
hair pulp/chrome
tan/retan/wet finish; hair save/chrome
tan/retan/wet finish; retan/wet finish;
no beaxnhouse; through-the-blue.
iv)
Sewer screenings generated by the
following subcategories of the leather
tanning and finishing industry:
hair
pulp/chrome tan/retan/wet finish; hair
save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
the-blue; and shearling.
v)
Wastewater treatment sludges generated
by the following subcategories of the
leather tanning and finishing industry:
hair pulp/chrome tan/retan/wet finish;
hair save/chrome tan/retan/wet finish;
retan/wet finish; no beamhouse; through-
125—208
37
the-blue; and shearling.
vi)
Wastewater treatment sludges generated
by the following subcategories of the
leather tanning and finishing industry:
hair pulp/chrome tan/retan/wet finish;
hair save/chrome tan/retan/wet finish;
and through-the-blue.
vii) Waste scrap leather from the leather
tanning industry, the shoe manufacturing
industry, and other leather product
manufacturing industries.
viii)
Wastewater treatment sludges from
the production of titanium dioxide
pigment using chromium—bearing ores
by the chloride process.
7)
Solid waste from the extraction, beneficiation and
processing of ores and minerals (including coal),
including phosphate rock and overburden from the
mining of uranium ore.
For purposes of this
subsection,
beneficiation of ores and minerals
is
restricted to the following activities:
crushing,
grinding, washing,
dissolution, crystallization,
filtration,
sorting,
sizing,
drying,
sintering,
pelletizing, briquetting, calcining to remove
water or carbon dioxide, roasting, autoclaving or
chlorination in preparation for leaching (except
where the roasting or autoclaving or
chlorination)/leaching sequence produces a final
or intermediate product that does not undergo
further beneficiation or processing), gravity
concentration, magnetic separation,
electrostatic
separation,
floatation,
ion exchange, solvent
extraction,
electrowinning, precipitation,
amalgamation, and heap, dump, vat tank and in situ
leaching.
For the purposes of this subsection,
solid waste from the processing of ores and
minerals will include only the following wastes:
A)
Slag from primary copper processing;
B)
Slag from primary lead processing;
C)
Red and brown muds from bauxite refining;
D)
Phosphogypsum from phosphoric acid
production;
E)
Slag from elemental phosphorus production;
125—209
38
F)
Gasifier ash from coal gasification;
G)
Process wastewater from coal gasification;
H)
Calcium sulfate wastewater treatment plant
sludge from primary copper processing;
I)
Slag tailings from primary copper processing;
J)
Fluorogypsum from hydrofluoric acid
production;
K)
Process wastewater from hydrofluoric acid
production;
L)
Air pollution control dust/sludge from iron
blast furnaces;
M)
Iron blast furnace slag;
N)
Treated residue from roasting/leaching of
chrome ore;
0)
Process wastewater from primary magnesium
processing by the anhydrous process;
P)
Process wastewater from phosphoric acid
production;
Q)
Basic oxygen furnace and open hearth furnace
air pollution control dust/sludge from carbon
steel production;
R)
Basic oxygen furnace and open hearth furnace
slag from carbon steel production;
5)
Chloride processing waste solids from
titanium tetrachioride production;
T)
Slag from primary zinc smelting;
and,
U)
Until June 30,
1991,
process wastewater,
acid
plant blowdown and wastewater treatment plant
solid3 from primary zinc smelting and
refining, except for wastewatcr treatment
plant solids which are hazardou3 by
characteristic and which arc not processed.
8)
Cement kiln dust waste.
9)
Solid waste which consists of discarded wood or
125—210
39
wood products which fails the test for the
toxicity characteristic solely for arsenic and
which
is not a hazardous waste for any other
reason or reasons if the waste is generated by
persons who utilize the arsenical-treated wood and
wood products for these materials’
intended end
use..
10)
Petroleum-contaminated media and debris that fail
the test for the toxicity characteristic of
Section 721.124 (hazardous waste codes D018
through D043 only)
and are subject to corrective
action regulations under 35 Ill.
Adm. Code 731.
~fl
Groundwater that exhibits the toxicity
characteristic in Section 721.124 that is
reiniected or reinfiltrated pursuant to existing
hydrocarbon recovery operations undertaken at
petroleum refineries, marketing terminals or bulk
Plants handling crude petroleum or intermediate
Products of petroleum refining until March
25,
1991.
c)
Hazardous wastes which are exempted from certain
regulations.
A hazardous waste which is generated in a
product or raw material storage tank,
a product or raw
material transport vehicle or vessel,
a product or raw
material pipeline, or in a manufacturing process unit
or an associated non—waste—treatment manufacturing
unit,
is not subject to regulation under 35 Ill. Adm.
Code 702,
703,
705 and 722 through 725 and 728 or to
the notification requirements of Section 3010 of RCRA
until it exits the unit in which it was generated,
unless the unit is a surface impoundment, or unless the
hazardous waste remains in the unit more than 90 days
after the unit ceases to be operated for manufacturing,
or for storage or transportation of product or raw
materials.
d)
Samples
1)
Except as provided in subsection
(d) (2), a sample
of solid waste or a sample of water,
soil or air,
which is collected for the sole purpose of testing
to determine its characteristics or composition,
is not subject to any requirements of this Part or
35
Ill. Adm.
Code 702,
703, 705 and 722 through
728.
The sample qualifies when:
A)
The sample is being transported to a
laboratory for the purpose of testing;
or
125—211
40
B)
The sample is being transported back to the
sample collector after testing; or
C)
The sample is being stored by the sample
collector before transport to a laboratory
for testing; or
D)
The sample is being stored in a laboratory
before testing; or
E)
The sample is being stored in a laboratory
for testing but before it is returned to the
sample collector; or
F)
The sample is being stored temporarily in the
laboratory after testing for a specific
purpose (for example, until conclusion of a
court case or enforcement action where
further testing of the sample may be
necessary).
2)
In order to qualify for the exemption in
subsection
(d) (1) (A)
and
(B),
a sample collector
shipping samples to a laboratory and a laboratory
returning samples to a sample collector must:
A)
Comply with U.S. Department of Transportation
(DOT), U.S. Postal Service
(USPS)
or any
other applicable shipping requirements; or
B)
Comply with the following requirements if the
sample collector determines that DOT, USPS or
other shipping requirements do not apply to
the shipment of the sample:
i)
Assure that the following information
accompanies the sample:
The sample
collector’s name, mailing address and
telephone number; the laboratory’s name,
mailing address and telephone number;
the quantity of the sample; the date of
the shipment; and a description of the
sample.
ii)
Package the sample so that it does not
leak,
spill or vaporize from its
packaging.
3)
This exemption does not apply if the laboratory
determines that the waste is hazardous but the
laboratory is no longer meeting any of the
conditions stated in subsection
(d) (1).
125—2 12
41
e)
Treatability study samples.
1)
Except as is provided in subsection
(e) (2),
persons who generate or collect samples for the
purpose of conducting treatability studies, as
defined in 35 Ill. Adm. Code 720.110,
are not
subject to any requirement of 35
Ill.
Adm. Code
721 through 723 or to the notification
requirements of Section 3010 of the Resource
Conservation and Recovery Act.
Nor are such
samples included in the quantity determinations of
Section 721.105 and 35
Ill. Adm. Code 722.134(d)
when:
A)
The sample is being collected and prepared
for transportation by the generator or sample
collector;
or,
B)
The sample is being accumulated or stored by
the generator or sample collector prior to
transportation to a laboratory or testing
facility; or
C)
The sample is being transported to the
laboratory or testing facility for the
purpose of conducting a treatability study.
2)
The exemption in subsection
(e) (1)
is applicable
to samples of hazardous waste being collected and
shipped for the purpose of conducting treatability
studies provided that:
A)
The generator or sample collector uses
(in
“treatability studies”) no more than 1000 kg
of any non—acute hazardous waste,
1 kg of
acute hazardous waste or 250 kg of soils,
water or debris contaminated with acute
hazardous waste for each process being
evaluated for each generated wastestream; and
B)
The mass of each shipment does not exceed
1000 kg of non—acute hazardous waste,
1 kg of
acute hazardous waste or 250 kg of soils,
water or debris contaminated with acute
hazardous waste; and
C)
The sample must be packaged so that it does
not leak,
spill or vaporize from its
packaging during shipment and the
requirements of subsections
(i) or
(ii) are
met.
125—213
42
i)
The transportation of each sample
shipment complies with U.S. Department
of Transportation (DOT),
U.S. Postal
Service
(USPS)
or any other applicable
shipping requirements; or
ii)
If the DOT, USPS or other shipping
requirements do not apply to the
shipment of the sample, the following
information must accompany the sample:
The name, mailing address and telephone
number of the originator of the sample;
the name,
address and telephone number
of the facility that will perform the
treatability study; the quantity of the
sample; the date of the shipment; and,
a
description of the sample,
including its
USEPA hazardous waste number.
D)
The sample is shipped to a laboratory or
testing facility which is exempt under
subsection
(f)
or has an appropriate RCRA
permit or interim status.
E)
The generator or sample collector maintains
the following records for a period ending
3
years after completion of the treatability
study:
i)
Copies of the shipping documents;
ii)
A copy of the contract with the facility
conducting the treatability study;
iii) Documentation showing:
The amount of
waste shipped under this exemption; the
name, address and TJSEPA identification
number of the laboratory or testing
facility that received the waste; the
date the shipment was made;
and, whether
or not unused samples and residues were
returned to the generator.
F)
The generator reports the information
required in subsection
(e) (2) (E) (iii)
in its
report under 35
Ill. Adm. Code 722.141.
3)
The Agency may grant requests, on a case—by—case
basis,
for quantity limits in excess of those
specified in subsection
(e) (2) (A), for up to an
additional 500 kg of any non-acute hazardous
125—2 14
43
waste,
1 kg of acute hazardous waste and 250 kg of
soils, water or debris contaminated with acute
hazardous waste,
to conduct further treatability
study evaluation when:
There has been an
equipment or mechanical failure during the conduct
of the treatability study; there is need to verify
the results of a previously conducted treatability
study; there is a need to study and analyze
alternative techniques within a previously
evaluated treatment process;
or, there is a need
to do further evaluation of an ongoing
treatability study to determine final
specifications for treatment.
The additional
quantities allowed are subject to all the
provisions in subsections
(e) (1) and
(e) (2) (B)
through
(F).
The generator or sample collector
must apply to the Agency and provide in writing
the following information:
A)
The reason why the generator or sample
collector requires additional quantity of
sample for the treatability study evaluation
and the additional quantity needed;
B)
Documentation accounting for all samples of
hazardous waste from the wastestream which
have been sent for or undergone treatability
studies, including the date each previous
sample was shipped, the quantity of each
previous shipment, the laboratory or testing
facility to which it was shipped, what
treatability study processes were conducted
on each sample shipped, and the available
results of each treatability study;
C)
A description of the technical modifications
or change in specifications which will be
evaluated and the expected results;
D)
If such further study
is being required due
to equipment or mechanical failure,
the
applicant must include information regarding
the reason for the failure or breakdown and
also include what procedures or equipment
have been made to protect against further
breakdowns;
and,
E)
Such other information as the Agency
determines is necessary.
4)
Final Agency determinations pursuant to this
subsection may be appealed to the Board.
125—2 15
44
f)
Samples undergoing treatability studies at laboratories
or testing facilities.
Samples undergoing treatability
studies and the laboratory or testing facility
conducting such treatability studies
(to the extent
such facilities are not otherwise subject to RCRA
requirements) are not subject to any requirement of
this Part, or of 35 Ill. Adm. Code
702,’ 703,
705, 722
through 726,
and 728,
or to the notification
requirements of Section 3010 of the Resource
Conservation and Recovery Act, provided that the
requirements of subsections
(f) (1) through
(f) (11) are
met.
A mobile treatment unit may qualify as a testing
facility subject to subsections
(f) (1) through
(f) (11).
Where a group of mobile treatment units are located at
the same site,
the limitations specified in subsections
(f) (1) through
(f) (11) apply to the entire group of
mobile treatment units collectively as if the group
were one mobile treatment unit.
1)
No less than 45 days before conducting
treatability studies, the facility notifies the
Agency in writing that it intends to conduct
treatability studies under this subsection.
2)
The laboratory or testing facility conducting the
treatability study has a USEPA identification
number.
3)
No more than a total of 250 kg of “as received”
hazardous waste is subjected to initiation of
treatability studies in any single day.
“As
received” waste refers to the waste as received in
the shipment from the generator or sample
collector.
4)
The quantity of “as received” hazardous waste
stored at the facility for the purpose of
evaluation in treatability studies does not exceed
1000 kg, the total of which can include 500 kg of
soils, water or debris contaminated with acute
hazardous waste or
1 kg of acute hazardous waste.
This quantity limitation does not include:
A)
Treatability study residues; and,
B)
Treatment materials (including nonhazardous
solid waste)
added to “as received” hazardous
waste.
5)
No more than 90 days have elapsed since the
treatability study for the sample was completed,
125—216
45
or no more than one year has elapsed since the
generator or sample collector shipped the sample
to the laboratory or testing facility, whichever
date first occurs.
6)
The treatability study does not involve the
placement of hazardous waste on the land or open
burning of hazardous waste.
7)
The facility maintains records for
3 years
following completion of each study that show
compliance with the treatment rate limits and the
storage time and quantity limits.
The following
specific information must be included for each
treatability study conducted:
A)
The name,
address and USEPA identification
number of the generator or sample collector
of each waste sample;
B)
The date the shipment was received;
C)
The quantity of waste accepted;
D)
The quantity of “as received” waste in
storage each day;
E)
The date the treatment study was initiated
and the amount of “as received” waste
introduced to treatment each day;
F)
The date the treatability study was
concluded;
G)
The date any unused sample or residues
generated from the treatability study were
returned to the generator or sample collector
or,
if sent to a designated facility, the
name of.the facility and the USEPA
identification number.
8)
The facility keeps, on-site,
a copy of the
treatability study contract and all shipping
papers associated with the transport of
treatability study samples to and from the
facility for a period ending
3 years from the
completion date of each treatability study.
9)
The facility prepares and submits a report to the
Agency by March 15 of each year that estimates the
number of studies and the amount of waste expected
to be used in treatability studies during the
125—217
46
current year,
and includes the following
information for the previous calendar year:
A)
The name,
address and USEPA identification
number of the facility conducting the
treatability studies;
B)
The types
(by process)
of treatability
studies conducted;
C)
The names and addresses of persons for whom
studies have been conducted (including their
USEPA identification numbers);
D)
The total quantity of waste in storage each
day;
E)
The quantity and types of waste subjected to
treatability studies;
F)
When each treatability study was conducted;
G)
The final disposition of residues and unused
sample from each treatability study;
10)
The facility determines whether any unused sample
or residues generated by the treatability study
are hazardous waste under Section 721.103 and,
if
so, are subject to
35
Ill. Adm. Code 702,
703 and
721 through 728, unless the residues and unused
samples are returned to the sample originator
under the subsection
(e)
exemption.
11)
The facility notifies the Agency by letter when
the facility is no longer planning to conduct any
treatability studies at the site.
(Source:
Amended at 15 Ill.
Reg.
,
effective
)
Section 721.131
Hazardous Wastes From Nonspecific Sources
~
The following solid wastes are listed hazardous wastes
from non—specific sources unless they are excluded
under 35
Ill. Adm. Code 720.120 and 720.122 and listed
in Appendix I.
EPA
Industry and Hazardous Waste
Haz-
Hazardous
.
ard
Waste No.
Code
125
—2 18
47
FOOl
The following spent halogenated
(T)
solvents used in degreasing:
tetra—
chloroethylene, trichloroethylene,
methylene chloride,
1,1,1-trichloro-
ethane,
carbon tetrachioride and
chlorinated fluorocarbons; all spent
solvent mixtures and blends used in
degreasing containing, before use,
a
total of ten percent or more
(by
volume)
of one or more of the above
halogenated solvents or those solvents
listed in F002, F004 or F005; and still
bottoms from the recovery of these
spent solvents and spent solvent
mixtures.
F002
The following spent halogenated
(T)
solvents:
tetrachloroethylene,
inethylene chloride, trichioroethylene,
1,1,1—trichloroethane, chlorobenzene,
1,1,2-trichloro—1,2, 2—trifluoroethane,
orthodichlorobenzene, trichioro-
fluoromethane and 1, 1, 2—trichioro—
ethane; all spent solvent mixtures and
blends containing, before use,
a total
of ten percent or more (by volume)
of
one or more of the above halogenated
solvents or those solvents listed in
FOOl,
F004 or F005;
and still bottoms
from the recovery of these spent
solvents and spent solvent mixtures.
F003
The following spent non-halogenated
(I)
solvents:
xylene,
acetone,
ethyl
acetate, ethyl benzene,
ethyl ether,
methyl isobutyl ketone, n—butyl
alcohol, cyclohexanone and methanol;
all spent solvent mixtures and blends
containing, before use, only the above
spent non—halogenated solvents; and all
spent solvent mixtures and blends
containing, before use, one or more of
the above non—halogenated solvents and
a total of ten percent or more
(by
volume)
of one or more of those
solvents listed in FOOl,
F002,
F004 or
F005;
and still bottoms from the
recovery of these spent solvents and
spent solvent mixtures.
12
5—2
19
48
F004
The following spent non-halogenated
(T)
solvents:
cresols and cresylic acid
and nitrobenzene; all spent solvent
mixtures and blends containing,
before
use, a total of ten percent or more (by
volume)
of one or more of the above
non—halogenated solvents or those
solvents listed
in FOOl, F002 or F005;
and still bottoms from the recovery of
these spent solvents and spent solvent
mixtures.
F005
The following spent non-halogenated
(I,
solvents:
toluene, methyl ethyl
T)
ketone, carbon disulfide,
isobutanol,
pyridine, benzene,
2—ethoxyethanol and
2—nitropropane;
all spent solvent
mixtures and blends, containing,
before
use, a total of ten percent or more (by
volume)
of one or more of the above
non—halogenated solvents or those
solvents listed in FOOl,
F002 or F004;
and still bottoms from the recovery of
these spent solvents and spent solvent
mixtures.
FOO6
Wastewater treatment sludges from
(T)
electroplating operations except from
the following processes:
(1)
sulfuric
acid anodizing of aluminum;
(2) tin
plating on carbon steel;
(3)
zinc
plating
(segregated basis)
on carbon
steel;
(4) aluminum or zinc—aluminum
plating on carbon steel;
(5)
cleaning/stripping associated with tin,
zinc and aluminum plating on carbon
steel; and
(6)
chemical etching and
milling of aluminum.
F019
See Below
F007
Spent cyanide plating bath solutions
(R,
from electroplating operations.
T)
F008
Plating bath residues from the bottom
(R,
of plating baths from electroplating
T)
operations where cyanides are used in
the process.
125—220
49
F009
Spent stripping and cleaning bath
(R,
solutions from electroplating
T)
operations where cyanides are used in
the process.
FOlO
Quenching bath res.idues from oil baths
(R,
from metal heat treating operations
T)
where cyanides are used in the process.
FOll
Spent cyanide solutions from salt bath
(R,
pot cleaning from metal heat treating
T)
operations.
F0l2
Quenching wastewater treatment sludges
(T)
from metal heat treating operations
where cyanides are used in the process.
F019
Wastewater treatment sludges from the
(T)
chemical conversion coating of aluminum
except from zirconium phosphating in
aluminum can washing when such
phosphating is an exclusive conversion
coating process.
F020
Wastes (except wastewater and spent
(H)
carbon from hydrogen chloride
purification) from the production or
manufacturing use
(as a reactant,
chemical intermediate or component in a
formulating process)
of tn— or tetra—
chlorophenol, or of intermediates used
to produce their pesticide derivatives.
(This listing does not include wastes
from the production of hexachlorophene
from highly purified 2,4,5-trichloro-
phenol.
)
FO21
Wastes (except wastewater and spent
(H)
carbon from hydrogen chloride
purification) from the production or
manufacturing use
(as a reactant,
chemical intermediate or component in a
formulating process)
of pentachloro—
phenol,
or of intermediates used to
produce its derivatives.
