ILLINOIS POLLUTION CONTROL BOARD
July 24, 1997
IN THE MATTER OF:
)
)
R96-10
RCRA UPDATE, USEPA REGULATIONS
)
(Identical in Substance Rules)
(July 1 through December 31, 1995)
)
______________________________________
IN THE MATTER OF:
)
)
R97-3
UIC UPDATE, USEPA REGULATIONS
)
(Identical-in-Substance Rules)
(January 1 through June 30, 1996)
)
______________________________________
IN THE MATTER OF:
)
)
R97-5
RCRA UPDATE, USEPA REGULATIONS
)
(Identical in Substance Rules)
(January 1 through June 30, 1996)
)
Proposed Rule. Proposal for Public Comment.
ORDER OF THE BOARD (by K.M. Hennessey):
Pursuant to Section 13(c) and 22.4(a) of the Environmental Protection Act (Act) [415
ILCS 5/13(c) & 22.4(a) (1996)], the Board proposes amendments to the Resource
Conservation and Recovery Act of 1976 (RCRA Subtitle C) hazardous waste regulations.
Section 22.4(a) provides for quick adoption of regulations that are "identical in
substance" to federal regulations adopted by USEPA to implement Sections 3001 through 3005
of RCRA, 42 U.S.C. ยงยง 6921-6925 (1996)) and that Title VII of the Act and Section 5 of the
Administrative Procedure Act (APA) [5 ILCS 100/5-35 & 5-40 (1996)] shall not apply.
Because this rulemaking is not subject to Section 5 of the APA, it is not subject to first notice
or to second notice review by the Joint Committee on Administrative Rules (JCAR). The
federal RCRA Subtitle C regulations are found at 40 CFR 260 through 268, 270 through 271,
279, and, more recently, 273.
This order is supported by a proposed opinion adopted on the same day. The Board
will submit Notices of Proposed Amendments for publication in the Illinois Register. The
complete text of the proposed rules follows.
IT IS SO ORDERED.
2
I, Dorothy M. Gunn, Clerk of the Illinois Pollution Control Board, certify that the
above order was adopted on the 24th day of July 1997, by a vote of 4-0.
Dorothy M. Gunn, Clerk
Illinois Pollution Control Board
3
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER b: PERMITS
PART 702
RCRA AND UIC PERMIT PROGRAMS
SUBPART A: GENERAL PROVISIONS
Section
702.101
Purpose, Scope, and Applicability
702.102
Purpose and Scope (Repealed)
702.103
Confidentiality of Informa
tion Submitted to the Agency or Board
702.104
References
702.105
Rulemaking
702.106
Adoption of Agency Criteria
702.107
Permit Appeals and Review of Agency Determinations
702.108
Variances and Adjusted Standards
702.109
Enforcement Actions
702.110
Definitions
SUBPART B: PERMIT APPLICATIONS
Section
702.120
Permit Application
702.121
Who Applies
702.122
Completeness
702.123
Information Requirements
702.124
Recordkeeping
702.125
Continuation of Expiring Permits
702.126
Signatories to Permit Applications and
Reports
SUBPART C: PERMIT CONDITIONS
Section
702.140
Conditions Applicable to all Permits
702.141
Duty to Comply
702.142
Duty to Reapply
702.143
Need to Halt or Reduce Activity Not a Defense
702.144
Duty to Mitigate
702.145
Proper Operation and Maintenance
702.146
Permit Actions
702.147
Property Rights
702.148
Duty to Provide Information
702.149
Inspection and Entry
702.150
Monitoring and Records
702.151
Signature Requirements
702.152
Reporting Requirements
702.160
Establishing Permit Conditions
702.161
Duration of Permits
702.162
Schedules of Compliance
702.163
Alternative Schedules of Compliance
702.164
Recording and Reporting
SUBPART D: ISSUED PERMITS
Section
702.181
Effect of a Permit
702.182
Transfer
702.183
Modification
702.184
Causes for Modification
702.185
Facility Siting
702.186
Revocation
702.187
Minor Modifications
4
AUTHORITY: Implementing Section 13 and 22.4 and authorized by Section 27 of
the Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
SOURCE: Adopted in R81-32, 47 PCB 93, at 6 Ill. Reg. 12479, effective May 17,
1982; amended in R82-19, at 53 PCB 131, 7 Ill. Reg. 14352, effective May 17,
1982; amended in R84-9 at 9 Ill. Reg. 11926, effective July 24, 1985; amended
in R85-23 at 10 Ill. Reg. 13274, effective July 29, 1986; amended in R86-1 at
10 Ill. Reg. 14083, effective August 12, 1986; amended in R86-28 at 11 Ill.
Reg. 6131, effective March 24, 1987; amended in R87-5 at 11 Ill. Reg. 19376,
effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2579, effective
January 15, 1988; amended in R87-29 at 12 Ill. Reg. 6673, effective March 28,
1988; amended in R87-39 at 12 Ill. Reg. 13083, effective July 29, 1988;
amended in R89-1 at 13 Ill. Reg. 18452, effective November 13, 1989; amended
in R89-2 at 14 Ill. Reg. 3089, effective February 20, 1990; amended in R89-9
at 14 Ill. Reg. 6273, effective April 16, 1990; amended in R92-10 at 17 Ill.
Reg. 5769, effective March 26, 1993; amended in R93-16 at 18 Ill. Reg. 6918,
effective April 26, 1994; amended in R94-5 at 18 Ill. Reg. 18284, effective
December 20, 1994; amended in R95-6 at 19 Ill. Reg. 9913, effective June 27,
1995; amended in R95-20 at 20 Ill. Reg. 11210, effective August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
SUBPART A: GENERAL PROVISIONS
Section 702.110
Definitions
The following definitions apply to 35 Ill. Adm. Code 702, 703, 704, and 705.
Terms not defined in this Section have the meaning given by the appropriate
Act. When a defined term appears in a definition, the defined term is
sometimes placed within quotation marks as to an aid to readers. When a
definition applies primarily to one or more programs, those programs appear in
parentheses after the defined terms.
"Act" or "Environmental Protection Act" means the Environmental
Protection Act [415 ILCS 5].
"Administrator" means the Administrator of the United States
Environmental Protection Agency, or an authorized representative.
"Agency" means the Illinois Environmental Protection Agency.
"Application" means the Agency forms for applying for a permit.
For RCRA, application also includes the information required by
the Agency under 35 Ill. Adm. Code 703.182 through 703.212
(contents of Part B of the RCRA application).
"Appropriate act and regulations" means the Resource Conservation
and Recovery Act (RCRA); Safe Drinking Water Act (SDWA); or the
"Environmental Protection Act", whichever is applicable; and
applicable regulations promulgated under those statutes.
"Approved program or
approved State" means a State or interstate
program that has been approved or authorized by EPA under 40 CFR
271 (19 9296) (RCRA) or Section 1422 of the SDWA (UIC).
"Aquifer" (RCRA and UIC) means a geological "formation", group of
formations, or part of a formation that is capable of yielding a
significant amount of water to a well or spring.
5
"Area of review" (UIC) means the area surrounding an injection
well described according to the criteria set forth in 35 Ill. Adm.
Code 730.106, or in the case of an area permit, the project area
plus a circumscribing area the width of that is either 402 meters
(1/4 of a mile) or a number calculated according to the criteria
set forth in 35 Ill. Adm. Code 730.106.
"Board" means the Illinois Pollution Control Board.
"Closure" (RCRA) means the act of securing a "Hazardous Waste
Management Facility" pursuant to the requirements of 35 Ill. Adm.
Code 724.
"Component" (RCRA) means any constituent part of a unit or any
group of constituent parts of a unit that are assembled to perform
a specific function (e.g., a pump seal, pump, kiln liner, or kiln
thermocouple).
"Contaminant" (UIC) means any physical, chemical, biological, or
radiological substance or matter in water.
"Corrective action management unit" or "CAMU" means an area within
a facility that is designated by the Agency under 35 Ill. Adm.
Code 724.Subpart S for the purpose of implementing corrective
action requirements under 35 Ill. Adm. Code 724.201 and RCRA
section 3008(h). A CAMU shall only be used for the management of
remediation wastes pursuant to implementing such corrective action
requirements at the facility.
BOARD NOTE: USEPA must also designate a CAMU until it grants this
authority to the Agency. See the note following 35 Ill. Adm. Code
724.652.
"CWA" means the Clean Water Act (formerly referred to as the
Federal Water Pollution Control Act or Federal Water Pollution
Control Act Amendments of 1972), P.L. 92-500, as amended by P.L.
95-217 and P.L. 95-576; 33 U.S.C. 1251 et seq. (19
9296).
"Date of approval by USEPA of the Illinois UIC program" means
March 3, 1984.
"Director" means the Director of the Illinois Environmental
Protection Agency or the Director's designee.
"Disposal" (RCRA) means the discharge, deposit, injection,
dumping, spilling, leaking, or placing of any "hazardous waste"
into or on any land or water so that such hazardous waste or any
constituent of the waste may enter the environment or be emitted
into the air or discharged into any waters, including groundwater.
"Disposal Facility" (RCRA) means a facility or part of a facility
at which "hazardous waste" is intentionally placed into or on the
land or water, and at which hazardous waste will remain after
closure. The term disposal facility does not include a corrective
action management unit into which remediation wastes are placed.
"Draft Permit" means a document prepared under 35 Ill. Adm. Code
705.141 indicating the Agency's tentative decision to issue, deny,
modify, terminate, or reissue a "permit". A notice of intent to
deny a permit, as discussed in 35 Ill. Adm. Code 705.141, is a
type of "draft permit". A denial of a request for modification,
as discussed in 35 Ill. Adm. Code 705.128, is not a "draft
6
permit". A "proposed permit" is not a "draft permit".
"Drilling Mud" (UIC) means a heavy suspension used in drilling an
"injection well", introduced down the drill pipe and through the
drill bit.
"Elementary neutralization unit" means a device which:
Is used for neutralizing wastes that are ha
zardous wastes
only because they exhibit the corrosivity characteristics
defined in 35 Ill. Adm. Code 721.122, or are listed in 35
Ill. Adm. Code 721.Subpart D only for this reason; and
Meets the definition of tank, tank system, container,
transport vehicle or vessel in 35 Ill. Adm. Code 720.110.
"Emergency Permit" means a RCRA or UIC "permit" issued in
accordance with 35 Ill. Adm. Code 703.221 or 704.163,
respectively.
"Environmental Protection Agency" ("EPA" or "USEPA") means the
United States Environmental Protection Agency.
"Exempted aquifer" (UIC) means an "aquifer" or its portion that
meets the criteria in the definition of "underground source of
drinking water" but which has been exempted according to the
procedures in 35 Ill. Adm. Code 702.105, 704.104, and 704.123(b).
"Existing hazardous waste management (HWM) facility" or "existing
facility" means a facility that was in operation or for which
construction commenced on or before November 19, 1980. A facility
has commenced construction if:
The owner or operator has obtained the Federal, State, and
local approvals or permits necessary to begin physical
construction; and
Either:
A continuous on-site, physical construction program
has begun; or
The owner or operator has entered into contractual
obligations--that cannot be canceled or modified
without substantial loss--for physical construction of
the facility to be completed within a reasonable time.
"Existing injection well" (UIC) means an "injection well" other
than a "new injection well".
"Facility mailing list" means the mailing list for a facility
maintained by the Agency in accordance with 35 Ill. Adm. Code
705.163(a).
"Facility or activity" means any "HWM facility", UIC "injection
well", or any other facility or activity (including land or
appurtenances thereto) that is subject to regulations under the
Illinois RCRA or UIC program.
"Facility mailing list" (RCRA) means the mailing list for a
facility maintained by the Agency in accordance with 35 Ill. Adm.
7
Code 705.163.
"Federal, State, and local approvals or permits necessary to begin
physical construction" means permits and approvals required under
Federal, State, or local hazardous waste control statutes,
regulations, or ordinances. (See 35 Ill. Adm. Code 700.102.)
"Final authorization" (RCRA) means approval by EPA of the Illinois
Hazardous Waste Management Program that has met the requirements
of Section 3006(b) of RCRA and the applicable requirements of 40
CFR 271, Subpart A (19
9296). EPA granted initial final
authorization on January 31, 1986.
"Fluid" (UIC) means any material or substance that flows or moves
whether in a semisolid, liquid, sludge, gas, or any other form or
state.
"Formation" (UIC) means a body of rock characterized by a degree
of lithologic homogeneity that is prevailingly, but not
necessarily, tabular and is mappable on the earth's surface or
traceable in the subsurface.
"Formation fluid" (UIC) means "fluid" present in a "formation"
under natural conditions, as opposed to introduced fluids, such as
"drilling mud".
"Functionally equivalent component" (RCRA) means a component that
performs the same function or measurement and which meets or
exceeds the performance specifications of another component.
"Generator" (RCRA) means any person, by site location, whose act
or process produces "hazardous waste" identified or listed in 35
Ill. Adm. Code 721.
"Groundwater" (RCRA and UIC) means a water below the land surface
in a zone of saturation.
"Hazardous Waste" (RCRA a
nd UIC) means a hazardous waste as
defined in 35 Ill. Adm. Code 721.103.
"Hazardous waste management facility" ("HWM facility") means all
contiguous land and structures, other appurtenances, and
improvements on the land, used for treating, storing, or disposing
of "hazardous waste". A facility may consist of several
"treatment", "storage", or "disposal" operational units (for
example, one or more landfills, surface impoundments, or
combinations of them).
"HWM facility" (RCRA) means "Hazardous Waste M
anagement facility".
"Injection well" (RCRA and UIC) means a "well" into which "fluids"
are being injected.
"Injection zone" (UIC) means a geological "formation", group of
formations, or part of a formation receiving fluids through a
"well".
"In operation" (RCRA) means a facility that is treating, storing,
or disposing of "hazardous waste".
"Interim authorization" (RCRA) means approval by EPA of the
8
Illinois Hazardous Waste Management program that has met the
requirements of Section 3006(g)(2) of RCRA and applicable
requirements of 40 CFR 271 (19
9296). This happened on May 17,
1982.
"Interstate agency" means an agency of two or more states
established by or under an agreement or compact approved by the
Congress, or any other agency of two or more states having
substantial powers or duties pertaining to the control of
pollution as determined and approved by the Administrator under
the "appropriate Act and regulations".
"Major facility" means any RCRA or UIC "facility or activity"
classified as such by the Regional Administrator or the Agency.
"Manifest" (RCRA and UIC) means the shipping document originated
and signed by the "generator" that contains the information
required by 35 Ill. Adm. Code 722.Subpart B.
"National Pollutant Discharge Elimination System" means the
program for issuing, modifying, revoking and reissuing,
terminating, monitoring, and enforcing permits and imposing and
enforcing pretreatment requirements under Section 12(f) of the
Environmental Protection Act and 35 Ill. Adm. Code 309.Subpart A
and 310. The term includes an "approved program".
"New HWM facility" (RCRA) means a "Hazardous Waste Management
facility" that began operation or for which construction commenced
after November 19, 1980.
"New injection well" (UIC) means a "well" that began injection
after the UIC program for the State of Illinois applicable to the
well is approved.
"Off-site" (RCRA) means any site that is not "on-site".
"On-site" (RCRA) means on the same or geographically contiguous
property that may be divided by public or private right(s)-of-way,
provided the entrance and exit between the properties is at a
cross-roads intersection, and access is by crossing as opposed to
going along, the right(s)-of-way. Non-contiguous properties owned
by the same person but connected by a right-of-way that the person
controls and to which the public does not have access, is also
considered on-site property.
"Owner or operator" means the owner or operator of any "facility
or activity" subject to regulation under the RCRA or UIC programs.
"Permit" means an authorization, license, or equivalent control
document issued to implement the requirements of this Part and 35
Ill. Adm. Code 703, 704, and 705.
"Permit" includes RCRA "permit by rule" (35 Ill. Adm. Code
703.141), UIC area permit (35 Ill. Adm. Code 704.162), and RCRA or
UIC "Emergency Permit" (35 Ill. Adm. Code 703.221 and 704.163).
"Permit" does not include RCRA interim status (35 Ill. Adm. Code
703.153 through 703.157), UIC authorization by rule (35 Ill. Adm.
Code 704.Subpart C), or any permit that has not yet been the
subject of final Agency action, such as a "Draft Permit" or a
"Proposed Permit".
9
"Person" means any individual, partnership, co-partnership, firm,
company, corporation, association, joint stock company, trust,
estate, political subdivision, state agency, or any other legal
entity, or their legal representative, agency, or assigns.
"Physical construction" (RCRA) means excavation, movement of
earth, erection of forms or structures or similar activity to
prepare an "HWM facility" to accept "hazardous waste".
"Plugging" (UIC) means the act or process of stopping the flow of
water, oil, or gas into or out of a formation through a borehole
or well penetrating that formation.
"POTW" means "publicly owned treatment works".
"Project" (UIC) means a group of wells in a single operation.
"Publicly owned treatment works" ("POTW") is as defined in 35 Ill.
Adm. Code 310.
"Radioactive waste" (UIC) means any waste that conta
ins
radioactive material in concentrations that exceed those listed in
10 CFR 20, Appendix B, Table II, Column 2, incorporated by
reference in 35 Ill. Adm. Code 720.111.
"RCRA" means the Solid Waste Disposal Act as amended by the
Resource Conservation and Recovery Act of 1976 (P.L. 94-580, as
amended by P.L. 95-609, P.L. 96-510, 42 U.S.C. 6901 et seq.
(199296)). For the purposes of regulation under 35 Ill. Adm. Code
700 through 705, 720 through 728, and 739, "RCRA" refers only to
RCRA Subtitle C. This does not include the RCRA Subtitle D
(municipal solid waste landfill) regulations, found in 35 Ill.
Adm. Code 810 through 815, and the RCRA Subtitle I (underground
storage tank) regulations found in 35 Ill. Adm. Code 731 and 732.
"RCRA permit" means a permit required under Section 21(f) of the
Environmental Protection Act.
"Regional Administrator" means the Regional Administrator for the
EPA Region in which the facility is located or the Regional
Administrator's designee.
"Schedule of compliance" m
eans a schedule of remedial measures
included in a "permit", including an enforceable sequence of
interim requirements (for example, actions, operations, or
milestone events) leading to compliance with the "appropriate Act
and regulations".
"SDWA" means the Safe Drinking Water Act (P.L. 93-523, as amended,
42 U.S.C. 300f et seq. (19
9296)).
"Site" means the land or water area where any "facility or
activity" is physically located or conducted, including adjacent
land used in connection with the facility or activity.
"SIC Code" means codes pursuant to the Standard Industrial
Classification Manual incorporated by reference in 35 Ill. Adm.
Code 720.111.
"State" means the State of Illinois.
10
"State Director" means the Director of the Illinois Environmental
Protection Agency.
"State/EPA Agreement" means an agreement between the Regional
Administrator and the State that coordinates EPA and State
activities, responsibilities, and programs including those under
the RCRA and SDWA.
"Storage" (RCRA) m
eans the holding of "hazardous waste" for a
temporary period, at the end of which the hazardous waste is
treated, disposed, or stored elsewhere.
"Stratum (plural strata)" (UIC) means a single sedimentary bed or
layer, regardless of thickness, that consists of generally the
same kind of rock material.
"Total dissolved solids" (UIC) means the total dissolved
(filterable) solids as determined by use of the method specified
in 40 CFR 136, incorporated by reference in 35 Ill. Adm. Code
720.111.
"Transfe r facility" means any transportation related facility
including loading docks, parking areas, storage areas, and other
similar areas where shipments of hazardous wastes are held during
the normal course of transportation.
"Transferee" (UIC) means the owner or operator receiving ownership
or operational control of the well.
"Transferor" (UIC) means the owner or operator transferring
ownership or operational control of the well.
"Transporter" (RCRA) means a person engaged in the off-site
transportation of "hazardous waste" by air, rail, highway, or
water.
"Treatment" (RCRA) means any method, technique, process, including
neutralization, designed to change the physical, chemical, or
biological character or composition of any "hazardous waste" so as
to neutralize such wastes, or so as to recover energy or material
resources from the waste, or so as to render such wastes non-
hazardous, or less hazardous; safer to transport, store, or
dispose of; or amenable for recovery, amenable for storage, or
reduced in volume.
"UIC" means the Underground Injection Control program.
"Underground Injection" (UIC) means a "well injection".
"Underground source of drinking water" ("USDW") (RCRA and UIC)
means an "aquifer" or its portion:
Which:
Supplies any public water system; or
Contains a sufficient quantity of groundwater to
supply a public water system; and
Currently supplies drinking water for human
consumption; or
11
Contains less than 10,000 mg/1 total dissolved solids;
and
That i s not an "exempted aquifer".
"USDW" (RCRA and UIC) means an "underground source of drinking
water".
"Wastewater treatment unit" means a device which:
Is part of a wastewater treatment facility that is subject
to regulation under 35 Ill. Adm. Code 309.Subpart A or 310;
and
Receives and treats or stores an influent wastewater that is
a hazardous waste as defined in 35 Ill. Adm. Code 721.103,
or generates and accumulates a wastewater treatment sludge
that is a hazardous waste as defined in 35 Ill. Adm. Code
721.103, or treats or stores a wastewater treatment sludge
that is a hazardous waste as defined in 35 Ill. Adm. Code
721.103; and
Meets the definition of tank or tank system in 35 Ill. Adm.
Code 720.110.
"Well" (UIC) means a bored, drilled, or driven shaft, or a dug
hole, whose depth is greater than the largest surface dimension.
"Well injection" (UIC) means the subsurface emplacement of
"fluids" through a bored, drilled, or driven "well"; or through a
dug well, where the depth of the dug well is greater than the
largest surface dimension.
BOARD NOTE: Derived from 40 CFR 144.3 (19
9496) and 270.2
(199496), as amended at 60 Fed. Reg. 33914 (June 29, 1995)
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER b: PERMITS
PART 703
RCRA PERMIT PROGRAM
SUBPART A: GENERAL PROVISIONS
Section
703.100
Scope and Relation to Other Parts
703.101
Purpose
703.110
References
SUBPART B: PROHIBITIONS
Section
703.120
Prohibitions in General
703.121
RCRA Permits
703.122
Specific Inclusions in Permit Program
703.123
Specific Exclusions from Permit Program
703.124
Discharges of Hazardous Waste
12
703.125
Reapplications
703.126
Initial Applications
703.127
Federal Permits (Repealed)
SUBPART C: AUTHORIZATION BY RULE AND INTERIM STATUS
Section
703.140
Purpose and Scope
703.141
Permits by Rule
703.150
Application by Existing HWM Facilities and Interim Status
Qualifications
703.151
Application by New HWM Facilities
703.152
Amended Part A Application
703.153
Qualifying for Interim Status
703.154
Prohibitions During Interim Status
703.155
Changes During Interim Status
703.156
Interim Status Standards
703.157
Grounds for Termination of Interim Status
703.158
Permits for Less Than an Entire Facility
703.159
Closure by Removal
703.160
Procedures for Closure Determination
SUBPART D: APPLICATIONS
Section
703.180
Applications in General
703.181
Contents of Part A
703.182
Contents of Part B
703.183
General Information
703.184
Facility Location Information
703.185
Groundwater Protection Information
703.186
Exposure Information
703.187
Solid Waste Management Units
703.188
Other Information
703.191
Public Participation: Pre-Application Public Notice and Meeting
703.192
Public Participation: Public Notice of Application
703.193
Public Participation: Information Repository
703.200
Specific Part B Application Information
703.201
Containers
703.202
Tank Systems
703.203
Surface Impoundme
nts
703.204
Waste Piles
703.205
Incinerators that Burn Hazardous Waste
703.206
Land Treatment
703.207
Landfills
703.208
Boilers and Industrial Furnaces Burning Hazardous Waste
703.209
Miscellaneous Units
703.210
Process Vents
703.211
Equipment
703.212
Drip Pads
703.213
Air Emission Controls for Tanks, Surface Impoundments, and
Containers
SUBPART E: SHORT TERM AND PHASED PERMITS
Section
703.221
Emergency Permits
703.222
Incinerator Conditions Prior to Trial Burn
703.223
Incinerator Conditions During Trial
Burn
703.224
Incinerator Conditions After Trial Burn
703.225
Trial Burns for Existing Incinerators
703.230
Land Treatment Demonstration
703.231
Research, Development and Demonstration Permits
703.232
Permits for Boilers and Industrial Furnaces Burning Hazardous
13
Waste
SUBPART F: PERMIT CONDITIONS OR DENIAL
Section
703.240
Permit Denial
703.241
Establishing Permit Conditions
703.242
Noncompliance Pursuant to Emergency Permit
703.243
Monitoring
703.244
Notice of Planned Changes (Repealed)
703.245
Twenty-four Hour Reporting
703.246
Reporting Requirements
703.247
Anticipated Noncompliance
703.248
Information Repository
SUBPART G: CHANGES TO PERMITS
Section
703.260
Transfer
703.270
Modification
703.271
Causes for Modification
703.272
Causes for Modification or Reissuance
703.273
Facility Siting
703.280
Permit Modification at the Request of the Permittee
703.281
Class 1 Modifications
703.282
Class 2 Modifications
703.283
Class 3 Modifications
703.Appendix A
Classification of Permit Modifications
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14289, effective October
12, 1983; amended in R83-24 at 8 Ill. Reg. 206, effective December 27, 1983;
amended in R84-9 at 9 Ill. Reg. 11899, effective July 24, 1985; amended in
R85-22 at 10 Ill. Reg. 1110, effective January 2, 1986; amended in R85-23 at
10 Ill. Reg. 13284, effective July 28, 1986; amended in R86-1 at 10 Ill. Reg.
14093, effective August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20702,
effective December 2, 1986; amended in R86-28 at 11 Ill. Reg. 6121, effective
March 24, 1987; amended in R86-46 at 11 Ill. Reg. 13543, effective August 4,
1987; amended in R87-5 at 11 Ill. Reg. 19383, effective November 12, 1987;
amended in R87-26 at 12 Ill. Reg. 2584, effective January 15, 1988; amended in
R87-39 at 12 Ill. Reg. 13069, effective July 29, 1988; amended in R88-16 at 13
Ill. Reg. 447, effective December 27, 1988; amended in R89-1 at 13 Ill. Reg.
18477, effective November 13, 1989; amended in R89-9 at 14 Ill. Reg. 6278,
effective April 16, 1990; amended in R90-2 at 14 Ill. Reg. 14492, effective
August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9616, effective June 17,
1991; amended in R91-1 at 15 Ill. Reg. 14554, effective September 30, 1991;
amended in R91-13 at 16 Ill Reg. 9767, effective June 9, 1992; amended in R92-
10 at 17 Ill. Reg. 5774, effective March 26, 1993; amended in R93-4 at 17 Ill.
Reg. 20794, effective November 22, 1993; amended in R93-16 at 18 Ill. Reg.
6898, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg. 12392,
effective July 29, 1994; amended in R94-5 at 18 Ill. Reg. 18316, effective
December 20, 1994; amended in R95-6 at 19 Ill. Reg. 9920, effective June 27,
1995; amended in R95-20 at 20 Ill. Reg. 11225, effective August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
SUBPART D: APPLICATIONS
Section 703.180
Applications in General
14
a)
This Subpart c ontains requirements for applications for RCRA
permits. A "Part A" application is required of all facilities to
obtain interim status. The "Part B" application is a prerequisite
to an actual permit, and need be filed for an existing facility
with interim status only when requested. New facilities must file
Part A and Part B at the same time;
b)
Subpart E contains requirements for applications for emergency
permits, trial burn permits and land treatment demonstration
permits;
c)
The application packag
e consists of the following:
1)
Information required by 35 Ill. Adm. Code 702.123;
2)
Part A (Section 703.181);
3)
Part B:
A)
General information (Section 703.183);
B)
Facility location information (Section 703.184);
C)
Groundwater protection information, if required
(Section 703.185);
D)
Specific information for each type of TSD unit, i.e.
tanks, surface impoundments, landfills, etc. (Sections
703.200 et seq.);
E)
Additional information to demonstrate compliance with
35 Ill. Adm. Code 724 (Section 703.183(t));
F)
Information for trial burn permits and land treatment
demonstrations (Subpart E).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 703.183
General Information
The following information is required in the Part B application for all HWM
facilities, except as 35 Ill. Adm. Code 724.101 provides otherwise:
a)
A general description of the facility;
b)
Chemical and physical analyses of the hazardous wastes and
hazardous debris to be handled at the facility. At a minimum,
these analyses must contain all the information which must be
known to treat, store or dispose of the wastes properly in
accordance with 35 Ill. Adm. Code 724;
c)
A copy of the waste analysis plan required by 35 Ill. Adm. Code
724.113(b) and, if applicable, 35 Ill. Adm. Code 724.113(c);
d)
A description of the security procedures and equipment required by
35 Ill. Adm. Code 724.114, or a justification demonstrating the
reasons for requesting a waiver of this requirement;
e)
A copy of the general inspection schedule required by 35 Ill. Adm.
Code 724.115(b). Include where applicable, as part of the
15
inspection schedule, specific requirements in 35 Ill. Adm. Code
724.274, 724.293(i), 724.295, 724.326, 724.354, 724.373, 724.403,
724.702, 724.933, 724.952, 724.953, 724.958,
724.984, 724.985,
724.986, and 724.988 , and 724.991 ;
f)
A justification of any request for a waiver of the preparedness
and prevention requirements of 35 Ill. Adm. Code 724.Subpart C;
g)
A copy of the contingency plan required by 35 Ill. Adm. Code
724.Subpart D;
BOARD NOTE: Include, where applicable, as part of the contingency
plan, specific requirements in 35 Ill. Adm. Code 724.327 and
724.355. 35 Ill. Adm. Code 724.355 has not yet been adopted.
h)
A description of procedures, structures, or equipment used at the
facility to:
1)
Prevent hazards in unloading operations (for example, ramps,
or special forklifts);
2)
Prevent runoff from hazardous waste handling areas to other
areas of the facility or environment, or to prevent flooding
(for example, berms, dikes, or trenches);
3)
Prevent contamination of water supplies;
4)
Mitigate effects of equipment failure and power outages;
5)
Prevent undue exposure of personnel to hazardous waste (for
example, protective clothing); and
6)
Prevent releases to the atmosphere.
i)
A description of precautions to prevent accidental ignition or
reaction of ignitable, reactive, or incompatible wastes, as
required to demonstrate compliance with 35 Ill. Adm. Code 724.117,
including documentation demonstrating compliance with 35 Ill. Adm.
Code 724.117(c);
j)
Traffic pattern, estimated volume (number and types of vehicles),
and control (for example, show turns across traffic lanes and
stacking lanes, if appropriate); describe access road surfacing
and load bearing capacity; and show traffic control signals;
k)
Facility location information, as required by Section 703.184;
l)
An outline of both the introductory and continuing training
programs by the owner or operator to prepare persons to operate or
maintain the HWM facility in a safe manner, as required to
demonstrate compliance with 35 Ill. Adm. Code 724.116. A brief
description of how training will be designed to meet actual job
tasks in accordance with requirements in 35 Ill. Adm. Code
724.116(a)(3);
m)
A copy of the closure plan and, where applicable, the post-closure
plan required by 35 Ill. Adm. Code 724.212, 724.218, and 724.297.
Include where applicable, as part of the plans, specific
requirements in 35 Ill. Adm. Code 724.278, 724.297, 724.328,
724.358, 724.380, 724.410, 724.451, 724.701, and 724.703;
16
n)
For hazardous waste disposal units that have been closed,
documentation that notices required under 35 Ill. Adm Code 724.219
have been filed;
o)
The most recent closure cost estimate for the facility, prepared
in accordance with 35 Ill. Adm. Code 724.242, and a copy of the
documentation required to demonstrate financial assurance under 35
Ill. Adm. Code 724.243. For a new facility, a copy of the
required documentation may be submitted 60 days prior to the
initial receipt of hazardous wastes, if it is later than the
submission of the Part B permit application;
p)
Where applicable, the most recent post-closure cost estimate for
the facility, prepared in accordance with 35 Ill. Adm. Code
724.244, plus a copy of the documentation required to demonstrate
financial assurance under 35 Ill. Adm. Code 724.245. For a new
facility, a copy of the required documentation may be submitted 60
days prior to the initial receipt of hazardous wastes, if it is
later than the submission of the Part B permit application;
q)
Where applicable, a copy of the insurance policy or other
documentation which comprises compliance with the requirements of
35 Ill. Adm. Code 724.247. For a new facility, documentation
showing the amount of insurance meeting the specification of 35
Ill. Adm. Code 724.247(a) and, if applicable, 35 Ill. Adm. Code
724.247(b) that the owner or operator plans to have in effect
before initial receipt of hazardous waste for treatment, storage,
or disposal. A request for an alternative level of required
coverage for a new or existing facility may be submitted as
specified in 35 Ill. Adm. Code 724.247(c);
r)
A topographic map showing a distance of 1000 feet around the
facility at a scale of 2.5 centimeters (1 inch) equal to not more
than 61.0 meters (200 feet). Contours must be shown on the map.
The contour interval must be sufficient to clearly show the
pattern of surface water flow in the vicinity of and from each
operational unit of the facility. For example, contours with an
interval of 1.5 meters (5 feet), if relief is greater than 6.1
meters (20 feet), or an interval of 0.6 meters (2 feet), if relief
is less than 6.1 meters (20 feet). Owners and operators of HWM
facilities located in mountainous areas shall use larger contour
intervals to adequately show topographic profiles of facilities.
The map must clearly show the following:
1)
Map scale and date;
2)
100-year floodp lain area;
3)
Surface waters including intermittent streams;
4)
Surrounding land uses (e.g., residential, commercial,
agricultural, recreational, etc.);
5)
A wind rose (i.e., prevailing windspeed and direction);
6)
Orientation of the map (north arrow);
7)
Legal boundaries of the HWM facility site;
8)
Access control (e.g., fences, gates, etc.);
17
9)
Injection and withdrawal wells both on-site and off-site;
10)
Buildings; treatment, storage, or disposal operations; or
other structures (e.g., recreation areas, runoff control
systems, access and internal roads, storm, sanitary and
process sewage systems, loading and unloading areas, fire
control facilities, etc.);
11)
Barriers for drainage or flood control;
12)
Location of operational units within the HWM facility site,
where hazardous waste is (or will be) treated, stored, or
disposed (include equipment cleanup areas);
BOARD NOTE: For large HWM facilities, the Agency shall
allow the use of other scales on a case by case basis.
s)
Applicants shall submit such information as the Agency determines
is necessary for it to determine whether to issue a permit and
what conditions to impose in any permit issued; and
t)
For land disposal facilities, if a case-by-case extension has been
approved under 35 Ill. Adm. Code 728.105 or if a petition has been
approved under 35 Ill. Adm. Code 728.106, a copy of the notice of
approval of the extension or of approval of the petition is
required.
u)
A summary of the pre
-application meeting, along
with a list of
attendees and their addresses, and copies of any written comments
or materials submitted at the meeting, as required under 35 Ill.
Adm. Code 703.191(c).
BOARD NOTE: Derived from 40 CFR 270.14(b) (199
46), as amended at
5961 Fed. Reg. 6295259996 (Dec. 6, 1994 Nov. 25, 1996 ).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 703.191
Public Participation: Pre-Application Public Notice and
Meeting
a)
Applicability. The requirements of this Section shall apply to
any RCRA Part B application seeking an initial permit for a
hazardous waste management unit. The requirements of this Section
shall also apply to any RCRA Part B application seeking renewal of
a permit for such a unit, where the renewal application is
proposing a significant change in facility operations. For the
purposes of this Section, a "significant change" is any change
that would qualify as a class 3 permit modification under Sections
703.283 and 703.Appendix A. The requirements of this Section do
not apply to permit modifications under Sections 703.280 through
703.283 or to applications that are submitted for the sole purpose
of conducting post
-closure activities or post
-closure activities
and corrective action at a facility.
b)
Prior to the submission of a RCRA Part B permit application for a
facility, the applicant must hold at least one meeting with the
public in order to solicit questions from the community and inform
the community of its proposed hazardous waste management
activities. The applicant shall post a sign
-in sheet or otherwise
provide a voluntary opportunity for attendees to provide their
names and addresses.
18
c)
The applicant shall submit to the Agency, as part of its RCRA Part
B permit application, a summary of the meeting, along with the
list of attendees and their addresses developed under subsection
(b) above and copies of any written comments or materials
submitted at the meeting, in accordance with Section 703.183.
d)
The applicant must provide public notice of the pre
-application
meeting at least 30 days prior to the meeting. The applicant must
maintain documentation of the notice, and provide that
documentation to the permitting agency upon request.
1)
The applicant shall provide public notice in each of the
following forms:
A)
A newspaper advertisement. The applicant shall
publish a notice in a newspaper of general circulation
in the county that hosts the proposed location of the
facility. The notice must fulfill the requirements
set forth in subsection (d)(2) below. In addition,
the Agency shall instruct the applicant to publish the
notice in newspapers of general circulation in
adjacent counties, where the Agency determines that
such publication is necessary to inform the affected
public. The notice must be published as a display
advertisement.
B)
A visible and accessible sign. The applicant shall
post a notice on a clearly marked sign at or near the
facility. The notice must fulfill the requirements
set forth in subsection (d)(2) below. If the
applicant places the sign on the facility property,
then the sign must be large enough to be readable from
the nearest point where the public would pass by the
site.
C)
A broadcast media announcement. The applicant shall
broadcast a notice at least once on at least one local
radio station or television station. The notice must
fulfill the requirements set forth in subsection
(d)(2) below. The applicant may employ another medium
with prior approval of the Agency.
D)
A notice to the Agency. The applicant shall send a
copy of the newspaper notice to the permitting agency
and to the appropriate units of State and local
government, in accordance with Section 705.163(a).
2)
The notices required under subsection (d)(1) above must
include:
A)
The date, time, and location of the meeting;
B)
A brief description of the purpose of the meeting;
C)
A brief description of the facility and proposed
operations, including the address or a map (e.g., a
sketched or copied street map) of the facility
location;
D)
A statement encouraging people to contact the facility
19
at least 72 hours before the meeting if they need
special access to participate in the meeting; and
E)
The name, address, and telephone number of a contact
person for the applicant.
BOARD NOTE: Derived from 40 CFR 124.31 (1996).
Source: Added at 21 Ill. Reg. ________, effective ____________________)
Section 703.192
Public Participation: Public Notice of Application
a)
Applicability. The requirements of this Section shall apply to
any RCRA Part B application seeking an initial permit for a
hazardous waste management unit. The requirements of this Section
shall also apply to any RCRA Part B application seeking renewal of
a permit for such a unit under 35 Ill. Adm. Code 702.125. The
requirements of this Section do not apply to permit modifications
under Sections 703.280 through 703.283 or a permit application
submitted for the sole purpose of conducting post
-closure
activities or post
-closure activities and corrective acti
on at a
facility.
b)
Notification at application submittal.
1)
The Agency shall provide public notice as set forth in
Section 35 Ill. Adm. Code 705.161, and notice to appropriate
units of State and local government as set forth in that
Section, that a Part B permit application has been submitted
to the Agency and is available for review.
2)
The notice shall be published within 10 calendar days after
the application is received by the Agency. The notice must
include:
A)
The name and telephone number of the applicant's
contact person;
B)
The name and telephone number of the appropriate
Agency regional office, as directed by the Agency, and
a mailing address to which information, opinions, and
inquiries may be directed throughout the permit review
process;
C)
An address to which people can write in order to be
put on the facility mailing list;
D)
The location where copies of the permit application
and any supporting documents can be viewed and copied;
E)
A brief description of the facility and proposed
operations, including the address or a map (e.g., a
sketched or copied street map) of the facility
location on the front page of the notice; and
F)
The date that the application was submitted.
c)
Concurrent with the notice required under subsection (b) above,
the Agency shall place the permit application and any supporting
documents in a location accessible to the public in the vicinity
of the facility or at the Agency regional office appropriate for
20
the facility.
BOARD NOTE: Derived from 40 CFR 124.32 (1996).
Source: Added at 21 Ill. Reg. ________, effective ____________________)
Section 703.193
Public Participation: Information Repository
a)
Applicability. The requirements of this Section shall apply to
any application seeking a RCRA permit for a hazardous waste
management unit.
b)
The Agency shall assess the need for an information repository on
a case -by-case basis. When assessing the need for an information
repository, the Agency shall consider a variety of factors,
including the following: the level of public interest; the type
of facility; the presence of an existing repository; and the
proximity to the nearest copy of the administrative record. If
the Agency determines, at any time after submittal of a permit
application, that there is a need for a repository, then the
Agency shall notify the facility that it must establish and
maintain an information repository. (See Section 703.248 for
similar provisions relating to the information repository during
the life of a permit).
c)
The information repository must contain all documents, reports,
data, and information deemed necessary by the Agency to fulfill
the purposes for which the repository is established. The Agency
will have the discretion to limit the contents of the repository.
d)
The information repository must be located and maintained at a
site chosen by the facility. If the Agency determines that the
chosen site unsuitable for the purposes and persons for which it
was established, due to problems with the location, hours of
availability, access, or other relevant considerations, then the
Agency shall specify a more appropriate site.
e)
The Agency shall specify requirements for the applicant for
informing the public about the information repository. At a
minimum, the Agency shall require the facility to provide a
written notice about the information repository to all individuals
on the facility mailing list.
f)
The facility owner or operator shall be responsible for
maintaining and updating the repository with appropriate
information throughout a time period specified by the Agency. The
Agency may close the repository if it determines that the
repository is no longer needed based on its consideration of the
factors in subsection (b) above.
BOARD NOTE: Derived from 40 CFR 124.33 (1996).
Source: Added at 21 Ill. Reg. ________, effective ____________________)
Section 703.213
Air Emission Controls for Tanks, Surface Impoundments, and
Containers
Except as otherwise provided in 35 Ill. Adm. Code 724.101, owners and
operators of tanks, surface impoundments, or containers that use air emission
controls in accordance with the requirements of 35 Ill. Adm. Code 724.Subpart
CC shall provide the following additional information:
21
a)
Documentation for each
floating roof cover installed on a tank
subject to 35 Ill. Adm. Code 724.984
(b)(2) or 724.984(b)(3)
(d)(1)
or (d)(2) that includes information prepared by the owner or
operator or provided by the cover manufacturer or vendor
describing the cover design, and certification by the owner or
operator that the cover meets the applicable design
specifications , as listed in 35 Ill. Adm. Code 725.991
(c)(e)(1) or
(f)(1) .
b)
Identification of each container area subject to the requirements
of 35 Ill. Adm. Code 724.Subpart CC and certification by the owner
or operator that the requirements of this Subpart are met.
c)
Documentation for each enclosure used to control air
pollutant
emissions from containers in accordance with the requirements of
35 Ill. Adm. Code
724.984(d)(5) or
724.986 (b)(2)(A) (e)(1)(ii) that
includes information prepared by the owner or operator or provided
by the manufacturer or vendor describing the enclosure design, and
certification by the owner or operator that the enclosure meets
the specifications listed in 35 Ill. Adm. Code
725.987(b)(2)(B) records for the most recent set of calculations
and measurements performed by the owner or operator to verify that
the enclosure meets the criteria of a permanent total enclosure,
as specified in "Procedure T
--Criteria for and Verification of a
Permanent or Temporary Total Enclosure" under 40 CFR 52.741,
appendix B, incorporated by reference in 35 Ill. Adm. Code
720.111 .
d)
Documentation for each floating membrane cover installed on a
surface impoundment in accordance with the requirements of 35 Ill.
Adm. Code 724.985(c) that includes information prepared by the
owner or operator or provided by the cover manufacturer or vendor
describing the cover design, and certification by the owner or
operator that the cover meets the specifications listed in 35 Ill.
Adm. Code 725.986(e) 264.985(c)(1) .
e)
Documentation for each closed-vent system and control device
installed in accordance with the requirements of 35 Ill. Adm. Code
724.987 that includes design and performance information
, as
specified in Section 703.124(c) and (d).
f)
An emission monitoring plan for both Method 21
in 40 CFR 60,
appendix A, incorporated by reference in 35 Ill. Adm. Code
720.111, and control device monitoring methods. This plan must
include the following information: monitoring points, monitoring
methods for control devices, monitoring frequency, procedures for
documenting exceedances, and procedures for mitigating
noncompliances.
g)
When an owner or operator of a facility subject to 35 Ill. Adm.
Code 725.Subpart CC cannot comply with 35 Ill. Adm. Code
724.Subpart CC by the date of permit issuance, the schedule of
implementation required under 35 Ill. Adm. Code 725.982.
BOARD NOTE: Derived from 40 CFR 270.27
(a), added at 59 Fed. Reg.
62952 (Dec. 6, 1994)
(1996), as amended at 61 Fed. Reg. 59996
(Nov. 25, 1996) .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
22
SUBPART E: SHORT TERM AND PHASED PERMITS
Section 703.221
Emergency Permits
a)
Notwithstanding any other provision of this Part or 35 Ill. Adm.
Code 702 or 705, in the event that the Agency finds an imminent
and substantial endangerment to human health or the environment
the Agency may issue a temporary emergency permit:
1)
To a non -permitted facility to allow treatment, storage or
disposal of hazardous waste; or
2)
To a permitted facility to allow treatment, storage or
disposal of a hazardous waste not covered by an effective
permit.
b)
This emergency permit:
1)
May be oral or written. If oral, it must be followed in
five days by a written emergency permit;
2)
Shall not exceed 90 days in duration;
3)
Shall clearly specify the hazardous wastes to be received
and the manner and location of their treatment, storage or
disposal;
4)
May be terminated by the Agency at any time without process
if it determines that termination is appropriate to protect
human health and the environment;
5)
Shall be accompanied by a public notice published under 35
Ill. Adm. Code 705.162 including:
A)
Name and address of the office granting the emergency
authorization;
B)
Name and location of the permitted HWM facility;
C)
A brief description of the wastes involved;
D)
A brief description of the action authorized and
reasons for authorizing it; and
E)
Duration of the emergency permit; and
6)
Shall incorporate, to the extent possible and not
inconsistent with the emergency situation, all applicable
requirements of this Part and 35 Ill. Adm. Code 724.
7)
Emergency permits which would authorize actions not in
compliance with Board rules, other than procedural
requirements, require a variance or provisional variance
pursuant to Title IX of the Environmental Protection Act and
35 Ill. Adm. Code 104.
(Board Note BOARD NOTE : SeeDerived from 40 CFR 270.61
(1996) .)
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
23
Section 703.223 Incinerator Conditions During Trial Burn
For the purposes of determining feasibility of compliance with the performance
standards of 35 Ill. Adm. Code 724.443 and of determining adequate operating
conditions under 35 Ill. Adm. Code 724.445, the Agency shall establish
conditions in the permit to a new hazardous waste incinerator to be effective
during the trial burn.
a)
Applica nts shall propose a trial burn plan, prepared under
subsection (b) below with Part B of the permit application;
b)
The trial burn plan must include the following information:
1)
An analysis of each waste or mixture of wastes to be burned
that includes:
A)
Heat value of the waste in the form and composition in
which it will be burned;
B)
Viscosity (if applicable), or description of physical
form of the waste;
C)
An identification of any hazardous organic
constituents listed in 35 Ill. Adm. Code 721.Appendix
H, that are present in the waste to be burned, except
that the applicant need not analyze for constituents
listed in 35 Ill. Adm. Code 721.Appendix H that would
reasonably not be expected to be found in the waste.
The constituents excluded from analysis must be
identified, and the basis for their exclusion stated.
The waste analysis must rely on analytical techniques
specified in "Test Methods for the Evaluation of Solid
Waste, Physical/Chemical Methods", U
.S. EPA
Publication SW-846, as incorporated by reference at 35
Ill. Adm. Code 720.111 and Section 703.110, or their
equivalent;
D)
An approximate quantification of the hazardous
constituents identified in the waste, within the
precision produced by the analytical methods specified
in "Test Methods for the Evaluation of Solid Waste,
Physical/Chemical Methods", U
.S. EPA Publication SW-
846, as incorporated by reference at 35 Ill. Adm. Code
720.111 and Section 703.110, or their equivalent;
2)
A detailed engineering description of the i
ncinerator for
which the permit is sought including:
A)
Manufacturer's name and model number of incinerator
(if available);
B)
Type of incinerator;
C)
Linear dimensions of the incinerator unit including
the cross sectional area of combustion chamber;
D)
Description of the auxiliary fuel system (type/feed);
E)
Capacity of prime mover;
24
F)
Description of automatic waste feed cut
-off system(s);
G)
Stack gas monitoring and pollution control equipment;
H)
Nozzle and burner design;
I)
Construction materials;
J)
Location and description of temperature, pressure and
flow indicating and control devices;
3)
A detailed description of sampling and monitoring
procedures, including sampling and monitoring locations in
the system, the equipment to be used, sampling and
monitoring frequency and planned analytical procedures for
sample analysis;
4)
A detailed test schedule for each waste for which the trial
burn is planned including date(s), duration, quantity of
waste to be burned and other factors relevant to the
Agency's decision under subsection (e) below;
5)
A detailed test protocol, including, for each waste
identified, the ranges of temperature, waste feed rate,
combustion gas velocity, use of auxiliary fuel and any other
relevant parameters that will be varied to affect the
destruction and removal efficiency of the incinerator;
6)
A description of, and planned operating conditions for, any
emission control equipment that will be used;
7)
Procedures for rapidly stoppi
ng waste feed, shutting down
the incinerator and controlling emissions in the event of an
equipment malfunction;
8)
Such other information as the Agency reasonably finds
necessary to determine whether to approve the trial burn
plan in light of the purposes of this subsection and the
criteria in subsection (e) below. Such information must be
requested by the Agency pursuant to 35 Ill. Adm. Code
705.123.
c)
The Agency, in reviewing the trial burn plan, shall evaluate the
sufficiency of the information provided and shall require the
applicant, pursuant to 35 Ill. Adm. Code 705.123, to supplement
this information, if necessary, to achieve the purposes of this
subsection;
d)
Based on the waste analysis data in the trial burn plan, the
Agency shall specify as trial Principal Organic Hazardous
Constituents (POHCs), those constituents for which destruction and
removal efficiencies must be calculated during the trial burn.
These trial POHCs must be specified by the Agency based on its
estimate of the difficulty of incineration of the constituents
identified in the waste analysis, their concentration or mass in
the waste feed, and, for wastes listed in 35 Ill. Adm. Code
721.Subpart D, the hazardous waste organic constituent of
constituents identified in 35 Ill. Adm. Code 721.Appendix G or H
as the basis for listing;
e)
The Agency shall approve a trial burn plan if it finds that:
25
1)
The trial burn is likely to determine whether the
incinerator performance standard required by 35 Ill. Adm.
Code 724.443 can be met;
2)
The trial burn itself will not present an imminent hazard to
human health or the environment;
3)
The trial burn will help the Agency to determine operating
requirements to be specified under 35 Ill. Adm. Code
724.445; and
4)
The information sought in subsections (e)(1) and (e)(3)
above cannot reasonably be developed through other means;
f)
The Agency shall send a notice to all persons on the facility
mailing list, as set forth in 35 Ill. Adm. Code 705.161(a), and to
the appropriate units of State and local government, as set forth
in that Section, announcing the scheduled commencement and
completion dates for the trial burn. The applicant may not
commence the trial burn until after the Agency has issued such
notice.
1)
This notice must be mailed within a reasonable time period
before the scheduled trial burn. An additional notice is
not required if the trial burn is delayed due to
circumstances beyond the control of the facility or the
Agency.
2)
This notice must contain:
A)
The name and telephone number of the applicant's
contact person;
B)
The name and telephone number of the Agency regional
office appropriate for the facility;
C)
The location where the approved trial burn plan and
any supporting documents can be reviewed and copied;
and
D)
An expected time period for commencement and
completion of the trial burn.
fg)
During each approved trial burn (or as soon after the burn as is
practicable), the applicant shall make the following
determinations:
1)
A quanti tative analysis of the trial POHCs, in the waste
feed to the incinerator;
2)
A quantitative analysis of the exhaust gas for the
concentration and mass emissions of the trial POHC's,
molecular oxygen and hydrogen chloride (HCl);
3)
A quantitative analysis of the scrubber water (if any), ash
residues and other residues, for the purpose of estimating
the fate of the trial POHCs;
4)
A computation of destruction and removal efficiency (DRE),
in accordance with the DRE formula specified in 35 Ill. Adm.
26
Code 724.443(a);
5)
If the HCl (hydrogen chloride) emission rate exceeds 1.8
kilograms of HCl per hour (4 pounds per hour), a computation
of HCl removal efficiency in accordance with 35 Ill. Adm.
Code 724.443(b);
6)
A computation of particulate emissions, in accordance with
35 Ill. Adm. Code 724.443(c);
7)
An identification of sources of fugitive emissions and their
means of control;
8)
A measurement of average, maximum and minimum temperatures
and combustion gas velocity;
9)
A continuous meas
urement of carbon monoxide (CO) in the
exhaust gas;
10)
Such other information as the Agency specifies as necessary
to ensure that the trial burn will determine compliance with
the performance standards in 35 Ill. Adm. Code 724.443 and
to establish the operating conditions required by 35 Ill.
Adm. Code 724.445 as necessary to meet that performance
standard.
gh)
The applicant shall submit to the Agency a certification that the
trial burn has been carried out in accordance with the approved
trial burn plan, and shall submit the results of all the
determinations required in subsection (f) above. This submission
must be made within 90 days of completion of the trial burn, or
later if approved by the Agency;
hi)
All data collected during any trial burn must be submitted to the
Agency following the completion of the trial burn;
ij)
All submissions required by this subsection must be certified on
behalf of the applicant by the signature of a person authorized to
sign a permit application or a report under 35 Ill. Adm. Code
702.126;
jk)
Based on the results of the trial burn, the Agency shall set the
operating requirements in the final permit according to 35 Ill.
Adm. Code 724.445. The permit modification must proceed as a
minor modification according to Section 703.280.
BOARD NOTE: Derived from 40 CFR 270.62(
ab)(19), as amended at 58
Fed. Reg. 46051 (Aug. 31, 1993)
(1996) .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 703.225
Trial Burns for Existing Incinerator
s
For the purpose of determining feasibility of compliance with the performance
standards of 35 Ill. Adm. code 724.443 and of determining adequate operating
conditions under 35 Ill. Adm. Code 724.445, the applicant for a permit for an
existing hazardous waste incinerator shall prepare and submit a trial burn
plan and perform a trial burn in accordance with Sections 703.205(b) and
703.223(b) through (
ie) and (g) through (j)
, or, instead, submit other
information as specified in Section 703.205(c).
The Agency shall announce its
intention to approve the trial burn plan in accordance with the timing and
27
distribution requirements of Section 703.223(f). The contents of the notice
must include: the name and telephone number of a contact person at the
facility; the name and telephone number of a contact office at the Agency; the
location where the trial burn plan and any supporting documents can be
reviewed and copied; and a schedule of the activities that are required prior
to permit issuance, including the anticipated time schedule for Agency
approval of the plan and the time period during which the trial burn would be
conducted. Applicants submitting information under Section 703.205(a) are
exempt from compliance with 35 Ill. Adm. Code 724.443 and 724.445 and,
therefore, are exempt from the requirement to conduct a trail burn.
Applicants whothat submit trial burn plans and receive approval before
submission of a permit application shall complete the trial burn and submit
the results, specified in Section 703.223(
fg), with Part B of the permit
application. If completion of this process conflicts with the date set for
submission of the Part B application, the applicant shall contact the Agency
to establish a later date for submission of the Part B application or the
trial burn results. Trial burn results must be submitted prior to issuance of
the permit. When the applicant submits a trail burn plan with Part B of the
permit application, the Agency shall specify a time period prior to permit
application, the Agency shall specify a time period prior to permit issuance
in which the trial burn must be conducted and the results submitted.
(Board Note BOARD NOTE : Derived from 40 CFR 270.62(d) (19
8896), as amended at
54 Fed. Reg. 4288, January 30, 1989
.)
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 703.232
Permits for Boilers and Industrial Furnaces Burning
Hazardous Waste
a)
General. Owners and operators of new boilers and industrial
furnaces (those not operating under the interim status standards
of 35 Ill. Adm. Code 726.203) are subject to subsection (b)
through (f) below. Boilers and industrial furnaces operating
under the interim status standards of 35 Ill. Adm. Code 726.203
are subject to subsection (g) below.
b)
Permit operating periods for new boilers and industrial furnaces.
A permit for a new boiler or industrial furnace must specify
appropriate conditions for the following operating periods:
1)
Pretrial burn period. For the period beginning with initial
introduction of hazardous waste and ending with initiation
of the trial burn, and only for the minimum time required to
bring the boiler or industrial furnace to a point of
operation readiness to conduct a trial burn, not to exceed
720 hours operating time when burning hazardous waste, the
Agency shall establish in the Pretrial Burn Period of the
permit conditions, including but not limited to allowable
hazardous waste feed rates and operating conditions. The
Agency shall extend the duration of this operational period
once, for up to 720 additional hours, at the request of the
applicant when good cause is shown. The permit most be
modified to reflect the extension according to Section
703.280 et seq.
A)
Applicants must submit a statement, with part B of the
permit application, that suggests the conditions
necessary to operate in compliance with the standards
of 35 Ill. Adm. Code 726.204 through 726.207 during
28
this period. This statement should include, at a
minimum, restrictions on the applicable operating
requirements identified in 35 Ill. Adm. Code 726.202
(e).
B)
The Agency shall review this statement and any other
relevant information submitted with part B of the
permit application and specify requirements for this
period sufficient to meet the performance standards of
35 Ill. Adm. Code 726.204 through 726.207 based on the
Agency's engineering judgment.
2)
Trial burn period. For the duration of the trial burn, the
Agency shall establish conditions in the permit for the
purposes of determining feasibility of compliance with the
performance standards of 35 Ill. Adm. Code 726.204 through
726.207 and determining adequate operating conditions under
35 Ill. Adm. Code 726.202(e). Applicants shall propose a
trial burn plan, prepared under subsection (c) below, to be
submitted with part B of the permit application.
3)
Post-trial burn period.
A)
For the period immediately following completion of the
trial burn, and only for the minimum period sufficient
to allow sample analysis, data computation and
submission of the trial burn results by the applicant,
and review of the trial burn results and modification
of the facility permit by the Agency to reflect the
trial burn results, the Agency shall establish the
operating requirements most likely to ensure
compliance with the performance standards of 35 Ill.
Adm. Code 726.204 through 726.207 based on the
Agency's engineering judgment.
B)
Applicants shall submit a statement, with part B of
the application, that identifies the conditions
necessary to operate during this period in compliance
with the performance standards of 35 Ill. Adm. Code
726.204 through 726.207. This statement should
include, at a minimum, restrictions on the operating
requirements provided by 35 Ill. Adm. Code 726.202
(e).
C)
The Agency shall review this statement and any other
relevant information submitted with part B of the
permit application and specify requirements of this
period sufficient to meet the performance standards of
35 Ill. Adm. Code 726.204 through 726.207 based on the
Agency's engineering judgment.
4)
Final permit period. For the final period of operation the
Agency shall develop operating requirements in conformance
with 35 Ill. Adm. Code 726.202(e) that reflect conditions in
the trial burn plan and are likely to ensure compliance with
the performance standards of 35 Ill. Adm. Code 726.204
through 726.207. Based on the trial burn results, the
Agency shall make any necessary modifications to the
operating requirements to ensure compliance with the
performance standards. The permit modification must proceed
according to Section 703.280 et seq.
29
c)
Requirements for trial burn plans. The trial burn plan must
include the following information. The Agency, in reviewing the
trial burn plan, shall evaluate the sufficiency of the information
provided and may require the applicant to supplement this
information, if necessary, to achieve the purposes of this
subsection.
1)
An analysis of each feed stream, including hazardous waste,
other fuels, and industrial furnace feed stocks, as fired,
that includes:
A)
Heating value, levels of antimony, arsenic, barium,
beryllium, cadmium, chromium, lead, mercury, silver,
thallium, total chlorine/chloride
, and ash;
B)
Viscosity or description of the physical form of the
feed stream;
2)
An analysis of each hazardous waste, as fired, including:
A)
An identification of any hazardous organic
constituents listed in 35 Ill. Adm. Code 721.Appendix
H that are present in the feed stream, except that
the applicant need not analyze for constituents listed
in 35 Ill. Adm. Code 721.Appendix H that would
reasonably not be expected to be found in the
hazardous waste. The constituents excluded from
analysis must be identified as the basis for this
exclusion explained. The analysis must be conducted
in accordance with analytical techniques specified in
"Test Methods for the Evaluation of Solid Waste,
Physical/Chemical Methods", U
.S. EPA Publication SW-
846, as incorporated by reference at 35 Ill. Adm. Code
720.111 and Section 703.110, or their equivalent.
B)
An approximate quantification of the hazardous
constituents identified in the hazardous waste, within
the precision produced by the analytical methods
specified in "Test Methods for the Evaluation of Solid
Waste, Physical/Chemical Methods", U
.S. EPA
Publication SW-846, as incorporated by reference at 35
Ill. Adm. Code 720.111 and Section 703.110, or other
equivalent.
C)
A description of blending procedures, if applicable,
prior to firing the hazardous waste, including a
detailed analysis of the hazardous waste prior to
blending, an analysis of the material with which the
hazardous waste prior to blending, an analysis of the
material with which the hazardous waste is blended,
and blending ratios.
3)
A detailed engineering description of the boiler or
industrial furnace, including:
A)
Manufacturer's name and model number of the boiler or
industrial furnace;
B)
Type of boiler or industrial furnace;
30
C)
Maximum design capacity in appropriate units;
D)
Descript ion of the Feed system for the hazardous
waste, and, as appropriate, other fuels and industrial
furnace feedstocks;
E)
Capacity of hazardous waste feed system;
F)
Description of automatic hazardous waste feed cutoff
system(s); and
G)
Description of any pollution control system; and
H)
Description of stack gas monitoring and any pollution
control monitoring systems.
4)
A detailed description of sampling and monitoring procedures
including sampling and monitoring locations in the system,
the equipment to be used, sampling and monitoring frequency
,
and sample analysis.
5)
A detailed test schedule for each hazardous waste for which
the trial burn is planned, including date(s), duration,
quantity of hazardous waste to be burned, and other factors
relevant to the Agency's decision under subsection (b)(2)
above.
6)
A detailed test protocol, including, for each hazardous
waste identified, the ranges of hazardous waste feed rate,
and, as appropriate, the feed rates of other fuels and
industrial furnace feedstocks, and any other relevant
parameters that may affect the ability of the boiler or
industrial furnace to meet the performance standards in 35
Ill. Adm. Code 726.204 through 726.207.
7)
A description of and planned operating conditions for any
emission control equipment that will be used.
8)
Procedures for rapidly stopping the hazardous waste feed and
controlling emissions in the event of an equipment
malfunction.
9)
Such other information as the Agency finds necessary to
determine whether to approve the trial burn plan in light of
the purposes of this subsection and the criteria in
subsection (b)(2) above.
d)
Trial burn procedures.
1)
A trial burn must be conducted to demonstrate conformance
with the standards of 35 Ill. Adm. Code 726.104 through
726.107.
2)
The Agency shall approve a trial burn plan if the Agency
finds that:
A)
The trial burn is likely to determine whether the
boiler or industrial furnace can meet the performance
standards of 35 Ill. Adm. Code 726.104 through
726.107.
31
B)
The trial burn itself will not present an imminent
hazard to human health and the environment;
C)
The trial burn will help the Agency to determine
operating requirements to be specified under 35 Ill.
Adm. Code 726.102(e); and
D)
The information sought in the trial burn cannot
reasonably be developed through other means.
3)
The Agency shall send a notice to all persons on the
facility mailing list, as set forth in 35 Ill. Adm. Code
705.161(a), and to the appropriate units of State and local
government, as set forth in that Section, announcing the
scheduled commencement and completion dates for the trial
burn. The applicant may not commence the trial burn until
after the Agency has issued such notice.
A)
This notice must be mailed within a reasonable time
period before the trial burn. An additional notice is
not required if the trial burn is delayed due to
circumstances beyond the control of the facility or
the Agency.
B)
This notice must contain:
i)
The name and telephone number of applicant's
contact person;
ii)
The name and telephone number of the Agency
regional office appropriate for the facility;
iii)
The location where the approved trial burn plan
and any supporting documents can be reviewed and
copied; and
iv)
An expected time period for commencement and
completion of the trial burn.
34)
The applicant shall submit to the Agency a certification
that the trial burn has been carried out in accordance with
the approved trial burn plan, and submit the results of all
the determinations required in subsection (c) above. The
Agency shall, in the trial burn plan, require that the
submission be made within 90 days after completion of the
trial burn, or later if the Agency determines that a later
date is acceptable.
45)
All data collected during any trial burn must be submitted
to the Agency following completion of the trial burn.
56)
All submissions required by this subsection must be
certified on behalf of the applicant by the signature of a
person authorized to sign a permit application or a report
under 35 Ill. Adm. Code 702.126.
e)
Special procedures for DRE trial burns. When a DRE trial burn is
required under 35 Ill. Adm. Code 726.104, the Agency shall specify
(based on the hazardous waste analysis data and other information
in the trial burn plan) as trial Principal Organic Hazardous
Constituents (POHCs) those compounds for which destruction and
32
removal efficiencies must be calculated during the trial burn.
These trial POHCs will be specified by the Agency based on
information including the Agency's estimate of the difficulty of
destroying the constituents identified in the hazardous waste
analysis, their concentrations or mass in the hazardous waste
feed, and, for hazardous waste containing or derived from wastes
listed in 35 Ill. Adm. Code 721.Subpart D, the hazardous waste
organic constituent(s) identified in 35 Ill. Adm. Code
721.Appendix G as the basis for listing.
f)
Determinations based on trial burn. During each approved trial
burn (or as soon after the burn as is practicable), the applicant
shall make the following determinations:
1)
A quantitative analysis of the levels of antimony, arsenic,
barium, beryllium, cadmium, chromium, lead, mercury,
thallium, silver, and chlorine/chloride
, in the feed streams
(hazardous waste, other fuels, and industrial furnace
feedstocks);
2)
When a DRE trial burn is required under 35 Ill. Adm. Code
726.204(a):
A)
A quantitative analysis of the trial POHCs in the
hazardous waste feed;
B)
A quantitative analysis of the stack gas for the
concentration and mass emissions of the trial POHCs;
and
C)
A computation of (DRE), in accordance with the DRE
formula specified in 35 Ill. Adm. Code 726.204(a).
3)
When a trial burn for chlorinated dioxins and furans is
required under 35 Ill. Adm. Code 726.204(e), a quantitative
analysis of the stack gas for the concentration and mass
emission rate of the 2,3,7,8-chlorinated tetra-octa
congeners of chlorinated dibenzo-p-dioxins and furans, and a
computation showing conformance with the emission standard.
4)
When a trial burn for PM, metals, or HCl/Chlorine gas is
required under 35 Ill. Adm. Code 726.205, 726.206(c) or (d)
or 726.207(b)(2) or (c), a quantitative analysis of the
stack gas for the concentrations and mass emissions of PM,
metals, or HCl and chlorine gas and computations showing
conformance with the applicable emission performance
standards;
5)
When a trial burn for DRE, metals, and HCl/Chlorine gas is
required under 35 Ill. Adm. Code 726.204(a), 726.206(c) or
(d), or 726.207(b)(2) or (c), a quantitative analysis of the
scrubber water (if any), ash residues, other residues, and
products for the purpose of estimating the fate of the trial
POHCs, metals, and chlorine/chloride;
6)
An identification of sources of fugitive emissions and their
means of control;
7)
A continuous measurement of carbon monoxide (CO), oxygen,
and, where required, hydrocarbons (HC), in the stack gas;
and
33
8)
Such other information as the Agency specifies
as necessary
to ensure that the trial burn will determine compliance with
the performance standards 35 Ill. Adm. Code 726.204 through
726.207 and to establish the operating conditions required
by 35 Ill. Adm. Code 726.204 through 726.207 and of
determining adequate operating conditions under 35 Ill. Adm.
Code 726.203, and to establish the operating conditions
required by 35 Ill. Adm. Code 726.202(e) as necessary to
meet those performance standards.
g)
Interim status boilers and industrial furnaces. for
the purpose
of determining feasibility of compliance with the performance
standards of 35 Ill. Adm. Code 726.204 through 726.207 and of
determining adequate operating conditions under 35 Ill. Adm. Code
726.203, applicants owning or operating existing boilers or
industrial furnaces operated under the interim status standards of
35 Ill. Adm. Code 726.203 shall either prepare and submit a trial
burn plan and perform a trial burn in accordance with the
requirements of the Section or submit other information as
specified in Section 703.208(a)(6).
The Agency shall announce its
intention to approve of the trial burn plan in accordance with the
timing and distribution requirements of subsection (d)(3) above.
The contents of the notice must include: the name and telephone
number of a contact person at the facility; the name and telephone
number of Agency regional office appropriate for the facility; the
location where the trial burn plan and any supporting documents
can be reviewed and copied; and a schedule of the activities that
are required prior to permit issuance, including the anticipated
time schedule for agency approval of the plan and the time periods
during which the trial burn would be conducted.
Applicants that
submit a trial burn plan and receive approval before submission of
the part B permit application shall complete the trial burn and
submit the results specified in subsection (f) above with the part
B permit application. If completion of this process conflicts
with the date set for submission of the part B application, the
applicant shall contact the Agency to establish a later date for
submission of the part B application or the trial burn results.
If the applicant submits a trial burn plan with part B of the
permit application, the trial burn must be conducted and the
results submitted within a time period prior to permit issuance to
be specified by the Agency.
BOARD NOTE: Derived from 40 CFR 270.66 (199
26), as amended at 58
Fed. Reg. 46051 (Aug. 31, 1993)
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART F: PERMIT CONDITIONS OR DENIAL
Section 703.240
Permit Denial
The Agency may, pursuant to the procedures of 35 Ill. Adm. Code 705, deny the
permit application either in its entirety or
only as to the active life of a
HWM facility or unit
only.
(Board Note BOARD NOTE : Derived from 40 CFR 270.29
(1996) , as adopted at 54
Fed. Reg. 9607, March 7, 1989.)
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
34
Section 703.248
Information Repository
The Agency may require the permittee to establish and maintain an information
repository at any time, based on the factors set forth in Section 703.193(b).
The information repository shall be governed by the provisions in Section
703.193(c) through (f).
BOARD NOTE: Derived from 40 CFR 270.30(m) (1996).
(Source: Added at 21 Ill. Reg. ________, effective ____________________)
SUBPART G: CHANGES TO PERMITS
Section 703.260
Transfer
a)
A permit may be transferred by the permittee to a ne
w owner or
operator only if the permit has been modified or reissued (under
subsection (b) or Section 703.272) to identify the new permittee
and incorporate such other requirements as are necessary under the
appropriate Act. The new owner or operator to whom the permit is
transferred shall comply with all the terms and conditions
specified in such permit.
b)
Changes in the ownership or operational control of a facility must
be made as a Class 1 modification with the prior written approval
of the Agency in accordance with Section 703.281. The new owner
or operator shall submit a revised permit application no later
than 90 days prior to the scheduled change. A written agreement
containing a specific date for transfer of permit responsibility
between the current and new permittees must also be submitted to
the Agency. When a transfer of ownership or operational control
occurs, the old owner or operator shall comply with the
requirements of 35 Ill. Adm. Code 724.Subpart H (Financial
Requirements), until the new owner or operator has demonstrated
compliance with that Subpart. The new owner or operator shall
demonstrate compliance with that Subpart within six months after
the date of change of operational control of the facility. Upon
demonstration to the Agency by the new owner or operator of
compliance with that Subpart, the Agency shall notify the old
owner or operator that the old owner or operator no longer needs
to comply with that Subpart as of the date of demonstration.
(Board Note: Derived from 4
0 CFR 270.40, as amended at 53 Fed.
Reg. 37934, September 28, 1988.)
(Board Note: The new operator may be required to employ a chief
operator whothat is certified pursuant to 35 Ill. Adm. Code 745.)
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 720
HAZARDOUS WASTE MANAGEMENT SYSTEM: GENERAL
35
SUBPART A: GE NERAL PROVISIONS
Section
720.101
Purpose, Scope and Applicability
720.102
Availability of Information; Confidentiality of Information
720.103
Use of Number and Gender
SUBPART B: DEFINITIONS
Section
720.110
Definitions
720.111
References
SUBPART C: RULEMAKING PETITIONS AND OTHER PROCEDURES
Section
720.120
Rulemaking
720.121
Alternative Equivalent Testing Methods
720.122
Waste Delisting
720.123
Petitions for Regulation as Universal Waste
720.130
Procedures for Solid Waste Determinations
720.131
Solid W aste Determinations
720.132
Boiler Determinations
720.133
Procedures for Determinations
720.140
Additional regulation of certain hazardous waste Recycling
Activities on a case-by-case Basis
720.141
Procedures for case-by-case regulation of hazardous waste
Recycling Activities
720.Appendix A
Overview of 40 CFR, Subtitle C Regulations
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
effective May 17, 1982; amended in R82-19 at 7 Ill. Reg. 14015, effective
October 12, 1983; amended in R84-9, 53 PCB 131 at 9 Ill. Reg. 11819, effective
July 24, 1985; amended in R85-22 at 10 Ill. Reg. 968, effective January 2,
1986; amended in R86-1 at 10 Ill. Reg. 13998, effective August 12, 1986;
amended in R86-19 at 10 Ill. Reg. 20630, effective December 2, 1986; amended
in R86-28 at 11 Ill. Reg. 6017, effective March 24, 1987; amended in R86-46 at
11 Ill. Reg. 13435, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg.
19280, effective November 12, 1987; amended in R87-26 at 12 Ill. Reg. 2450,
effective January 15, 1988; amended in R87-39 at 12 Ill. Reg. 12999, effective
July 29, 1988; amended in R88-16 at 13 Ill. Reg. 362, effective December 27,
1988; amended in R89-1 at 13 Ill. Reg. 18278, effective November 13, 1989;
amended in R89-2 at 14 Ill. Reg. 3075, effective February 20, 1990; amended in
R89-9 at 14 Ill. Reg. 6225, effective April 16, 1990; amended in R90-10 at 14
Ill. Reg. 16450, effective September 25, 1990; amended in R90-17 at 15 Ill.
Reg. 7934, effective May 9, 1991; amended in R90-11 at 15 Ill. Reg. 9323,
effective June 17, 1991; amended in R91-1 at 15 Ill. Reg. 14446, effective
September 30, 1991; amended in R91-13 at 16 Ill. Reg. 9489, effective June 9,
1992; amended in R92-1 at 16 Ill. Reg. 17636, effective November 6, 1992;
amended in R92-10 at 17 Ill. Reg. 5625, effective March 26, 1993; amended in
R93-4 at 17 Ill. Reg. 20545, effective November 22, 1993; amended in R93-16 at
18 Ill. Reg. 6720, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
12160, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17480,
effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9508, effective
June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10929, August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
36
SUBPART A: GENERA
L
Section 720.102
Availability of Information; Confidentiality of Information
a)
Availability and confidentiality of information is governed by
Illinois law, including Sections 7 and 7.1 of the Environmental
Protection Act (Ill. Rev. Stat. 1983, ch. 111 1/2, pars. 1007 and
1007.1) and 35 Ill. Adm. Code 101.107 and 120.
b)
Information required under 35 Ill. Adm. Code 722.153(a) and
722.183 that is submitted in a notification of intent to export a
hazardous waste will be provided to the U.S. Department of State
and the appropriate authorities in the transit and receiving or
importing countries regardless of any claims of confidentiality or
trade secret.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART B: DEFINITIONS
Section 720.111
References
a)
The following publications are incorporated by reference:
ANSI. Available from the American National Standards
Institute, 1430 Broadway, New York, New York 10018, 212-
354-3300:
ANSI B31.3 and B31.4. See ASME/AN
SI B31.3 and B31.4
ACI. Available from the American Concrete Institute, Box
19150, Redford Station, Detroit, Michigan 48219:
ACI 318-83: "Building Code Requirements for
Reinforced Concrete", adopted September, 1983.
API. Available from the American Petroleum Institute, 1220
L Street, N.W., Washington, D.C. 20005, 202-682-8000:
"Cathodic Protection of Underground Petroleum Storage
Tanks and Piping Systems", API Recommended Practice
1632, Second Edition, December, 1987.
"Evaporativ e Loss from External Floating-Roof Tanks",
API Publication 2517, Third Edition, February, 1989.
"Guide for Inspection of Refinery Equipment, Chapter
XIII, Atmospheric and Low Pressure Storage Tanks", 4th
Edition, 1981, reaffirmed December, 1987.
"Installation of Underground Petroleum Storage
Systems", API Recommended Practice 1615, Fourth
Edition, November, 1987.
APTI. Available from the Air and Waste Management
Association, Box 2861, Pittsburgh, PA 15230, 412-232-3444:
APTI Course 415: Control of Gaseous Emissions, USEPA
Publication EPA-450/2-81-005, December, 1981.