125—221
50
F022
Wastes
(except wastewater and spent
(H)
carbon from hydrogen chloride
purification) from the manufacturing
use
(as a reactant, chemical
intermediate or component in
a
formulating process)
of tetra—, penta—
or hexachlorobenzenes ‘under alkaline
conditions.
FO23
Wastes (except wastewater and spent
(H)
carbon from hydrogen chloride
purification) from the production of
materials on equipment previously used
for the production or manufacturing use
(as a reactant, chemical intermediate
or component in a formulating process)
of tn- and tetrachlorophenols.
(This
listing does not include wastes from
equipment used only for the production
or use of hexachlorophene from highly
purified 2,4,5— trichlorophenol.
F024
Process wastes including but not
(T)
limited to, distillation residues,
heavy ends,
tars,
and reactor cleanout
wastes, from the production of certain
chlorinated aliphatic hydrocarbons by
free radical catalyzed processes.
These chlorinated aliphatic
hydrocarbons are those having carbon
chain lengths ranging from one to and
including five, with varying amounts
and positions of chlorine substitution.
(This listing does not include
wastewaters, wastewater treatment
sludges,
spent catalysts and wastes
listed in this Section or Section
721.132.)
F025
Condensed light ends,
spent filters and
(T)
filter aids, and spent desicant wastes
from the production of certain
chlorinated aliphatic hydrocarbons by
free radical catalyzed processes.
These chlorinated aliphatic
hydrocarbons are those having carbon
chain lengths ranging from one to and
including five, with varying amounts
and positions of chlorine substitution.
125—222
51
F026
Wastes (except wastewater and spent
(H)
carbon from hydrogen chloride
purification) from the production of
materials on equipment previously used
for the manufacturing use
(as a
reactant, chemical intermediate or
component in a formulating process)
of
tetra—, penta— or hexachlorobenzene
under alkaline conditions.
FO27
Discarded unused formulations
(H)
containing tn—,
tetra— on pentachloro—
phenol or discarded unused formulations
containing compounds derived from these
chlonophenols.
(This listing does not
include formulations containing hexa—
chlorophene synthesized from
prepunified 2,4,5-tnichlorophenol as
the sole component).
F028
Residues resulting from the
(T)
incineration or thermal treatment of
soil contaminated with hazardous waste
numbers F020,
FO21, F022,
F023, F026
and F027.
125—223
52
F032
Wastewaters.
process
residuals,
ill
preservative dnippage and spent
formulations from wood preserving
processes generated at plants that
currently use or have previously used
chlorophenolic formulations
(except
potentially cross—contaminated wastes
that have had the F032 waste code
deleted in accordance with Section
721.135 and where the aenerator does
not resume or initiate use of chloro—
phenolic formulations).
This listing
does not include KOOl bottom sediment
s1ud~efrom the treatment of wastewater
from wood preserving processes that use
creosote or pentachiorophenol.
BOARD NOTE:
The listing of wastewaters
that have not come into contact with
process contaminants is staved
administratively.
The listing for
plants that have previously used
chlorophenolic formulations
is
administratively stayed whenever these
wastes are covered by the F034 or FO35
listings.
These stays will remain in
effect until further administrative
action is taken.
Furthermore, the FO32
listing is administratively stayed with
respect to the process area receiving
drippage of these wastes provided
persons desiring to continue operating
notify USEPA by August
6,
1991, of
their intent to upgrade or install drip
pads, and by November
6,
1991, provide
evidence to USEPA that they have
adequate financing to ~ay for drip pad
upgrades or installation,
as provided
in the administrative stay.
The stay
of listings will remain in effect until
February
6,
1992,
for existing drip
pads,
and until May 6,
1992, for new
drip pads.
125—224
53
F034
Wastewaters, process residuals,
(T)
preservative drippaqe and spent
formulations from wood preserving
processes generated at plants that use
creosote formulations.
This listing
does not include KOO1 bottom sediment
sludae from the treatment of wastewater
from wood preserving processes that use
creosote or pentachlorophenol.
BOARD NOTE:
The listing of wastewaters
that have not come into contact with
process contaminants
is staved
administratively.
These stays will
remain in effect until further
administrative action is taken.
Furthermore, the FO34 and F035 listings
are administratively stayed with
respect to the process area receiving
drippage of these wastes provided that,
by November
6,
1991,
persons desiring
to continue operating notify the Agency
of their intent to upgrade or install
drip pads,
and provide evidence to the
Agency that they have adeauate
financing to pay for drip Pad upgrades
or installation,
as provided in the
administrative stay.
The stay àf
listings will remain in effect until
February 6,
1992,
for existing drip
pads,
and until May 6,
1992.
for new
drip pads.
125—225
54
FO35
Wastewaters, process residuals,
fl~
preservative dnippage and spent
formulations from wood preserving
processes generated at plants that use
inorganic preservatives containing
arsenic or chromium.
This listing does
not include KOOl bottom sediment sludge
from the treatment of wastewater from
wood preserving processes that use
creosote or ~entachlorophenol.
BOARD NOTE:
The listing of wastewaters
that have not come into contact with
process contaminants is stayed
administratively.
These stays will
remain in effect until further
administrative action is taken.
Furthermore, the FO34 and F035 listings
are administratively stayed with
respect to the process area receiving
drippage of these wastes provided that,
by November 6,
1991, persons desiring
to continue operating notify the Agency
of their intent to upgrade or install
drip pads,
and provide evidence to the
Agency that they have adequate
financing to pay for drip pad upgrades
or installation,
as provided in the
administrative stay.
The stay of
listings will remain
in effect until
February 6,
1992,
for existing drip
pads, and until May
6,
1992,
for new
drip pads.
F037
Petroleum refinery primary oil/water!
in
solids separation sludge
--
Any sludge
generated from the gravitational
separation of oil/water/solids during
the storage or treatment of process
wastewaters and oily cooling
wastewaters from petroleum refineries.
Such sludges include, but are not
limited to. those generated in:
oil!
water/solids separators; tanks and
impoundments; ditches and other
conveyances; sumps; and stormwater
units receiving dry weather flow.
Sludges generated in storniwater units
that do not receive dry weather flow,
sludges aenerated in aggressive
biological treatment units as defined
in subsection
(b) (2)
(including sludges
125—226
55
generated in one or more additional
units after wastewaters have been
treated in aggressive biological
treatment units)
and K051 wastes are
not_included in this listing.
F038
Petroleum refinery secondary
(emulsified)
oil/water/solids
separation sludge
——
Any sludge or
float generated from the physical or
chemical separation of oil/water/solids
in process wastewaters and oily cooling
wastewaters from petroleum refineries.
Such wastes include, but are not
limited to, all sludges and floats
generated in:
induced air floatation
(IAF)
units,
tanks and impoundments,
and all sludges .generated in DAF units.
Sludges generated in storniwater units
that do not receive dry weather flow,
sludges generated in agaressive
biological treatment units as defined
in subsection
(b) (2)
(including sludges
generated in one or more additional
units after wastewaters have been
treated in aggressive biological
treatment units), F037, KO48 and KO51
wastes are not included in this
listing.
F039
Leachate resulting from the treatment,
(T)
storage or disposal of wastes
classified by more than one waste code
under Subpart
D, or from a mixture of
wastes classified under Subparts C and
D.
(Leachate resulting from the
management of one or more of the
following USEPA hazardous wastes and no
other hazardous wastes retains its
hazardous waste code(s):
FO2O,
FO21,
FO22, F023,
FO26, F027 or F028.)
BOARD NOTE:
The primary hazardous properties of these
materials have been indicated by the letters T
(Toxicity), R (Reactivity),
I
(Ignitability), and C
(Corrosivity).
The letter H indicates Acute Hazardous
Waste.
~j
Listing specific definitions.
jj~
For the purpose of the FO37 and F038 listings,
oil/water/solids is defined as oil or water or
125—22
7
56
solids.
~
For the purposes of the FO37 and F038 listings:
~j
Aggressive biolqgical treatment units are
defined as units which employ one of the
following four treatment methods:
activated
sludge; trickling filter; rotating biological
contactor for the continuous accelerated
biological oxidation of wastewaters; or,
high—rate aeration.
High—rate aeration is a
system of surface impoundments or tanks, in
which intense mechanical aeration is used to
completely mix the wastes, enhance biological
activity,
and:
il
The units employ a minimum of
6
horsepower per million gallons of
treatment volume; and either
.jJ~.
The hydraulic retention time of the unit
is no longer than
5 days;
or
iii) The hydraulic retention time is no
longer than 30 days and the unit does
not generate a sludge that is a
hazardous waste by the toxicity
characteristic.
~j
Generators and treatment,
storage or disposal
(TSD)
facilities~have the burden of proving
that their sludges are exempt from listing as
FO37 or F038 wastes under this definition.
Generators and TSD facilities shall maintain,
in their operating or other on site records,,
documents and data sufficient to prove that:
il
The unit is an aggressive biological
treatment unit as defined in this
subsection; and
£jj
The sludges sought to be exempted from
F037 or F038 were actually generated in
the aggressive biological treatment
unit.
fl
Time of generation.
For the purposes of:
~j
The F037 listing, sludges are considered to
be generated at the moment of deposition in
the unit, where deposition is defined as at
least a temporary cessation of lateral
125—228
57
particle movement.
The F038 listing:
il
Sludaes are considered to be generated
at the moment of deposition in the unit,
where deposition is defined as at least
a tem~orarvcessation of lateral
particle movement: and
jj).
Floats are considered to be ~enerated at
the moment theY are formed in the top of
the
unit.
(Source:
Amended at 15 Ill. Req.
,
effective
)
Section 721.132
Hazardous Waste from Specific Sources
The following solid wastes are listed hazardous wastes from
specific sources unless they are excluded under 35
Ill.
Adm. Code
720.120 and 720.122 and listed in Appendix I.
EPA
Hazardous
Hazard
Waste No.
Industry and Hazardous Waste
Code
Wood Preservation:
KOOl
Bottom sediment sludge from the treatment of
(T)
wastewaters from wood preserving processes
that use creosote and/or pentachlorophenol.
Inorganic Pigments:
K002
Wastewater treatment sludge from the
(T)
production of chrome yellow and orange
pigments.
KOO3
Wastewater treatment sludge from the
(T)
production of molybdate orange pigments.
K004
Wastewater treatment sludge from the
(T)
production of zinc yellow pigments.
K005
Wastewater treatment sludge from the
(T)
production of chrome green pigments.
KOO6
Wastewater treatment sludge from the
(T)
production of chrome oxide green pigments
(anhydrous and hydrated).
1
7S—229
58
K007
Wastewater treatment sludge from the
(T)
production of iron blue pigments.
K008
Oven residue from the production of chrome
(T)
oxide green pigments.
Organic Chemicals:
K009
Distillation bottoms from the production of
(T)
acetaldehyde from ethylene.
K010
Distillation side cuts from the production
(T)
of acetaldehyde from ethylene.
KOll
Bottom stream from the wastewater stripper
(R,T)
in the production of acrylonitrile.
1013
Bottom stream from the acetronitrile column
(T)
in the production of acrylonitrile.
K014
Bottoms from the acetontrile purification
(T)
column in the production of acrylonitnile.
K0l5
Still bottoms from the distillation of
(T)
benzyl chloride.
K016
Heavy
ends or distillation residues from the
(T)
production of carbon tetrachioride.
1017
Heavy ends (still bottoms)
from the
(T)
purification column in the production of
epichiorohydrin.
K018
Heavy ends from the fractionation column in
(T)
ethyl chloride production.
K019
Heavy ends from the distillation of ethylene
(T)
dichloride in ethylene dichioride
production.
K020
Heavy ends from the distillation of vinyl
(T)
chloride in vinyl chloride monomer
production.
K021
Aqueous spent antimony catalyst waste from
(T)
fluoromethanes production.
1022
Distillation bottom tars from the production
(T)
of phenol/acetone from cumene.
K023
Distillation light ends from the production
(T)
of phthalic anhydride from naphthalene.
125—230
59
1024
Distillation
bottoms
from
the
production
of
(T)
phthalic anhydride from naphthalene.
1093
Distillation light ends from the production
(T)
of phthalic anhydride from ortho-xylene.
1094
Distillation bottoms from the production of
(T)
phthalic anhydride from ortho-zylene.
1025
Distillation bottoms from the production of
(T)
nitrobenzene by the nitration of benzene.
K026
Stripping still tails from the production of
(T)
methyl ethyl pyridines.
1027
Centrifuge and distillation residues from
(R,T)
toluene diisocyanate production.
K028
Spent catalyst from the hydrochiorinator
(T)
reactor in the production of 1,1,1-tn-
chloroethane.
K029
Waste from the product stream stripper in
(T)
the production of 1,1,l-tnichloroethane.
1095
Distillation bottoms from the production of
(T)
1,1,l-tnichloroethane.
1096
Heavy ends from the heavy ends column from
(T)
the production of l,1,l-tnichloroethane.
K030
Column bottoms or heavy ends from the
(T)
combined production of trichloroethylene and
perchioroethylene.
KO83
Distillation bottoms from aniline
(T)
production.
1103
Process residues from aniline extraction
(T)
from the production of aniline.
Kl04
Combined wastewater streams generated from
(T)
nitrobenzene/aniline production.
1085
Distillation or fractionation column bottoms
(T)
from the production of chlorobenzenes.
1105
Separated aqueous stream from the reactor
(T)
product washing step in the production of
chlorobenzenes.
125—
23 1
60
K107
Column bottoms from product separation from
(C,T)
the production of 1,l-dimethylhydrazine
(UDMH)
from carboxylic acid hydrazides.
1108
Condensed column overheads from product
(I,T)
separation and condensed reactor vent gases
from the production of 1,1-dimethyihydrazine
(UDNH)
from carboxylic acid hydrazides.
1109
Spent filter cartridges from the product
(T)
purification from the production of 1,1—di-
methylhydrazine
(UDNH)
from carboxylic acid
hydrazides.
1110
Condensed column overheads from intermediate
(T)
separation from the production of 1,1-di-
methylhydrazine
(UDNH)
from carboxylic acid
hydrazides.
1111
Product wastewaters from the production of
(C,T)
dinitrotoluene via nitration of toluene.
K112
Reaction by-product water from the drying
(T)
column
in the production of toluenediamine
via hydrogenation of dinitrotoluene.
K113
Condensed liquid light ends from the
(T)
purification of toluenediamine in the
production of toluenediamine via
hydrogenation of dinitroluene.
K114
Vicinals from the purification of toluene-
(T)
diamine in the production of toluenediamine
via hydrogenation of dinitrotolune.
K115
Heavy ends from the purification of
(T)
toluenediamine in the production of
toluenediamine via hydrogenation of di-
nitrotoluene.
K1l6
Organic condensate from the solvent recovery
(T)
column in the production of toluene di—
isocyanate via phosgenation of toluenedi—
amine.
125—232
61
1117
Wastewater from the reactor vent gas
(T)
scrubber in the production of ethylene di-
bromide via bromination of ethene.
Kl18
Spent adsorbent solids from purification of
(T)
ethylene dibromide in the production of
ethylene dibromide via bromination of
ethene.
1136
Still bottoms from the purification of
(T)
ethylene dibromide in the production of
ethylene dibromide via bromination of
ethene.
Inorganic Chemicals:
1071
Brine purification muds from the mercury
(T)
cell process in chlorine production, where
separately prepurifled brine is not used.
1073
Chlorinated hydrocarbon waste from the
(T)
purification step of the diaphragm cell
process using graphite anodes in chlorine
production.
K106
Wastewater treatment sludge from the mercury
(T)
cell process in chlorine production.
Pesticides:
K031
By-product salts generated in the production
(T)
of MSMA and cacodylic acid.
1032
Wastewater treatment sludge from the
(T)
production of chlordane.
1033
Wastewater and scrub water from the
(T)
chlorination of cyclopentadiene
in the
production of chlordane.
1034
Filter solids from the filtration of hexa—
(T)
chlorocyclopentadiene in the production of
chlordane.
1097
Vacuum stripper discharge from the chlordane
(T)
chlorinator in the production of chiordane.
1035
Wastewater treatment sludges generated in
(T)
the production of creosote.
125—233
62
1036
Still bottoms from toluene reclamation
(T)
distillation in the production of di-
sulfoton.
K037
Wastewater treatment sludges from the
‘
(T)
production of disulfoton.
KO38
Wastewater from the washing and stripping of
(T)
phorate production.
K039
Filter cake from the filtration of diethyl-
(T)
phosphorodithioic acid in the production of
phorate.
1040
Wastewater treatment sludge from the
(T)
production of phorate.
KO41
Wastewater treatment sludge from the
(T)
production of toxaphene.
1098
Untreated process wastewater from the
(T)
production of toxaphene.
K042
Heavy ends or distillation residues from the
(T)
distillation of tetrachlorobenzene in the
production of 2,4,5-T.
1043
2,6-Dichiorophenol waste from the production
(T)
of 2,4—D.
K099
Untreated wastewater from the production of
(T)
2, 4—D.
K123
Process wastewater
(including supernates,
(T)
filtrates and washwaters)
from the
production of ethylenebisdithiocarbamic acid
and its salts.
1124
Reactor vent scrubber water from the
(C,T)
production of ethylenebisdithiocarbamic acid
and its salts.
1125
Filtration, evaporation and centrifugation
(T)
solids from the production of ethylenebis—
dithiocarbamic acid and its salts.
K126
Baghouse dust and floor sweepings in milling
(T)
and packaging operations from the production
or formulation of ethylenebisdithiocarbamic
acid and its salts.
125—234
63
1131
Wastewater from the reactor and spent
(C,T)
sulfuric acid from the acid dryer from the
production of methyl bromide.
1132
Spent absorbent and,wastewater separator
(T)
solids from the production of methyl
bromide.
Explosives:
K044
Wastewater treatment sludges from the
(R)
manufacturing and processing of explosives.
1045
Spent carbon from the treatment of
(R)
wastewater containing explosives.
K046
Wastewater treatment sludges from the
(T)
manufacturing, formulation and loading of
lead-based initiating compounds.
1047
Pink/red water from TNT operations.
(R)
Petroleum Refining:
1048
Dissolved air flotation
(DAF)
float from the
(T)
petroleum refining industry.
K049
Slop oil emulsion solids from the petroleum
(T)
refining industry.
1050
Heat exchanger bundle cleaning sludge from
(T)
the petroleum refining industry.
K051
API separator sludge from the petroleum
(T)
refining industry.
KO52
Tank bottoms
(leaded)
from the petroleum
(T)
refining industry.
Iron and Steel:
1061
Emission control dust/sludge from the
(T)
primary production of steel in electric
furnaces.
1062
Spent pickle liquor generated by steel
(C,T)
finishing operations of facilities within
the iron and steel industry (SIC Codes 331
and 332)
(as defined in 35 Ill. Adm. Code
720.110)
125—23 5
64
Primary Copper:
KO64
Acid plant blowdown slurry or sludge
(T)
resulting from the thickening of blowdown
slurry from primary copper production.
Primary Lead:
1065
Surface impoundment solids contained in and
(T)
dredged from surface impoundments at primary
lead smelting facilities.
Primary Zinc:
1066
After June 30, 1990, 3~ludgefrom treatment
(T)
of process wastewater or acid plant blowdown
from primary zinc production.
BOARD NOTE:
This waste listing is the subiect of a ludicial
remand in American Mining Congress v. EPA, 907 F.2d 1179
(D.D.C.
1990).
The Board intends that this listing not become
enforceable in Illinois until the first date upon which the Board
RCRA program becomes “not equivalent to the Federal program,”
within the meaning of Section 3006(b) of the RCRA Act,
42 U.S.C.
6926(b), the Board RCRA rules become “less stringent” than the
USEPA rules,
as this phrase
is used in Section 3009,
42 U.S.C.
6929, or the Board RCRA rules are not “identical in substance”
with the federal rules as that term is intended by Ill. Rev.
Stat.
1989 ch.
111 1/2,
pars.
1007.2’ and 1022.4 as a result of
some action by USEPA with regard to this listing in response to
the American Mining Conaress remand.
Primary Aluminum:
1088
Spent potliners from primary aluminum
(T)
reduction.
Ferroalloys:
1090
Emission control dust or sludge from
(T)
ferrochromiumsilicon production.
K091
Emission control dust or sludge from
(T)
ferrochromium production.
Secondary Lead:
K069
Emission control dust/sludge from secondary
(T)
lead smelting.
125—236
65
K100
Waste leaching solution from acid leaching
(T)
of emission control, dust/sludge from
secondary lead smelting.
Veterinary Pharmaceuticals:
K084
Wastewater treatment sludges generated
(T)
during the production of veterinary
pharmaceuticals from arsenic or organo—
arsenic compounds.
1101
Distillation tar residues from the
(T)
distillation of aniline—based compounds in
the production of veterinary pharmaceuticals
from arsenic or organoarsenic compounds.
1102
Residue from use of activated carbon for
(T)
decolorization in the production of
veterinary pharmaceuticals from arsenic or
organo—arsenic compounds.
Ink Formulation:
1086
Solvent washes and sludges, caustic washes
(T)
and sludges,
or water washes and sludges
from cleaning tubs and equipment used in the
formulation of ink from pigments, driers,
soaps and stabilizers containing chromium
and lead.
Coking:
K060
Ammonia still lime sludge from coking
(T)
operations.
1087
Decanter tank tar sludge from coking
(T)
operations.
(Source:
Amended at 15
Ill. Reg.
,
effective
)
Section 721.135
Wood Preserving Wastes
~j
Wastes from wood Preserving processes at plants that do
not resume or initiate use of chlorophenolic
preservatives will not meet the listing definition of
F032 once the ~enerator has met all of the requirements
of subsections
(b) and
(c).
These wastes may, however,
continue to meet another hazardous waste listing
description or may exhibit one or more of the hazardous
waste characteristics.
125—237
66
~
Generators shall either clean or replace all process
equipment that may have come into contact with
chlorophenolic formulations or constituents thereof,
including,
but not limited to, treatment cylinders,
sumps, tanks, piping systems, drip pads,
fork lifts and
trams.
in
a manner which minimizes or eliminates the
escape of hazardous waste or constituents,
leachate,
contaminated drippage or hazardous waste decomposition
products to the groundwater, surface water or
atmosphere.
Generators shall do one of the following:
~j
Prepare and follow an equipment cleaning ‘plan
and clean equipment in accordance with this
Section;
or
~j
Prepare and follow an equipment replacement
plan and replace equipment in accordance with
this Section; or
Qj
Document cleaning and replacement
in
accordance with this Section, carried out
after termination of use of chiorophenolic
preservatives.
~j
Cleaning requirements.
~j
Prepare and sign a written equipment cleaning
plan that describes:
J,j
The equipment to be cleaned.
JJJ
How the equipment will be cleaned.
iii)
The solvent to be used in cleaning.
jyj
How solvent rinses will be tested.
And,
yj
How cleaning residues will be disposed.
~j
Equipment must be cleaned as follows:
jj
Remove all visible residues from process
equipment.
jjj
Rinse process equipment with an
appropriate solvent until dioxins and
dibenzofurans are not detected in the
final solvent rinse.
~
Analytical requirements
125—238
67
jj
Rinses must be tested in accordance with
SW-846, Method 8290,
incorporated by
reference in 35 Ill.
Adm. Code 720.111.
jjj
“Not detected” means at or below the
lower method calibration limit
(NCL)
in
Method 8290, Table
1.
Qj
The aenerator must manage all residues from
the cleaning process as FO32 waste.
fl
Replacement requirements.
~j
Prepare and sign a written equipment
replacement plan that describes:
il
The equipment to be replaced
JJJ.
How the equipment will be replaced;
and
iii) How the equipment will be disposed of.
~j
The generator must manage the discarded
equipment as F032 waste.
j)
Documentation requirements.
Document that
previous equipment cleaning and replacement was
performed in accordance with this Section and
ocurred after cessation of use of chlorophenolic
preservatives.
~
The generator shall maintain the following records
documenting the cleaning and replacement as part of the
facility’s operating record:
fl
The name and address of the facility
21
Formulations previously used and the date on which
their use ceased in each process at the plant
~
Formulations currently used in each process at the
plant
4j.
The equipment cleaning or replacement plan
~
The name and address of any persons who conducted
the cleaning and replacement
~Qj
The dates on which cleaning and replacement were
accomplished
125—239
68
fl
The dates of sampling and testing
~
A description of the sample handling and
preparation techniques,
including techniques used
for extraction,containenization, preservation and
chain—of—custody of the samples
~j
A description of the tests performed,
the date the
tests were performed and the results of the tests
.1QI
The name and model numbers of the instrument(s)
used in performing the tests
fl)..
QA/OC documentation; and
~
The following statement signed by the generator or
the generator’s authorized representative:
I certify under penalty of law that all process
equipment required to be cleaned or replaced under
35
Ill. Adm. Code 721.135 was cleaned or replaced
as represented
in the equipment cleaning and
replacement plan and accompanying documentation.
I am aware that there are significant penalties
for providing false information, including the
possibility of fine or imprisonment.
(Source:
Added at 15
Ill.
Req.
,
effective
)
Section 721.Appendix C
Chemical Analysis Test Methods
The Board incorporates by reference 40 CFR 261, Appendix III
(1030),
as amended at 54 Fed.
Rcg.
41407, October
C,
1009,
and as
amended at 55 Fed.
fleg.
0948, March 9,
1900 and at 55 Fed.
fleg.
1840C, May 2,
190’O
(1990). as amended at 55 Fed. Req.
50483,
December
6.
1990.
This Section incorporates no future editions
or modifications.
(Source:
Amended at 15
Ill.
Reg.
,
effective
)
Section 721.Appendix G
Basis for Listing Hazardous Wastes
EPA
Hazardous
Waste No. Hazardous Constitutents for which Listed
FOOl
Tetrachioroethylene, methylene chloride, trichloro-
ethylene,
1,1, 1—trichloroethane, carbon tetrachloride,
chlorinated fluorocarbons.
125—240
69
F002
Tetrachloroethylene, methylene chloride, trichloro-
ethylene,
1,1,1-trichloroethane,
1,1,2-trichloro-
ethane,
chlorobenzene,
1,1,2—trichloro—1,2, 2— tn—
fluoroethane, ortho—dichlorobenzene, tnichlorofluoro—
methane.
F003
N.A.
F004
Cresols and cresylic acid,
nitrobenzene.
F005
Toluene, methyl ethyl ketone, carbon disulfide,
iso—
butanol, pynidine,
2-ethoxyethanol, benzene,
2—nitro-
propane
F006
Cadmium, hexavalent chromium,
nickel, cyanide
(complexed).
F007
Cyanide (salts).
F008
Cyanide (salts).
FOO9
Cyanide
(salts).
FOlO
Cyanide
(salts).
FOll
Cyanide (salts).
F012
Cyanide (complexed).
F019
Hexavalent chromium, cyanide (complexed).
FO2O
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans; tn— and tetrachlorophenols
and their chlorophenoxy derivative acids,
esters,
ethers, amines and other salts.
F02l
Penta- and hexachlorodibenzo-p-dioxins; penta- and
hexachlorodibenzofurans; pentachlorophenol and its
derivatives.
F022
Tetra-,
penta- and hexachlorodibenzo-p-dioxins; tetra—
penta— and hexachlorodibenzofurans.
F023
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans; tn— and tetrachlorophenols
and their chiorophenoxy derivative acids, esters,
ethers,
amines and other salts.
F024
Chloromethane, dichloromethane, trichloromethane,
carbon tetrachloride, chloroethylene,
1, 1—dichloro—
ethane,
1, 2—dichloroethane,
trans—i, 2—dichloroethyl—
ene,
1,1-dichioroethylene,
1,1,1—trichioroethane,
125—24 1
70
1, 1,2-tnichloroethane, tnichloroethylene,
1,1,1,2-
tetrachloroethane,
1,1,2,2—tetrachloroethane,
tetra—
chloroethylene,
pentachloroethane, hexachloroethane,
allyl chloride (3—chloropropene), dichlonopropane, di-
chioropropene,
2—chloro—1,3—butadiene, hexachloro—i,3—
butadiene, hexachlorocyclopentadiene, hexachiorocyclo—
hexane, benzene, chlorobenzene, dichlorobenzenes,
1,2
,
4—trichlorobenzene, tetrachlorobenzenes, penta—
chlorobenzene, hexachlorobenzene,
toluene, naphthalene.
F025
Chloromethane, dichloromethane, trichloromethane;
carbon tetrachloride; chloroethylene;
1,i-dichloro-
ethane;
1, 2-dichloroethane; trans-i,2-dichloroethyi-
ene;
1, l-dichloroethylene; 1,1,l-trichloroethane;
1,1,2—tnichioroethane;
tnichloroethylene; 1,1,1,2—
tetrachioroethane;
1,1,2,2-tetrachloroethane; tetra-
chloroethylene; pentachloroethane; hexachloroethane;
allyl chloride (3-chloropropene); dichloropropane; di-
chioropropene; 2-chloro-l, 3-butadiene; hexachloro-i,3-
butadiene;
hexachlorocyclopentadiene; benzene; chloro—
benzene; dichlorobenzene;
1,2,4—trichlorobenzene;
tetrachlorobenzene; pentachlorobenzene; hexachloro—
benzene; toluene; naphthalene.
FO26
Tetra-, penta-, and hexachlorodibenzo-p—dioxins; tetra-
penta—, and hexachlorodibenzofurans.
F027
retra-,
penta-, and hexachlorodibenzo-p—dioxins; tetra-
penta—, and hexachlorodibenzofurans; tn—, tetna—,
and pentachlonophenols and their chlorophenoxy
~enivative acids,
esters,
ethers, amine and other
salts.
FO28
retra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-
penta—, and hexachlorodibenzofurans; tn—,
tetra—,
and pentachiorophenols and their chlorophenoxy
lenivative acids, esters, ethers,
amine and other
salts.
F032
Benz (a)anthracene, benzo(a)pyrene,
libenz (a,h)anthnacene, indeno(l,2
,
3—cd)pyrene,
Dentachiorophenol, arsenic,
chromium,
tetra—,.. penta—,
~iexa—,heptachlorodibenzo—p—djoxins, tetra—, penta—,
~iexa—,heptachlorodibenzofurans.
F034
3enz (a) anthracene, benzo(k) fluoranthene,,
Denzo(a)pvrene, dibenz(a,h)anthracene.
indeno(l,2,3—
~d)pyrene, naphthalene, arsenic chromium.
F035
~rsenic. chromium and lead.
F037
3enzene.
benzo(a)pyrene,
chrysene,
lead, chromium.
125—242
71
F038
Benzene, benzp(a)pyrene,
chrysene,
lead, chromium.
FO39
All constituents for which treatment standards are
specified for multi—source leachate (wastewaters and
non-wastewaters)
under 35 Ill.
Adni. Code 728.Table B
(Constituent Concentrations in Waste)
1001
Pentachlorophenol, phenol,
2-chlorophenol, p-chloro-m—
cresol,
2,4-dimethylphenol, 2,4-dinitrophenol, tn-
chlorophenols, tetrachlorophenols,
2,4—dinitrophenol,
cresosote,
chrysene, naphthalene, fluoranthene, benzo—
(b)fluoranthene, benzo(a)pyrene,
indeno(1,2,3—cd)-
pyrene,
benz(a) anthracene, dibenz (a) anthracene,
ace—
naphthalene.
1002
Hexavalent chromium,
lead.
1003
Hexavalent chromium,
lead.
1004
Hexavalent chromuim.
K005
Hexavalent chromium,
lead.
K006
Hexavalent chromium.
1007
Cyanide (complexed), hexavalent chromium.
K008
Hexavalent chromium.
K009
Chloroform,
formaldehyde, methylene chloride, methyl
chloride, paraldehyde, formic acid.
1010
Chloroform,
formaldehyde, methylene chloride, methyl
chloride, paraldehyde, formic acid,
chloroacetaldehyde.
KOll
Acrylonitnile, acetonitnile, hydrocyanic acid.
K0l3
Hydro cyanic acid,
acrylonitnile, acetonitnile.
K014
Acetonitnile, acrylamide.
1015
Benzyl chloride, chlorobenzene, toluene, benzotni—
chloride.
1016
Hexachlorobenzene,
hexachlorobutadiene, carbon tetra—
chloride, hexachloroethane, perchioroethylene.
1017
Epichiorohydnin, chloroethers
bis(chloromethyl)
ether
and bis-(2-chloroethyl) ethers,
tnichloropropane, di-
chloropropanols.
125—243
72
1018
1,2-dichloroethane, tnichloroethylene, hexachlorobuta-
diene, hexachlorobenzene.
1019
Ethylene dichlonide,
1,1,l-tnichloroethane,
1,1,2-tn-
chloroethane, tetrachloroethanes
(1,1,2,2—tetrachloro—
ethane and 1,1,1, 2-tetrachloroethane), tnichloroethyi-
ene, tetrachloroethylene, carbon tetrachlonide, chloro-
form, vinyl chloride, vinylidene chloride.
1020
Ethylene dichlonide,
1,1,1-tnichioroethane,
1,1,2-tn-
chioroethane, tetrachloroethanes (1,1,2,2—tetrachioro—
ethane and 1,1,1, 2-tetrachloroethane), tnichloroethyl-
ene, tetrachloroethylene, carbon tetrachloride, chloro-
form, vinyl chloride, vinylidene chloride.
1021
Antimony, carbon tetrachlonide, chloroform.
1022
Phenol, tars (polycyclic aromatic hydrocarbons).
K023
Phthalic anhydride,
maleic anhydnide.
1024
Phthalic anhydnide,
1,4-naphthoguinone.
K025
Neta-dinitnobenzene,
2, 4-dinitrotoluene.
1026
Paraldehyde, pynidines,
2—picoline.
1027
Toluene diisocyanate, toluene-2,
4—diamine.
K028
1,1,1-tnichloroethane, vinyl chloride.
K029
l,2—dichlonoethane, 1,1,l—tnichloroethane, vinyl
chloride, vinylidene chloride, chloroform.
K030
Hexachlorobenzene, hexachiorobutadiene, hexachloro
ethane,
1,1,1,2—tetnachloroethane,
1,1,2, 2—tetra—
chloroethane, ethylene dichionide.
K03l
Arsenic.
1032
Hexachiorocyclopentadiene.
K033
Hexachlorocyclopentadiene.
1034
Hexachlorocyclopentadiene.
1035
Creosote, chrysene, naphthalene, fluonanthene, benzo—
(b)fluoranthene,
benzo(a)pyrene,
indeno(l,2, 3—cd)
pyrene, benzo(a)anthnacene, dibenzo(a)anthracene, ace~
naphthalene.
1036
Toluene, phosphorodithioic and phosphorothioic acid
125—244
73
esters.
1037
Toluene, phosphorodithioic and phosphorothioic acid
esters.
1038
Phorate,
formaldehyde, phosphorodithioic and phosphoro-
thioic acid esters.
1039
Phosphorodithioic and phosphorothioic acid esters.
1040
Phorate,
formaldehyde, phosphorodithioic and phosphoro-
thioic acid esters.
1041
Toxaphene.
1042
Hexachlorobenzene,
ortho—dichlorobenzene.
K043
2 ,4-dichlonophenol,
2, 6-dichlonophenol,
2,4,6—tn-
chlorophenol.
1044
NA.
1045
N.A.
1046
Lead
1047
N.A.
1048
Hexavalent chromium,
lead.
1049
Hexavalent chromium,
lead.
K050
Hexavalent chromium.
1051
Hexavalent chromium,
lead.
1052
Lead
1060
Cyanide, naphthalene, phenolic compounds, arsenic.
1061
Hexavalent chromium,
lead,
cadmium.
1062
Hexavalent chromium,
lead.
K064
Lead,
cadmium
1065
Lead,
cadmium
1066
Lead, cadmium
K069
Hexavalent chromium,
lead, cadmium.
125—245
74
1071
Mercury.
1073
Chloroform, carbon tetrachlonide, hexachloroethane,
tnichloroethane, tetrachlonoethylene, dichlonoethyl-
ene,
1,l,2,2—tetrachloroethane.
K083
Aniline,
diphenylamine, nitrobenzene, phenylenedi-
amine.
K084
Arsenic.
K085
Benzene, dichlorobenzenes,
tnichlorobenzenes,
tetra—
chlorobenzenes, pentachlonobenzene, hexachlorobenzene,
benzyl chloride.
K086
Lead,
hexavalent chromium.
K087
Phenol,
naphthalene.
K088
Cyanide (complexes)
1090
‘
Chromium
K09l
Chromium
1093
Phthalic anhydnide maleic anhydnide.
1094
Phthalic anhydnide.
1095
1,1,2-tnichlonoethane,
1,1,l,2—tetnachloroethane,
1, 1,2, 2—tetnachlonoethane.
K096
1, 2-dichloroethane,
1,1,1,—tnichlonoethane,
1,1,2—tni-
chlonoethane.
1097
Chlordane, heptachior.
K098
Toxaphene.
1099
2,4—dichlorophenol, 2,4,6-tnichlonophenol.
1100
Hexavalent chromium,
lead, cadmium.
Kl01
Arsenic.
1102
Arsenic.
1103
Aniline, nitrobenzene, ‘phenylenediamine.
K104
Aniline, benzene, diphenylamine, nitrobenzene,
phenyl-
enediamine.
125—246
75
1105
Benzene, monochlorobenzene, dichlorobenzenes,
2,4,6—
tnichlorophenol.
K106
Mercury.
K107
1,l-Dimethylhydrazine
(UDMH)
1108
i,l-Dimethylhydrazine
(TJDMH)
K1O9
i,l-Dimethylhydnazine
(UDMH)
KilO
1,l-Dimethylhydrazine
(UDMH)
1111
2, 4-Dinitrotoluene.
1112
2,4-Toluenediamine, o-toluidine, p—toluidine, aniline.
Kll3
2,4-Toluenediamine, o-toluidine, p—toluidine, aniline.
Kll4
2,4-Toluenediamine, o-toluidine, p—toluidine.
K1l5
2, 4-Toluenediamine.
K116
Carbon tetrachlonide, tetrachloroethylene,
chloroform,
phosgene.
Kl17
Ethylene dibnomide
Kl18
Ethylene dibromide
K123
Ethylene thiounea
1124
Ethylene thiourea
1125
Ethylene thiourea
1126
Ethylene thiounea
K131
Dimethyl sulfate, methyl bromide
1132
Methyl bromide
1136
Ethylene dibromide
N.A. ——Waste is hazardous because it fails the test for the
characteristic of ignitability, conrosivity or reactivity.
(Source:
Amended at
15 Ill. Reg.
,
effective
)
125—247
76
Section 721.Appendix H
Hazardous Constituents
Hazard-
Chemical
ous
Abstracts
Waste
Coemon
Name
Chemical
Abstracts
Name
Nurber
Nu~*er
Acetonitrile
Same
75-05-8
0003
Acetophenone
Ethanone,
1-phenyl-
98-86-2
0004
2-Acetytaminof
tuorene
Acetamide,
N-9H- fluoren-2-yl
-
53-96-3
0005
Acetyl
chloride
Same
75-36-5
0006
1-Acetyl-2-thiourea
Acetamide,
N-(aminothioxomethyl)-
591-08-2
P002
Acrolein
•
2-Propenat
107-02-8
P003
Acrylamide
2-Propenamide
79-06-1
0007
Acrylonitrile
2-Propenenitrile
107-13-1
0009
Aflatoxins
Same
1402-68-2
Aldicarb
Propanal,
2-n,ethyl-2-(methyLthio)-,
116-06-3
P070
0-
((methy(amino)carbonyloxime
Aldrin
1,4,5,8-Dimethanonaphthalene,
309-00-2
P004
1,2,3,4,10, 10-hexachtoro-
1,4,4a,5,8,8a-hexahydro-,
1-alpha,
4-alpha, 4a-beta,
5-alpha,
8-alpha,
8a-beta)-
Allyl
alcohol
‘
2-Propen-1-oL
107-18-6
P005
Alusinun
phosphide
Same
20859-73-8
P006
4-Aniinobiphenyl
(1,1 ‘-Biphenyl
-4-amine
92-67-1
5-(AminoinethyL)-3-isoxazoLol
3(2H)-Isoxazolone, 5-(aminomethyl)-
2763-96-4
P007
4-Miinopyridine
4-Pyridinamine
504-24-5
P008
Amitrole
1H-1,2,4-Triazot-3-amine
61-82-5
0011
Airinoniun
vanadate
Vanadic acid,
aninoniun
salt
7803-55-6
0119
Aniline
Benzenamine
62-53-3
U012
Antimony
Same
7440-36-0
Antimony
conç)ounds,
N.0.S.