37
ASME. Available from the American Society of Mechanical
Engineers, 345 East 47th Street, New York, NY 10017, 212-
705-7722:
"Chemical Plant and Petroleum Refinery Piping",
ASME/ANSI B31.3-1987, as supplemented by B31.3a-1988
and B31.3b-1988. Also available from ANSI.
"Liquid Transportation Systems for Hydrocarbons,
Liquid Petroleum Gas, Anhydrous Ammonia, and
Alcohols", ASME/ANSI B31.4-1986, as supplemented by
B31.4a-1987. Also available from ANSI.
ASTM. Available from American Society for Testing and
Materials, 1916 Race Street, Philadelphia, PA 19103, 215-
299-5400:
ASTM C 94-90, Standard Specification for Ready-Mixed
Concrete, approved March 30, 1990.
ASTM D 88-87, Standard Test Method for Saybolt
Viscosity, April 24, 1981, reapproved January, 1987.
ASTM D 93-85, Standard Test Methods for Flash Point by
Pensky-Martens Closed Tester, approved October 25,
1985.
ASTM D 1946-90, Standard
Practice for Analysis of
Reformed Gas by Gas Chromatography, Approved March 30,
1990.
ASTM D 2161-87, Standard Practice for Conversion of
Kinematic Viscosity to Saybolt Universal or to Saybolt
Furol Viscosity, March 27, 1987.
ASTM D 2267-88, Standard Test Method for Aromatics in
Light Naphthas and Aviation Gasolines by Gas
Chromatography, approved November 17, 1988.
ASTM D 2382-88, Standard Test Method for Heat of
Combustion of Hydrocarbon Fuels by Bomb Calorimeter
(High Precision Method), approved October 31, 1988.
ASTM D 2879-86, Standard Test Method for Vapor
Pressure-Temperature Relationship and Initial
Decomposition Temperature of Liquids by Isoteniscope,
approved October 31, 1986.
ASTM D 2879-92, Standard Test Method for Vapor
Pressure-Temperature Relationship and Initial
Decomposition Temperature of Liquids by Isoteniscope,
approved 1992.
ASTM D 3828-87, Standard Test Methods for Flash Point
of Liquids by Setaflash Closed Tester, approved
December 14, 1988.
ASTM E 16 8-88, Standard Practices for General
Techniques of Infrared Quantitative Analysis, approved
May 27, 1988.
38
ASTM E 169-87, Standard Practices for General
Techniques of Ultraviolet-Visible Quantitative
Analysis, approved February 1, 1987.
ASTM E 260-85, Standard Practice for Packed Column Gas
Chromatography, approved June 28, 1985.
ASTM E 926-88 C, Standard Test Methods for Preparing
Refuse-Derived Fuel (RDF) Samples for Analysis of
Metals, Bomb-Acid Digestion Method, approved March 25,
1988.
ASTM Method G 21-70 (1984a) -- Standard Practice for
Determining Resistance of Synthetic Polymer Materials
to Fungi
ASTM Method G 22-76 (1984b) -- Standard Practice for
Determining Resistance of Plastics to Bacteria.
GPO. Available from the Superintendent of Documents, U.S.
Government Printing Office, Washington, D.C. 20402, 202-
783-3238:
Standard Industrial Classification Manual (1972), and
1977 Supplement, republished in 1983
"Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods", USEPA Publication number
SW-846 (Third Edition, November, 1986), as amended by
Updates I (July, 1992), II (September, 1994), IIA
(August, 1993), and IIB (January, 1995) (Document
Number 955-001-00000-1).
NACE. Available from the National Association of Corrosion
Engineers, 1400 South Creek Dr., Houston, TX 77084, 713-
492-0535:
"Control of External Corrosion on Metallic Buried,
Partially Buried, or Submerged Liquid Storage
Systems", NACE Recommended Practice RP0285-85,
approved March, 1985.
NFPA. Available from the National Fire Protection
Association, Batterymarch Park, Boston, MA 02269, 617-770-
3000 or 800-344-3555:
"Flammable and Combustible Liquids Code" NFPA 30,
issued July 17, 1987. Also available from ANSI.
NTIS. Available from the U.S. Department of Commerce,
National Technical Information Service, 5285 Port Royal
Road, Springfield, VA 22161, 703-487-4600:
"Generic Quality Assurance Project Plan for Land
Disposal Restrictions Program", EPA/530-SW-87-011,
March 15, 1987. (Document number PB 88-170766.)
"Guidance on Air Quality Models", Revised 1986.
(Document number PB86-245-248 (Guideline) and PB88-
150-958 (Supplement)).
39
"Methods for Chemical Analysis of Water and Wastes",
Third Edition, March, 1983. (Document number PB 84-
128677).
"Methods Manual for Compliance with BIF Regulations",
December, 1990. (Document number PB91-120-006).
"Petitions to Delist Hazardous Wastes -- A Guidance
Manual", EPA/530-SW-85-003, April, 1985. (Document
Number PB 85-194488).
"Procedures Manual for Ground Water Monitoring at
Solid Waste Disposal Facilities", EPA-530/SW-611,
1977. (Document number PB 84-174820).
"Screening Procedures for Estimating the Air Quality
Impact of Stationary Sources", October, 1992,
Publication Number EPA-450/R-92-019.
OECD. Organisation for Economic Co
-operation and
Development, Environment Direcorate, 2 rue Andre Pascal,
75775 Paris Cedex 16, France):
OECD Guideline for Testing of Chemicals, Method 301B:
"CO
2
Evolution (Modified Sturm Test)", adopted 17
July 1992.
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) of 27 May 1988.
STI. Available from the Steel Tank Institute, 728 Anthony
Trail, Northbrook, IL 60062, 708-498-1980:
"Standard for Dual Wall Underground Steel Storage
Tanks" (1986).
USEPA. Available from United States Environmental
Protection Agency, Office of Drinking Water, State Programs
Division, WH 550 E, Washington, D.C. 20460:
"Technical Assistance Docum
ent: Corrosion, Its
Detection and Control in Injection Wells", EPA 570/9-
87-002, August, 1987.
USEPA. Available from Receptor Analysis Branch, USEPA (MD-
14), Research Triangle Park, NC 27711:
"Screening Procedures for Estimating the Air Quality
Impact of Stationary Sources, Revised", October, 1992,
Publication Number EPA-450/R-92-019.
USEPA. Available from RCRA Information Center (RIC), 1235
Jefferson -Davis Highway, first floor, Arlington, VA 22203
(Docket # F -94-IEHF-FFFFF):
OECD Green List of Wastes, Appendix 3 to the OECD
Council Decision C(92)39/FINAL (Concerning the Control
of Transfrontier Movements of Wastes Destined for
Recovery Operations) (May 1994).
OECD Red List of Wastes, Appendix 5 to the OECD
40
Council Decision C(92)39/FINAL (Concerning the COntrol
of Transfrontier Movements of Wastes Destined for
Recovery Operations) (May 1993).
OECD Yellow List of Wastes, Appendix 4 to the OECD
Council Decision C(92)39/FINAL (Concerning the COntrol
of Transfrontier Movements of Wastes Destined for
Recovery Operations) (May 1993).
Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) (May 27, 1988).
b)
Code of Federal Regulations. Available from the Superintendent of
Documents, U.S. Government Printing Office, Washington, D.C.
20401, 202-783-3238:
10 CFR 20, Appendix B (199
46)
40 CFR 51.100(ii) (199
46)
40 CFR 51, Subpart W (199
46)
40 CFR 52.741, Appendix B (1996)
40 CFR 60 (199 46), as amended at 59 Fed. Reg. 62924 (Dec. 6,
1994)
40 CFR 61, S ubpart V (199 46)
40 CFR 136 (199 46), as amended at 60 Fed. Reg. 17160 (Apr.
4, 1995)
40 CFR 142 (199 46)
40 CFR 220 (199 46)
40 CFR 260.20 (199
46)
40 CFR 264 (199 46)
40 CFR 268.Appendix IX (199
46)
40 CFR 302.4, 302.5 and 302.6 (199
46)
40 CFR 761 (199 46)
49 CFR 171 (199 56)
49 CFR 173 (199 56)
49 CFR 178 (199 46)
c)
Federal Statutes
Section 3004 of the Resource Conservation and Recovery Act (42
U.S.C. 6901 et seq.), as amended through December 31, 1987.
Sections 201(v), 201(w), and 360b(j) of the Federal Food, Drug,
and Cosmetic Act (FFDCA; 21 U.S.C. ยงยง
321(v), 321(w) & 512(j)), as
amended through October 25, 1994.
41
d)
This Section incorporates no later editions or amendments.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 721
IDENTIFICATION AND LISTING OF HAZARDOUS WA
STE
SUBPART A: GENERAL PROVISIONS
Section
721.101
Purpose and Scope
721.102
Definition of Solid Waste
721.103
Definition of Hazardous Waste
721.104
Exclusions
721.105
Special Requirements for Hazardous Waste Generated by Small
Quantity Generators
721.106
Requirements for Recyclable Materials
721.107
Residues of Hazardous Waste in Empty Containers
721.108
PCB Wastes Regulated under TSCA
721.109
Requirements for Universal Waste
SUBPART B: CRITERIA FOR IDENTIFYING THE CHARACTERISTICS
OF HAZARDOUS WASTE
AND FOR LISTING HAZARDOUS WASTES
Section
721.110
Criteria for Identifying the Characteristics of Hazardous Waste
721.111
Criteria for Listing Hazardous Waste
SUBPART C: CHARACTERISTICS OF HAZARDOUS WASTE
Section
721.120
General
721.121
Characteristic of Ignitability
721.122
Characteristic of Corrosivity
721.123
Characteristic of Reactivity
721.124
Toxicity Characteristic
SUBPART D: LISTS OF HAZARDOUS WASTE
Section
721.130
General
721.131
Hazardous Wastes From Nonspecific Sources
721.132
Hazardous Was te from Specific Sources
721.133
Discarded Commercial Chemical Products, Off-Specification Species,
Container Residues, and Spill Residues Thereof
721.135
Wood Preserving Wastes
721.Appendix A
Representative Sampling Methods
721.Appendix B
Method 1311 Toxicity Characteristic Leaching Procedure
(TCLP)
721.Appendix C
Chemical Analysis Test Methods
Table A
Analytical Characteristics of Organic Chemicals (Repealed)
Table B
Analytical Characteristics of Inorganic Species (Repealed)
Table C
Sample Preparation
/Sample Introduction Techniques (Repealed)
721.Appendix G
Basis for Listing Hazardous Wastes
721.Appendix H
Hazardous Constituents
721.Appendix I
Wastes Excluded by Administrative Action
Table A
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22
from Non-Specific Sources
42
Table B
Wastes Excluded by USEPA under 40 CFR 260.20 and 260.22 from
Specific Sources
Table C
Wastes Excluded by U.S. EPA under 40 CFR 260.20 and 260.22
from Commercial Chemical Products, Off-Specification
Species, Container Residues, and Soil Residues Thereof
Table D
Wastes Excluded by the Board by Adjusted Standard
721.Appendix J
Method of Analysis for Chlorinated Dibenzo-p-Dioxins and
Dibenzofurans (Repealed)
721.Appendix Z
Table to Section 721.102
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
effective as noted in 35 Ill. Adm. Code May 17, 1982; amended in R82-18, 51
PCB 31, at 7 Ill. Reg. 2518, effective February 22, 1983; amended in R82-19,
53 PCB 131, at 7 Ill. Reg. 13999, effective October 12, 1983; amended in R84-
34, 61 PCB 247, at 8 Ill. Reg. 24562, effective December 11, 1984; amended in
R84-9, at 9 Ill. Reg. 11834, effective July 24, 1985; amended in R85-22 at 10
Ill. Reg. 998, effective January 2, 1986; amended in R85-2 at 10 Ill. Reg.
8112, effective May 2, 1986; amended in R86-1 at 10 Ill. Reg. 14002, effective
August 12, 1986; amended in R86-19 at 10 Ill. Reg. 20647, effective December
2, 1986; amended in R86-28 at 11 Ill. Reg. 6035, effective March 24, 1987;
amended in R86-46 at 11 Ill. Reg. 13466, effective August 4, 1987; amended in
R87-32 at 11 Ill. Reg. 16698, effective September 30, 1987; amended in R87-5
at 11 Ill. Reg. 19303, effective November 12, 1987; amended in R87-26 at 12
Ill. Reg. 2456, effective January 15, 1988; amended in R87-30 at 12 Ill. Reg.
12070, effective July 12, 1988; amended in R87-39 at 12 Ill. Reg. 13006,
effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 382, effective
December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18300, effective November
13, 1989; amended in R90-2 at 14 Ill. Reg. 14401, effective August 22, 1990;
amended in R90-10 at 14 Ill. Reg. 16472, effective September 25, 1990; amended
in R90-17 at 15 Ill. Reg. 7950, effective May 9, 1991; amended in R90-11 at 15
Ill. Reg. 9332, effective June 17, 1991; amended in R91-1 at 15 Ill. Reg.
14473, effective September 30, 1991; amended in R91-12 at 16 Ill. Reg. 2155,
effective January 27, 1992; amended in R91-26 at 16 Ill. Reg. 2600, effective
February 3, 1992; amended in R91-13 at 16 Ill. Reg. 9519, effective June 9,
1992; amended in R92-1 at 16 Ill. Reg. 17666, effective November 6, 1992;
amended in R92-10 at 17 Ill. Reg. 5650, effective March 26, 1993; amended in
R93-4 at 17 Ill. Reg. 20568, effective November 22, 1993; amended in R93-16 at
18 Ill. Reg. 6741, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
12175, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17490,
effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9522, effective
June 27, 1995; amended in R95-20 at 20 Ill. Reg. 10963, August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
SUBPART A: GENERAL PROVISIONS
Section 721.104
Exclusions
a)
Materials that are not solid wastes. The following materials are
not solid wastes for the purpose of this Part:
1)
Sewage:
A)
Domestic sewage; and
B)
Any mixture of domestic sewage and other waste that
43
passes through a sewer system to publicly-owned
treatment works for treatment.
C)
"Domestic sewage" means untreated sanitary wastes that
pass through a sewer system.
2)
Industrial wastewater discharges that are point source
discharges with NPDES permits issued by the Agency pursuant
to Section 12(f) of the Environmental Protection Act and 35
Ill. Adm. Code 309.
BOARD NOTE: This exclusion applies
only to the actual point
source discharge. It does not exclude industrial
wastewaters while they are being collected, stored, or
treated before discharge, nor does it exclude sludges that
are generated by industrial wastewater treatment.
3)
Irrigation return flows.
4)
Source, special nuclear, or by-product material as defined
by the Atomic Energy Act of 1954, as amended (42 U.S.C. 2011
et seq.)
5)
Materials subjected to in-situ mining techniques that are
not removed from the ground as part of the extraction
process.
6)
Pulping liquors (i.e., black liquor) that are reclaimed in a
pulping liquor recovery furnace and then reused in the
pulping process, unless accumulated speculatively, as
defined in Section 721.101(c).
7)
Spent sulfuric acid used to produce virgin sulfuric acid
unless it is accumulated speculatively, as defined in
Section 721.101(c).
8)
Secondary materials that are reclaimed and returned to the
original process or processes in which they were generated
where they are reused in the production process, provided:
A)
Only tank storage is involved, and the entire process
through completion of reclamation is closed by being
entirely connected with pipes or other comparable
enclosed means of conveyance;
B)
Reclamation does not involve controlled flame
combustion (such as occurs in boilers, industrial
furnaces or incinerators);
C)
The secondary materials are never accumulated in such
tanks for over twelve months without being reclaimed;
and
D)
The reclaimed material is
not used to produce a fuel
or used to produce products that are used in a manner
constituting disposal.
9)
Wood preserving wastes.
A)
Spent wood preserving solutions that have been used
and which are reclaimed and reused for their original
44
intended purpose; and
B)
Wastewaters from the wood preserving process that have
been reclaimed and which are reused to treat wood.
10)
Hazardous waste numbers K060, K087, K141, K142, K143, K144,
K145, K147, and K148, and any wastes from the coke by-
products processes that are hazardous only because they
exhibit the toxicity characteristic specified in Section
721.124, when subsequent to generation these materials are
recycled to coke ovens, to the tar recovery process as a
feedstock to produce coal tar, or are mixed with coal tar
prior to the tar's sale or refining. This exclusion is
conditioned on there being no land disposal of the waste
from the point it is generated to the point it is recycled
to coke ovens, to tar recovery, to the tar refining
processes, or prior to when it is mixed with coal.
11)
Nonwastewater splash condenser dross residue from the
treatment of hazardous waste number K061 in high temperature
metals recovery units, provided it is shipped in drums (if
shipped) and not land disposed before recovery.
12)
Recovered oil from petroleum refining, exploration, and
production and from transportation incident thereto that is
to be inserted into the petroleum refining process (SIC Code
2911) along with normal process streams prior to crude
distillation or catalytic cracking
at or before a point
(other than direct insertion into a coker) where
contaminants are removed
. This exclusion applies to
recovered oil stored or transported prior to insertion,
except that the oil must not be stored in a manner involving
placement on the land and the oil must not be accumulated
speculatively before being recycled. Recovered oil is oil
that has been reclaimed from secondary materials (such as
wastewater) generated from normal petroleum refining,
exploration , and production, and
from transportation
practices. Recovered oil includes oil that is recovered
from refinery wastewater collection and treatment systems,
oil recovered from oil and gas drilling operations, and oil
recovered from wastes removed from crude oil storage tanks.
Recovered oil does not include (among other things) oil-
bearing hazardous wastes listed in 721.Subpart D (e.g., K048
through K052, F037, and F038). However, oil recovered from
such wastes may be considered recovered oil. Recovered oil
also does not include used oil as defined in 35 Ill. Adm.
Code 739.100.
b)
Solid wastes that are not hazardous wastes. The following solid
wastes are not hazardous wastes:
1)
Household waste, including household waste that has been
collected, transported, stored, treated, disposed, recovered
(e.g., refuse-derived fuel), or reused. "Household waste"
means any waste material (including garbage, trash, and
sanitary wastes in septic tanks) derived from households
(including single and multiple residences, hotels, and
motels, bunkhouses, ranger stations, crew quarters,
campgrounds, picnic grounds, and day-use recreation areas).
A resource recovery facility managing municipal solid waste
shall not be deemed to be treating, storing, disposing of,
45
or otherwise managing hazardous wastes for the purposes of
regulation under this Part, if such facility:
A)
Receives and burns only:
i)
Household waste (from single and multiple
dwellings, hotels, motels, and other residential
sources); and
ii)
Solid waste from commercial or industrial
sources that does not contain hazardous waste,
and
B)
Such facility does not accept hazardous waste and the
owner or operator of such facility has established
contractual requirements or other appropriate
notification or inspection procedures to assure that
hazardous wastes are not received at or burned in such
facility.
BOARD NOTE: The U.S. Supreme Court determined, in
City of Chicago v. Environmental Defense Fund, Inc.,
-- U.S. --, 114 S. Ct. 1588 (1994), th
at this
exclusion and RCRA section 3001(i) (42 U.S.C.
ยง 6921(i)) do not exclude the ash from facilities
covered by this subsection from regulation as a
hazardous waste. At 59 Fed. Reg. 29372 (June 7,
1994), USEPA granted facilities managing ash from such
facilities that is determined a hazardous waste under
721.Subpart C until December 7, 1994 to file a Part A
permit application pursuant to 35 Ill. Adm. Code
703.181. At 60 Fed. Reg. 6666 (Feb. 3, 1995), USEPA
stated that it interpreted that the point at which ash
becomes subject to RCRA Subtitle C regulation is when
that material leaves the combustion building
(including connected air pollution control equipment).
2)
Solid wastes generated by any of the following that are
returned to the soil as fertilizers:
A)
The growing and harvesting of agricultural crops, or
B)
The raising of animals, including animal manures.
3)
Mining overburden returned to the mine site.
4)
Fly ash waste, bottom ash waste, slag waste, and flue gas
emission control waste generated primarily from the
combustion of coal or other fossil fuels, except as provided
in 35 Ill. Adm. Code 726.212 for facilities that burn or
process hazardous waste.
5)
Drilling fluids, produced waters, and other wastes
associated with the exploration, development, or production
of crude oil, natural gas, or geothermal energy.
6)
Chromium wastes:
A)
Wastes that fail the test for the toxicity
characteristic (Sections 721.124 and 721.Appendix B)
because chromium is present or which are listed in
46
721.Subpart D due to the presence of chromium, that do
not fail the test for the toxicity characteristic for
any other constituent or which are not listed due to
the presence of any other constituent, and that do not
fail the test for any other characteristic, if it is
shown by a waste generator or by waste generators
that:
i)
The chromium in the waste is exclusively (or
nearly exclusively) trivalent chromium;
ii)
The waste is generated from an industrial
process that uses trivalent chromium exclusively
(or nearly exclusively) and the process does not
generate hexavalent chromium; and
iii)
The waste is typically and frequently managed in
non-oxidizing environments.
B)
Specific wastes that meet the standard in subsection
(b)(6)(A) above (so long as they do not fail the test
for the toxicity characteristic for any other
constituent and do not exhibit any other
characteristic) are:
i)
Chrome (blue) trimmings generated by the
following subcategories of the leather tanning
and finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
ii)
Chrome (blue) shavings generated by the
following subcategories of the leather tanning
and finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
iii)
Buffing dust generated by the following
subcategories of the leather tanning and
finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue;
iv)
Sewer screenings generated by the following
subcategories of the leather tanning and
finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
v)
Wastewater treatment sludges generated by the
following subcategories of the leather tanning
and finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, retan/wet finish, no
beamhouse, through-the-blue, and shearling;
vi)
Wastewater treatment sludges generated by the
47
following subcategories of the leather tanning
and finishing industry: hair pulp/chrome
tan/retan/wet finish, hair save/chrome
tan/retan/wet finish, and through-the-blue;
vii)
Waste scrap leather from the leather tanning
industry, the shoe manufacturing industry, and
other leather product manufacturing industries;
and
viii)
Wastewater treatment sludges from the production
of titanium dioxide pigment using chromium-
bearing ores by the chloride process.
7)
Solid waste from the extraction, beneficiation, and
processing of ores and minerals (including coal, phosphate
rock, and overburden from the mining of uranium ore), except
as provided by 35 Ill. Adm. Code 726.212 for facilities that
burn or process hazardous waste. For purposes of this
subsection, beneficiation of ores and minerals is restricted
to the following activities: crushing, grinding, washing,
dissolution, crystallization, filtration, sorting, sizing,
drying, sintering, pelletizing, briquetting, calcining to
remove water or carbon dioxide, roasting, autoclaving or
chlorination in preparation for leaching (except where the
roasting or autoclaving or chlorination and leaching
sequence produces a final or intermediate product that does
not undergo further beneficiation or processing), gravity
concentration, magnetic separation, electrostatic
separation, floatation, ion exchange, solvent extraction,
electrowinning, precipitation, amalgamation, and heap, dump,
vat tank, and in situ leaching. For the purposes of this
subsection, solid waste from the processing of ores and
minerals includes only the following wastes:
A)
Slag from primary copper processing,
B)
Slag from primary lead processing,
C)
Red and brown muds from bauxite refining,
D)
Phosphogypsum from phosphoric acid production,
E)
Slag from elementa
l phosphorus production,
F)
Gasifier ash from coal gasification,
G)
Process wastewater from coal gasification,
H)
Calcium sulfate wastewater treatment plant sludge from
primary copper processing,
I)
Slag tailings from primary copper processing,
J)
Fluorogypsum from hydrofluoric acid production,
K)
Process wastewater from hydrofluoric acid production,
L)
Air pollution control dust or sludge from iron blast
furnaces,
48
M)
Iron blast furnace slag,
N)
Treated residue from roast
ing and leaching of chrome
ore,
O)
Process wastewater from primary magnesium processing
by the anhydrous process,
P)
Process wastewater from phosphoric acid production,
Q)
Basic oxygen furnace and open hearth furnace air
pollution control dust or sludge from carbon steel
production,
R)
Basic oxygen furnace and open hearth furnace slag from
carbon steel production,
S)
Chloride processing waste solids from titanium
tetrachloride production, and
T)
Slag from primary zinc smelting.
8)
Cement kiln dust waste, except as provided by 35 Ill. Adm.
Code 726.212 for facilities that burn or process hazardous
waste.
9)
Solid waste that consists of discarded arsenical-treated
wood or wood products that fails the test for the toxicity
characteristic for hazardous waste codes D004 through D017
and which is not a hazardous waste for any other reason if
the waste is generated by persons that utilize the
arsenical-treated wood and wood products for these
materials' intended end use.
10)
Petroleu m-contaminated media and debris that fail the test
for the toxicity characteristic of Section 721.124
(hazardous waste codes D018 through D043 only) and which are
subject to corrective action regulations under 35 Ill. Adm.
Code 731.
11)
This subsection corresponds with 40 CFR 261.4(b)(11), which
expired by its own terms on January 25, 1993. This
statement maintains structural parity with USEPA
regulations.
12)
Used chloro fluoro carbon refrigerants from totally enclosed
heat transfer equipment, including mobile air conditioning
systems, mobile refrigeration, and commercial and industrial
air conditioning and refrigeration systems, that uses
chloro fluoro carbons as the heat transfer fluid in a
refrigeration cycle, provided the refrigerant is reclaimed
for further use.
13)
Non-terne plated used oil filters that are not mixed with
wastes listed in 721.Subpart D, if these oil filters have
been gravity hot-drained using one of the following methods:
A)
Puncturing the filter anti-drain back valve or
the
filter dome end and hot-draining;
B)
Hot-draining and crushing;
49
C)
Dismantling and hot-draining; or
D)
Any other equivalent hot-draining method that will
remove used oil.
14)
Used oil re-refining distillation bottoms that are used as
feedstock to manufacture asphalt products.
c)
Hazardous wastes that are exempted from certain regulations. A
hazardous waste that is generated in a product or raw material
storage tank, a product or raw material transport vehicle or
vessel, a product or raw material pipeline, or in a manufacturing
process unit, or an associated non-waste-treatment manufacturing
unit, is not subject to regulation under 35 Ill. Adm. Code 702,
703, 705, and 722 through 725, and 728 or to the notification
requirements of Section 3010 of RCRA until it exits the unit in
which it was generated, unless the unit is a surface impoundment,
or unless the hazardous waste remains in the unit more than 90
days after the unit ceases to be operated for manufacturing or for
storage or transportation of product or raw materials.
d)
Samples
1)
Except as provided in subsection (d)(2) below, a sample of
solid waste or a sample of water, soil, or air that is
collected for the sole purpose of testing to determine its
characteristics or composition is not subject to any
requirements of this Part or 35 Ill. Adm. Code 702, 703,
705, and 722 through 728. The sample qualifies when:
A)
The sample is being transported to a laboratory for
the purpose of testing;
B)
The sample is being transport
ed back to the sample
collector after testing;
C)
The sample is being stored by the sample collector
before transport to a laboratory for testing;
D)
The sample is being stored in a laboratory before
testing;
E)
The sample is being stored in a laboratory for testing
but before it is returned to the sample collector; or
F)
The sample is being stored temporarily in the
laboratory after testing for a specific purpose (for
example, until conclusion of a court case or
enforcement action where further testing of the sample
may be necessary).
2)
In order to qualify for the exemption in subsection
(d)(1)(A) or (d)(1)(B) above, a sample collector shipping
samples to a laboratory and a laboratory returning samples
to a sample collector shall:
A)
Comply with U.S. Department of Transportation (DOT),
U.S. Postal Service (USPS), or any other applicable
shipping requirements; or
50
B)
Comply with the following requirements if the sample
collector determines that DOT, USPS, or other shipping
requirements do not apply to the shipment of the
sample:
i)
Assure that the following information
accompanies the sample: The sample collector's
name, mailing address, and telephone number; the
laboratory's name, mailing address, and
telephone number; the quantity of the sample;
the date of the shipment; and a description of
the sample.
ii)
Package the sample so that it does not leak,
spill, or vaporize from its packaging.
3)
This exemption does not apply if the laboratory determines
that the waste is hazardous but the laboratory is no longer
meeting any of the conditions stated in subsection (d)(1)
above.
e)
Treatability study samples.
1)
Except as is provided in subsection (e)(2) below, a person
that generates or collects samples for the purpose of
conducting treatability studies, as defined in 35 Ill. Adm.
Code 720.110, are not subject to any requirement of 35 Ill.
Adm. Code 721 through 723 or to the notification
requirements of Section 3010 of the Resource Conservation
and Recovery Act. Nor are such samples included in the
quantity determinations of Section 721.105 and 35 Ill. Adm.
Code 722.134(d) when:
A)
The sample is being collected and prepared for
transportation by the generator or sample collector;
B)
The sample is being accumulated or stored by the
generator or sample collector prior to transportation
to a laboratory or testing facility; or
C)
The sample is being transported to the laboratory or
testing facility for the purpose of conducting a
treatability study.
2)
The exem ption in subsection (e)(1) above is applicable to
samples of hazardous waste being collected and shipped for
the purpose of conducting treatability studies provided
that:
A)
The generator or sample collector uses (in
"treatability studies") no more than 10,000 kg of
media contaminated with non-acute hazardous waste,
1000 kg of non-acute hazardous waste other than
contaminated media, 1 kg of acute hazardous waste, or
2500 kg of media contaminated with acute hazardous
waste for each process being evaluated for each
generated wastestream;
B)
The mass of each shipment does not exceed 10,000 kg;
the 10,000 kg quantity may be all media contaminated
with non-acute hazardous waste, or may include 2500 kg
51
of media contaminated with acute hazardous waste, 1000
kg of hazardous waste, and 1 kg of acute hazardous
waste;
C)
The sample must be packaged so that it does not leak,
spill, or vaporize from its packaging during shipment
and the requirements of subsections (e)(2)(C)(i) or
(e)(2)(C)(ii) , below , are met.
i)
The transportation of each sample shipment
complies with U.S. Department of Transportation
(DOT), U.S. Postal Service (USPS), or any other
applicable shipping requirements; or
ii)
If the DOT, USPS, or other shipping requirements
do not apply to the shipment of the sample, the
following information must accompany the sample:
The name, mailing address, and telephone number
of the originator of the sample; the name,
address, and telephone number of the facility
that will perform the treatability study; the
quantity of the sample; the date of the
shipment; and, a description of the sample,
including its USEPA hazardous waste number;
D)
The sample is shipped to a laboratory or testing
facility that is exempt under subsection (f) below, or
has an appropriate RCRA permit or interim status;
E)
The generator or sample collector maintains the
following records for a period ending three years
after completion of the treatability study:
i)
Copies of the shipping documents;
ii)
A copy of t he contract with the facility
conducting the treatability study;
iii)
Documentation showing: The amount of waste
shipped under this exemption; the name, address,
and USEPA identification number of the
laboratory or testing facility that received the
waste; the date the shipment was made; and
whether or not unused samples and residues were
returned to the generator; and
F)
The generator reports the information required in
subsection (e)(2)(E)(iii) above in its report under 35
Ill. Adm. Code 722.141.
3)
The Agency may grant requests on a case-by-case basis for up
to an additional two years for treatability studies
involving bioremediation. The Agency may grant requests, on
a case-by-case basis, for quantity limits in excess of those
specified in subsection (e)(2)(A) and (e)(2)(B) above and
(f)(4) below, for up to an additional 5000 kg of media
contaminated with non-acute hazardous waste, 500 kg of non-
acute hazardous waste, 2500 kg of media contaminated with
acute hazardous waste, and 1 kg of acute hazardous waste:
A)
In response to requests for authorization to ship,
52
store, and conduct further treatability studies on
additional quantities in advance of commencing
treatability studies. Factors to be considered in
reviewing such requests include the nature of the
technology, the type of process (e.g., batch versus
continuous), the size of the unit undergoing testing
(particularly in relation to scale-up considerations),
the time or quantity of material required to reach
steady-state operating conditions, or test design
considerations, such as mass balance calculations.
B)
In response to requests for authorization to ship,
store, and conduct treatability studies on additional
quantities after initiation or completion of initial
treatability studies when: There has been an
equipment or mechanical failure during the conduct of
the treatability study, there is need to verify the
results of a previously-conducted treatability study,
there is a need to study and analyze alternative
techniques within a previously-evaluated treatment
process, or there is a need to do further evaluation
of an ongoing treatability study to determine final
specifications for treatment.
C)
The additional quantities allowed and timeframes
allowed in subsections (e)(3)(A) and (e)(3)(B) above
are subject to all the provisions in subsections
(e)(1) and (e)(2)(B) through (e)(2)(F) above. The
generator or sample collector shall apply to the
Agency and provide in writing the following
information:
i)
The reason why the
generator or sample collector
requires additional time or quantity of sample
for the treatability study evaluation and the
additional time or quantity needed;
ii)
Documentation accounting for all samples of
hazardous waste from the wastestream that have
been sent for or undergone treatability studies,
including the date each previous sample from the
waste stream was shipped, the quantity of each
previous shipment, the laboratory or testing
facility to which it was shipped, what
treatability study processes were conducted on
each sample shipped, and the available results
of each treatability study;
iii)
A description of the technical modifications or
change in specifications that will be evaluated
and the expected results;
iv)
If such further study is being required due to
equipment or mechanical failure, the applicant
shall include information regarding the reason
for the failure or breakdown and also include
what procedures or equipment improvements have
been made to protect against further breakdowns;
and
v)
Such other information as the Agency determines
53
is necessary.
4)
Final Agency determinations pursuant to this subsection may
be appealed to the Board.
f)
Samples undergoing treatability studies at laboratories or testing
facilities. Samples undergoing treatability studies and the
laboratory or testing facility conducting such treatability
studies (to the extent such facilities are not otherwise subject
to RCRA requirements) are not subject to any requirement of this
Part, or of 35 Ill. Adm. Code 702, 703, 705, 722 through 726, and
728 or to the notification requirements of Section 3010 of the
Resource Conservation and Recovery Act, provided that the
requirements of subsections (f)(1) through (f)(11) below are met.
A mobile treatment unit may qualify as a testing facility subject
to subsections (f)(1) through (f)(11) below. Where a group of
mobile treatment units are located at the same site, the
limitations specified in subsections (f)(1) through (f)(11) below
apply to the entire group of mobile treatment units collectively
as if the group were one mobile treatment unit.
1)
No less than 45 days before conducting treatability studies,
the facility notifies the Agency in writing that it intends
to conduct treatability studies under this subsection.
2)
The laboratory or testing facility conducting the
treatability study has a USEPA identification number.
3)
No more than a total of 10,000 kg of "as received" media
contaminated with non-acute hazardous waste, 2500 kg of
media contaminated with acute hazardous waste, or 250 kg of
other "as received" hazardous waste is subject to initiation
of treatment in all treatability studies in any single day.
"As received" waste refers to the waste as received in the
shipment from the generator or sample collector.
4)
The quantity of "as received" hazardous waste stored at the
facility for the purpose of evaluation in treatability
studies does not exceed 10,000 kg, the total of which can
include 10,000 kg of media contaminated with non-acute
hazardous waste, 2500 kg of media contaminated with acute
hazardous waste, 1000 kg of non-acute hazardous wastes other
than contaminated media, and 1 kg of acute hazardous waste.
This quantity limitation does not include treatment
materials (including nonhazardous solid waste) added to "as
received" hazardous waste.
5)
No more than 90 days have elapsed since the treatability
study for the sample was completed, or no more than one year
(two years for treatability studies involving
bioremediation) has elapsed since the generator or sample
collector shipped the sample to the laboratory or testing
facility, whichever date first occurs. Up to 500 kg of
treated material from a particular waste stream from
treatability studies may be archived for future evaluation
up to five years from the date of initial receipt.
Quantities of materials archived are counted against the
total storage limit for the facility.
6)
The treatability study does not involve the placement of
hazardous waste on the land or open burning of hazardous
54
waste.
7)
The facility maintains records for three years following
completion of each study that show compliance with the
treatment rate limits and the storage time and quantity
limits. The following specific information must be included
for each treatability study conducted:
A)
The name, address, and USEPA identification number of
the generator or sample collector of each waste
sample;
B)
The date the shipment was received;
C)
The quantity of waste accepted;
D)
The quantity of "as received" waste in storage each
day;
E)
The date the treatment study was initiated and the
amount of "as received" waste introduced to treatment
each day;
F)
The date the treatability study was concluded;
G)
The date any unused sample or residues generated from
the treatability study were returned to the generator
or sample collector or, if sent to a designated
facility, the name of the facility and the USEPA
identification number.
8)
The facility keeps, on-site, a copy of the
treatability
study contract and all shipping papers associated with the
transport of treatability study samples to and from the
facility for a period ending three years from the completion
date of each treatability study.
9)
The facility prepares and submits a report to the Agency by
March 15 of each year that estimates the number of studies
and the amount of waste expected to be used in treatability
studies during the current year, and includes the following
information for the previous calendar year:
A)
The name, address, and USEPA identification number of
the facility conducting the treatability studies;
B)
The types (by process) of treatability studies
conducted;
C)
The names and addresses of persons for whom studies
have been conducted (including their USEPA
identification numbers);
D)
The total quantity of waste in storage each day;
E)
The quantity and types of waste subjected to
treatability studies;
F)
When each treatability study was conducted; and
G)
The final disposi
tion of residues and unused sample
55
from each treatability study.
10)
The facility determines whether any unused sample or
residues generated by the treatability study are hazardous
waste under Section 721.103 and, if so, are subject to 35
Ill. Adm. Code 702, 703, and 721 through 728, unless the
residues and unused samples are returned to the sample
originator under the subsection (e) exemption above.
11)
The facility notifies the Agency by letter when the facility
is no longer planning to conduct any treatability studies at
the site.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 721.105
Special Requirements for Hazardous Waste Generated by Small
Quantity Generators
a)
A generator is a conditionally exempt small quantity generator in
a calendar month if it generates no more than 100 kilograms of
hazardous waste in that month. 35 Ill. Adm. Code 700 explains the
relation of this to the 100 kg/mo exception of 35 Ill. Adm. Code
809.
b)
Except for those wastes iden
tified in subsections (e), (f), (g)
and (j) below, a conditionally exempt small quantity generator's
hazardous wastes are not subject to regulation under 35 Ill. Adm.
Code 702, 703, 705 and 722 through 726 and 728, and the
notification requirements of Section 3010 of Resource Conservation
and Recovery Act, provided the generator complies with the
requirements of subsections (f), (g) and (j) below.
c)
When making the quantity determinations of this Part and 35 Ill.
Adm. Code 722, the generator must include all hazardous waste that
it generates, except the following hazardous waste:
1)
Hazardous waste that is exempt from regulation under Section
721.104(c) through (f), 721.106(a)(3), 721.107(a)(1), or
721.108;
2)
Hazardous waste that is managed immediately upon generation
only in on -site elementary neutralization units, wastewater
treatment units, or totally enclosed treatment facilities,
as defined in 35 Ill. Adm. Code 720.110;
3)
Hazardous waste that is recycled, without prior storage or
accumulation, only in an on
-site process subject to
regulation under Section 721.106(c)(2);
4)
Hazardous waste that is used oil managed under the
requirements of Section 721.106(a)(4) and 35 Ill. Adm. Code
739;
5)
Hazardous waste that is spent lead
-acid batteries managed
under the requirements of 35 Ill. Adm. Code 726.Subpart G;
and
6)
Hazardous waste that is universal waste managed under
Section 721.109 and 35 Ill. Adm. Code 733.
d)
In determining the quantity of hazardous waste it generates, a
56
generator need not include:
1)
Hazardous waste when it is removed from on-site storage; or
2)
Hazardous waste produced by on-site treatment (including
reclamation) of its hazardous waste so long as the hazardous
waste that is treated was counted once; or
3)
Spent materials that are generated, reclaimed and
subsequently reused on-site, so long as such spent materials
have been counted once.
e)
If a generator generates acute hazardous waste in a calendar month
in quantities greater than set forth below, all quantities of that
acute hazardous waste are subject to full regulation under 35 Ill.
Adm. Code 702, 703, 705 and 722 through 726 and 728, and the
notification requirements of Section 3010 of the Resource
Conservation and Recovery Act:
1)
A total of one kilogram of one or more of the acute
hazardous wastes listed in Section 721.131, 721.132, or
721.133(e); or
2)
A total of 100 kilograms of any residue or contaminated
soil, waste or other debris resulting from the clean-up of a
spill, into or on any land or water, of any one or more of
the acute hazardous wastes listed in Section 721.131,
721.132, or 721.133(e).
BOARD NOTE: "Full regulation" means those regulations
applicable to generators of greater than 1000 kg of non-
acute hazardous waste in a calendar month.
f)
In order for acute hazardous wastes generated by a generator of
acute hazardous wastes in quantities equal to or less than those
set forth in subsection (e)(1) or (e)(2) above to be excluded from
full regulation under this Section, the generator must comply with
the following requirements:
1)
35 Ill. Adm. Code 722.111.
2)
The generator may accumulate acute hazardous waste on-site.
If the generator accumulates at any time acute hazardous
wastes in quantities greater than set forth in subsection
(e)(1) or (e)(2) above, all of those accumulated wastes are
subject to regulation under 35 Ill. Adm. Code 702, 703, 705
and 722 through 726 and 728, and the applicable notification
requirements of Section 3010 of the Resource Conservation
and Recovery Act. The time period of 35 Ill. Adm. Code
722.134(a), for accumulation of wastes on-site, begins when
the accumulated wastes exceed the applicable exclusion
limit.
3)
A conditionally exempt shall quantity generator may either
treat or dispose of its acute hazardous waste in an on-site
facility or ensure delivery to an off-site
storage,
treatment, storage, or disposal facility, provided that if
the on-site or off-site facility is located in the United
States, it fulfills either of which, if located in the United
States, meets any of the following conditions:
57
A)
The facility is permitted under 35 Ill. Adm. Code
702
and 703;
B)
The facility has interim status under 35 Ill. Adm.
Code 702, 703 and 725;
C)
The facility is authorized to manage hazardous waste
by a state with a hazardous waste management program
approved by USEPA pursuant to 40 CFR 271;
D)
The facility is permitted, licensed
, or registered by
a state to manage municipal or industrial solid waste
and, if managed in a municipal solid waste landfill
facility, the landfill is subject to 35 Ill. Adm. Code
810 through 817 or 40 CFR 258
;
E)
The facility is permitted, licensed, or registered by
a state to manage non-municipal non-hazardous waste
and, if managed in a non-municipal non-hazardous waste
disposal unit after January 1, 1998, the unit is
subject to the requirements of 40 CFR 257.5 through
257.30;
EF)
The facility is a facility that:
i)
Beneficially uses or reuses or legitimately
recycles or reclaims its waste; or
ii)
Treats its waste prior to beneficial use or
reuse, or legitimate recycling or reclamation;
or
FG)
For universal waste managed under 35 Ill. Adm. Code
733 or 40 CFR 273 , the facility is a universal waste
handler or destination facility subject to the
requirements of 35 Ill. Adm. Code 733
or 40 CFR 273 .
g)
In order for hazardous waste generated by a conditionally exempt
small quantity generator in quantities of less than 100 kilograms
of hazardous waste during a calendar month to be excluded from
full regulation under this Section, the generator must comply with
the following requirements:
1)
35 Ill. Adm. Code 722.111;
2)
The conditionally exempt small quantity generator may
accumulate hazardous waste on-site. If it accumulates at
any time more than a total of 1000 kilograms of the
generator's hazardous waste, all of those accumulated wastes
are subject to regulation under the special provisions of 35
Ill. Adm. Code 722 applicable to generators of between 100
kg and 1000 kg of hazardous waste in a calendar month as
well as the requirements of 35 Ill. Adm. Code 702, 703, 705
and 723 through 726 and 728, and the applicable notification
requirements of Section 3010 of the Resource Conservation
and Recovery Act. The time period of 35 Ill. Adm. Code
722.134(d) for accumulation of wastes on-site begins for a
small quantity generator when the accumulated wastes exceed
1000 kilograms;
3)
A conditionally exempt small quantity generator may either
58
treat or dispose of its hazardous waste in an on-site
facility or ensure delivery to an off-site
storage,
treatment, storage, or disposal facility,
provided that if
the on-site or off-site facility is located in
either of
which, if located in
the United States,
it fulfills meets any
of the following conditions:
A)
The facility is permitted under 35 Ill. Adm. Code 702
and 702 and 703;
B)
The facility has interim status under 35 Ill. Adm.
Code 702, 703 and 725;
C)
The facility is authorized to manage hazardous waste
by a state with a hazardous waste management program
approved by USEPA under 40 CFR 271 (1986);
D)
The facility is permitted, licensed
, or registered by
a state to manage municipal
or industrial solid waste
and, if managed in a municipal solid waste landfill
facility, the landfill is subject to 35 Ill. Adm. Code
810 through 817 or 40 CFR 258
;
E)
The facility is permitted, licensed, or registered by
a state to manage non-municipal non-hazardous waste
and, if managed in a non-municipal non-hazardous waste
disposal unit after January 1, 1998, the unit is
subject to the requirements of 40 CFR 257.5 through
257.30;
EF)
The facility is a facility that:
i)
Beneficially uses or re-uses, or legitimately
recycles or reclaims the small quantity
generator's waste; or
ii)
Treats its waste prior to beneficial use or re-
use, or legitimate recycling or reclamation; or
FG)
For universal waste managed under 35 Ill. Adm. Code
733 or 40 CFR 273 , the facility is a universal waste
handler or destination facility subject to the
requirements of 35 Ill. Adm. Code 733
or 40 CFR 273 .
h)
Hazardous waste subject to the reduced requirements of this
Section may be mixed with non-hazardous waste and remain subject
to these reduced requirements even though the resultant mixture
exceeds the quantity limitations identified in this Section,
unless the mixture meets any of the characteristics of hazardous
wastes identified in Subpart C.
i)
If a small quantity generator mixes a solid waste with a hazardous
waste that exceeds a quantity exclusion level of this Section, the
mixture is subject to full regulation.
j)
If a conditionally exempt small quantity generator's hazardous
wastes are mixed with used oil, the mixture is subject to 35 Ill.
Adm. Code 739, if it is destined to be burned for energy recovery.
Any material produced from such a mixture by processing,
blending, or other treatment is also so regulated if it is
destined to be burned for energy recovery.
59
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 721.106
Requirements for Recyclable Materials
a)
Recyclable materials:
1)
Hazardous wastes that are recycled are subject to the
requirements for generators, transporters, and storage
facilities of subsections (b) and (c) below, except for the
materials listed in subsections (a)(2) and (a)(3) below.
Hazardous wastes that are recycled will be known as
"recyclable materials".
2)
The following recyclable materials are not subject to the
requirements of this Section but are regulated under 35 Ill.
Adm. Code 726.Subparts C through H and all applicable
provisions in 35 Ill. Adm. Code 702, 703, and 705.
A)
Recyclable materials used in a manner constituting
disposal (35 Ill. Adm. Code 726.Subpart C);
B)
Hazardous wastes burned for energy recovery in boilers
and industrial furnaces that are not regulated under
35 Ill. Adm. Code 724.Subpart O or 725.Subpart O (35
Ill. Adm. Code 726.Subpart H);
C)
Recyclable materials from which precious metals are
reclaimed (35 Ill. Adm. Code 726.Subpart F);
D)
Spent lead-acid batteries that are being reclaimed (35
Ill. Adm. Code 726.Subpart G).
3)
The following recyclable materials are not subject to
regulation under 35 Ill. Adm. Code 722 through 726, 728, or
702, 703, or 705 and are not subject to the notification
requirements of Section 3010 of the Resource Conservation
and Recovery Act:
A)
Industrial ethyl alcohol that is reclaimed except
that, unless provided otherwise in an international
agreement as specified in 35 Ill. Adm. Code 722.158:
i)
A person initiating a shipment for reclamation
in a foreign country and any intermediary
arranging for the shipment shall comply with the
requirements applicable to a primary exporter in
35 Ill. Adm. Code 722.153; 722.156(a)(1) through
(a)(4), (a)(6), and (b); and 722.157; shall
export such materials only upon consent of the
receiving country and in conformance with the
USEPA Acknowledgement of Consent, as defined in
35 Ill. Adm. Code 722.Subpart E; and shall
provide a copy of the USEPA Acknowledgement of
Consent to the shipment to the transporter
transporting the shipment for export;
ii)
Transporters transporting a shipment for export
shall not accept a shipment if the transporter
knows that the shipment does not conform to the
60
USEPA Acknowledgement of Consent, shall ensure
that a copy of the USEPA Acknowledgement of
Consent accompanies the shipment, and shall
ensure that it is delivered to the facility
designated by the person initiating the
shipment;
B)
Scrap metal;
C)
Fuels produced from t
he refining of oil-bearing
hazardous wastes along with normal process streams at
a petroleum refining facility if such wastes result
from normal petroleum refining, production, and
transportation practices (this exemption does not
apply to fuels produced from oil recovered from oil-
bearing hazardous waste where such recovered oil is
already excluded under Section 721.104(a)(12));
D)
Petroleum refining wastes.
i)
Hazardous waste fuel produced from oil-bearing
hazardous wastes from petroleum refining,
production, or transportation practices or
produced from oil reclaimed from such hazardous
wastes, where such hazardous wastes are
reintroduced into a process that does not use
distillation or does not produce products from
crude oil, so long as the resulting fuel meets
the used oil specification under 35 Ill. Adm.
Code 726.140(e) and so long as no other
hazardous wastes are used to produce the
hazardous waste fuel;
ii)
Hazardous waste fuel produced from oil-bearing
hazardous waste from petroleum refining
production, and transportation practices, where
such hazardous wastes are reintroduced into a
refining process after a point at which
contaminants are removed, so long as the fuel
meets the used oil fuel specification under 35
Ill. Adm. Code 726.140(e); and
iii)
Oil reclaimed from oil-bearing hazardous wastes
from petroleum refining, production, and
transportation practices, which reclaimed oil is
burned as a fuel without reintroduction to a
refining process, so long as the reclaimed oil
meets the used oil fuel specification under 35
Ill. Adm. Code 726.140(e); and
E)
Petroleum coke produced from petroleum refinery
hazardous wastes containing oil by the same person
that generated the wastes unless the resulting coke
product exceeds one or more of the characteristics of
hazardous waste in 721.Subpart C.
4)
Used oil that is recycled and is also a hazardous waste
solely because it exhibits a hazardous characteristic is not
subject to the requirements of 35 Ill. Adm. Code 720 through
728, but it is regulated under 35 Ill. Adm. Code 739. Used
oil that is recycled includes any used oil that is reused
61
for any purpose following its original use (including the
purpose for which the oil was originally used). Such term
includes, but is not limited to, oil that is re-refined,
reclaimed, burned for energy recovery, or reprocessed.
5)
Hazardous waste that is exported to or imported from
designated member countries of the Organization for Economic
Cooperation and Development (OECD), as defined in Section
722.158(a)(1), for the purpose of recovery is subject to the
requirements of 35 Ill. Adm. Code 722.Subpart H if it is
subject to either the hazardous waste manifesting
requirements of 35 Ill. Adm. Code 722 or the universal waste
management standards of 35 Ill. Adm. Code 733.
b)
Generators and transporters of recyclable materials are subject to
the applicable requirements of 35 Ill. Adm. Code 722 and 723 and
the notification requirements under Section 3010 of the Resource
Conservation and Recovery Act, except as provided in subsection
(a) above.
c)
Storage and recycling:
1)
Owners or operators of facilities that store recyclable
materials before they are recycled are regulated under all
applicable provisions of 35 Ill. Adm. Code 702, 703, and
705; 724.Subparts A through L, AA,
and BB, and CC ; and
725.Subparts A through L, AA,
and BB, and CC ; 726; 728; and
the notification requirement under Section 3010 of the
Resource Conservation and Recovery Act, except as provided
in subsection (a) above. (The recycling process itself is
exempt from regulation, except as provided in subsection (d)
below.)
2)
Owners or operators of facilities that recycle recyclable
materials without storing them before they are recycled are
subject to the following requirements, except as provided in
subsection (a) above:
A)
Notification requirements under Section 3010 of the
Resource Conservation and Recovery Act,
B)
35 Ill. Adm. Code 725.171 and 725.172 (dealing with
the use of the manifest and manifest discrepancies),
and
C)
subsection (d) below.
d)
Owners or operators of facilities required to have a RCRA permit
pursuant to 35 Ill. Adm. Code 703 with hazardous waste management
units that recycle hazardous wastes are subject to 35 Ill. Adm.
Code 724.Subparts AA and BB and 725.Subparts AA and BB.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART D: LISTS OF HAZARDOUS WASTE
Section 721.132
Hazardous Waste from Specific Sources
The following solid wastes are listed hazardous wastes from specific sources
unless they are excluded under 35 Ill. Adm. Code 720.120 and 720.122 and
62
listed in Section 721.Appendix I.
EPA
Hazardous
Waste No.
Industry and Hazardous Waste
Hazard
Code
Wood Preservation:
K001
Bottom sediment sludge from the treatment of waste
-
waters from wood preserving processes that use
creosote or penta
chloro phenol.
(T)
Inorganic Pigments:
K002
Wastewater treatment sludge from the production of
chrome yellow and orange pigments.
(T)
K003
Wastewater treatment sludge from the production of
molybdate orange pigments.
(T)
K004
Wastewater treatment sludge from the production of
zinc yellow pigments.
(T)
K005
Wastewater treatment sludge from the production of
chrome green pigments.
(T)
K006
Wastewater treatment sludge from the production of
chrome oxide green pigments (anhydrous and
hydrated).
(T)
K007
Wastewater treatment sludge from the production of
iron blue pigments.
(T)
K008
Oven residue from the production of chrome oxide
green pigments.
(T)
Organic Chemicals:
K009
Distillation bottoms from the production of
acetaldehyde from ethylene.
(T)
K010
Distillation side cuts from the production of
acetaldehyde from ethylene.
(T)
K011
Bottom stream from the wastewater stripper in the
production of acrylonitrile.
(R,T)
K013
Bottom stream from the acetonitrile column in the
production of acrylonitrile.
(T)
K014
Bottoms from the acetonitrile purification column in
the production of acrylonitrile.
(T)
K015
Still bottoms from the distillation of benzyl
chloride.
(T)
K016
Heavy ends or distillation residues from the
production of carbon tetra
chloride.
(T)
K017
Heavy ends (still bottoms) from the purification
column in the production of epichloro
hydrin.
(T)
63
K018
Heavy ends from the fractionation column in ethyl
chloride production.
(T)
K019
Heavy ends from the distillation of ethylene di
-
chloride in ethylene dichloride production.
(T)
K020
Heavy ends from the distillation of vinyl chloride
in vinyl chloride monomer production.
(T)
K021
Aqueous spent antimony catalyst waste from
fluoromethanes production.
(T)
K022
Distillation bottom tars from the production of
phenol/acetone from cumene.
(T)
K023
Distillation light ends from the production of
phthalic anhydride from naphthalene.
(T)
K024
Distillation bottoms from the production of phthalic
anhydride from naphthalene.
(T)
K093
Distillation light ends from the production of
phthalic anhydride from ortho-xylene.
(T)
K094
Distillation bottoms from the production of phthalic
anhydride from ortho-xylene.
(T)
K025
Distillation bottoms from the production of
nitrobenzene by the nitration of benzene.
(T)
K026
Stripping still tails from the production of methyl
ethyl pyridines.
(T)
K027
Centrifuge and distillation residues from toluene
diisocyanate production.
(R,T)
K028
Spent catalyst from the hydrochlorinator reactor in
the production of 1,1,1-tri
chloro ethane.
(T)
K029
Waste from the product stream stripper in the
production of 1,1,1-tri
chloro ethane.
(T)
K095
Distillation bottoms from the production of 1,1,1-
trichloro ethane.
(T)
K096
Heavy ends from the heavy ends column from the
production of 1,1,1-tri
chloro ethane.
(T)
K030
Column bottoms or heavy ends from the combined
production of tri
chloro ethylene and perchloro
-
ethylene.
(T)
K083
Distillation bottoms from aniline production.
(T)
K103
Process residues from aniline extraction from the
production of aniline.
(T)
K104
Combined wastewater streams generated from
nitrobenzene/aniline production.
(T)
64
K085
Distillation or fractionation column bottoms
from the production of chloro
benzenes.
(T)
K105
Separated aqueous stream from the reactor product
washing step in the production of chloro
benzenes.
(T)
K107
Column bottoms from product separation from the
production of 1,1-di
methylhydrazine (UDMH) from
carboxylic acid hydrazides.
(C,T)
K108
Condensed column overheads from product separation
and condensed reactor vent gases from the production
of 1,1-di methylhydrazine (UDMH) from carboxylic acid
hydrazides.
(I,T)
K109
Spent filter cartridges from the product
purification from the production of 1,1-di
-
methylhydrazine (UDMH) from carboxylic acid
hydrazides.
(T)
K110
Condensed column overheads from intermediate
separation from the production of 1,1-di
-
methylhydrazine (UDMH) from carboxylic acid
hydrazides.
(T)
K111
Product wastewaters from the production of di
-
nitrotoluene via nitration of toluene.
(C,T)
K112
Reaction by-product water from the drying column in
the production of toluenedi
amine via hydrogenati
on
of dinitrotoluene.
(T)
K113
Condensed liquid light ends from the purification of
toluenedi amine in the production of toluenedi
amine
via hydrogenation of dinitrotoluene.
(T)
K114
Vicinals from the purification of toluene-di
amine in
the production of toluenedi
amine via hydrogenation
of dinitrotoluene.
(T)
K115
Heavy ends from the purification of toluenedi
amine
in the production of toluenedi
amine via
hydrogenation of di
nitrotoluene.
(T)
K116
Organic condensate from the solvent recovery column
in the production of toluene di
isocyanate via
phosgenation of toluenedi
amine.
(T)
K117
Wastewater from the reactor vent gas scrubber in the
production of ethylene di
bromide via bromination of
ethene.
(T)
K118
Spent adsorbent solids from purification of ethylene
dibromide in the production of ethylene di
bromide
via bromination of ethene.
(T)
K136
Still bottoms from the purification of ethylene di
-
bromide in the production of ethylene di
bromide via
bromination of ethene.
(T)
K156
Organic waste (including heavy ends, still bottoms,
(T)
65
light ends, spent solvents, filtrates, and
decantates) from the production of carbamates and
carbamoyl oximes.
(This listing does not apply to
wastes generated from the manufacture of 3-iodo-2-
propynyl n -butylcarbamate.)
K157
Wastewaters (including scrubber waters, condenser
waters, washwaters, and separation waters) from the
production of carbamates and carbamoyl oximes.
(This listing does not apply to wastes generated
from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
K158
Bag house dusts and filter/separation solids from
the production of carbamates and carbamoyl oximes.
(This listing does not apply to wastes generated
from the manufacture of 3-iodo-2-propynyl
n-butylcarbamate.)
(T)
K159
Organics from the treatment of thiocarbamate wastes.
(T)
K160
Solids (including filter wastes, separation solids,
and spent catalysts) from the production of
thiocarbamates and solids from the treatment of
thiocarbamate wastes.
(T)
K161
Purification solids (including filtration,
evaporation, and centrifugation solids), bag house
dust and floor sweepings from the production of
dithiocarbamate acids and their salts. (This listing
does not include K125 or K126.)
(R,T)
Inorganic Chemicals:
K071
Brine purification muds from the mercury cell
process in chlorine production, where separately
prepurified brine is not used.
(T)
K073
Chlorinated hydrocarbon waste from the purification
step of the diaphragm cell process using graphite
anodes in chlorine production.
(T)
K106
Wastewater treatment sludge from the mercury cell
process in chlorine production.
(T)
Pesticides:
K031
By-product salts generated in the production of MSMA
and cacodylic acid.
(T)
K032
Wastewater treatment sludge from the production of
chlordane.
(T)
K033
Wastewater and scrub water from the chlorination of
cyclopenta diene in the production of chlordane.
(T)
K034
Filter solids from the filtration of hexa
chloro -
cyclopenta diene in the production of chlordane.
(T)
K097
Vacuum stripper discharge from the chlordane
(T)
66
chlorinator in the production of chlordane.
K035
Wastewater treatment sludges generated in the
production of creosote.
(T)
K036
Still bottoms from toluene reclamation distillation
in the production of di
sulfoton.
(T)
K037
Wastewater treatment sludges from the production of
disulfoton.
(T)
K038
Wastewater from the washing and stripping of phorate
production.
(T)
K039
Filter cake from the filtration of di
ethylphosphoro -
dithioic acid in the production of ph
orate.
(T)
K040
Wastewater treatment sludge from the production of
phorate.
(T)
K041
Wastewater treatment sludge from the production of
toxaphene.
(T)
K098
Untreated process wastewater from the production of
toxaphene.
(T)
K042
Heavy ends or distillation residues from the
distillation of tetra
chloro benzene in the production
of 2,4,5-T.
(T)
K043
2,6-Di chloro phenol waste from the production of 2,4-
D.
(T)
K099
Untreated wastewater from the production of 2,4-D.
(T)
K123
Process wastewater (including supernates, filtrates
and washwaters) from the production of ethylene
bis-
dithiocarbamic acid and its salts.
(T)
K124
Reactor vent scrubber water from the production of
ethylene bisdithiocarbamic acid and its salts.
(C,T)
K125
Filtration, evaporation and centrifugation solids
from the production of ethylene
bisdithiocarbamic
acid and its salts.
(T)
K126
Baghouse dust and floor sweepings in milling and
packaging operations from the production or
formulation of ethylene
bisdithiocarbamic a cid and
its salts.
(T)
K131
Wastewater from the reactor and spent sulfuric acid
from the acid dryer from the production of methyl
bromide.
(C,T)
K132
Spent absorbent and wastewater separator solids from
the production of methyl bromide.
(T)
Explosives:
K044
Wastewater treatment sludges from the manufacturing
and processing of explosives.
(R)
67
K045
Spent carbon from the treatment of wastewater
containing explosives.
(R)
K046
Wastewater treatment sludges from the manufacturing,
formulation and loading of lead-based initiating
compounds.
(T)
K047
Pink/red water from TNT operations.
(R)
Petroleum Refining:
K048
Dissolved air flotation (DAF) float from the
petroleum refining industry.
(T)
K049
Slop oil emulsion solids from the petroleum refining
industry.
(T)
K050
Heat exchanger bundle cleaning sludge from the
petroleum refining industry.
(T)
K051
API separator sludge from the petroleum refining
industry.
(T)
K052
Tank bottoms (leaded) from the petroleum refining
industry.
(T)
Iron and Steel:
K061
Emission control dust/sludge from the primary
production of steel in electric furnaces.
(T)
K062
Spent pickle liquor generated by steel finishing
operations of facilities within the iron and steel
industry (SIC Codes 331 and 332) (as defined in 35
Ill. Adm. Code 720.110).
(C,T)
Primary Copper:
K064
Acid plant blowdown slurry or sludge resulting from
the thickening of blowdown slurry from primary
copper production.
(T)
Primary Lead:
K065
Surface impoundment solids contained in and dredged
from surface impoundments at primary lead smelting
facilities.
(T)
Primary Zinc:
K066
Sludge from treatment of process wastewater or acid
plant blowdown from primary zinc production.
(T)
BOARD NOTE: This waste listing is the subject of a
judicial remand in American Mining Congress v. EPA,
907 F.2d 1179 (D.D.C. 1990). The Board intends that
this listing not become enforceable in Illinois
until the first date upon which the Board RCRA
program becomes "not equivalent to the Federal
program", within the meaning of Section 3006(b) of
68
the RCRA Act, 42 U.S.C. 6926(b), the Board RCRA
rules become "less stringent" than the USEPA rules,
as this phrase is used in Section 3009, 42 U.S.C.
6929, or the Board RCRA rules are not "identical in
substance" with the federal rules as that term is
intended by 415 ILCS 5/7.2 and 22.4 as a result of
some action by USEPA with regard to this listing in
response to the American Mining Congress remand.
Primary Aluminum:
K088
Spent potliners from primary aluminum reduction.
(T)
Ferroalloys:
K090
Emission control dust or sludge from
ferrochromiumsilicon production.
(T)
K091
Emission control dust or sludge from ferrochromium
production.
(T)
Secondary Lead:
K069
Emission control dust/sludge from secondary lead
smelting.
(T)
BOARD NOTE: This listing is administratively stayed
for sludge generated from secondary acid scrubber
systems. The stay will remain in effect until this
note is removed.
K100
Waste leaching solution from acid leaching of
emission control dust/sludge from secondary lead
smelting.
(T)
Veterinary Pharmaceuticals:
K084
Wastewater treatment sludges generated during the
production of veterinary pharmaceuticals from
arsenic or organo-arsenic compounds.
(T)
K101
Distillation tar residues from the distillation of
aniline-based compounds in the production of
veterinary pharmaceuticals from arsenic or organo
-
arsenic compounds.
(T)
K102
Residue from use of activated carbon for
decolorization in the production of veterinary
pharmaceuticals from arsenic or organo-arsenic
compounds.
(T)
Ink Formulation:
K086
Solvent washes and sludges, caustic washes and
sludges, or water washes and sludges from cleaning
tubs and equipment used in the formulation of ink
from pigments, dryers, soaps and stabilizers
containing chromium and lead.
(T)
Coking:
K060
Ammonia still lime sludge from coking operations.
(T)
69
K087
Decanter tank tar sludge from coking operations.
(T)
K141
Process residues from the recovery of coal tar,
including, but not limited to, collecting sump
residues from the production of coke from coal or
the recovery of coke by-products produced from coal.
This listing does not include K087 (decanter tank
tar sludges from coking operations).
(T)
K142
Tar storage tank residues from the production of
coke from coal or from the recovery of coke by-
products produced from coal.
(T)
K143
Process residues from the recovery of light oil,
including, but not limited to, those generated in
stills, decanters, and wash oil recovery units from
the recovery of coke by-products produced from coal.
(T)
K144
Wastewater sump residues from light oil refining,
including, but not limited to, intercepting or
contamination sump sludges from the recovery of coke
by-products produced from coal.
(T)
K145
Residues from naphthalene collection and recovery
operations from the recovery of coke by-products
produced from coal.
(T)
K147
Tar storage tank residues from coal tar refining.
(T)
K148
Residues from coal tar distillation, including but
not limited to, still bottoms.
(T)
K149
Distillation bottoms from the production of alpha-
(or methyl-) chlorinated toluenes, ring-chlorinated
toluenes, benzoyl chlorides, and compounds with
mixtures of these functional groups. (This waste
does not include still bottoms from the distillation
of benzyl chloride.)
(T)
K150
Organic residuals, excluding spent carbon adsorbent,
from the spent chlorine gas and hydrochloric acid
recovery processes associated with the production of
alpha- (or methyl-) chlorinated toluenes, ring-
chlorinated toluenes, benzoyl chlorides, and
compounds with mixtures of these functional groups.
(T)
K151
Wastewater treatment sludges, excluding
neutralization and biological sludges, generated
during the treatment of wastewaters from the
production of alpha- (or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these
functional groups.
(T)
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 721.133
Discarded Commer cial Chemical Products, Off-Specification
Species, Container Residues, and Spill Residues Thereof
The following materials or items are hazardous wastes if and when they are
70
discarded or intended to be discarded as described in Section
721.102(a)(2)(A), when they are mixed with waste oil or used oil or other
material and applied to the land for dust suppression or road treatment, when
they are otherwise applied to the land in lieu of their original intended use
or when they are contained in products that are applied to land in lieu of
their original intended use, or when, in lieu of their original intended use,
they are produced for use as (or as a component of) a fuel, distributed for
use as a fuel, or burned as a fuel.
a)
Any commercial chemical product, or manufacturing chemical
intermediate having the generic name listed in subsection (e) or
(f) below.
b)
Any off-specification commercial chemical product or manufacturing
chemical intermediate which, if it met specifications, would have
the generic name listed in subsection (e) or (f) below.
c)
Any residue remaining in a container or inner liner removed from a
container that has held any commercial chemical product or
manufacturing chemical intermediate having the generic name listed
in subsection (e) or (f) below, unless the container is empty as
defined in Section 721.107(b)(3).
BOARD NOTE: Unless the residue is being beneficially used or
reused, or legitimately recycled or reclaimed, or being
accumulated, stored, transported, or treated prior to such use,
reuse, recycling, or reclamation, the Board considers the residue
to be intended for discard, and thus a hazardous waste. An
example of a legitimate reuse of the residue would be where the
residue remains in the container and the container is used to hold
the same commercial chemical product or manufacturing chemical
intermediate it previously held. An example of the discard of the
residue would be where the drum is sent to a drum reconditioner
that reconditions the drum but discards the residue.
d)
Any residue or contaminated soil, water, or other debris resulting
from the cleanup of a spill into or on any land or water of any
commercial chemical product or manufacturing chemical intermediate
having the generic name listed in subsection (e) or (f) below, or
any residue or contaminated soil, water, or other debris resulting
from the cleanup of a spill into or on any land or water, of any
off-specification chemical product or manufacturing chemical
intermediate which, if it met specifications, would have the
generic name listed in subsection (e) or (f) below.
BOARD NOTE: The phrase "commercial chemical product or
manufacturing chemical intermediate having the generic name listed
in ..." refers to a chemical substance that is manufactured or
formulated for commercial or manufacturing use which consists of
the commercially pure grade of the chemical, any technical grades
of the chemical that are produced or marketed, and all
formulations in which the chemical is the sole active ingredient.
It does not refer to a material, such as a manufacturing process
waste, that contains any of the substances listed in subsection
(e) or (f) below. Where a manufacturing process waste is deemed
to be a hazardous waste because it contains a substance listed in
subsection (e) or (f) below, such waste will be listed in either
Sections 721.131 or 721.132 or will be identified as a hazardous
waste by the characteristics set forth in Subpart C.
e)
The commercial chemical products, manufacturing chemical
71
intermediates, or off-specification commercial chemical products
or manufacturing chemical intermediates referred to in subsections
(a) through (d) above, are identified as acute hazardous waste (H)
and are subject to the small quantity exclusion defined in Section
721.105(e). These wastes and their corresponding EPA Hazardous
Waste Numbers are:
BOARD NOTE: For the convenience of the regulated community the
primary hazardous properties of these materials have been
indicated by the letters T (Toxicity), and R (Reactivity). The
absence of a letter indicates that the compound only is listed for
acute toxicity.
Hazardous
Waste No.
Chemical
Abstracts
No.