(not
otherwise
specified)
Aramite
Sulfurous acid, 2-chloroethyl-,
2-
140-57-8
(4-(1,1-dimethyLethyl )phenoxy
-1-
methytethyl ester
Arsenic
Arsenic
7440-38-2
Arsenic coopounds, N.0.S,
Arsenic acid
Arsenic acid H3AsO4
7778-39-4
P010
Arsenic pentoxide
Arsenic oxide As205
1303-28-2
P011
Arsenic trioxide
Arsenic oxide As203
1327-53-3
P012
Auramine
Benzenamine, 4,4’-carbonimidoyt-
492-80-8
0014
bis(N,N-dimethyl-
Azaserine
L-Serine, diazoacetate (ester)
115-02-6
0015
Barius
Same
7440-39-3
Baritin
coirpounds,
N.0.S.
Sariun cyanide
Same
542-62-1
P013
Benz(cacridine
Same
225-51-4
U016
Benzfaanthracene
Same
56-55-3
0018
Benzal chloride
Benzene,
(dichtoromethyl)-
98-87-3
0017
Benzene
Same
71-43-2
0018
Benzenearsonic acid
Arsonic acid, phenyl-
98-05-5
Benzidine
(1,1’-Biphenyl-4,4’-diamine
92-87-5
U021
Benzo (b
f tuoranthene
Benz (e acephenanthrytene
205-99-2
Benzotj)fluoranthene
Same
205-82-3
Benzo(k)ftuoranthene
207-08-9
Benzo(apyrene
Same
50-32-8
0022
p-Benzoquinone
2,5Cyc(ohexadiene-1,4-dione
106-51-4
0197
Benzotrichloride
Benzene,
(trichloromethyt)-
98-07-7
0023
Benzyl chloride
Benzene,
(chloronethyt)-
100-44-7
P028
Beryl(iun
Same
7440-41-7
P015
Berylliun coopounds,
N.0.S.
125—248
77
Bromoacetone
Bromoform
4-Bromophenyl
phenyl
ether
Brucine
Butyl benzyl phthalate
Cacodytic
acid
Cac*niun
Cackniun
conpounds,
PI.0.S.
Catciun chromate
Catciun
cyanide
Carbon
disulfide
Carbon
oxyftuoride
Carbon
tetrachloride
Chloral
Chlormthucil
Chlordane
Chlordane,
alpha
and
ganina
isomers
Chlorinated
benzenes,
N.OS.
Chlorinated
ethane,
N.0.S.
Chlorinated fluorocarbons, N.0.S.
Chlorinated
naphthalene,
N.0.S.
Chlorinated phenol, NOS.
Chlornaphazine
Ch loroacetaldehyde
Chloroalkyt
ethers,
N.0.S.
p-Chtoroaniline
Ch Iorobenzene
Chlorobenzi late
p-Ch loro-m-cresot
2-Chloroethyt
vinyl
ether
Chloroform
Chloromethyl methyl ether
beta-Ch loronaphthalene
o-Chlorophenot
1- (o-ChlorophenyL)thiourea
Chloroprene
3-Chloropropionitrile
Chromiun
Chromiun
coppounds,
N.0.S.
Chrysene
Citrus
red
No.
2
Coal tar creosote
Copper
cyanide
Creosote
Cresols
(Cresylic
acid)
Crotonaldehyde
Cyanides
(soluble
salts
and
coirplexes),
N.0.S.
Cyanogen
Cyanogen bromide
Cyanogen
chloride
Cycasin
2-CycI.ohexyl-4 ,6-dini trophenot
Cyctophosphamide
2-Propanone,
1-bromo-
Methane, tribromo-
Benzene,
1 -bromo-4-phenoxy-
Strychnidin-lO-one,
2,3-dimethoxy-
1,2-Benzenedicarboxylic acid,
butyl
phenylmethyt
ester
Arsenic
acid,
dimethyl-
Same
Chronic acid H2Cr0~,calciun salt
Calciun cyanide Ca~(CN)2
Same
Carbonic
difuoride
Methane,
tetrachloro-
Acetaldehyde,
trichloro-
Benzenebutanoic
acid,
4(bis-(2-
chloroethyt)amino
-
4,7-Methano-1H-
indene-
1,2,4,5,6,7,,8,8-octachloro-
2,3,3a,4,7,7a-hexahydro-
Naphthalenamine,
N,N’-bis(2-chloro-
ethyl)-
Acetaldehyde, chioro-
Benzenamine, 4-chloro-
Benzene, chloro-
Benzeneacetic
acid,
4-chioro-alpha-
(4-chlorophenyl )-alpha-hydroxy-,
ethyl
ester
Phenol, 4-chloro-3-methyL-
Ethene, (2-chtoroethoxy)-
Methane, trichloro-
Methane,
ch Ioromethoxy-
Waphthalene,
2-chloro-
Phenol,
2-chloro-
Thiourea,
(2-chlorophenyt)-
1 ,3-Butadiene, 2-chloro-
Propanenitrile, 3-chloro-
Same
Same
2-Haphthalenol,
1-((2,5-dimethoxy-
phenyt)azo)-
Same
Copper
cyanide
CuCH
Same
Phenol,
methyl-
2-Butenal
Ethanedinitrile
Cyanogen
bromide (CN)Br
Cyanogen
chloride
(CH)Cl
Beta-D-glucopyranoside, (methyl-OWN-
azoxy)methyl
-
Phenol, 2-cyclohexyl-4,6-dinitro-
2H-1,3,2-Oxazaphosphorin-2-amine,
N,P4-bis(2-chloroethyl)tetrahydro-,
2-oxide
598-31-2
75-25-2
101-55-3
357-57-3
85-68-7
75-60-5
0136
7440-43-9
59- 50-7
110-75-8
67-66-3
107-30-2
9 1-58-7
95-57-8
5344-82-1
126-99-8
542-76-7
7440-47-3
2 18-01-9
6358-53-8
8007-45-2
544-92-3
1319-
77-3
4170-30-3
460-19-5
506-68-3
506-77-4
14901-08-7
P017
0225
0030
P018
13765-19-0
592-01-8
75-
15-0
353-50-4
56-23-5
75
-87-6
305-03-3
57-74-9
0032
P021
P022
0033
0211
0034
0035
0036
0036
49403-1
0026
107-20-0
P023
106-47-8
108-90-7
510- 15-6
P024
U037
0038
0039
0042
0044
0046
0047
0048
P026
P027
0050
P029
0051
0052
0053
P030
P031
0246
P033
P034
0058
131-89-5
50- 18-0
125—249
78
o
ibenz(a,hacridine
Dibenz(a,jacridine
Dibenz
(a,h
anthracene
7H-Dibenzo(c,gcarbazole
Dibenzo(a,epyrene
Dibenzo(a,hpyrene
Dibenzo(a,ipyrene
1,2-Dibromo-3-chloropropane
Dibutyt phthalate
o-Dichtorobenzene
m-D i ch I
orobenzene
p-Dichlorobenzene
Dichtorobenzene,
N.0.S.
3,3’-Dichlorobenzidine
I,4-Dichtoro-2-butene
Di
chtorodi f
luoromethane
Dichloroethylene, PLO.S.
1,1-Dichloroethylene
1,2-Dichloroethylene
Dichloroethyl ether
Dichloroisopropyl ether
Di ch loromethoxyethane
Dichloromethyl ether
2,4-Di chlorophenol
2,6-Di chlorophenot
D ichlorophenytarsine
Oichtoropropane, PLO.S.
Dichloropropanol, N.0.S.
Dichloropropene, N.O.S.
1,3-Dichloropropene
Dieldrin
1,2:3,4-Diepoxybutane
Diethylarsine
1,4-Diethyteneoxide
Diethylhexyt
phthalate
N,N’ -Diethythydrazine
Acetic
acid,
(2,4-dichlorophenoxy)-
Acetic acid, (2,4-dichlorophenoxy)-,
salts
and
esters
5,12-Naphthacenedione,
8-acetyt-lO-
((3-amino-2,3,6- trideoxy-alpha- L-
lyxo-hexopyranosyt)oxy
-7,8,9,10-
tetrahydro-6,8,11-trihydroxy-l-meth-
oxy-, 8S-cis)-
Benzene,
1,1 ‘-(2,2-dichloroethyt-
idene)bis(4-chtoro-
Benzene,
1,1’-(dichloroethenyl-
idene)bfs(4-chloro-
Benzene, 1,1’-(2,2,2-trichloro-
ethyl
idene)bis
(4-chtoro-
Carbamothioic
acid,
bis(1-methyl-
ethyl)-,
S-(2,3-dichtoro-2-propenyl)
ester
Same
Same
Same
Same
Naphtho(1,2,3 ,4-def chrysene
0 ibenzo(b,defchrysene
Benzo (rst
pentaphene
Propane,
1,2-dibromo-3-chloro-
1,2-Benzenedicarboxytic
acid,
dibutyt
ester
Benzene,
1,2-dichloro-
Benzene,
1 ,3-dichtoro-
Benzene,
1 ,4-dichloro-
Benzene,
dichloro-
(1,1’-Biphenyl-4,4’-diamine,
3,3’-
dichloro-
2-Butene,
1,4-dichloro-
Methane, dichlorodifluoro-
DichioroethyLene
Ethene, 1,1-dichloro-
Ethene, 1,2-dichloro-, CE)-
Ethane,
1,1’ -oxybis(2-chloro-
Propane, 2,2’-oxybis(2-chloro-
Ethane,
1,1’
-
(methylenebis(oxy)bis-
t2-chloro-
Methane,
oxybis (ch Loro-
Phenol, 2,4-dichloro-
Phenol, 2,6-dichloro-
Arsonous dichloride, phenyt-
Propane, dichloro-
Propanol, dichloro-
1-Propene,
dichloro-
1-Propene,
1,3-dichtoro-
2,7:3,6-0 imethanonaphth (2,3-b
oxi
-
rene,
3,4,5,6,9,9-hexachloro-
la,2,2a,3,6,6a,7,7a-octahydro-,
Cia
alpha,
2
beta,
2a
alpha,
3
beta,
6
beta,
6a
alpha,
7
beta,
Ta
alpha)-
2,2’ -Bioxirane
Arsine,
diethyl-
1,4-Dioxane
1,2-Benzenedicarboxylic
acid,
bis(2-
ethylhexyl)
ester
Hydrazine,
1,2-diethyl-
94-75-7
0240
0240
20830-81 -3
0059
226-36-8
224-42-0
53-70-3
194-59-2
192-65 -4
189-64-0
189-55 -9
96-12-8
84-74-2
95-50-1
541-73-1
106-46-7
25321-22-6
91-94-1
764-41-0
75
-71-8
25323-30-2
75-35-4
156-60-5
111-44-4
108-60-1
111-91-1
542-88-1
120-83-2
87-65 -0
696-28-6
26638-19-7
26545-73-3
26952-23-8
542-75 -6
60-57-1
2,4-0
2,4-0,
salts
and
esters
Daunomyc
in
DOD
DDE
DDT
Diallate
72-54-8
0060
72-55-9
50-29-3
0061
2303-16-4
0062
U063
0064
0066
0069
0070
0071
0072
0073
0074
0075
0078
0079
0025
0027
U024
P016
0081
0082
P036
0084
P037
0085
P038
Ui08
0028
1464-53-5
692-42-2
123-91-1
117-81-7
1615-80-1
0086
125—250
79
0,o-Diethyl-S-methyl
dithiophosphate
Phosphorodithioic
acid,
0,0-diethyl
3288-58-2
0087
S-methyl
ester
Diethyl-p-nitrophenyt
phosphate
Phosphoric
acid,
diethyl
4-nitro-
311-45-5
P041
phenyt
ester
Diethyl
phthaLate
i,2-Benzenedicarboxytic
acid,
84-66-2
0088
diethyl ester
0,0-Diethyl 0-pyrazinyl phosphorothioate
Phosphorothioic
acid, 0,0-diethyt 0-
297-97-2
P040
pyrazinyt ester
Diethylstilbestrol
Phenol,
4,4’-(i,2-diethyl-i,2-
56-53-1
0089
•
ethenediyt)bis-,
(E)-
Dihydrosafrote
1,3-Benzodioxole, 5-propyl-
94-58-6
0090
Diisopropylftuorophosphate
(DFP)
Phosphoroftuoridic
acid,
bis(1-
55-91-4
P043
methylethyl) ester
Dimethoate
Phosphorodithioic acid, 0,0-dimethyL
60-51-5
P044
S- (2-(methylamino)-2-oxoethyl
ester
3,3’-Oimethoxybenzidine
(i,1’-Biphenyl-4,4’-diamine,
3,3’-
119-90-4
0091
dimethoxy-
p-Dimethylaminoazobenzene
Benzenamine,
N,N-dimethyl-4-(phenyl-
60-11-7
0093
azo)-
7,12-Dimethylbenzaanthracene
Benz(aanthracene,
7,12-dimethyl-
57-97-6
0094
3,3’-Dimethylbenzidine
(1,1’-Biphenyl-4,4’-diamine,
3,3’-
119-93-7
0095
dimethyl-
Dimethylcarbamoyt chloride
Carbonic chLoride, dimethyl-
79-44-7
0097
1,1-Dimethylhydrazine
Hydrazine,
1,1-dimethyl-
57-14-7
0098
i,2-Dimethylhydrazine
Hydrazine,
1,2-dimethyt-
540-73-8
0099
alpha,alplia-Dimethylphenethylamine
Benzeneethanamine,
alpha,
alpha-
122-09-8
P046
dimethyt
-
2,4-DimethyLphenol
Phenol, 2,4-dimethyl-
105-67-9
0101
Dimethylphthalate
1,2-Benzenedicarboxylic acid,
131-11-3
0102
dimethyt ester
Dimethyl sulfate
Sulfuric acid, dimethyl
ester
77-78-1
0103
Dinitrobenzene, NOS.
Benzene,
dinitro-
25154-54-5
4,6-Dinitro-o-cresol
Phenol, 2-methyl-4,6-dinitro-
534-52-1
P047
4,6-Dinitro-o-cresol salts
P047
2,4-Dinitrophenot
Phenol, 2,4-dinitro-
51-28-5
P048
2,4-Dinitrotoluene
Benzene,
1-methyl-2,4-dinitro-
121-14-2
U105
2,6-Dinitrotoluene
Benzene,
2-methyl-1,3-dinitro-
606-20-2
U106
Dinoseb
Phenol,
2-Ci-methylpropyl)-4,6-
88-85-7
P020
dinitro-
Di-n-octyl
phthalate
i,2-Benzenedicarboxylic
acid,
117-84-0
U107
dioctyl ester
Diphenylamine
Benzenamine,
N-phenyl-
122-39-4
1,2-Diphenylhydrazine
Hydrazine,
1,2-diphenyl-
122-66-7
U109
Di-n-propylnitrosamine
1-Propanamine,
N-nitroso-H-propyl-
621-64-7
U111
Disutfoton
Phosphorodithioic acid,
0,
0-diethyl
298-04-4
P039
S- (2-(ethytthio)ethyl
ester
Dithiobiuret
Thioimidodicarbonic diamide
541-53-7
P049
((H2N)C(S) 2NH
Endosulfan
6,9-Methano-2,4,3-benzodioxathiepen,
115-29-7
P050
6,7,8,9, 10,10-hexachloro-
1,5,5a,6,9,9a-hexahydro-,
3-oxide,
Endothal
7-Oxabicyclo(2.2.1)heptane-2,3-di
-
145-73-3
P088
carboxylic acid
Endrin
2,7:3,6-Dimethanonaphth(2,3-bloxi-
72-20-8
P051
rene,3,4,5
,6,9,9-hexachloro-
ia,2,2a,3,6,6a,7,7a-octahydro-,
Cia
aLpha,
2
beta,
2a
beta,
3
alpha,
6
aLpha,
6a
beta,
7
beta,
7a
alpha)-,
Endrin metaboLites
P051
Epichlorohydrin
Oxirane,
(chloromethyt)-
106-89-8
0041
Epinephrine
i,2-Benzenediol,
4-(1-hydroxy-2-
51-43-4
P042
(methylamino)ethyl-,
CR)-
Ethyl
carbamate
(urethane)
Carbamic acid,
ethyl ester
51-79-6
U238
125—251
80
Ethyl
cyanide
Propanenitrile
107-12-0
P101
Ethylenebisdithiocarbamic acid
Carbamodithioic
acid,
1,2-ethane-
111-54-6
0114
diylbis-
Ethytenebisdithiocarbamic
acid,
salts
and
0114
esters
Ethylene
dibromide
Ethane,
1,2-dibromo-
•
106-93-4
0067
Ethylene dichloride
Ethane,
i,2-dichloro-
107-062
0077
Ethylene
glycol monoethyl ether
Ethanol, 2-ethoxy-
110-80-5
0359
Ethyteneimine
Aziridine
151-56-4
P054
Ethylene
oxide
Oxirane
75-21-8
0115
Ethylenethiourea
2-Imidazotidinethione
96-45-7
0116
EthyLidine dichloride
Ethane,
i,1-dichloro-
75-34-3
0076
Ethyl
methacrytate
2-Propenoic
acid,
2-methyl-,
ethyl
97-63-2
0118
•
ester
Ethyl
methanesulfonate
Methanesutfonic
acid,
ethyl
ester
62-50-0
0119
Fairphur
Phosphorothioc acid, 0-14-
52-85-7
P097
((dimethylamino)sutfonylphenyl
0,0-dimethyl ester
Ftuoranthene
Same
206-44-0
0120
Fluorine
Same
7782-41-4
P056
Fluoroacetamide
Acetamide, 2-fluoro-
640-19-7
P057
Fluoroacetic
acid,
sodiun
salt
Acetic acid,
fluoro-,
sodiun
salt
62-74-8
P058
Formaldehyde
Same
50-00-0
0122
Formic acid
Same
64-18-16
0123
Clycidylatdehyde
Oxiranecarboxaldehyde
765-34-4
0126
Halomethanes,
N.0.S.
Heptachlor
4,7-Methano-1H-indene,
76-44-8
P059
•
1 ,4,5,6,7,8,8-heptachloro-3a,4,7,7a-
tetrahydro-
Heptachlor epoxide
2,5-Methano-2H-indeno(1,2boxirene,
1024-57-3
2,3,4,5,6, 7,7-heptachloro-
ia,lb,5,5a,6,6a-hexahydro-,
(la
alpha,
lb
beta,
2
alpha,
5
aLpha,
5a
beta,
6 beta, 6a alpha)-
Heptachlor epoxide (alpha, beta
and
gamna
isomers)
Heptach lorodibenzofurans
Heptachlorodibenzo-p-dioxi ns
HexachLorobenzene
Benzene, hexachtoro-
118-74-1
U127
Hexachlorobutadiene
1,3-Butadiene,
1,1,2,3,4,4-hexa-
87-68-3
U128
chloro-
Hexachlorocyclo-pentadiene
1,3-Cyclopentadiene,
1,2,3,4,5,5-
77-47-4
0130
hexach Ioro-
Hexachlorodi benzo-p-dioxins
Hexach Iorodi benzofurans
Hexachloroethane
Ethane, hexachloro-
67-72-1
0131
Hexachlorophene
Phenol, 2,2’-methytenebis(3,4,6-tri-
70-30-4
0132
chloro-
HexachLoropropene
i-Propene,
1,1,2,3,3,3-hexachLoro-
1888-71-7
0243
Hexaethyltetraphosphate
Tetraphosphoric
acid, hexaethyl
757-58-4
P062
ester
Hydrazine
Same
302-01-2
U133
Hydrogen cyanide
Hydrocyanic acid
74-90-8
P063
Hydrogen
fluoride
Hydrofluoric
acid
7664-39-3
0134
Hydrogen sulfide
Hydrogen suLfide H2S
7783-06-4
0135
lndeno(1,2,3-cdpyrene
Same
193-39-5
U137
Isobutyl
alcohol
1-Propanol,
2-methyl-
78-83-i
0140
Isodrin
i,4:5,8-Dimethanonaphthatene,
465-73-6
P060
1,2,3,4,10, 10-hexachloro-
i,4,4a,5,8,8a-hexahydro-,
Ci
alpha,
4
alpha,
4a
beta,
5
beta,
8
beta,
8a
beta)-,
Isosafrole
1,3-Benzodioxole, 5-(1-propenyl)-
120-58-1
U141
125—252
81
Lead
Lead
and
conpotrds,
N.0.S.
Lead
acetate
Lead
phosphate
Lead
subacetate
Li ndane
Maleic anhydride
Maleic
hydrazide
Matononitrile
Metpha tan
Mercury
Mercury conpounds, N.0S.
Mercury fulminate
Methacrytonitri le
Methapyrilene
Metho
Imyt
Methoxychbr
Methyl bromide
Methyl chloride
Methytchlorocarbonate
Methyl
chloroform
3-Methytcholanthrene
4,4’-Methylenebis(2-chloroaniline)
Methylene bromide
Methytene chloride
Methyl ethyl ketone (MEK)
Methyl ethyl ketone peroxide
Methyl hydrazine
Methyl
iodide
Methyl
isocyanate
2-Methyllactonitrile
Methyl methacrytate
Methyl
methanesutfonate
Methyl
parathion
Methylthiouraci I
Miton~ycinC
1 ,3,4-Metheno-2H-cyclobutalcdpenta-
len-2-one,
1,la,3,3a,4,5,5,5a,5b,6-
decachlorooctahydro-,
2-Butenoic
acid,
2-methyl-,
7-1(2,3-
dihydroxy-2- (1 -methoxyethyl )-3-
methyl-i-oxobutoxymethyl
-2,3,5,7a-
tetrahydro-1H-pyrrolizin-l-yL
ester,
(lS-(i-aLpha(Z),
7(2S*,
3R*),
7a
alpha-
Same
Acetic acid,
lead
(2+)
salt
Phosphoric acid,
lead (2+) salt
12:3)
Lead, bis(acetato-0)tetrahydroxytri
-
CycLohexane,
1,2,3,4,5,6-hexa-
chloro-,
1
alpha,
2
alpha,
3
beta,
4
aLpha,
5
aLpha,
6 beta)-
2,5-Furandione
3,6-Pyridazinedione, i,2-dihydro-
Propanedinitrile
L-Phenylatanine,
4- (bis(2-chloro-
ethyl)amino
-
Same
Futminic acid, mercury (2+) salt
2-Propenenitrile, 2-methyl-
i,2-Ethanediamine,
N,N-dimethyl-N’-
2-pyridinyt-N’
-
(2-thienytmethyl
)-
Ethanimidothioic acid,
N- (((methyl-
amino)carbonyl)oxy-,
methyl
ester
Benzene,
1,1’-(2,2,2-trichloroethyl-
idene)bis(4-methoxy-
Methane,
bromo-
Methane, chloro-
Carbonochloridic acid, methyl ester
Ethane,
i,1,i-trichtoro-
Benzcj3aceanthrylene, 1,2-dihydro-
3-methyl
-
Benzenamine, 4,4’
-methylenebi s(2-
chloro-
Methane,
dibromo-
Methane, dichloro-
2-Butanone
2-Butanone,
peroxide
Hydrazine, methyl-
Methane,
iodo-
Methane,
isocyanato-
Propanenitrile, 2-hydroxy-2-methyl-
2-Propenoic acid, 2-methyl-, methyl
ester
Methanesulfonic
acid, methyl ester
Phosphorothioic
acid,
0,0-dimethyl
0- (4-ni trophenyl)
ester
4-(1H)-Pyrimidinone,
2,3-dihydro-6-
methyl-2-thioxo-
Azirino(2’ ,3’ :3,4pyrrobotl
,2-
a
indote-4,7-dione,
6-amino-8-
(((aminocarbonyl)oxymethyt
-
1,1a,2,8,8a,8b-hexahydro-Ba-methoxy-
5-methyl-,
(la-S-(ia
alpha,
8
beta,
8a
alpha,
8b alpha)-,
Guanidine, N-methyl-N’-nitro-N-
nitroso-
7439-92-1
301-04-2
0144
7446-27-7
U145
1335-32-6
0166
58-89-9
0129
Kepone
Lasiocarpine
143-50-0
0142
303-34-1
0143
108-31-6
123-33-1
109-77-3
148-82-3
7439-97-6
628-86-4
126-98-7
91-80-5
16752-77-5
72-43-5
74-83-9
74-87-3
79-22-i
71-55-6
56-49-5
101-14-4
74-95-3
75-09-2
78-93-3
1338-23-4
60-34-4
74-88-4
624-83-9
75-86-5
80-62-6
U147
U148
0149
0150
0151
P065
0152
0155
P066
0247
0029
U045
Ui56
0226
U157
U158
0068
0080
0159
0160
P068
0138
P064
P069
0162
MNNG
66-27-3
298-00-0
P071
56-04-2
50-07-7
0164
0010
70-25-7
0163
125—253
82
Mustard gas
Ethane,
1,1’-thiobis(2-chboro-
505-60-2
0165
Naphthalene
Same
91-20-3
0165
1,4-Naphthoquinone
1,4-Naphthalenedione
130-15-4
0166
atpha-Naphthytamine
1-Naphthalenamine
134-32-7
0167
beta-Naphthylamine
2-Naphthalenami ne
91-59-8
0168
atpha-Naphthy( thiourea
Thi ourea,
I -naphthalenyl
-
86-88-4
P072
Nicket
Same
7440-02-0
Nickel
conpounds,
N0.S.
Nickel
carbonyl
Nickel
carbonyt
Ni(C0)4,- (T-4)-
13463-39-3
P073
Nickel cyanide
Nickel cyanide Mi(CN)2
557-19-7
P074
Nicotine
Pyridine, 3-(l-methyl-2-
54-11-5
P075
pyrrolidinyl)-,
CS)-
Nicotine salts
P075
Nitric oxide
Nitrogen oxide NO
10102-43-9
P076
p-Nitroaniline
Benzenamine,
4-nitro-
100-01-6
P077
Nitrobenzene
Benzene, nitro-
98-95-3
P078
Nitrogen dioxide
Nitrogen oxide NO2
10102-44-0
P078
Nitrogen
mustard
Ethanarnine,
2-chloro-N-(2-
51-75-2
cliloroethyl)-N-methyl
-
Nitrogen
mustard, hydrochloride salt
Nitrogen mustard N-oxide
Ethanainine, 2-chboro-N-C2-chloro-
126-85-2
ethyl)-N-methyl-,
N-oxide
Nitrogen mustard, N-oxide,
hydrochloride
salt
Nitroglycerin
1,2,3-Propanetriol, trinitrate
55-63-0
P081
p-Nitrophenol
Phenol, 4-nitro-
10002-7
0170
2-Nitropropane
Propane, 2-nitro-
79-46-9
0171
Nitrosamines, N.OS.
35576-91-i
N-Nitrosodi-n-butybamine
1-Butanamine, N-butyt-N-nitroso-
924-16-3
0172
N-Nitrosodiethanolamine
Ethanol, 2,2’-(nitrosoimino)bis-
1116-54-7
U173
N-Nitrosodiethylamine
Ethanamine,
H-ethyl -N-nitroso-
55-18-5
U174
N-Nitrosodimethylamine
Methanamine,
N-rnethyl-N-nitroso-
62-75-9
P082
N-Nitroso-Pl-ethylurea
Urea,
H-ethyl-N-nitroso-
759-73-9
U176
N-Nitrosomethylethylaniine
Ethanamine, N-methyl-N-nitroso-
10595-95-6
N-Nitroso-N-methyLurea
Urea,
N-methyl-N-nitroso-
684-93-5
0177
N-Nitroso-N-methylurethane
Carbonic acid, methylnitroso-, ethyl
615-53-2
0178
ester
H-Nitrosomethylvinylamine
Vinylamine, N-methyL-N-nitroso-
4549-40-0
P084
$-Nitrosomorpholine
Morphotine, 4-nitroso-
59-89-2
N-Nitrosonornicotine
Pyridine, 3-11-nitroso-2-
16543-55-8
pyrrolidinyl)-, (S)-
N-Nitrosopiperidine
Piperidine,
1-nitroso-
100-75-4
Ui79
N-Nitrosopyrrolidine
Pyrrolidirie,
1-nitroso-
930-55-2
0180
H-Nitrososarcosine
Glycine, N-methyl-N-nitroso-
13256-22-9
5-Nitro-o-toluidine
Benienamine, 2-methyl-5-nitro-
99-55-8
0181
Octamethylpyrophosphoramide
Diphosphorarnide, octamethyl-
152-16-9
P085
Osmiun
tetroxide
Osmiun
oxide
OSOL,
(T-4)
20816-12-0
P087
ParaLdehyde
1,3,5-Trioxane, 2,4,6-trimethyt-
123-63-7
0182
Parathion
Phosphorothioic acid, 0,0-diethyL 0-
56-38-2
P089
(4-nitrophenyt) ester
Pentachlorobenzene
Benzene,
pentachloro-
608-93-5
0183
Pentachlorodibenzo-p-dioxins
PentachI orodibenzofurans
Pentachloroethane
Ethane,
pentachboro-
76-01-7
U184
Pentachloronitrobenzene
(PCNB)
Benzene,
pentachloronitro-
82-68-8
0185
Pentachborophenot
Phenol,
pentachboro-
87-86-5
•
See
F027
Phenacetin
Acetainide, N-(4-ethoxyphenyl)-
62-44-2
0187
Phenol
Same
108-95-2
0188
Phenylenedi amine
Benzenedi amine
25265-76-3
Phenylmercury
acetate
Mercury,
(acetato-0)phenyl-
62-38-4
P092
Phenylthiourea
Thiourea,
phenyl-
103-85-5
P093
Phosgene
Carbonic
dichloride
75-44-5
P095
125—254
83
Phosphine
Phorate
Phthalic acid esters, N.OS
Phthalic anhydride
2-Picolme
Polychlorinated biphenyls, N0.S.
Potassiun cyanide
Potassiun silver cyanide
Pronamide
1,3-Propane
syltone
n-Propylamine
Propargyl
alcohol
Propylene dichLoride
I ,2-Propylenimi ne
Propylthiouraci I
Pyridine
Reserpine
Resorcinot
Saccharin
Saccharin saLts
SafroLe
Sd
eni us
Seleniun cospounds, N.OS.
Seleniun dioxide
Seleniun sulfide
Setenourea
Silver
Silver
conçounds,
N.0.S~
Silver
cyanide
Silvex (2,4,5-TP)
Sodit.sn
cyanide
Streptozotocin
Strychnine
Strychnine salts
TCDD
I ,2,4,5-Tetrachlorobenzene
Tetrachlorodibenzo-p-dioxins
Tetrachlorodibenzofurans
Tetrachloroethane, N.0.S.
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
2,3,4,6-Tetrachlorophenol
Tetraethyldithiopyrophosphate
Tetraethyl
lead
Tetraethylpyrophosphate
Tetrani
tromethane
That
hun
Thalliun
conpounds
ThaLhic
oxide
Same
Argentate(i-),
bis(cyano-C)-,
potassiun)
Benzamide, 3,5-dichloro-N-(1,1-di-
methyL-2-propynyL)-
1,2-Oxathiolane, 2,2-dioxide
1
-Propariamine
2-Propyn-i-ot
Propane,
i,2-dichloro-
Aziridine, 2-methyl-
4(1H)-Pyrimidinone,
2,3-dihydro-6-
propyl-2-thioxo-
Same
Yohithan-16-carboxytic acid,
11,17-
dimethoxy-i8- (3,4,5-trimethoxy-
benzoyL)oxy-,
methyl ester,
(3
beta,
16
beta,
17 alpha,
18
beta,
20
alpha)-,
I ,3-Benzenediol
1,2-Benzisothiazol-3(2H)-one,
1,1-
dioxide
i,3-Senzodioxole, 5-C2-propenyl)-
Same
Selenious acid
Seleniun sulfide SeS2
Same
Same
Silver cyanide A9CN
Propanoic acid, 2-12,4,5-
tn
chlorophenoxy)
-
Sodiun
cyanide NaCN
D-Glucose,
2-deoxy-2- ((methyl-
nitrosoamino)carbonylamino
-
Strychnidin-10-one
Dibenzob,e
(1,4dioxin,
2,3,7,8-
tetrachboro-
Benzene,
i,2,4,5-tetrachloro-
Ethane, tetrachloro-, NOS.
Ethane, 1,i,1,2-tetrachtoro-
Ethane, 1,1,2,2-tetrachloro-
Ethene, tetrachloro-
Phenol, 2,3,4,6-tetrachloro-
Thiodiphosphoric acid,
tetraethyl
ester
Plu~ane,tetraethyt-
Diphosphoric acid,
tetraethyl ester
Methane, tetranitro-
Same
ThaLliun oxide 11203
7803-51-2
P096
298-02-2
P094
108-46-3
81-07-2
94-59-7
7782-49-2
7783-00-8
7488-56-4
630-10-4
7440- 22-4
143-33-9
P106
18883-66-4
0206
57-24-9
P108
P108
1746-01-6
95-94-3
U207
25322-20-7
630-20-6
79-34-5
127-18-4
58-90-2
3689-24-5
78-00-2
107-49-3
509-14-8
7440-28-0
1316-32-5
P113
Same
Phosphorodithioic acid, 0,0-diethyl
5- ((ethylthio)methyl
ester
1,3-Isobenzof
urandi
one
Pynidine, 2-methyl-
85-44-9
109-06-8
151-50-8
506-61-6
0190
U191
P098
P099
23950-58-5
0192
1120-71-4
107-10-8
107- 19-7
78-87-5
75-55-8
51- 52-5
110-86-i
50-55-5
11193
Ui94
P102
U083
P067
U196
0200
0201
U202
U202
U203
0204
U205
P103
P104
See FG27
506-64-9
93-72-1
11208
0209
0210
See F027
P109
P110
Pill
P112
125—255
Thalliun
(1)
acetate
Thalhiun
(I)
carbonate
Thattiun
(I) chloride
Thalliun
(1)
nitrate
ThaItiun
selenite
Thalliun
(1)
sulfate
Thioacetarnide
Thiofanox
Thiomethanol
Th i
ophenot
Thiosemicarbazide
Thiourea
Thiram
Toluene
Tol uenedi
amine
Totuene-2,4-diamine
Toluene-2,6-diamine
Toluene-3,4-diamino
Totuene diisocyanate
o-Toluidine
o-Toluidine hydrochloride
p-To Iuidine
Toxaphene
1 ,2,4-TrichLorobenzene
1,1 ,2-Tnichloroethane
Tnichhoroethylene
Tnichhoromethanethi oh
Inchloromonofluoromethane
2,4,5-Trichlorophenot
2,4,6-Tn chlorophenol
2,6,5-1
Tnichloropropane, N_a_S.
1, 2,3-Tn chLoroproparie
0,0,0-Tr iethylphosphoroth ioate
1 ,3,5-Trinitnobenzene
Tnis(l-aziridinyl)phosphine sulfide
TnisC2,3-dibromopropyt) phosphate
Trypan
blue
Uracil mustard
Vanadiun
pentoxi
de
VinyL chloride
Warfanin
Wanfarin
Warfarin salts, when present at
concentrations less than 0.3.
Warfanin salts, when present at
concentrations greater than 0.3.
Zinc cyanide
Acetic acid, thaLhiun
(1+) saLt
Carbonic acid, dithalhiun
(1+) salt
Thalliun chloride lId
Nitric acid, thalhiun (1+) salt
Setenious acid, dithalliun (1+) salt
Sulfuric acid, dithalhiun
(1+) salt
Ethanethioamide
2-Butanone, 3,3-dimethyl-1-(methyh-
thio)-, 0-((methylamino)carbonyl-
oxime
Methanethiol
Benzenethiol
Hydrazinecarbothioamide
Same
Thioperoxydicarbonic diamide
((H2H)C(S)~S2, tetramethyl-
Benzene, methyl-
Benzenedi amino,
ar-methyl
-
i,3-Benzenediamine, 4-methyl-
1,3-Benzenediamine, 2-methyl-
1 ,2-Benzenediamine, 4-methyl-
Benzene,
1,3-diisocyanatomethyt-
Benzenamine, 2-methyl-
Benzeneamine, 2-methyl-, hydro-
chloride
Benzenamine,
4-methyL-
Same
Benzene,
i,2,4-tnichtoro-
Ethane,
1,i,2-tnichhoro-
Ethene, trichloro-
Methanethiol, tnichioro-
Methane,
tnichtorofluoro-
Phenol,
2,4,5-trichloro-
Phenol,
2,4,6-tnichloro-
Acetic acid, (2,4,5-trichLoro-
phenoxy)-
Propane,
1,2,3-trichioro-
Phosphorothioic acid, 0,0,0-tniethyl
ester
Benzene,
1,3,5-trinitro-
Aziridine,
1,l’,i”-phosphinothioyL-
idynetnis-
1-Propanol,
2,3-dibromo-,
phosphate
(3:1)
2,7-HaphthaLenedisulfonic acid,
3,3’
-
((3,3’-dimethyL
(1,1 ‘-biphenyl
-
4,4’-diyl)bis(azo)bis(5-amino-4-
hydroxy-,
tetrasodiun salt
2,4-(1H,3H)-Pynimidinedione,
5-
bis(2-chloroethyl)amino-
Vanadiun oxide V205
Ethene, chhoro-
2H-1-Benzopyran-2-one, 4-hydroxy-3-
(3-oxo-1-phenylbutyt)-, when present
at concentrations less than 03L
2H-1-Benzopyran-2-one, 4-hydroxy-3-
(3-oxo-i-phenylbutyt)-, when present
at concentrations greater than 0.3.
108-88-3
25376-45-8
95-80-7
823-60-5
496-72-0
26471-62-5
95-53-4
636-21-5
106-49-0
8001-35-2
120-82-1
79-00-5
79-01-6
75-70-7
75-69-4
95-95-4
88-06-2
93-76-5
25735-29-9
96-18-4
126-68-i
99-35-4
U234
52-24-4
126-72-7
0235
72-57-1
U236
84
563-68-8
6533-73-9
7791-12-0
10102-45-1
12039-52-0
7446-18-6
62-55-5
39196-18-4
74-93-1
108-98-5
79-19-6
62-56-6
137-26-8
U214
U21 5
U216
0217
P114
P115
U218
P045
Ui53
P014
P116
P219
0244
0220
U221
U223
U328
1)222
U353
P123
11227
U228
P118
U121
See F027
See F027
See F027
66-75-1
0237
1314-62-1
75-01-4
81-81-2
P120
U043
0248
Zinc cyanide ZnCCH)2
81-81-2
P001
U248
POOl
557-21-1
P121
125—256
85
•
Zinc
phosphide
Zinc
phosphide
P2Zn3,
when present
1314-84-7
P122
at
concentrations
greater
than
10.
Zinc
phosphide
Zinc
phosphide
P2Zn~,
when present
1314-84-7
U249
at concentrations o~10
or less.
(Source:
Amended
at 15 III. Reg.
,
effective
)
125—257
86
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER
C:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 722
STANDARDS
APPLICABLE
TO GENERATORS OF HAZARDOUS WASTE
SUBPART
A:
GENERAL
Section
722.110
722.111
722.112
Section
722.120
722.121
722.122
722.123
Section
722.130
722.131
722. 132
722.133
722.134
Section
722
.
140
722.141
722.142
722.143
722.144
Section
722.150
722.151
722.152
722. 153
722.154
722.155
722
.