Substance
P023
107-20-0
Acetaldehyde, chloro-
P002
591-08-2
Acetamide, N-(amino
thioxomethyl)
P057
640-19-7
Acetamide, 2-fluoro-
P058
62-74-8
Acetic acid, fluoro
-, sodium salt
P002
591-08-2
1-Acetyl-2-thiourea
P003
107-02-8
Acrolein
P070
116-06-3
Aldicarb
P203
1646-88-4
Aldicarb sulfone
P004
309-00-2
Aldrin
P005
107-18-6
Allyl alcohol
P006
20859-73-8
Aluminum phosphide (R,T)
P007
2763-96-4
5-(Amino methyl)-3-isoxazolol
P008
504-24-5
4-Amino pyridine
P009
131-74-8
Ammonium picrate (R)
P119
7803-55-6
Ammonium vanadate
P099
506-61-6
Argentate(1-), bis
(cyano-C) -, potassium
P010
7778-39-4
Arsenic acid H
3
AsO
4
P012
1327-53-3
Arsenic oxide As
2
O
3
P011
1303-28-2
Arsenic oxide As
2
O
5
P011
1303-28-2
Arsenic pentoxide
P012
1327-53-3
Arsenic tri oxide
P038
692-42-2
Arsine, di ethyl-
P036
696-28-6
Arsonous di chloride, phenyl-
P054
151-56-4
Aziridine
P067
75-55-8
Aziridine, 2-methyl
P013
542-62-1
Barium cyanide
P024
106-47-8
Benzenamine, 4-chloro-
P077
100-01-6
Benzenamine, 4-nitro-
P028
100-44-7
Benzene, (chloro methyl)-
P042
51-43-4
1,2-Benzenediol, 4-[1-hydroxy-2-
(methyl amino) ethyl] -, (R)-
P046
122-09-8
Benzeneethanamine, alpha,alpha-di
-
methyl-
P014
108-98-5
Benzenethiol
P127
1563-66-2
7-Benzofuranol, 2,3-dihydro-2,2-
dimethyl -, methylcarbamate
P188
57-64-7
Benzoic acid, 2-hydroxy
-, compound with
(3aS-cis)-1,2,3,3a,8,8a-hexahydro-
1,3a,8-tri methylpyrrolo [2,3-b] indol-5-
yl methyl carbamate ester (1:1)
P001
81-81-2
*
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-
oxo-1-phenylbutyl)
-, and salts, when
present at concentrations greater than
0.3%
72
P028
100-44-7
Benzyl chloride
P015
7440-41-7
Beryllium powder
P017
598-31-2
Bromoacetone
P018
357-57-3
Brucine
P045
39196-18-6
2-Butanone, 3,3-dimethyl-1-(methyl
-
thio)-, O-[methyl amino) carbonyl] oxime
P021
592-01-8
Calcium cyanide
P021
592-01-8
Calcium cyanide Ca(CN)
2
P189
55285-14-8
Carbamic acid, [(dibutyl
amino)- thio] -
methyl -, 2,3-dihydro-2,2-dimethyl-7-
benzofuranyl ester
P191
644-64-4
Carbamic acid, dimethyl
-, 1-[(dimethyl-
amino) carbonyl]-5-methyl-1H-pyrazol-3-
yl ester
P192
119-38-0
Carbamic acid, dimethyl
-, 3-methyl-1-
(1-methyl ethyl)-1H-pyrazol-5-yl ester
P190
1129-41-5
Carbamic acid, methyl
-, 3-methyl phenyl
ester
P127
1563-66-2
Carbofuran
P022
75-15-0
Carbon di sulfide
P095
75-44-5
Carbonic di chloride
P189
55285-14-8
Carbosulfan
P023
107-20-0
Chloro acetaldehyde
P024
106-47-8
p-Chloroaniline
P026
5344-82-1
1-(o-Chloro phenyl) thiourea
P027
542-76-7
3-Chloropropionitrile
P029
544-92-3
Copper cyanide
P029
544-92-3
Copper cyanide CuCN
P202
64-00-6
m-Cumenyl methylcarbamate
P030
Cyanides (soluble cyanide salts), not
otherwise specified
P031
460-19-5
Cyanogen
P033
506-77-4
Cyanogen chloride
P033
506-77-4
Cyanogen chloride CNCl
P034
131-89-5
2-Cyclohexyl-4,6-di
nitrophenol
P016
542-88-1
Dichloro methyl ether
P036
696-28-6
Dichloro phenylarsine
P037
60-57-1
Dieldrin
P038
692-42-2
Diethyl arsine
P041
311-45-5
Diethyl-p-nitrophenyl phosphate
P040
297-97-2
O,O-Di ethyl O-pyrazinyl
phosphorothioate
P043
55-91-4
Diisopropylfluorophosphate (DFP)
P191
644-64-4
Dimetilan
P004
309-00-2
1,4,5,8-Di methanonaphthalene,
1,2,3,4,10,10-hexa
chloro-1,4,4a,5,8,8a-
hexahydro-,
(1alpha,4alpha,4abeta,5alpha,8alpha,8ab
eta)-
P060
465-73-6
1,4,5,8-Di-methanonaphthalene,
1,2,3,4,10,10-hexa
chloro-1,4,4a,5,8,8a-
hexahydro-,
(1alpha,4alpha,4abeta,5beta,8beta,8abet
a)-
P037
60-57-1
2,7:3,6-Di methanona phth[2,3-b] oxirene,
3,4,5,6,9,9-hexa chloro-
1a,2,2a,3,6,6a,7,7a-octahydro
-,
(1aalpha,2beta,2aalpha,3beta,6beta,6aal
pha,7beta,7aalpha)-
P051
72-20-8
*
2,7:3,6-Di methanonaphth[2,3-b]
oxirene,
3,4,5,6,9,9-hexa chloro-
73
1a,2,2a,3,6,6a,7,7a-octahydro
-,
(1aalpha,2beta,2abeta,3alpha,6alpha,6ab
eta,7beta,7aalpha)
-, and metabolites
P044
60-51-5
Dimethoate
P046
122-09-8
alpha,alpha-Di methyl phenethyl amine
P047
534-52-1
*
4,6-Di nitro-o-cresol and salts
P048
51-28-5
2,4-Di nitrophenol
P020
88-85-7
Dinoseb
P085
152-16-9
Diphosphoramide, octamethyl-
P111
107-49-3
Diphosphoric acid, tetra
ethyl ester
P039
298-04-4
Disulfoton
P049
541-53-7
Dithiobiuret
P185
26419-73-8
1,3-Dithiolane-2-carbox
aldehyde, 2,4-
dimethyl -, O-[(methyl amino)- carbonyl]
-
oxime
P050
115-29-7
Endosulfan
P088
145-73-3
Endothall
P051
72-20-8
Endrin
P051
72-20-8
Endrin, and metabolites
P042
51-43-4
Epinephrine
P031
460-19-5
Ethanedi nitrile
P194
23135-22-0
Ethanimidothioc acid, 2-(di
methyl -
amino)-N-[[(methyl
amino) carbonyl] oxy]-
2-oxo-, methyl ester
P066
16752-77-5
Ethanimidothioic acid, N-[[(methyl
-
amino) carbonyl] oxy]-, methyl ester
P101
107-12-0
Ethyl cyanide
P054
151-56-4
Ethylenimine
P097
52-85-7
Famphur
P056
7782-41-4
Fluorine
P057
640-19-7
Fluoroacetamide
P058
62-74-8
Fluoroacetic acid, sodium salt
P198
23422-53-9
Formetanate hydro
chloride
P197
17702-57-7
Formparanate
P065
628-86-4
Fulminic acid, mercury (2+) salt (R,T)
P059
76-44-8
Heptachlor
P062
757-58-4
Hexaethyl tetra phosphate
P116
79-19-6
Hydrazinecarbothioamide
P068
60-34-4
Hydrazine, methyl-
P063
74-90-8
Hydrocyanic acid
P063
74-90-8
Hydrogen cyanide
P096
7803-51-2
Hydrogen phosphide
P060
465-73-6
Isodrin
P192
119-38-0
Isolan
P202
64-00-6
3-Isopropyl phenyl-N-methyl carbamate
P007
2763-96-4
3(2H)-Isoxazolone, 5-(amino
methyl)-
P196
15339-36-3
Manganese, bis(dimethyl
carbamo -
dithioato-S,S')-
P196
15339-36-3
Manganese dimethyl
dithio carbamate
P092
62-38-4
Mercury, (acetato-O)
phenyl-
P065
628-86-4
Mercury fulminate (R,T)
P082
62-75-9
Methanamine, N-methyl-N-nitroso-
P064
624-83-9
Methane, isocyanato-
P016
542-88-1
Methane, oxy bis[chloro-
P112
509-14-8
Methane, tetra nitro- (R)
P118
75-70-7
Methanethiol, tri
chloro-
P198
23422-53-9
Methanimidamide, N,N-dimethyl-N'-[3-
[[(methyl amino)-carbonyl] oxy]phenyl] -,
monohydro chloride
P197
17702-57-7
Methanimidamide, N,N-dimethyl-N'-[2-
methyl-4-[[(methyl
amino) carbonyl] oxy]-
74
phenyl]-
P199
2032-65-7
Methiocarb
P050
115-29-7
6,9-Methano-2,4,3-benzodi
oxathiepen,
6,7,8,9,10,10-hexa
chloro-1,5, 5a,6,9,9a-
hexahydro-, 3-oxide
P059
76-44-8
4,7-Methano-1H-indene, 1,4,5,6,7,8,8-
heptachloro-3a,4,7,7a-tetra
hydro-
P066
16752-77-5
Methomyl
P068
60-34-4
Methyl hydrazine
P064
624-83-9
Methyl isocyanate
P069
75-86-5
2-Methyllactonitrile
P071
298-00-0
Methyl parathion
P190
1129-41-5
Metolcarb
P129
315-8-4
Mexacarbate
P072
86-88-4
alpha-Naphthylthiourea
P073
13463-39-3
Nickel carbonyl
P073
13463-39-3
Nickel carbonyl Ni(CO)
4
, (T-4)-
P074
557-19-7
Nickel cyanide
P074
557-19-7
Nickel cyanide Ni(CN)
2
P075
54-11-5
*
Nicotine, and salts
P076
10102-43-9
Nitric oxide
P077
100-01-6
p-Nitroaniline
P078
10102-44-0
Nitrogen dioxide
P076
10102-43-9
Nitrogen oxide NO
P078
10102-44-0
Nitrogen oxide NO
2
P081
55-63-0
Nitroglycerine (R)
P082
62-75-9
N-Nitrosodi methyl amine
P084
4549-40-0
N-Nitrosomethyl vinylamine
P085
152-16-9
Octamethyl pyrophosphoramide
P087
20816-12-0
Osmium oxide OsO
4
, (T-4)-
P087
20816-12-0
Osmium tetroxide
P088
145-73-3
7-Oxabicyclo[2.2.1]
heptane-2,3-di -
carboxylic acid
P194
23135-22-0
Oxamyl
P089
56-38-2
Parathion
P034
131-89-5
Phenol, 2-cyclohexyl-4,6-di
nitro-
P128
315-18-4
Phenol, 4-(dimethyl
amino)-3,5-
dimethyl -, methyl carbamate (ester)
P199
2032-65-7
Phenol, (3,5-dimethyl-4-(methyl
thio)-,
methyl carbamate
P048
51-28-5
Phenol, 2,4-di nitro-
P047
534-52-1
*
Phenol, 2-methyl-4,6-di
nitro-, and
salts
P202
64-00-6
Phenol, 3-(1-methyl
ethyl) -, methyl
carbamate
P201
2631-37-0
Phenol, 3-methyl-5-(1-methyl
ethyl) -,
methyl carbamate
P020
88-85-7
Phenol, 2-(1-methylpropyl)-4,6-di
nitro-
P009
131-74-8
Phenol, 2,4,6-tri
nitro-, ammonium salt
(R)
P092
62-38-4
Phenylmercury acetate
P093
103-85-5
Phenylthiourea
P094
298-02-2
Phorate
P095
75-44-5
Phosgene
P096
7803-51-2
Phosphine
P041
311-45-5
Phosphoric acid, di
ethyl 4-nitrophenyl
ester
P039
298-04-4
Phosphorodi thioic acid, O,O-di
ethyl S-
[2-(ethyl thio)ethyl] ester
P094
298-02-2
Phosphorodi thioic acid, O,O-di
ethyl S-
[(ethyl thio)methyl] ester
75
P044
60-51-5
Phosphorodi thioic acid, O,O-di
methyl S-
[2-(methyl amino)-2 -oxoethyl] ester
P043
55-91-4
Phosphorofluoridic acid, bis
(1-methyl -
ethyl) ester
P089
56-38-2
Phosphorothioic acid, O,O-di
ethyl O-(4-
nitrophenyl) ester
P040
297-97-2
Phosphorothioic acid, O,O-di
ethyl O-
pyrazinyl ester
P097
52-85-7
Phosphorothioic acid, O-[4-[(di
methyl -
amino) sulfonyl)] phenyl] O,O-di methyl
ester
P071
298-00-0
Phosphorothioic acid, O,O-di
methyl O-
(4-nitrophenyl) ester
P204
57-47-6
Physostigmine
P188
57-64-7
Physostigmine salicylate
P110
78-00-2
Plumbane, tetra ethyl-
P098
151-50-8
Potassium cyanide
P098
151-50-8
Potassium cyanide KCN
P099
506-61-6
Potassium silver cyanide
P201
2631-37-0
Promecarb
P203
1646-88-4
Propanal, 2-methyl-2-(methyl-
sulfonyl) -, O-[(methyl amino) carbonyl]
oxime
P070
116-06-3
Propanal, 2-methyl-2-(methyl
thio)-, O-
[(methyl amino) carbonyl] oxime
P101
107-12-0
Propane nitrile
P027
542-76-7
Propane nitrile, 3-chloro-
P069
75-86-5
Propane nitrile, 2-hydroxy-2-methyl-
P081
55-63-0
1,2,3-Propane triol, tri nitrate- (R)
P017
598-31-2
2-Propanone, 1-bromo-
P102
107-19-7
Propargyl alcohol
P003
107-02-8
2-Propenal
P005
107-18-6
2-Propen-1-ol
P067
75-55-8
1,2-Propylenimine
P102
107-19-7
2-Propyn-1-ol
P008
504-24-5
4-Pyridinamine
P075
54-11-5
*
Pyridine, 3-(1-methyl-2-pyrrolidinyl)
-,
(S)- and salts
P204
57-47-6
Pyrrolo [2,3-b] indol-5-ol,
1,2,3,3a,8,8a-hexa
hydro-1,3a,8-tri -
methyl -, methyl carbamate (ester), (3aS-
cis)-
P114
12039-52-0
Selenious acid, di
thallium (1+) salt
P103
630-10-4
Selenourea
P104
506-64-9
Silver cyanide
P104
506-64-9
Silver cyanide AgCN
P105
26628-22-8
Sodium azide
P106
143-33-9
Sodium cyanide
P106
143-33-9
Sodium cyanide NaCN
P108
57-24-9
*
Strychnidin-10-one, and salts
P018
357-57-3
Strychnidin-10-one, 2,3-di
methoxy-
P108
57-24-9
*
Strychnine and salts
P115
7446-18-6
Sulfuric acid, di
thallium (1+) salt
P109
3689-24-5
Tetraethyldithiopyrophosphate
P110
78-00-2
Tetraethyl lead
P111
107-49-3
Tetraethylpyrophosphate
P112
509-14-8
Tetranitromethane (R)
P062
757-58-4
Tetraphosphoric acid, hexa
ethyl ester
P113
1314-32-5
Thallic oxide
P113
1314-32-5
Thallium oxide Tl
2
O
3
P114
12039-52-0
Thallium (I) selenite
76
P115
7446-18-6
Thallium (I) sulfate
P109
3689-24-5
Thiodiphosphoric acid, tetra
ethyl ester
P045
39196-18-4
Thiofanox
P049
541-53-7
Thioimidodicarbonic di amide
[(H
2
N)C(S)]
2
NH
P014
108-98-5
Thiophenol
P116
79-19-6
Thiosemicarbazide
P026
5344-82-1
Thiourea, (2-chloro
phenyl)-
P072
86-88-4
Thiourea, 1-naphthalenyl-
P093
103-85-5
Thiourea, phenyl-
P123
8001-35-2
Toxaphene
P185
26419-73-8
Tirpate
P118
75-70-7
Trichloro methane thiol
P119
7803-55-6
Vanadic acid, ammonium salt
P120
1314-62-1
Vanadium oxide V
2
O
5
P120
1314-62-1
Vanadium pentoxide
P084
4549-40-0
Vinylamine, N-methyl-N-nitroso-
P001
81-81-2
*
Warfarin, and salts, when present at
concentrations greater than 0.3%
P121
557-21-1
Zinc cyanide
P121
557-21-1
Zinc cyanide Zn(CN)
2
P205
137-30-4
Zinc, bis (dimethyl carbamo dithioato-
S,S')-
P122
1314-84-7
Zinc phosphide Zn
3
P
2
, when present at
concentrations greater than 10% (R,T)
P205
137-30-4
Ziram
BOARD NOTE: An asterisk (*) following the CAS number indicates
that the CAS number is given for the parent compound only.
f)
The commercial chemical products, manufacturing chemical
intermediates, or off-specification commercial chemical products
referred to in subsections (a) through (d) above, are identified
as toxic wastes (T) unless otherwise designated and are subject to
the small quantity exclusion defined in Section 721.105(a) and
(g). These wastes and their corresponding EPA Hazardous Waste
Numbers are:
BOARD NOTE: For the convenience of the regulated community, the
primary hazardous properties of these materials have been
indicated by the letters T (Toxicity), R (Reactivity), I
(Ignitability), and C (Corrosivity). The absence of a letter
indicates that the compound is only listed for toxicity.
Hazardous
Waste No.
Chemical
Abstracts
No.
Substance
U394
30558-43-1
A2213
U365
2212-67-1
H-Azepine-1-carbo
thioic acid, hexa
-
hydro-, S-ethyl ester
U001
75-07-0
Acetaldehyde (I)
U034
75-87-6
Acetaldehyde, tri
chloro -
U187
62-44-2
Acetamide, N-(4-ethoxyphenyl)-
U005
53-96-3
Acetamide, N-9H-fluoren-2-yl-
U240
P 94-75-7
Acetic acid, (2,4-di
chloro phenoxy) -,
salts and esters
U112
141-78-6
Acetic acid, ethyl ester (I)
U144
301-04-2
Acetic acid, lead (2+) salt
U214
563-68-8
Acetic acid, thallium (1+) salt
See F027
93-76-5
Acetic acid, (2,4,5-tri
chloro phenoxy)-
77
UOO2
67-64-1
Acetone (I)
UOO3
75-05-8
Acetonitrile (I,T)
U004
98-86-2
Acetophenone
U005
53-96-3
2-Acetyl aminofluorene
U006
75-36-5
Acetyl chloride (C,R,T)
U007
79-06-1
Acrylamide
U008
79-10-7
Acrylic acid (I)
U009
107-13-1
Acrylonitrile
U011
61-82-5
Amitrole
U012
62-53-3
Aniline (I,T)
U136
75-60-5
Arsinic acid, di methyl-
U014
492-80-8
Auramine
U015
115-02-6
Azaserine
U010
50-07-7
Azirino [2',3':3,4] pyrrolo [1,2-a] indole-
4,7-di one, 6-amino-8-[[(amino
carbonyl) -
oxy]methyl]-1,1a,2,8,8a,8b-hexa
hydro-
8a-methoxy-5-methyl
-, [1a-S-
(1aalpha,8beta,8aalpha,8balpha)]-
U280
101-27-9
Barban
U278
22781-23-3
Bendiocarb
U364
22961-82-6
Bendiocarb phenol
U271
17804-35-2
Benomyl
U157
56-49-5
Benz[j]aceanthrylene, 1,2-di
hydro-3-
methyl-
U016
225-51-4
Benz(c)acridine
U017
98-87-3
Benzal chloride
U192
23950-58-5
Benzamide, 3,5-di
chloro -N-(1,1-di -
methyl-2-propynyl)-
U018
56-55-3
Benz[a]anthracene
U094
57-97-6
Benz[a]anthracene, 7,12-di
methyl-
U012
62-53-3
Benzen amine (I,T)
U014
492-80-8
Benzen amine, 4,4'-carbonimidoyl
bis[N,N-
dimethyl-
U049
3165-93-3
Benzen amine, 4-chloro -2-methyl -,
hydrochloride
U093
60-11-7
Benzen amine, N,N-di methyl-4-(phenyl -
azo)-
U328
95-53-4
Benzen amine, 2-methyl-
U353
106-49-0
Benzen amine, 4-methyl-
U158
101-14-4
Benzen amine, 4,4'-methylene
bis[2-
chloro -
U222
636-21-5
Benzen amine, 2-methyl -, hydrochloride
U181
99-55-8
Benzen amine, 2-methyl-5-nitro-
U019
71-43-2
Benzene (I,T)
U038
510-15-6
Benzeneacetic acid, 4-chloro
-alpha-(4-
chloro phenyl)-alpha-hydroxy
-, ethyl
ester
U030
101-55-3
Benzene, 1-bromo-4-phenoxy-
U035
305-03-3
Benzenebutanoic acid, 4-[bis
(2-chloro -
ethyl) amino]-
U037
108-90-7
Benzene, chloro -
U221
25376-45-8
Benzenedi amine, ar-methyl-
U028
117-81-7
1,2-Benzenedi carboxylic acid, bis
(2-
ethylhexyl) ester
U069
84-74-2
1,2-Benzenedi carboxylic acid, di
butyl
ester
U088
84-66-2
1,2-Benzenedi carboxylic acid, di
ethyl
ester
U102
131-11-3
1,2-Benzenedi carboxylic acid, di
methyl
ester
U107
117-84-0
1,2-Benzenedi carboxylic acid, di
octyl
78
ester
U070
95-50-1
Benzene, 1,2-di chloro -
U071
541-73-1
Benzene, 1,3-di chloro -
U072
106-46-7
Benzene, 1,4-di chloro -
U060
72-54-8
Benzene, 1,1'-(2,2-di
chloro ethylidene) -
bis[4-chloro -
U017
98-87-3
Benzene, (di chloro methyl)-
U223
26471-62-5
Benzene, 1,3-di isocyanatomethyl- (R,T)
U239
1330-20-7
Benzene, di methyl- (I,T)
U201
108-46-3
1,3-Benzenedi ol
U127
118-74-1
Benzene, hexa chloro -
U056
110-82-7
Benzene, hexa hydro- (I)
U220
108-88-3
Benzene, methyl-
U105
121-14-2
Benzene, 1-methyl-2,4-di
nitro-
U106
606-20-2
Benzene, 2-methyl-1,3-di
nitro-
U055
98-82-8
Benzene, (1-methyl
ethyl)- (I)
U169
98-95-3
Benzene, nitro-
U183
608-93-5
Benzene, penta chloro -
U185
82-68-8
Benzene, penta chloro nitro-
U020
98-09-9
Benzenesulfonic acid chloride (C,R)
U020
98-09-9
Benzenesulfonyl chloride (C,R)
U207
95-94-3
Benzene, 1,2,4,5-tetra
chloro -
U061
50-29-3
Benzene, 1,1'-(2,2,2-tri
chloro ethyl-
idene) bis[4-chloro -
U247
72-43-5
Benzene, 1,1'-(2,2,2-tri
chloro ethyl-
idene) bis[4-methoxy-
U023
98-07-7
Benzene, (tri chloro methyl)-
U234
99-35-4
Benzene, 1,3,5-tri
nitro-
U021
92-87-5
Benzidene
U202
P 81-07-2
1,2-Benzisothiazol-3(2H)-one, 1,1-di
-
oxide, and salts
U203
94-59-7
1,3-Benzodi oxole, 5-(2-propenyl)-
U141
120-58-1
1,3-Benzodi oxole, 5-(1-propenyl)-
U090
94-58-6
1,3-Benzodi oxole, 5-propyl-
U278
22781-23-3
1,3-Benzo dioxol-4-ol, 2,2-di
methyl -,
methyl carbamate
U364
22961-82-6
1,3-Benzo dioxol-4-ol, 2,2-dimethyl-
U367
1563-38-8
7-Benzo furanol, 2,3-di hydro-2,2-di -
methyl-
U064
189-55-9
Benzo[rst]pentaphene
U248
P 81-81-2
2H-1-Benzopyran-2-one, 4-hydroxy-3-(3-
oxo-1-phenyl butyl) -, and salts, when
present at concentrations of 0.3% or
less
U022
50-32-8
Benzo[a]pyrene
U197
106-51-4
p-Benzoquinone
U023
98-07-7
Benzotri chloride (C,R,T)
U085
1464-53-5
2,2'-Bioxirane
U021
92-87-5
[1,1'-Biphenyl]-4,4'-di
amine
U073
91-94-1
[1,1'-Biphenyl]-4,4'-di
amine, 3,3'-di -
chloro -
U091
119-90-4
[1,1'-Biphenyl]-4,4'-di
amine, 3,3'-di -
methoxy-
U095
119-93-7
[1,1'-Biphenyl]-4,4'-di
amine, 3,3'-di -
methyl-
U401
97-74-5
Bis(dimethyl thiocarbamoyl) sulfide
U400
120-54-7
Bis(penta methylene) thiuram tetra sulfide
U225
75-25-2
Bromoform
U030
101-55-3
4-Bromophenyl phenyl ether
U128
87-68-3
1,3-Butadi ene, 1,1,2,3,4,4-hexa
chloro -
U172
924-16-3
1-Butan amine, N-butyl-N-nitroso-
79
U031
71-36-3
1-Butanol (I)
U159
78-93-3
2-Butanone (I,T)
U160
1338-23-4
2-Butanone, peroxide (R,T)
U053
4170-30-3
2-Butenal
U074
764-41-0
2-Butene, 1,4-di chloro - (I,T)
U143
303-34-4
2-Butenoic acid, 2-methyl
-, 7-[[2,3-di -
hydroxy-2-(1-methoxy
ethyl)-3-methyl-1-
oxobutoxy] methyl]-2,3,5,7a-tetra
hydro-
1H-pyrrolizin-1-yl ester, [1S-
[1alpha(Z), 7(2S*,3R*), 7aalpha]]-
U031
71-36-3
n-Butyl alcohol (I)
U392
2008-41-5
Butylate
U136
75-60-5
Cacodylic acid
U032
13765-19-0
Calcium chromate
U372
10605-21-7
Carbamic acid, 1H-benz
imidazol-2-yl,
methyl ester
U271
17804-35-2
Carbamic acid, [1-[(butyl
amino) -
carbonyl]-1H-benz
imidazol-2-yl] -,
methyl ester
U375
55406-53-6
Carbamic acid, butyl
-, 3-iodo-2-
propynyl ester
U280
101-27-9
Carbamic acid, (3-chloro
phenyl) -, 4-
chloro-2-butynyl ester
U238
51-79-6
Carbamic acid, ethyl ester
U178
615-53-2
Carbamic acid, methyl
nitroso -, ethyl
ester
U373
122-42-9
Carbamic acid, phenyl
-, 1-methyl ethyl
ester
U409
23564-05-8
Carbamic acid, [1,2-phenylenebis
(imino -
carbono thioyl)] bis-, dimethyl ester
U097
79-44-7
Carbamic chloride, di
methyl-
U379
136-30-1
Carbamo dithioic acid, dibutyl, sodium
salt
U277
95-06-7
Carbamo dithioic acid, diethyl
-, 2-
chloro-2-propenyl ester
U381
148-18-5
Carbamo dithioic acid, diethyl
-, sodium
salt
U383
128-03-0
Carbamodithioic acid, dimethyl,
potassium salt
U382
128-04-1
Carbamo dithioic acid, dimethyl
-, sodium
salt
U376
144-34-3
Carbamo dithioic acid, dimethyl
-, tetra -
anhydro sulfide with ortho
thioselenious
acid
U114
P 111-54-6
Carbamodi thioic acid, 1,2-ethanedi
yl-
bis-, salts and esters
U378
51026-28-9
Carbamo dithioic acid, (hydroxymethyl)
-
methyl -, mono potassium salt
U384
137-42-8
Carbamo dithioic acid, methyl
-, mono -
sodium salt
U377
137-41-7
Carbamo dithioic acid, methyl,- mono
-
potassium salt
U062
2303-16-4
Carbamothioic acid, bis
(1-methyl -
ethyl) -, S-(2,3-di chloro -2-propenyl)
ester
U389
2303-17-5
Carbamo thioic acid, bis(1-methyl
-
ethyl) -, S-(2,3,3-tri chloro-2-propenyl)
ester
U392
2008-41-5
Carbamo thioic acid, bis(2-methyl
-
propyl) -, S-ethyl ester
U391
1114-71-2
Carbamo thioic acid, butyl
ethyl-, S-
80
propyl ester
U386
1134-23-2
Carbamo thioic acid, cyclo
hexylethyl-,
S-ethyl ester
U390
759-94-4
Carbamo thioic acid, dipropyl
-, S-ethyl
ester
U387
52888-80-9
Carbamo thioic acid, dipropyl
-, S-
(phenyl methyl) ester
U385
1929-77-7
Carbamo thioic acid, dipropyl
-, S-propyl
ester
U279
63-25-2
Carbaryl
U372
10605-21-7
Carbendazim
U367
1563-38-8
Carbofuran phenol
U215
6533-73-9
Carbonic acid, di
thallium (1+) salt
U033
353-50-4
Carbonic di fluoride
U156
79-22-1
Carbonochloridic acid, methyl ester
(I,T)
U033
353-50-4
Carbon oxyfluoride (R,T)
U211
56-23-5
Carbon tetra chloride
U034
75-87-6
Chloral
U035
305-03-3
Chlorambucil
U036
57-74-9
Chlordanealpha and gamma isomers
U026
494-03-1
Chlornaphazin
U037
108-90-7
Chloro benzene
U038
510-15-6
Chloro benzilate
U039
59-50-7
p-Chloro -m-cresol
U042
110-75-8
2-Chloro ethyl vinyl ether
U044
67-66-3
Chloro form
U046
107-30-2
Chloro methyl methyl ether
U047
91-58-7
beta-Chloro naphthalene
U048
95-57-8
o-Chloro phenol
U049
3165-93-3
4-Chloro -o-toluidine, hydrochloride
U032
13765-19-0
Chromic acid H
2
CrO
4
, calcium salt
U050
218-01-9
Chrysene
U393
137-29-1
Copper, bis(dimethyl
carbamo dithioato-
S,S')-
U393
137-29-1
Copper dimethyl dithio carbamate
U051
Creosote
U052
1319-77-3
Cresol (Cresylic acid)
U053
4170-30-3
Crotonaldehyde
U055
98-82-8
Cumeme (I)
U246
506-68-3
Cyanogen bromide CNBr
U386
1134-23-2
Cycloate
U197
106-51-4
2,5-Cyclohexa diene-1,4-di one
U056
110-82-7
Cyclohexane (I)
U129
58-89-9
Cyclohexane, 1,2,3,4,5,6-hexa
chloro -,
(1alpha,2alpha,3beta,4alpha,5alpha,6bet
a)-
U057
108-94-1
Cyclohexanone (I)
U130
77-47-4
1,3-Cyclopenta diene, 1,2,3,4,5,5-hexa
-
chloro -
U058
50-18-0
Cyclophosphamide
U240
P 94-75-7
2,4-D, salts and esters
U059
20830-81-3
Daunomycin
U366
533-74-4
Dazomet
U060
72-54-8
DDD
U061
50-29-3
DDT
U062
2303-16-4
Diallate
U063
53-70-3
Dibenz[a,h]anthracene
U064
189-55-9
Dibenzo[a,i]pyrene
U066
96-12-8
1,2-Di bromo-3-chloro propane
U069
84-74-2
Dibutyl phthalate
81
U070
95-50-1
o-Dichloro benzene
U071
541-73-1
m-Dichloro benzene
U072
106-46-7
p-Dichloro benzene
U073
91-94-1
3,3'-Di chloro benzidine
U074
764-41-0
1,4-Di chloro -2-butene (I,T)
U075
75-71-8
Dichloro difluoromethane
U078
75-35-4
1,1-Di chloro ethylene
U079
156-60-5
1,2-Di chloro ethylene
U025
111-44-4
Dichloro ethyl ether
U027
108-60-1
Dichloro isopropyl ether
U024
111-91-1
Dichloro methoxy ethane
U081
120-83-2
2,4-Di chloro phenol
U082
87-65-0
2,6-Di chloro phenol
U084
542-75-6
1,3-Di chloro propene
U085
1464-53-5
1,2:3,4-Di epoxybutane (I,T)
U395
5952-26-1
Diethylene glycol, dicarbamate
U108
123-91-1
1,4-Di ethyleneoxide
U028
117-81-7
Diethylhexyl phthalate
U086
1615-80-1
N,N'-Di ethylhydrazine
U087
3288-58-2
O,O-Di ethyl S-methyl di
thiophosphate
U088
84-66-2
Diethyl phthalate
U089
56-53-1
Diethylstilbestrol
U090
94-58-6
Dihydrosafrole
U091
119-90-4
3,3'-Di methoxybenzidine
U092
124-40-3
Dimethyl amine (I)
U093
60-11-7
p-Dimethyl aminoazobenzene
U094
57-97-6
7,12-Di methyl benz[a]anthracene
U095
119-93-7
3,3'-Di methyl benzidine
U096
80-15-9
alpha, alpha-Di methyl -
benzylhydroperoxide (R)
U097
79-44-7
Dimethyl carbamoyl chloride
U098
57-14-7
1,1-Di methyl hydrazine
U099
540-73-8
1,2-Di methyl hydrazine
U101
105-67-9
2,4-Di methyl phenol
U102
131-11-3
Dimethyl phthalate
U103
77-78-1
Dimethyl sulfate
U105
121-14-2
2,4-Di nitrotoluene
U106
606-20-2
2,6-Di nitrotoluene
U107
117-84-0
Di-n-octyl phthalate
U108
123-91-1
1,4-Di oxane
U109
122-66-7
1,2-Di phenyl hydrazine
U110
142-84-7
Dipropyl amine (I)
U111
621-64-7
Di-n-propyl nitros amine
U403
97-77-8
Disulfiram
U041
106-89-8
Epichloro hydrin
U390
759-94-4
EPTC
U001
75-07-0
Ethanal (I)
U404
121-44-8
Ethanamine, N,N-diethyl-
U174
55-18-5
Ethanamine, N- ethyl-N-nitroso-
U155
91-80-5
1,2-Ethanedi amine, N,N-di methyl-N'-2-
pyridinyl-N'-(2-thienyl
methyl)-
U067
106-93-4
Ethane, 1,2-di bromo-
U076
75-34-3
Ethane, 1,1-di chloro -
U077
107-06-2
Ethane, 1,2-di chloro -
U131
67-72-1
Ethane, hexa chloro -
U024
111-91-1
Ethane, 1,1'-[methyl
enebis(oxy)] bis[2-
chloro -
U117
60-29-7
Ethane, 1,1'-oxy bis- (I)
U025
111-44-4
Ethane, 1,1'-oxy bis[2-chloro -
U184
76-01-7
Ethane, penta chloro -
U208
630-20-6
Ethane, 1,1,1,2-tetra
chloro -
82
U209
79-34-5
Ethane, 1,1,2,2-tetra
chloro -
U218
62-55-5
Ethanethioamide
U226
71-55-6
Ethane, 1,1,1-tri
chloro -
U227
79-00-5
Ethane, 1,1,2-tri
chloro -
U410
59669-26-0
Ethanimidothioic acid, N,N'- [thiobis
-
[(methyl imino) carbonyl oxy]]bis-,
dimethyl ester
U394
30558-43-1
Ethanimido thioic acid, 2-(dimethyl
-
amino)-N-hydroxy-2-oxo
-, methyl ester
U359
110-80-5
Ethanol, 2-ethoxy-
U173
1116-54-7
Ethanol, 2,2'-(nitroso
imino) bis-
U395
5952-26-1
Ethanol, 2,2'-oxy
bis-, dicarbamate
U004
98-86-2
Ethanone, 1-phenyl-
U043
75-01-4
Ethene, chloro -
U042
110-75-8
Ethene, (2-chloro
ethoxy)-
U078
75-35-4
Ethene, 1,1-di chloro -
U079
156-60-5
Ethene, 1,2-di chloro -, (E)-
U210
127-18-4
Ethene, tetra chloro -
U228
79-01-6
Ethene, tri chloro -
U112
141-78-6
Ethyl acetate (I)
U113
140-88-5
Ethyl acrylate (I)
U238
51-79-6
Ethyl carbamate (urethane)
U117
60-29-7
Ethyl ether
U114
P 111-54-6
Ethylenebisdithiocarbamic acid, salts
and esters
U067
106-93-4
Ethylene di bromide
U077
107-06-2
Ethylene di chloride
U359
110-80-5
Ethylene glycol monoethyl ether
U115
75-21-8
Ethylene oxide (I,T)
U116
96-45-7
Ethylenethiourea
U076
75-34-3
Ethylidene di chloride
U118
97-63-2
Ethyl methacrylate
U119
62-50-0
Ethyl methanesulfonate
U407
14324-55-1
Ethyl Ziram
U396
14484-64-1
Ferbam
U120
206-44-0
Fluoranthene
U122
50-00-0
Formaldehyde
U123
64-18-6
Formic acid (C,T)
U124
110-00-9
Furan (I)
U125
98-01-1
2-Furancarboxaldehyde (I)
U147
108-31-6
2,5-Furandi one
U213
109-99-9
Furan, tetra hydro- (I)
U125
98-01-1
Furfural (I)
U124
110-00-9
Furfuran (I)
U206
18883-66-4
Glucopyranose, 2-deoxy-2-(3-methyl-3-
nitroso ureido) -, D-
U206
18883-66-4
D-Glucose, 2-deoxy-2-[[(
methyl nitroso -
amino)-carbonyl] amino]-
U126
765-34-4
Glycidylaldehyde
U163
70-25-7
Guanidine, N-methyl-N'-nitro-N-nitroso-
U127
118-74-1
Hexachloro benzene
U128
87-68-3
Hexachloro butadi ene
U130
77-47-4
Hexachloro cyclopenta diene
U131
67-72-1
Hexachloro ethane
U132
70-30-4
Hexachloro phene
U243
1888-71-7
Hexachloro propene
U133
302-01-2
Hydrazine (R,T)
U086
1615-80-1
Hydrazine, 1,2-di
ethyl-
U098
57-14-7
Hydrazine, 1,1-di
methyl-
U099
540-73-8
Hydrazine, 1,2-di
methyl-
U109
122-66-7
Hydrazine, 1,2-di
phenyl-
83
U134
7664-39-3
Hydrofluoric acid (C,T)
U134
7664-39-3
Hydrogen fluoride (C,T)
U135
7783-06-4
Hydrogen sulfide
U135
7783-06-4
Hydrogen sulfide H
2
S
U096
80-15-9
Hydroperoxide, 1-methyl-1-phenyl
ethyl-
(R)
U116
96-45-7
2-Imidazolidinethione
U137
193-39-5
Indeno [1,2,3-cd] pyrene
U375
55406-53-6
3-Iodo-2-propynyl n-
butylcarbamate
U396
14484-64-1
Iron, tris(dimethyl carbamo dithioato -
S,S')-
U190
85-44-9
1,3-Isobenzofurandi
one
U140
78-83-1
Isobutyl alcohol (I,T)
U141
120-58-1
Isosafrole
U142
143-50-0
Kepone
U143
303-34-4
Lasiocarpene
U144
301-04-2
Lead acetate
U146
1335-32-6
Lead, bis(acetato-O) tetrahydroxytri -
U145
7446-27-7
Lead phosphate
U146
1335-32-6
Lead subacetate
U129
58-89-9
Lindane
U163
70-25-7
MNNG
U147
108-31-6
Maleic anhydride
U148
123-33-1
Maleic hydrazide
U149
109-77-3
Malononitrile
U150
148-82-3
Melphalan
U151
7439-97-6
Mercury
U384
137-42-8
Metam Sodium
U152
126-98-7
Methacrylonitrile (I,T)
U092
124-40-3
Methan amine, N-methyl- (I)
U029
74-83-9
Methane, bromo-
U045
74-87-3
Methane, chloro- (I,T)
U046
107-30-2
Methane, chloro methoxy -
U068
74-95-3
Methane, dibromo-
U080
75-09-2
Methane, dichloro -
U075
75-71-8
Methane, dichloro difluoro -
U138
74-88-4
Methane, iodo-
U119
62-50-0
Methanesulfonic acid, ethyl ester
U211
56-23-5
Methane, tetrachloro -
U153
74-93-1
Methanethiol (I,T)
U225
75-25-2
Methane, tribromo-
U044
67-66-3
Methane, trichloro -
U121
75-69-4
Methane, trichloro fluoro -
U036
57-74-9
4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8-
octachloro -2,3,3a,4,7,7a-hexa
hydro-
U154
67-56-1
Methanol (I)
U155
91-80-5
Methapyrilene
U142
143-50-0
1,3,4-Metheno-2H-cyclobuta
[cd]pentalen-
2-one, 1,1a,3,3a,4,5,5,5a,5b,6-
decachloro octahydro-
U247
72-43-5
Methoxychlor
U154
67-56-1
Methyl alcohol (I)
U029
74-83-9
Methyl bromide
U186
504-60-9
1-Methyl butadiene (I)
U045
74-87-3
Methyl chloride (I,T)
U156
79-22-1
Methyl chloro carbonate (I,T)
U226
71-55-6
Methyl chloro form
U157
56-49-5
3-Methyl cholanthrene
U158
101-14-4
4,4'-Methyl enebis(2-chloro aniline)
U068
74-95-3
Methylene bromide
U080
75-09-2
Methylene chloride
84
U159
78-93-3
Methyl ethyl ketone (MEK) (I,T)
U160
1338-23-4
Methyl ethyl ketone peroxide (R,T)
U138
74-88-4
Methyl iodide
U161
108-10-1
Methyl isobutyl ketone (I)
U162
80-62-6
Methyl methacrylate (I,T)
U161
108-10-1
4-Methyl-2-pentanone (I)
U164
56-04-2
Methyl thiouracil
U010
50-07-7
Mitomycin C
U365
2212-67-1
Molinate
U059
20830-81-3
5,12-Naphthacenedi
one, 8-acetyl-10-[(3-
amino-2,3,6-tri deoxy)- alpha-L-lyxo-
hexapyranosyl )oxyl]-7,8,9,10-tetra
-
hydro-6,8,11-tri hydroxy-1-methoxy
-,
(8S-cis)-
U167
134-32-7
1-Naphthalen amine
U168
91-59-8
2-Naphthalen amine
U026
494-03-1
Naphthalene amine, N,N'- bis(2-chloro -
ethyl)-
U165
91-20-3
Naphthalene
U047
91-58-7
Naphthalene, 2-chloro
-
U166
130-15-4
1,4-Naphthalenedi
one
U236
72-57-1
2,7-Naphthalenedi
sulfonic acid, 3,3
'-
[(3,3'-di methyl-[1,1'-biphenyl]-4,4'-
diyl)bis(azo)bis[5-amino-4-hydroxy]
-,
tetrasodium salt
U279
63-25-2
1-Naphthalenol, methyl carbamate
U166
130-15-4
1,4-Naphthoquinone
U167
134-32-7
alpha- Naphthyl amine
U168
91-59-8
beta-Naphthyl amine
U217
10102-45-1
Nitric acid, thallium (1+) salt
U169
98-95-3
Nitrobenzene (I,T)
U170
100-02-7
p-Nitrophenol
U171
79-46-9
2-Nitro propane (I,T)
U172
924-16-3
N-Nitroso di-n-butyl amine
U173
1116-54-7
N-Nitroso diethanol amine
U174
55-18-5
N-Nitroso diethylamine
U176
759-73-9
N-Nitroso-N-ethyl
urea
U177
684-93-5
N-Nitroso-N-methyl
urea
U178
615-53-2
N-Nitroso-N-methyl
urethane
U179
100-75-4
N-Nitroso piperidine
U180
930-55-2
N-Nitroso pyrrolidine
U181
99-55-8
5-Nitro-o-toluidine
U193
1120-71-4
1,2-Oxathiolane, 2,2-di
oxide
U058
50-18-0
2H-1,3,2-Oxazaphosphorin-2-amine, N,N-
bis(2-chloro ethyl) tetrahydro-, 2-oxide
U115
75-21-8
Oxirane (I,T)
U126
765-34-4
Oxiranecarboxyaldehyde
U041
106-89-8
Oxirane, ( chloro methyl )-
U182
123-63-7
Paraldehyde
U391
1114-71-2
Pebulate
U183
608-93-5
Pentachloro benzene
U184
76-01-7
Pentachloro ethane
U185
82-68-8
Pentachloro nitrobenzene (PCNB)
See F027
87-86-5
Pentachloro phenol
U161
108-10-1
Pentanol, 4-methyl-
U186
504-60-9
1,3-Penta diene (I)
U187
62-44-2
Phenacetin
U188
108-95-2
Phenol
U048
95-57-8
Phenol, 2-chloro -
U039
59-50-7
Phenol, 4-chloro -3-methyl-
U081
120-83-2
Phenol, 2,4-di chloro -
85
U082
87-65-0
Phenol, 2,6-di chloro -
U089
56-53-1
Phenol, 4,4'-(1,2-di
ethyl-1,2-ethenedi
-
yl)bis-, (E)-
U101
105-67-9
Phenol, 2,4-di methyl-
U052
1319-77-3
Phenol, methyl-
U132
70-30-4
Phenol, 2,2'-methyl
enebis[3,4,6-tri -
chloro -
U411
114-26-1
Phenol, 2-(1-methyl
ethoxy) -, methyl -
carbamate
U170
100-02-7
Phenol, 4-nitro-
See F027
87-86-5
Phenol, pentachloro -
See F027
58-90-2
Phenol, 2,3,4,6-tetra
chloro -
See F027
95-95-4
Phenol, 2,4,5-tri
chloro -
See F027
88-06-2
Phenol, 2,4,6-tri
chloro -
U150
148-82-3
L-Phenyl alanine , 4-[bis(2-chloro ethyl) -
amino]-
U145
7446-27-7
Phosphoric acid, lead (2+) salt (2:3)
U087
3288-58-2
Phosphorodi thioic acid, O,O-di ethyl S-
methyl ester
U189
1314-80-3
Phosphorus sulfide (R)
U190
85-44-9
Phthalic anhydride
U191
109-06-8
2-Picoline
U179
100-75-4
Piperidine, 1-nitroso-
U400
120-54-7
Piperidine, 1,1'-(
tetrathiodicarbono -
thioyl)- bis-
U383
128-03-0
Potassium dimethyl dithio carbamate
U378
51026-28-9
Potassium n-hydroxy methyl-n-methyl di-
thiocarbamate
U377
137-41-7
Potassium n- methyl dithio carbamate
U192
23950-58-5
Pronamide
U194
107-10-8
1-Propan amine (I,T)
U111
621-64-7
1-Propan amine, N-nitroso-N-propyl-
U110
142-84-7
1-Propan amine, N- propyl- (I)
U066
96-12-8
Propane, 1,2-di bromo-3-chloro -
U083
78-87-5
Propane, 1,2-di chloro -
U149
109-77-3
Propanedi nitrile
U171
79-46-9
Propane, 2-nitro- (I,T)
U027
108-60-1
Propane, 2,2'-oxy
bis[2-chloro -
See F027
93-72-1
Propanoic acid, 2-(2,4,5-tri
chloro -
phenoxy)-
U193
1120-71-4
1,3-Propane sultone
U235
126-72-7
1-Propanol, 2,3-di
bromo-, phosphate
(3:1)
U140
78-83-1
1-Propanol, 2-methyl- (I,T)
U002
67-64-1
2-Propanone (I)
U007
79-06-1
2-Propenamide
U084
542-75-6
1-Propene, 1,3-di
chloro -
U243
1888-71-7
1-Propene, 1,1,2,3,3,3-hexa
chloro -
U009
107-13-1
2-Propenenitrile
U152
126-98-7
2-Propenenitrile, 2-methyl- (I,T)
U008
79-10-7
2-Propenoic acid (I)
U113
140-88-5
2-Propenoic acid, ethyl ester (I)
U118
97-63-2
2-Propenoic acid, 2-methyl
-, ethyl
ester
U162
80-62-6
2-Propenoic acid, 2-methyl
-, methyl
ester (I,T)
U373
122-42-9
Propham
U411
114-26-1
Propoxur
See F027
93-72-1
Propionic acid, 2-(2,4,5-tri
chloro -
phenoxy)-
U194
107-10-8
n-Propyl amine (I,T)
86
U083
78-87-5
Propylene di chloride
U387
52888-80-9
Prosulfocarb
U148
123-33-1
3,6-Pyridazinedi one, 1,2-di hydro-
U196
110-86-1
Pyridine
U191
109-06-8
Pyridine, 2-methyl-
U237
66-75-1
2,4-(1H,3H)- Pyrimidinedi one, 5-[bis(2-
chloro ethyl) amino]-
U164
58-04-2
4(1H)- Pyrimidinone, 2,3-di
hydro-6-
methyl-2-thioxo-
U180
930-55-2
Pyrrolidine, 1-nitroso-
U200
50-55-5
Reserpine
U201
108-46-3
Resorcinol
U202
P 81-07-2
Saccharin and salts
U203
94-59-7
Safrole
U204
7783-00-8
Selenious acid
U204
7783-00-8
Selenium di oxide
U205
7488-56-4
Selenium sulfide
U205
7488-56-4
Selenium sulfide SeS
2
(R,T)
U376
144-34-3
Selenium, tetrakis (dimethyl dithio -
carbamate)
U015
115-02-6
L-Serine, diazoacetate (ester)
See F027
93-72-1
Silvex (2,4,5-TP)
U379
136-30-1
Sodium dibutyl dithio carbamate
U381
148-18-5
Sodium diethyl dithio carbamate
U382
128-04-1
Sodium dimethyl dithio carbamate
U206
18883-66-4
Streptozotocin
U277
95-06-7
Sulfallate
U103
77-78-1
Sulfuric acid, dimethyl ester
U189
1314-80-3
Sulfur phosphide (R)
See F027
93-76-5
2,4,5-T
U402
1634-02-2
Tetrabutylthiuram disulfide
U207
95-94-3
1,2,4,5-Tetra chloro benzene
U208
630-20-6
1,1,1,2-Tetra chloro ethane
U209
79-34-5
1,1,2,2-Tetra chloro ethane
U210
127-18-4
Tetrachloro ethylene
See F027
58-90-2
2,3,4,6-Tetra chloro phenol
U213
109-99-9
Tetrahydrofuran (I)
U401
97-74-5
Tetramethyl thiuram monosulfide
U366
533-74-4
2H-1,3,5-Thia diazine- 2-thione, tetra
-
hydro-3,5-di methyl-
U214
563-68-8
Thallium (I) acetate
U215
6533-73-9
Thallium (I) carbonate
U216
7791-12-0
Thallium (I) chloride
U216
7791-12-0
Thallium chloride
TlCl
U217
10102-45-1
Thallium (I) nitrate
U218
62-55-5
Thioacetamide
U410
59669-26-0
Thiodicarb
U153
74-93-1
Thiomethanol (I,T)
U402
1634-02-2
Thioperoxy dicarbonic diamide, tetra-
butyl
U403
97-77-8
Thioperoxy dicarbonic diamide, tetra -
ethyl
U244
137-26-8
Thioperoxydi carbonic diamide
[(H
2
N)C(S)]
2
S
2
, tetramethyl -
U409
23564-05-8
Thiophanate -methyl
U219
62-56-6
Thiourea
U244
137-26-8
Thiram
U220
108-88-3
Toluene
U221
25376-45-8
Toluenedi amine
U223
26471-62-5
Toluene di isocyanate (R,T)
U328
95-53-4
o-Toluidine
87
U353
106-49-0
p-Toluidine
U222
636-21-5
o-Toluidine hydrochloride
U389
2303-17-5
Triallate
U011
61-82-5
1H-1,2,4-Tri azol-3-amine
U227
79-00-5
1,1,2-Tri chloro ethane
U228
79-01-6
Trichloro ethylene
U121
75-69-4
Trichloro monofluoromethane
See F027
95-95-4
2,4,5-Tri chloro phenol
See F027
88-06-2
2,4,6-Tri chlorophenol
U404
121-44-8
Triethyl amine
U234
99-35-4
1,3,5-Tri nitrobenzene (R,T)
U182
123-63-7
1,3,5-Tri oxane, 2,4,6-tri methyl-
U235
126-72-7
Tris(2,3-di bromopropyl) phosphate
U236
72-57-1
Trypan blue
U237
66-75-1
Uracil mustard
U176
759-73-9
Urea, N-ethyl-N- nitroso-
U177
684-93-5
Urea, N-methyl-N-
nitroso-
U385
1929-77-7
Vernolate
U043
75-01-4
Vinyl chloride
U248
P 81-81-2
Warfarin, and salts, when present at
concentrations of 0.3% or less
U239
1330-20-7
Xylene (I)
U200
50-55-5
Yohimban-16-carboxylic acid, 11,17-di
-
methoxy-18-[(3,4,5-tri
methoxybenzoyl)-
oxy]-, methyl ester,
(3beta,16beta,17alpha,18beta,20alpha)-
U407
14324-55-1
Zinc, bis(diethyl carbamo dithioato -
S,S')-
U249
1314-84-7
Zinc phosphide Zn
3
P
2
, when present at
concentrations of 10% or less
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 721.Appendix G
Basis for Listing Hazardous Wastes
EPA
hazardous
waste No.
Hazardous constituents for which listed
F001
Tetrachloroethylene,
methylene chloride,
trichloroethylene, 1,1,1-
trichloroethane, carbon tetrachloride, chlorinated fluorocarbons.
F002
Tetrachloroethylene,
methylene chloride,
trichloroethylene, 1,1,1-
trichloroethane, 1,1,2-trichlorethane,
chlorobenzene, 1,1,2-trichloro-
1,2,2-trifluoroethane,
ortho-dichlorobenzene,
trichlorofluoromethane.
F003
N.A.
F004
Cresols and cresylic acid, nitrobenzene.
F005
Toluene, methyl ethyl
ketone, carbon disulfide,
isobutanol, pyridine, 2-
ethoxyethanol, benzene, 2-nitropropane.
F006
Cadmium, hexavalen
t chromium, nickel, cyanide (
complexed).
F007
Cyanide (salts).
F008
Cyanide (salts).
F009
Cyanide (salts).
F010
Cyanide (salts).
F011
Cyanide (salts).
F012
Cyanide ( complexed).
F019
Hexavalent chromium, cyanide (
complexed).
F020
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans;
tri- and tetrachlorophenols and their
clorophenoxy derivative acids, esters, ethers, amines and other salts.
F021
Penta- and hexachlorodibenzo-p-dioxins;
penta- and
88
hexachlorodibenzofurans; pentachlorophenol and its derivatives.
F022
Tetra-, penta- and hexachlorodibenzo-p-dioxins; tetra
-, penta- and
hexachlorodibenzofurans.
F023
Tetra- and pentachlorodibenzo-p-dioxins; tetra- and
pentachlorodibenzofurans;
tri- and tetra- chlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amines and other salts.
F024
Chloromethane, dichloromethane,
trichloromethane, carbon tetrachloride,
chloroethylene, 1,1-dichloroethane, 1,2-dichloroethane, trans-1,2-
dichloroethylene, 1,1-dichloroethylene, 1,1,1-trichloroethane, 1,1,2-
trichloroethane,
trichloroethylene, 1,1,1,2-tetrachloroethane, 1,1,2,2-
tetrachloroethane,
tetrachloroethylene,
pentachloroethane,
hexachloroethane,
allyl chloride (3-chloropropene),
dichloropropane,
dichloropropene, 2-chloro-1,3-butadiene, hexachloro-1,3-butadiene,
hexachlorochylopentadiene,
hexachlorocylohexane, benzene,
chlorobenzene,
dichlorobenzenes, 1,2,4-trichlorobenzene,
tetrachlorobenzenes,
pentachlorobenzene,
hexachlorobenzene, toluene, naphthalene.
F025
Chloromethane, dicloromethane, trichloromethane; carbon tetrachloride;
chloroethylene; 1,1-dichloroethane; 1,2-dichloroethane; trans-1,2-
dichloroethylene; 1,1-dichloroethylene; 1,1,1-trichloroethane; 1,1,2-
trichloroethane;
trichloroethylene; 1,1,1,2-tetrachloroethane; 1,1,2,2-
tetrachloroethane;
tetrachloroethylene;
pentachloroethane;
hexachloroethane;
allyl chloride (3-chloropropene);
dichloropropane;
dichloropropene; 2-chloro-1,3-butadiene; hexachloro-1,3-butadiene;
hexachlorocyclopentadiene; benzene;
chlorobenzene; dichlorobenzene;
1,2,4-trichlorobenzene;
tetrachlorobenzene;
pentachlorobenzene;
hexachlorobenzene; toluene; naphthalene.
F026
Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra
-, penta-, and
hexachlorodibenzofurans.
F027
Tetra-, penta, and hexachlorodibenzo-p-dioxins; tetra
-, penta-, and
hexachlorodibenzofurans;
tri-, tetra -, and pentachlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amine and other salts.
F028
Tetra-, penta-, and hexachlorodibenzo-p-dixons;tetra
-, penta-, and
hexachlorodibenzofurans;
tri-, tetra -, and pentachlorophenols and their
chlorophenoxy derivative acids, esters, ethers, amine and other salts.
F032
Benz(a) anthracene, benzo(a) pyrene, dibenz( a,h)anthracene, indeno(1,2,3-
cd)pyrene, pentachlorophenol, arsenic, chromium, tetra
-, penta-, hexa-,
heptachlorordibenzo-p-dioxins, tetra
-, penta-, hexa-,
heptachlorodibenzofurans.
F034
Benz(a) anthracene, benzo(k) fluoranthene, benzo(a) pyrene,
dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene, naphthalene, arsenic
chromium.
F035
Arsenic, chromiu m and lead.
F037
Benzene, benzo(a) pyrene, chrysene, lead, chromium.
F038
Benzene, benzo(a) pyrene, chrysene, lead, chromium.
F039
All constituents for which treatment standards are specified for
multi-
source leachate (wastewaters and non-wastewaters) under 35 Ill. Adm.
Code 728.Table B (Constituent Concentrations in Waste).
K001
Pentachlorophenol, phenol, 2-chlorophenol, p-chloro-m-cresol, 2,4-
dimethylphenol, 2,4-
dinitrophenol, trichlorophenols,
tetrachlorophenols, 2,4-
dinitrophenol, cresosote, chrysene,
naphthalene, fluoranthene, benzo(b) fluoranthene, benzo(a) pyrene,
indeno(1,2,3-cd) pyrene, benz(a) anthracene, dibenz(a) anthracene,
acenaphthalene.
K002
Hexavalent chromium, lead.
K003
Hexavalent chromium, lead.
K004
Hexavalent chromium.
K005
Hexavalent chromium, lead.
K006
Hexavalent chromium.
K007
Cyanide ( complexed), hexavalent chromium.
K008
Hexavalent chromium.
K009
Chloroform, formaldehyde,
methylene chloride, methyl chloride,
89
paraldehyde, formic acid.
K010
Chloroform, formaldehyde,
methylene chloride, methyl chloride,
paraldehyde, formic acid,
chloroacetaldehyde.
K011
Acrylonitrile, acetonitrile,
hydrocyanic acid.
K013
Hydrocyanic acid, acrylonitrile, acetonitrile.
K014
Acetonitrile, acrylamide.
K015
Benzyl chloride,
chlorobenzene, toluene,
benzotrichloride.
K016
Hexachlorobenzene,
hexachlorobutadiene, carbon tetrachloride,
hexachloroethane,
perchloroethylene.
K017
Epichlorohydrin,
chloroethers [ bis(chloromethyl) ether and
bis- (2-
chloroethyl) ethers],
trichloropropane,
dichloropropanols.
K018
1,2-dichlor oethane, trichloroethylene,
hexachlorobutadiene,
hexachlorobenzene.
K019
Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
tetrachloroethane),
trichloroethylene,
tetrachloroethylene, carbon
tetrachloride, chloroform, vinyl chloride,
vinylidene chloride.
K020
Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
tetrachloro-ethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-
tetrachloroethane),
trichloroethylene,
tetrachloroethylene, carbon
tetrachloride, chloroform, vinyl chloride,
vinylidene chloride.
K021
Antimony, carbon tetrachloride, chloroform.
K022
Phenol, tars ( polycyclic aromatic hydrocarbons).
K023
Phthalic anhydride,
maleic anhydride.
K024
Phthalic anhydride, 1,4-naphthoguinone.
K025
Meta-dinitrobenzene, 2,4-dinitrotoluene.
K026
Paraldehyde, pyridines, 2-picoline.
K027
Toluene diisocyanate, toluene-2,4-diamine.
K028
1,1,1-trichloroethane, vinyl chloride.
K029
1,2-dichloroethane, 1,1,1-trichloroethane, vinyl chloride,
vinylidene
chloride, chloroform.
K030
Hexachlorobenzene,
hexachlorobutadiene,
hexachloroethane, 1,1,1,2-
tetrachloroethane, 1,1,2,2-tetrachloroethane, ethylene dichloride.
K031
Arsenic.
K032
Hexachlorocyclopentadiene.
K033
Hexachlorocyclopentadiene.
K034
Hexachlorocyclopentadiene.
K035
Creosote, chrysene, naphthalene,
fluoranthene, benzo(b) fluoranthene,
benzo(a)- pyrene, indeno(1,2,3-cd)
pyrene, benzo(a) anthracene,
dibenzo(a) anthracene, acenaphthalene.
K036
Toluene, phosphorodithioic and
phosphorothioic acid esters.
K037
Toluene, phosphorodithioic and
phosphorothioic acid esters.
K038
Phorate, formaldehyde,
phosphorodithioic and
phosphorothioic acid
esters.
K039
Phosphorodithioic and
phosphorothioic acid esters.
K040
Phorate, formaldehyde,
phosphorodithioic and
phosphorothioic acid
esters.
K041
Toxaphene.
K042
Hexachlorobenzene,
ortho-dichlorobenzene.
K043
2,4-dichlorophenol, 2,6-dichlorophenol, 2,4,6-trichlorophenol.
K044
N.A.
K045
N.A.
K046
Lead.
K047
N.A.
K048
Hexavalent chromium, lead.
K049
Hexavalent chr omium, lead.
K050
Hexavalent chromium.
K051
Hexavalent chromium, lead.
K052
Lead.
K060
Cyanide, naphthalene,
phenolic compounds, arsenic.
K061
Hexavalent chromium, lead, cadmium.
90
K062
Hexavalent chromium, lead.
K064
Lead, cadmium.
K065
Lead, cadmium.
K066
Lead, cadmium.
K069
Hexavalent chromium, lead, cadmium.
K071
Mercury.
K073
Chloroform, carbon tetrachloride,
hexachloroethane,
trichloroethane,
tetrachloroethylene,
dichloroethylene, 1,1,2,2-tetrachloroethane.
K083
Aniline, diphenylamine, nitrobenzene,
phenylenediamine.
K084
Arsenic.
K085
Benzene, dichlorobenzenes,
trichlorobenzenes,
tetrachlorobenzenes,
pentachlorobenzene,
hexachlorobenzene, benzyl chloride.
K086
Lead, hexavalent chromium.
K087
Phenol, naphthalene.
K088
Cyanide (complexes).
K090
Chromium.
K091
Chromium.
K093
Phthalic anhydride,
maleic anhydride.
K094
Phthalic anhydride.
K095
1,1,2-trichloroethane, 1,1,1,2-tetrachloroethane, 1,1,2,2-
tetrachloroethane.
K096
1,2-dichloroethane, 1,1,1-trichloroethane, 1,1,2-trichloroethane.
K097
Chlordane, hept achlor.
K098
Toxaphene.
K099
2,4-dichlorophenol, 2,4,6-trichlorophenol.
K100
Hexavalent chromium, lead, cadmium.
K101
Arsenic.
K102
Arsenic.
K103
Aniline, nitrobenzene,
phenylenediamine.
K104
Aniline, benzene,
diphenylamine, nitrobenzene,
phynylenediamine.
K105
Benzene, monochlorobenzene,
dichlorobenzenes, 2,4,6-trichlorophenol.
K106
Mercury.
K111
2,4-Dinitrotoluene.
K112
2,4-Toluenediamine, o-
toluidine, p- toluidine, aniline.
K113
2,4-Toluenediamine, o-
toluidine, p- toluidine, aniline.
K114
2,4-Toluenediamin
e, o-toluidine, p- toluidine.
K115
2,4-Toluenediamine.
K116
Carbon tetrachloride,
tetrachloroethylene, chloroform, phosgene.
K117
Ethylene dibromide.
K118
Ethylene dibromide.
K123
Ethylene thiourea.
K124
Ethylene thiourea.
K125
Ethylene thiourea.
K126
Ethylene thiourea.
K131
Dimethyl sulfate, methyl bromide.
K132
Methyl bromide.
K136
Ethylene dibromide.
K141
Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
K142
Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
K143
Benzene, benz(a) anthracene, benzo(b) fluoranthene, benzo(k) fluoranthene.
K144
Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
benzo(k) fluoranthene, dibenz( a,h)anthracene.
K145
Benzene, benz(a) anthracene, benzo(a) pyrene, dibenz( a,h)anthracene,
naphthalene.
K147
Benzene, benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
K148
Benz(a) anthracene, benzo(a) pyrene, benzo(b) fluoranthene,
benzo(k) fluoranthene, dibenz( a,h)anthracene, indeno(1,2,3-cd) pyrene.
K149
Benzotrichloride, benzyl chloride, chloroform,
chloromethane,
91
chlorobenzene, 1,4-dichlorobenzene,
hexachlorobenzene,
pentachlorobenzene, 1,2,4,5-tetrachlorobenzene, toluene.
K150
Carbon tetrachloride, chloroform,
chloromethane, 1,4-dichlorobenzene,
hexachlorobenzene,
pentachlorobenzene, 1,2,4,5-tetrachlorobenzene,
1,1,2,2-tetrachloroethane,
tetrachloroethylene, 1,2,4-trichlorobenzene.
K151
Benzene, carbon tetrachloride, chloroform,
hexachlorobenzene,
pentachlorobenzene, toluene, 1,2,4,5-tetrachlorobenzene,
tetrachloroethylene.
K156
Benomyl, carbaryl, carbendazim, carbofuran, carbosulfan, formaldehyde,
methylene chloride,
triethylamine.
K157
Carbon tetrachloride, formaldehyde, methyl chloride,
methylene chloride,
pyridine, triethylamine.
K158
Benomyl, carbendazim, carbofuran, carbosulfan, chloroform,
methylene
chloride.
K159
Benzene, butylate, EPTC, molinate, pebulate, vernolate.
K160 Benzene, butylate, EPTC, molinate, pebulate, vernolate.
K161
Antimony, arsenic,
metam-sodium, ziram.
N.A.--Waste is hazardous because it fails the test for the
characteristic of
ignitability, corrosivity or reactivity.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 721.Appendix H Hazardous Constituents
Common Name
Chemical Abstracts Name
Chemical
Abstracts
Number
Hazard
ous
Waste
Number
A2213
Ethanimidothioic acid, 2 -
(dimethyl amino)-N-hydroxy-
2-oxo-, methyl ester
30558-43-
1
U394
Acetonitrile
Same
75-05-8
U003
Acetophenone
Ethanone, 1-phenyl-
98-86-2
U004
2-Acetylamino fluorene
Acetamide, N-9H-fluoren-2-
yl-
53-96-3
UOO5
Acetyl chloride
Same
75-36-5
U006
1-Acetyl-2-thio urea
Acetamide, N-
(aminothioxomethyl)-
591-08-2
P002
Acrolein
2-Propenal
107-02-8
P003
Acrylamide
2-Propenamide
79-06-1
U007
Acrylonitrile
2-Propenenitrile
107-13-1
U009
Aflatoxins
Same
1402-68-2
Aldicarb
Propanal, 2-methyl-2-
(methylthio)-, O-
[(methylamino)carbonyl]
-
oxime
116-06-3
P070
Aldicarb sulfone
Propanal, 2 -methyl-2-
(methyl sulfonyl )-,
O-[(methylamino) carbonyl] -
oxime
1646-88-4
P203
Aldrin
1,4,5,8-Dimethano
naph-
thalene, 1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-
hexahydro-, (1-alpha,4-
alpha,4a-beta,5-alpha,8-
alpha,8a-beta)-
309-00-2
P004
Allyl alcohol
2-Propen-1-ol
107-18-6
P005
Allyl chloride
1-Propene, 3-chloro-
107-18-6
92
Aluminum phosphide
Same
20859-73-
8
P006
4-Aminobiphenyl
[1,1'-Biphenyl]-4-amine
92-67-1
5-(Aminomethyl)-3-isoxazolol
3(2H)- Isoxazolone, 5-
(aminomethyl )-
2763-96-4
P007
4-Aminopyridine
4-Pyridinamine
504-24-5
P008
Amitrole
1H-1,2,4-Triazol-3-amine
61-82-5
U011
Ammonium vanadate
Vanadic acid, ammonium
salt
7803-55-6
U119
Aniline
Benzenamine
62-53-3
U012
Antimony
Same
7440-36-0
Antimony compounds, N.O.S.
(not otherwise specified)
Aramite
Sulfurous acid, 2-
chloroethyl-, 2-[4-(1,1-
dimethyl ethyl) phenoxy]-1-
methylethyl ester
140-57-8
Arsenic
Arsenic
7440-38-2
Arsenic compounds, N.O.S.
Arsenic acid
Arsenic acid H
3
AsO
4
7778-39-4
P010
Arsenic pentoxide
Arsenic oxide As
2
O
5
1303-28-2
PO11
Arsenic trioxide
Arsenic oxide As
2
O
3
1327-53-3
P012
Auramine
Benzenamine, 4,4'-carbon
-
imidoyl bis[N, N- dimethyl-
492-80-8
U014
Azaserine
L-Serine, diazoacetate
(ester)
115-02-6
U015
Barban
Carbamic acid, (3
-chloro -
phenyl) -, 4-chloro-2-
butynyl ester
101-27-9
U280
Barium
Same
7440-39-3
Barium compounds, N.O.S.
Barium cyanide
Same
542-62-1
P013
Bendiocarb
1,3-Benzo dioxol-4-ol-
2,2-dimethyl -, methyl
carbamate
22781-23-
3
U278
Bendiocarb phenol
1,3-Benzo dioxol-4-ol-2,2-
dimethyl -,
22961-82-
6
U364
Benomyl
Carbamic acid, [1
-
[(butylamino)carbonyl]-1H-
benzimidazol-2-yl] -,
methyl ester
17804-35-
2
U271
Benz[c] acridine
Same
225-51-4
U016
Benz[a] anthra cene
Same
56-55-3
U018
Benzal chloride
Benzene, ( dichloromethyl)-
98-87-3
U017
Benzene
Same
71-43-2
U018
Benzenearsonic acid
Arsonic acid, phenyl-
98-05-5
Benzidine
[1,1'-Biphenyl]-4,4'-
diamine
92-87-5
U021
Benzo[b] fluoranthene
Benz[e] acephenanthrylene
205-99-2
Benzo[j] fluoranthene
Same
205-82-3
Benzo(k) fluoranthene
Same
207-08-9
Benzo[a] pyrene
Same
50-32-8
U022
p-Benzoquinone
2,5-Cyclohexadiene-1,4-
dione
106-51-4
U197
Benzotrichloride
Benzene,
(trichloromethyl)-
98-07-7
U023
Benzyl chloride
Benzene, ( chloromethyl)-
100-44-7
P028
Beryllium powder
Same
7440-41-7
P015
Beryllium compounds, N.O.S.
Bis(pentamethylene )thiuram
tetrasulfide
Piperidine, 1,1' -(tetra-
thiodicarbono thioyl )-bis-
120-54-7
U400
93
Bromoacetone
2-Propanone, 1-bromo-
598-31-2
P017
Bromoform
Methane, tribromo-
75-25-2
U225
4-Bromophenyl phenyl ether
Benzene, 1-bromo-4-
phenoxy-
101-55-3
U030
Brucine
Strychnidin-10-one, 2,3-
dimethoxy-
357-57-3
P018
Butylate
Carbamo thioic acid, bis-
(2-methyl propyl) -, S-ethyl
ester
2008-41-5
U392
Butyl benzyl phthalate
1,2-Benzenedicarboxylic
acid, butyl phenylmethyl
ester
85-68-7
Cacodylic acid
Arsenic acid, dimethyl-
75-60-5
U136
Cadmium
Same
7440-43-9
Cadmium compounds, N.O.S.
Calcium chromate
Chromic acid H
2
CrO
4
,
calcium salt
13765-19-
0
U032
Calcium cyanide
Calcium cyanide Ca(CN)
2
592-01-8
P021
Carbaryl
1-Naphthalenol, methyl -
carbamate
63-25-2
U279
Carbendazim
Carbamic acid, 1H
-benz-
imidazol-2-yl, methyl
ester
10605-21-
7
U372
Carbofuran
7-Benzofuranol, 2,3
-di-
hydro-2,2-dimethyl
-,
methyl carbamate
1563-66-2
P127
Carbofuran phenol
7-Benzo furanol, 2,3-
dihydro-2,2-dimethyl
-
1563-38-8
U367
Carbosulfan
Carbamic acid, [(
dibutyl -
amino) thio] methyl -,
2,3-dihydro-2,2-dimethyl-
7-benzo furanyl ester
55285-14-
8
P189
Carbon disulfide
Same
75-15-0
P022
Carbon oxyfluoride
Carbonic difuoride
353-50-4
U033
Carbon tetra chloride
Methane, tetrachloro-
56-23-5
U211
Chloral
Acetaldehyde, trichloro-
75-87-6
U034
Chlorambucil
Benzenebutanoic acid,
4[bis-(2-chloroethyl)
-
amino]-
305-03-3
U035
Chlordane
4,7-Methano-1H-indene,
1,2,4,5,6,7,8,8-octa
-
chloro-2,3,3a,4,7,7a-hexa
-
hydro-
57-74-9
U036
Chlordane, alpha and gamma
isomers
U036
Chlorinated benzenes, N.O.S.
Chlorinated ethane, N.O.S.
Chlorinated fluorocarbons,
N.O.S.
Chlorinated naphthalene,
N.O.S.
Chlorinated phenol, N.O.S.
Chlornaphazine
Naphthalenamine, N,N'-
bis(2-chloro ethyl)-
494-03-1
U026
Chloroacet aldehyde
Acetaldehyde, chloro-
107-20-0
P023
Chloroalkyl ethers, N.O.S.
p-Chloroaniline
Benzenamine, 4-chloro-
106-47-8
P024
Chlorobenzene
Benzene, chloro-
108-90-7
U037
Chlorobenzilate
Benzeneacetic acid, 4-
chloro-alpha-(4-
chlorophenyl)-alpha-
510-15-6
U038
94
hydroxy-, ethyl ester
p-Chloro-m-cresol
Phenol, 4-chloro-3-methyl-
59-50-7
U039
2-Chloroethyl vinyl ether
Ethene, (2-chloroethoxy)-
110-75-8
U042
Chloroform
Methane, trichloro-
67-66-3
U044
Chloromethyl methyl ether
Methane, chloromethoxy-
107-30-2
U046
beta-Chloro naphthalene
Naphthalene, 2-chloro-
91-58-7
U047
o-Chlorophenol
Phenol, 2-chloro-
95-57-8
U048
1-(o-Chloro phenyl )thiourea
Thiourea, (2-chloro
-
phenyl)-
5344-82-1
P026
Chloroprene
1,3-Butadiene, 2-chloro-
126-99-8
3-Chloropropio nitrile
Propanenitrile, 3-chloro-
542-76-7
P027
Chromium
Same
7440-47-3
Chromium compounds, N.O.S.
Chrysene
Same
218-01-9
U050
Citrus red No. 2
2-Naphthalenol, 1-[(2,5-
dimethoxy phenyl) azo]-
6358-53-8
Coal tar creosote
Same
8007-45-2
Copper cyanide
Copper cyanide CuCN
544-92-3
P029
Copper dimethyl dithio carbamate
Copper, bis(dimethyl -
carbamo dithioato -S,S') -,
137-29-1
U393
Creosote
Same
U051
Cresols ( Cresylic acid)
Phenol, methyl-
1319-77-3
U052
Crotonaldehyde
2-Butenal
4170-30-3
U053
m-Cumenyl methyl carbamate
Phenol, 3 -(methyl ethyl)-,
methyl carbamate
64-00-6
P202
Cyanides (soluble salts and
complexes), N.O.S.
P030
Cyanogen
Ethanedinitrile
460-19-5
P031
Cyanogen bromide
Cyanogen bromide (CN)Br
506-68-3
U246
Cyanogen chloride
Cyanogen chloride (CN)
Cl
506-77-4
P033
Cycasin
Beta-D- glucopyranoside,
(methyl-ONN- azoxy)methyl-
14901-08-
7
Cycloate
Carbamo thioic acid, cyclo-
hexylethyl-, S-ethyl ester
1134-23-2
U386
2-Cyclohexyl-4,6-dinitro
phenol
Phenol, 2-cyclohexyl-4,6-
dinitro-
131-89-5
P034
Cyclophosphamide
2H-1,3,2-Oxazaphosphorin-
2-amine, N,N- bis(2-chloro -
ethyl) tetrahydro-, 2-oxide
50-18-0
U058
2,4-D
Acetic acid, (2,4-
dichloro phenoxy)-
94-75-7
U240
2,4-D, salts and esters
Acetic acid, (2,4-
dichlorophenoxy)-, salts
and esters
U240
Daunomycin
5, 12-Naphthacenedione, 8-
acetyl-10-[(3-amino-2,3,6-
trideoxy-alpha-L-lyxo-
hexopyranosyl) oxy]-
7,8,9,10-tetrahydro-
6,8,11-tri hydroxy-l-meth -
oxy-, 8S-cis)-
20830-81-
3
U059
Dazomet
2H-1,3,5-thia diazine-2-
thione, tetra hydro-3,5-
dimethyl
533-74-4
U366
DDD
Benzene, 1,1'-(2,2-
dichloro ethylidene) bis[4-
chloro-
72-54-8
U060
DDE
Benzene, 1,1'-( dichloro -
ethenyl idene)bis[4-chloro-
72-55-9
DDT
Benzene, 1,1'-(2,2,2-tri
-
chloro ethylidene) bis[4-
50-29-3
U061
95
chloro-
Diallate
Carbamothioic acid, bis(1-
methyl ethyl)-, S-(2,3-
dichloro-2-pro penyl) ester
2303-16-4
U062
Dibenz[ a,h]acridine
Same
226-36-8
Dibenz[ a,j]acridine
Same
224-42-0
Dibenz[ a,h]anthracene
Same
53-70-3
U063
7H-Dibenzo [c,g]carbazole
Same
194-59-2
Dibenzo[ a,e]pyrene
Naphtho[1,2,3,4-def]
-
chrysene
192-65-4
Dibenzo[ a,h]pyrene
Dibenzo[ b,def] chrysene
189-64-0
Dibenzo[ a,i]pyrene
Benzo[ rst]pentaphene
189-55-9
U064
1,2-Dibromo-3-chloropropane
Propane, 1,2-dibromo-3-
chloro-
96-12-8
U066
Dibutyl phthalate
1,2-Benzenedicarboxylic
acid, dibutyl ester
84-74-2
U069
o-Dichloro benzene
Benzene, 1,2-dichloro-
95-50-1
U070
m-Dichloro benzene
Benzene, 1,3-dichloro-
541-73-1
U071
p-Dichloro benzene
Benzene, 1,4-dichloro-
106-46-7
U072
Dichlorobenzene, N.O.S.
Benzene, dichloro-
25321-22-
6
3,3'-Dichloro benzidine
[1,1'-Biphenyl]-4,4'-
diamine, 3,3'-dichloro-
91-94-1
U073
1,4-Dichloro-2-butene
2-Butene, 1,4-dichloro-
764-41-0
U074
Dichlorodifluoromethane
Methane, dichlorodifluoro-
75-71-8
U075
Dichloro ethylene , N.O.S.
Dichloroethylene
25323-30-
2
1,1-Dichloro ethylene
Ethene, 1,1-dichloro-
75-35-4
U078
1,2-Dichloro ethylene
Ethene, 1,2-dichloro-,
(E)-
156-60-5
U079
Dichloroethyl ether
Ethane, 1,1'-oxybis[2-
chloro-
111-44-4
U025
Dichloroiso propyl ether
Propane, 2,2'-oxybis[2-
chloro-
108-60-1
U027
Dichloromethoxy ethane
Ethane, 1,1'-[ methylene -
bis(oxy)bis[2-chloro-
111-91-1
U024
Dichloromethyl ether
Methane, oxybis[chloro-
542-88-1
P016
2,4-Dichloro phenol
Phenol, 2,4-dichloro-
120-83-2
U081
2,6-Dichloro phenol
Phenol, 2,6-dichloro-
87-65-0
U082
Dichlorophenyl arsine
Arsonous dichloride,
phenyl-
696-28-6
P036
Dichloropropane, N.O.S.
Propane, dichloro-
26638-19-
7
Dichloro propanol , N.O.S.
Propanol, dichloro-
26545-73-
3
Dichloropropene, N.O.S.
1-Propene, dichloro-
26952-23-
8
1,3-Dichloro propene
1-Propene, 1,3-dichloro-
542-75-6
U084
Dieldrin
2,7:3,6-Dimethanonaphth
[2,
3-b]oxirene,3,4,5,6,9,9-
hexachloro-1a,2,2a,3,6,
6a,7,7a-octahydro-,
(1aalpha,2beta,2aalpha,3be
ta,6beta,6aalpha,7beta,7aa
lpha)-
60-57-1
P037
1,2:3,4-Diepoxy butane
2,2'-Bioxirane
1464-53-5
U085
Diethylarsine
Arsine, diethyl-
692-42-2
P038
Diethylene glycol,
dicarbamate
Ethanol, 2,2' -oxybis -,
dicarbamate
5952-26-1
U395
1,4-Diethylene oxide
1,4-Dioxane
123-91-1
U108
Diethylhexyl phthalate
1,2-Benzenedicarboxylic
117-81-7
U028
96
acid, bis(2-ethylhexyl)
ester
N,N'-Diethyl hydrazine
Hydrazine, 1,2-diethyl-
1615-80-1
U086
O,O-Diethyl-S-methyl
dithio -
phosphate
Phosphorodithioic acid,
O,O-diethyl S-methyl ester
3288-58-2
U087
Diethyl-p- nitrophenyl
phosphate
Phosphoric acid, diethyl
4-nitro phenyl ester
311-45-5
P041
Diethyl phthalate
1,2-Benzenedicarboxylic
acid, diethyl ester
84-66-2
U088
O,O-Diethyl O- pyrazinyl
phosphoro thioate
Phosphorothioic acid, O,O-
diethyl O- pyrazinyl ester
297-97-2
P040
Diethylstil bestrol
Phenol, 4,4'-(1,2-diethyl-
1,2-ethene diyl)bis-, (E)-
56-53-1
U089
Dihydrosafrole
1,3-Benzodioxole, 5-
propyl-
94-58-6
U090
Diisopropylfluorophosph
ate
(DFP)
Phosphorofluoridic acid,
bis(1-methylethyl) ester
55-91-4
P043
Dimethoate
Phosphorodithioic acid,
O,O-dimethyl S-[2-( methyl -
amino)-2-oxo ethyl] ester
60-51-5
P044
Dimetilan
Carbamic acid, dimethyl -,
1- [(dimethyl amino)
carbonyl]-5-methyl-1H-
pyrazol-3-yl ester
644-64-4
P191
3,3'-Dimethoxy benzidine
[1,1'-Biphenyl]-4,4'-
diamine, 3,3'-dimethoxy-
119-90-4
U091
p-Dimethyl aminoazobenzene
Benzenamine, N,N-dimethyl-
4-(phenyl azo)-
60-11-7
U093
7,12-Dimethyl benz[a] anthra cene
Benz[a] anthracene, 7,12-
dimethyl-
57-97-6
U094
3,3'-Dimethyl benzidine
[1,1'-Biphenyl]-4,4'-
diamine, 3,3'-dimethyl-
119-93-7
U095
Dimethylcarbam oyl chloride
Carbamic chloride,
dimethyl-
79-44-7
U097
1,1-Dimethyl hydrazine
Hydrazine, 1,1-dimethyl-
57-14-7
U098
1,2-Dimethyl hydrazine
Hydrazine, 1,2-dimethyl-
540-73-8
U099
alpha,alpha-Dimethylphen
-
ethylamine
Benzeneethanamine, alpha,
alpha- dimethyl-
122-09-8
P046
2,4-Dimethyl phenol
Phenol, 2,4-dimethyl-
105-67-9
U101
Dimethyl phthalate
1,2-Benzenedicarboxylic
acid, dimethyl ester
131-11-3
U102
Dimethyl sulfate
Sulfuric acid, dimethyl
ester
77-78-1
U103
Dinitrobenzene, N.O.S.