156
722. 157
Section
722.160
Purpose,
Scope and Applicability
Hazardous Waste Determination
USEPA Identification Numbers
SUBPART B:
THE MANIFEST
General Requirements
Acquisition of Manifests
Number of Copies
Use of the Manifest
SUBPART C:
PRE-TRANSPORT REQUIREMENTS
Packaging
Labeling
Marking
Placarding
Accumulation Time
SUBPART D:
RECORDKEEPING
AND
REPORTING
Recordkeeping
Annual Reporting
Exception Reporting
Additional Reporting
Special Requirements for Generators of between 100 and
1000 kilograms per month
SUBPART
E:
EXPORTS OF HAZARDOUS WASTE
Applicability
Definitions
General Requirements
Notification of Intent to Export
Special Manifest Requirements
Exception Report
Annual Reports
Recordkeeping
SUBPART
F:
IMPORTS OF HAZARDOUS WASTE
Imports of Hazardous Waste
125—258
87
SUBPART G:
FARMERS
Section
722.170
Farmers
Appendix A
Hazardous Waste Manifest
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act (Ill. Rev.
Stat.
1989,
ch.
111½, pars.
1022.4 and 1027).
SOURCE:
Adopted in R81-22,
43 PCB 427,
at 5
Ill.
Reg. 9781,
effective as noted in 35 Ill. Adm. Code 700.106; amended and
codified in R81—22, 45 PCB 317,
at
6 Ill.
Reg.
4828, effective as
noted in 35 Ill. Adm. Code 700.106; amended in R82—18,
51
PCB 31,
at
7. Ill. Reg.
2518, effective February 22,
1983; amended in R84—
9 at 9 Ill. Reg.
11950, effective July 24,
1985; amended in R85-
22 at 10
Ill.
Reg. 1131, effective January 2,
1986; amended in
R86-1 at 10 Ill.
Reg.
14112, effective August 12,
1986; amended
in R86—l9 at
10 Ill.
Reg.
20709, effective December 2,
1986;
amended in R86-46 at
11
Ill. Reg.
13555, effective August
4,
1987; amended in R87-5 at
1.
Ill. Reg.
19392, effective November
12,
1987; amended in R87-39 at 12 Ill.
Reg.
13129,
effective July
29,
1988; amended in R88-16 at 13
Ill. Reg.
452, effective
December 27,
1988;
amended in R89-1 at 13 Ill.
Reg.
18523,
effective November 13,
1989; amended in R90—l0 at 14
Ill.
Reg.
16653, effective September 25,
1990; amended in R90—ll at 15
Ill.
Reg.
9644, effective June 17,
1991; amended in R91—l at 15
Ill.
Reg.
,
effective
SUBPART C:
PRE-TRANSPORT REQUIREMENTS
Section 722.134
Accumulation Time
a)
Except as provided in subsections
(d),
(e) or
(f), a
generator is exemPt from all the reciuireTnents
in
35
Ill. Adm.
Code 725.Subparts G and H, except for
35 Ill.
Adm. Code 725.211 and 725.214 and may accumulate
hazardous waste on—site for 90 days or less without a
permit or without having interim status~provided that:
1)
The waste is placed~.
~j
~in containers and the generator complies
with 35
Ill. Adm. Code 725.Subpart
1j.
or
~j
Ithe waste i~placed in tanks and the
generator complies with 35
Ill.
Adm. Code
725.Subpart J except 35 Ill. Adm. Code
725.297(c)
and 725.300--;
or
~j
On drip pads and the generator complies with
125—259
88
35 Ill.
Adm. Code 725.Subpart W and maintains
the following records at the facility:
jj.
A description of the procedures that
will be followed to ensure that all
wastes are removed from the drip ~ad and
associated collection system at least
once every 90 days: and
iil
Documentation of each waste removal,
including the quantity of waste removed
from the drip ~ad and the sump or
collection system and the date and time
of removal.
In addition, 3uch a
gei’terator
is
exempt from all the
requirements in
35
Iii.
Adm. Code
725.Cubparts G and H, except for
35
Ill.
Adm. Code 725.211 Qnd 725.214;
BOARD
NOTE:
The
“in
addition”
hr~~ri
paragraph is in the introduction to
subsection
(a).
2)
The date upon which each period of accumulation
begins is clearly marked and visible for
inspection on each container;
3)
While being accumulated on—site, each container
and tank is labeled or marked clearly with the
words,
“Hazardous Waste”, and
4)
The generator complies with the requirements for
owners or operators in 35
Ill. Adm. Code
725.Subparts C and D, with 35 Ill. Adm. Code
725.116 and 728.107(a)
(4).
b)
A generator who accumulates hazardous waste for more
than 90 days is an operator of a storage facility and
is subject to the requirements of 35 Ill.
Adm. Code 724
and 725 and the permit requirements of 35
Iii.
Adm.
Code 702, 703 and 705 unless the generator has been
granted an extension of the 90-day period.
If
hazardous wastes must remain on—site for longer than 90
days due to unforeseen,
temporary, and uncontrollable
circumstances, the generator may seek an extension of
up to 30 days by means of a variance or provisional
variance, pursuant to Section 37 of the Environmental
Protection Act.
C)
Accumulation near point of generation.
1)
A generator may accumulate as much as 55 gallons
125—260
89
of hazardous waste or one quart of acutely
hazardous waste, listed in 35 Ill.
Adm. Code
721.133(e)
in containers at or near any point of
generation where wastes initially accumulate,
which is under the control of the operator of the
process generating the waste, without a permit or
interim status and without complying with
paragraph
(a) provided the generator:
A)
Complies with 35 Ill.
Adm. Code 725.271,
725.272 and 725.273(a); and
B)
marks the generator’s containers either with
the words “Hazardous Waste” or with other
words that identify the contents of the
containers.
2)
A generator who accumulates either hazardous waste
or acutely hazardous waste listed in 35
Ill. Adm.
Code 721.133(e)
in excess of the amounts listed in
subsection
(c) (1)
at or near any point of
generation must,
with respect to that amount of
excess waste, comply within three days with
subsection
(a) or other applicable provisions of
this chapter.
During the three day period the
generator must continue to comply with subsection
(c) (1).
The generator must mark the container
holding the excess accumulation of hazardous waste
with the date the excess amount began
accumulating.
d)
A generator who generates greater than 100 kilograms
but less than 1000 kilograms of hazardous waste in a
calendar month may accumulate hazardous waste on—site
for 180 days or less without a permit or without having
interim status provided that:
1)
The quantity of waste accumulated on—site never
exceeds 6000 kilograms;
2)
The generator complies with the requirements of 35
Ill. Adm. Code 725.Subpart
I, except the generator
need not comply with 35 Ill.
Adm. Code 725.276;
3)
The generator complies with the requirements of 35
Ill. Adm. Code 725.301;
4)
The generator complies with the requirements of
subsections
(a) (2) and
(a) (3) and the requirements
of
35
Ill. Adm. Code 725.Subpart C; and
5)
The generator complies with the following
125—261
90
requirements:
A)
At all times there must be at least one
employee either on the premises or on call
(i.e., available to respond to an emergency
by reaching the facility within a.short
period of time) with the responsibility for
coordinating all emergency response measures
specified in subsection
(d) (4) (D).
The
employee is the emergency coordinator.
B)
The generator shall post the following
information next to the telephone:
i)
The name and telephone number of the
emergency coordinator:
ii)
Location of fire extinguishers and spill
control material, and if present, fire
alarm:
and
iii) The telephone number of the fire
department, unless the facility has a
direct alarm.
C)
The generator shall ensure that all employees
are thoroughly familiar with proper waste
handling and emergency procedures,
relevant
to their responsibilities during normal
facility operations and emergencies:
D)
The emergency coordinator or designee shall
respond to any emergencies that. arise.
The
applicable responses are as follows:
i)
In the event of a fire,
call the fire
department or attempt to extinguish it
using a fire extinguisher:
ii)
In the event of a spill, contain the
flow of hazardOus waste to the extent
possible, and as soon as is practicable,
clean up the hazardous waste and any
contaminated materials or soil:
iii)
In the event of a fire,
explosion or
other release which could threaten human
health outside the facility or when the
generator has knowledge that a spill has
reached surface water, the generator
shall immediately notify the National
Response Center
(using its 24-hour toll
125—262
91
free number 800/424-8802).
The report
must include the following information:
the name, address and USEPA
identification number
(35 Ill. Adm. Code
722.112)
of the generator;
date, time
and type of jncident (e.g., spill or
fire); quantity and type of hazardous
waste involved in the incident; extent
of injuries, if any; and, estimated
quantity and disposition of recoverable
materials,
if any.
e)
A generator who generates greater than 100 kilograms
but less than 1000 kilograms of hazardous waste in a
calendar month and who must transport the waste,
or
offer the waste for transportation,
over a distance of
200 miles or more for off—site treatment,
storage or
disposal may accumulate hazardous waste on—site for 270
days or less without a permit or without having interim
status provided that the generator complies with the
requirements of subsection
(d).
f)
A generator who generates greater than 100 kilograms
but less than 1000 kilograms of hazardous waste in a
calendar month and who accumulates hazardous waste in
quantities exceeding 6000 kg or accumulates hazardous
waste for more than 180 days
(or for more than 270 days
if the generator must transport the waste,
or offer the
waste for transportation, over a distance of 200 miles
or more)
is an operator of
a storage facility and is
subject to the requirements of 35
Ill. Adm. Code 724
and 725 and the permit requirements of 35 Ill.
Adm.
Code 703 unless the generator has been granted an
extension to the 180-day (or 270-day if applicable)
period.
If hazardous wastes must remain on—site for
longer than 180 days
(or 270 days if applicable)
due to
unforeseen, temporary and uncontrollable circumstances,
the generator may seek an extension of up to 30 days by
means of variance or provisional variance pursuant to
Section 37 of the Environmental Protection Act.
(Source:
Amended at 15 Ill. Reg.
,
effective
)
125—263
92
TITLE 35:
ENVIRONMENTAL PROTECTION
SUBTITLE G:
WASTE DISPOSAL
CHAPTER I:
POLLUTION CONTROL BOARD
SUBCHAPTER
c:
HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 724
STANDARDS FOR OWNERS
AND
OPERATORS OF HAZARDOUS WASTE
TREATMENT,
STORAGE
AND
DISPOSAL FACILITIES
SUBPART A:
GENERAL PROVISIONS
Section
724.101
Purpose, Scope and Applicability
724.103
Relationship to Interim Status Standards
SUBPART B:
GENERAL FACILITY STANDARDS
Section
724.110
Applicability
724.111
Identification Number
724.112
Required Notices
724.113
General Waste Analysis
724.114
Security
724.115
General Inspection Requirements
724.116
Personnel Training
724.117
General Requirements for Ignitable, Reactive or
Incompatible Wastes
724.118
Location Standards
SUBPART C:
PREPAREDNESS AND PREVENTION
Section
724.130
Applicability
724.131
Design and Operation of Facility
724.132
Required Equipment
724.133
Testing and Maintenance of Equipment
724.134
Access to Communications or Alarm System
724.135
Required Aisle Space
724.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN
AND
EMERGENCY PROCEDURES
Section
724 .150
Applicability
724.151
Purpose and Implementation of Contingency Plan
724.152
Content of Contingency Plan
724.153
Copies of Contingency Plan,
724.154
Amendment of Contingency Plan
724.155
Emergency Coordinator
724.156
Emergency Procedures
SUBPART
E:
MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section
724.170
Applicability
724.171
Use of Manifest System
724.172
Manifest Discrepancies
125—264
93
724.173
Operating Record
724.174
Availability, Retention and Disposition of Records
724.175
Annual Report
724.176
Unmanifested Waste Report
724.177
Additional Reports
SUBPART F:
RELEASES FROM SOLID WASTE MANAGEMENT UNITS
App. icabi1ity
Required Programs
Groundwater Protection Standard
Hazardous Constituents
Concentration Limits
Point of Compliance
Compliance Period
General Groundwater Monitoring Requirements
Detection Monitoring Program
Compliance Monitoring Program
Corrective Action Program
Corrective Action for Solid Waste Management Units
SUBPART G:
CLOSURE AND POST-CLOSURE
Applicability
Closure Performance Standard
Closure Plan; Amendment of Plan
Closure; Time Allowed For Closure
Disposal or Decontamination of Equipment,
Structures
and Soils
Certification of Closure
Survey Plat
Post—closure Care and Use of Property
Post—closure Plan; Amendment of Plan
Post—closure Notices
Certification of Completion of Post-closure Care
SUBPART H:
FINANCIAL REQUIREMENTS
Section
724.240
Applicability
724.241
Definitions of Terms As Used In This Subpart
724.242
Cost Estimate for Closure
724.243
Financial Assurance for Closure
724.244
Cost Estimate for Post-closure Care
724.245
Financial Assurance for Post—closure Care
724.246
Use of a Mechanism for Financial Assurance of Both
Closure and Post—closure Care
724.247
Liability Requirements
724.248
Incapacity of Owners or Operators, Guarantors or
Financial Institutions
724.251
Wording of the Instruments
Section
724. 190
724.191
724.192
724.193
724.194
724.195
724.196
724.197
724.198
724
.
199
724.200
724.201
Section
724.210
724.211
724.212
724.213
724.214
724.215
724.216
724.217
724.218
724.219
724.220
125—265
94
SUBPART I:
USE AND MANAGEMENT OF CONTAINERS
Applicability
Condition of Containers
Compatibility of Waste With Container
Management of Containers
Inspections
Containment
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Closure
SUBPART
J:
TANK SYSTEMS
Section
724.290
724.291
724.292
724.293
724.294
724 .295
724.296
‘724.297
724.298
724 .299
724.300
Section
724.320
724.321
724.322
724.326
724.327
724.328
724.329
724. 330
724.331
Applicability
Assessment
of
Existing
Tank
System’s
Integrity
Design and Installation of New Tank Systems or
Components
Containment and Detection of Releases
General Operating Requirements
Inspections
Response to Leaks or Spills and Disposition of Leaking
or unfit—for—use Tank Systems
Closure and Post—Closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Special Requirements for Hazardous Wastes F020,
F021,
F022,
F023,
F026 and F027
SUBPART K:
SURFACE IMPOUNDMENTS
Applicability
Design and Operating Requirements
Double—lined Surface Impoundments:
Exemption from
Subpart
F: Ground—water Protection Requirements
(Repealed)
Monitoring and Inspection
Emergency Repairs; Contingency Plans
-
Closure and Post—closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for• Incompatible Wastes
Special Requirements for Hazardous Wastes F020,
F021,
F022,
F023,
F026 and F027
SUBPART L:
WASTE PILES
Section
724.350
724.351
Design and Operating Requirements
724.352
Double-lined Piles:
Exemption from Subpart F:
water Protection Requirements
(Repealed)
724.353
Inspection of Liners:
Exemption from Subpart
F:
Ground—water Protection Requirements
(Repealed)
Section
724.270
724.271
724.272
724.273
724.274
724.275
724.276
724.277
724.278
Applicability
Ground-
125—266
95
724.354
724.356
724.357
724.358
724.359
Section
724 .370
724.371
724 .372
724.373
724.376
724.378
724.379
724.380
724.381
724.382
724.383
Section
724.400
724 .401
724 .402
Monitoring and Inspection
Special Requirements, for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Closure and Post—closure Care
Special Requirements for Hazardous Wastes F020, F021,
F022,
F023, F026 and F027
SUBPART
N:
LAND
TREATMENT
Applicability
Treatment Program
Treatment Demonstration
Design and Operating Requirements
Food—chain Crops
Unsaturated Zone Monitoring
Recordkeeping
Closure and Post-closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Special Requirements for Hazardous Wastes F020,
F021,
F022, F023, F026 and F027
SUBPART
N:
LANDFILLS
Applicability
Design and Operating Requirements
Double-lined Landfills:
Exemption from Subpart
F:
Ground—water Protection Requirements
(Repealed)
Monitoring and Inspection
Surveying and Recordkeeping
Closure and Post—closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Special Requirements for Bulk and Containerized Liquids
Special Requirements for Containers
Disposal of Small Containers of Hazardous Waste
in
Overpacked Drums
(Lab Packs)
724.417
Special Requirements for Hazardous Wastes F020, F021,
F022,
F023, F026 and F027
SUBPART 0:
INCINERATORS
Applicability
Waste Analysis
Principal Organic Hazardous Constituents
(POHCs)
Performance Standards
Hazardous Waste Incinerator Permits
Operating Requirements
Monitoring and Inspections
Closure
724.403
724.409
724.410
724.412
724.413
724.414
724.415
724.416
Section
724.440
724.441
724.442
724 .443
724 .444
724 .445
724 .447
724.451
125—267
96
SUBPART W:
DRIP PADS
Applicability
_______
Assessment of existing drip pad integrity
________
Design and operating requirements
Inspections
________
Closure
_______
Design and installation of new drip pads
SUBPART X:
MISCELLANEOUS UNITS
Section
724.701
Applicability
724.701
Environmental Performance Standards
724.702
Monitoring, Analysis, Inspection, Response, Reporti.ng
and Corrective Action
724.703
Post-closure Care
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS VENTS
Applicability
Definitions
Standards:
Process Vents
Standards:
Closed—vent Systems and Control Devices
Test methods and procedures
Recordkeeping requirements
Reporting Rrequirements
SUBPART BB:
AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Applicability
Definitions
Standards:
Standards:
Standards:
Service
Standards:
Sampling Connecting Systems
Standards:
Open—ended Valves or Lines
Standards:
Valves in Gas/Vapor or Light Liquid Service
Standards:
Pumps, Valves, Pressure Relief Devices and
Other Connectors
Standards:
Delay of Repair
Standards:
Closed—vent Systems and Control Devices
Alternative Percentage Standard for Valves
Skip Period Alternative for Valves
Test Methods and Procedures
Recordkeeping Requirements
Reporting Requirements
Appendix A
Recordkeeping Instructions
Appendix B
EPA Report Form and Instructions
(Repealed)
Appendix D
Cochran’s Approximation to the Behrens-Fisher
Student’s T-Test
Section
724.670
724.671
724. 672
724. 673
724.674
724.675
Section
724.930
724.931
724.932
724.933
724.934
724.935
724.936
Section
724.950
724.951
724.952
724.953
724
.
954
724 .955
724.956
724.957
724
.
958
724.959
724.960
724.961
724.962
724.963
724.964
724.965
Pumps in Light Liquid Service
Compressors
Pressure Relief Devices in Gas/Vapor
125—268
97
Appendix E
Examples of Potentially Incompatible Waste
Appendix I
Groundwater Monitoring List
AUTHORITY:•
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill.
Rev. Stat.
1989,
ch.
111½, pars.
1022.4 and 1027).
‘SOURCE:
Adopted in R82—l9,
53 PCB 131, at
7 Ill.
Reg.
14059,
effective October 12,
1983; amended in R84-9 at
9
Ill. Reg.
11964, effective July 24,
1985;
amended in R85-22 at 10 Ill. Reg.
1136, eftective January
2,
1986; amended in R86—1 at 10
Ill. Reg.
14119, effective August 12,
1986; amended in R86—28 at 11 Ill.
Reg.
6138, effective March 24,
1987; amended in R86—28 at 11
Ill.
Reg.
8684, effective April 21,
1987; amended
in. R86—46 at 11 Ill.
Reg.
13577, effective August
4,
1987; amended in R87—5 at 11
Ill.
Reg.
19397, effective November 12,
1987; amended in R87-39 at
12
Ill.
Reg.
13135, effective July 29,
1988; amended in R88—l6 at 13
Ill. Reg. 458, effective December 28,
1988; amended in R89—l at
13
Ill. Reg.
18527, effective November 13,
1989; amended in R90-
2 at 14 Ill.
Reg.
14511,
effective August 22,
1990; amended in
R90—10 at
14
Ill. Reg.
16658, effective September 25,
1990;
amended in R90—11 at 15
Ill.
Reg. 9654, effective June 17,
1991;
amended in R91—1 at 15
Ill.
Reg.
,
effective
SUBPART J:
TANK SYSTEMS
Section 724.290
Applicability
The requirements of this Subpart apply to owners and operators of
facilities that use tank systems for treating or storing ~
treating hazardous waste,
except as otherwise provided in
subsections (a)~—e~(b)
or
(c)
or in Section 724.101.
a)
Tank systems that are used to store or treat hazardous
waste which contains no free liquids and are situated
inside a building with an impermeable floor are
exempted from the requirements in Section 724.293.
To
demonstrate the absence or presence of free liquids in
the stored or treated waste, EPA Method 9095
(Paint
Filter Liquids Test) as described in “Test Methods for
Evaluating Solid Wastes Physical/Chemical Methods “EPA
Publication No.
SW-846), incorporated by reference in
35
Ill. Adm. Code 720.111, must be used.
b)
Tank systems,
including sumps,
as defined in 35 Ill.
Adin. Code 720.110, that serve as part of a secondary
containment system to collect or contain releases of
hazardous wastes are exempted from the requirements in
Section 724.293 (a)
-
~j
Tanks.
sumps and other such collection devices or
125—269
98
systems used in coniunction with drip pads,
as defined
in 35
Ill. Adm. Code 720.110 and regulated under
Subpart W, must meet the requirements of this Subpart.
(Source:
Amended at
15 Ill.
Reg.
,
effective
)
SUBPART W:
DRIP PADS
Section 724.670
Applicability
~j
The requirements of this Subpart apply to owners and
operators of facilities that use new or existing drip
p~dsto convey treated wood drippage, precipitation or
surface water run—on to an associated collection
system.
fl.
“Existing drip pads”
are:
~j
Those constructed before December 6, 1990
and
~j
Those for which the owner or operator has a
design and has entered into binding financial
or other agreements for construction prior to
December 6,
1990.
~j
All other drip pads are “new drip pads”.
~j
The owner or operator of any drip pad that is inside or
under a structure that provides protection from
precipitation so that neither run—off nor run—on is
generated is not sublect to regulation under Section
724.673(e)
or
(f).
(Source:
Added at 15
Ill. Reg.
,
effective
)
Section 724.671
Assessment of existing drip pad integrity
flj..
For each existing drip pad, the owner or operator shall
evaluate the drip pad and determine that it meets all
of the requirements of this Subpart, except the
requirements for liners and leak detection systems of
Section 724.673(b).
No later than June
6,
1991, the
owner or operator shall obtain and keep on file at the
facility a written assessment of the drip pad, reviewed
and certified by an independent, qualified registered
professional engineer that attests to the results of
the evaluation.
The assessment must be reviewed,
updated and re-certified annually until all upgrades,
repairs or modifications necessary to achieve
125—270
99
compliance with all of the standards of Section 724.673
are complete.
The evaluation must document the extent
to which the drip Pad meets each of the design and
operating standards of Section 724.673,
except the
standards for liners and leak detection systems,
specified in Section’ 724.673(b), and must document the
aae of the drip ~ad to the extent possible, to document
compliance with subsection
(bY.
~
The owner or operator shall develop a written plan for
upgrading, repairing and modifying the drip pad to meet
the requirements of Section 724.673(b) and submit the
plan to the A~encvno later than
2 years before the
date that all repairs, upgrades and modifications will
be complete.
This written plan must describe all
changes to be made to the drip pad in sufficient detail
to document compliance with all the requirements of
Section 724.673
and must document the age of the drip
pad to the extent possible.
The Plan must be reviewed
and certified by an independent qualified, registered
professional engineer.
All upgrades, repairs and
modifications must be completed in accordance with the
following:
fl.
For existing drip pads of known and documentable
age, all upgrades, repairs and modifications must
be completed bY June 6,
1993,
or when the drip Pad
has reached 15 years of
age, whichever comes
later.
~j.. For existing drip Pads for which the a~ecannot be
documented,
by June 6~1999; but,
if the age of
the facility is greater than 7 years,
all
upgrades, repairs and modifications must be
completed by the time the facility reaches 15
years of age or by June 6.
1993, whichever comes
later.
~j.. The owner or operator may petition the Board for
an extension of the deadline in subsection
(b) (11
or
(2)
Al
The owner or operator shall file a petition
for a RCRA variance as specified in 35
Ill.
Adm. Code 104.
~j
The Board will arant the petition for
extension if
it finds that:
jL.
The drip pad meets all of the
requirements of Section 724.673,
except
those for liners and leak detection
125—2
7
1
100
systems specified in Section 724.673(b)
and
jjj
That it will continue to be protective
of human health and the environment.
~j
Uion completion of all upgrades, repairs and
modifications, the owner or operator shall submit to
the Agency, the as-built drawings for the drip pad,
to~etherwith a certification by an independent,
qualified, registered professional engineer attesting
that the drip ~ad conforms to the drawings.
~j
If the drip pad is found to be leaking or unfit for
use, the owner or operator shall comply with the
provisions of Section 724.673(m)
or close the drip pad
in accordance with Section 724.675.
(Source:
Added at 15
Ill. Reg.
,
effective
Section 724.672
Design and installation of new drip pads
Owners and operators of new drip pads shall ensure that the pads
are designed,
installed and operated in accordance with all of
the applicable requirements of Sections 724.673, 724.674 and
724. 675.
(Source:
Added at 15
Ill. Reg.
,
effective
Section 724.673
Design and operating requirements
Drip pads must:
fl
Not be constructed of earthen materials, wood or
asphalt,
unless the asphalt
is structurally
supported
21
Be sloped to free—drain to the associated
collection system treated wood drippage,
rain,
other waters,
or solutions of drippage and water
or other wastes
~j
Have a curb or berm around the perimeter
j).
Be impermeable, e.g.,
concrete pads must be
sealed,
coated or covered with an impermeable
material such that the entire surface where
drippage occurs or may run across is capable of
containing such drippage and mixtures of drippage
and precipitation, materials or other wastes while
125—272
101
being
routed
to
an
associated
collection
system
and
BOARD NOTE:
The requirement that new drip pads be
impermeable, e.g., that new drip pads be sealed,
coated or covered with an impermeable material,
is
administratively stayed.
The stay will remain in
effect until further administrative action is
taken.
~j
Be of sufficient structural strength and thickness
to prevent failure due to physical contact,
climatic conditions, the stress of installation
and the stress of daily operations,
e.g.,
variable
and moving loads such as vehicle traffic, movement
of wood.
etc.
BOARD NOTE:
In -iudging the structural integrity
requirement of this subsection,
the Aaency should
generally consider applicable standards
established by professional organizations
generally recognized by the industry,
including
ACI 318 or ASTM C94,
incorporated by reference in
35 Ill.
Adm. Code 720.111.
~j
A new drip pad or an existing drip pad, after the
deadline established in Section 724.671(b), must have:
jj
A synthetic liner installed below the drip pad
that is designed, constructed and installed to
prevent leakage from the drip ~ad into the
adiacent subsurface soil or groundwater or surface
water at any time during the active life
(including the closure period)
of the drip pad.
The liner must be constructed of materials that
will prevent waste from being absorbed into the
liner and to prevent releases into the adlacent
subsurface soil or groundwater or surface water
during the active life of the facility.
The liner
must be:
Al
Constructed of materials that have
appropriate chemical properties and
sufficient stren~thand thickness to prevent
failure due to pressure gradients (including
static head and external hydrogeologic
forces). physical contact with the waste or
drip pad leakage to which they are exposed,
climatic conditions,
the stress of
installation and the stress of daily
operation (including stresses from vehicular
traffic on the drip pad)
125—273
102
~l
Placed upon a foundation or base capable of
providing su~~ortto the- liner and resistance
to pressure gradients above and below the
liner to prevent failure of the liner due to
settlement, compression or uplift; and
Qj
Installed to cover all surrounding earth that
could come in contact with the waste or
leakage; and
21
A leakage detection system immediately above the
liner that is designed, constructed, maintained
and operated to detect leakage from the drip pad.
The leakage detection system must be:
Al
Constructed of materials that are:
jj.
Chemically resistant to the waste
managed in the drip pad and the leakage
that might be generated;
and
jJJ
Of sufficient strength and thickness to
prevent collapse under the pressures
exerted by overlaying materials and by
any equipment used at the drip pad; and
~j.
Designed and operated to function without
clogging through the scheduled closure of the
drip pad;
and
~
Designed so that it will detect the failure
of the drip pad or the presence• of a release
of hazardous waste or accumulated liquid at
the earliest practicable time.
çj
Drip pads must be maintained such that they remain free
of cracks, gaps,
corrosion or other deterioration that
could cause hazardous waste to be released from the
drip pad.
BOARD NOTE:
See subsection
(m)
for remedial action
required if deterioration or leakage is detected.
~j
The drip ~ad and associated collection system must be
designed and operated to convey, drain and collect
liquid resulting from drippage or precipitation in
order to prevent run—off.
~j
Unless the drip pad is protected by a structure, as
described in Section 724.670(b), the owner or operator
shall design, construct,
operate and maintain a run—on
125—27
4
103
control system capable of preventing flow onto the drip
pad during peak discharge from at least
a 24-hour, 25-
year storm, unless the system has sufficient excess
capacity to contain any run—on that might enter the
system.
.~j..
Unless the drip ~ad is protected by a structure or
cover, as described in Section 724.670(b).
the owner or
operator shall design,
construct, operate and maintain
a run—off mana~ementsystem to collect and control at
least the water volume resulting from a 24—hour,
25—
year storm.
g~
The drip pad must be evaluated to determine that it
meets the requirements of subsections
(a) through
(f).
The owner or operator shall obtain a statement from an
independent, qualified,
registered professional
engineer certifying that the drip pad design meets the
requirements of this Section.
hi
Drippage and accumulated precipitation must be removed
from the associated collection system as necessary to
prevent overflow onto the drip pad.
jj
The drip pad surface must be cleaned thoroughly at
least once every seven days such that accumulated
residues of hazardous waste or other materials are
removed, using an appropriate and effective cleaning
technique,
including but not limited to,
rinsing,
washing with detergents or other appropriate solvents,
or steam cleaning.
The owner or operator shall
document,
in the facility’s operating log, the date and
time of each cleaning and the cleaning procedure used.
jI
Drip pads must be operated and maintained in a manner
to minimize tracking of hazardous waste or hazardous
waste constituents off the drip pad as a result of
activities by personnel or equipment.
jçj
After being removed from the treatment vessel, treated
wood from pressure and non—pressure processes must be
held on the drip pad until drippage has ceased.
The
owner or operator shall maintain records sufficient to
document that all treated wood is held on the pad,
in
accordance with this Section,
following treatment.
IL
Collection and holding units associated with run-on and
run-off control systems must be emptied or otherwise
managed as soon as possible after storms to maintain
design capacity of the system.
~j
Throughout the active life of the drip pad and as
12
5—27 5
104
specified in the permit,
if the owner or operator
detects a condition that could lead to or has caused
a
release of hazardous waste,
the condition must be
repaired within a reasonably prompt period of time
following discovery,
in accordance with’the following
procedures:
fl
Upon detection of a condition that may have caused
or has caused a release of hazardous waste
(e.g.,
upon detection of leakage in the leak detection
system)., the owner or operator shall:
Al
Enter a record of the discovery in the
facility operating log
~j
Immediately remove from service the portion
of the drip pad affected by the condition
çj
Determine what steps must be taken to repair
the drip pad, clean up any leakage from below
the drip pad, and establish a schedule for
accomplishing the clean up and repairs
Qj
Within 24 hours after discovery of the
condition, notify the A~encvof the condition
and, within 10 working days,
provide written
notice to the Agency with a description of
the steps that will be taken to repair the
drip pad and clean up any leakage,
and the
schedule for accomplishing this work.
21
The. Agency shall:
review the information
submitted; make a determination regarding whether
the pad must be removed from service completely or
partially until repairs and clean up are complete;
and notify the owner or operator of the
determination and the underlying rationale in
writing.
fl
Upon completing all repairs and clean up. the
owner or operator shall notify the Agency in
writing and provide a certification, signed by an
independent, qualified,
registered professional
engineer, that the repairs and clean up have been
completed according to the written plan submitted
in accordance with subsection
(m) (1) (D).
ni
If a permit
is necessary, the Agency shall specify in
the permit all design and operating practices that are
necessary to ensure that the requirements of this
Section are satisfied.
125—276
105
~j.
The owner or operator shall maintain, as part of the
facility operating log, documentation of past’o~erating
and waste handling practices.
This must include
identification of preservative formulations used in the
past, a description of drippaqe management practices
and a description of treated wood storage and handling
practices.
(Source:
Added at 15 Ill.
Reg.
,
effective
)
Section 724.674
Inspections
~J..
During construction or installation, liners and cover
systems
(e.g..
membranes,
sheets or coatings) must be
inspected for uniformity, damage and imperfections
(e.g.. holes, cracks, thin spots or foreign materials).
Immediately after construction or installation, liners
must be inspected and certified as meeting the
requirements of Section 724.673 by an independent.
qualified,
registered professional engineer.
The
certification must be maintained at the facility as
part of the facility operating record.
After
installation liners and covers must be inspected to
ensure tight seams and loints and the absence of tears.
punctures or blisters.
hi
While a drip Pad is in operation,
it must be inspected
weekly and after storms to detect evidence of any of
the following:
fl
Deterioration, malfunctions or improper operation
of run—on and run—off control systems
21
The presence of leakage
in and proper functioning
of leak detection system.
fl
Deterioration or cracking of the drip Pad surface.
BOARD NOTE:
See Section 724.672(m)
for remedial
action required
if deterioration or leakage is
detected.
(Source:
Added at 15 Ill.
Reg.
,
effective
Section 724.675
Closure
~j
At closure, the owner or operator shall remove or
decontaminate all waste residues, contaminated
containment system components
(pad,
liners,
etc.).
contaminated subsoils, and structures and equipment
125—277
106
contaminated with waste and leakage, and manage them as
hazardous waste.
~j
If, after removing or decontaminating all residues and
making all reasonable efforts to effect removal or
decontamination of contaminated components,
subsoils.
structures and equipment as required in subsection
(a),
the owner or operator finds that not all contaminated
subsoils can be practically removed or decontaminated,
the operator shall close the unit and perform post—
closure_care in accordance with closure and post
closure care requirements that apply to landfills
(Section 724.410).
For permitted units, the
requirement to have a permit continues throughout the
post— closure period.
In addition. for the purposes of
closure. post closure and financial responsibility,
such a drip ~ad is then considered to be a landfill,
and the owner or operator shall meet all of the
requirements for landfills specified in Subparts G and
H.
~
Existing drip Pads without liners.
..j
The owner or operator of an existing drip pad that
does not comply with the liner requirements of
Section 724.673(b) (1)
shall:
Al
Include in the closure plan for the drip ~ad
under Section 724.212 both a plan for
complying with subsection
(a) and a
contingent plan for complying with subsection
(b)
in case not all contaminated subsoils can
be practicably removed at closure; and
~j
Prepare a contingent post—closure plan under
Section 724.218 for complying with subsection
(b)
in case not all contaminated subsoils can
be practicably removed at closure.
21
The cost estimates calculated under Sections
724.212 and 724.244 for closure and post closure
care of a drip ~ad sublect to this subsection must
include the cost of complying with the contingent
closure plan and the contingent post closure plan,
but are not required to include the cost of
expected closure under subsection
(a).
(Source:
Added at 15 Ill. Reg.
,
effective
125—27
8
107
TITLE
35:
ENVIRONMENTAL
PROTECTION
SUBTITLE
G:.
WASTE
DISPOSAL
CHAPTER I:
POLLUTION CONTROL
BOARD
SUBCHAPTER c:
HAZARDOUS
WASTE OPERATING REQUIREMENTS
PART 725
INTERIM STATUS STANDARDS FOR OWNERS
AND
OPERATORS OF HAZARDOUS
WASTE TREATMENT, STORAGE AND DISPOSAL FACILITIES
SUBPART A:
GENERAL PROVISIONS
Purpose, Scope and Applicability
Imminent Hazard Action
SUBPART
B:
GENERAL
FACILITY
STANDARDS
Applicability
USEPA
Identification
Number
Required Notices
General Waste Analysis
Security
General Inspection Requirements
Personnel Training
General Requirements for Ignitable, Reactive or
Incompatible Wastes
725.118
Location Standards
SUBPART
C:
PREPAREDNESS AND PREVENTION
Applicability
Maintenance and Operation of Facility
Required Equipment
Testing and Maintenance of Equipment
Access to Communications or Alarm System
Required Aisle Space
Arrangements with Local Authorities
SUBPART D:
CONTINGENCY
PLAN
AND EMERGENCY PROCEDURES
Section
725.150
725. 151
725.152
725.153
725.154
725.155
725.156
Applicability
Purpose and Implementation of Contingency Plan
Content of Contingency Plan
Copies of Contingency Plan
Amendment of Contingency Plan
Emergency Coordinator
Emergency Procedures
Applicability
Use
of
Manifest
System
Manifest
Discrepancies
Section
725.101
725.104
Section
725.110
725.111
725.112
725.113
725. 114
725.115
725.116
725. 117
Section
725. 130
725.131
725. 132
725. 133
725. 134
725. 135
725. 137
Section
725.170
725.171
725.172
SUBPART
E:
MANIFEST SYSTEM,
RECORDKEEPING
AND
REPORTING
125—279
108
725.173
725.174
725.175
725.176
725.177
Section
725.190
725.191
725.192
725.193
725.194
Section
725.210
725.211
725. 212
725.213
725.214
725.215
725.216
725.217
725. 218
725. 219
725.220
Operating Record
Availability, Retention and Disposition of Records
Annual Report
Unmanifested Waste Report
Additional Reports
SUBPART F:
GROUNDWATER MONITORING
App. icabi1ity
Groundwater Monitoring System
Sampling and Analysis
Preparation, Evaluation and Response
Recordkeeping and Reporting
SUBPART
G:
CLOSURE
AND
POST-CLOSURE
Applicability
Closure Performance Standard
Closure Plan; Amendment of Plan
Closure; Time Allowed for Closure
Disposal or Decontamination of Equipment,
Structures
and Soils
Certification of Closure
Survey Plat
Post—closure Care and Use of Property
Post—closure Plan; Amendment of Plan
Post—Closure Notices
Certification of Completion of Post-Closure Care
Section
725.240
725. 241
725. 242
725.243
725.244
725.245
SUBPART
H:
FINANCIAL
REQUIREMENTS
Applicability
Definitions of Terms as Used in this Subpart
Cost Estimate for Closure
Financial Assurance for Closure
Cost Estimate for Post—closure Care
Financial Assurance for Post—closure Monitoring and
Maintenance
725.246
Use of a Mechanism for Financial Assurance of Both
Closure and Post—closure Care
Liability Requirements
Incapacity of Owners or Operators, Guarantors or
Financial Institutions
725.251
Promulgation of Forms
(Repealed)
SUBPART I:
USE
AND
MANAGEMENT OF CONTAINERS
Applicability
Condition of Containers
Compatibility of Waste with Container
Management of Containers
725.247
725.248
Section
725.270
725.271
725. 272
725. 273
725.274
Inspections
125—280
109
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART J:
TANK SYSTEMS
Applicability
Assessment of Existing Tank System’s Integrity
Design and Installation of New Tank Systems or
Components
Containment and Detection of Releases
General Operating Requirements
Inspections
Response to leaks or spills and disposition of Tank
Systems
Closure and Post—Closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Waste Analysis and Trial Tests
Generators of 100 to 1000 kg/mo.
SUBPART
K:
SURFACE IMPOUNDMENTS
Applicability
Design Requirements
General Operating Requirements
Containment System
Waste Analysis and Trial Tests
Inspections
Closure and Post—Closure Care
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART L:
WASTE PILES
App?icabi1ity
Protection from Wind
Waste Analysis
Containment
Design Requirements
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Closure and Post—Closure Care
SUBPART N:
LAND
TREATMENT
Applicability
General Operating Requirements
Waste Analysis
Food Chain Crops
Unsaturated Zone (Zone of Aeration) Monitoring
Recordkeeping
Closure and Post—closure
725.276
725.277
Section
725.290
725.291
725.292
725.293
725.294
725.295
725.296
725.297
725.298
725.299
725.300
725.30.