Benzene, dinitro-
25154-54-
5
4,6-Dinitro-o-cresol
Phenol, 2-methyl-4,6-
dinitro-
534-52-1
P047
4,6-Dinitro-o-cresol salts
P047
2,4-Dinitro phenol
Phenol, 2,4-dinitro-
51-28-5
P048
2,4-Dinitro toluene
Benzene, 1-methyl-2,4-
dinitro-
121-14-2
U105
2,6-Dinitro toluene
Benzene, 2-methyl-1,3-
dinitro-
606-20-2
U106
Dinoseb
Phenol, 2-(1-
methylpropyl)-4,6-dinitro-
88-85-7
P020
Di-n-octyl phthalate
1,2-Benzenedicarboxylic
acid, dioctyl ester
117-84-0
U107
Diphenylamine
Benzenamine, N-phenyl-
122-39-4
1,2-Diphenyl hydrazine
Hydrazine, 1,2-diphenyl-
122-66-7
U109
Di-n-propyl nitros amine
1-Propanamine, N-nitroso-
N-propyl-
621-64-7
U111
97
Disulfiram
Thioperoxy dicarbonic
diamide, tetraethyl
97-77-8
U403
Disulfoton
Phosphorodithioic acid,
O,O-diethyl S-[2-(
ethyl-
thio)ethyl] ester
298-04-4
P039
Dithiobiuret
Thioimidodicarbonic
diamide [(H
2
N)C(S)]
2
NH
541-53-7
P049
Endosulfan
6, 9-Methano-2,4,3-benzo
-
dioxathie-
pen,6,7,8,9,10,10-
hexachloro-1,5,5a,6,9,9a-
hexahydro-, 3-oxide,
115-29-7
P050
Endothal
7-
Oxabicyclo[2.2.1]heptane-
2,3-di carboxylic acid
145-73-3
P088
Endrin
2,7:3,6-Dimethanonaphth
-
[2,3-b] oxirene,
3,4,5,6,9,9-hexa chloro-
1a,2,2a,3,6,6a,7,7a-
octahydro-, (1a
alpha,2beta,2abeta,3alpha,
6alpha,6abeta,7beta,7aalph
a)-,
72-20-8
P051
Endrin metabolites
P051
Epichlorohydrin
Oxirane, ( chloromethyl)-
106-89-8
U041
Epinephrine
1,2-Benzenediol, 4-[1-
hydroxy-2-( methyl amino)-
ethyl]-, (R)-
51-43-4
P042
EPTC
Carbamo thioic acid,
dipropyl -, S-ethyl ester
759-94-4
U390
Ethyl carbamate (urethane)
Carbamic acid, ethyl ester
51-79-6
U238
Ethyl cyanide
Propanenitrile
107-12-0
P101
Ethylenebisdithiocarbamic acid
Carbamodithioic acid, 1,2-
ethane diylbis-
111-54-6
U114
Ethylenebisdithiocarbamic
acid, salts and esters
U114
Ethylene dibromide
Ethane, 1,2-dibromo-
106-93-4
U067
Ethylene dichloride
Ethane, 1,2-dichloro-
107-06-2
U077
Ethylene glycol monoethyl
ether
Ethanol, 2-ethoxy-
110-80-5
U359
Ethyleneimine
Aziridine
151-56-4
P054
Ethylene oxide
Oxirane
75-21-8
U115
Ethylenethiourea
2-Imidazolidinethione
96-45-7
U116
Ethylidine dichloride
Ethane, 1,1-dichloro-
75-34-3
U076
Ethyl methacrylate
2-Propenoic acid, 2-
methyl-, ethyl ester
97-63-2
U118
Ethyl methanesulfonate
Methanesulfonic acid,
ethyl ester
62-50-0
U119
Ethyl Ziram
Zinc, bis(diethyl carbamo -
dithioato -S,S') -
14324-55-
1
U407
Famphur
Phosphorothioc acid, O-[4-
[(dimethylamino) sulfonyl] -
phenyl] O,O- dimethyl ester
52-85-7
P097
Ferbam
Iron, tris(dimethyl -
carbamo dithioato -S,S') -,
14484-64-
1
U396
Fluoranthene
Same
206-44-0
U120
Fluorine
Same
7782-41-4
P056
Fluoroacetamide
Acetamide, 2-fluoro-
640-19-7
P057
Fluoroacetic acid, sodium salt
Acetic acid, fluoro-,
sodium salt
62-74-8
P058
Formaldehyde
Same
50-00-0
U122
98
Formetanate hydrochloride
Methanimid amide,
N,N-dimethyl-N'-[3-
[[(methyl amino)carbonyl] -
oxy]phenyl] -, monohydro-
chloride
23422-53-
9
P198
Formic acid
Same
64-18-16
U123
Formparanate
Methanimid amide,
N,N-dimethyl-N'-[2-methyl-
4-[[(methyl amino)-
carbonyl] oxy]phenyl] -
17702-57-
7
P197
Glycidylaldehyde
Oxiranecarboxaldehyde
765-34-4
U126
Halomethanes, N.O.S.
Heptachlor
4,7-Methano-1H-
indene,1,4,5,6,7,8,8-
heptachloro-3a,4,7,7a-
tetrahydro-
76-44-8
P059
Heptachlor epoxide
2,5-Methano-2H-indeno[1,
2b]oxirene, 2,3,4,5,6,7,7-
heptachloro-
1a,1b,5,5a,6,6a-hexa
hydro-
,
(1aalpha,1bbeta,2alpha,5al
pha,5abeta,6beta,6aalpha)-
1024-57-3
Heptachlor epoxide (alpha,
beta, and gamma isomers)
Heptachlorodibenzofurans
Heptachlorodibenzo-p-dioxins
Hexachloro benzene
Benzene, hexachloro-
118-74-1
U127
Hexachloro butadiene
1,3-Butadiene,
1,1,2,3,4,4-hexa chloro-
87-68-3
U128
Hexachlorocyclo-pentadiene
1,3-Cyclopentadiene,
1,2,3,4,5,5-hexa chloro-
77-47-4
U130
Hexachlorodi benzo-p-dioxins
Hexachlorodi benzofurans
Hexachloroethane
Ethane, hexachloro-
67-72-1
U131
Hexachlorophene
Phenol, 2,2'-methylene
-
bis[3,4,6-tri chloro-
70-30-4
U132
Hexachloropro pene
1-Propene, 1,1,2,3,3,3-
hexachloro-
1888-71-7
U243
Hexaethyltetra phosphate
Tetraphosphoric acid,
hexaethyl ester
757-58-4
P062
Hydrazine
Same
302-01-2
U133
Hydrogen cyanide
Hydrocyanic acid
74-90-8
P063
Hydrogen fluoride
Hydrofluoric acid
7664-39-3
U134
Hydrogen sulfide
Hydrogen sulfide H2S
7783-06-4
U135
Indeno[1,2,3-cd] pyrene
Same
193-39-5
U137
3-Iodo-2-propynyl-n-butyl
-
carbamate
Carbamic acid, butyl
-,
3-iodo-2-propynyl ester
55406-53-
6
U375
Isobutyl alcohol
1-Propanol, 2-methyl-
78-83-1
U140
Isodrin
1,4:5,8-Dimethano
naph-
thalene,1,2,3,4,10,10-
hexachloro-1,4,4a,5,8,8a-
hexahydro-,
(1alpha,4alpha,4abeta,5bet
a,8beta,8abeta)-,
465-73-6
P060
Isolan
Carbamic acid, dimethyl -,
3-methyl-1-(1-methyl
-
ethyl)-1H-pyrazol-5-yl
ester
119-38-0
P192
Isosafrole
1,3-Benzodioxole, 5-(1-
propenyl)-
120-58-1
U141
99
Kepone
1,3,4-Metheno-2H-cyclo
-
buta[cd]pentalen-2-one,
1,1a,3,3a,4,5,5,5a,5b,6-
decachlorooctahydro-,
143-50-0
U142
Lasiocarpine
2-Butenoic acid, 2-methyl-
, 7-[[2,3-dihydroxy-2-(1-
methoxyethyl)-3-methyl-1-
oxobutoxy]methyl]-
2,3,5,7a-tetrahydro-1H-
pyrrol izin-l-yl ester,
[1S-[1-
alpha(Z),7(2S*,3R*),7aalph
a]]-
303-34-1
U143
Lead
Same
7439-92-1
Lead and compounds, N.O.S.
Lead acetate
Acetic acid, lead (2+)
salt
301-04-2
U144
Lead phosphate
Phosphoric acid, lead (2+)
salt (2:3)
7446-27-7
U145
Lead subacetate
Lead, bis(acetato-O) tetra-
hydroxy tri-
1335-32-6
U146
Lindane
Cyclohexane, 1,2,3,4,5,6-
hexachloro-,
1alpha,2alpha,3beta,4alpha
,5alpha,6beta)-
58-89-9
U129
Maleic anhydride
2,5-Furandione
108-31-6
U147
Maleic hydrazide
3,6-Pyridazinedione, 1,2-
dihydro-
123-33-1
U148
Malononitrile
Propanedinitrile
109-77-3
U149
Manganese dimethyl dithio -
carbamate
Manganese, bis(dimethyl -
carbamo dithioato -S,S') -,
15339-36-
3
P196
Melphalan
L-Phenylalanine, 4-[
bis(2-
chloro ethyl) amino]-
148-82-3
U150
Mercury
Same
7439-97-6
U151
Mercury compounds, N.O.S.
Mercury fulminate
Fulminic acid, mercury
(2+) salt
628-86-4
P065
Metam Sodium
Carbamo dithioic acid,
methyl -, monosodium salt
137-42-8
U384
Methacrylo nitrile
2-Propenenitrile, 2-
methyl-
126-98-7
U152
Methapyrilene
1,2-Ethanediamine, N,N-
dimethyl-N'-2-pyridinyl-
N'-(2-thienylmethyl)-
91-80-5
U155
Methiocarb
Phenol, (3,5 -dimethyl-4-
(methylthio) -, methyl -
carbamate
2032-65-7
P199
Metholmyl
Ethanimidothioic acid, N-
[[(methyl -
amino)carbonyl] oxy]-,
methyl ester
16752-77-
5
P066
Methoxychlor
Benzene, 1,1'-(2,2,2-
trichloro ethylidene) bis[4-
methoxy-
72-43-5
U247
Methyl bromide
Methane, bromo-
74-83-9
U029
Methyl chloride
Methane, chloro-
74-87-3
U045
Methylchloro carbonate
Carbonochloridic acid,
methyl ester
79-22-1
U156
Methyl chloroform
Ethane, 1,1,1-trichloro-
71-55-6
U226
3-Methylchol anthrene
Benz[j] aceanthrylene, 1,2-
dihydro-3-methyl-
56-49-5
U157
100
4,4'-Methylene bis(2-chloro -
aniline)
Benzenamine, 4,4'-
methylene bis[2-chloro-
101-14-4
U158
Methylene bromide
Methane, dibromo-
74-95-3
U068
Methylene chloride
Methane, dichloro-
75-09-2
U080
Methyl ethyl ketone (MEK)
2-Butanone
78-93-3
U159
Methyl ethyl ketone peroxide
2-Butanone, peroxide
1338-23-4
U160
Methyl hydrazine
Hydrazine, methyl-
60-34-4
P068
Methyl iodide
Methane, iodo-
74-88-4
U138
Methyl isocyanate
Methane, isocyanato-
624-83-9
P064
2-Methyl lactonitrile
Propanenitrile, 2-hydroxy-
2-methyl-
75-86-5
P069
Methyl methacrylate
2-Propenoic acid, 2-
methyl-, methyl ester
80-62-6
U162
Methyl methane sulfonate
Methanesulfonic acid,
methyl ester
66-27-3
Methyl parathion
Phosphorothioic acid, O,O-
dimethyl O-(4-nitrophenyl)
ester
298-00-0
P071
Methylthiour acil
4-(1H)- Pyrimidinone, 2,3-
dihydro-6-methyl-2-thioxo-
56-04-2
U164
Metolcarb
Carbamic acid, methyl
-,
3-methyl phenyl ester
1129-41-5
P190
Mexacarbate
Phenol, 4 -(dimethylamino)-
3,5-dimethyl -, methyl -
carbamate (ester)
315-18-4
P128
Mitomycin C
Azirino[2', 3':3,
4]pyrrolo[1, 2-a]indole-4,
7-dione, 6-amino-8-
[[(aminocarbonyl )oxy]-
methyl]-1,1a,2,8,8a,8b-
hexahydro-8a-methoxy-5-
methyl-, [1a-S-
(1aalpha,8beta,8aalpha,8ba
lpha)]-,
50-07-7
U010
Molinate
1H-Azepine-1-carbo thioic
acid, hexahydro -, S-ethyl
ester
2212-67-1
U365
MNNG
Guanidine, N-methyl-N'-
nitro-N-nitroso-
70-25-7
U163
Mustard gas
Ethane, 1,1'-thiobis[2-
chloro-
505-60-2
U165
Naphthalene
Same
91-20-3
U165
1,4-Naphtho quinone
1,4-Naphthalenedione
130-15-4
U166
alpha- Naphthyl amine
1-Naphthalenamine
134-32-7
U167
beta-Naphthyl amine
2-Naphthalenamine
91-59-8
U168
alpha- Naphthyl thiourea
Thiourea, 1-naphthalenyl-
86-88-4
P072
Nickel
Same
7440-02-0
Nickel compounds, N.O.S.
Nickel carbonyl
Nickel carbonyl Ni(CO)
4
,
(T-4)-
13463-39-
3
P073
Nickel cyanide
Nickel cyanide Ni(CN)
2
557-19-7
P074
Nicotine
Pyridine, 3-(1-methyl-2-
pyrrolidinyl)-, (S)-
54-11-5
P075
Nicotine salts
P075
Nitric oxide
Nitrogen oxide NO
10102-43-
9
P076
p-Nitroaniline
Benzenamine, 4-nitro-
100-01-6
P077
Nitrobenzene
Benzene, nitro-
98-95-3
P078
Nitrogen dioxide
Nitrogen oxide NO
2
10102-44-
0
P078
Nitrogen mustard
Ethanamine, 2-chloro-N-(2-
51-75-2
101
chloroethyl)-N-methyl-
Nitrogen mus tard, hydro -
chloride salt
Nitrogen mustard N-oxide
Ethanamine, 2-chloro-N-(2-
chloro ethyl)-N-methyl-, N-
oxide
126-85-2
Nitrogen mus tard, N-oxide,
hydrochloride salt
Nitroglycerin
1,2,3-Propanetriol,
trinitrate
55-63-0
P081
p-Nitrophenol
Phenol, 4-nitro-
100-02-7
U170
2-Nitropropane
Propane, 2-nitro-
79-46-9
U171
Nitrosamines, N.O.S.
35576-91-
1
N-Nitrosodi-n-butylamine
1-Butanamine, N-butyl-N-
nitroso-
924-16-3
U172
N-Nitroso diethanolamine
Ethanol, 2,2'-( nitroso -
imino) bis-
1116-54-7
U173
N-Nitrosodi ethylamine
Ethanamine, N-ethyl-N-
nitroso-
55-18-5
U174
N-Nitrosodi methylamine
Methanamine, N-methyl-N-
nitroso-
62-75-9
P082
N-Nitroso-N-ethylurea
Urea, N-ethyl-N- nitroso-
759-73-9
U176
N-Nitroso methyl ethylamine
Ethanamine, N-methyl-N-
nitroso-
10595-95-
6
N-Nitroso-N-methylurea
Urea, N-methyl-N-
nitroso-
684-93-5
U177
N-Nitroso-N-methylurethane
Carbamic acid,
methylnitroso-, ethyl
ester
615-53-2
U178
N-Nitroso methyl vinylamine
Vinylamine, N-methyl-N-
nitroso-
4549-40-0
P084
N-Nitroso morpholine
Morpholine, 4-nitroso-
59-89-2
N-Nitroso nornicotine
Pyridine, 3-(1-nitroso-2-
pyrrolidinyl)-, (S)-
16543-55-
8
N-Nitroso piperidine
Piperidine, 1-nitroso-
100-75-4
U179
N-Nitroso pyrrolidine
Pyrrolidine, 1-nitroso-
930-55-2
U180
N-Nitroso sarcosine
Glycine, N-methyl-N-
nitroso-
13256-22-
9
5-Nitro-o-tolu idine
Benzenamine, 2-methyl-5-
nitro-
99-55-8
U181
Octamethylpyro phosphor amide
Diphosphoramide,
octamethyl-
152-16-9
P085
Osmium tetroxide
Osmium oxide OsO
4
, (T-4)
20816-12-
0
P087
Oxamyl
Ethanimidothioc acid,
2-(dimethyl amino)-N-
[[(methyl amino)carbonyl] -
oxy]-2-oxo -, methyl ester
23135-22-
0
P194
Paraldehyde
1,3,5-Trioxane, 2,4,6-tri
-
methyl-
123-63-7
U182
Parathion
Phosphorothioic acid, O,O-
diethyl O-(4-nitro
phenyl)
ester
56-38-2
P089
Pebulate
Carbamothioic acid,
butyl-
ethyl-, S-propyl ester
1114-71-2
U391
Pentachloro benzene
Benzene, pentachloro-
608-93-5
U183
Pentachlorodi benzo-p-dioxins
Pentachlorodi benzofurans
Pentachloro ethane
Ethane, pentachloro-
76-01-7
U184
Pentachloro nitrobenzene (PCNB)
Benzene, pentachloronitro-
82-68-8
U185
Pentachloro phenol
Phenol, pentachloro-
87-86-5
See
102
F027
Phenacetin
Acetamide, N-(4-
ethoxyphenyl)-
62-44-2
U187
Phenol
Same
108-95-2
U188
Phenylenediamine
Benzenediamine
25265-76-
3
Phenylmercury acetate
Mercury, ( acetato-
O)phenyl-
62-38-4
P092
Phenylthiourea
Thiourea, phenyl-
103-85-5
P093
Phosgene
Carbonic dichloride
75-44-5
P095
Phosphine
Same
7803-51-2
P096
Phorate
Phosphorodithioic acid,
O,O-diethyl S-
[(ethylthio)methyl] ester
298-02-2
P094
Phthalic acid esters, N.O.S.
Phthalic anhydride
1,3-Isobenzofurandione
85-44-9
U190
Physostigmine
Pyrrolo [2,3-b] indol-5-ol,
1,2,3,3a,8,8a-hexa
hydro-
1,3a,8-trimethyl -, methyl -
carbamate (ester),
(3aS-cis)-
57-47-6
P204
Physostigmine salicylate
Benzoic acid, 2 -hydroxy -,
compound with (3aS
-cis)-
1,2,3,3a,8,8a-hexa
hydro-
1,3a,8-trimethyl pyrrolo -
[2,3-b] indol-5-yl methyl -
carbamate ester (1:1)
57-64-7
P188
2-Picoline
Pyridine, 2-methyl-
109-06-8
U191
Polychlorinated biphenyls,
N.O.S.
Potassium cyanide
Same
151-50-8
P098
Potassium dimethyl dithio -
carbamate
Carbamodithioc acid,
dimethyl, potassium salt
128-03-0
U383
Potassium n-hydroxy methyl-n-
methyl-dithio carbamate
Carbamodithioc acid,
(hydroxy methyl )methyl -,
monopotassium salt
51026-28-
9
U378
Potassium n -methyl dithio -
carbamate
Carbamo dithioc acid,
methyl- monopotassium salt
137-41-7
U377
Potassium silver cyanide
Argentate(1-), bis(cyano-
C)-, potassium)
506-61-6
P099
Potassium pentachlorophenate
Pentachlorophenol,
potassium salt
7778736
None
Promecarb
Phenol, 3 -methyl-5-(1-
methyl ethyl) -, methyl
carbamate
2631-37-0
P201
Pronamide
Benzamide, 3,5-dichloro-N-
(1,1-di methyl-2-propynyl)-
23950-58-
5
U192
1,3-Propane sultone
1,2-Oxathiolane, 2,2-
dioxide
1120-71-4
U193
Propham
Carbamic acid, phenyl
-,
1-methyl ethyl ester
122-42-9
U373
Propoxur
Phenol, 2 -(1-methyl -
ethoxy) -, methyl carbamate
114-26-1
U411
n-Propylamine
1-Propanamine
107-10-8
U194
Propargyl alcohol
2-Propyn-1-ol
107-19-7
P102
Propylene dichloride
Propane, 1,2-dichloro-
78-87-5
U083
1,2-Propylen imine
Aziridine, 2-methyl-
75-55-8
P067
Propylthio uracil
4(1H)- Pyrimidinone, 2,3-
dihydro-6-propyl-2-thioxo-
51-52-5
Prosulfocarb
Carbamothioic acid,
dipropyl -, S-(phenyl -
52888-80-
9
U387
103
methyl) ester
Pyridine
Same
110-86-1
U196
Reserpine
Yohimban-16-carboxylic
acid, 11,17-dimethoxy-18-
[(3,4,5-tri methoxy-
benzoyl) oxy]-, methyl
ester,
(3beta,16beta,17alpha,18be
ta,20alpha)-,
50-55-5
U200
Resorcinol
1,3-Benzenediol
108-46-3
U201
Saccharin
1,2-Benzisothiazol-3(2H)-
one, 1,1-dioxide
81-07-2
U202
Saccharin salts
U202
Safrole
1,3-Benzodioxole, 5-(2-
propenyl)-
94-59-7
U203
Selenium
Same
7782-49-2
Selenium compounds, N.O.S.
Selenium dioxide
Selenious acid
7783-00-8
U204
Selenium sulfide
Selenium sulfide SeS
2
7488-56-4
U205
Selenium, tetrakis(dimethyl-
dithiocarbamate
Carbamo dithioic acid,
dimethyl -, tetraanhydro -
sulfide with orthothio-
selenious acid
144-34-3
U376
Selenourea
Same
630-10-4
P103
Silver
Same
7440-22-4
Silver com pounds, N.O.S.
Silver cyanide
Silver cyanide AgCN
506-64-9
P104
Silvex (2,4,5-TP)
Propanoic acid, 2-(2,4,5-
trichlorophenoxy)-
93-72-1
See
F027
Sodium cyanide
Sodium cyanide NaCN
143-33-9
P106
Sodium dibutyl dithio carbamate
Carbamodithioic acid,
dibutyl -, sodium salt
136-30-1
U379
Sodium diethyl dithio carbamate
Carbamodithioic acid,
diethyl -, sodium salt
148-18-5
U381
Sodium dimethyl dithio carbamate
Carbamodithioic acid,
dimethyl -, sodium salt
128-04-1
U382
Sodium pentachlorophenate
Pentachlorophenol, sodium
salt
131522
None
Streptozotocin
D-Glucose, 2-deoxy-2-
[[methyl nitroso amino)ca-
rbonyl]amino]-
18883-66-
4
U206
Strychnine
Strychnidin-10-one
57-24-9
P108
Strychnine salts
P108
Sulfallate
Carbamodithioic acid,
diethyl -, 2-chloro-2-
propenyl ester
95-06-7
U277
TCDD
Dibenzo[ b,e][1,4]dioxin,
2,3,7,8-tetrachloro-
1746-01-6
Tetrabutyl thiuram disulfide
Thioperoxydicarbonic
diamide, tetrabutyl
1634-02-2
U402
Tetrabutylmethyl thiuram
monosulfide
Bis(dimethyl thiocarbamoyl )
sulfide
97-74-5
U401
1,2,4,5-Tetra chlorobenzene
Benzene, 1,2,4,5-
tetrachloro-
95-94-3
U207
Tetrachlorodi benzo-p-dioxins
Tetrachlorodi benzofurans
Tetrachloro ethane , N.O.S.
Ethane, tetrachloro-,
N.O.S.
25322-20-
7
1,1,1,2-Tetra chloro ethane
Ethane, 1,1,1,2-
tetrachloro-
630-20-6
U208
1,1,2,2-Tetra chloro ethane
Ethane, 1,1,2,2-
79-34-5
U209
104
tetrachloro-
Tetrachloro ethylene
Ethene, tetrachloro-
127-18-4
U210
2,3,4,6-Tetra chloro phenol
Phenol, 2,3,4,6-
tetrachloro-
58-90-2
See
F027
2,3,4,6-Tetra chloro phenol,
potassium salt
Same
53535276
None
2,3,4,6-Tetra chloro phenol,
sodium salt
Same
25567559
None
Tetraethyl dithiopyrophosphate
Thiodiphosphoric acid,
tetraethyl ester
3689-24-5
P109
Tetraethyl lead
Plumbane, tetraethyl-
78-00-2
P110
Tetraethyl pyrophosphate
Diphosphoric acid,
tetraethyl ester
107-49-3
P111
Tetranitro methane
Methane, tetranitro-
509-14-8
P112
Thallium
Same
7440-28-0
Thallium compounds
Thallic oxide
Thallium oxide Tl
2
O
3
1314-32-5
P113
Thallium (I) acetate
Acetic acid, thallium (1+)
salt
563-68-8
U214
Thallium (I) carbonate
Carbonic acid, dithallium
(1+) salt
6533-73-9
U215
Thallium (I) chloride
Thallium chloride
TlCl
7791-12-0
U216
Thallium (I) nitrate
Nitric acid, thallium (1+)
salt
10102-45-
1
U217
Thallium selenite
Selenious acid, dithallium
(1+) salt
12039-52-
0
P114
Thallium (I) sulfate
Sulfuric acid, dithallium
(1+) salt
7446-18-6
P115
Thioacetamide
Ethanethioamide
62-55-5
U218
Thiodicarb
Ethanimido thioic acid,
N,N'-[thiobis[( methyl -
imino) carbonyloxy]]- bis-,
dimethyl ester
59669-26-
0
U410
Thiofanox
2-Butanone, 3,3-dimethyl-
1-(methyl thio)-, O-
[(methylamino)carbonyl]
-
oxime
39196-18-
4
P045
Thiophanate-methyl
Carbamic acid,
[1,2-phyenyl enebis( imino-
carbono thioyl )]-bis-,
dimethyl ester
23564-05-
8
U409
Thiomethanol
Methanethiol
74-93-1
U153
Thiophenol
Benzenethiol
108-98-5
P014
Thiosemicarb azide
Hydrazinecarbothioamide
79-19-6
P116
Thiourea
Same
62-56-6
P219
Thiram
Thioperoxydicarbonic
diamide [(H
2
N)C(S)]
2
S
2
,
tetramethyl-
137-26-8
U244
Tirpate
1,3-Dithiolane-2-carbox
-
aldehyde, 2,4 -dimethyl -,
O-[(methyl amino)carbonyl]
oxime
26419-73-
8
P185
Toluene
Benzene, methyl-
108-88-3
U220
Toluenediamine
Benzenediamine, ar-methyl-
25376-45-
8
U221
Toluene-2,4-diamine
1,3-Benzenediamine, 4-
methyl-
95-80-7
Toluene-2,6-di amine
1,3-Benzenediamine, 2-
methyl-
823-40-5
Toluene-3,4-di amine
1,2-Benzenediamine, 4-
methyl-
496-72-0
105
Toluene diisocyanate
Benzene, 1,3-diisocyanato
-
methyl-
26471-62-
5
U223
o-Toluidine
Benzenamine, 2-methyl-
95-53-4
U328
o-Toluidine hydro chloride
Benzeneamine, 2-methyl-,
hydrochloride
636-21-5
U222
p-Toluidine
Benzenamine, 4-methyl-
106-49-0
U353
Toxaphene
Same
8001-35-2
P123
Triallate
Carbamothioic acid,
bis-
(1-methyl ethyl) -,
S-(2,3,3-tri chloro-2-
propenyl) ester
2303-17-5
U389
1,2,4-Tri chloro benzene
Benzene, 1,2,4-trichloro-
120-82-1
1,1,2-Tri chloro ethane
Ethane, 1,1,2-trichloro-
79-00-5
U227
Trichloro ethylene
Ethene, trichloro-
79-01-6
U228
Trichloromethanethiol
Methanethiol, trichloro-
75-70-7
P118
Trichloro monofluoro methane
Methane, trichlorofluoro-
75-69-4
U121
2,4,5-Tri chloro phenol
Phenol, 2,4,5-trichloro-
95-95-4
See
F027
2,4,6-Tri chloro phenol
Phenol, 2,4,6-trichloro-
88-06-2
See
F027
2,4,5-T
Acetic acid, (2,4,5-
trichloro phenoxy)-
93-76-5
See
F027
Trichloropro pane, N.O.S.
25735-29-
9
1,2,3-Tri chloro propane
Propane, 1,2,3-trichloro-
96-18-4
Triethylamine
Ethanamine, N,N -diethyl -
121-44-8
U404
O,O,O- Triethyl phosphoro thioate
Phosphorothioic acid,
O,O,O- triethyl ester
126-68-1
1,3,5-Trinitro benzene
Benzene, 1,3,5-trinitro-
99-35-4
U234
Tris(l- aziridinyl)phosphine
sulfide
Aziridine, 1,1',1"-phos
-
phinothioyl idynetris-
52-24-4
Tris(2,3-di bromopropyl)
phosphate
1-Propanol, 2,3-dibromo-,
phosphate (3:1)
126-72-7
U235
Trypan blue
2,7-Naphthalenedisulfonic
acid, 3,3'-[(3,3'-
dimethyl [1,1'-biphenyl]-
4,4'-diyl) bis(azo)]bis[5-
amino-4-hydroxy-,
tetrasodium salt
72-57-1
U236
Uracil mustard
2,4-(1H,3H)-
Pyrimidinedione, 5-[
bis(2-
chloroethyl)amino]-
66-75-1
U237
Vanadium pentoxide
Vanadium oxide V
2
O
5
1314-62-1
P120
Vernolate
Carbamothioc acid,
dipropyl -, S-propyl ester
1929-77-7
U385
Vinyl chloride
Ethene, chloro-
75-01-4
U043
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl
-
butyl)-, when present at
concentrations less than
0.3%
81-81-2
U248
Warfarin
2H-1-Benzopyran-2-one, 4-
hydroxy-3-(3-oxo-1-phenyl
-
butyl)-, when present at
concentrations greater
than 0.3%
81-81-2
P001
Warfarin salts, when present
at concentrations less than
0.3%
U248
Warfarin salts, when present
at concentrations greater than
P001
106
0.3%
Zinc cyanide
Zinc cyanide Zn(CN)
2
557-21-1
P121
Zinc phosphide
Zinc phosphide P
2
Zn
3
, when
present at concentrations
greater than 10%
1314-84-7
P122
Zinc phosphide
Zinc phosphide P
2
Zn
3
, when
present at concentrations
of 10% or less
1314-84-7
U249
Ziram
Zinc, bis(dimethyl carbamo -
dithioato -S,S') - (T-4)-
137-30-4
P205
Note: The abbreviation N.O.S. (not otherwise specified) signifies those
members of the general class not specifically listed by name in this Section.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 722
STANDARDS APPLICABLE TO GENERATORS OF HAZARDOUS WASTE
SUBPART A: GENERAL
Section
722.110
Purpose, Scope and Applicability
722.111
Hazardous Waste Determination
722.112
USEPA Identification Numbers
SUBPART B: THE MANIFEST
Section
722.120
General Requirements
722.121
Acquisition of Manifests
722.122
Number of Copies
722.123
Use of the Manifest
SUBPART C: PRE-TRANSPORT REQUIREMENTS
Section
722.130
Packaging
722.131
Labeling
722.132
Marking
722.133
Placarding
722.134
Accumulation Time
SUBPART D: RECORDKEEPING AND REPORTING
Section
722.140
Recordkeeping
722.141
Annual Reporting
722.142
Exception Reporting
722.143
Additional Reporting
722.144
Special Requirements for Generators of between 100 and 1000
kilograms per month
SUBPART E: EXPORTS OF HAZARDOUS WASTE
Section
722.150
Applicability
722.151
Definitions
722.152
General Requirements
722.153
Notification of Intent to Export
107
722.154
Special Manifest Requirements
722.155
Exception Report
722.156
Annual Reports
722.157
Recordkeeping
722.158
International Agreements
SUBPART F: IMPORTS OF HAZARDOUS WASTE
Section
722.160
Imports of Hazardous Waste
SUBPART G: FARMERS
Section
722.170
Farmers
SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
FOR RECOVERY WITHIN THE OECD
Section
262.180 Applicability
262.181 Definitions
262.182 General Conditions
262.183 Notification and Consent
262.184 Tracking Document
262.185 Contracts
262.186 Provisions Relating to Recognized Traders
262.187 Reporting and Recordkeeping
262.189 OECD Waste Lists
722.Appendix A
Hazardous Waste Manifest
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
effective May 17, 1982; amended in R82-18, 51 PCB 31, at 7 Ill. Reg. 2518,
effective February 22, 1983; amended in R84-9 at 9 Ill. Reg. 11950, effective
July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1131, effective January 2,
1986; amended in R86-1 at 10 Ill. Reg. 14112, effective August 12, 1986;
amended in R86-19 at 10 Ill. Reg. 20709, effective December 2, 1986; amended
in R86-46 at 11 Ill. Reg. 13555, effective August 4, 1987; amended in R87-5 at
11 Ill. Reg. 19392, effective November 12, 1987; amended in R87-39 at 12 Ill.
Reg. 13129, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 452,
effective December 27, 1988; amended in R89-1 at 13 Ill. Reg. 18523, effective
November 13, 1989; amended in R90-10 at 14 Ill. Reg. 16653, effective
September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9644, effective June 17,
1991; amended in R91-1 at 15 Ill. Reg. 14562, effective October 1, 1991;
amended in R91-13 at 16 Ill. Reg. 9833, effective June 9, 1992; amended in
R92-1 at 16 Ill. Reg. 17696, effective November 6, 1992; amended in R93-4 at
17 Ill. Reg. 20822, effective November 22, 1993; amended in R95-6 at 19 Ill.
Reg. 9935, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11236,
August 1, 1996 ; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________,
effective ____________________
.
SUBPART A: GENERAL
Section 722.110
Purpose, Scope and Applicability
a)
These regulations establish standards for generators of hazardous
waste.
108
b)
35 Ill. Adm. Code 721.105(c) and (d) must be used to determine the
applicability of provisions of this Part that are dependent on
calculations of the quantity of hazardous waste generated per
month.
c)
A generator whothat treats, stores or disposes of hazardous waste
on-site must only comply with the following Sections of this Part
with respect to that waste: Section 722.111 for determining
whether or not the generator has a hazardous waste, Section
722.112 for obtaining an EPA identification number, Section
722.140(c) and (d) for
recordkeeping, Section 722.143 for
additional reporting and, if applicable, Section 722.170 for
farmers.
d)
Any person whothat exports or imports hazardous waste
into the
United States subject to the hazardous waste manifesting
requirements of 35 Ill. Adm. Code 722 or subject to the universal
waste management standards of 35 Ill. Adm. Code 733 to or from
countries listed in Section 722.158(a)(1) for recovery
must comply
with the standards applicable to generators established in this
Part722.Subpart H .
e)
A farmer whothat generates waste pesticides which are hazardous
waste and whothat complies with all of the requirements of Section
722.151 is not required to comply with other standards in this
Part, or 35 Ill. Adm. Code 702, 703, 724 725 or 728 with respect
to such pesticides.
f)
A person whothat generates a hazardous waste as defined by 35 Ill.
Adm. Code 721 is subject to the compliance requirements and
penalties prescribed in Title VIII and XII of the Environmental
Protection Act if he does not comply with the requirements of this
Part.
g)
An owner or operator
whothat initiates a shipment of hazardous
waste from a treatment, storage or disposal facility must comply
with the generator standards established in this Part.
BOARD NOTE: The provisions of Section 722.134 are applicable to
the on-site accumulation of hazardous waste by generators.
Therefore, the provisions of Section 722.134 only apply to owners
or operators whothat are shipping hazardous waste which they
generated at that facility. A generator
whothat treats, stores or
disposes of hazardous waste on-site must comply with the
applicable standards and permit requirements set forth in 35 Ill.
Adm. Code 702, 703, 724, 725, 726 and 728.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART C: PRE-TRANSPORT REQUIREMENTS
Section 722.134
Accumulation Time
a)
Except as provided in subsections (d), (e), or (f) below, a
generator is exempt from all the requirements in 35 Ill. Adm. Code
725.Subparts G and H, except for 35 Ill. Adm. Code 725.211 and
725.214, and may accumulate hazardous waste on-site for 90 days or
less without a permit or without having interim status, provided
that:
109
1)
The waste is placed:
A)
In containers and the generator complies with 35 Ill.
Adm. Code 725.Subpart
s I, AA, BB, and CC ; or
B)
In tanks and the generator complies with 35 Ill. Adm.
Code 725.Subparts J
, (except 35 Ill. Adm. Code
725.297(c) and 725.300
), AA, BB, and CC
; or
C)
On drip pads and the generator complies with 35 Ill.
Adm. Code 725.Subpart W and maintains the following
records at the facility:
i)
A description of the procedures that will be
followed to ensure that all wastes are removed
from the drip pad and associated collection
system at least once every 90 days, and
ii)
Documentation of each waste removal, including
the quantity of waste removed from the drip pad
and the sump or collection system and the date
and time of removal; or
D)
In containment buildings and the generator complies
with 35 Ill. Adm. Code 725.Subpart DD (has placed its
Professional Engineer (PE) certification that the
building complies with the design standards specified
in 35 Ill. Adm. Code 725.1101 in the facility's
operating record prior to the date of initial
operation of the unit). The owner or operator shall
maintain the following records at the facility:
i)
A written description of procedures to ensure
that each waste volume remains in the unit for
no more than 90 days, a written description of
the waste generation and management practices
for the facility showing that they are
consistent with respecting the 90 day limit, and
documentation that the procedures are complied
with; or
ii)
Documentation that the unit is emptied at least
once every 90 days.
BOARD NOTE: The "in addition" hanging
subsection that appears in the Federal rules
after 40 CFR 262.34(a)(1)(iv)(B) is in the
introduction to subsection (a) above.
2)
The date upon which each period of accumulation begins is
clearly marked and visible for inspection on each container;
3)
While being accumulated on-site, each container and tank is
labeled or marked clearly with the words "Hazardous Waste",
and
4)
The generator complies with the requirements for treatment,
storage, and disposal facility owners or operators in 35
Ill. Adm. Code 725.Subparts C and D and with 35 Ill. Adm.
Code 725.116 and 728.107(a)(4).
110
b)
A generator that accumulates hazardous waste for more than 90 days
is an operator of a storage facility and is subject to the
requirements of 35 Ill. Adm. Code 724 and 725 and the permit
requirements of 35 Ill. Adm. Code 702, 703 and 705 unless the
generator has been granted an extension of the 90-day period. If
hazardous wastes must remain on-site for longer than 90 days due
to unforeseen, temporary, and uncontrollable circumstances, the
generator may seek an extension of up to 30 days by means of a
variance or provisional variance, pursuant to Section 37 of the
Environmental Protection Act and 35 Ill. Adm. Code 180 (Agency
procedural regulations).
c)
Accumulation near the point of generation.
1)
A generator may accumulate as much as 55 gallons of
hazardous waste or one quart of acutely hazardous waste
listed in 35 Ill. Adm. Code 721.133(e) in containers at or
near any point of generation where wastes initially
accumulate that is under the control of the operator of the
process generating the waste without a permit or interim
status and without complying with subsection (a) above,
provided the generator:
A)
Complies with 35 Ill. Adm. Code 725.271, 725.272 and
725.273(a), and
B)
Marks the generator's containers either with the words
"Hazardous Waste" or with other words that identify
the contents of the containers.
2)
A generator that accumulates either hazardous waste or
acutely hazardous waste listed in 35 Ill. Adm. Code
721.133(e) in excess of the amounts listed in subsection
(c)(1) above at or near any point of generation must, with
respect to that amount of excess waste, comply within three
days with subsection (a) above or other applicable
provisions of this Chapter. During the three day period the
generator must continue to comply with subsection (c)(1)
above. The generator must mark the container holding the
excess accumulation of hazardous waste with the date the
excess amount began accumulating.
d)
A generator that generates greater than 100 kilograms but less
than 1000 kilograms of hazardous waste in a calendar month may
accumulate hazardous waste on-site for 180 days or less without a
permit or without having interim status provided that:
1)
The quantity of waste accumulated on-site never exceeds 6000
kilograms;
2)
The generator complies with the requirements of 35 Ill. A
dm.
Code 725.Subpart I (except 35 Ill. Adm. Code 725.276 and
725.278);
3)
The generator complies with the requirements of 35 Ill. Adm.
Code 725.301;
4)
The generator complies with the requirements of subsections
(a)(2) and (c)(3) above, 35 Ill. Adm. Code 725.Subpart C,
and 35 Ill. Adm. Code 728.107(a)(4); and
111
5)
The generator complies with the following requirements:
A)
At all times there must be at least one employee
either on the premises or on call (i.e., available to
respond to an emergency by reaching the facility
within a short period of time) with the responsibility
for coordinating all emergency response measures
specified in subsection (d)(5)(D) below. The employee
is the emergency coordinator.
B)
The generator shall post the following information
next to the telephone:
i)
The name and telephone number of the emergency
coordinator;
ii)
Location of fire extinguishers and spill control
material and, if present, fire alarm; and
iii)
The telephone number of the fire depar
tment,
unless the facility has a direct alarm.
C)
The generator shall ensure that all employees are
thoroughly familiar with proper waste handling and
emergency procedures, relevant to their
responsibilities during normal facility operations and
emergencies;
D)
The emergency coordinator or designee shall respond to
any emergencies that arise. The applicable responses
are as follows:
i)
In the event of a fire, call the fire department
or attempt to extinguish it using a fire
extinguisher;
ii)
In the event of a spill, contain the flow of
hazardous waste to the extent possible and, as
soon as is practicable, clean up the hazardous
waste and any contaminated materials or soil;
iii)
In the event of a fire, explosion, or other
release that could threaten human health outside
the facility, or when the generator has
knowledge that a spill has reached surface
water, the generator shall immediately notify
the National Response Center (using its 24-hour
toll free number 800-424-8802). The report must
include the following information: the name,
address, and U .S. EPA identification number (35
Ill. Adm. Code 722.112) of the generator; the
date, time, and type of incident (e.g., spill or
fire); the quantity and type of hazardous waste
involved in the incident; the extent of
injuries, if any; and the estimated quantity and
disposition of recoverable materials, if any.
e)
A generator that generates greater than 100 kilograms but less
than 1000 kilograms of hazardous waste in a calendar month and
that must transport the waste or offer the waste for
transportation over a distance of 200 miles or more for off-site
112
treatment, storage, or disposal may accumulate hazardous waste on-
site for 270 days or less without a permit or without having
interim status, provided that the generator complies with the
requirements of subsection (d) above.
f)
A generator that generates greater than 100 kilograms but less
than 1000 kilograms of hazardous waste in a calendar month and
that accumulates hazardous waste in quantities exceeding 6000 kg
or accumulates hazardous waste for more than 180 days (or for more
than 270 days if the generator must transport the waste or offer
the waste for transportation over a distance of 200 miles or more)
is an operator of a storage facility and is subject to the
requirements of 35 Ill. Adm. Code 724 and 725 and the permit
requirements of 35 Ill. Adm. Code 703 unless the generator has
been granted an extension to the 180-day (or 270-day if
applicable) period. If hazardous wastes must remain on-site for
longer than 180 days (or 270 days if applicable) due to
unforeseen, temporary, and uncontrollable circumstances, the
generator may seek an extension of up to 30 days by means of
variance or provisional variance pursuant to Section 37 of the
Environmental Protection Act.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART E: EXPORTS OF HAZARDOUS WASTE
Section 722.153
Notification of Intent to Export
a)
The Board incorporates by reference 40 CFR 262.53
(199196), as
amended at 56 Fed. Reg. 43705, September 4, 1991
. This Part
incorporates no future editions or amendments.
b)
A primary exporter of hazardous waste shall notify USEPA in
accordance with 40 CFR 262.53
(1996) .
c)
The primary exporter shall send the Agency a copy of
theeach
notice sent to USEPA pursuant to subsection (b)
above .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 722.156
Annual Reports
a)
The Board incorporates by reference 40 CFR 262.56 (19
9196), as
amended at 56 Fed. Reg. 43705, September 4, 1991
. This Part
incorporates no future editions or amendments.
b)
Primary exporters of hazardous waste shall file with USEPA, no
later than March 1 of each year, a report as specified in 40 CFR
262.56 (1996) .
c)
The primary exporter shall send the Agency a copy of
theeach
report sent to USEPA.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 722.158
International Agreements
a)
Any person that exports or imports hazardous waste subject to
either the manifest requirements of this Part or the universal
waste management standards of 35 Ill. Adm. Code 733 which is
113
shipped to or from designated member countries of the Organization
for Economic Cooperation and Development (OECD), as defined in
subsection (a)(1) below, for purposes of recovery is subject to
the requirements of 722.Subpart H. The requirements of
722.Subparts E and F do not apply where 722.Subpart H applies.
1)
For the purposes of this Subpart, the designated OECD
countries are Australia, Austria, Belgium, Denmark, Finland,
France, Germany, Greece, Iceland, Ireland, Italy, Japan,
Luxembourg, Netherlands, New Zealand, Norway, Portugal,
Spain, Sweden, Switzerland, Turkey, the United Kingdom, and
the United States.
2)
Only for the purposes of transit under this Subpart, Canada
and Mexico are considered OECD member countries.
b)
Any person that exports hazardous waste to or imports hazardous
waste from any of a designated OECD member country for purposes
other than recovery (e.g., incineration, disposal), Mexico (for
any purpose), or Canada (for any purpose) remains subject to the
requirements of 722.Subparts E and F.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
SUBPART H: TRANSFRONTIER SHIPMENTS OF HAZARDOUS WASTE
FOR RECOVERY WITHIN THE OECD
Section 722.180
Applicability
a)
The requirements of this Subpart apply to imports and exports of
wastes that are considered hazardous under U.S. national
procedures and which are destined for recovery operations in any
of the countries listed in Section 722.158(a)(1). A waste is
considered hazardous under U.S. national procedures if it meets
the definition of hazardous waste in 35 Ill. Adm. Code 721.103 and
it is subject to either the manifesting requirements at 35 Ill.
Adm. Code 722.Subpart B, to the universal waste management
standards of 35 Ill. Adm. Code 733.
b)
Any person ( notifier, consignee, or recovery facility operator)
that mixes two or more wastes (including hazardous and
non-hazardous wastes) or otherwise subjects two or more wastes
(including hazardous and non
-hazardous wastes) to physical or
chemical transformation operations, and thereby creates a new
hazardous waste, becomes a generator and assumes all subsequent
generator duties under this Subchapter and any
notifier duties
under this Subpart, as applicable.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.181
Definitions
The following definitions apply to this Subpart:
"Competent authorities" means the regulatory authorities of
concerned countries having jurisdiction over
transfrontier
movements of wastes destined for recovery operations.
"Concerned countries" means the exporting and importing OECD
member countries and any OECD member countries of transit.
114
"Consignee" means the person to whom possession or other form of
legal control of the waste is assigned at the time the waste is
received in the importing country.
"Country of transit" means any designated OECD country in Section
722.158(a)(1) and (a)(2) other than the exporting or importing
country across which a
transfrontier movement of wastes is planned
or takes place.
"Exporting country" means any designated OECD member country in
Section 722.158(a)(1) from which a
transfrontier movement of
wastes is planned or has commenced.
"Importing country" means any designated OECD country in Section
722.158(a)(1) to which a
transfrontier movement of wastes is
planned or takes place for the purpose of submitting the wastes to
recovery operations therein.
"Notifier" means the person under the jurisdiction of the
exporting country that has, or will have at the time the planned
transfrontier movement commences, possession or other forms of
legal control of the wastes and that proposes their
transfrontier
movement for the ultimate purpose of submitting them to recovery
operations. When the United States (U.S.) is the exporting
country, notifier is interpreted to mean a person domiciled in the
U.S.
"OECD area" means all land or marine areas under the national
jurisdiction of any designated OECD member country in Section
722.158. When the regulations refer to shipments to or from an
OECD country, this means OECD area.
"Recognized trader" means a person that, with appropriate
authorization of concerned countries, acts in the role of
principal to purchase and subsequently sell wastes; this person
has legal control of such wastes from time of purchase to time of
sale; such a person may act to arrange and facilitate
transfrontier movements of wastes destined for recovery
operations.
"Recovery facility" means an entity which, under applicable
domestic law, is operating or is authorized to operate in the
importing country to receive wastes and to perform recovery
operations on them.
"Recovery operations" means activities leading to resource
recovery, recycling, reclamation, direct re
-use, or alternative
uses, as listed in Table 2.B of the Annex of OECD Council Decision
C(88)90(Final) of 27 May 1988, incorporated by reference in 35
Ill. Adm. Code 720.111, which include the following activities:
R1
Use as a fuel (other than in direct incineration) or
other means to generate energy,
R2
Solvent reclamation or regeneration,
R3
Recycling or reclamation of organic substances which
are not used as solvents,
R4
Recycling or reclamation of metals and metal
115
compounds,
R5
Recycling or reclamation of other inorganic materials,
R6
Regeneration of acids or bases,
R7
Recovery of components used for pollution control,
R8
Recovery of components from catalysts,
R9
Used oil re -refining or other reuses of previously
used oil,
R10
Land treatment resulting in benefit to agriculture or
ecological improvement,
R11
Uses of residual materials obtained from any of the
operations numbered R1 through R10,
R12
Exchange of wastes for submission to any of the
operations numbered R1 through R11, and
R13
Accumulation of material intended for any operation in
Table 2.B.
"Transfrontier movement" means any shipment of wastes destined for
recovery operations from an area under the national jurisdiction
of one OECD member country to an area under the national
jurisdiction of another OECD member country.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.182
General Conditions
a)
Scope. The level of control for exports and imports of waste is
indicated by assignment of the waste to a green, amber, or red
list and by U.S. national procedures, as defined in Section
722.180(a). The green, amber, and red lists are incorporated by
reference in Section 722.89 (e).
1)
Wastes on the green list are subject to existing controls
normally applied to commercial transactions, except as
provided below:
A)
Green-list wastes that are considered hazardous under
U.S. national procedures are subject to amber
-list
controls.
B)
Green-list wastes that are sufficiently contaminated
or mixed with amber
-list wastes, such that the waste
or waste mixture is considered hazardous under U.S.
national procedures, are subject to amber
-list
controls.
C)
Green-list wastes that are sufficiently contaminated
or mixed with other wastes subject to red
-list
controls, such that the waste or waste mixture is
considered hazardous under U.S. national procedures,
must be handled in accordance with the red
-list
controls.
116
2)
Wastes on the amber list that are considered hazardous under
U.S. national procedures, as defined in Section 722.180(a),
are subject to the amber
-list controls of th
is Subpart. If
amber-list wastes are sufficiently contaminated or mixed
with other wastes subject to red
-list controls, such that
the waste or waste mixture is considered hazardous under
U.S. national procedures, the wastes must be handled in
accordance with the red
-list controls.
3)
Wastes on the red list that are considered hazardous under
U.S. national procedures, as defined in Section 722.180(a),
are subject to the red
-list controls of this Subpart.
BOARD NOTE: Some wastes on the amber or red lists are not
listed or otherwise identified as hazardous under RCRA
(e.g., polychlorinated
biphenyls) and therefore are not
subject to the amber
- or red -list controls of this Subpart.
Regardless of the status of the waste under RCRA, however,
other federal environmental statutes (e.g., the Toxic
Substances Control Act) may restrict certain waste imports
or exports. Such restrictions continue to apply without
regard to this Subpart.
4)
Wastes not yet assigned to a list are eligible for
transfrontier movements, as follows:
A)
If such wastes are considered hazardous under U.S.
national procedures, as defined in Section 722.180(a),
these wastes are subject to the red
-list controls; or
B)
If such wastes are not considered hazardous under U.S.
national procedures, as defined in Section 722.80(a),
such wastes may move as though they appeared on the
green list.
b)
General conditions applicable to
transfrontier movements of
hazardous waste.
1)
The waste must be destined for recovery operations at a
facility that, under applicable domestic law, is operating
or is authorized to operate in the importing country;
2)
The transfrontier movement must be in compliance with
applicable international transport agreements; and
BOARD NOTE: These international agreements include, but are
not limited to, the Chicago Convention (1944), ADR (1957),
ADNR (1970), MARPOL Convention (1973/1978), SOLAS Convention
(1974), IMDG Code (1985), COTIF (1985), and RID (1985).
3)
Any transit of waste through a non
-OECD me mber country must
be conducted in compliance with all applicable international
and national laws and regulations.
c)
Provisions relating to re
-export for recovery to a third country.
1)
Re-export of wastes subject to the amber
-list control system
from the U.S., as the importing country, to a third country
listed in Section 722.158(a)(1) may occur only after a
notifier in the U.S. provides notification to and obtains
consent of the competent authorities in the third country,
117
the original exporting country, and new transit countries.
The notification must comply with the notice and consent
procedures in Section 722.183 for all concerned countries
and the original exporting country. The competent
authorities of the original exporting country, as well as
the competent authorities of all other concerned countries,
have 30 days to object to the proposed movement.
A)
The 30 -day period begins once the competent
authorities of both the initial exporting country and
new importing country issue
Acknowledgements of
Receipt of the notification.
B)
The transfrontier movement may commence if no
objection has been lodged after the 30
-day period has
passed or immediately after written consent is
received from all relevant OECD importing and transit
countries.
2)
Re-export of waste subject to the red
-list control system
from the original importing country to a third country
listed in Section 722.158(a)(1) may occur only following
notification of the competent authorities of the third
country, the original exporting country, and new transit
countries by a notifier in the original importing country in
accordance with Section 722.183. The
transfrontier movement
may not proceed until receipt by the original importing
country of written consent from the competent authorities of
the third country, the original exporting country, and new
transit countries.
3)
In the case of re
-export of amber or red
-list wastes to a
country other than those in Section 722.158(a)(1),
notification to and consent of the competent authorities of
the original OECD member country of export and any OECD
member countries of transit is required as specified in
subsections (c)(1) and (c)(2) above in addition to
compliance with all international agreements and
arrangements to which the first importing OECD member
country is a party and all applicable regulatory
requirements for exports from the first importing country.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.183
Notification and Consent
a)
Applicability. Consent must be obtained from the competent
authorities of the relevant OECD importing and transit countries
prior to exporting hazardous waste destined for recovery
operations subject to this Subpart. Hazardous wastes subject to
amber-list controls are subject to the requirements of subsection
(b) below; hazardous wastes subject to red
-list controls are
subject to the requirements of subsection (c) below; and wastes
not identified on any list are subject to the requirements of
subsection (d) below.
b)
Amber-list wastes. The export from the U.S. of hazardous wastes,
as described in Section 722.180(a), that appear on the amber list
is prohibited unless the notification and consent requirements of
subsection (b)(1) or subsection (b)(2) below are met.
118
1)
Transactions requiring specific consent:
A)
Notification. At least 45 days prior to commencement
of the transfrontier movement, the
notifier must
provide written notification in English of the
proposed transfrontier movement to the Office of
Enforcement and Compliance Assurance, Office of
Compliance, Enforcement Planning, Targeting and Data
Division (2222A), Environmental Protection Agency, 401
M St., SW., Washington, DC 20460, and the Illinois
Environmental Protection Agency, Bureau of Land,
Division of Land Pollution Control,
P.O. Box 19276,
Springfield, IL 62794-9276, with the words "Attention:
OECD Export Notification" prominently displayed on the
envelope. This notification must include all of the
information identified in subsection (e) below. In
cases where wastes having similar physical and
chemical characteristics, the same United Nations
classification, and the same RCRA waste codes are to
be sent periodically to the same recovery facility by
the same notifier, the notifier may submit one
notification of intent to export these wastes in
multiple shipments during a period of up to one year.
B)
Tacit consent. If no objection has been lodged by any
concerned country (i.e., exporting, importing, or
transit countries) to a notification provided pursuant
to subsection (b)(1)(A) above within 30 days after the
date of issuance of the Acknowledgment of Receipt of
notification by the competent authority of the
importing country, the
transfrontier movement may
commence. Tacit consent expires one calendar year
after the close of the 30 day period;
renotification
and renewal of all consents is required for exports
after that date.
C)
Written consent. If the competent authorities of all
the relevant OECD importing and transit countries
provide written consent in a period less than 30 days,
the transfrontier movement may commence immediately
after all necessary consents are received. Written
consent expires for each relevant OECD importing and
transit country one calendar year after the date of
that country's consent unless otherwise specified;
renotification and renewal of each expired consent is
required for exports after that date.
2)
Shipments to facilities pre
-approved by the competent
authorities of the importing countries to accept specific
wastes for recovery:
A)
The notifier must provide USEPA and the Agency the
information identified in subsection (e) below in
English, at least 10 days in advance of commencing
shipment to a pre
-approved facility. The notification
should indicate that the recovery facility is
pre-approved, and may apply to a single specific
shipment or to multiple shipments as described in
subsection (b)(1)(A) above. This information must be
sent to the Office of Enforcement and Compliance
Assurance, Office of Compliance, Enforcement Planning,
119
Targeting and Data Division (2222A), Environmental
Protection Agency, 401 M St., SW., Washington, DC
20460, and the Illinois Environmental Protection
Agency, Bureau of Land, Division of Land Pollution
Control, P.O. Box 19276, Springfield, IL 62794-9276,
with the words "OECD Export
Notification --Pre-approved
Facility" prominently displayed on the envelope.
B)
Shipments may commence after the notification required
in subsection (b)(1)(A) above has been received by the
competent authorities of all concerned countries,
unless the notifier has received information
indicating that the competent authorities of one or
more concerned countries objects to the shipment.
c)
Red-list wastes. The export from the U.S. of hazardous wastes, as
described in Section 722.180(a), that appear on the red list is
prohibited unless notice is given pursuant to subsection (b)(1)(A)
above and the notifier receives written consent from the importing
country and any transit countries prior to commencement of the
transfrontier movement.
d)
Unlisted wastes. Wastes not assigned to the green, amber, or red
list that are considered hazardous under U.S. national procedures,
as defined in Section 722.180(a), are subject to the notification
and consent requirements established for red
-list wastes in
accordance with subsection (c) above. Unlisted wastes that are
not considered hazardous under U.S. national procedures, as
defined in Section 722.80(a), are not subject to amber or red
controls when exported or imported.
e)
Notification information. Notifications submitted under this
Section must include:
1)
Serial number or other accepted identifier of the
notification form;
2)
Notifier name and EPA identification number (if applicable),
address, and telephone and
telefax numbers;
3)
Importing recovery facility name, address, telephone and
telefax numbers, and technologies employed;
4)
Consignee name (if not the owner or operator of the recovery
facility) address, and telephone and
telefax numbers;
whether the consignee will engage in waste exchange or
storage prior to delivering the waste to the final recovery
facility; and identification of recovery operations to be
employed at the final recovery facility;
5)
Intended transporters or their agents;
6)
Country of export and relevant competent authority and point
of departure;
7)
Countries of transit and relevant competent authorities and
points of entry and departure;
8)
Country of import and relevant competent authority and point
of entry;
120
9)
Statement of whether the notification is a single
notification or a general notification. If general, include
period of validity requested;
10)
Date foreseen for commencement of
transfrontier movement;
11)
Designation of waste type(s) from the appropriate list
(amber or red and waste list code), descriptions of each
waste type, estimated total quantity of each, RCRA waste
code, and United Nations number for each waste type; and
12)
Certification/Declaration signed by the
notifier that states
as follows:
"I certify that the above information is complete and
correct to the best of my knowledge. I also certify that
legally -enforceable written contractual obligations have
been entered into, and that any applicable insurance or
other financial guarantees are or shall be in force covering
the transfrontier movement.
Name:-------------------------------------------------------
Signature: --------------------------------------------------
Date:------------------------------------------------------"
BOARD NOTE: The U.S. does not currently require financial
assurance; however, U.S. exporters may be asked by other
governments to provide and certify to such assurance as a
condition of obtaining consent to a proposed movement.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.184
Tracking Document
a)
All U.S. parties subject to the contract provisions of Section
722.185 must ensure that a tracking document meeting the
conditions of Section 722.184(b) accompanies each
transfrontier
shipment of wastes subject to amber
-list or red -list controls from
the initiation of the shipment until it reaches the final recovery
facility, including cases in which the waste is stored or
exchanged by the consignee prior to shipment to the final recovery
facility, except as provided in Section 262.184(a)(1) and (a)(2).
1)
For shipments of hazardous waste within the U.S. solely by
water (bulk shipments only), the generator must forward the
tracking document with the manifest to the last water (bulk
shipment) transporter to handle the waste in the U.S. if
exported by water, (in accordance with the manifest routing
procedures at Section 722.123(c)).
2)
For rail shipments of hazardous waste within the U.S. which
originate at the site of generation, the generator must
forward the tracking document with the manifest (in
accordance with the routing procedures for the manifest in
Section 722.123(d)) to the next non
-rail transporter, if
any, or the last rail transporter to handle the waste in the
U.S. if exported by rail.
b)
The tracking document must include all information required under
121
Section 722.183 (for notification) and the following:
1)
The date shipment commenced;
2)
The name (if not
notifier), address, and telephone and
telefax numbers of primary exporter;
3)
The company name and USEPA identification number of all
transporters;
4)
Identification (license, registered name or registration
number) of means of transport, including types of packaging;
5)
Any special precautions to be taken by transporters;
6)
A certification or declaration signed by
notifier that no
objection to the shipment has been lodged as follows:
"I certify that the above information is complete and
correct to the best of my knowledge. I also certify that
legally -enforceable written contractual obligations have
been entered into, that any applicable insurance or other
financial guarantees are or shall be in force covering the
transfrontier movement, and that:"
"1. All necessary consents have been received;" OR
"2. The shipment is directed at a recovery facility within
the OECD area and no objection has been received from any of
the concerned countries within the 30 day tacit consent
period;" OR
"3. The shipment is directed at a recovery facility
pre-authorized for that type of waste within the OECD area;
such an authorization has not been revoked, and no objection
has been received from any of the concerned countries."
(delete sentences that are not applicable)
"Name: ------------------------------------------------------
Signature: --------------------------------------------------
Date:-------------------------------------------------"; and
7)
The appropriate signatures for each custody transfer (e.g.
transporter, consignee, and owner or operator of the
recovery facility).
c)
Notifiers also must comply with the special manifest requirements
of 35 Ill. Adm. Code 722.154(a), (b), (c), (e), and (i) and
consignees must comply with the import requirements of 35 Ill.
Adm. Code 722.Subpart F.
d)
Each U.S. person that has physical custody of the waste from the
time the movement commences until it arrives at the recovery
facility must sign the tracking document (e.g. transporter,
consignee, and owner or operator of the recovery facility).
e)
Within 3 working days of the receipt of imports subject to this
Subpart, the owner or operator of the U.S. recovery facility must
122
send signed copies of the tracking document to the
notifier, to
the Office of Enforcement and Compliance Assurance, Office of
Compliance, Enforcement Planning, Targeting and Data Division
(2222A), Environmental Protection Agency, 401 M St., SW.,
Washington, DC 20460, and to the competent authorities of the
exporting and transit countries.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.185
Contracts
a)
Transfrontier movements of hazardous wastes subject to amber or
red control procedures are prohibited unless they occur under the
terms of a valid written contract, chain of contracts, or
equivalent arrangements (when the movement occurs between parties
controlled by the same corporate or legal entity). Such contracts
or equivalent arrangements must be executed by the
notifier and
the owner or operator of the recovery facility, and must specify
responsibilities for each. Contracts or equivalent arrangements
are valid for the purposes of this Section only if persons
assuming obligations under the contracts or equivalent
arrangements have appropriate legal status to conduct the
operations specified in the contract or equivalent arrangement.
b)
Contracts or equivalent arrangements must specify the following
names and USEPA identification numbers, where available:
1)
The generator of each type of waste;
2)
Each person that will have physical custody of the wastes;
3)
Each person that will have legal control of the wastes; and
4)
The recovery facility.
c)
Contracts or equivalent arrangements must specify which party to
the contract will assume responsibility for alternate management
of the wastes if its disposition cannot be carried out as
described in the notification of intent to export. In such cases,
contracts must specify the following:
1)
That the person having actual possession or physical control
over the wastes will immediately inform the
notifier and the
competent authorities of the exporting and importing
countries and, if the wastes are located in a country of
transit, the competent authorities of that country; and
2)
That the person specified in the contract will assume
responsibility for the adequate management of the wastes in
compliance with applicable laws and regulations including,
if necessary, arranging their return to the original country
of export.
d)
Contracts must specify that the consignee will provide the
notification required in Section 722.182(c) prior to re
-export of
controlled wastes to a third country.
e)
Contracts or equivalent arrangements must include provisions for
financial guarantees, if required by the competent authorities of
any concerned country, in accordance with applicable national or
international law requirements.
123
BOARD NOTE: Financial guarantees so required are intended to
provide for alternative recycling, disposal, or other means of
sound management of the wastes in cases where arrangements for the
shipment and the recovery operations cannot be carried out as
foreseen. The U.S. does not require such financial guarantees at
this time; however, some OECD countries do. It is the
responsibility of the
notifier to ascertain and comply with such
requirements; in some cases, transporters or consignees may refuse
to enter into the necessary contracts absent specific references
or certifications to financial guarantees.
f)
Contracts or equivalent arrangements must contain provisions
requiring each contracting party to comply with all applicable
requirements of this Subpart.
g)
Upon request by USEPA or the Agency, U.S.
notifiers, consignees,
or recovery facilities shall submit to USEPA and the Agency copies
of contracts, chain of contracts, or equivalent arrangements (when
the movement occurs between parties controlled by the same
corporate or legal entity). Information contained in the
contracts or equivalent arrangements for which a claim of
confidentiality is asserted in accordance with 35 Ill. Adm. Code
120 will be treated as confidential and will be disclosed by the
Agency only as provided in 35 Ill. Adm. Code 120.
BOARD NOTE: Although the U.S. does not require routine submission
of contracts at this time, OECD Council Decision C(92)39/FINAL
allows members to impose such requirements. When other OECD
countries require submission of partial or complete copies of the
contract as a condition to granting consent to proposed movements,
USEPA or the Agency will request the required information; absent
submission of such information, some OECD countries may deny
consent for the proposed movement.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.186
Provisions Relating to Recognized Traders
a)
A recognized trader that takes physical custody of a waste and
conducts recovery operations (including storage prior to recovery)
is acting as the owner or operator of a recovery facility and must
be so authorized in accordance with all applicable federal laws.
b)
A recognized trader acting as a
notifier or consignee for
transfrontier shipments of waste must comply with all the
notifier
or consignee requirements of this Subpart.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.187
Reporting and Recordkeeping
a)
Annual reports. For all waste movements subject to this Subpart,
persons (e.g., notifiers, recognized traders) that meet the
definition of primary exporter in Section 722.151 shall file an
annual report with the Office of Enforcement and Compliance
Assurance, Office of Compliance, Enforcement Planning, Targeting
and Data Division (2222A), U.S. Environmental Protection Agency,
401 M St., SW., Washington, DC 20460 and the Illinois
Environmental Protection Agency, Bureau of Land, Division of Land
Pollution Control,
P.O. Box 19276, Springfield, IL 62706-9276, no
124
later than March 1 of each year summarizing the types, quantities,
frequency, and ultimate destination of all such hazardous waste
exported during the previous calendar year. (If the primary
exporter is required to file an annual report for waste exports
that are not covered under this Subpart, the person filing may
include all export information in one report provided the
following information on exports of waste destined for recovery
within the designated OECD member countries is contained in a
separate Section). Such reports shall include the following
information:
1)
The USEPA identification number, name, and mailing and site
address of the notifier filing the report;
2)
The calendar year covered by the report;
3)
The name and site address of each final recovery facility;
4)
By final recovery facility, for each hazardous waste
exported, a description of the hazardous waste, the USEPA
hazardous waste number (from 35 Ill. Adm. Code 721.Subpart C
or 721.Subpart D), the designation of waste type(s) from the
OECD waste list and applicable waste code from the OECD
lists, DOT hazard class, the name and USEPA identification
number (where applicable) for each transporter used, the
total amount of hazardous waste shipped pursuant to this
Subpart, and number of shipments pursuant to each
notification;
5)
In even numbered years, for each hazardous waste exported,
except for hazardous waste produced by exporters of greater
than 100 kilograms (kg) but less than 1000 kg in a calendar
month, and except for hazardous waste for which information
was already provided pursuant to Section 722.141:
A)
A description of the efforts undertaken during the
year to reduce the volume and toxicity of waste
generated; and
B)
A description of the changes in volume and toxicity of
the waste actually achieved during the year in
comparison to previous years to the extent such
information is available for years prior to 1984; and
6)
A certification signed by the person acting as primary
exporter that states as follows:
"I certify under penalty of law that I have personally
examined and am familiar with the information submitted in
this and all attached documents, and that based on my
inquiry of those individuals immediately responsible for
obtaining the information, I believe that the submitted
information is true, accurate, and complete. I am aware that
there are significant penalties for submitting false
information including the possibility of fine and
imprisonment."
b)
Exception reports. Any person that meets the definition of
primary exporter in Section 722.151 shall file with USEPA and the
Agency an exception report in lieu of the requirements of Section
722.142 if any of the following occurs:
125
1)
The person has not received a copy of the tracking
documentation signed by the transporter stating point of
departure of the waste from the United States within 45 days
from the date it was accepted by the initial transporter;
2)
Within 90 days from the date the waste was accepted by the
initial transporter, the
notifier has not received written
confirmation from the recovery facility that the hazardous
waste was received; or
3)
The waste is returned to the United States.
c)
Recordkeeping.
1)
Persons that meet the definition of primary exporter in
Section 722.151 shall keep the following records:
A)
A copy of each notification of intent to export and
all written consents obtained from the competent
authorities of concerned countries, for a period of at
least three years from the date the hazardous waste
was accepted by the initial transporter;
B)
A copy of each annual report, for a period of at least
three years from the due date of the report; and
C)
A copy of any exception reports and a copy of each
confirmation of delivery (i.e., tracking
documentation) sent by the recovery facility to the
notifier, for at least three years from the date the
hazardous waste was accepted by the initial
transporter or received by the recovery facility,
whichever is applicable.
2)
The periods of retention referred to in this Section are
extended automatically during the course of any unresolved
enforcement action regarding the regulated activity or as
requested by USEPA or the Agency.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
Section 722.189
OECD Waste Lists
a)
General. For the purposes of this Subpart, a waste is considered
hazardous under U.S. national procedures, and hence subject to
this Subpart, if the waste:
1)
Meets the Federal definition of hazardous waste in 35 Ill.
Adm. Code 721.103; and
2)
Is subject to either the hazardous waste manifesting
requirements of 35 Ill. Adm. Code 722.Subpart B or the
universal waste management standards of 35 Ill. Adm. Code
733.
b)
If a waste is hazardous under subsection (a) above and it appears
on the amber or red list, it is subject to either the amber
- or
red-list requirements, as appropriate;
c)
If a waste is hazardous under subsection (a) above and it does not
126
appear on either amber or red lists, it is subject to the red
-list
requirements.
d)
The appropriate control procedures for hazardous wastes and
hazardous waste mixtures are addressed in Section 722.182.
e)
The OECD Green List of Wastes (revised May 1994), Amber List of
Wastes (revised May 1993), and Red List of Wastes (revised May
1993), as set forth in Appendix 3, Appendix 4 and Appendix 5,
respectively, to the OECD Council Decision C(92)39/FINAL
(Concerning the Control of Transfrontier Movements of Wastes
Destined for Recovery Operations), incorporated by reference in 35
Ill. Adm. Code 720.111.
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 723
STANDARDS APPLICABLE TO
TRANSPORTERS OF HAZARDOUS WASTE
SUBPART A: GENERAL
Section
723.110 Scope
723.111 USEPA Identification Number
723.112 Transfer Facility Requirements
SUBPART B: COMPLIANCE WITH THE MANIFEST SYSTEM
AND RECORDKEEPING
Section
723.120 The Manifest System
723.121 Compliance with the Manifest
723.122 Recordkeeping
SUBPART C: HAZARDOUS WASTE DISCHARGES
Section
723.130 Immediate Action
723.131 Discharge Clean Up
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81
-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
1982; amended and codified in R81
-22, 45 PCB 17, at 6 Ill. Reg. 4828,
effective May 17, 1982; amended in R84
-9, at 9 Ill. Reg. 11961, effective July
24, 1985; amended in R86
-19, at 10 Ill. Reg. 20718, effective December 2,
1986; amended in R86
-46 at 11 Ill. Reg. 13570, effective August 4, 1987;
amended in R87 -5 at 11 Ill. Reg. 19412, effective November 12, 1987; amended
in R95-6 at 19 Ill. Reg. 9945, effective June 27, 1995
; amended in R96-10/R97-
3/R97-5 at 21 Ill. Reg. ________, effective ____________________
.
SUBPART A: GENERAL
Section 723.110
Scope
127
a)
These regulations establish standards which apply to persons
transporting hazardous waste into, out of or through Illinois if
the transportation requires a manifest under
Part35 Ill. Adm. Code
722.
b)
These regulations do not apply to on
-site transportation of
hazardous waste by generators or by owners or operators of
permitted hazardous waste management facilities.
c)
A transporter of hazardous waste must also comply with
Part35 Ill.
Adm. Code 722, "Standards Applicable to Generators of Hazardous
Waste", if he:
1)
Transports hazardous waste into the United States from
abroad; or
2)
Mixes hazardous waste of different DOT shipping descriptions
by placing them into a single container.
BOARD NOTE: Transporters
whothat store hazardous waste are
required to comply with the storage standards in
Parts35
Ill. Adm. Code 724 and 725 and the permit requirements of 40
CFR Part 122.
d) Part 700 contains rules concerning application of other Board
regulations. A transporter of hazardous waste subject to the
manifesting requirements of 35 Ill. Adm. Code 722 or the waste
management standards of 35 Ill. Adm. Code 733 that is being
imported from or exported to any of the countries listed in 35
Ill. Adm. Code 722.158(a)(1) for purposes of recovery is subject
to this Subpart and to all other relevant requirements of 35 Ill.
Adm. Code 722.Subpart H, including, but not limited to, 35 Ill.
Adm. Code 722.184 for tracking documents.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART B: COMPLIANCE WITH THE MANIFEST SYSTEM
AND RECORDKEEPING
Section 723.120
The Manifest System
a)
No acceptance without a manifest.
1)
A transporter shall not accept hazardous waste from a
generator unless it is accompanied by a manifest signed in
accordance with the provisions of 35 Ill. Adm. Code 722
.120.
In the case of exports
other than those subject
subject to
35 Ill. Adm. Code 722.Subpart H
, a transporter shall not
accept such waste from a primary exporter or other person:
1
A)
If the transporter knows the shipment does not conform
with the USEPA Acknowledgement of Consent (as defined
in 35 Ill. Adm. Code 722.151); and
2
B)
Unless, in addition to a manifest signed in accordance
with 35 Ill. Adm. Code 722.120, the waste is also
accompanied by a USEPA Acknowledgement of Consent
which, except for shipment by rail, is attached to the
manifest (or shipping paper for exports by water (bulk
shipment)).
128
2)
For exports of hazardous waste subject to the requirements
of 35 Ill. Adm. Code 722.Subpart H, a transporter may not
accept hazardous waste without a tracking document that
includes all information required by 35 Ill. Adm. Code
722.184.
b)
Before transporting the hazardous waste, the transporter shall
sign and date the manifest acknowledging acceptance of the
hazardous waste from the generator. The transporter shall return
a signed copy to the generator before leaving the generator's
property.
c)
The transporter shall ensure that the manifest accompanies the
hazardous waste. In the case of exports, the transporter shall
ensure that a copy of the USEPA Acknowledgement of Consent also
accompanies the hazardous waste.
d)
A transporter whothat delivers a hazardous waste to another
transporter or to the designated facility shall:
1)
Obtain the date of delivery and the handwritten signature of
that transporter or of the owner or operator of the
designated facility on the manifest; and
2)
Retain one copy of the manifest in accordance with Section
723.122; and
3)
Give the remaining copies of the manifest to the accepting
transporter or designated facility.
e)
The requirements of subsections (c), (d) and (f) do not apply to
water (bulk shipment) transporters if:
1)
The hazardous waste is delivered by water (bulk shipment) to
the designated facility; and
2)
A shipping paper containing all the information required on
the manifest (excluding the USEPA identification numbers,
generator certification and signatures) accompanies the
hazardous waste and, for exports, a USEPA Acknowledgement of
Consent accompanies the hazardous waste; and
3)
The delivering transporter obtains the date of delivery and
handwritten signature of the owner or operator designated
facility on either the manifest or the shipping paper; and
4)
The person delivering the hazardous waste to the initial
water (bulk shipment) transporter obtains the date of
delivery and signature of the water (bulk shipment)
transporter on the manifest and forwards it to the
designated facility; and
5)
A copy of the shipping paper or manifest is retained by each
water (bulk shipment) transporter in accordance with Section
723.122.
f)
For shipments involving rail transportation, the requirements of
subsections (c), (d) and (e) do not apply and the following
requirements do apply:
129
1)
When accepting hazardous waste from a non-rail transporter,
the initial rail transporter shall:
A)
Sign and date the manifest acknowledging acceptance of
the hazardous waste;
B)
Return a signed copy of the manifest to the non-rail
transporter;
C)
Forward at least three copies of the manifest to:
i)
The next non-rail transporter, if any; or,
ii)
The designated facility, if the shipment is
delivered to that facility by rail; or
iii)
The last rail transporter designated to handle
the waste in the United States;
D)
Retain one copy of the manifest and rail shipping
paper in accordance with Section 723.122.
2)
Rail transporters shall ensure that a shipping paper
containing all the information required on the manifest
(excluding the USEPA identification numbers, generator
certification and signatures) and, for exports, a USEPA
Acknowledgement of Consent accompanies the hazardous waste
at all times.
(Board Note:Intermediate rail transporters are not required
to sign either the manifest or shipping paper.)
3)
When delivering hazardous waste to the designated facility,
a rail transporter shall:
A)
Obtain the date of delivery and handwritten signature
of the owner or operator of the designated facility on
the manifest or the shipping paper (if the manifest
has not been received by the facility); and
B)
Retain a copy of the manifest or signed shipping paper
in accordance with Section 723.122.
4)
When delivering hazardous waste to a non-rail transporter a
rail transporter shall:
A)
Obtain the date of delivery and the handwritten
signature of the next non-rail transporter on the
manifest; and
B)
Retain a copy of the manifest in accordance with
Section 723.122.
5)
Before accepting hazardous waste from a rail transporter, a
non-rail transporter shall sign and date the manifest and
provide a copy to the rail transporter.
g)
Transporters whothat transport hazardous waste out of the United
States shall:
1)
Indicate on the manifest the date the hazardous waste left
130
the United States; and
2)
Sign the manifest and retain one copy in accordance with
Section 723.122(c); and
3)
Return a signed copy of the manifest to the generator; and
4)
Give a copy of the manifest to a United States Customs
official at the point of departure from the United States.
h)
A transporter transporting hazardous waste from a generator
whothat generates greater than 100 kilograms but less than 1000
kilograms of hazardous waste in a calendar month need not comply
with the requirements of this Section or those of Section 723.122
provided that:
1)
The waste is being transported pursu
ant to a reclamation
agreement provided for in 35 Ill. Adm. Code 722.120(e);
2)
The transporter records, on a log or shipping paper, the
following information for each shipment:
A)
The name, address and USEPA Identification Number (35
Ill. Adm. Code 722.112) of the generator of the waste;
B)
The quantity of waste accepted;
C)
All shipping information required by the United States
Department of Transportation;
D)
The date the waste is accepted; and
3)
The transporter carries this record
when transporting waste
to the reclamation facility; and
4)
The transporter retains these records for a period of at
least three years after termination or expiration of the
agreement.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 724
STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS WASTE
TREATMENT, STORAGE,
AND DISPOSAL FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
724.101
Purpose, Scope and Applicability
724.103
Relationship to Interim Status Standards
SUBPART B: GENERAL FACILITY STANDARDS
Section
724.110
Applicability
724.111
Identification Number
724.112
Required Notices
131
724.113
General Waste Analysis
724.114
Security
724.115
General Inspection Requirements
724.116
Personnel Training
724.117
General Requirements for Ignitable, Reactive or Incompatible
Wastes
724.118
Location Standards
724.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
724.130
Applicability
724.131
Design and Operation of Facility
724.132
Required Equipment
724.133
Testing and Maintenance of Equipment
724.134
Access to Communications or Alarm System
724.135
Required Aisle Space
724.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
724.150
Applicability
724.151
Purpose and Implementation of Contingency Plan
724.152
Content of Contingenc
y Plan
724.153
Copies of Contingency Plan
724.154
Amendment of Contingency Plan
724.155
Emergency Coordinator
724.156
Emergency Procedures
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section
724.170
Applicability
724.171
Use of Manifest System
724.172
Manifest Discrepancies
724.173
Operating Record
724.174
Availability, Retention and Disposition of Records
724.175
Annual Report
724.176
Unmanifested Waste Report
724.177
Additional Reports
SUBPART F: RELEASES FROM SOLID WASTE MANAGEMENT UNIT
S
Section
724.190
Applicability
724.191
Required Programs
724.192
Groundwater Protection Standard
724.193
Hazardous Constituents
724.194
Concentration Limits
724.195
Point of Compliance
724.196
Compliance Period
724.197
General Groundwater Monitoring Requirements
724.198
Detection Monitoring Program
724.199
Compliance Monitoring Program
724.200
Corrective Action Program
724.201
Corrective Action for Solid Waste Management Units
SUBPART G: CLOSURE AND POST-CLOSURE
Section
724.210
Applicability
724.211
Closure Performance Standard
724.212
Closure Plan; Amendment of Plan
724.213
Closure; Time Allowed For Closure
132
724.214
Disposal or Decontamination of Equipment, Structures and Soils
724.215
Certification of Closure
724.216
Survey Plat
724.217
Post-closure Care and Use of Property
724.218
Post-closure Plan; Amendment of Plan
724.219
Post-closure Notices
724.220
Certification of Completion of Post-closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
724.240
Applicability
724.241
Definitions of Terms As Used
In This Subpart
724.242
Cost Estimate for Closure
724.243
Financial Assurance for Closure
724.244
Cost Estimate for Post-closure Care
724.245
Financial Assurance for Post-closure Care
724.246
Use of a Mechanism for Financial Assurance of Both Closure and
Post-closure Care
724.247
Liability Requirements
724.248
Incapacity of Owners or Operators, Guarantors or Financial
Institutions
724.251
Wording of the Instruments
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
724.270
Applicability
724.271
Conditi on of Containers
724.272
Compatibility of Waste With Container
724.273
Management of Containers
724.274
Inspections
724.275
Containment
724.276
Special Requirements for Ignitable or Reactive Waste
724.277
Special Requirements for Incompatible Wastes
724.278
Closure
724.279
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
724.290
Applicability
724.291
Assessment of Existing Tank System's Integrity
724.292
Design and Installation of New Tank Systems or Components
724.293
Containment and Detection of
Releases
724.294
General Operating Requirements
724.295
Inspections
724.296
Response to Leaks or Spills and Disposition of Leaking or unfit-
for-use Tank Systems
724.297
Closure and Post-Closure Care
724.298
Special Requirements for Ignitable or Reactive Waste
724.299
Special Requirements for Incompatible Wastes
724.300
Air Emission Standards
SUBPART K: SURFACE IMPOUNDMENTS
Section
724.320
Applicability
724.321
Design and Operating Requirements
724.322
Action Leakage Rate
724.323
Response Actions
724.326
Monitoring and Inspection
724.327
Emergency Repairs; Contingency Plans
724.328
Closure and Post-closure Care
724.329
Special Requirements for Ignitable or Reactive Waste
133
724.330
Special Requirements for Incompatible Wastes
724.331
Special Requirements for Hazardous Wastes F020, F021, F022, F023,
F026 and F027
724.332
Air Emission Standards
SUBPART L: WASTE PILES
Section
724.350
Applicability
724.351
Design and Operating Requirements
724.352
Action Leakage Rate
724.353
Response Action Plan
724.354
Monitor ing and Inspection
724.356
Special Requirements for Ignitable or Reactive Waste
724.357
Special Requirements for Incompatible Wastes
724.358
Closure and Post-closure Care
724.359
Special Requirements for Hazardous Wastes F020, F021, F022, F023,
F026 and F027
SUBPART M: LAND TREATMENT
Section
724.370
Applicability
724.371
Treatment Program
724.372
Treatment Demonstration
724.373
Design and Operating Requirements
724.376
Food-chain Crops
724.378
Unsaturated Zone Monitoring
724.379
Recordkeeping
724.380
Closure and Post-closure Care
724.381
Special Requirements for Ignitable or Reactive Waste
724.382
Special Requirements for Incompatible Wastes
724.383
Special Requirements for Hazardous Wastes F020, F021, F022, F023,
F026 and F027
SUBPART N: LANDFILLS
Section
724.400
Applicability
724.401
Design and Operating Requirements
724.402
Action Leakage Rate
724.403
Monitoring and Inspection
724.404
Response Actions
724.409
Surveying and Recordkeeping
724.410
Closure and Post-closure Care
724.412
Special Requiremen
ts for Ignitable or Reactive Waste
724.413
Special Requirements for Incompatible Wastes
724.414
Special Requirements for Bulk and Containerized Liquids
724.415
Special Requirements for Containers
724.416
Disposal of Small Containers of Hazardous Waste in
Overpacked
Drums (Lab Packs)
724.417
Special Requirements for Hazardous Wastes F020, F021, F022, F023,
F026 and F027
SUBPART O: INCINERATORS
Section
724.440
Applicability
724.441
Waste Analysis
724.442
Principal Organic Hazardous Constituents (POHCs)
724.443
Performance Standards
724.444
Hazardous Waste Incinerator Permits
724.445
Operating Requirements
724.447
Monitoring and Inspections
724.451
Closure
134
SUBPART S: CORRECTIVE ACTION FOR SOLID WASTE MANAGEMENT UNITS
Section
724.652
Corrective Action Management Units
724.653
Temporary Units
SUBPART W: DRIP PADS
Section
724.670
Applicability
724.671
Assessment of existing drip pad integrity
724.672
Design and installation of new drip pads
724.673
Design and operating requirements
724.674
Inspections
724.675
Closure
SUBPART X: MISCELLANEOUS UNITS
Section
724.700
Applicability
724.701
Environmental Performance Standards
724.702
Monitoring, Analysis, Inspection, Response, Reporting and
Corrective Action
724.703
Post-closure Care
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
724.930
Applicability
724.931
Definitions
724.932
Standards: Process Vents
724.933
Standards: Closed-vent Systems and Control Devices
724.934
Test methods and procedures
724.935
Recordkeeping requirements
724.936
Reporting Requirements
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section
724.950
Applicability
724.951
Definitions
724.952
Standards: Pumps in Light Liquid Service
724.953
Standards: Compressors
724.954
Standards: Pressure Relief Devices in Gas/Vapor Service
724.955
Standards: Sampling Connecting Systems
724.956
Standards: Open-ended Valves or Lines
724.957
Standards: Valves in Gas/Vapor or Light Liquid Service
724.958
Standards: Pumps, Valves, Pressure Relief Devices and Other
Connectors
724.959
Standards: Delay of Repair
724.960
Standards: Closed-vent Systems and Control Devices
724.961
Alternative Percentage Standard for Valves
724.962
Skip Period Alternative for Valves
724.963
Test Methods and Procedures
724.964
Recordkeeping Requirements
724.965
Reporting Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
SURFACE IMPOUNDMENTS, AND CONTAINERS
Section
724.980
Applicability
724.981
Definitions
724.982
Standards: General
724.983
Waste Determination Procedures
724.984
Standards: Tanks
135
724.985
Standards: Surface
Impoundments
724.986
Standards: Containers
724.987
Standards: Closed-vent Systems and Control Devices
724.988
Inspection and Monitoring Requirements
724.989
Recordkeeping Requirements
724.990
Reporting Requirements
724.991
Alternative Control Requirements for Tanks
SUBPART DD: CONTAINMENT BUILDINGS
Section
724.1100
Applicability
724.1101
Design and operating standards
724.1102
Closure and Post-closure Care
724.Appendix A
Recordkeeping Instructions
724.Appendix B
EPA Report Form and Instructions (Repealed)
724.Appendix D
Cochran's Approximation to the
Behrens-Fisher Student's T-
Test
724.Appendix E
Examples of Potentially Incompatible Waste
724.Appendix I
Groundwater Monitoring List
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R82-19, 53 PCB 131, at 7 Ill. Reg. 14059, effective
October 12, 1983; amended in R84-9 at 9 Ill. Reg. 11964, effective July 24,
1985; amended in R85-22 at 10 Ill. Reg. 1136, effective January 2, 1986;
amended in R86-1 at 10 Ill. Reg. 14119, effective August 12, 1986; amended in
R86-28 at 11 Ill. Reg. 6138, effective March 24, 1987; amended in R86-28 at 11
Ill. Reg. 8684, effective April 21, 1987; amended in R86-46 at 11 Ill. Reg.
13577, effective August 4, 1987; amended in R87-5 at 11 Ill. Reg. 19397,
effective November 12, 1987; amended in R87-39 at 12 Ill. Reg. 13135,
effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 458, effective
December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18527, effective November
13, 1989; amended in R90-2 at 14 Ill. Reg. 14511, effective August 22, 1990;
amended in R90-10 at 14 Ill. Reg. 16658, effective September 25, 1990; amended
in R90-11 at 15 Ill. Reg. 9654, effective June 17, 1991; amended in R91-1 at
15 Ill. Reg. 14572, effective October 1, 1991; amended in R91-13 at 16 Ill.
Reg. 9833, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg. 17702,
effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5806, effective
March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20830, effective November 22,
1993; amended in R93-16 at 18 Ill. Reg. 6973, effective April 26, 1994;
amended in R94-7 at 18 Ill. Reg. 12487, effective July 29, 1994; amended in
R94-17 at 18 Ill. Reg. 17601, effective November 23, 1994; amended in R95-6 at
19 Ill. Reg. 9951, effective June 27, 1995; amended in R95-20 at 20 Ill. Reg.
11244, August 1, 1996
; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________,
effective ____________________
.
SUBPART B: GENERAL FACILITY STANDARDS
Section 724.112
Required Notices
a)
Receipt from a foreign source.
1)
The owner or operator of a facility that has arranged to
receive hazardous waste from a foreign source must notify
the Regional Administrator in writing at least four weeks in
advance of the date the waste is expected to arrive at the
facility. Notice of subsequent shipments of the same waste
136
from the same foreign source is not required.
2)
The owner or operator of a recovery facility that has
arranged to receive hazardous waste subject to 35 Ill. Adm.
Code 722.Subpart H must provide a copy of the tracking
document bearing all required signatures to the
notifier, to
the Office of Enforcement and Compliance Assurance, Office
of Compliance, Enforcement Planning, Targeting and Data
Division (2222A), Environmental Protection Agency, 401 M
St., SW., Washington, DC 20460; to the Bureau of Land,
Division of Land Pollution Control, Illinois Environmental
Protection Agency,
P.O. Box 19276, Springfield, IL 62794-
9276; and to the competent authorities of all other
concerned countries within three working days of receipt of
the shipment. The original of the signed tracking document
must be maintained at the facility for at least three years.
b)
The owner or operator of a facility that receives hazardous waste
from an off -site source (except where the owner or operator is
also the generator) must inform the generator in writing that the
owner or operator has the appropriate permit(s) for, and will
accept, the waste the generator is shipping. The owner or
operator must keep a copy of this written notice as part of the
operating record.
c)
Before transferring ownership or operation of a facility during
its operating life, or of a disposal facility during the
post-closure care period, the owner or operator must notify the
new owner or operator in writing of the requirements of this Part
and 35 Ill. Adm. Code 702 and 703.
BOARD NOTE: An owner's or operator's failure to noti
fy the new
owner or operator of the requirements of this Part in no way
relieves the new owner or operator of his obligation to comply
with all applicable requirements.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.113
General Waste Analysis
a)
Analysis:
1)
Before an owner or operator treats, stores, or disposes of
any hazardous wastes, or non-hazardous wastes if applicable
under Section 724.213(d), the owner or operator shall obtain
a detailed chemical and physical analysis of a
representative sample of the wastes. At a minimum, the
analysis must contain all the information that must be known
to treat, store, or dispose of the waste in accordance with
this Part and 35 Ill. Adm. Code 728.
2)
The analysis may include data developed under 35 Ill. Adm.
Code 721 and existing published or documented data on the
hazardous waste or on hazardous waste generated from similar
processes.
BOARD NOTE: For example, the facility's records of analyses
performed on the waste before the effective date of these
regulations or studies conducted on hazardous waste
generated from processes similar to that which generated the
waste to be managed at the facility may be included in the
137
data base required to comply with subsection (a)(1) above.
The owner or operator of an off-site facility may arrange
for the generator of the hazardous waste to supply part or
all of the information required by subsection (a)(1) above,
except as otherwise specified in 35 Ill. Adm. Code
728.107(b) and (c). If the generator does not supply the
information, and the owner or operator chooses to accept a
hazardous waste, the owner or operator is responsible for
obtaining the information required to comply with this
Section.
3)
The analysis must be repeated as necessary to ensure that it
is accurate and up to date. At a minimum, the analysis must
be repeated:
A)
When the owner or operator is notified, or has reason
to believe, that the process or operation generating
the hazardous waste, or non-hazardous waste if
applicable under Section 724.213(d), has changed; and
B)
For off-site facilities, when the results of the
inspection required in subsection (a)(4) below
indicate that the hazardous waste received at the
facility does not match the waste designated on the
accompanying manifest or shipping paper.
4)
The owner or operator of an off-site facility shall inspect
and, if necessary, analyze each hazardous waste shipment
received at the facility to determine whether it matches the
identity of the waste specified on the accompanying manifest
or shipping paper.
b)
The owner or operator shall develop and follow a written waste
analysis plan that describes the procedures that it will carry out
to comply with subsection (a) above. The owner or operator shall
keep this plan at the facility. At a minimum, the plan must
specify:
1)
The parameters for which each hazardous waste, or non-
hazardous waste if applicable under Section 724.213(d), will
be analyzed and the rationale for the selection of these
parameters (i.e., how analysis for these parameters will
provide sufficient information on the waste's properties to
comply with subsection (a) above).
2)
The test methods that will be used to test for these
parameters.
3)
The sampling method that will be used to obtain a
representative sample of the waste to be analyzed. A
representative sample may be obtained using either:
A)
One of the sampling methods described in 35 Ill. Adm.
Code 721.Appendix A; or
B)
An equivalent sampling met
hod.
BOARD NOTE: See 35 Ill. Adm. Code 720.121.
4)
The frequency with which the initial analysis of the waste
will be reviewed or repeated to ensure that the analysis is
138
accurate and up to date.
5)
For off-site facilities, the waste analyses that hazardous
waste generators have agreed to supply.
6)
Where applicable, the methods that will be used to meet the
additional waste analysis requirements for specific waste
management methods as specified in Sections 724.117,
724.414, 724.441, 724.934(d), 724.963(d), and 724.983 and 35
Ill. Adm. Code 728.107.
7)
For surface impoundments exempted from land disposal
restrictions under 35 Ill. Adm. Code 728.104(a), the
procedures and schedules for:
A)
The sampling of impoundment contents;
B)
The analysis of test data; and
C)
The annual removal of residues that are not
delisted
under 35 Ill. Adm. Code 720.122 or which exhibit a
characteristic of hazardous waste and either:
i)
Do not meet applicable treatment standards of 35
Ill. Adm. Code 728.Subpart D; or
ii)
Where no treatment standards have been
established, such residues are prohibited from
land disposal under 35 Ill. Adm. Code 728.132 or
728.139 or such residues are prohibited from
land disposal under 35 Ill. Adm. Code
728.133(f).
8)
For owners and operators seeking an exemption to the air
emission standards of 724.Subpart CC in accordance with
Section 724.982:
A) TIf direct measurement is used for the waste
determination, t he procedures and schedules for waste
sampling and analysis and the analysis of test data to
verify the exemption
, and.
B) Each generator's notice and certification of the
volatile organic concentration in the waste if the
waste is received from off
siteIf knowledge of the
waste is used for the waste determination, any
information prepared by the facility owner or operator
or by the generator of the waste, if the waste is
received form off-site, that is used as the basis for
knowledge of the waste
.
c)
For off-site facilities, the waste analysis plan r
equired in
subsection (b) above must also specify the procedures that will be
used to inspect and, if necessary, analyze each shipment of
hazardous waste received at the facility to ensure that it matches
the identity of the waste designated on the accompanying manifest
or shipping paper. At a minimum, the plan must describe:
1)
The procedures that will be used to determine the identity
of each movement of waste managed at the facility;
139
2)
The sampling method that will be used to obtain a
representative sample of the waste to be identified, if the
identification method includes sampling; and
3)
The procedures that the owner or operator of an off-site
landfill receiving containerized hazardous waste will use to
determine whether a hazardous waste generator or
treater has
added a biodegradable
sorbent to the waste in the container.
BOARD NOTE: 35 Ill. Adm. Code 703 requires that the waste
analysis plan be submitted with Part B of the permit
application.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 724.171
Use of Manifest System
a)
If a facility receives hazardous waste accompanied by a manifest,
the owner or operator, or the owner or operator's agent, must:
1)
Sign and date each copy of the manifest to certify that the
hazardous waste covered by the manifest was received;
2)
Note any significant discrepancies in the manifest (as
defined in Section 724.172(a)) on each copy of the manifest;
BOARD NOTE: The Board does not intend that the owner or
operator of a facility whose procedures under Section
724.113(c) include waste analysis must perform that analysis
before signing the manifest and giving it to the
transporter. Section 724.172(b), however, requires
reporting an unreconciled discrepancy discovered during
later analysis.
3)
Immediately give the transporter at least one copy of the
signed manifest;
4)
Within 30 days after the delivery, send a copy of the
manifest to the generator and to the Agency; and
5)
Retain at the facility a copy of each manifest for at least
three years from the date of delivery.
b)
If a facility receives, from a rail or water (bulk shipment)
transporter, hazardous waste which is accompanied by a shipping
paper containing all the information required on the manifest
(excluding the EPA identification numbers, generator's
certification, and signatures), the owner or operator, or the
owner or operator's agent, must:
1)
Sign and date each copy of the ma
nifest or shipping paper
(if the manifest has not been received) to certify that the
hazardous waste covered by the manifest or shipping paper
was received;
2)
Note any significant discrepancies (as defined in Section
724.172(a)) in the manifest or shipping paper (if the
manifest has not been received) on each copy of the manifest
140
or shipping paper.
BOARD NOTE: The Board does not intend that the owner or
operator of a facility whose procedures under Section
724.113(c) include waste analysis must perform that analysis
before signing the shipping paper and giving it to the
transporter. Section 724.172(b), however, requires reporting
an unreconciled discrepancy discovered during later
analysis.
3)
Immediately give the rail or water (bulk shipment)
transporter at least one copy of the manifest or shipping
paper (if the manifest has not been received);
4)
Within 30 days after the delivery, send a copy of the signed
and dated manifest to the generator and to the Agency;
however, if the manifest has not been received within 30
days after delivery, the owner or operator, or the owner or
operator's agent, must send a copy of the shipping paper
signed and dated to the generator; and
BOARD NOTE: Section 722.123(c) requires the generator to
send three copies of the manifest to the facility when
hazardous waste is sent by rail or water (bulk shipment).
5)
Retain at the facility a copy of the manifest and shipping
paper (if signed in lieu of the manifest at the time of
delivery) for at least three years from the date of
delivery.
c)
Whenever a shipment of hazardous waste is initiated from a
facility, the owner or operator of that facility must comply with
the requirements of 35 Ill. Adm. Code 722.
BOARD NOTE: The provisions of 35 Ill. Adm. Code 722.134 are
applicable to the on
-site accumulation of hazardous wastes by
generators. Therefore, the provisions of Section 722.134 only
apply to owners or operators
whothat are shipping hazardous waste
which they generated at that facility.
d)
Within three working days of the receipt of a shipment subject to
35 Ill. Adm. Code 722.Subpart H, the owner or operator of the
facility must provide a copy of the tracking document bearing all
required signatures to the
notifier; to the Office of Enforcement
and Compliance Assurance, Office of Compliance, Enforcement
Planning, Targeting and Data Division (2222A), Environmental
Protection Agency, 401 M St., SW., Washington, DC 20460; to the
Bureau of Land, Division of Land Pollution Control, Illinois
Environmental Protection Agency,
P.O. Box 19276, Springfield, IL
62794-9276; and to competent authorities of all other concerned
countries. The original copy of the tracking document must be
maintained at the facility for at least three years from the date
of signature.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section 724.279
Air Emission Standards
141
The owner or operator shall manage all hazardous waste placed in a container
in accordance with the requirements of 724.Subpart
s AA, BB, and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART J: TANK SYSTEMS
Section 724.300
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a tank in
accordance with the requirements of 724.Subpart
s AA, BB, and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART K: SURFACE IMPOUNDMENTS
Section 724.332
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a surface
impoundment in accordance with the requirements of 724.Subpart
s BB and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART N: LANDFILLS
Section 724.414
Special Requirements for Bulk and Containerized Liquids
a)
This subsection corresponds with 40 CFR 264.314(a), which pertains
to pre May 8, 1985 actions, a date long since passed. This
statement maintains structural consistency with U
.S. EPA rules.
b)
The placement of bulk or non
-containerized liquid hazardous waste
or hazardous waste containing free liquids (whether or not
sorbents have been added) in any landfill is prohibited.
c)
To demonstrate the absence or presence of free liquids in either a
containerized or a bulk waste, the following test must be used:
Method 9095 (Paint Filter Liquids Test) as described in "Test
Methods for Evaluating Solid Wastes, Physical/Chemical Methods",
U.S. EPA Publication No. SW
-846, incorporated by reference in 35
Ill. Adm. Code 720.111.
d)
Containers holding free liquids must not be placed in a landfill
unless;
1)
All free -standing liquid:
A)
has been removed by decanting or other methods;
B)
has been mixed with
sorbent or solidified so that
free-standing liquid is no longer observed; or
C)
has been otherwise eliminated; or
2)
The container is very small, such as an
ampule; or
3)
The container is designed to hold free liquids for use other
than storage, such as a battery or capacitor; or
142
4)
The container is a lab pack as defined in Section 724.416
and is disposed of in accordance with Section 724.416.
e)
Sorbents used to treat free liquids to be disposed of in landfills
must be nonbiodegradable.
Nonbiodegradable
sorbents are:
materials listed or described in subsection (e)(1) below;
materials that pass one of the tests in subsection (e)(2) below;
or materials that are determined by the Board to be
nonbiodegradable through the 35 Ill. Adm. Code 106 adjusted
standard process.
1)
Nonbiodegradable
sorbents are:
A)
Inorganic minerals, other inorganic materials, and
elemental carbon (e.g.,
aluminosilicates, clays,
smectites, Fuller's earth,
bentonite, calcium
bentonite, montmorillonite,
calcined montmorillonite,
kaolinite, micas (
illite), vermiculites, zeolites;
calcium carbonate (organic free limestone);
oxides/hydroxides,
alumina, lime, silica (sand),
diatomaceous earth;
perlite (volcanic glass); expanded
volcanic rock; volcanic ash; cement kiln dust; fly
ash; rice hull ash; activated charcoal (activated
carbon)); or
B)
High molecular weight synthetic polymers (e.g.,
polyethylene, high density polyethylene (HDPE),
polypropylene, polystrene, poly urethane, polycrylate,
polynorborene, polyisobutylene, ground synthetic
rubber, cross-linked
allylstrene and tertiary butyl
copolymers). This does not include polymers derived
from biological material or polymers specifically
designed to be degradable; or
C)
Mixtures of these
nonbiodegradable materials.
2)
Tests for nonbiodegradable
sorbents:
A)
The sorbent material is determined to be
nonbiodegradable under ASTM Method G21-70 (1984a)
--
"Standard Practice for Determining Resistance of
Synthetic Polymer Materials to Fungi", incorporated by
reference in 35 Ill. Adm. Code 720.111;
or
B)
The sorbent material is determined to be
nonbiodegradable under ASTM Method G22-76 (1984b)
--
"Standard Practice for Determining Resistance of
Plastics to Bacteria", incorporated by reference in 35
Ill. Adm. Code 720.111
.; or
C)
The sorbent material is determined to be non-
biodegradable under OECD test 301B [CO
2
Evolution
(Modified Sturm Test)], incorporated by reference in
35 Ill. Adm. Code 720.111.
f)
The placement of any liquid that is not a hazardous waste in a
landfill is prohibited (35 Ill. Adm. Code 729.311).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
143
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 724.930
Applicability
a)
This Subpart applies to owners and operators of facilities that
treat, store or dispose of hazardous wastes (except as provided in
Section 724.101).
b)
Except for Sections 724.934(d) and (e), this Subpart applies to
process vents associated with distillation, fractionation, thin-
film evaporation, solvent extraction, or air or steam stripping
operations that manage hazardous wastes with organic
concentrations of at least 10
ppmw (parts per million by weight),
if these operations are conducted in:
1)
Units that are subject to the permitting requirements of 35
Ill. Adm. Code 703;
or
2)
A unit (including a
hHazardous waste recycling unit
s) that
areis not exempt from permitting under the provisions of 35
Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
unit that is not a 90
-day tank or container) and that is
located onat a hazardous waste management
facilit iesy
otherwise subject to the permitting requirements of 35 Ill.
Adm. Code 703 .; or
3)
A unit that is exempt from permitting under the provisions
of 35 Ill. Adm. Code 722.134(a) (i.e., a 90
-day tank or
container).
c)
If the owner or operator of process vents subject to the
requirements of Sections 724.932 through 724.936 has received a
RCRA permit prior to December 21, 1990, the requirements of
Sections 724.932 through 724.936 must be incorporated when the
permit is reissued under 35 Ill. Adm. Code 705.201 or reviewed
under 35 Ill. Adm. Code 702.161.
BOARD NOTE: The requirements of Sections 724.932 through 724.936
apply to process vents on hazardous waste recycling units
previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
exemptions under 35 Ill. Adm. Code 721.104, 722.134 and 724.101(g)
are not affected by these requirements.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.933
Standards: Closed-vent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control
devices used to comply with provisions of this Part shall
comply with the provisions of this Section.
2)
The owner or operator of an exist
ing facility that cannot
install a closed-vent system and control device to comply
with the provisions of this Subpart on the effective date
that the facility becomes subject to the provisions of this
Subpart shall prepare an implementation schedule that
includes dates by which the closed-vent system and control
device will be installed and in operation. The controls
144
must be installed as soon as possible, but the
implementation schedule may allow up to
1830 months after
the effective date that the facility becomes subject to this
Subpart for installation and startup. All units that begin
operation after December 21, 1990, must comply with the
rules immediately (i.e., must have control devices installed
and operating on startup of the affected unit); the 2-year
implementation schedule does not apply to these units.
b)
A control device involving vapor recovery (e.g., a condenser or
adsorber) must be designed and operated to recover the organic
vapors vented to it with an efficiency of 95 weight percent or
greater unless the total organic emission limits of Section
724.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler,
or process heater) must be designed and operated to reduce the
organic emissions vented to it by 95 weight percent or greater; to
achieve a total organic compound concentration of 20
ppmv,
expressed as the sum of the actual compounds and not in carbon
equivalents, on a dry basis, corrected to 3 percent oxygen; or to
provide a minimum residence time of 0.50 seconds at a minimum
temperature of 760
ยฐ
C. If a boiler or process heater is used as
the control device, then the vent stream must be introduced into
the flame zone of the boiler or process heater.
d)
Flares:
1)
A flare must be designed for and operated with no visible
emissions, as determined by the methods specified in
subsection (e)(1), except for periods not to exceed a total
of 5 minutes during any 2 consecutive hours.
2)
A flare must be operated with a flame present at all times,
as determined by the methods specified in subsection
(f)(2)(C) below.
3)
A flare must be used only if the net heating value of the
gas being combusted is 11.2 MJ/
scm (300 Btu/ scf) or greater
and the flare is steam-assisted or air-assisted or if the
net heating value of the gas being combusted is 7.45 MJ/
scm
(200 Btu/ scf) or greater and the flare is
nonassisted. The
net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2)
below.
4)
Exit Velocity.
A)
A steam-assisted or
nonassisted flare must be designed
for and operated with an exit velocity, as determined
by the methods specified in subsection (e)(3) below,
less than 18.3 m/s (60 ft/s), except as provided in
subsections (d)(4)(B) and (d)(4)(C) below.
B)
A steam-assisted or
nonassisted flare designed for and
operated with an exit velocity, as determined by the
methods specified in subsection (e)(3) below, equal to
or greater than 18.3 m/s (60 ft/s) but less than 122
m/s (400 ft/s) is allowed if the net heating value of
the gas being combusted is greater than 37.3 MJ/
scm
145
(1000 Btu/ scf).
C)
A steam-assisted or
nonassisted flare designed for and
operated with an exit velocity, as determined by the
methods specified in subsection (e)(3) below, less
than the velocity, V, as determined by the method
specified in subsection (e)(4) below and less than 122
m/s (400 ft/s) is allowed.
5)
An air-assisted flare must be designed and op
erated with an
exit velocity less than the velocity, V, as determined by
the method specified in subsection (e)(5) below.
6)
A flare used to comply with this Section must be steam-
assisted, air-assisted, or
nonassisted.
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference
in 35 Ill. Adm. Code 720.111, must be used to determine the
compliance of a flare with the visible emission provisions
of this Subpart. The observation period is 2 hours and must
be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare
must be calculated using the following equation:
Where:
H
T
is the net heating value of the sample in MJ/
scm;
where the net enthalpy per mole of
offgas is based on
combustion at 25
ยฐ
C and 760 mm Hg, but the standard
temperature for determining the volume
corrersponding
to 1 mole is 20
ยฐ
C.
K = 1.74 E -7 (1/ppm)(g
mol/scm)(MJ/kcal) where
standard temperature for (g
mol/scm) 20
ยฐ
C.
ฮฃ
(Xi) means the sum of the values of X for each
component i, from i=1 to n.
C
i
is the concentration of sample component i in
ppm
on a wet basis, as measured for
organics by Reference
Method 18 in 40 CFR 60, and for carbon monoxide, by
ASTM D 1946-90, incorporated by reference in 35 Ill.
Adm. Code 720.111.
H
i
is the net heat of combustion of sample component
i, kcal/ gmol at 25
ยฐ
C and 760 mm Hg. The heats of
combustion must be determined using ASTM D 2382,
incorporated by reference in 35 Ill. Adm. Code
720.111, if published values are not available or
cannot be calculated.
T
i=1
n
i
i
H
= K
C
H
ร
ร
โ
146
3)
The actual exit velocity of a flare must be determined by
dividing the volumetric flow rate (in units of standard
temperature and pressure), as determined by Reference
Methods 2, 2A, 2C, or 2D in 40 CFR 60, incorporated by
reference in 35 Ill. Adm. Code 720.111, as appropriate, by
the unobstructed (free) cross-sectional area of the flare
tip.
4)
The maximum allowed velocity in m/s
, V for a flare complying
with subsection (d)(4)(C) must be determined by the
following equation:
Where:
log
10
means logarithm to the base 10
H
T
is the net heating value as determined in
subsection (e)(2).
5)
The maximum allowed velocity in m/s, V for an air-assisted
flare must be determined by the following equation:
Where:
H
T
is the net heating value as determined in
subsection (e)(2) below.
f)
The owner or operator shall mo
nitor and inspect each control
device required to comply with this Section to ensure proper
operation and maintenance of the control device by implementing
the following requirements:
1)
Install, calibrate, maintain, and operate according to the
manufacturer's specifications a flow indicator that provides
a record of stream flow from each affected process vent to
the control device at least once every hour. The flow
indicator sensor must be installed in the vent stream at the
nearest feasible point to the control device inlet but
before the point at which the vent streams are combined.
2)
Install, calibrate, maintain, and operate according to the
manufacturer's specifications a device to continuously
monitor control device operation as specified below:
A)
For a thermal vapor incinerator, a temperature
monitoring device equipped with a continuous recorder.
The device must have accuracy of ยฑ1 percent of the
temperature being monitored in
ยฐ
C or ยฑ0.5
ยฐ
C,
whichever is greater. The temperature sensor must be
installed at a location in the combustion chamber
downstream of the combustion zone.
10
T
V
=
H
+ 28.8
31.7
log
max
147
B)
For a catalytic vapor incinerator, a temperature
monitoring device equipped with a continuous recorder.
The device must be capable of monitoring temperature
at two locations and have an accuracy of ยฑ1 percent of
the temperature being monitored in
ยฐ
C or ยฑ0.5
ยฐ
C,
whichever is greater. One temperature sensor must be
installed in the vent stream at the nearest feasible
point to the catalyst bed inlet and a second
temperature sensor must be installed in the vent
stream at the nearest feasible point to the catalyst
bed outlet.
C)
For a flare, a heat sensing monitoring device equipped
with a continuous recorder that indicates the
continuous ignition of the pilot flame.
D)
For a boiler or process heater having a design heat
input capacity less than 44 MW, a temperature
monitoring device equipped with a continuous recorder.
The device must have an accuracy of ยฑ1 percent of the
temperature being monitored in
ยฐ
C or ยฑ0.5
ยฐ
C,
whichever is greater. The temperature sensor must be
installed at a location in the furnace downstream of
the combustion zone.
E)
For a boiler or process heater having a design heat
input capacity greater than or equal to 44 MW, a
monitoring device equipped with a continuous recorder
to measure parameters that indicate good combustion
operating practices are being used.
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous
recorder to measure the concentration level of
the organic compounds in the exhaust vent stream
from the condenser; or
ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable
of monitoring temperature
at two locations and
havewith an accuracy of ยฑ1 percent of the
temperature being monitored in
ยฐ
C or ยฑ0.5
ยฐ
C,
whichever is greater.
OneThe temperature sensor
must be installed at a location in the exhaust
vent stream from the condenser
, and a second
temperature sensor must be installed at a
location in the coolant fluid
exiting the
condenser (i.e., product side)
.
G)
For a carbon adsorption system that regenerates the
carbon bed directly in the control device such as a
fixed-bed carbon
adsorber, either:
i)
A monitoring device equipped with a continuous
recorder to measure the concentration level of
the organic compounds in the exhaust vent stream
from the carbon bed, or
ii)
A monitoring device equipped with a continuous
148
recorder to measure a parameter that indicates
the carbon bed is regenerated on a regular,
predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsection (f)(1) and (f)(2) at least once each operating
day to check control device operation and, if necessary,
immediately implement the corrective measures necessary to
ensure the control device operates in compliance with the
requirements of this Section.
g)
An owner or operator using a carbon adsorption system such as a
fixed-bed carbon
adsorber that regenerates the carbon bed directly
onsite in the control device shall replace the existing carbon in
the control device with fresh carbon at a regular, predetermined
time interval that is no longer than the carbon service life
established as a requirement of Section 724.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system such as a
carbon canister that does not regenerate the carbon bed directly
onsite in the control device shall replace the existing carbon in
the control device with fresh carbon on a regular basis by using
one of the following procedures:
1)
Monitor the concentration level of the organic compounds in
the exhaust vent stream from the carbon adsorption system on
a regular schedule, and replace the existing carbon with
fresh carbon immediately when carbon breakthrough is
indicated. The monitoring frequency must be daily or at an
interval no greater than 20 percent of the time required to
consume the total carbon working capacity established as a
requirement of Section 724.935(b)(4)(C)(vii), whichever is
longer.
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design
carbon replacement interval established as a requirement of
Section 724.935(b)(4)(C)(vii).
i)
An alternative operational or process parameter may be monitored
if the operator demonstrates that the parameter will ensure that
the control device is operated in conformance with these standards
and the control device's design specifications.
j)
An owner or operator o
f an affected facility seeking to comply
with the provisions of this Part by using a control device other
than a thermal vapor incinerator, catalytic vapor incinerator,
flare, boiler, process heater, condenser, or carbon adsorption
system is required to develop documentation including sufficient
information to describe the control device operation and identify
the process parameter or parameters that indicate proper operation
and maintenance of the control device.
k) Closed vent systems. A closed vent system must meet either of the
following design requirements:
1) CA closed-vent system
s must be designed
for andto operate d
with no detectable emissions, as indicated by an instrument
reading of less than 500
ppmv above background
and by visual
inspections , as determined by the methods specified at
Section 724.934(b)
., and by visual inspections; or
149
2) Closed-vent systems must be monitored to determine
compliance with this Section during the initial leak
detection monitoring, which must be conducted by the date
that the facility becomes subject to the provisions of this
Section annually, and at other times as specified in the
RCRA permit. For the annual leak detection monitoring after
the initial leak detection monitoring, the owner or operator
is not required to monitor those closed-vent system
components that operate in vacuum service or those closed-
vent system joints, seams, or other connections that are
permanently or semi-permanently sealed (e.g., a welded joint
between two sections of metal pipe or a bolted and
gasketed
pipe flange). A closed -vent system must be designed to
operate at a pressure below atmospheric pressure. The
system must be equipped with at least one pressure gauge or
other pressure measurement device that can be read from a
readily accessible location to verify that negative pressure
is being maintained in the closed
-vent system when the
control device is operating.
3) Detectable emissions, as indicated by an instrument reading
greater than 500
ppm and visual inspections, must be
controlled as soon as practicable, but not later than 15
calendar days after the emission is detected.
4) A first attempt at repair must be made no later than 5
calendar days after the emission is detected..
l)
The owner or operator shall monitor and inspect each closed-vent
system required to comply with this Section to ensure proper
operation and maintenance of the closed
-vent system by
implementing the following requirements:
1)
Each closed -vent system that is used to comply with
subsection (k)(1) above shall be inspected and monitored in
accordance with the following requirements:
A)
An initial leak detection monitoring of the
closed -vent system shall be conducted by the owner or
operator on or before the date that the system becomes
subject to this Section. The owner or operator shall
monitor the closed
-vent system components and
connections using the procedures specified in Section
724.934(b) to demonstrate that the closed
-vent system
operates with no detectable emissions, as indicated by
an instrument reading of less than 500
ppmv above
background.
B)
After initial leak detection monitoring required in
subsection (l)(1)(A) above, the owner or operator
shall inspect and monitor the closed
-vent system as
follows:
i)
Closed -vent system joints, seams, or other
connections that are permanently or
semi-permanently sealed (e.g., a welded joint
between two sections of hard piping or a bolted
and gasketed ducting flange) must be visually
inspected at least once per year to check for
defects that could result in air pollutant
150
emissions. The owner or operator shall monitor
a component or connection using the procedures
specified in Section 724.934(b) to demonstrate
that it operates with no detectable emissions
following any time the component is repaired or
replaced (e.g., a Section of damaged hard piping
is replaced with new hard piping) or the
connection is unsealed (e.g., a flange is
unbolted).
ii)
Closed -vent system components or connections
other than those specified in subsection
(l)(1)(B)(i) above must be monitored annually
and at other times as requested by the Regional
Administrator, except as provided for in
subsection (o) below, using the procedures
specified in Section 724.934(b) to demonstrate
that the components or connections operate with
no detectable emissions.
C)
In the event that a defect or leak is detected, the
owner or operator shall repair the defect or leak in
accordance with the requirements of subsection (l)(3)
below.
D)
The owner or operator shall maintain a record of the
inspection and monitoring in accordance with the
requirements specified in Section 724.935.
2)
Each closed -vent system that is used to comply with
subsection (k)(2) above must be inspected and monitored in
accordance with the following requirements:
A)
The closed -vent system must be visually inspected by
the owner or operator to check for defects that could
result in air pollutant emissions. Defects include,
but are not limited to, visible cracks, holes, or gaps
in ductwork or piping or loose connections.
B)
The owner or operator shall perform an initial
inspection of the closed
-vent system on or before the
date that the system becomes subject to this Section.
Thereafter, the owner or operator shall perform the
inspections at least once every year.
C)
In the event that a defect or leak is detected, the
owner or operator shall repair the defect in
accordance with the requirements of subsection (l)(3)
below.
D)
The owner or operator shall maintain a record of the
inspection and monitoring in accordance with the
requirements specified in Section 724.935.
3)
The owner or operator shall repair all detected defects as
follows:
A)
Detectable emissions, as indicated by visual
inspection or by an instrument reading greater than
500 ppmv above background, must be controlled as soon
as practicable, but not later than 15 calendar days
151
after the emission is detected, except as provided for
in subsection (l)(3)(C) below.
B)
A first attempt at repair must be made no later than
five calendar days after the emission is detected.
C)
Delay of repair of a closed
-vent system for which
leaks have been detected is allowed if the repair is
technically infeasible without a process unit
shutdown, or if the owner or operator determines that
emissions resulting from immediate repair would be
greater than the fugitive emissions likely to result
from delay of repair. Repair of such equipment must
be completed by the end of the next process unit
shutdown.
D)
The owner or operator shall maintain a record of the
defect repair in accordance with the requirements
specified in Section 724.935.
lm) CA closed-vent system
s andor control device s used to comply with
provisions of this Subpart must be operated at all times when
emissions may be vented to
themit.
mn)
The owner or operator using a carbon adsorption system
to control
air pollutant emissions
shall document that all carbon removed
that is a hazardous waste and that is removed
from a carbon
adsorption system to comply with subsections (g) and (h)
abovethe
control device is managed in one of the following manners
,
regardless of the volatile organic concentration of the carbon
:
1)
It is regenerated or reactivated in a thermal treatment unit
that is permitted under 724.Subpart
X,meets one of the
following:
A)
The owner or operator of the unit has been issued a
final permit under 35 Ill. Adm. Code 702, 703, and 705
that implements the requirements of 724.Subpart X; or
B)
The unit is equipped with and operating air emission
controls in accordance with the applicable
requirements of 724.Subparts AA and CC or 35 Ill. Adm.
Code 725.Subparts AA and CC; or
C)
The unit is equipped with and operating air emission
controls in accordance with a national emission
standard for hazardous air pollutants under 40 CFR 61
or 40 CFR 63.
2)
It is incinerated
by a process that is permitted under
724.Subpart O, orin a hazardous waste incinerator for which
the owner or operator has done either of the following:
A)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 724.Subpart O, or
B)
The owner or operator has certified compliance in
accordance with the interim status requirements of 35
Ill. Adm. Code 725.Subpart O.
152
3)
It is burned in a boiler or industrial furnace
that is
permitted under 724.Subpart
H.for which the owner or
operator has done either of the following:
A)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
726.Subpart H, or
B)
The owner or operator has designed and operates the
boiler or industrial furnace in accordance with the
interim status requirements of 35 Ill. Adm. Code
726.Subpart H.
o)
Any components of a closed
-vent system that are designated, as
described in Section 724.935(c)(9), as unsafe to monitor are
exempt from the requirements of subsection (l)(1)(B)(ii) above if
both of the following conditions are fulfilled:
1)
The owner or operator of the closed
-vent system has
determined that the components of the closed
-vent system are
unsafe to monitor because monitoring personnel would be
exposed to an immediate danger as a consequence of complying
with subsection (l)(1)(B)(ii) above; and
2)
The owner or operator of the closed
-vent system adheres to a
written plan that requires monitoring the closed
-vent system
components using the procedure specified in subsection
(l)(1)(B)(ii) as frequently as practicable during
safe-to-monitor times.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.934
Test methods and procedures
a)
Each owner or operator subject to the provisions of this Subpart
shall comply with the test methods and procedures requirements
provided in this Section
b)
When a closed-vent system is tested for compliance with no
detectable emissions, as required in Section 724.933(
kl), the test
must comply with the following requirements:
1)
Monitoring must comply with Reference Metho
d 21 in 40 CFR
60, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The detection instrument must meet the performance criteria
of Reference Method 21.
3)
The instrument must be calibrated before use on each day of
its use by the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10
ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a
concentration of approximately, but less than, 10,000
ppm methane or n-hexane.
5)
The background level must be determined as set forth in
153
Reference Method 21.
6)
The instrument probe must be traversed around all potential
leak interfaces as close to the interface as possible as
described in Reference Method 21.
7)
The arithmetic difference between the maximum concentration
indicated by the instrument and the background level is
compared with 500
ppm for determining compliance.
c)
Performance tests to determine compliance with Section 724.932(a)
and with the total organic compound concentration limit of Section
724.933(c) must comply with the following:
1)
Performance tests to determine total organic compound
concentrations and mass flow rates entering and exiting
control devices must be conducted and data reduced in
accordance with the following reference methods and
calculation procedures:
A)
Method 2 in 40 CFR 60 for velocity and volumetric flow
rate.
B)
Method 18 in 40 CFR 60 for organic content.
C)
Each performance test must consist of three separate
runs, each run conducted for at least 1 hour under the
conditions that exist when the hazardous waste
management unit is operating at the highest load or
capacity level reasonably expected to occur. For the
purpose of determining total organic compound
concentrations and mass flow rates, the average of
results of all runs applies. The average must be
computed on a time-weighed basis.
D)
Total organic mass flow rates must be determined by
the following equation:
F = K * Q * SUM( Ci * MWi)
Where:
F is the total organic mass flow rate, kg/h.
K = 4.16 E -8, conversion factor for molar
volume, kg- mol/cubic m, at 293 K and 760 mm Hg.
Q = volumetric flow rate of gases entering or
exiting control device,
dscm/h, as determined by
Method 2 in 40 CFR 60, incorporated by reference
in 35 Ill. Adm. Code 720.111.
SUM(Xi) means the sum of the values of X for
each component i, from i=1 to n.
n = number of organic compounds in the vent gas.
Ci is the organic concentration in
ppm, dry
basis, of compound i in the vent gas, as
determined by Method 18 in 40 CFR 60.
154
MWi is the molecular weight of organic compound
i in the vent gas, kg/kg-
mol.
Where:
E
h
= The total organic mass flow rate, kg/h.
Q
2sd
= The volumetric flow rate of gases entering
or exiting control device,
dscm/h, as
determined by Method 2 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm.
Code 720.111.
n = The number of organic compounds in the vent
gas.
C
i
= The organic concentration in
ppm, dry
basis, of compound i in the vent gas, as
determined by Method 18 in 40 CFR 60.
MW
i
= The molecular weight of organic compound i
in the vent gas, kg/kg-
mol.
0.0416 = The conversion factor for molar volume,
kg-mol/m
3
, at 293 K and 760 mm Hg.
10
-6
= The conversion factor from
ppm.
E)
The annual total organic emission rate must be
determined by the following equation:
A = F *
ร
HOURS
Where:
A is total organic e
mission rate, kg/y.
F is the total organic mass flow rate, kg/h, as
calculated in subsection (c)(1)(D)
above .
HOURS is the total annual hours of operation for
the affected unit.
F)
Total organic emissions from all affected process
vents at the facility must be determined by summing
the hourly total organic mass emissions rates (F as
determined in subsection (c)(1)(D)
above ) and by
summing the annual total organic mass emission rates
(A as determined in subsection (c)(1)(E)
above ) for
all affected process vents at the facility.
2)
The owner or operator shall record such process information
h
2sd
i
i
-6
E
= Q
x(
n
i = 1
C
x MW
)x0.0416x10
โ
155
as is necessary to determine the conditions of the
performance tests. Operations during periods of startup,
shutdown and malfunction do not constitute representative
conditions for the purpose of a performance test.
3)
The owner or operator of an affected facility shall provide,
or cause to be provided, performance testing facilities as
follows:
A)
Sampling ports adequate for the test methods speci
fied
in subsection (c)(1)
above .
B)
Safe sampling platform(s).
C)
Safe access to sampling platform(s).
D)
Utilities for sampling and testing equipment.
4)
For the purpose of making compliance determinations, the
time-weighted average of the results of the three runs must
apply. In the event that a sample is accidentally lost or
conditions occur in which one of the three runs must be
discontinued because of forced shutdown, failure of an
irreplaceable portion of the sample train, extreme
meteorological conditions or other circumstances beyond the
owner or operator's control, compliance may, upon the
Agency's approval, be determined using the average of the
results of the two other runs.
d)
To show that a process vent associated with a hazardous waste
distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation is not subject to
the requirements of this Subpart, the owner or operator shall make
an initial determination that the time-weighted, annual average
total organic concentration of the waste managed by the waste
management unit is less than 10
ppmw using one of the following
two methods:
1)
Direct measurement of the organic concentration of the waste
using the following procedures:
A)
The owner or operator shall take a minimum of four
grab samples of waste for each wastestream managed in
the affected unit under process conditions expected to
cause the maximum waste organic concentration.
B)
For waste generated onsite, the grab sampl
es must be
collected at a point before the waste is exposed to
the atmosphere such as in an enclosed pipe or other
closed system that is used to transfer the waste after
generation to the first affected distillation,
fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation. For
waste generated offsite, the grab samples must be
collected at the inlet to the first waste management
unit that receives the waste provided the waste has
been transferred to the facility in a closed system
such as a tank truck and the waste is not diluted or
mixed with other waste.
C)
Each sample must be analyzed and the total organic
156
concentration of the sample must be computed using
Method 9060 or 8240 of SW-846
, (incorporated by
reference under 35 Ill. Adm. Code 720.111.
D)
The arithmetic mean of the results of the analyses of
the four samples apply for each wastestream managed in
the unit in determining the time-weighted, annual
average total organic concentration of the waste. The
time-weighted average is to be calculated using the
annual quantity of each waste stream processed and the
mean organic concentration of each wastestream managed
in the unit.
2)
Using knowledge of the waste to determine that its total
organic concentration is less than 10
ppmw. Documentation
of the waste determination is required. Examples of
documentation that must be used to support a determination
under this subsection include:
A)
Production process information documenting that no
organic compounds are used.
B)
Information that the waste is generated by a process
that is identical to a process at the same or another
facility that has previously been demonstrated by
direct measurement to generate a wastestream having a
total organic content less than 10
ppmw, or
C)
Prior speciation analysis results on the same
wastestream where it is also documented that no
process changes have occurred since that analysis that
could affect the waste total organic concentration.
e)
The determination that di
stillation, fractionation, thin-film
evaporation, solvent extraction, or air or steam stripping
operations which manage hazardous wastes with time-weighted,
annual average total organic concentrations less than 10
ppmw must
be made as follows:
1)
By the effective date that the facility becomes subject to
the provisions of this Subpart or by the date when the waste
is first managed in a waste management unit, whichever is
later; and
2)
For continuously generated waste, annually; or
3)
Whenever there is a change in the waste being managed or a
change in the process that generates or treats the waste.
f)
When an owner or operator and the Agency do not agree on whether a
distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation manages a
hazardous waste with organic concentrations of at least 10
ppmw
based on knowledge of the waste, the procedures in Method 8240 in
SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111,
must be used to resolve the dispute.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.935
Recordkeeping requirements
157
a)
Compliance Required.
1)
Each owner or operator subject to the provisions of this
Subpart shall comply with the
recordkeeping requirements of
this Section.
2)
An owner or operator of more than one hazardous waste
management unit subject to the provisions of this Subpart
may comply with the
recordkeeping requirements for these
hazardous waste management units in one
recordkeeping system
if the system identifies each record by each hazardous waste
management unit.
b)
Owners and operators shall record the following information in the
facility operating record:
1)
For facilities that comply with the provisions of Section
724.933(a)(2), an implementation schedule that includes
dates by which the closed-vent system and control device
will be installed and in operation. The schedule must also
include a rationale of why the installation cannot be
completed at an earlier date. The implementation schedule
must be in the facility operating record by the effective
date that the facility becomes subject to the provisions of
this Subpart.
2)
Up-to-date documentation of compliance with the process vent
standards in Section 724.932, including:
A)
Information and data identifying all affected process
vents, annual throughput and operating hours of each
affected unit, estimated emission rates for each
affected vent and for the overall facility (i.e., the
total emissions for all affected vents at the
facility), and the approximate location within the
facility of each affected unit (e.g., identify the
hazardous waste management units on a facility plot
plan).
B)
Information and data supporting determination of vent
emissions and emission reductions achieved by add-on
control devices based on engineering calculations or
source tests. For the purpose of determining
compliance, determinations of vent emissions and
emission reductions must be made using operating
parameter values (e.g., temperatures, flow rates, or
vent stream organic compounds and concentrations) that
represent the conditions that result in maximum
organic emissions, such as when the waste management
unit is operating at the highest load or capacity
level reasonably expected to occur. If the owner or
operator takes any action (e.g., managing a waste of
different composition or increasing operating hours of
affected waste management units) that would result in
an increase in total organic emissions from affected
process vents at the facility, then a new
determination is required.
3)
Where an owner or operator chooses to use test data to
determine the organic removal efficiency or total organic
compound concentration achieved by the control device, a
158
performance test plan. The test plan must include:
A)
A description of how it is determined that the planned
test is going to be conducted when the hazardous waste
management unit is operating at the highest load or
capacity level reasonably expected to occur. This
must include the estimated or design flow rate and
organic content of each vent stream and define the
acceptable operating ranges of key process and control
device parameters during the test program.
B)
A detailed engineering description of the closed-vent
system and control device including:
i)
Manufacturer's name and model number of control
device.
ii)
Type of control device.
iii)
Dimensions of the control device.
iv)
Capacity.
v)
Construction materials.
C)
A detailed description of sampling and monitoring
procedures, including sampling and monitoring
locations in the system, the equipment to be used,
sampling and monitoring frequency, and planned
analytical procedures for sample analysis.
4)
Documentation of compliance with Section 724.933 must
include the following information:
A)
A list of all information references and sources used
in preparing the documentation.
B)
Records including the dates of each compliance test
required by Section 724.933(k).
C)
If engineering calculations are used, a design
analysis, specifications, drawings, schematics, and
piping and instrumentation diagrams based on the
appropriate sections of APTI Course 415 (incorporated
by reference in 35 Ill. Adm. Code 720.111) or other
engineering texts, approved by the Agency, that
present basic control device design information.
Documentation provided by the control device
manufacturer or vendor that describes the control
device design in accordance with subsections
(b)(4)(C)(i) through (vii)
, below , may be used to
comply with this requirement. The design analysis
must address the vent stream characteristics and
control device operation parameters as specified
below.
i)
For a thermal vapor incinerator, the design
analysis must consider the vent stream
composition, constituent concentrations and flow
rate. The design analysis must also establish
the design minimum and average temperature in
159
the combustion zone and the combustion zone
residence time.
ii)
For a catalytic va
por incinerator, the design
analysis must consider the vent stream
composition, constituent concentrations, and
flow rate. The design analysis must also
establish the design minimum and average
temperatures across the catalyst bed inlet and
outlet.
iii)
For a boiler or process heater, the design
analysis must consider the vent stream
composition, constituent concentrations and flow
rate. The design analysis must also establish
the design minimum and average flame zone
temperatures, combustion zone residence time and
description of method and location where the
vent stream is introduced into the combustion
zone.
iv)
For a flare, the design analysis must consider
the vent stream composition, constituent
concentrations, and flow rate. The design
analysis must also consider the requirements
specified in Section 724.933(d).
v)
For a condenser, the design analysis must
consider the vent stream composition,
constituent concentrations, flow rate, relative
humidity and temperature. The design analysis
must also establish the design outlet organic
compound concentration level, design average
temperature of the condenser exhaust vent stream
and design average temperatures of the coolant
fluid at the condenser inlet and outlet.
vi)
For a carbon adsorption system such as a fixed-
bed adsorber that regenerates the carbon bed
directly onsite in the control device, the
design analysis must consider the vent stream
composition, constituent concentrations, flow
rate, relative humidity and temperature. The
design analysis must also establish the design
exhaust vent stream organic compound
concentration level, number and capacity of
carbon beds, type and working capacity of
activated carbon used for carbon beds, design
total steam flow over the period of each
complete carbon bed regeneration cycle, duration
of the carbon bed steaming and cooling/drying
cycles, design carbon bed temperature after
regeneration, design carbon bed regeneration
time and design service life of carbon.
vii)
For a carbon adsorpt
ion system such as a carbon
canister that does not regenerate the carbon bed
directly onsite in the control device, the
design analysis must consider the vent stream
composition, constituent concentrations, flow
rate, relative humidity and temperature. The
160
design analysis must also establish the design
outlet organic concentration level, capacity of
carbon bed, type and working capacity of
activated carbon used for carbon bed and design
carbon replacement interval based on the total
carbon working capacity of the control device
and source operating schedule.
D)
A statement signed and dated by the owner or operator
certifying that the operating parameters used in the
design analysis reasonably represent the conditions
that exist when the hazardous waste management unit is
or would be operating at the highest load or capacity
level reasonably expected to occur.
E)
A statement signed and dated by the owner or operator
certifying that the control device is designed to
operate at an efficiency of 95 percent or greater
unless the total organic concentration limit of
Section 724.932(a) is achieved at an efficiency less
than 95 weight percent or the total organic emission
limits of Section 724.932(a) for affected process
vents at the facility are attained by a control device
involving vapor recovery at an efficiency less than 95
weight percent. A statement provided by the control
device manufacturer or vendor certifying that the
control equipment meets the design specifications may
be used to comply with this requirement.
F)
If performance tests are used to demonstrate
compliance, all test results.
c)
Design documentation and monitoring operating and inspection
information for each closed-vent system and control device
required to comply with the provisions of this Part must be
recorded and kept up-to-date in the facility operating record.
The information must include:
1)
Description and date of each modification that is made to
the closed-vent system or control device design.
2)
Identification of
operating parameter, description of
monitoring device, and diagram of monitoring sensor location
or locations used to comply with Section 724.933(f)(1) and
(2).
3)
Monitoring, operating and inspection information required by
Section 724.933(f) through (k).
4)
Date, time and duration of each period that occurs while the
control device is operating when any monitored parameter
exceeds the value established in the control device design
analysis as specified below:
A)
For a thermal vapor incinerator d
esigned to operate
with a minimum residence time of 0.50 second at a
minimum temperature of 760 C, any period when the
combustion temperature is below 760 C.
B)
For a thermal vapor incinerator designed to operate
with an organic emission reduction efficiency of 95
161
weight percent or greater, any period when the
combustion zone temperature is more than 28 C below
the design average combustion zone temperature
established as a requirement of subsection
(b)(4)(C)(i) , above.
C)
For a catalytic vapor inci
nerator, any period when:
i)
Temperature of the vent stream at the catalyst
bed inlet is more than 28 C below the average
temperature of the inlet vent stream established
as a requirement of subsection (b)(4)(C)(ii)
,
above; or
ii)
Temperature difference across the catalyst bed
is less than 80 percent of the design average
temperature difference established as a
requirement of subsection (b)(4)(C)(ii)
, above.
D)
For a boiler or process heater, any period when:
i)
Flame zone temperature is
more than 28 C below
the design average flame zone temperature
established as a requirement of subsection
(b)(4)(C)(iii) , above; or
ii)
Position changes where the vent stream is
introduced to the combustion zone from the
location established as a requirement of
subsection (b)(4)(C)(iii)
, above.
E)
For a flare, period when the pilot flame is not
ignited.
F)
For a condenser that complies with Section
724.933(f)(2)(F)(i), any period when the organic
compound concentration level or readings of organic
compounds in the exhaust vent stream from the
condenser are more than 20 percent greater than the
design outlet organic compound concentration level
established as a requirement of subsection
(b)(4)(C)(v) , above.
G)
For a condenser that complies with Section
724.933(f)(2)(F)(ii), any period when:
i)
Temperature of the exhaust vent stream from the
condenser is more than 6 C above the design
average exhaust vent stream temperature
established as a requirement of subsection
(b)(4)(C)(v) , above.
ii)
Temperature of the coolant fluid exiting the
condenser is more than 6 C above the design
average coolant fluid temperature at the
condenser outlet established as a requirement of
subsection (b)(4)(C)(v)
, above.
H)
For a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed
directly onsite in the control device and complies
162
with Section 724.933(f)(2)(G)(i), any period when the
organic compound concentration level or readings of
organic compounds in the exhaust vent stream from the
carbon bed are more than 20 percent greater than the
design exhaust vent stream organic compound
concentration level established as a requirement of
subsection (b)(4)(C)(vi)
, above.
I)
For a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed
directly onsite in the control device and complies
with Section 724.933(f)(2)(G)(ii), any period when the
vent stream continues to flow through the control
device beyond the predetermined carbon bed
regeneration time established as a requirement of
subsection (b)(4)(C)(vi)
, above.
5)
Explanation for each period recorded under subsection
(c)(4) , above, of the cause for control device operating
parameter exceeding the design value and the measures
implemented to correct the control device operation.
6)
For a carbon adsorption system operated subject to
requirements specified in Section 724.933(g) or (h)(2), any
date when existing carbon in the control device is replaced
with fresh carbon.
7)
For a carbon adsorption system operated subject to
requirements specified in Section 724.933(h)(1), a log that
records:
A)
Date and time when control device is monitored for
carbon breakthrough and the monitoring device reading.
B)
Date when existing carbon in the control device is
replaced with fresh carbon.
8)
Date of each control device startup and shutdown.
9)
An owner or operator designating any components of a closed-
vent system as unsafe to monitor pursuant to Section
724.933(o) shall record in a log that is kept in the
facility operating record the identification of closed
-vent
system components that are designated as unsafe to monitor
in accordance with the requirements of Section 724.933(o),
an explanation for each closed
-vent system component stating
why the closed -vent system component is unsafe to monitor,
and the plan for monitoring each closed
-vent system
component.
10)
When each leak is detected as specified in Section
724.933(l), the following information must be recorded:
A)
The instrument identification number, the closed
-vent
system component identification number, and the
operator name, initials, or identification number.
B)
The date the leak was detected and the date of first
attempt to repair the leak.
C)
The date of successful repair of the leak.
163
D)
Maximum instrument reading measured by Method 21 of 40
CFR 60, appendix A, incorporated by reference in 35
Ill. Adm. Code 720.111, after it is successfully
repaired or determined to be
nonrepairable.
E)
"Repair delayed" and the reason for the delay if a
leak is not repaired within 15 calendar days after
discovery of the leak.
i)
The owner or operator may develop a written
procedure that identifies the conditions that
justify a delay of repair. In such cases,
reasons for delay of repair may be documented by
citing the relevant sections of the written
procedure.
ii)
If delay of repair was caused by depletion of
stocked parts, there must be documentation that
the spare parts were sufficiently stocked
on-site before depletion and the reason for
depletion.
d)
Records of the monitoring, operating
, and inspection information
required by subsections (c)(3) through
(c)(810), above, needmust
be kept onlyat least 3 years following the date of each
occurrence, measurement, corrective action, or record
.
e)
For a control device other than a thermal vapor incinerator,
catalytic vapor incinerator, flare, boiler, process heater,
condenser or carbon adsorption system, the Agency shall specify
the appropriate recordkeeping requirements.
f)
Up-to-date information and data used to determine whether or not a
process vent is subject to the requirements in Section 724.932,
including supporting documentation as required by Section
724.934(d)(2), when application of the knowledge of the nature of
the hazardous wastestream or the process by which it was produced
is used, must be recorded in a log that is kept in the facility
operating record.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 724.950
Applicability
a)
The regulations in this Subpart apply to owners and operators of
facilities that treat, store, or dispose of hazardous wastes
(except as provided in Section 724.101).
b)
Except as provided in Section 724.964(k), this Subpart applies to
equipment that contains or contacts hazardous wastes with organic
concentrations of at least 10 percent by weight that are managed
in one of the following
:
1) UA units that areis subject to the RCRA permitting
requirements of 35 Ill. Adm. Code
702, 703, and 705 , or
2)
HA unit (including a h
azardous waste recycling unit
s) that
164
areis not exempt from permitting under the provisions of 35
Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
unit that is not a "90-day" tank or container) and that is
located onat a hazardous waste management
facilit iesy
otherwise subject to the permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705 ., or
3)
A unit that is exempt from permitting under the provisions
of 35 Ill. Adm. Code 722.134(a) (i.e., a "90
-day" tank or
container).
c)
If the owner or operator of equipment subject to the requirements
of Sections 724.952 through 724.965 has received a RCRA permit
prior to December 21, 1990, the requirements of Sections 724.952
through 724.965 must be incorporated when the permit is reissued
under 35 Ill. Adm. Code 705.201 or reviewed under 35 Ill. Adm.
Code 702.161.
d)
Each piece of equipment to which this Subpart applies must be
marked in such a manner that it can be distinguished readily from
other pieces of equipment.
e)
Equipment that is in vacuum service is excluded from the
requirements of Sections 724.952 to 724.960, if it is identified
as required in Section 724.964(g)(5).
f)
Equipment that contains or contacts hazardous waste with an
organic concentration of at least 10 percent by weight for a
period of less than 300 hours per calendar year is excluded from
the requirements of Sections 264.952 through 264.960 if it is
identified as required in Section 724.964(g)(6).
BOARD NOTE: The requirements of Sections 724.952 through 724.965
apply to equipment associated with hazardous waste recycling units
previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
exemptions under 35 Ill. Adm. Code 721.104
, 722.134 and 724.101(g)
are not affected by these requirements.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.955
Standards: Sampling Connecting Systems
a)
Each sampling connection
system must be equipped with a closed
-
purge, closed-loop, or
system or closed-vent system.
This system
must collect the sample purge for return to the process or for
routing to the appropriate treatment system. Gases displaced
during filling of the sample container are not required to be
collected or captured.
b)
Each closed-purge
, closed-loop, or
system or closed-vent system as
required in subsection (a) must
meet one of the following
requirements :
1)
Return the purged
hazardous waste stream process fluid
directly to the hazardous waste management
process line with
no detectable emissions to atmosphere
; or
2)
Collect and recycle the purged
hazardous waste stream with
no detectable emissions to
atmosphere process fluid ; or
3)
Be designed and operated to capture and transport all the
165
purged hazardous wastestream process fluid to waste
management unit that complies with the applicable
requirements of Sections 724.984 through 724.986 or
a
control device that complies with the requirements of
Section 724.960.
c)
In-situ sampling systems
and sampling systems without purges
are
exempt from the requirements of subsections (a) and (b)
above .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.958
Standards: Pumps, Valves, Pressure Relief Devices and Other
Connectors
a)
Pumps and valves in heavy liquid service, pressure relief devices
in light liquid or heavy liquid service and flanges and other
connectors must be monitored within 5 days by the method specified
in Section 724.963(b), if evidence of a potential leak is found by
visual, audible, olfactory, or any other detection method.
b)
If an instrument reading of 10,000
ppm or greater is measured, a
leak is detected.
c)
Repairs
1)
When a leak is detected, it must be repaired as soon as
practicable, but not later than 15 calendar days after it is
detected, except as provided in Section 724.959.
2)
The first attempt at repair must be made no later than 5
calendar days after each leak is detected.
d)
First at tempts at repair include, but are not limited to, the best
practices described under Section 724.957(e).
e)
Any connector that is inaccessible or is ceramic or ceramic-lined
(e.g., porcelain, glass, or glass
-lined) is exempt from the
monitoring requirements of subsection (a) above and from the
recordkeeping requirements of Section 724.964.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.964
Recordkeeping Requirements
a)
Lumping Units
1)
Each owner or operator
subject to the provisions of this
Subpart shall comply with the
recordkeeping requirements of
this Section.
2)
An owner or operator of more than one hazardous waste
management unit subject to the provisions of this Subpart
may comply with the
recordkeeping requirements for these
hazardous waste management units in one
recordkeeping system
if the system identifies each record by each hazardous waste
management unit.
b)
Owners and operators shall record the following information in the
facility operating record:
1)
For each piece of equipment to which this Subpart applies:
166
A)
Equipment identification number and hazardous waste
management unit identification.
B)
Approximate locations within the facility (e.g.,
identify the hazardous waste management unit on a
facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total
organics in the hazardous
wastestream at the equipment.
E)
Hazardous waste state at the equipment (e.g., gas-
vapor or liquid).
F)
Method of compliance with the standard (e.g., "monthly
leak detection and repair" or "equipped with dual
mechanical seals").
2)
for facilities than comply with the provisions of Section
724.933(a)(2), an implementation schedule as specified in
that Section.
3)
Where an owner or operator chooses to use test data to
demonstrate the organic removal efficiency or total organic
compound concentration achieved by the control device, a
performance test plan as specified in Section 724.935(b)(3).
4)
Documentation of compliance with Section 724.960, including
the detailed design documentation or performance test
results specified in Section 724.935(b)(4).
c)
When each leak is detected as specified in Sections 724.952,
724.953, 724.957 or 724.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked
with the equipment identification number, the date evidence
of a potential leak was found in accordance with Section
724.958(a), and the date the leak was detected, must be
attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be
removed after it has been repaired.
3)
The identification on a valve may be removed after it has
been monitored for 2 successive months as specified in
Section 724.957(c) and no leak has been detected during
those 2 months.
d)
When each leak is detected as specified in Sections 724.952,
724.953, 724.957 or 724.958, the following information must be
recorded in an inspection log and must be kept in the facility
operating record:
1)
The instrument and operator identification numbers and the
equipment identification number.
2)
The date evidence of a potential leak was found in
accordance with Section 724.958(a).
167
3)
The date the leak was detected and the dates of each attempt
to repair the leak.
4)
Repair methods applied in each attempt to repair the leak.
5)
"Above 10,000", if the maximum instrument reading measured
by the methods specified in Section 724.963(b) after each
repair attempt is equal to or greater than 10,000
ppm.
6)
"Repair delayed" and the reason for the delay if a leak is
not repaired within 15 calendar days after discovery of the
leak.
7)
Documentation supporting the delay of repair of a valve in
compliance with Section 724.959(c).
8)
The signature of the owner or operator (or designate) whose
decision it was that repair could not be effected without a
hazardous waste management unit shutdown.
9)
The expected date of successful repair of the leak if a le
ak
is not repaired within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection
information for each closed-vent system and control device
required to comply with the provisions of Section 724.960 must be
recorded and kept up-to-date in the facility operating record as
specified in Section 724.935(c)(1) and
(c)(2), and monitoring,
operating and inspection information in Section 724.935(c)(3)
through (c)(8).
f)
For a control d evice other than a thermal vapor incinerator,
catalytic vapor incinerator, flare, boiler, process heater,
condenser, or carbon adsorption system, the Agency shall specify
the appropriate recordkeeping requirements, indicating proper
operation and maintenance of the control device, in the RCRA
permit.
g)
The following information pertaining to all equipment subject to
the requirements in Sections 724.952 through 724.960 must be
recorded in a log that is kept in the facility operating record:
1)
A list o f identification numbers for equipment (except
welded fittings) subject to the requirements of this
Subpart.
2)
List of Equipment
A)
A list of identification numbers for equipment that
the owner or operator elects to designate for no
detectable emissions, as indicated by an instrument
reading of less than 500
ppm above background, under
the provisions of Sections 724.952(e), 724.953(i) and
724.957(f).
B)
The designation of this equipment as subject to the
requirements of Sections 724.952(e), 724.953(i) or
724.957(f) must be signed by the owner or operator.
168
3)
A list of equipment identification numbers for pressure
relief devices required to comply with Section 724.954(a).
4)
Compliance tests.
A)
The dates of each compliance test required in Sections
724.952(e), 724.953(i), 724.954 and 724.957(f).
B)
The background level measured during each compliance
test.
C)
The maximum instrument reading measured at the
equipment during each compliance test.
5)
A list of identification numbe
rs for equipment in vacuum
service.
6)
Identification, either by list or location (area or group)
of equipment that contains or contacts hazardous waste with
an organic concentration of at least 10 percent by weight
for a period of less than 300 hours per year.
h)
The following information pertaining to all valves subject to the
requirements of Section 724.957(g) and (h) must be recorded in a
log that is kept in the facility operating record:
1)
A list of identification numbers for valves that are
designated as unsafe to monitor, an explanation for each
valve stating why the valve is unsafe to monitor, and the
plan for monitoring each valve.
2)
A list of identification numbers for valves that are
designated as difficult to monitor, an explanation for each
valve stating why the valve is difficult to monitor, and the
planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility
operating record for valves complying with Section 724.962:
1)
A schedule o f monitoring.
2)
The percent of valves found leaking during each monitoring
period.
j)
The following information must be recorded in a log that is kept
in the facility operating record:
1)
Criteria required in Section 724.952(d)(5)(B) and
724.953(e)(2) and an explanation of the design criteria.
2)
Any changes to these criteria and the reasons for the
changes.
k)
The following information must be recorded in a log that is kept
in the facility operating record for use in determining exemptions
as provided in Section 724.950 and other specific Subparts:
1)
An analysis determining the design capacity of the hazardous
waste management unit.