Section
725.320
725.321
725.322
725.323
725.325
725.326
725.328
725. 329
725. 330
Section
725.350
725.351
725. 352
725. 353
725. 354
725.356
725. 357
725.358
Section
725.370
725.372
725. 373
725.376
725.378
725. 379
725.380
125—28 1
110
725.381
725.382
Section
725.400
725.401
725.402
725.409
725.410
725.412
725.413
725.414
725.415
725.416
Section
725.440
725.441
725.445
725.447
725.451
725.452
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART N:
LANDFILLS
Applicability
Design Requirements
General Operating Requirements
Surveying and Recordkeeping
Closure and Post—Closure
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
Special Requirements for Liquid Wastes
Special Requirements for Containers
Disposal of Small Containers of Hazardous Waste in
Overpacked Drums
(Lab Packs)
SUBPART
0:
INCINERATORS
Applicability
Waste Analysis
General Operating Requirements
Monitoring and Inspection
Closure
Interim Status Incinerators Burning Particular
Hazardous Wastes
SUBPART P:
THERMAL TREATMENT
Other Thermal Treatment
General Operating Requirements
Waste Analysis
Monitoring and Inspections
Closure
Open Burning; Waste Explosives
Interim Status Thermal Treatment Devices Burning
Particular Hazardous Waste
SUBPART
Q:
CHEMICAL,
PHYSICAL
AND
BIOLOGICAL
TREATMENT
Applicability
General Operating Requirements
Waste Analysis and Trial Tests
Inspections
Closure
Special Requirements for Ignitable or Reactive Waste
Special Requirements for Incompatible Wastes
SUBPART
R:
UNDERGROUND
INJECTION
Section
725.530
Applicability
Section
725.470
725.473
725.475
725.477
725.481
725.482
725.483
Section
725.500
725.501
725.502
725.503
725.504
725.505
725.506
125—282
111
SUBPART
W:
DRIP
PADS
SUBPART AA:
AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
725.930
725.931
725.932
725.933
725.934
725. 935
Process Vents
Standards:
Closed—vent Systems and Control Devices
Test
methods
and
procedures
Recordkeeping Requirements
SUBPART
BB:
AIR
EMISSION
STANDARDS
FOR
EQUIPMENT
LEAKS
Applicability
Definitions
Standards:
Pumps in Light Liquid Service
Standards:
Compressors
Standards:
Pressure Relief Devices in Gas/Vapor
Service
Standards:
Sampling Connecting Systems
Standards:
Open—ended Valves or Lines
Standards:
Valves in Gas/Vapor or Light Liquid Service
Standards:
Pumps, Valves, Pressure Relief Devices,
Flanges and Other Connectors
Standards:
Delay of Repair
Standards:
Closed—vent Systems and Control Devices
Percent Leakage Alternative for Valves
Skip Period Alternative for Valves
Test Methods and Procedures
Recordkeeping Requirements
AUTHORITY:
Implementing Section 22.4 and authorized by Section
27 of the Environmental Protection Act
(Ill. Rev. Stat.
1989,
ch.
111—1/2, pars.
1022.4 and 1027).
SOURCE:
Adopted in R81—22,
43 PCB 427, at 5 Ill. Reg.
9781,
effective as noted in 35
Ill. Adm. Code 700.106; amended and
codified in R8l—22,
45 PCB 317, at
6 Ill.
Reg. 4828,
effective as
noted in 35 Ill. Adm. Code 700.106; amended in R82—l8,
51 PCB
Section
725. 540
.725. 541
725.542
725. 543
725.544
725.545
A~~l
icabi1ity
Assessment of existing drip pad integrity
Design and installation of new drip cads
Design and operating requirements
Inspections
-
Closure
Applicability
Definitions
Standards:
Section
725.950
725.951
725. 952
725.953
725.954
725.
955
725.956
725.957
725. 958
725. 959
725.960
725.961
725.962
725.963
725.964
Appendix A
Appendix B
Appendix C
Appendix D
Appendix E
Recordkeeping Instructions
EPA Report Form and Instructions
(Repealed)
EPA Interim Primary Drinking Water Standards
Tests for Significance
Examples of Potentially Incompatible ‘Waste
125—283
112
831, at
7
Ill.
Reg.
2518, effective February 22,
1983; amended in
R82—19,
53 PCB 131,
at
7
Ill.
Reg.
14034, effective October 12,
1983; amended in R84-9,
at
9
Ill. Reg.
11869, effective July 24,
1985; amended in R85—22 at 10 Ill.
Reg.
1085, effective January
2,
1986; amended in R86—1 at 10
Ill. Reg.
14069, effective August
12,
1986;
amended in R86—28 at 11 Ill. Reg.
6044,
effective March
24,
1987;
amended in R86—46 at 11 Ill. Reg.
13489, effective
August 4,
1987; amended
in R87—5 at 11 Ill. Reg.
19338, effective
November 10,
1987; amended in R87—26 at 12 Ill.
Reg.
2485,
effective January 15,
1988; amended in R87-39 at 12
Ill. Reg.
13027, e1~fectiveJuly 29,
1988;
amended in R88—16 at 13 Ill. Reg.
437, effective December 28,
1988; amended in R89-1 at 13
Ill.
Reg.
18354, effective November 13,
1989; amended in R90—2 at
14
Ill. Reg.
14447, effective August 22,
1990; amended in R90—10 at
14 Ill.
Reg.
16498, effective September 25,
1990; amended in R90-
11 at 15 Ill. Reg.
9398, effective June 17,
1991; amended in R91-
1 at 15
Ill.
Reg.
,
effective
SUBPART J:
TANK SYSTEMS
Section 725.290
Applicability
The regulations of this Subpart apply to owners and operators of
facilities that use tank systems for storing or treating
hazardous waste,
except as otherwise provided in subsections (a)~
e~—(b) or
(c), or in Section 725.101.
a)
Tank systems that are used to store or treat hazardous
waste which contains no free liquids and that are
situated inside a building with an impermeable floor
are exempted from the requirements in Section 725.293.
To demonstrate the absence or presence of free liquids
in the stored/treated waste, USEPA Method 9095
(Paint
Filter Liquids Test) as described in “Test Methods for
Evaluating Solid Wastes, Physical/Chemical Methods”
(EPA Publication No. SW-846),
incorporated by reference
in 35 Ill.
Adm..
Code 720.111, must be used.
b)
Tank systems,
including sumps,
as defined in 35 Ill.
Adm. Code 720.110, that serve as part of a secondary
containment system to collect or contain releases of
hazardous wastes are exempted from the requirements in
Section 725.293(a).
~j
Tanks,
sunips and other collection devices used in’
conjunction with drip pads,
as defined in 35
Ill.
Adni.
Code 720.110 and regulated under Subpart W, must meet
the requirements of this Subpart.
(Source:
Amended at 15 Ill.
Reg.
,
effective
)
125—284
113
SUBPART
W:
DRIP
PADS
Section 725.540
Applicability
~j
The requirements of this Subpart apply to owners and
operators of facilities that use new or existing drip
pads to convey treated wood drippage, precipitation or
surface water run-on to an associated collection
system.
fl.
“Existing drip pads” are:
Al
Those constructed before December
6,
1990
and
~j
Those for which the owner or operator has a
design and has entered into binding financial
or other agreements for construction prior to
December 6,
1990.
21
All other drip cads are “new drip pads”.
hi
The owner or operator of any drip pad that is inside or
under a structure that provides protection from
precipitation so that neither run—off nor run—on is
generated is not subject to regulation under Section
725.543(e)
or
(f).
(Source:
Added at 15 Ill.
Reg.
,
effective
Section 725.541
Assessment of existing drip pad integrity
~
For each existing drip pad, the owner or operator shall
evaluate the drip pad and determine that it meets all
of the requirements of this Subpart, except the
requirements for liners and leak detection systems of
Section 725.543(b).
No later than June 6,
1991, the
owner or operator shall obtain and keep on file at the
facility a written assessment of the drip pad, reviewed
and certified by an independent, qualified registered
professional engineer that attests to the results of
the evaluation.
The assessment must be reviewed,
updated and re-certified annually until all upgrades,
repairs or modifications necessary to achieve
compliance with all of the standards of Section 725.543
are complete.
The evaluation must justify and document
the extent to which the drip ~ad meets each of the
design and operating standards of Section 725.543,
except the standards for liners and leak detection
systems, specified in Section 725.543(b).
and must
document the age of the drip pad to the extent
125—285
114
possible,
to document compliance with subsection
(b).
~j
The owner or operator shall develop a written plan for
upgrading, repairing and modifying the drip pad to meet
the requirements of Section 725.543(b) and submit the
plan to the Agency no later than
2 years before the
date that all repairs, upgrades and modifications will
be complete.
This written plan must describe all
changes to be made to the drip pad in sufficient detail
to document compliance with all the requirements of
Section 725.543 and must document the age of the drip
pad to the extent possible.
The plan must be reviewed
and certified by an independent qualified, registered
professional engineer.
All upgrades, repairs and
modifications must be completed in accordance with the
following:
fl
For existing drip pads of known and documentable
age,
all upgrades, repairs and modifications must
be completed by June
6.
1993, or when the drip pad
has reached 15 years of age, whichever comes
later.
21
For existing drip pads for which the age cannot be
documented, by June 6,
1999; but,
if the age of
the facility is greater than 7 years,
all
upgrades, repairs and modifications must be
completed by the time the facility reaches
15
years of age or by June 6,
1993. whichever comes
later.
~j
The owner or operator may petition the Board for
an extension of the deadline
in subsection
(b) (1)
or
(2).
Al
The owner or operator shall file a petition
for a RCRA variance as specified in 35
Ill.
Adm. Code 104.
~j
The Board will grant the petition for
extension if it finds that:
Jj.
The drip ~ad meets all of the
requirements of Section 725.543, except
those for liners and leak detection
systems specified in Section 725.543(b)
and
.jJJ.
That it will continue to be protective
of human health and the environment.
~
Upon completion of all repairs and modifications, the
125—286
115
owner or operator shall submit to the Agency, the as—
built drawings for the drip pad, to~etherwith a
certification by an independent,
qualified, registered
professional engineer attesting that the drip pad
conforms to the drawings.
~j
If the drip ~ad is found to be leaking or unfit for
use, the owner or operator shall comply with the
provisions of Section 725.543(m)
or close the drip Pad
in accordance with Section 725.545.
(Source:
Added at 15
Ill.
Reg.
,
effective
Section 725.542
Design and installation of new drip pads
Owners and operators of new drip pads shall ensure that the pads
are designed, installed and operated in accordance with all of
the applicable requirements of Sections 725.543,
725.544 and
725. 545.
(Source:
Added at 15 Ill. Reg.
,
effective
)
Section 725.543
Design
arid operating requirements
Drip pads must:
fl
Not be constructed of earthen materials,
wood or
asphalt,
unless the asphalt is structurally
supported
21
Be
sloped
to
free—drain
to the associated
collection
system
treated
wood
drippage,
rain,
other
waters,
or
solutions
of
drippage
and
water
or
other
wastes
fl
Have
a
curb
or
berm
around
the
perimeter
4j
Be
impermeable,
e.g., concrete pads must be
sealed, coated or covered with an impermeable
material such that the entire surface where
drippage occurs or may run across is capable of
containing such drippage and mixtures of drippage
and precipitation, materials or other wastes while
being routed to an associated collection system
and
BOARD NOTE:
The requirement that new drip cads be
impermeable,
e.g.,
that new drip pads be sealed,
coated or covered with an impermeable material,
is
administratively stayed.
The stay will remain in
125—287
116
effect until further administrative action is
taken.
~J
Be of sufficient structural strength and thickness
to prevent failure due to physical contact,
climatic conditions, the stress of installation
and the stress of daily operations,
e.g.. variable
and moving loads such as vehicle traffic, movement
of wood,
etc.
BOARD NOTE:
In judging the structural integrity
requirement of this subsection,
the Agency should
generally consider applicable standards
established by professional organizations
generally recognized by the industry, including
ACI 318 or ASTM C94, incorporated by reference in
35
Ill. Adm. Code 720.111.
hi
A new drip pad or an existing drip pad, after the
deadline established in Section 725.541(b), must have:
fl..
A synthetic liner installed below the drip pad
that is designed, constructed and installed to
prevent leakage from the drip pad into the
adjacent subsurface soil or groundwater or surface
water at any time during the active life
(including the closure period) of the drip pad.
The liner must be constructed of materials that
will prevent waste from being absorbed into the
liner and prevent releases into the adjacent
subsurface soil or grbundwater or surface water
during the active life of the facility.
The liner
must be:
Al
Constructed of materials that have
appropriate chemical properties and
sufficient strength and thickness to prevent
failure due to pressure gradients (including
static head and external hydroqeologic
forces), physical contact with the waste or
drip pad leakage to which they are exposed,
climatic conditions, the stress of
installation and the stress of daily
operation (including stresses from vehicular
traffic on the drip pad)
~J..
Placed upon a foundation or base capable of
providing support to the liner and resistance
to pressure gradients above and below the
liner to prevent failure of the liner due to
settlement, compression or uplift; and
125—288
117
~l
Installed to cover
all
surrounding
earth
that
could come in contact with the waste or
leakage; and
21
A leakage detection system immediately above the
liner that
is designed, constructed. maintained
and operated to detect leaka~efrom the drip pad.
The leakage detection system must be:
Al
Constructed of materials that are:
j)
Chemically resistant to the waste
managed in the drip ~ad and the leakage
that might be generated
jjl
Designed and operated to function
without clogging through the scheduled
closure of the drip pad; and
iii) Of sufficient strength and thickness to
prevent collapse under the pressures
exerted bY overlaying materials and by
any equipment used at the drip pad; and
~j
Designed so that it will detect the failure
of the drip pad or the presence of a release
of hazardous waste or accumulated liquid at
the earliest practicable time.
ci
Drip pads must be maintained such that they remain free
of cracks,
gaps, corrosion or other deterioration that
could cause hazardous waste to be released from the
drip pad.
BOARD NOTE:
See subsection
(m)
for remedial action
required if deterioration or leaka~eis detected.
The drip ~ad and associated collection system must be
designed and operated to convey, drain and collect
liquid resulting from drippage or precipitation in
order to Prevent run—off.
~j
Unless the drip pad is Protected by a structure, as
described in Section 725.540(b).
the owner or oPerator
shall design,
construct, operate and maintain a run—on
control system capable of preventing flow onto the drip
pad during Peak discharge from at least a 24-hour.
25-
year storm, unless the system has sufficient excess
capacity to contain any run—on that might enter the
system.
-
fl
Unless the drip pad is protected by a structure or
125—289
118
cover, as described in Section 725.540(b), the owner or
operator shall design,
construct,
operate and maintain
a run—off management system to collect and control at
least the water volume resulting from a 24—hour, 25—
year storm.
gJ.
The drim pad must be evaluated to determine that it
meets the requirements of subsections
(a) through
(f).
The owner or operator shall obtain a statement from an
independent, qualified, registered professional
engineer certifying that the drip oad design meets the
requirements of this Section.
hi
Drippage and accumulated precipitation must be removed
from the associated collection system as necessary to
prevent overflow onto the drip pad.
il
The drip pad surface must be cleaned thoroughly at
least once every seven days such that accumulated
residues of hazardous waste or other materials are
removed, using an appropriate and effective cleaning
technique,
including but not limited to,
rinsing,
washing with detergents or other appropriate solvents,
or steam cleaning.
The owner or operator shall
document, in the facility’s operating log, the date and
time of each cleaning and the cleaning procedure.
jj
Drip pads must be operated and maintained in a manner
to minimize tracking of hazardous waste or hazardous
waste constituents off the drip pad as a result of
activities by personnel or equipment.
~j
After being removed from the treatment vessel, treated
wood from pressure and non—pressure processes must be
held on the drip pad until drippage has ceased.
The
owner or operator shall maintain records sufficient to
document that all treated wood is held on the pad,
in
accordance with this Section, following treatment.
IL
Collection and holding units associated with run-on and
run—off control systems must be emptied or otherwise
managed as soon as possible after storms to maintain
design capacity of the system.
~J
Throughout the active life of the drip pad,
if the
owner or operator detects a condition that may have
caused or has caused a release of hazardous waste, the
condition must be repaired within a reasonably prompt
period of time following discovery,
in accordance with
the following procedures:
fl
Upon detection of a condition that may have caused
125—290
119
or has caused a release of hazardous waste
(e.g.,
upon detection of leakage in the leak detection
system),
the owner or operator shall:
Al
Enter a record of the discovery in the
facility operating log
~j
Immediately remove from service the portion
of the drip ~ad affected by the condition
Q.).
Determine what steps must be taken to repair
the drip pad, clean up any leakage from below
the drip pad, and establish a schedule for
accomplishing the clean u~and repairs
Qj
Within 24 hours after discovery of the
condition, notify the Agency of the condition
and, within 10 working days, provide written
notice to the Agency with a description of
the steps that will be taken to repair the’
drip pad and clean up any leakage, and the
schedule for accomplishing this work.
21
The Agency shall:
review the information
submitted; make a determination regarding whether
the pad must be removed from service completely or
partially until repairs and clean up are complete;
and notify the owner or operator of the
determination and the underlying rationale in
writing.
fl
Upon completing all repairs and clean
~rn.
the
owner or operator shall notify the Agency in
writing and provide a certification, signed by an
independent, gualified, registered professional
engineer, that the repairs and clean up have been
completed according to the written plan submitted
in accordance with subsection
(m) (1) (D).
~fl
The owner or operator shall maintain,
as cart of the
facility operating log, documentation of past operating
and waste handling practices.
This must include
identification of preservative formulations used in the
past,
a description of drippage mana~ementpractices
and a description of treated wood storage and handling
practices.
(Source:
Added at 15
Ill.
Reg.
,
effective
Section 725.544
Inspections
125—29 1
120
~j
During construction or installation, liners and cover
systems
(e.g.. membranes,
sheets or coatings) must be
inspected for uniformity,
damage and imperfections
(e.g., holes, cracks, thin spots or foreign materials).
Immediately after construction or installation, liners
must be inspected and certified as meeting the
requirements of Section 725.543 by an independent,
qualified,
registered professional engineer.
The
certification must be maintained at the facility as
part of the facility operating record.
After
installation liners and covers must be inspected to
ensure tight seams and joints and the absence of tears,
punctures or blisters.
hi
While a drip pad is in operation,
it must be inspected
weekly
and after storms to detect evidence of any of
the following:
fl
Deterioration, malfunctions or improper operation
of run—on and run—off control systems
21
The presence of leakage in and proper functioning
of leak detection system.
~j
Deterioration or cracking of the drip pad surface.
BOARD NOTE:
See Section 725.543(m)
for remedial
action required if deterioration or leakage
is
detected.
(Source:
Added at 15
Ill.
Reg.
,
effective
)
Section 725.545
Closure
~j
At closure, the owner or operator shall remove or
decontaminate all waste residues, contaminated
containment system components
(pad,
liners,
etc.),
contaminated subsoils, and structures and equipment
contaminated with waste and leakage, and manage them as
hazardous waste.
-
hi
If, after removing or decontaminating all residues and
making all reasonable efforts to effect removal or
decontamination of contaminated components, subsoils,
structures and equipment as required in subsection
(a),
the owner or operator finds that not all contaminated
subsoils can be practically removed or decontaminated,
The operator shall close the unit and perform post—
closure care in accordance with closure and post—
closure care requirements that apply to landfills
(Section 725.410).
For permitted units,
the
125—292
121
requirement to have a permit continues throughout the
post— closure period.
ci
Existing drip Pads without liners.
fl
The owner or operator of an existing drip pad that
does not com~lvwith the liner requirements of
Section 725.543(b) (1)
shall:
Al
Include in the closure Plan for the drip Pad
under Section 725.212 both a plan for
compJyin~with subsection
(a) and a
contingent plan for comPlying with subsection
(b) ~n case not all contaminated subsoils can
be practicably removed at closure; and
~j
PrePare a contingent post—closure Plan under
Section 725.218 .for complying with subsection
(b)
in case not all contaminated subsoils can
be ~ract1cably removed at closure.
21
The cost estimates calculated under Sections
725.212 and 725.244 for closure and post closure
care of a drip pad subject to this subsection must
include the cost of complying with the contingent
closure plan and the contingent post closure plan.
but are not required to include the cost of
exPected closure under subsection
(a).
(Source:
Added at 15
Ill. Reg.
,
effective
)
125—293