2)
A statement listing the hazardous waste influent to and
169
effluent from each hazardous waste management unit subject
to the requirements in Sections 724.960 and an analysis
determining whether these hazardous wastes are heavy
liquids.
3)
An up-to-date analysis and the supporting information and
data used to determine whether or not equipment is subject
to the requirements in Sections 724.952 through 724.960.
The record must include supporting documentation as required
by Section 724.963(d)(3) when application of the knowledge
of the nature of the hazardous wastestream or the process by
which it was produced is used. If the owner or operator
takes any action (e.g., changing the process that produced
the waste) that could result in an increase in the total
organic content of the waste contained in or contacted by
equipment determined not to be subject to the requirements
in Sections 724.952 through 724.960, then a new
determination is required.
l)
Records of the equipment leak information required by subsection
(d) above and the operating information required by subsection (e)
above need be kept only 3 years.
m)
The owner or operator of any facility that is subject to this
Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61,
Subpart V, incorporated by reference in 35 Ill. Adm. Code 720.111,
may elect to determine compliance with this Subpart by
documentation either pursuant to Section 724.964, or pursuant to
those provisions of 40 CFR 60 or 61, to the extent that the
documentation under the regulation at 40 CFR 60 or 61 duplicates
the documentation required under this Subpart. The documentation
under the regulation at 40 CFR 60 or 61 must be kept with or made
readily available with the facility operating record.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
SURFACE IMPOUNDMENTS, AND CONTAINERS
Section 724.980
Applicability
a)
The requirements of this Subpart apply, effective October 6, 1996,
to owners and operators of all facilities that treat, store, or
dispose of hazardous waste in tanks, surface
impoundments, or
containers subject to 724.Subparts I, J, or K, except as Section
724.101 and subsection (b) below provide otherwise.
BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
(Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828
(May 19, 1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed.
Reg. 28508 (June 5, 1996), USEPA delayed the effective date until
October 6, 1996. If action by USEPA or a decision of a federal
court changes the effectiveness of these regulations, the Board
does not intend that the 724.Subpart CC rules be enforceable to
the extent that they become more stringent that the federal
regulations upon which they are based.
b)
The requirements of this Subpart do not apply to the following
waste management units at the facility:
170
1)
A waste management unit that holds hazardous waste placed in
the unit before October 6, 1996, and in which no hazardous
waste is added to the unit on or after this date.
2)
A container that has a design capacity less than or equal to
0.1 m
3
(3.5 ft
3
or 26.4 gal).
3)
A tank in which an owner or operator has stopped adding
hazardous waste and the owner or operator has begun
implementing or completed closure pursuant to an approved
closure plan.
4)
A surface impoundment in whic
h an owner or operator has
stopped adding hazardous waste (except to implement an
approved closure plan) and the owner or operator has begun
implementing or completed closure pursuant to an approved
closure plan.
5)
A waste management unit that is used solely for on-site
treatment or storage of hazardous waste that is generated as
the result of implementing remedial activities required
pursuant to the Act or Board regulations or under the
corrective action authorities of RCRA sections 3004(u),
3004(v) or 3008(h); CERCLA authorities; or similar federal
or state authorities.
6)
A waste management unit that is used solely for the
management of radioactive mixed waste in accordance with all
applicable regulations under the authority of the Atomic
Energy Act (42 U.S.C. 2011 et seq.) and the Nuclear Waste
Policy Act.
7)
A hazardous waste management unit that the owner or operator
certifies is equipped with and operating air emission
controls in accordance with the requirements of an
applicable federal Clean Air Act regulation codified under
40 CFR 60, 61, or 63. For the purpose of complying with
this subsection, a tank for which the air emission control
includes an enclosure, as opposed to a cover, must be in
compliance with the enclosure and control device
requirements of Section 724.984(i), except as provided in
Section 724.982(c)(5).
8)
A tank that has a process vent, as defined in 35 Ill. Adm.
Code 724.931.
c)
For the owner and operator of a facility subject to this Subpart
and whothat received a final RCRA permit prior to October 6, 1996,
the requirements of this Subpart shall be incorporated into the
permit when the permit is reissued, renewed, or modified in
accordance with the requirements of 35 Ill. Adm. Code 703 and 705.
Until such date when the owner and operator receives a final
permit incorporating the requirements of this Subpart, the owner
and operator is subject to the requirements of 35 Ill. Adm. Code
725.Subpart CC.
d)
The requirements of this Subpart, except for the
recordkeeping
requirements specified in Section 724.989(i) are stayed for a tank
or container used for the management of hazardous waste generated
by organic peroxide manufacturing and its associated laboratory
operations, when the owner or operator of the unit meets all of
171
the following conditions:
1)
The owner or operator identifies that the tank or container
receives hazardous waste generated by an organic peroxide
manufacturing process producing more than one functional
family of organic peroxides or multiple organic peroxides
within one functional family, that one or more of these
organic peroxides could potentially undergo self-
accelerating thermal decomposition at or below ambient
temperatures, and that organic peroxides are the predominant
products manufactured by the process. For the purposes of
this subsection, "organic peroxide" means an organic
compound that contains the bivalent
-O-O- structure and
which may be considered to be a
sturctural derivative of
hydrogen peroxide where one or both of the hydrogen atoms
has been replaced by an organic radical.
2)
The owner or operator prepares documentation, in accordance
with Section 724.989(i), explaining why an undue safety
hazard would be created if air emission controls specified
in Sections 724.984 through 724.987 are installed and
operated on the tanks and containers used at the facility to
manage the hazardous waste generated by the organic peroxide
manufacturing process or processes meeting the conditions of
subsection (d)(1) above.
3)
The owner or opera
tor notifies the Agency in writing that
hazardous waste generated by an organic peroxide
manufacturing process or processes meeting the conditions of
subsection (d)(1) above are managed at the facility in tanks
or containers meeting the conditions of subsection (d)(2)
above. The notification must state the name and address of
the facility and be signed and dated by an authorized
representative of the facility owner or operator.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.982
Standards: General
a)
This Section applies to the management of hazardous waste in
tanks, surface impoundments, and containers subject to this
Subpart.
b)
The owner or operator shall control air emissions from each waste
management unit in accordance with standards specified in Section
724.984 through 724.987, as applicable to the waste management
unit, except as provided for in subsection (c) below.
c)
A waste management
unittank, surface impoundment, or container
is
exempt ed from standards specified in Sections 724.984 through
724.987, as applicable, provided that all hazardous waste placed
in the waste management unit is
determined by the owner or
operator to meet
either one of the following
conditions :
1) The average VO concentration of
theA tank, surface
impoundment, or container for which all
hazardous waste
entering the unit has an average VO concentration
at the
point of waste origination
isof less than 100500 parts per
million by weight (
ppmw). The average VO concentration
shall be determined by the procedures specified in Section
724.983(a). The owner or operator shall review and update,
172
as necessary, this determination at least once every 12
months following the date of the initial determination for
the hazardous waste streams entering the unit.
2) TA tank, surface impoundment, or container for which t
he
organic content of
all the hazardous waste
entering the
waste management unit
has been reduced by an organic
destruction or removal process that achieves any one of the
following conditions:
A)
The process removes or destroys the
organics contained
in the hazardous waste to a level such that the
average VO concentration of the hazardous waste at the
point of waste treatment is less than the exit
concentration limit (C
t
) established for the process.
The average VO concentration of the hazardous waste
at the point of waste treatment and the exit
concentration limit for the process shall be
determined using the procedures specified in Section
724.983(b).
B)
The proce ss removes or destroys the
organics contained
in the hazardous waste to a level such that the
organic reduction efficiency (R) for the process is
equal to or greater than 95 percent, and the average
VO concentration of the hazardous waste at the point
of waste treatment is less than
50100 ppmw. The
organic reduction efficiency for the process and the
average VO concentration of the hazardous waste at the
point of waste treatment shall be determined using the
procedures specified in Section 724.983(b).
C)
The process removes or destroys the
organics contained
in the hazardous waste to a level such that the actual
organic mass removal rate (MR) for the process is
equal to or greater than the required organic mass
removal rate (RMR) established for the process. The
required organic mass removal rate and the actual
organic mass removal rate for the process shall be
determined using the procedures specified in Section
724.983(b).
D)
The process is a biological process that destroys or
degrades the organics contained in the hazardous waste
so that either of the following conditions is met:
i)
The organic reduction efficiency (R) for the
process is equal to or greater than 95 percent,
and the organic biodegradation efficiency (
R
bio
)
for the process is equal to or greater than 95
percent. The organic reduction efficiency and
the organic biodegradation efficiency for the
process shall be determined
in accordance
withusing the procedures specified in Section
724.983(b).
ii)
The total actual organic m
ass biodegradation
rate ( MR
bio
) for all hazardous waste treated by
the process is equal to or greater than the
required organic mass removal rate (RMR). The
required organic mass removal rate and the
173
actual organic mass
biodegradation rate for the
process shall be determined using the procedures
specified in Section 724.983(b).
E)
The process removes or destroys the
organics contained
in the hazardous waste and meets all of the following
conditions:
i) All of the materials entering the process are
hazardous wastes.
ii)
From the point of waste origination through the
point where the hazardous waste enters the
treatment process, the hazardous waste is
continuously managed in waste management units
whichthat use air emission controls in
accordance with the standards specified in
Sections 724.984 through 724.987, as applicable
to the waste management unit.
ii)
From the point of waste origination through the
point where the hazardous waste enters the
treatment process, any transfer of the hazardous
waste is accomplished through continuous
hard-piping or other closed system transfer that
does not allow exposure of the waste to the
atmosphere.
BOARD NOTE: The USEPA considers a drain system
that meets the requirements of 40 CFR 63,
subpart RR, "National Emission Standards for
Individual Drain Systems", to be a closed
system.
iii)
The average VO concentration of the hazardous
waste at the point of waste treatment is less
than the lowest average VO concentration at the
point of waste origination, determined for each
of the individual hazardous waste streams
entering the process
, or 100500 ppmw, whichever
value is lower. The average VO concentration of
each individual hazardous waste stream at the
point of waste origination shall be determined
using the procedure
s specified in Section
724.983(a). The average VO concentration of the
hazardous waste at the point of waste treatment
shall be determined using the procedure
s
specified in Section 724.983(b).
F)
A process that removes or destroys the
organics
contained in the hazardous waste to a level such that
the organic reduction efficiency (R) for the process
is equal to or greater than 95 percent and the owner
or operator certifies that the average VO
concentration at the point of waste origination for
each of the individual waste streams entering the
process is less than 10,000
ppmw. The organic
reduction efficiency for the process and the average
VO concentration of the hazardous waste at the point
of waste origination shall be determined using the
procedures specified in Section 724.983(b) and Section
174
724.983(a), respectively.
FG)
A hazardous waste incinerator for which
either of the
owner or operator has
either following conditions is
true:
i) BThe owner or operator has b
een issued a final
permit under 35 Ill. Adm. Code
702, 703, and
705, and designs and operates the unit in
accordance with that implements the requirements
of 724726.Subpart OH; or
ii) HThe owner or operator h
as certified
compliance designed and operates the incinerator
in accordance with the interim status
requirements of 35 Ill. Adm. Code 725.Subpart O.
GH)
A boiler or industrial furnace for which
either of the
owner or operator has
either following conditions is
true:
i) BThe owner or operator has b
een issued a final
permit under 35 Ill. Adm. Code
702, 703, and
705, and designs and operates the unit in
accordance with that implements the requirements
of 724726.Subpart H; or
ii)
The owner or operator h
as certified
compliance designed and operates the boiler or
industrial furnace in accordance
with the
interim status requirements of 35 Ill. Adm. Code
726.Subpart H.
I)
For the purpose of determining the performance of an
organic destruction or removal process in accordance
with the conditions in each of subsections (c)(2)(A)
through (c)(2)(F) above, the owner or operator shall
account for VO concentrations determined to be below
the limit of detection of the analytical method by
using the following VO concentration:
i)
If Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, is used for the analysis, one
-half the
blank value determined in the method.
ii)
If any other analytical method is used, one
-half
the limit of detection established for the
method.
3)
A tank used for biological treatment of hazardous waste in
accordance with the requirements of subsection (c)(2)(D)
above.
4)
A tank, surface impoundment, or container for which all
hazardous waste placed in the unit fulfills either of the
following conditions:
A)
It meets the numerical concentration limits for
organic hazardous constituents, applicable to the
hazardous waste, as specified in 35 Ill. Adm. Code
175
728.Table T; or
B)
It has been treated by the treatment technology
established by USEPA for the waste in 35 Ill. Adm.
Code 728.142(a), or treated by an equivalent method of
treatment approved by the Agency pursuant to 35 Ill.
Adm. Code 728.142(b).
5)
A tank used for bulk feed of hazardous waste to a waste
incinerator and all of the following conditions are met:
A)
The tank is located inside an enclosure vented to a
control device that is designed and operated in
accordance with all applicable requirements specified
under 40 CFR 61, subpart FF, "National Emission
Standards for Benzene Waste Operations", incorporated
by reference in 35 Ill. Adm. Code 720.111, for a
facility at which the total annual benzene quantity
from the facility waste is equal to or greater than 10
megagrams (11 tons) per year;
B)
The enclosure and control device serving the tank were
installed and began operation prior to November 25,
1996; and
C)
The enclosure is designed and operated in accordance
with the criteria for a permanent total enclosure as
specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111. The enclosure may have permanent or
temporary openings to allow worker access; passage of
material into or out of the enclosure by conveyor,
vehicles, or other mechanical or electrical equipment;
or to direct air flow into the enclosure. The owner
or operator shall perform the verification procedure
for the enclosure as specified in Section 5.0 to
"Procedure T --Criteria for and Verification of a
Permanent or Temporary Total Enclosure" annually.
d) When a process is used for the purpose of treating a hazardous
waste to meet one of the sets of conditions specified in
subsections (c)(2)(A) through (c)(2)(E) above, each material
removed from or exiting the process that is not a hazardous waste
but which has an average VO concentration equal to or greater than
100 ppmw shall be managed in a waste management unit in accordance
with the requirements of subsection (b) above.
ed)
The Agency may at any time perform or request that the owner or
operator perform a waste determination for a hazardous waste
managed in a tank, surface impoundment, or container that is
exempted from using air emission controls under the provisions of
this Section as follows:
1)
The waste determination for average VO concentration of a
hazardous waste at the point of waste origination shall be
performed using direct measurement in accordance with the
applicable requirements of Section 724.983(a). The waste
determination for a hazardous waste at the point of waste
treatment shall be performed in accordance with the
176
applicable requirements of Section 724.983(b).
2)
In performing a waste determination pursuant to subsection
(d)(1) above, the sample preparation and analysis shall be
conducted as follows:
A)
In accordance with the method used by the owner or
operator to perform the waste analysis, except in the
case specified in subsection (d)(2)(B) below.
B)
If the Agency determines that the method used by the
owner or operator was not appropriate for the
hazardous waste managed in the tank, surface
impoundment, or container, then the Agency may choose
an appropriate method.
23)
Where the owner or operator is requested to perform the
waste determination, the Agency may elect to have an
authorized representative observe the collection of the
hazardous waste samples used for the analysis.
34)
Where the results of the waste determination performed or
requested by the Agency do not agree with the results of a
waste determination performed by the owner or operator using
knowledge of the waste, then the results of the waste
determination performed in accordance with the requirements
of subsection ( ed)(1) above shall be used to establish
compliance with the requirements of this Subpart.
45)
Where the owner or operator has used an averaging period
greater than one hour for determining the average VO
concentration of a hazardous waste at the point of waste
origination, the Agency may elect to establish compliance
with this Subpart by performing or requesting that the owner
or operator perform a waste determination using direct
measurement based on waste samples collected within a one-
hour period as follows:
A)
The average VO concentration of t
he hazardous waste at
the point of waste origination shall be determined by
direct measurement in accordance with the requirements
of Section 724.983(a).
B)
Results of the waste determination performed or
requested by the Agency showing that the average VO
concentration of the hazardous waste at the point of
waste origination is equal to or greater than
100500
ppmw shall constitute noncompliance with this Subpart,
except in a case as provided for in subsection
(ed)(4)(C) below.
C)
Where the average
VO concentration of the hazardous
waste at the point of waste origination previously has
been determined by the owner or operator using an
averaging period greater than one hour to be less than
100500 ppmw but because of normal operating process
variations the VO concentration of the hazardous waste
determined by direct measurement for any given one-
hour period may be equal to or greater than
100500
ppmw, information that was used by the owner or
operator to determine the average VO concentration of
177
the hazardous waste (e.g., test results, measurements,
calculations, and other documentation) and recorded in
the facility records in accordance with the
requirements of Section 724.983(a) and Section 724.989
shall be considered by the Agency together with the
results of the waste determination performed or
requested by the Agency in establishing compliance
with this Subpart.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.983
Waste Determination Procedures
a)
Waste det ermination procedure for average volatile organic (VO)
concentration of a hazardous waste at the point of waste
origination.
1)
An owner or operator shall determine the average VO
concentration at the point of waste origination for each
hazardous waste placed in
a waste management unit
s exempted
under the provisions of Section 724.982(c)(1) from using air
emission controls in accordance with standards specified in
Section 724.984 through Section 724.987, as applicable to
the waste management unit.
2)
The average VO concentration
of a hazardous waste
at the
point of waste origination
for a hazardous waste
shallmay be
determined in accordance with the procedures specified in 35
Ill. Adm. Code 725.984(a)(2) through (a)(
64).
b)
Waste determination procedures for treated hazardous waste.
1)
An owner or operator shall perform the applicable waste
determination s for each treated hazardous waste placed in
a
waste management unit
s exempted under the provisions of
Section 724.982(c)(2) from using air emission controls in
accordance with standards specified in Section
s 724.984
through 724.987, as applicable to the waste management unit.
2)
The waste determination for a treated hazardous waste shall
be performed in accordance with the procedures specified in
35 Ill. Adm. Code 725.984(b)(2) through (b)(
109), as
applicable to the treated hazardous waste.
c)
Procedure to determine the maximum organic vapor pressure of a
hazardous waste in a tank.
1)
An owner or operator shall determine the maximum organic
vapor pressure for each hazardous waste placed in
a tanks
using air emission Tank Level 1 controls in accordance with
standards specified in Section 724.984(c).
2)
The maximum organic vapor pressure of the hazardous waste
shallmay be determined in accordance with the procedures
specified in 35 Ill. Adm. Code 725.984(c)(2) through (c)(4).
d)
The procedure for determining no detectable organic emissions for
the purpose of complying with this Subpart must be conducted in
accordance with the procedures specified in 40 CFR 265.984(d).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
178
Section 724.984
Standards: Tanks
a) This Section applies to owners and operators of tanks subject to
this Subpart into which any hazardous waste is placed, except for
the following tanks:
1) A tank in which all hazardous waste entering the tank meets
the conditions specified in Section 724.982(c), or
2) A tank used for biological treatment of hazardous waste in
accordance with the requirements of Section
724.982(c)(2)(D).
b) The owner or operator shall place the hazardous waste into one of
the following tanks:
1) A tank equipped with a cover (e.g., a fixed roof) that is
vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (d)
below;
2) A tank equipped with a fixed roof and internal floating roof
in accordance with the requirements of Section 724.991;
3) A tank equipped with an external floating roof in accordance
with the requirements of Section 724.991; or
4) A pressure tank that is designed to operate as a closed
system such that the tank operates with no detectable
organic emissions at all times that hazardous waste is in
the tank except as provided for in subsection (g) below.
c) As an alternative to complying with subsection (b) above, an owner
or operator may place hazardous waste in a tank equipped with a
cover (e.g., a fixed roof) meeting the requirements specified in
subsection (d)(1) below when the hazardous waste is determined to
meet all of the following conditions:
1) The hazardous waste is not mixed, stirred, agitated, or
circulated within the tank by the owner or operator using a
process that results in splashing, frothing, or visible
turbulent flow on the waste surface during normal process
operations;
2) The hazardous waste in the tank is not heated by the owner
or operator except during conditions requiring that the
waste be heated to prevent the waste from freezing or to
maintain adequate waste flow conditions for continuing
normal process operations;
3) The hazardous waste in the tank is not treated by the owner
or operator using a waste stabilization process or a process
that produces an exothermic reaction; and
4) The maximum organic vapor pressure of the hazardous waste in
the tank, as determined using the procedure specified in
Section 724.983(c), is less than the following applicable
value:
A) If the tank design capacity is equal to or greater
179
than 151 m
3
(5333 ft
3
or 39,887 gal), then the maximum
organic vapor pressure shall be less than 5.2
kPa
(0.75 psia or 39 mm Hg);
B) If the tank design capacity is equal to or greater
than 75 m
3
(2649 ft
3
or 19,810 gal) but less than 151
m
3
(5333 ft
3
or 39,887 gal), then the maximum organic
vapor pressure shall be less than 27.6
kPa (4.0 psia
or 207 mm Hg); or
C) If the tank design capacity is less than 75 m
3
(2649
ft
3
or 19,810 gal), then the maximum organic vapor
pressure shall be less than 76.6
kPa (11.1 psia or 574
mm Hg).
d) To comp ly with subsection (b)(1) above, the owner or operator
shall design, install, operate, and maintain a cover that vents
the organic vapors emitted from hazardous waste in the tank
through a closed-vent system connected to a control device.
1) The cover shall be designed and operated to meet the
following requirements:
A) The cover and all cover openings (e.g., access
hatches, sampling ports, and gauge wells) shall be
designed to operate with no detectable organic
emissions when all cover openings are secured in a
closed, sealed position; and
B) Each cover opening shall be secured in a closed,
sealed position (e.g., covered by a
gasketed lid or
cap) at all times that hazardous waste is in the tank
except as provided for in subsection (f) below.
2) The closed-vent system and control device shall be designed
and operated in accordance with the requirements of Section
724.987.
e) The owner and operator shall install, operate, and maintain
enclosed pipes or other closed-systems to:
BOARD NOTE: U .S. EPA considers a drain system that meets the
requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
a "closed-system". The Board intends that this meaning be
included in the use of that term for the purposes of this Subpart.
1) Transfer all hazardous waste to the tank from another tank,
surface impoundment, or container subject to this Subpart
except for those hazardous wastes that meet the conditions
specified in Section 724.982(c); and
2) Transfer all hazardous waste from the tank to
another tank,
surface impoundment, or container subject to this Subpart
except for those hazardous wastes that meet the conditions
specified in Section 724.982(c).
f) Each cover opening shall be secured in a closed, sealed position
(e.g., covered by a
gasketed lid) at all times that hazardous
waste is in the tank except when it is necessary to use the cover
opening to:
180
1) Add, remove, inspect, or sample the material in the tank;
2) Inspect, maintain, repair, or replace equipment located
inside the tank; or
3) Vent gases or vapors from the tank to a closed-vent system
connected to a control device that is designed and operated
in accordance with the requirements of Section 724.987.
g) One or more safety devices that vent directly to the atmosphere
may be used on the tank, cover, closed-vent system, or control
device provided each safety device meets all of the following
conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the tank or closed-vent system
connected to a control device; and
2) The safety device remains in a closed, sealed position at
all times, except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the tank, cover, closed-vent
system, or control device in accordance with good
engineering and safety practices for handling flammable,
combustible, explosive, or other hazardous materials. An
example of an unplanned event is a sudden power outage.
a)
The provisions of this Section apply to the control of air
pollutant emissions from tanks for which Section 724.982(b)
references the use of this Section for such air emission control.
b)
The owner or operator shall control air pollutant emissions from
each tank subject to this Section in accordance with the following
requirements, as applicable:
1)
For a tank that manages hazardous waste that meets all of
the conditions specified in subsections (b)(1)(A) through
(b)(1)(C) below, the owner or operator shall control air
pollutant emissions from the tank in accordance with the
Tank Level 1 controls specified in subsection (c) below or
the Tank Level 2 controls specified in subsection (d) below.
A)
The hazardous waste in the tank has a maximum organic
vapor pressure that is less than the maximum organic
vapor pressure limit for the tank's design capacity
category as follows:
i)
For a tank design capacity equal to or greater
than 151 m
3
(39,900 gal), the maximum organic
vapor pressure limit for the tank is 5.2
kPa
(0.75 psig).
ii)
For a tank design capacity equal to or greater
than 75 m
3
(19,800 gal) but less than 151 m
3
(39,900 gal), the maximum organic vapor pressure
limit for the tank is 27.6
kPa (4.00 psig).
iii)
For a tank design capacity less than 75 m
3
(19,800 gal), the maximum organic vapor pressure
limit for the tank is 76.6
kPa (11.1 psig).
181
B)
The hazardous waste in the tank is not heated by the
owner or operator to a temperature that is greater
than the temperature at which the maximum organic
vapor pressure of the hazardous waste is determined
for the purpose of complying with subsection (b)(1)(A)
above.
C)
The hazardous waste in the tank is not treated by the
owner or operator using a waste stabilization process,
as defined in 35 Ill. Adm. Code 725.981.
2)
For a tank that manages hazardous waste that does not meet
all of the conditions specified in subsections (b)(1)(A)
through (b)(1)(C) above, the owner or operator shall control
air pollutant emissions from the tank by using Tank Level 2
controls in accordance with the requirements of subsection
(d) below. Examples of tanks required to use Tank Level 2
controls include a tank used for a waste stabilization
process and a tank for which the hazardous waste in the tank
has a maximum organic vapor pressure that is equal to or
greater than the maximum organic vapor pressure limit for
the tank's design capacity category as specified in
subsection (b)(1)(A) above.
c)
Owners and operators controlling air pollutant emissions from a
tank using Tank Level 1 controls must meet the requirements
specified in subsections (c)(1) through (c)(4) below:
1)
The owner or operator shall determine the maximum organic
vapor pressure for a hazardous waste to be managed in the
tank using Tank Level 1 controls before the first time the
hazardous waste is placed in the tank. The maximum organic
vapor pressure must be determined using the procedures
specified in Section 724.983(c). Thereafter, the owner or
operator shall perform a new determination whenever changes
to the hazardous waste managed in the tank could potentially
cause the maximum organic vapor pressure to increase to a
level that is equal to or greater than the maximum organic
vapor pressure limit for the tank design capacity category
specified in subsection (b)(1)(A) below, as applicable to
the tank.
2)
The tank must be equipped with a fixed roof designed to meet
the following specifications:
A)
The fixed roof and its closure devices must be
designed to form a continuous barrier over the entire
surface area of the hazardous waste in the tank. The
fixed roof may be a separate cover installed on the
tank (e.g., a removable cover mounted on an open
-top
tank) or may be an integral part of the tank
structural design (e.g., a horizontal cylindrical tank
equipped with a hatch).
B)
The fixed roof must be installed in a manner such that
there are no visible cracks, holes, gaps, or other
open spaces between roof Section joints or between the
interface of the roof edge and the tank wall.
C)
Each opening in the fixed roof must be either:
182
i)
Equipped with a closure device designed to
operate such that when the closure device is
secured in the closed position there are no
visible cracks, holes, gaps, or other open
spaces in the closure device or between the
perimeter of the opening and the closure device;
or
ii)
Connected by a closed
-vent system that is vented
to a control device. The control device must
remove or destroy
organics in the vent stream,
and it must be operating whenever hazardous
waste is managed in the tank.
D)
The fixed roof and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and will maintain the integrity of the
fixed roof and closure devices throughout their
intended service life. Factors to be considered when
selecting the materials for and designing the fixed
roof and closure devices must include the following:
the organic vapor permeability; the effects of any
contact with the hazardous waste or its vapors managed
in the tank; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
used for the tank on which the fixed roof is
installed.
3)
Whenever a hazardous waste is in the tank, the fixed roof
must be installed with each closure device secured in the
closed position, except as follows:
A)
Opening of closure devices or removal of the fixed
roof is allowed at the following times:
i)
To provide access to the tank for performing
routine inspection, maintenance, or other
activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample the
liquid in the tank, or when a worker needs to
open a hatch to maintain or repair equipment.
Following completion of the activity, the owner
or operator shall promptly secure the closure
device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues
from the bottom of tank.
B)
Opening of a spring
-loaded pressure -vacuum relief
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the tank internal pressure in accordance
with the tank design specifications. The device must
be designed to operate with no detectable organic
emissions when the device is secured in the closed
position. The settings at which the device opens must
be established such that the device remains in the
183
closed position whenever the tank internal pressure is
within the internal pressure operating range
determined by the owner or operator based on the tank
manufacturer recommendations, applicable regulations,
fire protection and prevention codes, standard
engineering codes and practices, or other requirements
for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples
of normal operating conditions that may require these
devices to open are during those times when the tank
internal pressure exceeds the internal pressure
operating range for the tank as a result of loading
operations or diurnal ambient temperature
fluctuations.
C)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
4)
The owner or operator shall inspect the air emission control
equipment in accordance with the following requirements.
A)
The fixed roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof sections or
between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure
devices; and broken or missing hatches, access covers,
caps, or other closure devices.
B)
The owner or operator shall perform an initial
inspection of the fixed roof and its closure devices
on or before the date that the tank becomes subject to
this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year
except under the special conditions provided for in
subsection (l) below.
C)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
D)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 724.989(b).
d)
Owners and operators controlling air pollutant emissions from a
tank using Tank Level 2 controls must use one of the following
tanks:
1)
A fixed -roof tank equipped with an internal floating roof in
accordance with the requirements specified in subsection (e)
below;
2)
A tank equipped with an external floating roof in accordance
with the requirements specified in subsection (f) below;
3)
A tank vented through a closed
-vent system to a control
device in accordance with the requirements specified in
184
subsection (g) below;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) below; or
5)
A tank located inside an enclosure that is vented through a
closed -vent system to an enclosed combustion control device
in accordance with the requirements specified in subsection
(i) below.
e)
The owner or operator that controls air pollutant emissions from a
tank using a fixed roof with an internal floating roof shall meet
the requirements specified in subsections (e)(1) through (e)(3)
below.
1)
The tank must be equipped with a fixed roof and an internal
floating roof in accordance with the following requirements:
A)
The internal floating roof must be designed to float
on the liquid surface except when the floating roof
must be supported by the leg supports.
B)
The internal floating roof must be equipped with a
continuous seal between the wall of the tank and the
floating roof edge that meets either of the following
requirements:
i)
A single continuous seal that is either a
liquid -mounted seal or a metallic shoe seal, as
defined in 35 Ill. Adm. Code 725.981; or
ii)
Two continuous seals mounted one above the
other. The lower seal may be a vapor
-mounted
seal.
C)
The internal floating roof must meet the following
specifications:
i)
Each opening in a
noncontact internal floating
roof except for automatic bleeder vents (vacuum
breaker vents) and the rim space vents is to
provide a projection below the liquid surface.
ii)
Each opening in the internal floating roof must
be equipped with a
gasketed cover or a
gasketed
lid except for leg sleeves, automatic bleeder
vents, rim space vents, column wells, ladder
wells, sample wells, and stub drains.
iii)
Each penetration of the internal floating roof
for the purpose of sampling must have a slit
fabric cover that covers at least 90 percent of
the opening.
iv)
Each automatic bleeder vent and rim space vent
must be gasketed.
v)
Each penetration of the internal floating roof
that allows for passage of a ladder must have a
gasketed sliding cover.
185
vi)
Each penetration of the internal floating roof
that allows for passage of a column supporting
the fixed roof must have a flexible fabric
sleeve seal or a
gasketed sliding cover.
2)
The owner or operator shall operate the tank in accordance
with the following requirements:
A)
When the floating roof is resting on the leg supports,
the process of filling, emptying, or refilling must be
continuous and must be completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all
times when the roof is floating, except when the roof
is being floated off or is being landed on the leg
supports.
C)
Prior to filling the tank, each cover, access hatch,
gauge float well or lid on any opening in the internal
floating roof must be bolted or fastened closed (i.e.,
no visible gaps). Rim space vents must be set to open
only when the internal floating roof is not floating
or when the pressure beneath the rim exceeds the
manufacturer's recommended setting.
3)
The owner or operator shall inspect the internal floating
roof in accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to
any of the following: when the internal floating roof
is not floating on the surface of the liquid inside
the tank; when liquid has accumulated on top of the
internal floating roof; when any portion of the roof
seals have detached from the roof rim; when holes,
tears, or other openings are visible in the seal
fabric; when the gaskets no longer close off the
hazardous waste surface from the atmosphere; or when
the slotted membrane has more than 10 percent open
area.
B)
The owner or operator shall inspect the internal
floating roof components as follows, except as
provided in subsection (e)(3)(C) below:
i)
Visually inspect the internal floating roof
components through openings on the fixed
-roof
(e.g., manholes and roof hatches) at least once
every 12 months after initial fill, and
ii)
Visually inspect the internal floating roof,
primary seal, secondary seal (if one is in
service), gaskets, slotted membranes, and sleeve
seals (if any) each time the tank is emptied and
degassed and at least once every 10 years.
C)
As an alternative to performing the inspections
specified in subsection (e)(3)(B) above for an
internal floating roof equipped with two continuous
186
seals mounted one above the other, the owner or
operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted
membranes, and sleeve seals (if any) each time the
tank is emptied and degassed and at least every five
years.
D)
Prior to each inspection required by subsection
(e)(3)(B) or (e)(3)(C) above, the owner or operator
shall notify the Agency in advance of each inspection
to provide the Agency with the opportunity to have an
observer present during the inspection. The owner or
operator shall notify the Agency of the date and
location of the inspection as follows:
i)
Prior to each visual inspection of an internal
floating roof in a tank that has been emptied
and degassed, written notification must be
prepared and sent by the owner or operator so
that it is received by the Agency at least 30
calendar days before refilling the tank, except
when an inspection is not planned, as provided
for in subsection (e)(3)(D)(ii) below.
ii)
When a visual inspection is not planned and the
owner or operator could not have known about the
inspection 30 calendar days before refilling the
tank, the owner or operator shall notify the
Agency as soon as possible, but no later than
seven calendar days before refilling of the
tank. This notification may be made by
telephone and immediately followed by a written
explanation for why the inspection is unplanned.
Alternatively, written notification, including
the explanation for the unplanned inspection,
may be sent so that it is received by the Agency
at least seven calendar days before refilling
the tank.
E)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
F)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 724.989(b).
f)
The owner or operator that controls air pollutant emissions from a
tank using an external floating roof must meet the requirements
specified in subsections (f)(1) through (f)(3) below.
1)
The owner or operator shall design the external floating
roof in accordance with the following requirements:
A)
The external floating roof must be designed to float
on the liquid surface except when the floating roof
must be supported by the leg supports.
B)
The floating roof must be equipped with two continuous
seals, one above the other, between the wall of the
tank and the roof edge. The lower seal is referred to
187
as the primary seal, and the upper seal is referred to
as the secondary seal.
i)
The primary seal must be a liquid
-mounted seal
or a metallic shoe seal, as defined in 35 Ill.
Adm. Code 725.981. The total area of the gaps
between the tank wall and the primary seal must
not exceed 212 square centimeters (cm
2
) per
meter (10.0 square inches (in
2
) per foot) of
tank diameter, and the width of any portion of
these gaps must not exceed 3.8 centimeters (cm)
(1.5 in). If a metallic shoe seal is used for
the primary seal, the metallic shoe seal must be
designed so that one end extends into the liquid
in the tank and the other end extends a vertical
distance of at least 61 cm (24 in) above the
liquid surface.
ii)
The secondary seal must be mounted above the
primary seal and cover the annular space between
the floating roof and the wall of the tank. The
total area of the gaps between the tank wall and
the secondary seal must not exceed 21.2 cm
2
per
meter (1.00 in
2
per foot) of tank diameter, and
the width of any portion of these gaps must not
exceed 1.3 cm (0.51 in).
C)
The external floating roof must meet the following
specifications:
i)
Except for automatic bleeder vents (vacuum
breaker vents) and rim space vents, each opening
in a noncontact external floating roof must
provide a projection below the liquid surface.
ii)
Except for automatic bleeder vents, rim space
vents, roof drains, and leg sleeves, each
opening in the roof must be equipped with a
gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must
be equipped with a cover designed to be bolted
or fastened when the cover is secured in the
closed position.
iv)
Each automatic bleeder vent and each rim space
vent must be equipped with a gasket.
v)
Each roof drain that empties into the liquid
managed in the tank must be equipped with a
slotted membrane fabric cover that covers at
least 90 percent of the area of the opening.
vi)
Each unslotted and slotted guide pole well must
be equipped with a
gasketed sliding cover or a
flexible fabric sleeve seal.
vii)
Each unslotted guide pole must be equipped with
a gasketed cap on the end of the pole.
viii)
Each slotted guide pole must be equipped with a
188
gasketed float or other device which closes off
the liquid surface from the atmosphere.
ix)
Each gauge hatch and each sample well must be
equipped with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance
with the following requirements:
A)
When the floating roof is resting on the leg supports,
the process of filling, emptying, or refilling must be
continuous and must be completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents,
roof drains, and leg sleeves, each opening in the roof
must be secured and maintained in a closed position at
all times except when the closure device must be open
for access.
C)
Covers on each access hatch and each gauge float well
must be bolted or fastened when secured in the closed
position.
D)
Automatic bleeder vents must be set closed at all
times when the roof is floating, except when the roof
is being floated off or is being landed on the leg
supports.
E)
Rim space vents must be set to open only at those
times that the roof is being floated off the roof leg
supports or when the pressure beneath the rim seal
exceeds the manufacturer's recommended setting.
F)
The cap on the end of each
unslotted guide pole must
be secured in the closed position at all times except
when measuring the level or collecting samples of the
liquid in the tank.
G)
The cover on each gauge hatch or sample well must be
secured in the closed position at all times except
when the hatch or well must be opened for access.
H)
Both the primary seal and the secondary seal must
completely cover the annular space between the
external floating roof and the wall of the tank in a
continuous fashion except during inspections.
3)
The owner or operator shall inspect the external floating
roof in accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external
floating roof seal gaps in accordance with the
following requirements:
i)
The owner or operator shall perform measurements
of gaps between the tank wall and the primary
seal within 60 calendar days after initial
operation of the tank following installation of
the floating roof and, thereafter, at least once
every five years.
189
ii)
The owner or operator shall perform measurements
of gaps between the tank wall and the secondary
seal within 60 calendar days after initial
operation of the tank following installation of
the floating roof and, thereafter, at least once
every year.
iii)
If a tank ceases to hold hazardous waste for a
period of one year or more, subsequent
introduction of hazardous waste into the tank
must be considered an initial operation for the
purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) above.
iv)
The owner or operator shall determine the total
surface area of gaps in the primary seal and in
the secondary seal individually using the
procedure of subsection (f)(3)(D) below.
v)
In the event that the seal gap measurements do
not conform to the specifications in subsection
(f)(1)(B) above, the owner or operator shall
repair the defect in accordance with the
requirements of subsection (k) below.
vi)
The owner or operator shall maintain a record of
the inspection in accordance with the
requirements specified in Section 724.989(b).
B)
The owner or operator shall visually inspect the
external floating roof in accordance with the
following requirements:
i)
The floating roof and its closure devices must
be visually inspected by the owner or operator
to check for defects that could result in air
pollutant emissions. Defects include, but are
not limited to any of the following conditions:
holes, tears, or other openings in the rim seal
or seal fabric of the floating roof; a rim seal
detached from the floating roof; all or a
portion of the floating roof deck being
submerged below the surface of the liquid in the
tank; broken, cracked, or otherwise damaged
seals or gaskets on closure devices; and broken
or missing hatches, access covers, caps, or
other closure devices.
ii)
The owner or operator shall perform an initial
inspection of the external floating roof and its
closure devices on or before the date that the
tank becomes subject to this Section.
Thereafter, the owner or operator shall perform
the inspections at least once every year except
for the special conditions provided for in
subsection (l) below.
iii)
In the event that a defect is detected, the
owner or operator shall repair the defect in
accordance with the requirements of subsection
(k) below.
190
iv)
The owner or operator shall maintain a record of
the inspection in accordance with the
requirements specified in Section 724.989(b).
C)
Prior to each inspection required by subsection
(f)(3)(A) or (f)(3)(B), the owner or operator shall
notify the Agency in advance of each inspection to
provide the Agency with the opportunity to have an
observer present during the inspection. The owner or
operator shall notify the Agency of the date and
location of the inspection as follows:
i)
Prior to each inspection to measure external
floating roof seal gaps as required under
subsection (f)(3)(A) above, written notification
must be prepared and sent by the owner or
operator so that it is received by the Agency at
least 30 calendar days before the date the
measurements are scheduled to be performed.
ii)
Prior to each visual inspection of an external
floating roof in a tank that has been emptied
and degassed, written notification must be
prepared and sent by the owner or operator so
that it is received by the Agency at least 30
calendar days before refilling the tank, except
when an inspection is not planned as provided
for in subsection (f)(3)(C)(iii) below.
iii)
When a visual inspection is not planned and the
owner or operator could not have known about the
inspection 30 calendar days before refilling the
tank, the owner or operator shall notify the
Agency as soon as possible, but no later than
seven calendar days before refilling of the
tank. This notification may be made by
telephone and immediately followed by a written
explanation for why the inspection is unplanned.
Alternatively, written notification, including
the explanation for the unplanned inspection,
may be sent so that it is received by the Agency
at least seven calendar days before refilling
the tank.
D)
Procedure for determining the total surface area of
gaps in the primary seal and the secondary seal:
i)
The seal gap measurements must be performed at
one or more floating roof levels when the roof
is floating off the roof supports.
ii)
Seal gaps, if any, must be measured around the
entire perimeter of the floating roof in each
place where a 0.32 cm (0.125 in) diameter
uniform probe passes freely (without forcing or
binding against the seal) between the seal and
the wall of the tank and measure the
circumferential distance of each such location.
iii)
For a seal gap measured under subsection (f)(3)
191
above, the gap surface area must be determined
by using probes of various widths to measure
accurately the actual distance from the tank
wall to the seal and multiplying each such width
by its respective
circumferential distance.
iv)
The total gap area must be calculated by adding
the gap surface areas determined for each
identified gap location for the primary seal and
the secondary seal individually, and then
dividing the sum for each seal type by the
nominal perimeter of the tank. These total gap
areas for the primary seal and secondary seal
are then compared to the respective standards
for the seal type, as specified in subsection
(f)(1)(B) above.
BOARD NOTE: Subsections (f)(3)(D)(i) through
(f)(3)(D)(iv) correspond with 40 CFR
264.1084(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4),
which the Board has codified here to comport
with Illinois Administrative Code format
requirements.
g)
The owner or operator that controls air pollutant emissions from a
tank by venting the tank to a control device shall meet the
requirements specified in subsections (g)(1) through (g)(3) below.
1)
The tank must be covered by a fixed roof and vented directly
through a closed -vent system to a control device in
accordance with the following requirements:
A)
The fixed roof and its closure devices must be
designed to form a continuous barrier over the entire
surface area of the liquid in the tank.
B)
Each opening in the fixed roof not vented to the
control device must be equipped with a closure device.
If the pressure in the vapor
headspace underneath the
fixed roof is less than atmospheric pressure when the
control device is operating, the closure devices must
be designed to operate such that when the closure
device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in
the closure device or between the perimeter of the
cover opening and the closure device. If the pressure
in the vapor headspace underneath the fixed roof is
equal to or greater than atmospheric pressure when the
control device is operating, the closure device must
be designed to operate with no detectable organic
emissions.
C)
The fixed roof and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and will maintain the integrity of the
fixed roof and closure devices throughout their
intended service life. Factors to be considered when
selecting the materials for and designing the fixed
roof and closure devices must include the following:
organic vapor permeability; the effects of any contact
192
with the liquid and its vapor managed in the tank; the
effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the
tank on which the fixed roof is installed.
D)
The closed -vent system and control device must be
designed and operated in accordance with the
requirements of Section 724.987.
2)
Whenever a hazardous waste is in the tank, the fixed roof
must be installed with each closure device secured in the
closed position and the vapor
headspace underneath the fixed
roof vented to the control device except as follows:
A)
Venting to the control device is not required, and
opening of closure devices or removal of the fixed
roof is allowed at the following times:
i)
To provide access to the tank for performing
routine inspection, maintenance, or other
activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to
open a hatch to maintain or repair equipment.
Following completion of the activity, the owner
or operator shall promptly secure the closure
device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues
from the bottom of a tank.
B)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air
emission control equipment in accordance with the following
procedures:
A)
The fixed roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to
any of the following: visible cracks, holes, or gaps
in the roof sections or between the roof and the tank
wall; broken, cracked, or otherwise damaged seals or
gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure
devices.
B)
The closed -vent system and control device must be
inspected and monitored by the owner or operator in
accordance with the procedures specified in Section
724.987.
C)
The owner or operator shall perform an initial
inspection of the air emission control equipment on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall
193
perform the inspections at least once every year
except for the special conditions provided for in
subsection (l) below.
D)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
E)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 724.989(b).
h)
The owner or operator that controls air pollutant emissions by
using a pressure tank must meet the following requirements.
1)
The tank must be designed not to vent to the atmosphere as a
result of compression of the vapor
headspace in the tank
during filling of the tank to its design capacity.
2)
All tank openings must be equipped with closure devices
designed to operate with no detectable organic emissions as
determined using the procedure specified in Section
724.983(d).
3)
Whenever a hazardous waste is in the tank, the tank must be
operated as a closed system that does not vent to the
atmosphere except in the event that a safety device, as
defined in 35 Ill. Adm. Code 725.981, is required to open to
avoid an unsafe condition.
i)
The owner or operator that controls air pollutant emissions by
using an enclosure vented through a closed
-vent system to an
enclosed combustion control device must meet the requirements
specified in subsections (i)(1) through (i)(4) below.
1)
The tank must be located inside an enclosure. The enclosure
must be designed and operated in accordance with the
criteria for a permanent total enclosure, as specified in
"Procedure T --Criteria for and Verification of a Permanent
or Temporary Total Enclosure" under 40 CFR 52.741, appendix
B, incorporated by reference in 35 Ill. Adm. Code 720.111.
The enclosure may have permanent or temporary openings to
allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means;
entry of permanent mechanical or electrical equipment; or
direct airflow into the enclosure. The owner or operator
shall perform the verification procedure for the enclosure,
as specified in Section 5.0 to "Procedure T
--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure", initially when the enclosure is first installed
and, thereafter, annually.
2)
The enclosure must be vented through a closed
-vent system to
an enclosed combustion control device that is designed and
operated in accordance with the standards for either a vapor
incinerator, boiler, or process heater specified in Section
724.987.
3)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may
be installed and operated as necessary on any enclosure,
closed -vent system, or control device used to comply with
194
the requirements of subsections (i)(1) and (i)(2) above.
4)
The owner or operator shall inspect and monitor the
closed -vent system and control device as specified in
Section 724.987.
j)
The owner or operator shall transfer hazardous waste to a tank
subject to this Section in accordance with the following
requirements:
1)
Transfer of hazardous waste, except as provided in
subsection (j)(2) below, to the tank from another tank
subject to this Section or from a surface impoundment
subject to Section 724.985 must be conducted using
continuous hard -piping or another closed system that does
not allow exposure of the hazardous waste to the atmosphere.
For the purpose of complying with this provision, an
individual drain system is considered to be a closed system
when it meets the requirements of 40 CFR 63, subpart RR,
"National Emission Standards for Individual Drain Systems",
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) above do not apply
when transferring a hazardous waste to the tank under any of
the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 724.982(c)(1) at the
point of waste origination.
B)
The hazardous waste has been treated by an organic
destruction or removal process to meet the
requirements in Section 724.982(c)(2).
k)
The owner or operator shall repair each defect detected during an
inspection performed in accordance with the requirements of
subsection (c)(4), (e)(3), (f)(3), or (g)(3) above, as follows:
1)
The owner or operator shall make first efforts at repair of
the defect no later than five calendar days after detection,
and repair must be completed as soon as possible but no
later than 45 calendar days after detection except as
provided in subsection (k)(2) below.
2)
Repair of a defect may be delayed beyond 45 calendar days if
the owner or operator determines that repair of the defect
requires emptying or temporary removal from service of the
tank and no alternative tank capacity is available at the
site to accept the hazardous waste normally managed in the
tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating
the hazardous waste managed in the tank stops operation.
Repair of the defect must be completed before the process or
unit resumes operation.
l)
Following the initial inspection and monitoring of the cover, as
required by the applicable provisions of this Subpart, subsequent
inspection and monitoring may be performed at intervals longer
than one year under the following special conditions:
1)
In the case when inspecting or monitoring the cover would
195
expose a worker to dangerous, hazardous, or other unsafe
conditions, then the owner or operator may designate a cover
as an "unsafe to inspect and monitor cover" and comply with
all of the following requirements:
A)
Prepare a written explanation for the cover stating
the reasons why the cover is unsafe to visually
inspect or to monitor, if required.
B)
Develop and implement a written plan and schedule to
inspect and monitor the cover, using the procedures
specified in the applicable Section of this Subpart,
as frequently as practicable during those times when a
worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely
underground, an owner or operator is required to inspect and
monitor, as required by the applicable provisions of this
Section, only those portions of the tank cover and those
connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground
surface.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.985
Standards: Surface
Impoundments
a) This Section applies to owners and operators of surface
impoundments subject to this Subpart into which any hazardous
waste is placed except for the following surface
impoundments:
1) A surface impoundment in which all hazardous waste entering
the surface impoundment meets the conditions specified in
Section 724.982(c); or
2) A surface impoundment used for biological treatment of
hazardous waste in accordance with the requirements of
Section 724.982(c)(2)(D).
b) The owner or operator shall place the hazardous waste into a
surface impoundment equipped with a cover (e.g., an air-supported
structure or a rigid cover) that is vented through a closed-vent
system to a control device meeting the requirements specified in
subsection (d) below.
c) As an alternative to complying with subsection (b) above, an owner
or operator may place hazardous waste in a surface impoundment
equipped with a floating membrane cover meeting the requirements
specified in subsection (e) below when the hazardous waste is
determined to meet all of the following conditions:
1) The hazardous waste is not mixed, stirred, agitated, or
circulated within the surface impoundment by the owner or
operator using a process that results in splashing,
frothing, or visible turbulent flow on the waste surface
during normal process operations;
2) The hazardous waste in the surface impoundment is not heated
by the owner or operator; and
3) The hazardous waste is not treated by the owner or operator
196
using a waste stabilization process or a process that
produces an exothermic reaction.
d) To comply with subsection (b)(1) above, the owner or operator
shall design, install, operate, and maintain a cover that vents
the organic vapors emitted from hazardous waste in the surface
impoundment through a closed-vent system connected to a control
device.
1) The cover shall be designed and operated to meet the
following requirements:
A) The cover and all cover openings (e.g., access
hatches, sampling ports, and gauge wells) shall be
designed to operate with no detectable organic
emissions when all cover openings are secured in a
closed, sealed position;
B) Each cover opening shall be secured in the closed,
sealed position (e.g., covered by a
gasketed lid or
cap) at all times that hazardous waste is in the
surface impoundment, except as provided for in
subsection (g) below; and
C) The closed-vent system and control device shall be
designed and operated in accordance with Section
724.987.
e) To comply wit h subsection (c) above, the owner or operator shall
design, install, operate, and maintain a floating membrane cover
that meets all of the requirements specified in 35 Ill. Adm. Code
725.986(e)(1) through (e)(4).
f) The owner or operator shall install, operate, and maintain
enclosed pipes or other closed-systems to
BOARD NOTE: U.S. EPA considers a drain system that meets the
requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
a "closed-system". The Board intends that this meaning be
included in the use of that term for the purposes of this Subpart.
1) Transfer all hazardous waste to the surface impoundment from
another tank, surface impoundment, or container subject to
this Subpart except for those hazardous wastes that meet the
conditions specified in Section 724.982(c); and
2) Transfer all hazardous waste from the surface impoundment to
another tank, surface impoundment, or container subject to
this Subpart except for those hazardous wastes that meet the
conditions specified in Section 724.982(c).
g) Each cover opening shall be secured in the closed, sealed position
(e.g., a cover by a
gasketed lid or cap) at all times that
hazardous waste is in the surface impoundment except when it is
necessary to use the cover opening to:
1) Add, remove, inspect, or sample the material in the surface
impoundment;
2) Inspect, maintain, repair, or replace equipment located
underneath the cover;
197
3) Remove treatment residues from the surface impoundment in
accordance with the requirements of 35 Ill. Adm. Code 728.4;
or
4) Vent gases or vapors from the surface impoundment to a
closed-vent system connected to a control device that is
designed and operated in accordance with the requirements of
Section 724.987.
h) One or more safety devices that vent directly to the atmosphere
may be installed on the cover, closed-vent system, or control
device provided each device meets all of the following conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the surface impoundment or the
closed-vent system connected to a control device; and
2) The safety device remains in a closed, sealed position at
all times, except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the cover, closed-vent system, or
control device in accordance with good engineering and
safety practices for handling flammable, combustible,
explosive, or other hazardous materials. An example of an
unplanned event is a sudden power outage.
a)
The provisions of this Section apply to the control of air
pollutant emissions from surface
impoundments for which Section
724.982(b) references the use of this Section for such air
emission control.
b)
The owner or operator shall control air pollutant emissions from
the surface impoundment by installing and operating either of the
following:
1)
A floating membrane cover in accordance with the provisions
specified in subsection (c) below; or
2)
A cover that is vented through a closed
-vent system to a
control device in accordance with the provisions specified
in subsection (d) below.
c)
The owner or operator that controls air pollutant emissions from a
surface impoundment using a floating membrane cover must meet the
requirements specified in subsections (c)(1) through (c)(3) below.
1)
The surface impoundment must be equipped with a floating
membrane cover designed to meet the following
specifications:
A)
The floating membrane cover must be designed to float
on the liquid surface during normal operations and
form a continuous barrier over the entire surface area
of the liquid.
B)
The cover must be fabricated from a synthetic membrane
material that is either:
i)
High density polyethylene (HDPE) with a
thickness no less than 2.5 millimeters (mm)
198
(0.098 in); or
ii)
A material or a composite of different materials
determined to have both organic permeability
properties that are equivalent to those of the
material listed in subsection (c)(1)(B)(i) above
and chemical and physical properties that
maintain the material integrity for the intended
service life of the material.
C)
The cover must be installed in such a manner that
there are no visible cracks, holes, gaps, or other
open spaces between cover section seams or between the
interface of the cover edge and its foundation
mountings.
D)
Except as provided for in subsection (c)(1)(E) below,
each opening in the floating membrane cover must be
equipped with a closure device so designed as to
operate that when the closure device is secured in the
closed position there are no visible cracks, holes,
gaps, or other open spaces in the closure device or
between the perimeter of the cover opening and the
closure device.
E)
The floating membrane cover may be equipped with one
or more emergency cover drains for removal of
stormwater. Each emergency cover drain must be
equipped with a slotted membrane fabric cover that
covers at least 90 percent of the area of the opening
or a flexible fabric sleeve seal.
F)
The closure devices must be made of suitable materials
that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will
maintain the integrity of the closure devices
throughout their intended service life. Factors to be
considered when selecting the materials of
construction and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the
liquid and its vapor managed in the surface
impoundment; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
used for the surface impoundment on which the floating
membrane cover is installed.
2)
Whenever a hazardous waste is in the surface impoundment,
the floating membrane cover must float on the liquid and
each closure device must be secured in the closed position,
except as follows:
A)
Opening of closure devices or removal of the cover is
allowed at the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or
other activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample the
liquid in the surface impoundment, or when a
199
worker needs to open a hatch to maintain or
repair equipment. Following completion of the
activity, the owner or operator shall promptly
replace the cover and secure the closure device
in the closed position, as applicable.
ii)
To remove accumulated sludge or other residues
from the bottom of surface impoundment.
B)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
3)
The owner or operator shall inspect the floating membrane
cover in accordance with the following procedures:
A)
The floating membrane cover and its closure devices
must be visually inspected by the owner or operator to
check for defects that could result in air pollutant
emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the cover section
seams or between the interface of the cover edge and
its foundation mountings; broken, cracked, or
otherwise damaged seals or gaskets on closure devices;
and broken or missing hatches, access covers, caps, or
other closure devices.
B)
The owner or operator shall perform an initial
inspection of the floating membrane cover and its
closure devices on or before the date that the surface
impoundment becomes subject to this Section.
Thereafter, the owner or operator shall perform the
inspections at least once every year except for the
special conditions provided for in subsection (g)
below.
C)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (f) below.
D)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 724.989(c).
d)
The owner or operator that controls air pollutant emissions from a
surface impoundment using a cover vented to a control device shall
meet the requirements specified in subsections (d)(1) through
(d)(3) below.
1)
The surface impoundment must be covered by a cover and
vented directly through a closed
-vent system to a control
device in accordance with the following requirements:
A)
The cover and its closure devices must be designed to
form a continuous barrier over the entire surface area
of the liquid in the surface impoundment.
B)
Each opening in the cover not vented to the control
device must be equipped with a closure device. If the
pressure in the vapor
headspace underneath the cover
is less than atmospheric pressure when the control
200
device is operating, the closure devices must be
designed to operate such that when the closure device
is secured in the closed position there are no visible
cracks, holes, gaps, or other open spaces in the
closure device or between the perimeter of the cover
opening and the closure device. If the pressure in
the vapor headspace underneath the cover is equal to
or greater than atmospheric pressure when the control
device is operating, the closure device must be
designed to operate with no detectable organic
emissions using the procedure specified in Section
724.983(d).
C)
The cover and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and will maintain the integrity of the
cover and closure devices throughout their intended
service life. Factors to be considered when selecting
the materials for and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the
liquid or its vapors managed in the surface
impoundment; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
used for the surface impoundment on which the cover is
installed.
D)
The closed -vent system and control d
evice must be
designed and operated in accordance with the
requirements of Section 724.987.
2)
Whenever a hazardous waste is in the surface impoundment,
the cover must be installed with each closure device secured
in the closed position and the vapor
headspace underneath
the cover vented to the control device except as follows:
A)
Venting to the control device is not required, and
opening of closure devices or removal of the cover is
allowed at the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or
other activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample
liquid in the surface impoundment, or when a
worker needs to open a hatch to maintain or
repair equipment. Following completion of the
activity, the owner or operator shall promptly
secure the closure device in the closed position
or reinstall the cover, as applicable, to the
surface impoundment.
ii)
To remove accumulated sludge or other residues
from the bottom of surface impoundment.
B)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
201
3)
The owner or operator shall inspect and monitor the air
emission control equipment in accordance with the following
procedures:
A)
The surface impoundment cover and its closure devices
shall be visually inspected by the owner or operator
to check for defects that could result in air
pollutant emissions. Defects include, but are not
limited to, visible cracks, holes, or gaps in the
cover section seams or between the interface of the
cover edge and its foundation mountings; broken,
cracked, or otherwise damaged seals or gaskets on
closure devices; and broken or missing hatches, access
covers, caps, or other closure devices.
B)
The closed -vent system and control device must be
inspected and monitored by the owner or operator in
accordance with the procedures specified in Section
724.987.
C)
The owner or operator shall perform an initial
inspection of the air emission control equipment on or
before the date that the surface impoundment becomes
subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once
every year except for the special conditions provided
for in subsection (g) below.
D)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (f) below.
E)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 724.989(c).
e)
The owner or operator shall transfer hazardous waste to a surface
impoundment subject to this Section in accordance with the
following requirements:
1)
Transfer of hazardous waste, except as provided in
subsection (e)(2) below, to the surface impoundment from
another surface impoundment subject to this Section or from
a tank subject to Section 724.984 must be conducted using
continuous hard-piping or another closed system that does
not allow exposure of the waste to the atmosphere. For the
purpose of complying with this provision, an individual
drain system is considered to be a closed system when it
meets the requirements of 40 CFR 63, Subpart RR, "National
Emission Standards for Individual Drain Systems",
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (e)(1) above do not apply
when transferring a hazardous waste to the surface
impoundment under either of the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 724.982(c)(1) at the
point of waste origination.
B)
The hazardous waste has been treated by an organic
202
destruction or removal process to meet the
requirements in Section 724.982(c)(2).
f)
The owner or operator shall repair each defect detected during an
inspection performed in accordance with the requirements of
subsection (c)(3) or (d)(3) above as follows:
1)
The owner or operator shall make first efforts at repair of
the defect no later than five calendar days after detection
and repair must be completed as soon as possible but no
later than 45 calendar days after detection except as
provided in subsection (f)(2) below.
2)
Repair of a defect may be delayed beyond 45 calendar days if
the owner or operator determines that repair of the defect
requires emptying or temporary removal from service of the
surface impoundment and no alternative capacity is available
at the site to accept the hazardous waste normally managed
in the surface impoundment. In this case, the owner or
operator shall repair the defect the next time the process
or unit that is generating the hazardous waste managed in
the surface impoundment stops operation. Repair of the
defect must be completed before the process or unit resumes
operation.
g)
Following the initial inspection and monitoring of the cover as
required by the applicable provisions of this Subpart, subsequent
inspection and monitoring may be performed at intervals longer
than one year in the case when inspecting or monitoring the cover
would expose a worker to dangerous, hazardous, or other unsafe
conditions. In this case, the owner or operator may designate the
cover as an "unsafe to inspect and monitor cover" and comply with
all of the following requirements:
1)
Prepare a written explanation for the cover stating the
reasons why the cover is unsafe to visually inspect or to
monitor, if required.
2)
Develop and implement a written plan and schedule to inspect
and monitor the cover using the procedures specified in the
applicable Section of this Subpart as frequently as
practicable during those times when a worker can safely
access the cover.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.986
Standards: Containers
a) This Section applies to the owners and operators of containers
having design capacities greater than 0.1 m
3
(3.5 ft
3
or 26.4 gal)
subject to this Subpart into which any hazardous waste is placed
except for a container in which all hazardous waste entering the
container meets the conditions specified in Section 724.982(c).
b) An owner or operator shall manage hazardous waste in containers
using the following procedures:
1) The owner or operator shall place the hazardous waste into
one of the following containers, except when a container is
used for hazardous waste treatment as required by subsection
(b)(2) below:
203
A) A container that is equipped with a cover which
operates with no detectable organic emissions when all
container openings (e.g., lids, bungs, hatches, and
sampling ports) are secured in a closed, sealed
position. The owner or operator shall determine that
a container operates with no detectable emissions by
testing each opening on the container for leaks in
accordance with Method 21 in 40 CFR 60, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, the first time any portion of the hazardous
waste is placed into the container. If a leak is
detected and cannot be repaired immediately, the
hazardous waste shall be removed from the container
and the container not used to meet the requirements of
this subsection until the leak is repaired and the
container is retested.
B) A container having a design capacity less than or
equal to 0.46 m
3
(16.2 ft
3
or 122 gal) that is
equipped with a cover and complies with all applicable
Department of Transportation regulations on packaging
hazardous waste for transport under 49 CFR 178,
incorporated by reference at 35 Ill. Adm. Code
720.111.
i) A container that is managed in accordance with
the requirements of 49 CFR 178, incorporated by
reference at 35 Ill. Adm. Code 720.111, for the
purpose of complying with this Subpart, is not
subject to any exceptions to the 49 CFR 178
regulations, except as noted in subsection
(b)(1)(B)(ii) below.
ii) A lab pack that is managed in accordance with
the requirements of 49 CFR 178, incorporated by
reference at 35 Ill. Adm. Code 720.111, for the
purpose of complying with this Subpart, may
comply with the exceptions for combination
packagings specified in 49 CFR 173.12(b),
incorporated by reference at 35 Ill. Adm. Code
720.111.
C) A container that is attached to or forms a part of any
truck, trailer, or
railcar and that has been
demonstrated within the preceding 12 months to be
organic vapor tight when all container openings are in
a closed, sealed position (e.g., the container hatches
or lids are gasketed and latched). For the purpose of
meeting the requirements of this subsection, a
container is organic vapor tight if the container
sustains a pressure change of not more than 0.75
kPa
(0.11 psig or 5.6 mm Hg) within 5 minutes after it is
pressurized to a minimum of 4.50
kPa (0.65 psig or
33.7 mm Hg). This condition is to be demonstrated
using the pressure test specified in Method 27 of 40
CFR 60, Appendix A, and a pressure measurement device
which has a precision of ยฑ2.5 mm water and which is
capable of measuring above the pressure at which the
container is to be tested for vapor tightness.
204
2) An owner or operator treating hazardous waste in a container
by either a waste stabilization process, any process that
requires the addition of heat to the waste, or any process
that produces an exothermic reaction shall meet the
following requirements:
A) Whenever it is necessary for the container to be open
during the treatment process, the container shall be
located inside an enclosure that is vented through a
closed-vent system to a control device.
B) The enclosure shall be a structure that is designed
and operated in accordance with the following
requirements:
i) The enclosure shall be a structure that is
designed and operated with sufficient airflow
into the structure to capture the organic vapors
emitted from the hazardous waste in the
container and vent the vapors through the
closed-vent system to the control device.
ii) The enclosure may have permanent or temporary
openings to allow worker access, passage of
containers through the enclosure by conveyor or
other mechanical means, entry of permanent
mechanical or electrical equipment, or to direct
airflow into the enclosure. The pressure drop
across each opening in the enclosure shall be
maintained at a pressure below atmospheric
pressure so that whenever an open container is
placed inside the enclosure no organic vapors
released from the container exit the enclosure
through the opening. The owner or operator
shall determine that an enclosure achieves this
condition by measuring the pressure drop across
each opening in the enclosure. If the pressure
within the enclosure is equal to or greater than
atmospheric pressure then the enclosure does not
meet the requirements of this Section.
C) The closed-vent system and control device shall be
designed and operated in accordance with the
requirements of Section 724.987.
3) An owner or operator transferring hazardous waste into a
container having a design capacity greater than 0.46 m
3
(16.2 ft
3
or 122 gal) shall meet the following requirements:
A) Hazardous waste transfer by pumping shall be performed
using a conveyance system that uses a tube (e.g.,
pipe, hose) to add the waste into the container.
During transfer of the waste into the container, the
cover shall remain in place and all container openings
shall be maintained in a closed, sealed position
except for those openings through which the tube
enters the container and as provided for in subsection
(c) below. The tube shall be positioned in a manner
so that:
i) The tube outlet continuously remains submerged
205
below the waste surface at all times waste is
flowing through the tube;
ii) The lower bottom edge of the tube outlet is
located at a distance no greater than two inside
diameters of the tube or 15.25 cm (6.0 in),
whichever distance is greater, from the bottom
of the container at all times waste is flowing
through the tube; or
iii) The tube is connected to a permanent port
mounted on the bottom of the container so that
the lower edge of the port opening inside the
container is located at a distance equal to or
less than 15.25 cm (6.0 in) from the container
bottom.
B) Hazardous waste transferred by a means other than
pumping shall be performed such that during transfer
of the waste into the container, the cover remains in
place and all container openings are maintained in a
closed, sealed position except for those openings
through which the hazardous waste is added and as
provided for in subsection (d) below.
c) Each con tainer opening shall be maintained in a closed, sealed
position (e.g., covered by a
gasketed lid) at all times that
hazardous waste is in the container except when it is necessary to
use the opening to:
1) Add, remove, inspect, or sample the material in the
container;
2) Inspect, maintain, repair, or replace equipment located
inside the container; or
3) Vent gases or vapors from a cover located over or enclosing
an open container to a closed-vent system connected to a
control device that is designed and operated in accordance
with the requirements of Section 724.987.
d) One or more safety devices that vent directly to the atmosphere
may be used on the container, cover, enclosure, closed-vent
system, or control device provided each device meets all of the
following conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the container, cover, enclosure, or
closed-vent system connected to a control device; and
2) The safety device remains in a closed, s
ealed position at
all times except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the container, cover, enclosure,
closed-vent system, or control device in accordance with
good engineering and safety practices for handling
flammable, combustible, explosive, or other hazardous
materials. An example of an unplanned event is a sudden
power outage.
a)
The provisions of this Section apply to the control of air
206
pollutant emissions from containers for which Section 724.982(b)
references the use of this Section for such air emission control.
b)
General requirements.
1)
The owner or operator shall control air pollutant emissions
from each container subject to this Section in accordance
with the following requirements, as applicable to the
container, except when the special provisions for waste
stabilization processes specified in subsection (b)(2) below
apply to the container.
A)
For a container having a design capacity greater than
0.1 m
3
(26 gal) and less than or equal to 0.46 m
3
(120
gal), the owner or operator shall control air
pollutant emissions from the container in accordance
with the Container Level 1 standards specified in
subsection (c) below.
B)
For a container having a design capacity greater than
0.46 m
3
(120 gal) that is not in light material
service, the owner or operator shall control air
pollutant emissions from the container in accordance
with the Container Level 1 standards specified in
subsection (c) below.
C)
For a container having a design capacity greater than
0.46 m
3
(120 gal) that is in light material service,
the owner or operator shall control air pollutant
emissions from the container in accordance with the
Container Level 2 standards specified in subsection
(d) below.
2)
When a container having a design capacity greater than 0.1
m
3
(26 gal) is used for treatment of a hazardous waste by a
waste stabilization process, the owner or operator shall
control air pollutant emissions from the container in
accordance with the Container Level 3 standards specified in
subsection (e) below at those times during the waste
stabilization process when the hazardous waste in the
container is exposed to the atmosphere.
c)
Container Level 1 standards.
1)
A container using Container Level 1 controls is one of the
following:
A)
A container that meets the applicable U.S. Department
of Transportation (USDOT) regulations on packaging
hazardous materials for transportation, as specified
in subsection (f) below.
B)
A container equipped with a cover and closure devices
that form a continuous barrier over the container
openings so that when the cover and closure devices
are secured in the closed position there are no
visible holes, gaps, or other open spaces into the
interior of the container. The cover may be a
separate cover installed on the container (e.g., a lid
on a drum or a suitably secured tarp on a roll-off
box) or may be an integral part of the container
207
structural design (e.g., a "portable tank" or bulk
cargo container equipped with a screw
-type cap).
C)
An open -top container in which an organic
-vapor
suppressing barrier is placed on or over the hazardous
waste in the container such that no hazardous waste is
exposed to the atmosphere. One example of such a
barrier is application of a suitable organic
-vapor
suppressing foam.
2)
A container used to meet the requirements of subsection
(c)(1)(B) or (c)(1)(C) above must be equipped with covers
and closure devices, as applicable to the container, that
are composed of suitable materials to minimize exposure of
the hazardous waste to the atmosphere and to maintain the
equipment integrity for as long as it is in service.
Factors to be considered in selecting the materials of
construction and designing the cover and closure devices
must include the following: the organic vapor permeability;
the effects of contact with the hazardous waste or its vapor
managed in the container; the effects of outdoor exposure of
the closure device or cover material to wind, moisture, and
sunlight; and the operating practices for which the
container is intended to be used.
3)
Whenever a hazardous waste is in a container using Container
Level 1 controls, the owner or operator shall install all
covers and closure devices for the container, as applicable
to the container, and secure and maintain each closure
device in the closed position except as follows:
A)
Opening of a closure device or cover is allowed for
the purpose of adding hazardous waste or other
material to the container as follows:
i)
In the case when the container is filled to the
intended final level in one continuous
operation, the owner or operator shall promptly
secure the closure devices in the closed
position and install the covers, as applicable
to the container, upon conclusion of the filling
operation.
ii)
In the case when discrete quantities or batches
of material intermittently are added to the
container over a period of time, the owner or
operator shall promptly secure the closure
devices in the closed position and install
covers, as applicable to the container, upon
either the container being filled to the
intended final level; the completion of a batch
loading after which no additional material will
be added to the container within 15 minutes; the
person performing the loading operation leaving
the immediate vicinity of the container; or the
shutdown of the process generating the material
being added to the container, whichever
condition occurs first.
B)
Opening of a closure device or cover is allowed for
the purpose of removing hazardous waste from the
208
container as follows:
i)
For the purpose of meeting the requirements of
this Section, an empty container, as defined in
35 Ill. Adm. Code 721.107(b), may be open to the
atmosphere at any time (i.e., covers and closure
devices are not required to be secured in the
closed position on an empty container).
ii)
In the case when discrete quantities or batches
of material are removed from the container but
the container does not meet the conditions to be
an empty container as defined in 35 Ill. Adm.
Code 721.107(b), the owner or operator shall
promptly secure the closure devices in the
closed position and install covers, as
applicable to the container, upon the completion
of a batch removal after which no additional
material will be removed from the container
within 15 minutes or the person performing the
unloading operation leaves the immediate
vicinity of the container, whichever condition
occurs first.
C)
Opening of a closure device or cover is allowed when
access inside the container is needed to perform
routine activities other than transfer of hazardous
waste. Examples of such activities include those
times when a worker needs to open a port to measure
the depth of or sample the material in the container,
or when a worker needs to open a manhole hatch to
access equipment inside the container. Following
completion of the activity, the owner or operator
shall promptly secure the closure device in the closed
position or reinstall the cover, as applicable to the
container.
D)
Opening of a spring
-loaded pressure -vacuum relief
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the internal pressure of the container in
accordance with the container design specifications.
The device must be designed to operate with no
detectable organic emissions when the device is
secured in the closed position. The settings at which
the device opens must be established such that the
device remains in the closed position whenever the
internal pressure of the container is within the
internal pressure operating range determined by the
owner or operator based on container manufacturer
recommendations, applicable regulations, fire
protection and prevention codes, standard engineering
codes and practices, or other requirements for the
safe handling of flammable, ignitable, explosive,
reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to
open are during those times when the internal pressure
of the container exceeds the internal pressure
operating range for the container as a result of
loading operations or diurnal ambient temperature
209
fluctuations.
E)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 1
controls shall inspect the containers and their covers and
closure devices as follows:
A)
In the case when a hazardous waste already is in the
container at the time the owner or operator first
accepts possession of the container at the facility
and the container is not emptied (i.e., does not meet
the conditions for an empty container as specified in
35 Ill. Adm. Code 721.107(b)) within 24 hours after
the container is accepted at the facility, the owner
or operator shall visually inspect the container and
its cover and closure devices to check for visible
cracks, holes, gaps, or other open spaces into the
interior of the container when the cover and closure
devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair
the defect in accordance with the requirements of
subsection (c)(4)(C) below.
B)
In the case when a container used for managing
hazardous waste remains at the facility for a period
of one year or more, the owner or operator shall
visually inspect the container and its cover and
closure devices initially and thereafter, at least
once every 12 months, to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (c)(4)(C) below.
C)
When a defect is detected for the container, cover, or
closure devices, the owner or operator shall make
first efforts at repair of the defect no later than 24
hours after detection and repair must be completed as
soon as possible but no later than five calendar days
after detection. If repair of a defect cannot be
completed within five calendar days, then the
hazardous waste must be removed from the container and
the container must not be used to manage hazardous
waste until the defect is repaired.
5)
The owner or operator shall maintain at the facility a copy
of the procedure used to determine that containers with
capacity of 0.46 m
3
(120 gal) or greater, which do not meet
applicable DOT regulations, as specified in subsection (f)
below, are not managing hazardous waste in light material
service.
d)
Container Level 2 standards.
1)
A container using Container Level 2 controls is one of the
following:
210
A)
A container that meets the applicable U.S. Department
of Transportation (USDOT) regulations on packaging
hazardous materials for transportation as specified in
subsection (f) below.
B)
A container that operates with no detectable organic
emissions, as defined in 35 Ill. Adm. Code 725.981,
and determined in accordance with the procedure
specified in subsection (g) below.
C)
A container that has been demonstrated within the
preceding 12 months to be vapor
-tight by using 40 CFR
60, appendix A, Method 27, incorporated by reference
in 35 Ill. Adm. Code 720.111, in accordance with the
procedure specified in subsection (h) below.
2)
Transfer of hazardous waste in or out of a container using
Container Level 2 controls must be conducted in such a
manner as to minimize exposure of the hazardous waste to the
atmosphere, to the extent practical, considering the
physical properties of the hazardous waste and good
engineering and safety practices for handling flammable,
ignitable, explosive, reactive, or other hazardous
materials. Examples of container loading procedures that
the EPA considers to meet the requirements of this
subsection include using any one of the following: a
submerged -fill pipe or other sub
merged -fill method to load
liquids into the container; a vapor
-balancing system or a
vapor-recovery system to collect and control the vapors
displaced from the container during filling operations; or a
fitted opening in the top of a container through which the
hazardous waste is filled and subsequently purging the
transfer line before removing it from the container opening.
3)
Whenever a hazardous waste is in a container using Container
Level 2 controls, the owner or operator shall install all
covers and closure devices for the container, and secure and
maintain each closure device in the closed position, except
as follows:
A)
Opening of a closure device or cover is allowed for
the purpose of adding hazardous waste or other
material to the container as follows:
i)
In the case when the container is filled to the
intended final level in one continuous
operation, the owner or operator shall promptly
secure the closure devices in the closed
position and install the covers, as applicable
to the container, upon conclusion of the filling
operation.
ii)
In the case when discrete quantities or
batches of material intermittently are
added to the container over a period of
time, the owner or operator shall promptly
secure the closure devices in the closed
position and install covers, as applicable
to the container, upon either the
container being filled to the intended
211
final level; the completion of a batch
loading after which no additional material
will be added to the container within 15
minutes; the person performing the loading
operation leaving the immediate vicinity
of the container; or the shutdown of the
process generating the material being
added to the container, whichever
condition occurs first.
B)
Opening of a closure device or cover is allowed for
the purpose of removing hazardous waste from the
container as follows:
i)
For the purpose of meeting the requirements of
this Section, an empty container as defined in
35 Ill. Adm. Code 721.107(b) may be open to the
atmosphere at any time (i.e., covers and closure
devices are not required to be secured in the
closed position on an empty container).
ii)
In the case when discrete quantities or batches
of material are removed from the container but
the container does not meet the conditions to be
an empty container as defined in 35 Ill. Adm.
Code 721.107(b), the owner or operator shall
promptly secure the closure devices in the
closed position and install covers, as
applicable to the container, upon the completion
of a batch removal after which no additional
material will be removed from the container
within 15 minutes or the person performing the
unloading operation leaves the immediate
vicinity of the container, whichever condition
occurs first.
C)
Opening of a closure device or cover is allowed when
access inside the container is needed to perform
routine activities other than transfer of hazardous
waste. Examples of such activities include those
times when a worker needs to open a port to measure
the depth of or sample the material in the container,
or when a worker needs to open a manhole hatch to
access equipment inside the container. Following
completion of the activity, the owner or operator
shall promptly secure the closure device in the closed
position or reinstall the cover, as applicable to the
container.
D)
Opening of a spring
-loaded, pressure
-vacuum relief
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the internal pressure of the container in
accordance with the container design specifications.
The device must be designed to operate with no
detectable organic emission when the device is secured
in the closed position. The settings at which the
device opens must be established such that the device
remains in the closed position whenever the internal
pressure of the container is within the internal
212
pressure operating range determined by the owner or
operator based on container manufacturer
recommendations, applicable regulations, fire
protection and prevention codes, standard engineering
codes and practices, or other requirements for the
safe handling of flammable, ignitable, explosive,
reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to
open are during those times when the internal pressure
of the container exceeds the internal pressure
operating range for the container as a result of
loading operations or diurnal ambient temperature
fluctuations.
E)
Opening of a safety device, as defined in 35 Ill. Adm.
Code 725.981, is allowed at any time conditions
require doing so to avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 2
controls shall inspect the containers and their covers and
closure devices as follows:
A)
In the case when a hazardous waste already is in the
container at the time the owner or operator first
accepts possession of the container at the facility
and the container is not emptied (i.e., does not meet
the conditions for an empty container as specified in
35 Ill. Adm. Code 721.107(b)) within 24 hours after
the container arrives at the facility, the owner or
operator shall visually inspect the container and its
cover and closure devices to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (d)(4)(C) below.
B)
In the case when a container used for managing
hazardous waste remains at the facility for a period
of one year or more, the owner or operator shall
visually inspect the container and its cover and
closure devices initially and thereafter, at least
once every 12 months, to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (d)(4)(C) below.
C)
When a defect is detected for the container, cover, or
closure devices, the owner or operator shall make
first efforts at repair of the defect no later than 24
hours after detection, and repair must be completed as
soon as possible but no later than five calendar days
after detection. If repair of a defect cannot be
completed within five calendar days, then the
hazardous waste must be removed from the container and
the container must not be used to manage hazardous
waste until the defect is repaired.
213
e)
Container Level 3 standards.
1)
A container using Container Level 3 controls is one of the
following:
A)
A container that is vented directly through a
closed -vent system to a control device in accordance
with the requirements of subsection (e)(2)(B) below.
B)
A container that is vented inside an enclosure which
is exhausted through a closed
-vent system to a control
device in accordance with the requirements of
subsections (e)(2)(A) and (e)(2)(B) below.
2)
The owner or operator shall meet the following requirements,
as applicable to the type of air emission control equipment
selected by the owner or operator:
A)
The container enclosure must be designed and operated
in accordance with the criteria for a permanent total
enclosure as specified in "Procedure T
--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111. The enclosure may have permanent or
temporary openings to allow worker access; passage of
containers through the enclosure by conveyor or other
mechanical means; entry of permanent mechanical or
electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the
verification procedure for the enclosure as specified
in Section 5.0 to "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" initially when the enclosure is first
installed and, thereafter, annually.
B)
The closed -vent system and control device must be
designed and operated in accordance with the
requirements of Section 724.987.
3)
Safety devices, as defined in 35 Ill. Adm. Code 725.981, may
be installed and operated as necessary on any container,
enclosure, closed
-vent system, or control device used to
comply with the requirements of subsection (e)(1) above.
4)
Owners and operators using Container Level 3 controls in
accordance with the provisions of this Subpart shall inspect
and monitor the closed
-vent systems and control devices as
specified in Section 724.987.
5)
Owners and operators that use Container Level 3 controls in
accordance with the provisions of this Subpart shall prepare
and maintain the records specified in Section 724.989(d).
f)
For the purpose of compliance with subsection (c)(1)(i) or
(d)(1)(A) above, containers must be used that meet the applicable
U.S. Department of Transportation (DOT) regulations on packaging
hazardous materials for transportation as follows:
1)
The container meets the applicable requirements specified in
214
49 CFR 178, "Specifications for Packaging", or 49 CFR 179,
"Specifications for Tank Cars", both incorporated by
reference in 35 Ill. Adm. Code 720.111.
2)
Hazardous waste is managed in the container in accordance
with the applicable requirements specified in 49 CFR 107,
Subpart B, "Exemptions"; 49 CFR 172, "Hazardous Materials
Table, Special Provisions, Hazardous Materials
Communications, Emergency Response Information, and Training
Requirements"; 49 CFR 173, "
Shippers --General Requirements
for Shipments and Packages"; and 49 CFR 180, "Continuing
Qualification and Maintenance of
Packagings", each
incorporated by reference in 35 Ill. Adm. Code 720.111.
3)
For the purpose of complying with this Subpart, no
exceptions to the 49 CFR 178 or 179 regulations are allowed,
except as provided for in subsection (f)(4) below.
4)
For a lab pack that is managed in accordance with the
requirements of 49 CFR 178, incorporated by reference in 35
Ill. Adm. Code 720.111, for the purpose of complying with
this Subpart, an owner or operator may comply with the
exceptions for combination
packagings specified in 49 CFR
173.12(b).
g)
The owner or operator shall use the procedure specified in Section
724.983(d) for determining a container operates with no detectable
organic emissions for the purpose of complying with subsection
(d)(1)(B) above.
1)
Each potential leak interface (i.e., a location where
organic vapor leakage could occur) on the container, its
cover, and associated closure devices, as applicable to the
container, must be checked. Potential leak interfaces that
are associated with containers include, but are not limited
to the following: the interface of the cover rim and the
container wall; the periphery of any opening on the
container or container cover and its associated closure
device; and the sealing seat interface on a spring
-loaded
pressure -relief valve.
2)
The test must be performed when the container is filled with
a material having a volatile organic concentration
representative of the range of volatile organic
concentrations for the hazardous wastes expected to be
managed in this type of container. During the test, the
container cover and closure devices must be secured in the
closed position.
h)
Procedure for determining a container to be vapor
-tight using
Method 27 of 40 CFR 60, appendix A for the purpose of complying
with subsection (d)(1)(C) above.
1)
The test must be performed in accordance with Method 27 of
40 CFR 60, appendix A, incorporated by reference in 35 Ill.
Adm. Code 720.111.
2)
A pressure measurement device must be used that has a
precision of ยฑ 2.5 mm (0.098 in) water and that is capable
of measuring above the pressure at which the container is to
be tested for vapor tightness.
215
3)
If the test results determined by Method 27 indicate that
the container sustains a pressure change less than or equal
to 750 Pascals (0.11 psig) within five minutes after it is
pressurized to a minimum of 4,500
Pascals (0.65 psig), then
the container is determined to be vapor
-tight.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.987
Standards: Closed-vent Systems and Control Devices
a)
This Section applies to each closed-vent system and control device
installed and operated by the owner or operator to control air
emissions in accordance with standards of this Subpart.
b)
The closed-vent system shall meet the following req
uirements:
1)
The closed-vent system shall route the gases, vapors, and
fumes emitted from the hazardous waste in the waste
management unit to a control device that meets the
requirements specified in subsection (c) below.
2)
The closed-vent system shall be designed and operated in
accordance with the requirements specified in Section
724.933(k).
3) If the closed-vent system contains one or more bypass
devices that could be used to divert all or a portion of the
gases, vapors, or fumes from entering the control device,
the owner or operator shall meet the following requirements:
A) For each bypass device, except as provided for in
subsection (b)(3)(B) below, the owner or operator
shall either:
i) Install, calibrate, maintain, and operate a flow
indicator at the inlet to the bypass device that
indicates at least once every 15 minutes whether
gas, vapor, or fume flow is present in the
bypass device; or
ii) Secure a valve installed at the inlet to the
bypass device in the closed position using a
car-seal or a lock-and-key type configuration.
The owner or operator shall visually inspect the
seal or closure mechanism at least once every
month to verify that the valve is maintained in
the closed position.
B) Low leg drains, high point bleeds, analyzer vents,
open-ended valves or lines, and safety devices are not
subject to the requirements of subsection (b)(3)(A)
above.
3)
When the closed -vent system includes bypass devices that
could be used to divert the gas or vapor stream to the
atmosphere before entering the control device, each bypass
device must be equipped with either a flow indicator, as
specified in subsection (b)(3)(A) below, or a seal or
locking device, as specified in subsection (b)(3)(B) below.
For the purpose of complying with this subsection, low leg
216
drains, high point bleeds, analyzer vents, open
-ended valves
or lines, spring loaded pressure relief valves, and other
fittings used for safety purposes are not considered to be
bypass devices.
A)
If a flow indicator is used to comply with subsection
(b)(3) above, the indicator must be installed at the
inlet to the bypass line used to divert gases and
vapors from the closed
-vent system to the atmosphere
at a point upstream of the control device inlet. For
the purposes of this subsection, a flow indicator
means a device that indicates the presence of either
gas or vapor flow in the bypass line.
B)
If a seal or locking device is used to comply with
subsection (b)(3) above, the device must be placed on
the mechanism by which the bypass device position is
controlled (e.g., valve handle or damper lever) when
the bypass device is in the closed position such that
the bypass device cannot be opened without breaking
the seal or removing the lock. Examples of such
devices include, but are not limited to, a car
-seal or
a lock -and-key configuration valve. The owner or
operator shall visually inspect the seal or closure
mechanism at least once every month to verify that the
bypass mechanism is maintained in the closed position.
4)
The closed -vent system must be inspected and monitored by
the owner or operator in accordance with the procedure
specified in Section 724.933(l).
c)
The control device shall meet the following requirements:
1)
The control device shall be one of the following devices:
A)
A control device designed and operated to reduce the
total organic content of the inlet vapor stream vented
to the control device by at least 95 percent by
weight;
B)
An enclosed combustion device designed and operated in
accordance with the requirements of Section
724.933(c); or
C)
A flare designed and operated in accordance with the
requirements of Section 724.933(d).
2) The control device shall be operating at all times when
gases, vapors, or fumes are vented from the waste management
unit through the closed-vent system to the control device.
2)
The owner or operator that elects to use a closed
-vent
system and control device to comply with the requirements of
this Section shall comply with the requirements specified in
subsections (c)(2)(A) through (c)(2)(F) below.
A)
Periods of planned routine maintenance of the control
device, during which the control device does not meet
the specifications of subsections (c)(1)(A),
(c)(1)(B), or (c)(1)(C) above, as applicable, must not
exceed 240 hours per year.
217
B)
The specifications and requirements in subsections
(c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
devices do not apply during periods of planned routine
maintenance.
C)
The specifications and requirements in subsections
(c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
devices do not apply during a control device system
malfunction.
D)
The owner or operator shall demonstrate compliance
with the requirements of subsection (c)(2)(A) above
(i.e., planned routine maintenance of a control
device, during which the control device does not meet
the specifications of subsections (c)(1)(A),
(c)(1)(B), or (c)(1)(C) above, as applicable, must not
exceed 240 hours per year) by recording the
information specified in Section 724.989(e)(1)(E).
E)
The owner or operator shall correct control device
system malfunctions as soon as practicable after their
occurrence in order to minimize excess emissions of
air pollutants.
F)
The owner or operator shall operate the closed
-vent
system so that gases, vapors, or fumes are not
actively vented to the control device during periods
of planned maintenance or control device system
malfunction (i.e., periods when the control device is
not operating or not operating normally), except in
cases when it is necessary to vent the gases, vapors,
or fumes to avoid an unsafe condition or to implement
malfunction corrective actions or planned maintenance
actions.
3)
The owner or operator using a carbon adsorption system to
comply with subsection (c)(1) above shall operate and
maintain the control device in accordance with the following
requirements:
A)
Following the initial startup of the control device,
all activated carbon in the control device shall be
replaced with fresh carbon on a regular basis in
accordance with the requirements of Section 724.933(g)
or Section 724.933(h).
B)
All carbon removed from the control device shall be
managed in accordance with the requirements of Section
724.933( mn).
4)
An owner or operator using a control device other than a
thermal vapor incinerator, flare, boiler, process heater,
condenser, or carbon adsorption system to comply with
subsection (c)(1) above shall operate and maintain the
control device in accordance with the requirements of
Section 724.933(j).
5)
The owner or operator shall demonstrate that a control
device achieves the performance requirements of subsection
(c)(1) above, as follows:
218
A)
An owner or operator shall demonstrate using either a
performance test, as specified in subsection (c)(5)(C)
below, or a design analysis, as specified in
subsection (c)(5)(D) below, the performance of each
control device except for the following:
i)
A flare;
ii)
A boiler or process heater with a design heat
input capacity of 44 megawatts or greater;
iii)
A boiler or process heater into which the vent
stream is introduced with the primary fuel;
iv)
A boiler or process heater industrial furnace
burning hazardous waste for which the owner or
operator has been issued a final permit under 35
Ill. Adm. Code 702, 703, and 705 and designs has
designed and operates the unit in accordance
with the interim status requirements of 35 Ill.
Adm. Code 726.Subpart H; or
v)
A boiler or process heater industrial furnace
burning hazardous waste for which the owner or
operator has certified compliance designed and
operates in accordance
with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
B)
An owner or operator shall demonstrate the performance
of each flare in accordance with the requirements
specified in Section 724.933(e).
C)
For a performance test conducted to meet the
requirements of subsection (c)(5)(A) above, the owner
or operator shall use the test methods and procedures
specified in Section 724.934(c)(1) through (c)(4).
D)
For a design analysis conducted to meet the
requirements of subsection (c)(5)(A) above, the design
analysis shall meet the requirements specified in
Section 724.935(b)(4)(C).
E)
The owner or operator shall demonstrate that a carbon
adsorption system achieves the performance
requirements of subsection (c)(1) above based on the
total quantity of
organics vented to the atmosphere
from all carbon adsorption system equipment that is
used for organic adsorption, organic
desorption or
carbon regeneration, organic recovery, and carbon
disposal.
6)
If the owner or operator and the Agency do not agree on a
demonstration of control device performance using a design
analysis then the disagreement shall be resolved using the
results of a performance test performed by the owner or
operator in accordance with the requirements of subsection
(c)(5)(C) above. The Agency may choose to have an
authorized representative observe the performance test.
7)
The control device must be inspected and monitored by the
219
owner or operator in accordance with the procedures
specified in 35 Ill. Adm. Code 724.933(f)(2) and 35 Ill.
Adm. Code 724.933(l). The readings from each monitoring
device required by 35 Ill. Adm. Code 724.933(f)(2) must be
inspected at least once each operating day to check control
device operation. Any necessary corrective measures must be
immediately implemented to ensure the control device is
operated in compliance with the requirements of this
Section.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.988
Inspection and Monitoring Requirements
a) This Section applies to an owner or operator using air emission
controls in accordance with the requirements of Sections 724.984
through 724.987.
b) Each cover used in accordance with requirements of Section 724.984
through 724.986 shall be visually inspected and monitored for
detectable organic emissions by the owner or operator using the
procedure specified in 35 Ill. Adm. Code 725.989(f)(1) through
(f)(7), except as follows:
1) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in 35 Ill.
Adm. Code 725.989(f)(1) through (f)(7) for the following
tank covers:
A) A tank internal floating roof that is inspected and
monitored in accordance with the requirements of
Section 724.991; or
B) A tank external floating roof that is inspected and
monitored in accordance with the requirements of
Section 724.991.
2) If a tank is buried partia
lly or entirely underground, an
owner or operator is required to perform the cover
inspection and monitoring requirements specified in 35 Ill.
Adm. Code 725.989(f)(1) through (f)(7) only for those
portions of the tank cover and those connections to the tank
cover or tank body (e.g., fill ports, access hatches, gauge
wells, etc.) that extend to or above the ground surface and
can be opened to the atmosphere.
3) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in 35 Ill.
Adm. Code 725.989(f)(1) through (f)(7) for a container that
meets all requirements specified in either Section
724.986(b)(1)(B) or (b)(1)(C).
4) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in 35 Ill.
Adm. Code 725.989(f)(1) through (f)(7) for an enclosure used
to control air emissions from containers in accordance with
the requirements of Section 724.986(b)(2).
c) Each closed-vent system used in accordance with the
requirements
of Section 724.987 shall be inspected and monitored by the owner
or operator in accordance with the procedure specified in Section
220
724.933(k).
d) Each control device used in accordance with the requirements of
Section 724.987 shall be inspected and monitored by the owner or
operator in accordance with the procedures specified in Sections
724.933(f) (2) and 724.933(i). The readings from each monitoring
device required by Section 724.933(f)(2) shall be inspected at
least once each operating day to check control device operation.
Any necessary corrective measures should be immediately
implemented to ensure the control device is operated in compliance
with the requirements of Section 264.987.
e) The owner or operator shall develop and implement a written plan
and schedule to perform all inspection and monitoring requirements
of this section. The owner or operator shall incorporate this
plan and schedule into the facility inspection plan required under
Section 724.115.
a)
The owner or operator shall inspect and monitor air emission
control equipment used to comply with this Subpart in accordance
with the applicable requirements specified in Section 724.984
through Section 724.987.
b)
The owner or operator shall develop and implement a written plan
and schedule to perform the inspections and monitoring required by
subsection (a) above. The owner or operator shall incorporate
this plan and schedule into the facility inspection plan required
under 35 Ill. Adm. Code 724.115.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.989
Recordkeeping Requirements
a) Each owner or operator of a facility subject to requirements in
this Subpart shall record and maintain the following information
as applicable:
1) Documentation for each cover installed on a tank in
accordance with the requirements of Section 724.984(b)(2) or
(b)(3) that includes information prepared by the owner or
operator or provided by the cover manufacturer or vendor
describing the cover design, and certification by the owner
or operator that the cover meets the applicable design
specifications as listed in 35 Ill. Adm. Code 725.991(c).
2) Documentation for each floating membrane cover installed on
a surface impoundment in accordance with the requirements of
Section 724.985(c) that includes information prepared by the
owner or operator or provided by the cover manufacturer or
vendor describing the cover design, and certification by the
owner or operator that the cover meets the specifications
listed in 35 Ill. Adm. Code 725.986(e).
3) Documentation for each enclosure used to control air
emissions from containers in accordance with the
requirements of Section 724.986(b)(2)(A) that includes
information prepared by the owner or operator or provided by
the manufacturer or vendor describing the enclosure design,
and certification by the owner or operator that the
enclosure meets the specifications listed in Section
724.986(b)(2)(B).
221
4) Documentation for each closed-vent system and control device
installed in accordance with the requirements of Section
724.987 that includes:
A) Certification that is signed and dated by the owner or
operator stating that the control device is designed
to operate at the performance level documented by a
design analysis as specified in subsection (a)(4)(B)
below or by performance tests as specified in
subsection (a)(4)(C) below when the tank, surface
impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to
occur.
B) If a design analysis is used, then design
documentation as specified in Section 724.935(b)(4).
The documentation shall include information prepared
by the owner or operator or provided by the control
device manufacturer or vendor that describes the
control device design in accordance with Section
724.935(b)(4)(C) and certification by the owner or
operator that the control equipment meets the
applicable specifications.
C) If performance tests are used, then a performance test
plan as specified in Section 724.935(b)(3) and all
test results.
D) Information as required by Section 724.935(c)(1) and
(c)(2).
5) Records for all Method 27 tests performed by the owner or
operator for each container used to meet the requirements of
Section 724.986(b)(1)(C).
6) Records for all visual inspections conducted in accordance
with the requirements of Section 724.988.
7) Records for all monitoring for detectable organic emissions
conducted in accordance with the requirements of Section
724.988.
8) Records of the date of each attempt to repair a leak, repair
methods applied, and the date of successful repair.
9) Records for all continuous monitoring conducted in
accordance with the requirements of Section 724.988.
10) Records of the management of carbon removed from a carbon
adsorption system conducted in accordance with Section
724.987(c)(3)(B).
11) Records for all inspections of each cover installed on a
tank in accordance with the requirements of Section
724.984(b)(2) or (b)(3) that includes information as listed
in 35 Ill. Adm. Code 725.991(c).
b) An owner or operator electing to use air emission controls for a
tank in accordance with the conditions specified in Section
724.984(c) shall record the following information:
222
1) Date and time each waste sample is collected for direct
measurement of maximum organic vapor pressure in accordance
with Section 724.983(c).
2) Results of each determination of the maximum organic vapor
pressure of the waste in a tank performed in accordance with
Section 724.983(c).
3) Records specifying the tank dimensions and design capacity.
c) An owner or operator electing to use air emission controls for a
tank in accordance with the requirements of Section 724.991 shall
record the information required by Section 724.991(c).
d) An owner or operator electing not to use air emission controls for
a particular tank, surface impoundment, or container subject to
this Subpart in accordance with the conditions specified in
Section 724.982(c) shall record the information used by the owner
or operator for each waste determination (e.g., test results,
measurements, calculations, and other documentation) in the
facility operating log. If analysis results for waste samples are
used for the waste determination, then the owner or operator shall
record the date, time, and location that each waste sample is
collected in accordance with applicable requirements of Section
724.983.
e) An owner or operator electing to comply with requirements in
accordance with Section 724.982(c)(2)(E) or Section
724.982(c)(2)(F) shall record the identification number for the
incinerator, boiler, or industrial furnace in which the hazardous
waste is treated.
f) An owner or operator designating a cover as unsafe to inspect and
monitor pursuant to 35 Ill. Adm. Code 725.989(f)(5) or difficult
to inspect and monitor pursuant to 35 Ill. Adm. Code 725.989(f)(6)
shall record in a log that is kept in the facility operating
record the following information:
1) A list of identification numbers for tank
s with covers that
are designated as unsafe to inspect and monitor in
accordance with the requirements of 35 Ill. Adm. Code
725.989(f)(5), an explanation for each cover stating why the
cover is unsafe to inspect and monitor, and the plan and
schedule for inspecting and monitoring each cover.
2) A list of identification numbers for tanks with covers that
are designated as difficult to inspect and monitor in
accordance with the requirements of 35 Ill. Adm. Code
725.989(f)(6), an explanation for each cover stating why the
cover is difficult to inspect and monitor, and the plan and
schedule for inspecting and monitoring each cover.
g) All records required by subsections (a) through (f) above, except
as required in subsections (a)(1) through (a)(4), shall be
maintained in the operating record for a minimum of 3 years. All
records required by subsections (a)(1) through (a)(4) above shall
be maintained in the operating record until the air emission
control equipment is replaced or otherwise no longer in service.
a)
Each owner or operator of a facility subject to requirements in
223
this Subpart shall record and maintain the information specified
in subsections (b) through (i) below, as applicable to the
facility. Except for air emission control equipment design
documentation and information required by subsection (i) below,
records required by this Section must be maintained in the
operating record for a minimum of three years. Air emission
control equipment design documentation must be maintained in the
operating record until the air emission control equipment is
replaced or is otherwise no longer in service. Information
required by subsection (i) below must be maintained in the
operating record for as long as the tank or container is not using
air emission controls specified in Sections 724.984 through
724.987, in accordance with the conditions specified in Section
724.984(d).
b)
The owner or operator of a tank using air emission controls in
accordance with the requirements of Section 724.984 shall prepare
and maintain records for the tank that include the following
information:
1)
For each tank using air emission controls in accordance with
the requirements of Section 724.984, the owner or operator
shall record:
A)
A tank identification number (or other unique
identification description as selected by the owner or
operator).
B)
A record for each inspection required by Section
724.984 that includes the following information:
i)
Date inspection was conducted.
ii)
For each defect detected during the inspection,
the following information: the location of the
defect, a description of the defect, the date of
detection, and corrective action taken to repair
the defect. In the event that repair of the
defect is delayed in accordance with the
provisions of Section 724.984, the owner or
operator shall also record the reason for the
delay and the date that completion of repair of
the defect is expected.
2)
In addition to the information required by subsection (b)(1)
above, the owner or operator shall record the following
information, as applicable to the tank:
A)
The owner or operator using a fixed roof to comply
with the Tank Level 1 control requirements specified
in Section 724.984(c) shall prepare and maintain
records for each determination for the maximum organic
vapor pressure of the hazardous waste in the tank
performed in accordance with the requirements of
Section 724.984(c). The records must include the date
and time the samples were collected, the analysis
method used, and the analysis results.
B)
The owner or operator using an internal floating roof
to comply with the Tank Level 2 control requirements
specified in Section 724.984(e) shall prepare and
224
maintain documentation describing the floating roof
design.
C)
Owners and operators using an external floating roof
to comply with the Tank Level 2 control requirements
specified in Section 724.984(f) shall prepare and
maintain the following records:
i)
Documentation describing the floating roof
design and the dimensions of the tank.
ii)
Records for each seal gap inspection required by
Section 724.984(f)(3) describing the results of
the seal gap measurements. The records must
include the date that the measurements were
performed, the raw data obtained for the
measurements, and the calculations of the total
gap surface area. In the event that the seal
gap measurements do not conform to the
specifications in Section 724.984(f)(1), the
records must include a description of the
repairs that were made, the date the repairs
were made, and the date the tank was emptied, if
necessary.
D)
Each owner or operator using an enclosure to comply
with the Tank Level 2 control requirements specified
in Section 724.984(i) shall prepare and maintain the
following records:
i)
Records for the most recent set of calculations
and measurements performed by the owner or
operator to verify that the enclosure meets the
criteria of a permanent total enclosure as
specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111.
ii)
Records required for the closed
-vent system and
control device in accordance with the
requirements of subsection (e) below.
c)
The owner or operator of a surface impoundment using air emission
controls in accordance with the requirements of Section 724.985
shall prepare and maintain records for the surface impoundment
that include the following information:
1)
A surface impoundment identification number (or other unique
identification description as selected by the owner or
operator).
2)
Documentation describing the floating membrane cover or
cover design, as applicable to the surface impoundment, that
includes information prepared by the owner or operator or
provided by the cover manufacturer or vendor describing the
cover design, and certification by the owner or operator
that the cover meets the specifications listed in Section
724.985(c).
225
3)
A record for each inspection required by Section 724.985
that includes the following information:
A)
Date inspection was conducted.
B)
For each defect detected during the inspection the
following information: the location of the defect, a
description of the defect, the date of detection, and
corrective action taken to repair the defect. In the
event that repair of the defect is delayed in
accordance with the provisions of Section 724.985(f),
the owner or operator shall also record the reason for
the delay and the date that completion of repair of
the defect is expected.
4)
For a surface impoundment equipped with a cover and vented
through a closed -vent system to a control device, the owner
or operator shall prepare and maintain the records specified
in subsection (e).
d)
The owner or operator of containers using Container Level 3 air
emission controls in accordance with the requirements of Section
724.986 shall prepare and maintain records that include the
following information:
1)
Records for the most recent set of calculations and
measurements performed by the owner or operator to verify
that the enclosure meets the criteria of a permanent total
enclosure as specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total Enclosure"
under 40 CFR 52.741, appendix B, incorporated by reference
in 35 Ill. Adm. Code 720.111.
2)
Records required for the closed
-vent system and control
device in accordance with the requirements of subsection (e)
below.
e)
The owner or operator using a closed
-vent system and control
device in accordance with the requirements of Section 724.987
shall prepare and maintain records that include the following
information:
1)
Documentation for the closed
-vent system and control device
that includes:
A)
Certification that is signed and dated by the owner or
operator stating that the control device is designed
to operate at the performance level documented by a
design analysis as specified in subsection (e)(1)(B)
of this Section or by performance tests as specified
in subsection (e)(1)(C) below when the tank, surface
impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to
occur.
B)
If a design analysis is used, then design
documentation, as specified in Section 724.935(b)(4).
The documentation must include information prepared
by the owner or operator or provided by the control
device manufacturer or vendor that describes the
control device design in accordance with Section
226
724.935(b)(4)(C) and certification by the owner or
operator that the control equipment meets the
applicable specifications.
C)
If performance tests are used, then a performance test
plan as specified in Section 724.935(b)(3) and all
test results.
D)
Information as required by Section 724.935(c)(1) and
Section 724.935(c)(2), as applicable.
E)
An owner or operator shall record, on a semiannual
basis, the information specified in subsections
(e)(1)(E)(i) and (e)(1)(E)(ii) below for those planned
routine maintenance operations that would require the
control device not to meet the requirements of Section
724.987(c)(1)(A), (c)(1)(B), or (c)(1)(C) above, as
applicable.
i)
A description of the planned routine maintenance
that is anticipated to be performed for the
control device during the next six-month period.
This description must include the type of
maintenance necessary, planned frequency of
maintenance, and lengths of maintenance periods.
ii)
A description of the planned routine maintenance
that was performed for the control device during
the previous six -month period. This description
must include the type of maintenance performed
and the total number of hours during those six
months that the control device did not meet the
requirements of Section 724.987(c)(1)(A),
(c)(1)(B), or (c)(1)(C), as applicable, due to
planned routine maintenance.
F)
An owner or operator shall record the information
specified in subsections (e)(1)(F)(i) through
(e)(1)(F)(iii) below for those unexpected control
device system malfunctions that would require the
control device not to meet the requirements of Section
724.987 (c)(1)(A), (c)(1)(B), or (c)(1)(C) above, as
applicable.
i)
The occurrence and duration of each malfunction
of the control device system.
ii)
The duration of each period during a malfunction
when gases, vapors, or fumes are vented from the
waste management unit through the closed
-vent
system to the control device while the control
device is not properly functioning.
iii)
Actions taken during periods of malfunction to
restore a malfunctioning control device to its
normal or usual manner of operation.
G)
Records of the management of carbon removed from a
carbon adsorption system conducted in accordance with
Section 724.987(c)(3)(B).
227
f)
The owner or operator of a tank, surface impoundment, or container
exempted from standards in accordance with the provisions of
Section 724.982(c) shall prepare and maintain the following
records, as applicable:
1)
For tanks, surface
impoundments, or containers exempted
under the hazardous waste organic concentration conditions
specified in Section 724.982(c)(1) or (c)(2), the owner or
operator shall record the information used for each waste
determination (e.g., test results, measurements,
calculations, and other documentation) in the facility
operating log. If analysis results for waste samples are
used for the waste determination, then the owner or operator
shall record the date, time, and location that each waste
sample is collected in accordance with applicable
requirements of Section 724.983.
2)
For tanks, surface
impoundments, or containers exempted
under the provisions of Section 724.982(c)(2)(G) or Section
724.982(c)(2)(H), the owner or operator shall record the
identification number for the incinerator, boiler, or
industrial furnace in which the hazardous waste is treated.
g)
An owner or operator designating a cover as "unsafe to inspect and
monitor" pursuant to Section 724.984(l) or Section 724.985(g)
shall record in a log that is kept in the facility operating
record the following information: the identification numbers for
waste management units with covers that are designated as "unsafe
to inspect and monitor", the explanation for each cover stating
why the cover is unsafe to inspect and monitor, and the plan and
schedule for inspecting and monitoring each cover.
h)
The owner or operator of a facility that is subject to this
Subpart and to the control device standards in 40 CFR 60, Subpart
VV or 40 CFR 61, Subpart V, incorporated by reference in 35 Ill.
Adm. Code 720.111, may elect to demonstrate compliance with the
applicable Sections of this Subpart by documentation either
pursuant to this Subpart, or pursuant to the provisions of 40 CFR
60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
documentation required by 40 CFR 60 or 61 duplicates the
documentation required by this Section.
i)
For each tank or container not using air emission controls
specified in Sections 724.984 through 724.987 in accordance with
the conditions specified in Section 724.980(d), the owner or
operator shall record and maintain the following information:
1)
A list of the individual organic peroxide compounds
manufactured at the facility that meet the conditions
specified in Section 724.980(d)(1).
2)
A description of how the hazardous waste containing the
organic peroxide compounds identified pursuant to subsection
(i)(1) above are managed at the facility in tanks and
containers. This description must include the following
information:
A)
For the tanks used at the facility to ma
nage this
hazardous waste, sufficient information must be
provided to describe
the following for
each tank: a
facility identification number for the tank, the
228
purpose and placement of this tank in the management
train of this hazardous waste, and the procedures used
to ultimately dispose of the hazardous waste managed
in the tanks.
B)
For containers used at the facility to manage this
hazardous waste, sufficient information must be
provided to describe each tank: a facility
identification number for the container or group of
containers, the purpose and placement of this
container or group of containers in the management
train of this hazardous waste, and the procedures used
to ultimately dispose of the hazardous waste managed
in the containers.
3)
An explanation of why managing the hazardous waste
containing the organic peroxide compounds identified
pursuant to subsection (i)(1) above in the tanks or
containers identified pursuant to subsection (i)(2) above
would create an undue safety hazard if the air emission
controls specified in Sections 724.984 through 724.987 were
installed and operated on these waste management units.
This explanation must include the following information:
A)
For tanks used at the facility to manage this
hazardous waste, sufficient information must be
provided to explain
the following : how use of
the required air emission controls on the tanks
would affect the tank design features and
facility operating procedures currently used to
prevent an undue safety hazard during management
of this hazardous waste in the tanks; and why
installation of safety devices on the required
air emission controls, as allowed under
Section
724.984(g) this Subpart , would not address those
situations in which evacuation of tanks equipped
with these air emission controls is necessary
and consistent with good engineering and safety
practices for handling organic peroxides.
B)
For containers used at the facility to manage
this hazardous waste, sufficient information
must be provided to explain
the following : how
use of the required air emission controls on the
tanks would affect the container design features
and handling procedures currently used to
prevent an undue safety hazard during management
of this hazardous waste in the containers; and
why installation of safety devices on the
required air emission controls, as allowed under
Section 724.986(d)
this Subpart , would not
address those situations in which evacuation of
containers equipped with these air emission
controls is necessary and consistent with good
engineering and safety practices for handling
organic peroxides.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.990
Reporting Requirements
229
a)
Each owner or operator managing hazardous waste in a tank, surface
impoundment, or container exempted from using air emission
controls under the provisions of Section 724.982(c) shall report
to the Agency each occurrence when hazardous waste is placed in
the waste management unit in noncompliance with the conditions
specified in Section 724.982(c)(1) or (c)(2), as applicable.
Examples of such occurrences include placing in the waste
management unit a hazardous waste having an average VO
concentration equal to or greater than
100500 ppmw at the point of
waste origination or placing in the waste management unit a
treated hazardous waste that fails to meet the applicable
conditions specified in Section 724.982(c)(2)(A) through
(c)(2)( EF). The owner or operator shall submit a written report
within 15 calendar days of the time that the owner or operator
becomes aware of the occurrence. The written report shall contain
the U.S. EPA identification number, the facility name and address,
a description of the noncompliance event and the cause, the dates
of the noncompliance, and the actions taken to correct the
noncompliance and prevent re
occurrence of the noncompliance. The
report shall be signed and dated by an authorized representative
of the owner or operator.
b)
Each owner or operator using air emission contro
ls on a tank in
accordance with the requirements Section 724.984(c) shall report
to the Agency each occurrence when hazardous waste is managed in
the tank in noncompliance with the conditions specified in Section
724.984 (c)(1) through (c)(4)
(b). The owner or operator shall
submit a written report within 15 calendar days of the time that
the owner or operator becomes aware of the occurrence. The
written report shall contain the U
.S. EPA identification number,
the facility name and address, a description of the noncompliance
event and the cause, the dates of the noncompliance, and the
actions taken to correct the noncompliance and prevent
reoccurrence of the noncompliance. The report shall be signed and
dated by an authorized representative of the owner or operator.
c)
Each owner or operator using a control device in accordance with
the requirements of Section 724.987 shall submit a semiannual
written report to the Agency excepted as provided for in
subsection (d) below. The report shall describe each occurrence
during the previous 6-month period when
either of the two
following events occurs:
a control device is operated
continuously for 24 hours or longer in noncompliance with the
applicable operating values defined in Section 724.935(c)(4) or
when a flare is operated with visible emissions
for five minutes
or longer in a two-hour period,
as defined in Section 724.933(d).
The written report shall include the U. S. EPA identification
number, the facility name and address, and an explanation why the
control device could not be returned to compliance within 24
hours, and actions taken to correct the noncompliance. The report
shall be signed and dated by an authorized representative of the
owner or operator.
d)
A report to the Agency in accordance with the requirements of
subsection (c) above is not required for a 6-month period during
which all control devices subject to this Subpart are operated by
the owner or operator so that both of the following conditions
result: during no period of 24 hours or longer did a control
device operate continuously in noncompliance with the applicable
operating values defined in Section 724.935(c)(4)
orand ano flare
was operate d with visible emissions
for five minutes or longer in
230
a two-hour period
, as defined in Section 724.933(d).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 724.991
Alternative Control Requirements for Tanks
(Repealed)
a) This Section applies to owners and operators of tanks that elect
to comply with Section 724.984(b)(2) or Section 724.984(b)(3).
1) The owner or operator that elects to comply with Section
724.984(b)(2) shall design, install, operate, and maintain a
fixed roof and internal floating roof that meet the
requirements specified in 35 Ill. Adm. Code 725.991(a)(1)(A)
through (a)(1)(I).
2) The owner or operator that elects to comply with Section
724.984(b)(3) shall design, install, operate, and maintain
an external floating roof that meets the requirements
specified in 35 Ill. Adm. Code 725.991(a)(2)(A) through
(a)(2)(C).
3) The owner or operator may elect to comply with Section
264.984(b)(2) or (b)(3) using an alternative means of
emission limitation as specified in 35 Ill. Adm. Code
725.991(a)(3).
b) The owner or operator shall inspect and monitor the control
equipment in accordance with the following requirements:
1) For a tank equipped with a fixed roof and internal floating
roof in accordance with the requirements of subsection
(a)(1) above, the owner or operator shall perform the
inspection and monitoring requirements specified in 35 Ill.
Adm. Code 725.991(b)(1).
2) For a tank equipped with an external floating roof in
accordance with the requirements of subsection (a)(2) above,
the owner or operator shall perform the inspection and
monitoring requirements specified in 35 Ill. Adm. Code
725.991(b)(2).
c) The owner or operator shall record the following information in
the operating record in accordance with the requirements of
Section 724.989(a)(1) and (a)(11):
1) For a tank equipp
ed with a fixed roof and internal floating
roof in accordance with the requirements of subsection
(a)(1) above, the owner or operator shall record the
information listed in 35 Ill. Adm. Code 725.991(c)(1).
2) For a tank equipped with an external floating roof in
accordance with the requirements of subsection (a)(1) above,
the owner or operator shall record the information listed in
35 Ill. Adm. Code 725.991(c)(2).
(Source: R
epealed at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
231
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 725
INTERIM STATUS STANDARDS FOR OWNERS AND OPERATORS OF HAZARDOUS
WASTE TREATMENT, STORAGE, AND DISPOSAL FACILITIES
SUBPART A: GENERAL PROVISIONS
Section
725.101
Purpose, Scope and Applicability
725.104
Imminent Hazard Action
SUBPART B: GENERAL FACILITY STANDARDS
Section
725.110
Applicability
725.111
USEPA Identification Number
725.112
Required N otices
725.113
General Waste Analysis
725.114
Security
725.115
General Inspection Requirements
725.116
Personnel Training
725.117
General Requirements for Ignitable, Reactive, or Incompatible
Wastes
725.118
Location Standards
725.119
Construction Quality Assurance Program
SUBPART C: PREPAREDNESS AND PREVENTION
Section
725.130
Applicability
725.131
Maintenance and Operation of Facility
725.132
Required Equipment
725.133
Testing and Maintenance of Equipment
725.134
Access to Communications or Alarm System
725.135
Required Aisle Space
725.137
Arrangements with Local Authorities
SUBPART D: CONTINGENCY PLAN AND EMERGENCY PROCEDURES
Section
725.150
Applicability
725.151
Purpose and Implementation of Contingency Plan
725.152
Content of Contingency Plan
725.153
Copies of Contingency Plan
725.154
Amendment of Contingency Plan
725.155
Emergency Coordinator
725.156
Emergency Procedures
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section
725.170
Applicability
725.171
Use of Manifest System
725.172
Manifest Discrepancies
725.173
Operating Record
725.174
Availability, Retention and Disposition of Records
725.175
Annual Report
725.176
Unmanifested Waste Report
725.177
Additional Reports
SUBPART F: GROUNDWATER MONITORING
Section
725.190
Applicability
725.191
Groundwater Monitoring System
725.192
Sampling and Analysis
232
725.193
Preparation, Evaluation and Response
725.194
Recordkeeping and Reporting
SUBPART G: CLOSURE AND POST-CLOSURE
Section
725.210
Applicability
725.211
Closure Performance Standard
725.212
Closure Plan; Amendment of Plan
725.213
Closure; Time Allowed for Closure
725.214
Disposal or Decontamination of Equipment, Structures and Soils
725.215
Certification of Closure
725.216
Survey Plat
725.217
Post-closure Care and Use of Property
725.218
Post-closure Plan; Amendment of Plan
725.219
Post-Closure Notices
725.220
Certification of Completion of Post-Closure Care
SUBPART H: FINANCIAL REQUIREMENTS
Section
725.240
Applicability
725.241
Definitions of Terms as Used in this Subpart
725.242
Cost Estimate for Closure
725.243
Financial Assurance for Closure
725.244
Cost Estimate for Post-closure Care
725.245
Financial Assurance for Post-closure Monitoring and Maintenance
725.246
Use of a Mechanism for Financial Assurance of Both Closure and
Post-closure Care
725.247
Liability Requirements
725.248
Incapacity of Owners or Operators, Guarantors or Financial
Institutions
725.251
Promulgation of Forms (Repealed)
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
Section
725.270
Applicability
725.271
Conditi on of Containers
725.272
Compatibility of Waste with Container
725.273
Management of Containers
725.274
Inspections
725.276
Special Requirements for Ignitable or Reactive Waste
725.277
Special Requirements for Incompatible Wastes
725.278
Air Emission Standards
SUBPART J: TANK SYSTEMS
Section
725.290
Applicability
725.291
Assessment of Existing Tank System's Integrity
725.292
Design and Installation of New Tank Systems or Components
725.293
Containment and Detection of Releases
725.294
General Operating R
equirements
725.295
Inspections
725.296
Response to leaks or spills and disposition of Tank Systems
725.297
Closure and Post-Closure Care
725.298
Special Requirements for Ignitable or Reactive Waste
725.299
Special Requirements for Incompatible Wastes
725.300
Waste Analysis and Trial Tests
725.301
Generators of 100 to 1000 kg/mo
725.302
Air Emission Standards
SUBPART K: SURFACE IMPOUNDMENTS
Section
233
725.320
Applicability
725.321
Design and Operating Requirements
725.322
Action Leakage Rate
725.323
Respons e Actions
725.324
Containment System
725.325
Waste Analysis and Trial Tests
725.326
Monitoring and Inspections
725.328
Closure and Post-Closure Care
725.329
Special Requirements for Ignitable or Reactive Waste
725.330
Special Requirements for Incompatible Wastes
725.331
Air Emission Standards
SUBPART L: WASTE PILES
Section
725.350
Applicability
725.351
Protection from Wind
725.352
Waste Analysis
725.353
Containment
725.354
Design and Operating Requirements
725.355
Action Leakage Rates
725.356
Special Re quirements for Ignitable or Reactive Waste
725.357
Special Requirements for Incompatible Wastes
725.358
Closure and Post-Closure Care
725.359
Response Actions
725.360
Monitoring and Inspection
SUBPART M: LAND TREATMENT
Section
725.370
Applicability
725.372
General Operating Requirements
725.373
Waste Analysis
725.376
Food Chain Crops
725.378
Unsaturated Zone (Zone of Aeration) Monitoring
725.379
Recordkeeping
725.380
Closure and Post-closure
725.381
Special Requirements for Ignitable or Reactive Waste
725.382
Special Requirements for Incompatible Wastes
SUBPART N: LANDFILLS
Section
725.400
Applicability
725.401
Design Requirements
725.402
Action Leakage Rate
725.403
Response Actions
725.404
Monitoring and Inspection
725.409
Surveying and Recordkeeping
725.410
Closure and Post-Closure
725.412
Special Requirements for Ignitable or Reactive Waste
725.413
Special Requirements for Incompatible Wastes
725.414
Special Requirements for Liquid Wastes
725.415
Special Requirements for Containers
725.416
Disposal o f Small Containers of Hazardous Waste in
Overpacked
Drums (Lab Packs)
SUBPART O: INCINERATORS
Section
725.440
Applicability
725.441
Waste Analysis
725.445
General Operating Requirements
725.447
Monitoring and Inspection
725.451
Closure
234
725.452
Interim Status Incinerators Burning Particular Hazardous Wastes
SUBPART P: THERMAL TREATMENT
Section
725.470
Other Thermal Treatment
725.473
General Operating Requirements
725.475
Waste Analysis
725.477
Monitoring and Inspections
725.481
Closure
725.482
Open Bur ning; Waste Explosives
725.483
Interim Status Thermal Treatment Devices Burning Particular
Hazardous Waste
SUBPART Q: CHEMICAL, PHYSICAL AND BIOLOGICAL TREATMENT
Section
725.500
Applicability
725.501
General Operating Requirements
725.502
Waste Analysis and Trial Tests
725.503
Inspections
725.504
Closure
725.505
Special Requirements for Ignitable or Reactive Waste
725.506
Special Requirements for Incompatible Wastes
SUBPART R: UNDERGROUND INJECTION
Section
725.530
Applicability
SUBPART W: DRIP PADS
Section
725.540
Applicability
725.541
Assessment of existing drip pad integrity
725.542
Design and installation of new drip pads
725.543
Design and operating requirements
725.544
Inspections
725.545
Closure
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section
725.930
Applicability
725.931
Definitions
725.932
Standards: Process Vents
725.933
Standards: Closed-vent Systems and Control Devices
725.934
Test methods and procedures
725.935
Recordkeeping Requirements
SUBPART BB: AIR EMISSION STAND
ARDS FOR EQUIPMENT LEAKS
Section
725.950
Applicability
725.951
Definitions
725.952
Standards: Pumps in Light Liquid Service
725.953
Standards: Compressors
725.954
Standards: Pressure Relief Devices in Gas/Vapor Service
725.955
Standards: Sampling Connecting Systems
725.956
Standards: Open-ended Valves or Lines
725.957
Standards: Valves in Gas/Vapor or Light Liquid Service
725.958
Standards: Pumps, Valves, Pressure Relief Devices, Flanges and
Other Connectors
725.959
Standards: Delay of Repair
725.960
Standards: Closed-vent Systems and Control Devices
725.961
Percent Leakage Alternative for Valves
725.962
Skip Period Alternative for Valves
235
725.963
Test Methods and Procedures
725.964
Recordkeeping Requirements
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
SURFACE IMPOUNDMENTS, AND CONTAINERS
Section
725.980
Applicability
725.981
Definitions
725.982
Schedule for Implementation of Air Emission Standards
725.983
Standards: General
725.984
Waste Determination Procedures
725.985
Standards: Tanks
725.986
Standards: Surface
Impoundments
725.987
Standards: Containers
725.988
Standards: Closed-vent Systems and Control Devices
725.989
Inspection and Monitoring Requirements
725.990
Recordkeeping Requirements
725.991
Alternative Tank Emission Control Requirements
(Repealed)
SUBPART DD: CONTAINMENT BUILDINGS
Section
725.1100
Applicability
725.1101
Design and operating standards
725.1102
Closure and Post Closure-Care
725.Appendix A
Recordkeeping Instructions
725.Appendix B
EPA Report Form and Instructions
(Repealed)
725.Appendix C
EPA Interim Primary Drinking Water Standards
725.Appendix D
Tests for Significance
725.Appendix E
Examples of Potentially Incompatible Waste
725.Appendix F
Compounds With Henry's Law Constant Less Than 0.1 Y/X (at
25
ยฐ
C)
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R81-22, 43 PCB 427, at 5 Ill. Reg. 9781, effective May 17,
1982; amended and codified in R81-22, 45 PCB 317, at 6 Ill. Reg. 4828,
effective May 17, 1982; amended in R82-18, 51 PCB 831, at 7 Ill. Reg. 2518,
effective February 22, 1983; amended in R82-19, 53 PCB 131, at 7 Ill. Reg.
14034, effective October 12, 1983; amended in R84-9, at 9 Ill. Reg. 11869,
effective July 24, 1985; amended in R85-22 at 10 Ill. Reg. 1085, effective
January 2, 1986; amended in R86-1 at 10 Ill. Reg. 14069, effective August 12,
1986; amended in R86-28 at 11 Ill. Reg. 6044, effective March 24, 1987;
amended in R86-46 at 11 Ill. Reg. 13489, effective August 4, 1987; amended in
R87-5 at 11 Ill. Reg. 19338, effective November 10, 1987; amended in R87-26 at
12 Ill. Reg. 2485, effective January 15, 1988; amended in R87-39 at 12 Ill.
Reg. 13027, effective July 29, 1988; amended in R88-16 at 13 Ill. Reg. 437,
effective December 28, 1988; amended in R89-1 at 13 Ill. Reg. 18354, effective
November 13, 1989; amended in R90-2 at 14 Ill. Reg. 14447, effective August
22, 1990; amended in R90-10 at 14 Ill. Reg. 16498, effective September 25,
1990; amended in R90-11 at 15 Ill. Reg. 9398, effective June 17, 1991; amended
in R91-1 at 15 Ill. Reg. 14534, effective October 1, 1991; amended in R91-13
at 16 Ill. Reg. 9578, effective June 9, 1992; amended in R92-1 at 16 Ill. Reg.
17672, effective November 6, 1992; amended in R92-10 at 17 Ill. Reg. 5681,
effective March 26, 1993; amended in R93-4 at 17 Ill. Reg. 20620, effective
November 22, 1993; amended in R93-16 at 18 Ill. Reg. 6771, effective April 26,
1994; amended in R94-7 at 18 Ill. Reg. 12190, effective July 29, 1994; amended
in R94-17 at 18 Ill. Reg. 17548, effective November 23, 1994; amended in R95-6
at 19 Ill. Reg. 9566, effective June 27, 1995; amended in R95-20 at 20 Ill.
Reg. 11078, August 1, 1996
; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
236
________, effective ____________________
.
SUBPART B: GENERAL FACILITY STANDARDS
Section 725.112
Required Notices
a)
Receipt from a foreign source.
1)
The owner or operator of a facility that has arranged to
receive hazardous waste from a foreign source must notify
the Regional Administrator in writing at least four weeks in
advance of the date the waste is expected to arrive at the
facility. Notice of subsequent shipments of the same waste
from the same foreign source is not required.
2)
The owner or operator of a recovery facility that has
arranged to receive hazardous waste subject to 35 Ill. Adm.
Code 722.Subpart H must provide a copy of the tracking
document bearing all required signatures to the
notifier, to
the Office of Enforcement and Compliance Assurance, Office
of Compliance, Enforcement Planning, Targeting and Data
Division (2222A), Environmental Protection Agency, 401 M
St., SW., Washington, DC 20460; to the Bureau of Land,
Division of Land Pollution Control, Illinois Environmental
Protection Agency,
P.O. Box 19276, Springfield, IL 62794-
9276; and to the competent authorities of all other
concerned countries within three working days of receipt of
the shipment. The original of the signed tracking document
must be maintained at the facility for at least three years.
b)
Before transferring ownership or operation of a facility during
its operating life, or of a disposal facility during the
post-closure care period, the owner or operator must notify the
new owner or operator in writing of the requirements of this Part
and 35 Ill. Adm. Code 702 and 703 (Also see 40 35 Ill. Adm. Code
703.155.
BOARD NOTE: An owner's or operator's failure to notify the new
owner or operator of the requirements of this Part in no way
relieves the new owner or operator of his obligation to comply
with all applicable requirements.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.113
General Waste Analysis
a)
Waste analysis:
1)
Before an owner or operator treats, stores, or disposes of
any hazardous wastes, or non-hazardous wastes if applicable
under Section 725.213(d), the owner or operator shall obtain
a detailed chemical and physical analysis of a
representative sample of the wastes. At a minimum, the
analysis must contain all the information that must be known
to treat, store, or dispose of the waste in accordance with
this Part and 35 Ill. Adm. Code 728.
2)
The analysis may include data developed under 35 Ill. Adm.
Code 721 and existing published or documented data on the
hazardous waste or on waste generated from similar
237
processes.
BOARD NOTE: For example, the facility's record of analyses
performed on the waste before the effective date of these
regulations or studies conducted on hazardous waste
generated from processes similar to that which generated the
waste to be managed at the facility may be included in the
data base required to comply with subsection (a)(1) above,
except as otherwise specified in 35 Ill. Adm. Code
728.107(b) and (c). The owner or operator of an off-site
facility may arrange for the generator of the hazardous
waste to supply part or all of the information required by
subsection (a)(1) above. If the generator does not supply
the information and the owner or operator chooses to accept
a hazardous waste, the owner or operator is responsible for
obtaining the information required to comply with this
Section.
3)
The analysis must be repeated as necessary to ensure that it
is accurate and up to date. At a minimum, the analysis must
be repeated:
A)
When the owner or operator is notified or has reason
to believe that the process or operation generating
the hazardous waste, or non-hazardous waste if
applicable under Section 725.213(d), has changed; and
B)
For off-site facilities, when the
results of the
inspection required in subsection (a)(4) below
indicate that the hazardous waste received at the
facility does not match the waste designated on the
accompanying manifest or shipping paper.
4)
The owner or operator of an off-site facility shall inspect
and, if necessary, analyze each hazardous waste movement
received at the facility to determine whether it matches the
identity of the waste specified on the accompanying manifest
or shipping paper.
b)
The owner or operator shall develop a
nd follow a written waste
analysis plan that describes the procedures that the owner or
operator will carry out to comply with subsection (a) above. The
owner or operator shall keep this plan at the facility. At a
minimum, the plan must specify:
1)
The parameters for which each hazardous waste, or non-
hazardous waste if applicable under Section 725.213(d), will
be analyzed and the rationale for the selection of these
parameters (i.e., how analysis for these parameters will
provide sufficient information on the waste's properties to
comply with subsection (a) above.
2)
The test methods that will be used to test for these
parameters.
3)
The sampling method that will be used to obtain a
representative sample of the waste to be analyzed. A
representative sample may be obtained using either:
A)
One of the sampling methods described in 35 Ill. Adm.
Code 721.Appendix A, or
238
B)
An equivalent sampling method.
BOARD NOTE: See 35 Ill. Adm. Code 720.120(c) for
related discussion.
4)
The freque ncy with which the initial analysis of the waste
will be reviewed or repeated to ensure that the analysis is
accurate and up-to-date.
5)
For off-site facilities, the waste analyses that hazardous
waste generators have agreed to supply.
6)
Where applicable, the methods that will be used to meet the
additional waste analysis requirements for specific waste
management methods, as specified in Sections 725.300,
725.325, 725.352, 725.373, 725.414, 725.441, 725.475,
725.502, 725.934(d), 725.963(d), and 725.984, and 35 Ill.
Adm. Code 728.107.
7)
For surface impoundments exempted from land disposal
restrictions under 35 Ill. Adm. Code 728.104(a), the
procedures and schedules for:
A)
The sampling of impoundment contents;
B)
The analysis of test data; and
C)
The annual removal of residues that are not
delisted
under 35 Ill. Adm. Code 720.122 or that exhibit a
characteristic of hazardous waste and either:
i)
Do not meet the applicable treatment standards
of 35 Ill. Adm. Code 728.Subpart D, or
ii)
Where no treatment standards have been
established: Such residues are prohibited from
land disposal under 35 Ill. Adm. Code 728.132 or
728.139.
8)
For owners and operators seeking an exemption to the air
emission standards of 724.Subpart CC of this part in
accordance with Section 725.983:
A) TIf direct measurement is used for the waste
determination, t he procedures and schedules for waste
sampling and analysis and the analysis of test data to
verify the exemption.
B) Each generator's not
ice and certification of the
volatile organic concentration in the waste if the
waste is received from
offsite If knowledge of the
waste is used for the waste determination, any
information prepared by the facility owner or
operator, or by the generator of the waste if the
waste is received form off-site, that is used as the
basis for knowledge of the waste
.
c)
For off-site facilities, the waste analysis plan required in
subsection (b) above must also specify the procedures that will be
used to inspect and, if necessary, analyze each movement of
239
hazardous waste received at the facility to ensure that it matches
the identity of the waste designated on the accompanying manifest
or shipping paper. At a minimum, the plan must describe:
1)
The procedures that will be used to determine the identity
of each movement of waste managed at the facility; and
2)
The sampling method that will be used to obtain a
representative sample of the waste to be identified if the
identification method includes sampling.
3)
The procedures that the owner or operator of an off-site
landfill receiving containerized hazardous waste will use to
determine whether a hazardous waste generator or
treater has
added a biodegradable
sorbent to the waste in the container.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART E: MANIFEST SYSTEM, RECORDKEEPING AND REPORTING
Section 725.171
Use of Manifest System
a)
If a facility receives hazardous waste accompanied by a manifest,
the owner or operator or his agent must:
1)
Sign and date each copy of the manifest to certify that the
hazardous waste covered by the manifest was received;
2)
Note any significant discrepancies in the manifest, as
defined in Section 725.172(a), on each copy of the manifest;
BOARD NOTE: An owner or operator of a facility whose
procedures under Section 725.113(c) include waste analysis
need not perform that analysis before signing the manifest
and giving it to the transporter. Section 725.172(b),
however, requires the owner or operator to report any
unreconciled discrepancy discovered during later analysis.
3)
Immediately give the transporter at least one copy of the
signed manifest;
4)
Send a copy of the manifest to each of the generator and the
Agency within 30 days of the date of delivery; and
5)
Retain at the facility a copy of each manifest for at least
three years from the date of delivery.
b)
If a facility receives from a rail or water (bulk shipment)
transporter hazardous waste that is accompanied by a shipping
paper containing all the information required on the manifest
(excluding the U .S. EPA identification numbers, generator's
certification and signatures), the owner or operator or its agent
must:
1)
Sign and date each copy of the manifest or shipping paper
(if the manifest has not been received) to certify that the
hazardous waste covered by the manifest or shipping paper
was received;
2)
Note any significant discrepancies, as defined in Section
240
725.172(a), in the manifest or shipping paper (if the
manifest has not been received) on each copy of the manifest
or shipping paper;
BOARD NOTE: The owner or operator of a facility whose
procedures under Section 725.113(c) include waste analysis
need not perform that analysis before signing the shipping
paper and giving it to the transporter. Section 725.172(b),
however, requires reporting an
unreconciled discrepancy
discovered during later analysis.
3)
Immediately give the rail or water (bulk shipment)
transporter at least one copy of the manifest or shipping
paper (if the manifest has not been received);
4)
Send a copy of the signed and dated manifest to the
generator and to the Agency within 30 days after the
delivery; however, if the manifest has not been received
within 30 days after delivery, the owner or operator, or his
agent, must send a copy of the shipping paper signed and
dated to the generator; and
BOARD NOTE: 35 Ill. Adm. Code 722.123(c) requires the
generator to send three copies of the manifest to the
facility when hazardous waste is sent by rail or water (bulk
shipment).
5)
Retain at the facility a copy of the manifest and shipping
paper (if signed in lieu of the manifest at the time of
delivery) for at least three years from the date of
delivery.
c)
Whenever a shipment of hazardous waste is initiated from a
facility, the owner or operator of that facility must comply with
the requirements of 35 Ill. Adm. Code 722.
BOARD NOTE: The provisions of 35 Ill. Adm. Code 722.134 are
applicable to the on
-site accumulation
of hazardous wastes by
generators. Therefore, the provisions of 35 Ill. Adm. Code
722.134 apply only to owners or operators that are shipping
hazardous waste that they generated at that facility.
d)
Within three working days of the receipt of a shipment subject to
35 Ill. Adm. Code 722.Subpart H, the owner or operator of the
facility must provide a copy of the tracking document bearing all
required signatures to the
notifier; to the Office of Enforcement
and Compliance Assurance, Office of Compliance, Enforcement
Planning, Targeting and Data Division (2222A), Environmental
Protection Agency, 401 M St., SW., Washington, DC 20460; to the
Bureau of Land, Division of Land Pollution Control, Illinois
Environmental Protection Agency,
P.O. Box 19276, Springfield, IL
62794-9276; and to competent authorities of all other concerned
countries. The original copy of the tracking document must be
maintained at the facility for at least three years from the date
of signature.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART I: USE AND MANAGEMENT OF CONTAINERS
241
Section 725.278
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a container
in accordance with the requirements of 724.Subpart
s AA, BB, and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART J: TANK SYSTEMS
Section 725.302
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a tank in
accordance with the requirements of 724.Subparts AA, BB, and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART K: SURFACE IMPOUNDMENTS
Section 725.331
Air Emission Standards
The owner or operator shall manage all hazardous waste placed in a surface
impoundment in accordance with the requirements of 724.Subpart
s BB and CC.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART N: LANDFILLS
Section 725.414
Special Requirements for Liquid Wastes
a)
This subsection corresponds with 40 CFR 265.314(a), which pertains
to the placement of bulk or non-containerized liquid waste or
waste containing free liquids in a landfill prior to May 8, 1985.
This statement maintains structural consistency with U
.S. EPA
rules.
b)
The placement of bulk or non
-containerized liquid hazardous waste
or hazardous waste containing free liquids (whether or not
sorbents have been added) in any landfill is prohibited.
c)
Containers holding free liquids must not be placed in a lan
dfill
unless;
1)
All free -standing liquid:
A)
has been removed by decanting or other methods;
B)
has been mixed with
sorbent or solidified so that
free-standing liquid is no longer observed; or
C)
has been otherwise eliminated; or
2)
The container is very small, such as an
ampule; or
3)
The container is designed to hold free liquids for use other
than storage, such as a battery or capacitor; or
4)
The container is a lab pack as defined in Section 724.416
and is disposed of in accordance with Section 724.416.
242
d)
To demonstrate the absence or presence of free liquids in either a
containerized or a bulk waste, the following test must be used:
Method 9095 (Paint Filter Liquids Test), as described in "Test
Methods for Evaluating Solid Wastes, Physical/Chemical Methods",
U.S. EPA Publication No. SW
-846, incorporated by reference in 35
Ill. Adm. Code 720.111.
e)
The placement of any liquids that is not a hazardous waste in a
landfill is prohibited (35 Ill. Adm. Code 729.311).
f)
Sorbents used to treat free liquids to be disposed of in landfills
must be nonbiodegradable.
Nonbiodegradable
sorbents are:
materials listed or described in subsection (f)(1) below;
materials that pass one of the tests in subsection (f)(2) below;
or materials that are determined by Board to be
nonbiodegradable
through the 35 Ill. Adm. Code 106 adjusted standard process.
1)
Nonbiodegradable
sorbents are:
A)
Inorganic minerals, other inorganic materials, and
elemental carbon (e.g.,
aluminosilicates, clays,
smectites, Fuller's earth,
bentonite, calcium
bentonite, montmorillonite,
calcined montmorillonite,
kaolinite, micas (
illite), vermiculites, zeolites;
calcium carbonate (organic free limestone);
oxides/hydroxides,
alumina, lime, silica (sand),
diatomaceous earth;
perlite (volcanic glass); expanded
volcanic rock; volcanic ash; cement kiln dust; fly
ash; rice hull ash; activated charcoal/activated
carbon); or
B)
High molecular weight synthetic polymers (e.g.,
polyethylene, high density polyethylene (HDPE),
polypropylene, polystyrene, polyurethane,
polyacrylate, polynorborene, polysobutylene, ground
synthetic rubber, cross-linked
allylstyrene and
tertiary butyl copolymers). This does not include
polymers derived from biological material or polymers
specifically designed to be degradable; or
C)
Mixtures of these
nonbiodegradable materials.
2)
Tests for nonbiodegradable
sorbents.
A)
The sorbent material is determined to be
nonbiodegradable under ASTM Method G21-70 (1984a)
--
"Standard Practice for Determining Resistance of
Synthetic Polymer Materials to Fungi", incorporated by
reference in 35 Ill. Adm. Code 720.111;
or
B)
The sorbent material is determined to be
nonbiodegradable under ASTM Method G22-76 (1984b)
--
"Standard Practice for Determining Resistance of
Plastics to Bacteria", incorporated by reference in 35
Ill. Adm. Code 720.111
; or
C)
The sorbent material is determined to be non-
biodegradable under OECD test 301B [CO
2
Evolution
(Modified Sturm Test)], incorporated by reference in
35 Ill. Adm. Code 720.111.
243
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART AA: AIR EMISSION STANDARDS FOR PROCESS VENTS
Section 725.930
Applicability
a)
This Subpart applies to owners and operators of facilities that
treat, store or dispose of hazardous wastes (except as provided in
Section 725.101).
b)
Except for Section
s 725.934(d) and 725.935 (e), this Subpart
applies to process vents associated with distillation,
fractionation, thin-film evaporation, solvent extraction, or air
or steam stripping operations that manage hazardous wastes with
organic concentrations of at least 10
ppmw (parts per million by
weight), if these operations are conducted in
one of the
following :
1) UA units that areis subject to the permitting requirements
of 35 Ill. Adm. Code
702, 703, and 705 ; or
2) HA unit (including a h
azardous waste recycling unit
s) that
areis not exempt from permitting under the provisions of 35
Ill. Adm. Code 262.34(a) (i.e., a hazardous waste recycling
unit that is not a 90-day tank or container) and that is
located on a hazardous waste management
facilities facility
otherwise subject to the permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705 .
BOARD NOTE: The requirements of Sections 725.932 through
725.936 apply to process vents on hazardous waste recycling
units previously exempt under 35 Ill. Adm. Code
721.106(c)(1). Other exemptions under 35 Ill. Adm. Code
721.104, 722.134 and 725.101(c) are not affected by these
requirements.
c)
Agency deci sions pursuant to this Part must be made in writing,
are in the nature of permit decisions pursuant to Section 39 of
the Environmental Protection Act and may be appealed to the Board
pursuant to 35 Ill. Adm. Code 105.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.933
Standards: Closed-vent Systems and Control Devices
a)
Compliance Required.
1)
Owners or operators of closed-vent systems and control
devices used to comply with provisions of this Part shall
comply with the provisions of this Section.
2)
The owner or operator of an existing facility that cannot
install a closed-vent system and control device to comply
with the provisions of this Subpart on the effective date
that the facility becomes subject to the provisions of this
Subpart shall prepare an implementation schedule that
includes dates by which the closed-vent system and control
device will be installed and in operation. The controls
must be installed as soon as possible, but the
244
implementation schedule may allow up to
1830 months after
the effective date that the facility becomes subject to this
Subpart for installation and startup. All units that begin
operation after December 21, 1990, must comply with the
rules immediately (i.e., must have control devices installed
and operating on startup of the affected unit); the 2-year
implementation schedule does not apply to these units.
b)
A control device involving vapor recovery (e.g., a condenser or
adsorber) must be designed and operated to recover the organic
vapors vented to it with an efficiency of 95 weight percent or
greater unless the total organic emission limits of Section
725.932(a)(1) for all affected process vents is attained at an
efficiency less than 95 weight percent.
c)
An enclosed combustion device (e.g., a vapor incinerator, boiler,
or process heater) must be designed and operated to reduce the
organic emissions vented to it by 95 weight percent or greater; to
achieve a total organic compound concentration of 20
ppmv,
expressed as the sum of the actual compounds, not carbon
equivalents, on a dry basis corrected to 3 percent oxygen; or to
provide a minimum residence time of 0.50 seconds at a minimum
temperature of 760
ยฐ
C. If a boiler or process heater is used as
the control device, then the vent stream must be introduced into
the flame combustion zone of the boiler or process heater.
d)
Flares
1)
A flare must be designed for and operated with no visible
emissions as determined by the methods specified in
subsection (e)(1) below except for periods not to exceed a
total of 5 minutes during any 2 consecutive hours.
2)
A flare must be operated with a flame present at all times,
as determined by the methods specified in subsection
(f)(2)(c) below.
3)
A flare must be used only if the net heating value of the
gas being combusted is 11.2 MJ/
scm (300 Btu/ scf) or greater
if the flare is steam-assisted or air-assisted, or if the
net heating value of the gas being combusted is 7.45 MJ/
scm
(200 Btu/ scf) or greater if the flare is
nonassisted. The
net heating value of the gas being combusted must be
determined by the methods specified in subsection (e)(2)
below.
4)
Exit Velocity.
A)
A steam-assisted or
nonassisted flare must be designed
for and operated with an exit velocity, as determined
by the methods specified in subsection (e)(3) below,
less than 18.3 m/s (60 ft/s), except as provided in
subsections (d)(4)(B) and (d)(4)(C) below.
B)
A steam-assisted or
nonassisted flare designed for and
operated with an exit velocity, as determined by the
methods specified in subsection (e)(3) below, equal to
or greater than 18.3 m/s (60 ft/s) but less than 122
m/s (400 ft/s) is allowed if the net heating value of
the gas being combusted is greater than 37.3 MJ/
scm
(1000 Btu/ scf).
245
C)
A steam-assisted or
nonassisted flare designed for and
operated with an exit velocity, as determined by the
methods specified in subsection (e)(3) below, less
than the velocity, V as determined by the method
specified in subsection (e)(4) and less than 122 m/s
(400 ft/s) is allowed.
5)
An air-assisted flare must be designed and operated with an
exit velocity less than the velocity, V as determined by the
method specified in subsection (e)(5) below.
6)
A flare used to comply with this Section must be steam-
assisted, air-assisted, or
nonassisted.
e)
Compliance determination and equations.
1)
Reference Method 22 in 40 CFR 60, incorporated by reference
in 35 Ill. Adm. Code 720.111, must be used to determine the
compliance of a flare with the visible emission provisions
of this Subpart. The observation period is 2 hours and must
be used according to Method 22.
2)
The net heating value of the gas being combusted in a flare
must be calculated using the following equation:
Where:
H
T
is the net heating value of the sample in MJ/
scm;
where the net enthalpy per mole of
offgas is based on
combustion at 25
ยฐ
C and 760 mm Hg, but the standard
temperature for determining the volume
corrersponding
to 1 mole is 20
ยฐ
C.
K = 1.74
ร
10
-7
(1/ppm)(g mol/scm)(MJ/kcal) where
standard temperature for (g
mol/scm) 20
ยฐ
C.
ฮฃ
X
i
means the sum of the values of X for each
component i, from i=1 to n.
C
i
is the concentration of sample component i in
ppm
on a wet basis, as measured for
organics by Reference
Method 18 in 40 CFR 60, and for carbon monoxide, by
ASTM D 1946-90, incorporated by reference in 35 Ill.
Adm. Code 720.111.
H
i
is the net heat of combustion of sample component
i, kcal/ gmol at 25
ยฐ
C and 760 mm Hg. The heats of
combustion must be determined using ASTM D 2382-88,
incorporated by reference in 35 Ill. Adm. Code
720.111, if published values are not available or
T
i
i
H
= K
i
n
C
H
ร
=
โ
ร
1
246
cannot be calculated.
3)
The actual exit velocity of a flare must be determined by
dividing the volumetric flow rate (in units of standard
temperature and pressure), as determined by Reference
Methods 2, 2A, 2C, or 2D in 40 CFR 60, incorporated by
reference in 35 Ill. Adm. Code 720.111, as appropriate, by
the unobstructed (free) cross-sectional area of the flare
tip.
4)
The maximum allowed velocity in m/s, V for a flare complying
with subsection (d)(4)(C) above must be determined by the
following equation:
Where:
Log
10
means logarithm to the base 10
H
T
is the net heating value as determined in
subsection (e)(2) above.
5)
The maximum allowed velocity in m/s, V for an air-assisted
flare must be determined by the following equation:
Where:
H
T
is the net heating value as determined in
subsection (e)(2) above.
f)
The owner or operator shall monitor and inspect each control
device required to comply with this Section to ensure proper
operation and maintenance of the control device by implementing
the following requirements:
1)
Install, calibrate, maintain, and operate according to the
manufacturer's specifications a flow indicator that provides
a record of vent stream flow from each affected process vent
to the control device at least once every hour. The flow
indicator sensor must be installed in the vent stream at the
nearest feasible point to the control device inlet but
before being combined with other vent streams.
2)
Install, calibrate, maintain, and operate according to the
manufacturer's specifications a device to continuously
monitor control device operation as specified below:
A)
For a thermal vapor incinerator, a temperature
monitoring device equipped with a continuous recorder.
The device must have accuracy of ยฑ 1 percent of the
temperature being monitored in
ยฐ
C or ยฑ 0.5
ยฐ
C,
whichever is greater. The temperature sensor must be
installed at a location in the combustion chamber
log(
)
(
.
) /
.
V
H
T
=
+
288
317
V = 8.706 +0.7084 H
T
247
downstream of the combustion zone.
B)
For a catalytic vapor incinerator, a temperature
monitoring device equipped with a continuous recorder.
The device must be capable of monitoring temperature
at two locations and have an accuracy of ยฑ 1 percent
of the temperature being monitored in C or ยฑ 0.5
ยฐ
C,
whichever is greater. One temperature sensor must be
installed in the vent stream at the nearest feasible
point to the catalyst bed inlet and a second
temperature sensor must be installed in the vent
stream at the nearest feasible point to the catalyst
bed outlet.
C)
For a flare, a heat sensing monitoring device equipped
with a continuous recorder that indicates the
continuous ignition of the pilot flame.
D)
For a boiler or process heater having a design heat
input capacity less than 44 MW, a temperature
monitoring device equipped with a continuous recorder.
The device must have an accuracy of ยฑ 1 percent of
the temperature being monitored in
ยฐ
C or ยฑ 0.5
ยฐ
C,
whichever is greater. The temperature sensor must be
installed at a location in the furnace downstream of
the combustion zone.
E)
For a boiler or process heater having a design heat
input capacity greater than or equal to 44 MW, a
monitoring device equipped with a continuous recorder
to measure parameters that indicates good combustion
operating practices are being used.
F)
For a condenser, either:
i)
A monitoring device equipped with a continuous
recorder to measure the concentration level of
the organic compounds in the exhaust vent stream
from the condenser; or
ii)
A temperature monitoring device equipped with a
continuous recorder. The device must be capable
of monitoring temperature
at two locations and
havewith an accuracy of ยฑ1 percent of the
temperature being monitored in
degrees Celsius
(
ยฐ
C) or ยฑ0.5
ยฐ
C, whichever is greater.
OneThe
temperature sensor must be installed at a
location in the exhaust vent stream from the
condenser , and a second temperature sensor must
be installed at a location in the coolant fluid
exiting the condenser
(i.e., product side)
.
G)
For a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed
directly in the control device, either:
i)
A monitoring device equipped with a continuous
recorder to measure the concentration level of
the organic compounds in the exhaust vent stream
from the carbon bed; or
248
ii)
A monitoring device equipped with a continuous
recorder to measure a parameter that indicates
the carbon bed is regenerated on a regular,
predetermined time cycle.
3)
Inspect the readings from each monitoring device required by
subsection (f)(1) and (f)(2) above at least once each
operating day to check control device operation and, if
necessary, immediately implement the corrective measures
necessary to ensure the control device operates in
compliance with the requirements of this Section.
g)
An owner or operator using a carbon adsorption system such as a
fixed-bed carbon
adsorber that regenerates the carbon bed directly
onsite in the control device shall replace the existing carbon in
the control device with fresh carbon at a regular, predetermined
time interval that is no longer than the carbon service life
established as a requirement of Section 725.935(b)(4)(C)(vi).
h)
An owner or operator using a carbon adsorption system, such as a
carbon canister, that does not regenerate the carbon bed directly
onsite in the control device shall replace the existing carbon in
the control device with fresh carbon on a regular basis by using
one of the following procedures:
1)
Monitor the concentration level of the organic compounds in
the exhaust vent stream from the carbon adsorption system on
a regular schedule, and replace the existing carbon with
fresh carbon immediately when carbon breakthrough is
indicated. The monitoring frequency must be daily or at an
interval no greater than 20 percent of the time required to
consume the total carbon working capacity established as a
requirement of Section 725.935(b)(4)(C)(vii), whichever is
longer.
2)
Replace the existing carbon with fresh carbon at a regular,
predetermined time interval that is less than the design
carbon replacement interval established as a requirement of
Section 725.935(b)(4)(C)(vii).
i)
An owner or operator of an affected facility seeking to comply
with the provisions of this Part by using a control device other
than a thermal vapor incinerator, catalytic vapor incinerator,
flare, boiler, process heater, condenser, or carbon adsorption
system is required to develop documentation including sufficient
information to describe the control device operation and identify
the process parameter or parameters that indicate proper operation
and maintenance of the control device.
j) Closed vent systems. A closed vent system must meet either of the
following design requirements:
1) CA closed-vent system
s must be designed
for andto operate d
with no detectable emissions, as indicated by an instrument
reading of less than 500
ppmv above background
and by visual
inspections , as determined by the methods specified at
Section 725.934(b)
., and by visual inspections; or
2) Closed-vent systems must be monitored to determine
compliance with this Section during the initial leak
detection monitoring, which must be conducted by the date
249
that the facility becomes subject to the provisions of this
Section annually, and at other times as specified by the
Agency pursuant to Section 725.930(c). For the annual leak
detection monitoring after the initial leak detection
monitoring, the owner or operator is not required to monitor
those closed-vent system components that continuously
operate in vacuum service or those closed-vent system
joints, seams, or other connections that are permanently or
semi-permanently sealed (e.g., a welded joint between two
sections of metal pipe or a bolted and
gasketed pipe
flange). A closed -vent s ystem must be designed to operate at
a pressure below atmospheric pressure. The system must be
equipped with at least one pressure gauge or other pressure
measurement device that can be read from a readily
accessible location to verify that negative pressure is
being maintained in the closed
-vent system when the control
device is operating.
3) Detectable emissions, as indicated by an instrument reading
greater than 500
ppm and visual inspections, must be
controlled as soon as practicable, but not later than 15
calendar days after the emission is detected.
4) A first attempt at repair must be made no later than 5
calendar days after the emission is detected..
k)
The owner or operator shall monitor and inspect each closed-vent
system required to comply with this Section to ensure proper
operation and maintenance of the closed
-vent system by
implementing the following requirements:
1)
Each closed -vent system that is used to comply with
subsection (j)(1) above shall be inspected and monitored in
accordance with the following requirements:
A)
An initial leak detection monitoring of the
closed -vent system shall be conducted by the owner or
operator on or before the date that the system becomes
subject to this Section. The owner or operator shall
monitor the closed
-vent system components and
connections using the procedures specified in Section
725.934(b) to demonstrate that the closed
-vent system
operates with no detectable emissions, as indicated by
an instrument reading of less than 500
ppmv above
background.
B)
After initial leak detection monitoring required in
subsection (k)(1)(A) above, the owner or operator
shall inspect and monitor the closed
-vent system as
follows:
i)
Closed -vent system joints, seams, or other
connections that are permanently or
semi-permanently sealed (e.g., a welded joint
between two Sections of hard piping or a bolted
and gasketed ducting flange) must be visually
inspected at least once per year to check for
defects that could result in air pollutant
emissions. The owner or operator shall monitor
a component or connection using the procedures
specified in Section 725.934(b) to demonstrate
250
that it operates with no detectable emissions
following any time the component is repaired or
replaced (e.g., a Section of damaged hard piping
is replaced with new hard piping) or the
connection is unsealed (e.g., a flange is
unbolted).
ii)
Closed -vent system components or connections
other than those specified in subsection
(k)(1)(B)(i) above must be monitored annually
and at other times as requested by the Regional
Administrator, except as provided for in
subsection (n) below, using the procedures
specified in Section 725.934(b) to demonstrate
that the components or connections operate with
no detectable emissions.
C)
In the event that a defect or leak is detected, the
owner or operator shall repair the defect or leak in
accordance with the requirements of subsection (k)(3)
below.
D)
The owner or operator shall maintain a record of the
inspection and monitoring in accordance with the
requirements specified in Section 725.935.
2)
Each closed -vent system that is used to comply with
subsection (j)(2) above must be inspected and monitored in
accordance with the following requirements:
A)
The closed -vent system must be visually inspected by
the owner or operator to check for defects that could
result in air pollutant emissions. Defects include,
but are not limited to, visible cracks, holes, or gaps
in ductwork or piping or loose connections.
B)
The owner or operator shall perform an initial
inspection of the closed
-vent system on or before the
date that the system becomes subject to this Section.
Thereafter, the owner or operator shall perform the
inspections at least once every year.
C)
In the event that a defect or leak is detected, the
owner or operator shall repair the defect in
accordance with the requirements of subsection (k)(3)
below.
D)
The owner or operator shall maintain a record of the
inspection and monitoring in accordance with the
requirements specified in Section 725.935.
3)
The owner or operator shall repair all detected defects as
follows:
A)
Detectable emissions, as indicated by visual
inspection or by an instrument reading greater than
500 ppmv above background, must be controlled as soon
as practicable, but not later than 15 calendar days
after the emission is detected, except as provided for
in subsection (k)(3)(C) below.
251
B)
A first attempt at repair must be made no later than
five calendar days after the emission is detected.
C)
Delay of repair of a closed
-vent system for which
leaks have been detected is allowed if the repair is
technically infeasible without a process unit
shutdown, or if the owner or operator determines that
emissions resulting from immediate repair would be
greater than the fugitive emissions likely to result
from delay of repair. Repair of such equipment must
be completed by the end of the next process unit
shutdown.
D)
The owner or operator shall maintain a record of the
defect repair in accordance with the requirements
specified in Section 725.935.
kl) CA closed-vent system
s andor control device s used to comply with
provisions of this Subpart must be operated at all times when
emissions may be vented to
themit.
lm)
The owner or operator using a carbon adsorption system
to control
air pollutant emissions
shall document that all carbon removed
that is a hazardous waste and that is removed
from the control
device is managed in one of the following manners
, regardless of
the volatile organic concentration of the carbon
:
1)
It is regenerated or reactivated in a thermal treatment unit
that is permitted under 35 Ill. Adm. Code 724.Subpart X or
725.Subpart P,meets one of the following:
A)
The owner or operator of the unit has been issued a
final permit under 35 Ill. Adm. Code 702, 703, and 705
that implements the requirements of 35 Ill. Adm. Code
724.Subpart X; or
B)
The unit is equipped with and operating air emission
controls in accordance with the applicable
requirements of 725.Subparts AA and CC or 35 Ill. Adm.
Code 724; or
C)
The unit is equipped with and operating air emission
controls in accordance with a national emission
standard for hazardous air pollutants under 40 CFR 61
or 40 CFR 63.
2)
It is incinerated
by a process that is permitted under 35
Ill. Adm. Code 724.Subpart O or 725.Subpart O,
orin a
hazardous waste incinerator for which the owner or operator
has done either of the following:
A)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
724.Subpart O, or
B)
The owner or operator has designed and operates the
incinerator in accordance with the interim status
requirements of 725.Subpart O; or
3)
It is burned in a boiler or industrial furnace
that is
252
permitted under 35 Ill. Adm. Code 726.Subpart
H.for which
the owner or operator has done either of the following:
A)
The owner or operator has been issued a final permit
under 35 Ill. Adm. Code 702, 703, and 705 that
implements the requirements of 35 Ill. Adm. Code
726.Subpart H, or
B)
The owner or operator has designed and operates the
boiler or industrial furnace in accordance with the
interim status requirements of 35 Ill. Adm. Code
726.Subpart H.
n)
Any components of a closed
-vent system that are designated, as
described in Section 725.935(c)(9), as unsafe to monitor are
exempt from the requirements of subsection (k)(1)(B)(ii) above if
both of the following conditions are fulfilled:
1)
The owner or operator of the closed
-vent system has
determined that the components of the closed
-vent system are
unsafe to monitor because monitoring personnel would be
exposed to an immediate danger as a consequence of complying
with subsection (k)(1)(B)(ii) above; and
2)
The owner or operator of the closed
-vent system adheres to a
written plan that requires monitoring the closed
-vent system
components using the procedure specified in subsection
(k)(1)(B)(ii) as frequently as practicable during
safe-to-monitor times.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.934
Test Methods and Procedures
a)
Each owner or operator subject to the provisions of this Subpart
shall comply with the test methods and procedures requirements
provided in this Section
b)
When a closed-vent system is tested for compliance with no
detectable emissions, as required in Section 725.933(
jk), the test
must comply with the following requirements:
1)
Monitoring must comply with Reference Method 21 in 40 CF
R
60, incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The detection instrument must meet the performance criteria
of Reference Method 21.
3)
The instrument must be calibrated before use on each day of
its use by the procedures specified in Reference Method 21.
4)
Calibration gases must be:
A)
Zero air (less than 10
ppm of hydrocarbon in air).
B)
A mixture of methane or n-hexane and air at a
concentration of approximately, but less than, 10,000
ppm methane or n-hexane.
5)
The background level must be determined as set forth in
Reference Method 21.
253
6)
The instrument probe must be traversed around all potential
leak interfaces as close to the interface as possible as
described in Reference Method 21.
7)
The arithmetic difference between the maximum concentration
indicated by the instrument and the background level is
compared with 500
ppm for determining compliance.
c)
Performance tests to determine compliance with Section 725.932(a)
and with the total organic compound concentration limit of Section
725.933(c) must comply with the following:
1)
Performance tests to determine total organic compound
concentrations and mass flow rates entering and exiting
control devices must be conducted and data reduced in
accordance with the following reference methods and
calculation procedures:
A)
Method 2 in 40 CFR 60 for velocity and volumetric flow
rate.
B)
Method 18 in 40 CFR 60 for organic content.
C)
Each performance test must consist of three separate
runs, each run conducted for at least 1 hour under the
conditions that exist when the hazardous waste
management unit is operating at the highest load or
capacity level reasonably expected to occur. For the
purpose of determining total organic compound
concentrations and mass flow rates, the average of
results of all runs applies. The average must be
computed on a time-weighed basis.
D)
Total organic mass flow rates must be determined by
the following equation:
F = K * Q * SUM( Ci * MWi)
Where:
F is the total organic mass flow rate, kg/h.
K = 4.16 E -8, conversion factor for molar
volume, kg- mol/cubic m, at 293 K and 760 mm Hg.
Q = volumetric flow rate of gases entering or
exiting control device,
dscm/h, as determined by
Method 2 in 40 CFR 60, incorporated by reference
in 35 Ill. Adm. Code 720.111.
SUM(Xi) means the sum of the values of X for
each component i, from i=1 to n.
n = number of organic compounds in the vent gas.
Ci is the organic concentration in
ppm, dry
basis, of compound i in the vent gas, as
determined by Method 18 in 40 CFR 60.
MWi is the molecular weight of organic compound
254
i in the vent gas, kg/kg-
mol.
Where:
E
h
= The total organic mass flow rate, kg/h.
Q
2sd
= The volumetric flow rate of gases entering
or exiting control device,
dscm/h, as
determined by Method 2 in 40 CFR 60,
incorporated by reference in 35 Ill. Adm.
Code 720.111.
n = The number of organic compounds in the vent
gas.
C
i
= The organic concentration in
ppm, dry
basis, of compound i in the vent gas, as
determined by Method 18 in 40 CFR 60.
MW
i
= The molecular weight of organic compound i
in the vent gas, kg/kg-
mol.
0.0416 = The conversion factor for molar volume,
kg-mol/m
3
, at 293 K and 760 mm Hg.
10
-6
= The conversion factor from
ppm.
E)
The annual total organic emission rate must be
determined by the following equation:
A = F *
ร
HOURS
Where:
A is total organic emission rate,
kg/y.
F is the total organic mass flow rate, kg/h, as
calculated in subsection (c)(1)(D)
above .
HOURS is the total annual hours of operation for
the affected unit.
F)
Total organic emissions from all affected process
vents at the facility must be determined by summing
the hourly total organic mass emissions rates (F as
determined in subsection (c)(1)(D)
above ) and by
summing the annual total organic mass emission rates
(A as determined in subsection (c)(1)(E)
above ) for
all affected process vents at the facility.
2)
The owner or operator shall record such process information
as is necessary to determine the conditions of the
h
2sd
i
i
-6
E
= Q
x(
n
i = 1
C
x MW
)x0.0416x10
โ
255
performance tests. Operations during periods of startup,
shutdown and malfunction do not constitute representative
conditions for the purpose of a performance test.
3)
The owner or operator of an affected facility shall provide,
or cause to be provided, performance testing facilities as
follows:
A)
Sampling ports adequate for the test methods specified
in subsection (c)(1)
above .
B)
Safe sampling platform(s).
C)
Safe access to sampling platform(s).
D)
Utilities for sampling and testing equipment.
4)
For the purpose of making compliance determinations, the
time-weighted average of the results of the three runs must
apply. In the event that a sample is accidentally lost or
conditions occur in which one of the three runs must be
discontinued because of forced shutdown, failure of an
irreplaceable portion of the sample train, extreme
meteorological conditions or other circumstances beyond the
owner or operator's control, compliance may, upon the
Agency's approval, be determined using the average of the
results of the two other runs.
d)
To show that a process vent associated with a hazardous waste
distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation is not subject to
the requirements of this Subpart, the owner or operator shall make
an initial determination that the time-weighted, annual average
total organic concentration of the waste managed by the waste
management unit is less than 10
ppmw using one of the following
two methods:
1)
Direct measurement of the organic concentration of the waste
using the following procedures:
A)
The owner or operator shall take a minimum of four
grab samples of waste for each wastestream managed in
the affected unit under process conditions expected to
cause the maximum waste organic concentration.
B)
For waste generated onsite, the grab samples must be
collected at a point before the waste is exposed to
the atmosphere such as in an enclosed pipe or other
closed system that is used to transfer the waste after
generation to the first affected distillation,
fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation. For
waste generated offsite, the grab samples must be
collected at the inlet to the first waste management
unit that receives the waste provided the waste has
been transferred to the facility in a closed system
such as a tank truck and the waste is not diluted or
mixed with other waste.
C)
Each sample must be analyzed and the total organic
concentration of the sample must be computed using
256
Method 9060 or 8240 of SW-846
, (incorporated by
reference under 35 Ill. Adm. Code 720.111.
D)
The arithmetic mean of the results of the analyses of
the four samples apply for each wastestream managed in
the unit in determining the time-weighted, annual
average total organic concentration of the waste. The
time-weighted average is to be calculated using the
annual quantity of each waste stream processed and the
mean organic concentration of each wastestream managed
in the unit.
2)
Using knowledge of the waste to determine that its total
organic concentration is less than 10
ppmw. Documentation
of the waste determination is required. Examples of
documentation that must be used to support a determination
under this subsection include:
A)
Production process information documenting that no
organic compounds are used.
B)
Information that the waste is generated by a process
that is identical to a process at the same or another
facility that has previously been demonstrated by
direct measurement to generate a wastestream having a
total organic content less than 10
ppmw, or
C)
Prior speciation analysis results on the same
wastestream where it is documented that no process
changes have occurred since that analysis that could
affect the waste total organic concentration.
e)
The determination that distillation, fracti
onation, thin-film
evaporation, solvent extraction, or air or steam stripping
operations which manage hazardous wastes with time-weighted,
annual average total organic concentrations less than 10
ppmw must
be made as follows:
1)
By the effective date that the facility becomes subject to
the provisions of this Subpart or by the date when the waste
is first managed in a waste management unit, whichever is
later; and
2)
For continuously generated waste, annually; or
3)
Whenever there is a change in th
e waste being managed or a
change in the process that generates or treats the waste.
f)
When an owner or operator and the Agency do not agree on whether a
distillation, fractionation, thin-film evaporation, solvent
extraction, or air or steam stripping operation manages a
hazardous waste with organic concentrations of at least 10
ppmw
based on knowledge of the waste, the procedures in Method 8240 in
SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111,
must be used to resolve the dispute.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.935
Recordkeeping Requirements
a)
Compliance Required.
257
1)
Each owner or operator subject to the provisions of this
Subpart shall comply with the
recordkeeping requirements of
this Section.
2)
An owner or operator of more than one hazardous waste
management unit subject to the provisions of this Subpart
may comply with the
recordkeeping requirements for these
hazardous waste management units in one
recordkeeping system
if the system identifies each record by each hazardous waste
management unit.
b)
Owners and operators shall record the following information in the
facility operating record:
1)
For facilities that comply with the provisions of Section
725.933(a)(2), an implementation schedule that includes
dates by which the closed-vent system and control device
will be installed and in operation. The schedule must also
include a rationale of why the installation cannot be
completed at an earlier date. The implementation schedule
must be in the facility operating record by the effective
date that the facility becomes subject to the provisions of
this Subpart.
2)
Up-to-date documentation of compliance with the process vent
standards in Section 725.932, including:
A)
Information and data identifying all affected process
vents, annual throughput and operating hours of each
affected unit, estimated emission rates for each
affected vent and for the overall facility (i.e., the
total emissions for all affected vents at the
facility), and the approximate location within the
facility of each affected unit (e.g., identify the
hazardous waste management units on a facility plot
plan).
B)
Information and data supporting determination of vent
emissions and emission reductions achieved by add-on
control devices based on engineering calculations or
source tests. For the purpose of determining
compliance, determinations of vent emissions and
emission reductions must be made using operating
parameter values (e.g., temperatures, flow rates, or
vent stream organic compounds and concentrations) that
represent the conditions that result in maximum
organic emissions, such as when the waste management
unit is operating at the highest load or capacity
level reasonably expected to occur. If the owner or
operator takes any action (e.g., managing a waste of
different composition or increasing operating hours of
affected waste management units) that would result in
an increase in total organic emissions from affected
process vents at the facility, then a new
determination is required.
3)
Where an owner or operator chooses to use test date to
determine the organic removal efficiency or total organic
compound concentration achieved by the control device, a
performance test plan. The test plan must include:
258
A)
A description of how it is determined that the planned
test is going to be conducted when the hazardous waste
management unit is operating at the highest load or
capacity level reasonably expected to occur. This
must include the estimated or design flow rate and
organic content of each vent stream and define the
acceptable operating ranges of key process and control
device parameters during the test program.
B)
A detailed engineering description of the closed-vent
system and control device including:
i)
Manufacturer's name and model number of control
device.
ii)
Type of control device.
iii) Dimensions of the control device.
iv)
Capacity.
v)
Construction materials.
C)
A detailed description of s
ampling and monitoring
procedures, including sampling and monitoring
locations in the system, the equipment to be used,
sampling and monitoring frequency, and planned
analytical procedures for sample analysis.
4)
Documentation of compliance with Section 725.933 must
include the following information:
A)
A list of all information references and sources used
in preparing the documentation.
B)
Records, including the dates of each compliance test
required by Section 725.933(j).
C)
If engineering calculations are used, a design
analysis, specifications, drawings, schematics, and
piping and instrumentation diagrams based on the
appropriate sections of APTI Course 415 (incorporated
by reference in 35 Ill. Adm. Code 720.111) or other
engineering texts, approved by the Agency, that
present basic control device design information.
Documentation provided by the control device
manufacturer or vendor that describes the control
device design in accordance with subsections
(b)(4)(C)(i) through (vii)
, below , may be used to
comply with this requirement. The design analysis
must address the vent stream characteristics and
control device operation parameters as specified
below.
i)
For a thermal vapor incinerator, the design
analysis must consider the vent stream
composition, constituent concentrations and flow
rate. The design analysis must also establish
the design minimum and average temperature in
the combustion zone and the combustion zone
259
residence time.
ii)
For a catalytic vapor incinerator, the
design
analysis must consider the vent stream
composition, constituent concentrations, and
flow rate. The design analysis must also
establish the design minimum and average
temperatures across the catalyst bed inlet and
outlet.
iii)
For a boiler or process heater, the design
analysis must consider the vent stream
composition, constituent concentrations and flow
rate. The design analysis must also establish
the design minimum and average flame zone
temperatures, combustion zone residence time and
description of method and location where the
vent stream is introduced into the combustion
zone.
iv)
For a flare, the design analysis must consider
the vent stream composition, constituent
concentrations, and flow rate. The design
analysis must also consider the requirements
specified in Section 725.933(d).
v)
For a condenser, the design analysis must
consider the vent stream composition,
constituent concentrations, flow rate, relative
humidity and temperature. The design analysis
must also establish the design outlet organic
compound concentration level, design average
temperature of the condenser exhaust vent stream
and design average temperatures of the coolant
fluid at the condenser inlet and outlet.
vi)
For a carbon adsorption system such as a fixed-
bed adsorber that regenerates the carbon bed
directly onsite in the control device, the
design analysis must consider the vent stream
composition, constituent concentrations, flow
rate, relative humidity and temperature. The
design analysis must also establish the design
exhaust vent stream organic compound
concentration level, number and capacity of
carbon beds, type and working capacity of
activated carbon used for carbon beds, design
total steam flow over the period of each
complete carbon bed regeneration cycle, duration
of the carbon bed steaming and cooling/drying
cycles, design carbon bed temperature after
regeneration, design carbon bed regeneration
time and design service life of carbon.
vii)
For a carbon adsorption system such as a
carbon
canister that does not regenerate the carbon bed
directly onsite in the control device, the
design analysis must consider the vent stream
composition, constituent concentrations, flow
rate, relative humidity and temperature. The
design analysis must also establish the design
260
outlet organic concentration level, capacity of
carbon bed, type and working capacity of
activated carbon used for carbon bed and design
carbon replacement interval based on the total
carbon working capacity of the control device
and source operating schedule.
D)
A statement signed and dated by the owner or operator
certifying that the operating parameters used in the
design analysis reasonably represent the conditions
that exist when the hazardous waste management unit is
or would be operating at the highest load or capacity
level reasonably expected to occur.
E)
A statement signed and dated by the owner or operator
certifying that the control device is designed to
operate at an efficiency of 95 percent or greater
unless the total organic concentration limit of
Section 725.932(a) is achieved at an efficiency less
than 95 weight percent or the total organic emission
limits of Section 725.932(a) for affected process
vents at the facility are attained by a control device
involving vapor recovery at an efficiency less than 95
weight percent. A statement provided by the control
device manufacturer or vendor certifying that the
control equipment meets the design specifications may
be used to comply with this requirement.
F)
If performance tests are used to demonstrate
compliance, all test results.
c)
Design documentation and monitoring operating and inspection
information for each closed-vent system and control device
required to comply with the provisions of this Part must be
recorded and kept up-to-date in the facility operating record.
The information must include:
1)
Description and date of each modification that is made to
the closed-vent system or control device design.
2)
Identification of operating parameter,
description of
monitoring device, and diagram of monitoring sensor location
or locations used to comply with Section 725.933(f)(1) and
(2).
3)
Monitoring, operating and inspection information required by
Section 725.933(f) through (k).
4)
Date, time and duration of each period that occurs while the
control device is operating when any monitored parameter
exceeds the value established in the control device design
analysis as specified below:
A)
For a thermal vapor incinerator designed to operate
with a minimum residence time of 0.50 second at a
minimum temperature of 760 C, any period when the
combustion temperature is below 760 C.
B)
For a thermal vapor incinerator designed to operate
with an organic emission reduction efficiency of 95
percent or greater, any period when the combustion
261
zone temperature is more than 28 C below the design
average combustion zone temperature established as a
requirement of subsection (b)(4)(C)(i)
, above.
C)
For a catalytic vapor incinerator, any period when:
i)
Temperature of the vent stream at the catalyst
bed inlet is more than 28 C below the average
temperature of the inlet vent stream established
as a requirement of subsection (b)(4)(C)(ii)
,
above; or
ii)
Temperature difference across the catalyst bed
is less than 80 percent of the design average
temperature difference established as a
requirement of subsection (b)(4)(C)(ii)
, above.
D)
For a boiler or process heater, any period when:
i)
Flame zone temperature is more than 28 C below
the design average flame zone temperature
established as a requirement of subsection
(b)(4)(C)(iii) , above; or
ii)
Position changes where the vent stream is
introduced to the combustion zone from the
location established as a requirement of
subsection (b)(4)(C)(iii)
, above.
E)
For a flare, period when the pilot flame is not
ignited.
F)
For a condenser that complies with Section
725.933(f)(2)(F)(i), any period when the organic
compound concentration level or readings of organic
compounds in the exhaust vent stream from the
condenser are more than 20 percent greater than the
design outlet organic compound concentration level
established as a requirement of subsection
(b)(4)(C)(v) , above.
G)
For a condenser that complies with Section
725.933(f)(2)(F)(ii), any period when:
i)
Temperature of the exhaust vent stream from the
condenser is more than 6 C above the design
average exhaust vent stream temperature
established as a requirement of subsection
(b)(4)(C)(v) , above.
ii)
Temperature of the coo
lant fluid exiting the
condenser is more than 6 C above the design
average coolant fluid temperature at the
condenser outlet established as a requirement of
subsection (b)(4)(C)(v)
, above.
H)
For a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed
directly onsite in the control device and complies
with Section 725.933(f)(2)(G)(i), any period when the
organic compound concentration level or readings of
organic compounds in the exhaust vent stream from the
262
carbon bed are more than 20 percent greater than the
design exhaust vent stream organic compound
concentration level established as a requirement of
subsection (b)(4)(C)(vi)
, above.
I)
For a carbon adsorption system such as a fixed-bed
carbon adsorber that regenerates the carbon bed
directly onsite in the control device and complies
with Section 725.933(f)(2)(G)(ii), any period when the
vent stream continues to flow through the control
device beyond the predetermined carbon bed
regeneration time established as a requirement of
subsection (b)(4)(C)(vi)
, above.
5)
Explanation for each period recorded under subsection
(c)(4) , above, of the cause for control device operating
parameter exceeding the design value and the measures
implemented to correct the control device operation.
6)
For carbon adsorption systems operated subject to
requirements specified in Section 725.933(g) or (h)(2), any
date when existing carbon in the control device is replaced
with fresh carbon.
7)
For carbon adsorption systems opera
ted subject to
requirements specified in Section 725.933(h)(1), a log that
records:
A)
Date and time when control device is monitored for
carbon breakthrough and the monitoring device reading.
B)
Date when existing carbon in the control device is
replaced with fresh carbon.
8)
Date of each control device startup and shutdown.
9)
An owner or operator designating any components of a closed-
vent system as unsafe to monitor pursuant to Section
725.933(n) shall record in a log that is kept in the
facility operating record the identification of closed
-vent
system components that are designated as unsafe to monitor
in accordance with the requirements of Section 725.933(n),
an explanation for each closed
-vent system component stating
why the closed -vent system component is unsafe to monitor,
and the plan for monitoring each closed
-vent system
component.
10)
When each leak is detected as specified in Section
725.933(k), the following information must be recorded:
A)
The instrument identification number, the closed
-vent
system component identification number, and the
operator name, initials, or identification number.
B)
The date the leak was detected and the date of first
attempt to repair the leak.
C)
The date of successful repair of the leak.
D)
Maximum instrument reading measured by Method 21 of 40
CFR 60, appendix A, incorporated by reference in 35
263
Ill. Adm. Code 720.111, after it is successfully
repaired or determined to be
nonrepairable.
E)
"Repair delayed" and the reason for the delay if a
leak is not repaired within 15 calendar days after
discovery of the leak.
i)
The owner or operator may develop a written
procedure that identifies the conditions that
justify a delay of repair. In such cases,
reasons for delay of repair may be documented by
citing the relevant sections of the written
procedure.
ii)
If delay of repair was caused by depletion of
stocked parts, there must be documentation that
the spare parts were sufficiently stocked
on-site before depletion and the re
ason for
depletion.
d)
Records of the monitoring, operating and inspection information
required by subsections (c)(3) through (
810), above , need be kept
only 3 must be maintained by the owner or
operater for at least
three years following the date of each occurrence, measurement,
corrective action, or record
.
e)
For a control device other than a thermal vapor incinerator,
catalytic vapor incinerator, flare, boiler, process heater,
condenser or carbon adsorption system, monitoring and inspection
information indicating proper operation and maintenance of the
control device must be recorded in the facility operating record.
f)
Up-to-date information and data used to determine whether or not a
process vent is subject to the requirements in Section 725.932,
including supporting documentation as required by Section
725.934(d)(2), when application of the knowledge of the nature of
the hazardous wastestream or the process by which it was produced
is used, must be recorded in a log that is kept in the facility
operating record.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART BB: AIR EMISSION STANDARDS FOR EQUIPMENT LEAKS
Section 725.950
Applicability
a)
The regulations in this Subpart apply to owners and operators of
facilities that treat, store, or dispose of hazardous wastes
(except as provided in Section 725.101).
b)
Except as provided in Section 725.964(
jk), this Subpart applies to
equipment that contains or contacts hazardous wastes with organic
concentrations of at least 10 percent by weight that are managed
in one of the following
:
1) UA units that areis subject to the RCRA permitting
requirements of 35 Ill. Adm. Code
702, 703, and 705 , or
2) HA unit (including a h
azardous waste recycling unit
s) that
areis not exempt from permitting under the provisions of 35
264
Ill. Adm. Code 722.134(a) (i.e., a hazardous waste recycling
unit that is not a "90-day" tank or container) and that is
located onat a hazardous waste management
facilit iesy
otherwise subject to the permitting requirements of 35 Ill.
Adm. Code 702, 703, and 705 ., or
3)
A unit that is exempt from permitting under the provisions
of 35 Ill. Adm. Code 722.134(a) (i.e., a "90
-day" tank or
container).
c)
Each piece of equipment to which this Subpart applies must be
marked in such a manner that it can be distinguished readily from
other pieces of equipment.
d)
Equipment that is in vacuum service is excluded from the
requirements of Sections 725.952 to 725.960, if it is identified
as required in Section 725.964(g)(5).
e)
Equipment that contains or contacts hazardous waste with an
organic concentration of at least 10 percent by weight for a
period of less than 300 hours per calendar year is excluded from
the requirements of Sections 265.952 through 265.960 if it is
identified as required in Section 725.964(g)(6).
BOARD NOTE: The requirements of Sections 725.952 through 725.964
apply to equipment associated with hazardous waste recycling units
previously exempt under 35 Ill. Adm. Code 721.106(c)(1). Other
exemptions under 35 Ill. Adm. Code 721.104
, 722.134 and 725.101(e)
are not affected by these requirements.
ef)
Agency decisions pursuant to this Part must be made in writing,
are in the nature of permit decisions pursuant to Section 39 of
the Environmental Protection Act and may be appealed to the Board
pursuant to 35 Ill. Adm. Code 105.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.955
Standards: Sampling Connecting Systems
a)
Each sampling connection syst
em must be equipped with a closed
-
purge, closed-loop, or
system or closed-vent system.
This system
must collect the sample purge for return to the process or for
routing to the appropriate treatment system. Gases displaced
during filling of the sample container are not required to be
collected or captured.
b)
Each closed-purge
, closed-loop, or
system or closed-vent system as
required in subsection (a) must
meet one of the following
requirements :
1)
Return the purged
hazardous waste stream process fluid
directly to the hazardous waste management
process line with
no detectable emissions to atmosphere
; or
2)
Collect and recycle the purged
hazardous waste stream with
no detectable emissions to
atmosphere process fluid ; or
3)
Be designed and operated to capture and transport all the
purged hazardous wastestream process fluid to waste
management unit that complies with the applicable
requirements of Sections 725.985 through 725.987 or
a
265
control device that complies with the requirements of
Section 725.960.
c)
In-situ sampling systems
and sampling systems without purges
are
exempt from the requirements of subsections (a) and (b)
above .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.958
Standards: Pumps, Valves, Pressure Relief Devices, Flanges
and other Connectors
a)
Pumps and valves in heavy liquid service, pressure relief devices
in light liquid or heavy liquid service and flanges and other
connectors must be monitored within 5 days by the method specified
in Section 725.963(b), if evidence of a potential leak is found by
visual, audible, olfactory, or any other detection method.
b)
If an instrument reading of 10,000
ppm or greater is measured, a
leak is detected.
c)
Repairs
1)
When a leak is detected, it must be repaired as soon as
practicable, but not later than 15 calendar days after it is
detected, except as provided in Section 725.959.
2)
The first attempt at repair must be made no later than 5
calendar days after each leak is detected.
d)
First attempts at repair include, but are not limited to, the best
practices described under Section 725.957(e).
e)
Any connector that is inaccessible or is ceramic or ceramic-lined
(e.g., porcelain, glass, or glass
-lined) is exempt from the
monitoring requirements of subsection (a) above and from the
recordkeeping requirements of Section 725.964.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.964
Recordkeeping Requirements
a)
Lumping Units
1)
Each owner or ope
rator subject to the provisions of this
Subpart shall comply with the
recordkeeping requirements of
this Section.
2)
An owner or operator of more than one hazardous waste
management unit subject to the provisions of this Subpart
may comply with the
recordkeeping requirements for these
hazardous waste management units in one
recordkeeping system
if the system identifies each record by each hazardous waste
management unit.
b)
Owners and operators shall record the following information in the
facility operating record:
1)
For each piece of equipment to which this Subpart applies:
A)
Equipment identification number and hazardous waste
management unit identification.
266
B)
Approximate locations within the facility (e.g.,
identify the hazardous waste management unit on a
facility plot plan).
C)
Type of equipment (e.g., a pump or pipeline valve).
D)
Percent-by-weight total
organics in the hazardous
wastestream at the equipment.
E)
Hazardous waste state at the equipment (e.g. gas/vapor
or liquid).
F)
Method of compliance with the standard (e.g. "monthly
leak detection and repair" or "equipped with dual
mechanical seals").
2)
for facilities than comply with the provisions of Section
725.933(a)(2), an implementation schedule as specified in
that Section.
3)
Where an owner or operator chooses to use test data to
demonstrate the organic removal efficiency or total organic
compound concentration achieved by the control device, a
performance test plan as specified in Section 725.935(b)(3).
4)
Documentation of compliance with Section 725.960, including
the detailed design documentation or performance test
results specified in Section 725.935(b)(4).
c)
When each leak is detected as specified in Sections 725.952,
725.953, 725.957 or 725.958, the following requirements apply:
1)
A weatherproof and readily visible identification, marked
with the equipment identification number, the date evidence
of a potential leak was found in accordance with Section
725.958(a), and the date the leak was detected, must be
attached to the leaking equipment.
2)
The identification on equipment except on a valve, may be
removed after it has been repaired.
3)
The identification on a valve may be removed after it has
been monitored for 2 successive months as specified in
Section 725.957(c) and no leak has been detected during
those 2 months.
d)
When each leak is detected as specified in Sections 725.952,
725.953, 725.957 or 725.958, the following information must be
recorded in an inspection log and must be kept in the facility
operating record:
1)
The instrument and operator identification numbers and the
equipment identification number.
2)
The date evidence of a potential leak was found in
accordance with Section 725.958(a).
3)
The date the leak was detected and the dates of each attempt
to repair the leak.
267
4)
Repair methods applied in each attempt to repair the leak.
5)
"Above 10,000", if the maximum instrument reading measured
by the methods specified in Section 725.963(b) after each
repair attempt is equal to or greater than 10,000
ppm.
6)
"Repair delayed" and the reason for the delay if a leak is
not repaired within 15 calendar days after discovery of the
leak.
7)
Documentation supporting the delay of repair of a valve in
compliance with Section 725.959(c).
8)
The signature of the owner or operator (or designate) whose
decision it was that repair could not be effected without a
hazardous waste management unit shutdown.
9)
The expected date of successful repair of the leak if a
leak
is not repaired within 15 calendar days.
10)
The date of successful repair of the leak.
e)
Design documentation and monitoring, operating and inspection
information for each closed-vent system and control device
required to comply with the provisions of Section 725.960 must be
recorded and kept up-to-date in the facility operating record as
specified in Section 725.935(c)(1) and
(c)(2), and monitoring,
operating and inspection information in Section 725.935(c)(3)
through (c)(8).
f)
For a contro l device other than a thermal vapor incinerator,
catalytic vapor incinerator, flare, boiler, process heater,
condenser, or carbon adsorption system, monitoring and inspection
information indicating proper operation and maintenance of the
control device must be recorded in the facility operating record.
g)
The following information pertaining to all equipment subject to
the requirements in Sections 725.952 through 725.960 must be
recorded in a log that is kept in the facility operating record:
1)
A list of identification numbers for equipment (except
welded fittings) subject to the requirements of this
Subpart.
2)
List of Equipment
A)
A list of identification numbers for equipment that
the owner or operator elects to designate for no
detectable emissions, as indicated by an instrument
reading of less than 500
ppm above background, under
the provisions of Sections 725.952(e), 725.953(i) and
725.957(f).
B)
The designation of this equipment as subject to the
requirements of Sections 725.952(e), 725.953(i) or
725.957(f) must be signed by the owner or operator.
3)
A list of equipment identification numbers for pressure
relief devices required to comply with Section 725.954(a).
4)
Compliance tests.
268
A)
The dates of each compliance test required in Sections
725.952(e), 725.953(i), 725.954
, and 725.957(f).
B)
The background level measured during each compliance
test.
C)
The maximum instrument reading measured at the
equipment during each compliance test.
5)
A list of identification nu
mbers for equipment in vacuum
service.
6)
Identification, either by list or location (area or group)
of equipment that contains or contacts hazardous waste with
an organic concentration of at least 10 percent by weight
for a period of less than 300 hours per year.
h)
The following information pertaining to all valves subject to the
requirements of Section 725.957(g) and (h) must be recorded in a
log that is kept in the facility operating record:
1)
A list of identification numbers for valves that ar
e
designated as unsafe to monitor, an explanation for each
valve stating why the valve is unsafe to monitor, and the
plan for monitoring each valve.
2)
A list of identification numbers for valves that are
designated as difficult to monitor, an explanation for each
valve stating why the valve is difficult to monitor, and the
planned schedule for monitoring each valve.
i)
The following information must be recorded in the facility
operating record for valves complying with Section 725.962:
1)
A schedul e of monitoring.
2)
The percent of valves found leaking during each monitoring
period.
j)
The following information must be recorded in a log that is kept
in the facility operating record:
1)
Criteria required in Section 725.952(d)(5)(B) and
725.953(e)(2) and an explanation of the criteria.
2)
Any changes to these criteria and the reasons for the
changes.
k)
The following information must be recorded in a log that is kept
in the facility operating record for use in determining exemptions
as provided in Section 725.950 and other specific Subparts:
1)
An analysis determining the design capacity of the hazardous
waste management unit.
2)
A statement listing the hazardous waste influent to and
effluent from each hazardous waste management unit subject
to the requirements in Sections 725.960 and an analysis
determining whether these hazardous wastes are heavy
liquids.
269
3)
An up-to-date analysis and the supporting information and
data used to determine whether or not equipment is subject
to the requirements in Sections 725.952 through 725.960.
The record must include supporting documentation as required
by Section 725.963(d)(3) when application of the knowledge
of the nature of the hazardous wastestream or the process by
which it was produced is used. If the owner or operator
takes any action (e.g., changing the process that produced
the waste) that could result in an increase in the total
organic content of the waste contained in or contacted by
equipment determined not to be subject to the requirements
in Sections 725.952 through 725.960, then a new
determination is required.
l)
Records of the equipment leak information required by subsection
(d) (above) and the operating information required by subsection
(e) (above) need be kept only 3 years.
m)
The owner or operator of any facility that is subject to this
Subpart and to regulations at 40 CFR 60, Subpart VV, or 40 CFR 61,
Subpart V, incorporated by reference in 35 Ill. Adm. Code 720.111,
may elect to determine compliance with this Subpart by
documentation either pursuant to Section 725.964, or pursuant to
those provisions of 40 CFR 60 or 61, to the extent that the
documentation under the regulation at 40 CFR 60 or 61 duplicates
the documentation required under this Subpart. The documentation
under the regulation at 40 CFR 60 or 61 must be kept with or made
readily available with the facility operating record.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART CC: AIR EMISSION STANDARDS FOR TANKS,
SURFACE IMPOUNDMENTS, AND CONTAINERS
Section 725.980
Applicability
a)
The requirements of this Subpart apply, effective October 6, 1996,
to owners and operators of all facilities that treat, store, or
dispose of hazardous waste in tanks, surface
impoundments, or
containers that are subject to 725.Subpart I, J, or K, except as
Section 725.101 and subsection (b) below provide otherwise.
BOARD NOTE: USEPA adopted these regulations at 59 Fed. Reg. 62896
(Dec. 6, 1994), effective June 6, 1995. At 60 Fed. Reg. 26828
(May 19, 1995), 60 Fed. Reg. 56952 (Nov. 13, 1995), and 61 Fed.
Reg. 28508 (June 5, 1996), USEPA delayed the effective date until
October 6, 1996. If action by USEPA or a decision of a federal
court changes the effectiveness of these regulations, the Board
does not intend that 725.Subpart CC be enforceable to the extent
that it becomes more stringent that the federal regulations upon
which they are based.
b)
The requirements of this Subpart do not apply to the following
waste management units at the facility:
1)
A waste management unit that holds hazardous waste placed in
the unit before October 6, 1996 and in which no hazardous
waste is added to the unit on or after this date.
270
2)
A container that has a design capacity less than or equal to
0.1 m
3
(3.5 ft
3
or 26.4 gal).
3)
A tank in which an owner or operator has stopped adding
hazardous waste and the owner or operator has begun
implementing or completed closure pursuant to an approved
closure plan.
4)
A surface impoundment in which an
owner or operator has
stopped adding hazardous waste (except to implement an
approved closure plan) and the owner or operator has begun
implementing or completed closure pursuant to an approved
closure plan.
5)
A waste management unit that is used solely for on-site
treatment or storage of hazardous waste that is generated as
the result of implementing remedial activities required
pursuant to the Act or Board regulations or under the
corrective action authorities of RCRA sections 3004(u),
3004(v) or 3008(h); CERCLA authorities; or similar federal
or state authorities.
6)
A waste management unit that is used solely for the
management of radioactive mixed waste in accordance with all
applicable regulations under the authority of the Atomic
Energy Act (42 U.S.C. 2011 et seq.) and the Nuclear Waste
Policy Act.
7)
A hazardous waste management unit that the owner or operator
certifies is equipped with and operating air emission
controls in accordance with the requirements of an
applicable federal Clean Air Act regulation codified under
40 CFR 60, 61, or 63. For the purpose of complying with
this subsection, a tank for which the air emission control
includes an enclosure, as opposed to a cover, must be in
compliance with the enclosure and control device
requirements of Section 725.985(i), except as provided in
Section 725.983(c)(5).
8)
A tank that has a process vent, as defined in 35 Ill. Adm.
Code 725.931.
c)
For the owner and operator of a facility subject to this Subpart
whothat has received a final RCRA permit prior to October 6, 1996,
the following requirements apply:
1)
The requirements of 35 Ill. Adm. Code 724.Subpart CC must be
incorporated into the permit when the permit is reissued,
renewed, or modified in accordance with the requirements of
35 Ill. Adm. Code 703 and 705.
2)
Until the date when the permit is reissued, renewed, or
modified in accordance with the requirements of 35 Ill. Adm.
Code 703 and 705, the owner and operator is subject to the
requirements of this Subpart.
d)
The re quirements of this Subpart, except for the
recordkeeping
requirements specified in Section 725.990(i) are stayed for a tank
or container used for the management of hazardous waste generated
by organic peroxide manufacturing and its associated laboratory
operations, when the owner or operator of the unit meets all of
271
the following conditions:
1)
The owner or operator identifies that the tank or container
receives hazardous waste generated by an organic peroxide
manufacturing process producing more than one functional
family of organic peroxides or multiple organic peroxides
within one functional family, that one or more of these
organic peroxides could potentially undergo self-
accelerating thermal decomposition at or below ambient
temperatures, and that organic peroxides are the predominant
products manufactured by the process. For the purposes of
this subsection, "organic peroxide" means an organic
compound that contains the bivalent
-O-O- structure and
which may be considered to be a
sturctural derivative of
hydrogen peroxide where one or both of the hydrogen atoms
has been replaced by an organic radical.
2)
The owner or operator prepares documentation, in accordance
with Section 725.990(i), explaining why an undue safety
hazard would be created if air emission controls specified
in Sections 725.985 through 725.988 are installed and
operated on the tanks and containers used at the facility to
manage the hazardous waste generated by the organic peroxide
manufacturing process or processes meeting the conditions of
subsection (d)(1) above.
3)
The owner or operator notifies the Agency in writing that
hazardous waste generated by an organic peroxide
manufacturing process or processes meeting the conditions of
subsection (d)(1) above are managed at the facility in tanks
or containers meeting the conditions of subsection (d)(2)
above. The notification must state the name and address of
the facility and be signed and dated by an authorized
representative of the facility owner or operator.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.981
Definitions
As used in this Subpart and in 35 Ill. Adm. Code 724, all terms not defined
herein shall have the meaning given to them in the Act and 35 Ill. Adm. Code
720 through 726.
"Average volatile organic concentration" or "average VO
concentration" means the mass-weighted average volatile organic
concentration of a hazardous waste, as determined in accordance
with the requirements of Section 725.984.
"Closure device" means a cap, hatch, lid, plug, seal, valve, or
other type of fitting that blocks an opening in a cover so that
when the device is secured in the closed position it prevents or
reduces air pollutant emissions to the atmosphere. Closure
devices include devices that are detachable from the cover (e.g.,
a sampling port cap), manually operated (e.g., a hinged access lid
or hatch), or automatically operated (e.g., a spring
-loaded
pressure relief valve).
"Continuous seal" means a seal that forms a continuous closure
that completely covers the space between the edge of the floating
roof and the wall of a tank. A continuous seal may be a
vapor-mounted seal, liquid
-mounted seal, or metallic shoe seal. A
272
continuous seal may be constructed of fastened segments so as to
form a continuous seal.
"Cover" means a device
or system that is placed on orprovides a
continuous barrier
over athe hazardous waste
such that the entire
hazardous waste surface area is enclosed and
sealed managed in a
unit to prevent or reduce air emissions to the atmosphere. A
cover may have openings
(such as access hatches, sampling ports,
and gauge wells ) that are necessary for operation, inspection,
maintenance, or repair of the unit on which the cover is
installed
provided that each opening is closed and sealed when not in
used.
Examples of covers include a fixed roof installed on a tank, a
floating membrane cover installed on a surface impoundment, a lid
installed on a drum, or an enclosure in which an open container is
placed during waste
treatment. A cover may be a separate piece of
equipment which can be detached and removed from the unit or a
cover may be formed by structural features permanently integrated
into the design of the unit.
"Enclosure" means a structure that surrounds a tank or container,
captures organic vapors emitted from the tank or container, and
vents the captured vapors through a closed
-vent system to a
control device.
"External floating roof" means a pontoon
-type or double-deck type
floating roofcover that rests on the surface of a hazardous waste
being managed in a tank
that haswith no fixed roof.
"Fixed roof" means a
rigid cover that is installed mounted on a
unit in a stationary position
so that itand does not move with
fluctuations in the level of the
hazardous waste placed material
managed in a tankthe unit .
"Floating membrane cover" means a cover consisting of a synthetic
flexible membrane material that rests upon and is supported by the
hazardous waste being managed in a surface impoundment.
"Floating roof" m
eans a pontoon-type or double-deck-
typecover
consisting of a double deck, pontoon single deck, or internal
floating cover that rests upon and is supported by the
hazardous
wastematerial being managed in a tankcontained , and is equipped
with a closure continuous seal or seals to close the space between
the cover edge and the tank wall
.
"Hard-piping" means pipe or tubing that is manufactured and
properly installed in accordance with relevant standards and good
engineering practices.
"In light material service" means the container is used to manage
a material for which both of the following conditions apply: the
vapor pressure of one or more of the organic constituents in the
material is greater than 0.3
kilopascals ( kPa) at 20
ยฐ
C (1.2 inches
H
2
O at 68
ยฐ
F); and the total concentration of the pure organic
constituents having a vapor pressure greater than 0.3
kPa at 20
ยฐ
C
(1.2 inches H
2
O at 68
ยฐ
F) is equal to or greater than 20 percent by
weight.
"Internal floating roof" means a
floating roofcover that rests or
floats on the material surface (but not necessarily in complete
contact with it)
of a hazardous waste being managed
inside a tank
273
that has a fixed roof.
"Liquid-mounted seal" means a foam or liquid-filled primary seal
mounted in contact with the hazardous waste between the tank wall
and the floating roof, continuously around the circumference of
the tank.
"Malfunction" means any sudden, infrequent, and not reasonably
preventable failure of air pollution control equipment, process
equipment, or a process to operate in a normal or usual manner. A
failure that is caused in part by poor maintenance or careless
operation is not a malfunction.
"Maximum organic vapor pressure" means the equilibrium partial
pressure exerted by the hazardous waste contained in a tank,
determined at the temperature equal to either:
The local maximum monthly average temperature as reported by
the National Weather Service, when the hazardous waste is
stored or treated at ambient temperature, or
The highest calendar-m
onth average temperature of the
hazardous waste, when the hazardous waste is stored at
temperatures above the ambient temperature or when the
hazardous waste is stored or treated at temperatures below
the ambient temperature.
"Maximum organic vapor pressure" means the sum of the individual
organic constituent partial pressures exerted by the material
contained in a tank at the maximum vapor pressure
-causing
conditions (i.e., temperature, agitation, pH effects of combining
wastes, etc.) reasonably expected to occur in the tank. For the
purpose of this Subpart, maximum organic vapor pressure is
determined using the procedures specified in Section 725.984(c).
"Metallic shoe seal" means a continuous seal that is constructed
of metal sheets that are held vertically against the wall of the
tank by springs, weighted levers, or other mechanisms and which is
connected to the floating roof by braces or other means. A
flexible coated fabric (envelope) spans the annular space between
the metal sheet and the floating roof.
"No detectable organic emissions" means no escape of
organics from
a device or system
to the atmosphere, as determined
: using the
procedure specified in Section 725.984(d).
By an instrument reading less than 500 parts per million by
volume ( ppmv) above the background level at each joint,
fitting, and seal, when measured in accordance with the
requirements of Method 21 in 40 CFR 60, Appendix A, and
By no visible openings or defects in the device or system
such as rips, tears, or gaps.
"Point of waste origination" means as follows:
When the facility owner or operator is the generator of the
hazardous waste, the "point of waste origination" means the
point where a solid waste produced by a system, process, or
waste management unit is determined to be a hazardous waste,
as defined in 35 Ill. Adm. Code 721.
274
BOARD NOTE: In this case, this term is being used in a
manner similar to the use of the term "point of generation"
in air standards established for waste management operations
under authority of the federal Clean Air Act in 40 CFR 60,
61, and 63.
When the facility owner and operator are not the generator
of the hazardous waste, "point of waste origination" means
the point where the owner or operator accepts delivery or
takes possession of the hazardous waste.
"Point of waste treatment" means the point where a hazardous waste
to be treated in accordance with Section 725.983(c)(2)
exits a
waste management unit used to destroy, degrade, or remove
organics
in the hazardous waste
the treatment process
. Any waste
determination must be made before the waste is conveyed, handled,
or otherwise managed in a manner that allows the waste to
volatilize to the atmosphere.
"Safety device" means a closure device, such as a pressure relief
valve, frangible disc, fusible plug, or any other type of device,
which functions exclusively to prevent physical damage or
permanent deformation to a unit or its air emission control
equipment by venting gases or vapors directly to the atmosphere
during unsafe conditions resulting from an unplanned, accidental,
or emergency event. For the purpose of this Subpart, a safety
device is not used for routine venting of gases or vapors from the
vapor headspace underneath a cover such as during filling of the
unit or to adjust the pressure in this vapor
headspace in response
to normal daily diurnal ambient temperature fluctuations. A
safety device is designed to remain in a closed position during
normal operations and open only when the internal pressure, or
another relevant parameter, exceeds the device threshold setting
applicable to the air emission control equipment as determined by
the owner or operator based on manufacturer recommendations,
applicable regulations, fire protection and prevention codes,
standard engineering codes and practices, or other requirements
for the safe handling of flammable, ignitable, explosive,
reactive, or hazardous materials.
"Single -seal system" means a floating roof having one continuous
seal. This seal may be vapor
-mounte d, liquid -mounted, or a
metallic shoe seal.
"Vapor-mounted seal" means a
foam-filled primary seal mounted
continuous ly around the circumference of the tank so that there is
an annular seal that is mounted so that there is a
vapor space
underneath between the hazardous waste in the unit and the bottom
of the seal. The annular vapor space is bounded by the bottom of
the primary seal, the tank wall, the hazardous waste surface, and
the floating roof.
"Volatile organic concentration" or "VO concentration"
means the
fraction by weight of organic compounds
contained in a hazardous
waste expressed in terms of parts per million (
ppmw), as
determined by direct measurement
, using Method 25D,
or by
knowledge of the waste, in accordance with the requirements of
Section 725.984. For the purpose of determining the VO
concentration of a hazardous waste, organic compounds with a
Henry's law constant value of at least 0.1 mole-fraction-in-the-
275
gas-phase/mole-fraction-in the liquid-phase (0.1 Y/X) (which can
also be expressed as 1.8
ร
10
-6
atmospheres/gram
-mole/m
3
) at 25
ยฐ
C
(77
ยฐ
F) must be included. Section 725.Appendix F presents a list
of compounds known to have a Henry's law constant value less than
the cutoff level.
"Waste determination" means performing all applicable procedures
in accordance with the requirements of Section 725.984 to
determine whether a hazardous waste meets standards specified in
this Subpart. Examples of a waste determination include
performing the procedures in accordance with the requirements of
Section 725.984 to determine the average VO concentration of a
hazardous waste at the point of waste origination, determining the
average VO concentration of a hazardous waste at the point of
waste treatment and comparing the results to the exit
concentration limit specified for the process used to treat the
hazardous waste,
determining the organic reduction efficiency and
the organic biodegradation efficiency for a biological process
used to treat a hazardous waste and comparing the results to the
applicable standards, or determining the maximum volatile organic
vapor pressure for a hazardous waste in a tank and comparing the
results to the applicable standards.
"Waste stabilization process" means any physical or chemical
process used to either reduce the mobility of hazardous
constituents in a hazardous waste or eliminate free liquids as
determined by Test Method 9095 (Paint Filter Liquids Test) in
"Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods", incorporated by reference in Section 720.111. A waste
stabilization process includes mixing the hazardous waste with
binders or other materials and curing the resulting hazardous
waste and binder mixture. Other synonymous terms used to refer to
this process are "waste fixation" or "waste solidification".
This
does not include the addition of absorbent materials to the
surface of a waste to absorb free liquid without mixing,
agitation, or subsequent curing.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.983
Standards: General
a)
This Section applies to the management of hazardous waste in
tanks, surface impoundments, and containers subject to this
Subpart.
b)
The owner or operator shall control air emissions from each waste
management unit in accordance with standards specified in Sections
725.985 through Section 725.988, as applicable to the waste
management unit, except as provided for in subsection (c) below.
c)
A waste management
unittank, surface impoundment, or container
is
exempted from standards specified in Section
s 725.985 through
Section 725.988, provided that all hazardous waste placed in the
waste management unit is
determined by the owner or operator to
meet either one of the following
conditions :
1) The average VO concentration of
theA tank, surface
impoundment, or container for which all
hazardous waste
entering the unit has an average VO concentration
at the
point of waste origination
isof less than 100500 parts per
million by weight (
ppmw). The average VO concentration must
276
be determined by the procedures specified in Section
725.984(a). The owner or operator shall review and update,
as necessary, this determination at least once every 12
months following the date of the initial determination for
the hazardous waste streams entering the unit.
2) TA tank, surface impoundment, or container for which t
he
organic content of
all the hazardous waste
entering the
waste management unit
has been reduced by an organic
destruction or removal process that achieves any one of the
following conditions:
A)
The process removes or destroys the
organics contained
in the hazardous waste to such a level that the
average VO concentration of the hazardous waste at the
point of waste treatment is less than the exit
concentration limit (C
t
) established for the process.
The average VO concentration of the hazardous waste
at the point of waste treatment and the exit
concentration limit for the process must be determined
using the procedures specified in Section 725.984(b).
B)
The process removes or destroys the
organics contained
in the hazardous waste to such a level that the
organic reduction efficiency (R) for the process is
equal to or greater than 95 percent, and the average
VO concentration of the hazardous waste at the point
of waste treatment is less than
50100 ppmw. The
organic reduction efficiency for the process and the
average VO concentration of the hazardous waste at the
point of waste treatment must be determined using the
procedures specified in Section 725.984(b).
C)
The process removes or destroys the
organics contained
in the hazardous waste to a level such that the actual
organic mass removal rate (MR) for the process is
equal to or greater than the required organic mass
removal rate (RMR) established for the process. The
required organic mass removal rate and the actual
organic mass removal rate for the process shall be
determined using the procedures specified in Section
724.983(b).
D)
The process is a biological process that destroys or
degrades the organics contained in the hazardous waste
so that either of the following conditions is met:
i)
The organic reduction efficiency (R) for the
process is equal to or greater than 95 percent,
and the organic biodegradation efficiency (
R
bio
)
for the process is equal to or greater than 95
percent. The organic reduction efficiency and
the organic biodegradation efficiency for the
process must be determined
in accordance
withusing the procedures specified in Section
725.984(b).
ii)
The total actual organic mass
biodegradation
rate ( MR
bio
) for all hazardous waste treated by
the process is equal to or greater than the
required organic mass removal rate (RMR). The
277
required organic mass removal rate and the
actual organic mass
biodegradation rate for the
process must be determined using the procedures
specified in Section 725.984(b).
E)
The process is one that removes or destroys the
organics contained in the hazardous waste and meets
all of the following conditions:
i) All of the materials entering the proc
ess are
hazardous wastes.
ii)
From the point of waste origination through the
point where the hazardous waste enters the
treatment process, the hazardous waste is
continuously managed in waste management units
that use air emission controls in accordance
with the standards specified in Section 725.985
through Section 725.988, as applicable to the
waste management unit.
ii)
From the point of waste origination through the
point where the hazardous waste enters the
treatment process, any transfer of the hazardous
waste is accomplished through continuous
hard-piping or other closed system transfer that
does not allow exposure of the waste to the
atmosphere.
BOARD NOTE: The USEPA considers a drain system
that meets the requirements of 40 CFR 63,
subpart RR, "National Emission Standards for
Individual Drain Systems", to be a closed
system.
iii)
The average VO concentration of the hazardous
waste at the point of waste treatment is less
than the lowest average VO concentration at the
point of waste origination determined for each
of the individual hazardous waste streams
entering the process or
100500 ppmw, whichever
value is lower. The average VO concentration of
each individual hazardous waste stream at the
point of waste origination must be determined
using the procedure
s specified in Section
725.984(a). The average VO concentration of the
hazardous waste at the point of waste treatment
must be determined using the procedure
s
specified in Section 725.984(b).
F)
A process that removes or destroys the
organics
contained in the hazardous waste to a level such that
the organic reduction efficiency (R) for the process
is equal to or greater than 95 percent and the owner
or operator certifies that the average VO
concentration at the point of waste origination for
each of the individual waste streams entering the
process is less than 10,000
ppmw. The organic
reduction efficiency for the process and the average
VO concentration of the hazardous waste at the point
of waste origination shall be determined using the
278
procedures specified in Section 724.983(b) and Section
724.983(a), respectively.
FG)
A hazardous waste incinerator for which
either of the
owner or operator has
either following conditions is
true:
i) BThe owner or operator has b
een issued a final
permit under 35 Ill. Adm. Code
702, 703, and
705, and designs and operates the unit in
accordance with that implements the requirements
of 724726.Subpart OH; or
ii)
The owner or operator has
certified compliance
for the unitdesigned and operates the
incinerator in accordance
with the interim
status requirements of 725.Subpart O.
GH)
A boiler or industrial furnace for which
either of the
owner or operator has
either following conditions is
true:
i) BThe owner or operator has b
een issued a final
permit under 35 Ill. Adm. Code
702, 703, and
705, and designs and operates the unit in
accordance with that implements the requirements
of 35 Ill. Adm. Code 726.Subpart H, or
ii)
The owner or operator has
certified
compliance designed and operates the industrial
furnace or incinerator in accordance
for the
unit with the interim status requirements of 35
Ill. Adm. Code 726.Subpart H.
I)
For the purpose of determining the performance of an
organic destruction or removal process in accordance
with the conditions in each of subsections (c)(2)(A)
through (c)(2)(F) above, the owner or operator shall
account for VO concentrations determined to be below
the limit of detection of the analytical method by
using the following VO concentration:
i)
If Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, is used for the analysis, one
-half the
blank value determined in the method.
ii)
If any other analytical method is used, one
-half
the limit of detection established for the
method.
3)
A tank used for biological treatment of hazardous waste in
accordance with the requirements of subsection (c)(2)(D)
above.
4)
A tank, surface impoundment, or container for which all
hazardous waste placed in the unit fulfills either of the
following two conditions:
A)
It meets the numerical concentration limits for
organic hazardous constituents, applicable to the
279
hazardous waste, as specified in 35 Ill. Adm. Code
728.Table T; or
B)
It has been treated by the treatment technology
established by USEPA for the waste in 35 Ill. Adm.
Code 728.142(a), or treated by an equivalent method of
treatment approved by the Agency pursuant to 35 Ill.
Adm. Code 728.142(b).
5)
A tank used for bulk feed of hazardous waste to a waste
incinerator and all of the following conditions are met:
A)
The tank is located inside an enclosure vented to a
control device that is designed and operated in
accordance with all applicable requirements specified
under 40 CFR 61, subpart FF, "National Emission
Standards for Benzene Waste Operations", incorporated
by reference in 35 Ill. Adm. Code 720.111, for a
facility at which the total annual benzene quantity
from the facility waste is equal to or greater than 10
megagrams (11 tons) per year;
B)
The enclosure and control device serving the tank were
installed and began operation prior to November 25,
1996; and
C)
The enclosure is designed and operated in accordance
with the criteria for a permanent total enclosure as
specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111. The enclosure may have permanent or
temporary openings to allow worker access; passage of
material into or out of the enclosure by conveyor,
vehicles, or other mechanical or electrical equipment;
or to direct air flow into the enclosure. The owner
or operator shall perform the verification procedure
for the enclosure as specified in Section 5.0 to
"Procedure T --Criteria for and Verification of a
Permanent or Temporary Total Enclosure" annually.
d) When a process is used for the purpose of treating a hazardous
waste to meet one of the sets of conditions specified in
subsections (c)(2)(A) through (c)(2)(E) above, each material
removed from or exiting the process that is not a hazardous waste
but which has an average VO concentration equal to or greater than
100 ppmw shall be managed in a waste management unit in accordance
with the requirements of subsection (b) above.
ed)
The Agency may at any time perform or request that the owner or
operator perform a waste determination for a hazardous waste
managed in a tank, surface impoundment, or container that is
exempted from using air emission controls under the provisions of
this Section as follows:
1)
The waste determination for average VO concentration of a
hazardous waste at the point of waste origination must be
performed using direct measurement in accordance with the
applicable requirements of Section 725.984(a). The waste
determination for a hazardous waste at the point of waste
280
treatment must be performed in accordance with the
applicable requirements of Section 725.984(b).
2)
In performing a waste determination pursuant to subsection
(d)(1) above, the sample preparation and analysis shall be
conducted as follows:
A)
In accordance with the method used by the owner or
operator to perform the waste analysis, except in the
case specified in subsection (d)(2)(B) below.
B)
If the Agency determines that the method used by the
owner or operator was not appropriate for the
hazardous waste managed in the tank, surface
impoundment, or container, then the Agency may choose
an appropriate method.
23)
Where the owner or operator
is requested to perform the
waste determination, the Agency may elect to have an
authorized representative observe the collection of the
hazardous waste samples used for the analysis.
34)
Where the results of the waste determination performed or
requested by the Agency do not agree with the results of a
waste determination performed by the owner or operator using
knowledge of the waste, then the results of the waste
determination performed in accordance with the requirements
of subsection ( ed)(1) above must be used to establish
compliance with the requirements of this Subpart.
45)
Where the owner or operator has used an averaging period
greater than one hour for determining the average VO
concentration of a hazardous waste at the point of waste
origination, the Agency may elect to establish compliance
with this Subpart by performing or requesting that the owner
or operator perform a waste determination using direct
measurement, based on waste samples collected within a 1-
hour period as follows:
A)
The average VO concentration of the hazardous waste at
the point of waste origination must be determined by
direct measurement in accordance with the requirements
of Section 725.984(a).
B)
Results of the waste determination performed or
requested by the Agency showing that the average VO
concentration of the hazardous waste at the point of
waste origination is equal to or greater than
100500
ppmw shall constitute noncompliance with this Subpart,
except in a case as provided for in subsection
(ed)(4)(C) below.
C)
Where the average VO concentration of the hazardous
waste at the point of waste origination previously has
been determined by the owner or operator using an
averaging period greater than one hour to be less than
100500 ppmw but because of normal operating process
variations the VO concentration of the hazardous waste
determined by direct measurement for any given 1-hour
period may be equal to or greater than
100500 ppmw,
information that was used by the owner or operator to
281
determine the average VO concentration of the
hazardous waste (e.g., test results, measurements,
calculations, and other documentation) and recorded in
the facility records in accordance with the
requirements of Sections 725.984(a) and 725.990 must
be considered by the Agency together with the results
of the waste determination performed or requested by
the Agency in establishing compliance with this
Subpart.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.984
Waste Determination Pro
cedures
a)
Waste determination procedure for volatile organic (VO)
concentration of a hazardous waste at the point of waste
origination.
1)
An owner or operator shall determine the average VO
concentration at the point of waste origination for each
hazardous waste placed in a waste management unit exempted
under the provisions of Section 725.983(c)(1) from using air
emission controls in accordance with standards specified in
Section 725.985 through Section 725.988, as applicable to
the waste management unit.
2) When the facility owner or operator is the generator of the
hazardous waste,
tThe owner or operator shall determine the
average VO concentration of
thea hazardous waste
at the
point of waste origination must be determined
using either
direct measurement, as specified in subsection (a)(
53)
below, or by knowledge of the waste, as specified in
subsection (a)( 64) below , for each hazardous waste generated
as follows: .
A) When the hazardous waste is generated as part of a
continuous process, the owner or operator shall:
i) Perform an initial waste determination of the
average VO concentration of the waste stream
before the first time any portion of the
material in the waste stream is placed in a
waste management unit subject to this Subpart
and thereafter update the information used for
the waste determination at least once every 12
months following the date of the initial waste
determination; and
ii) Perform a new waste determination whenever
changes to the source generating the waste
stream are reasonably likely to cause the
average VO concentration of the hazardous waste
to increase to a level that is equal to or
greater than the applicable VO concentration
limits specified in Section 725.983.
B) When the hazardous waste is generated as part of a
batch process that is performed repeatedly but not
necessarily continuously, the owner or operator shall:
i) Perform an initial waste determination of the
282
average VO concentration for one or more
representative waste batches generated by the
process, before the first time any portion of
the material in the batches is placed in a waste
management unit subject to this Subpart, and
thereafter update the information used for the
waste determination at least once every 12
months following the date of the initial waste
determination; and
ii) Perform a new waste determination whenever
changes to the process generating the waste
batches are reasonably likely to cause the
average VO concentration of the hazardous waste
to increase to a level that is equal to or
greater than the applicable VO concentration
limits specified in Section 725.983.
3) When the facility owner and operator is not the generator of
the hazardous waste, the owner or operator shall determine
the average VO concentration of the hazardous waste using
either direct measurement, as specified in subsection (a)(5)
below, or knowledge of the waste, as specified in subsection
(a)(6) below, for each hazardous waste entering the facility
as follows:
A) When the hazardous waste
enters the facility as a
continuous flow of material through a pipeline or
other means (e.g., wastewater stream), the owner or
operator shall:
i) Perform an initial waste determination of the
waste stream before the first time any portion
of the material in the waste stream is placed in
a waste management unit subject to this Subpart,
and thereafter update the information used for
the waste determination at least once every 12
months following the date of the initial waste
determination; and
ii) Perform a new waste determination whenever
changes to the source generating the waste
stream are reasonably likely to cause the
average VO concentration of the hazardous waste
to increase to a level that is equal to or
greater than the applicable VO concentration
limits specified in Section 725.983.
B) When the hazardous waste enters the facility in a
container, the owner or operator shall perform a waste
determination for the material held in each container.
4) Where the average VO concentration of
the hazardous waste is
determined by the owner or operator to be less than 100
ppmw, but because of normal operating variations in the
source or process generating the hazardous waste the VO
concentration of the hazardous waste may be equal to or
greater than 100
ppmw at any given time during the averaging
period, the owner or operator shall prepare and enter in the
facility operating record information that specifies the
following:
283
A) The maximum and minimum VO concentration values for
the hazardous waste that occur during that averaging
period used for the waste determination;
B) The operating conditions or circumstances under which
the VO concentration of the hazardous waste will be
equal to or greater than 100
ppmw; and
C) The information and calculations used by the owner or
operator to determine the average VO concentration of
the hazardous waste.
53) Procedure for using
dDirect measurement to determine average
VO concentration of a hazardous waste at the point of waste
origination.
A)
Identification.
The owner or operator shall identify
and record the point of waste origination for the
hazardous waste. All waste samples used to determine
the average VO concentration of the hazardous waste
must be collected at this point.
B) The owner or operator shall designate and record the
averaging period to be used for determining the
average VO concentration for the hazardous waste. The
averaging period must not exceed one year. An initial
waste determination must be performed for each
averaging period.
B)
Sampling. Samples of the hazardous waste stream must
be collected at the point of waste origination in a
manner such that volatilization of
organics contained
in the waste and in the subsequent sample is minimized
and an adequately representative sample is collected
and maintained for analysis by the selected method.
i)
The averaging period to be used for determining
the average VO concentration for the hazardous
waste stream on a mass
-weighted average basis
must be designated and recorded. The averaging
period can represent any time interval that the
owner or operator determines is appropriate for
the hazardous waste stream but must not exceed
one year.
ii)
A sufficient number of samples, but no less than
four samples, must be collected for the
hazardous waste stream to represent the complete
range of compositions and quantities that occur
during the entire averaging period due to normal
variations in the operating conditions for the
source or process generating the hazardous waste
stream. Examples of such normal variations are
seasonal variations in waste quantity or
fluctuations in ambient temperature.
iii)
All samples must be collected and handled in
accordance with written procedures prepared by
the owner or operator and documented in a site
sampling plan. This plan must describe the
284
procedure by which representative samples of the
hazardous waste stream are collected such that a
minimum loss of organics occurs throughout the
sample collection and handling process, and by
which sample integrity is maintained. A copy of
the written sampling plan must be maintained
on-site in the facility operating records. An
example of an acceptable sampling plan includes
a plan incorporating sample collection and
handling procedures in accordance with the
requirements specified in "Test Methods for
Evaluating Solid Waste, Physical/Chemical
Methods," EPA Publication SW
-846, incorporated
by reference in 35 Ill. Adm. Code 720.111, or in
Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
C) The owner or operator shall identify each discrete
quantity of the material composing the hazardous waste
represented by the averaging period designated in
subsection (a)(5)(B) above. An example of a discrete
quantity of material composing a hazardous waste
generated as part of a continuous process is the
quantity of material generated during a process
operating mode defined by a specific set of operating
conditions that are normal for the process. An
example of a discrete quantity of material composing a
hazardous waste generated as part of a batch process
that is performed repeatedly but not necessarily
continuously is the total quantity of material
composing a single batch generated by the process. An
example of a discrete quantity of material composing a
hazardous waste delivered to a facility in a container
is the total quantity of material held in the
container.
C)
Analysis. Each collected sample must be prepared and
analyzed in accordance with one or more of the methods
listed in subsections (a)(3)(C)(i) through
(a)(3)(C)(ix), including appropriate quality assurance
and quality control (QA/QC) checks and use of target
compounds for calibration. If Method 25D in 40 CFR
60, appendix A, incorporated by reference in 35 Ill.
Adm. Code 720.111 is not used, then one or more
methods should be chosen that are appropriate to
ensure that the waste determination accounts for and
reflects all organic compounds in the waste with
Henry's law constant values at least 0.1 mole-
fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
phase (0.1 Y/X) [which can also be expressed as 1.8 x
10
-6
atmospheres/gram
-mole/m
3
] at 25
ยฐ
C (77
ยฐ
F). Each
of the analytical methods listed in subsections
(a)(3)(C)(ii) through (a)(3)(C)(vii) below has an
associated list of approved chemical compounds, for
which USEPA considers the method appropriate for
measurement. If an owner or operator uses USEPA
Method 624, 625, 1624, or 1625 in 40 CFR 136, appendix
A, incorporated by reference in 35 Ill. Adm. Code
720.111, to analyze one or more compounds that are not
on that method's published list, the Alternative Test
285
Procedure contained in 40 CFR 136.4 and 136.5,
incorporated by reference in 35 Ill. Adm. Code
720.111, must be followed. If an owner or operator
uses USEPA Method 8260(B) or 8270(C) in "Test Methods
for Evaluating Solid Waste, Physical/Chemical
Methods", EPA Publication SW
-846, incorporated by
reference in 35 Ill. Adm. Code 720.111, to analyze one
or more compounds that are not on that method's
published list, the procedures in subsection
(a)(3)(C)(viii) below must be followed. At the
owner's or operator's discretion, the concentration of
each individual chemical constituent measured in the
waste by a method other than Method 25D may be
corrected to the concentration had it been measured
using Method 25D by multiplying the measured
concentration by the constituent
-specific adjustment
factor (f
m25D
), as specified in subsection (a)(4)(C)
below. Constituent
-specific adjustment fa
ctors (f
m25D
)
can be obtained by contacting the USEPA, Waste and
Chemical Processes Group, Office of Air Quality
Planning and Standards, Research Triangle Park, NC
27711.
i)
Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
ii)
Method 624 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
iii)
Method 625 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111. Perform corrections to the compounds
for which the analysis is being conducted based
on the "accuracy as recovery" using the factors
in Table 7 of the method.
iv)
Method 1624 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
v)
Method 1625 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
vi)
Method 8260(B) in "Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods", EPA
Publication SW -846, incorporated by reference in
35 Ill. Adm. Code 720.111. Maintain a formal
quality assurance program consistent with the
requirements of Method 8260(B). The quality
assurance program must include the elements set
forth in subsection (a)(3)(E) below.
vii)
Method 8270(C) in "Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods", EPA
Publication SW -846, incorporated by reference in
35 Ill. Adm. Code 720.111. Maintain a formal
quality assurance program consistent with the
requirements of Method 8270(C). The quality
286
assurance program must include the elements set
forth in subsection (a)(3)(E) below.
viii)
Any other USEPA standard method that has been
validated in accordance with "Alternative
Validation Procedure for EPA Waste and
Wastewater Methods", 40 CFR 63, appendix D,
incorporated by reference in 35 Ill. Adm. Code
720.111. As an alternative, other EPA standard
methods may be validated by the procedure
specified in subsection (a)(3)(C)(ix) below.
ix)
Any other analysis method that has been
validated in accordance with the procedures
specified in Section 5.1 or Section 5.3, and the
corresponding calculations in Section 6.1 or
Section 6.3, of Method 301 in 40 CFR 63,
appendix A, incorporated by reference in 35 Ill.
Adm. Code 720.111. The data are acceptable if
they meet the criteria specified in Section
6.1.5 or Section 6.3.3 of Method 301. If
correction is required under Section 6.3.3 of
Method 301, the data are acceptable if the
correction factor is within the range 0.7 to
1.30. Other Sections of Method 301 are not
required.
D) The following procedure must be used measure the VO
concentration for each discrete quantity of material
identified in subsection (a)(5)(C) above:
i) A sufficient number of samples, but in no case
fewer than four, must be collected to represent
the organic composition for the entire discrete
quantity of hazardous waste being tested. All
of the samples must be collected within a 1-hour
period. Sufficient information must be prepared
and recorded to document the waste quantity
represented by the samples and, as applicable,
the operating conditions for the source or
process generating the hazardous waste
represented by the samples.
ii) Each sample must be collected in accordance with
the requirements specified in "Test Methods for
Evaluating Solid Waste, Physical/Chemical
Methods", incorporated by reference in Section
720.111.
iii) Each collected sample must be prepared and
analyzed in accordance with the requirements of
Method 25D in 40 CFR 60, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
iv) The measured VO concentration for the discrete
quantity of hazardous waste must be determined
by using the results for all samples analyzed in
accordance with subsection (a)(5)(D)(iii) above
and the following equation:
287
C =
1
n
x
n
i = 1
C
i
โ
Where:
C = Measured VO concentration of the
discrete quantity of hazardous
waste, in ppmw.
i = Individual sample "i" of the
hazardous waste collected in
accordance with the requirements of
SW-846.
n = Total number of samples of hazardous
waste collected (at least 4) within
a 1-hour period.
C
i
= VO concentration measured by Method
25D for sample "i", in
ppmw.
E) The average VO concentration of the hazardous waste
must be determined using the following procedure:
i) When the facility owner or operator is the
generator of the hazardous waste, a sufficient
number of VO concentration measurements for the
hazardous waste must be performed in accordance
with the requirements of subsection (a)(5)(D)
above to represent the complete range of
hazardous waste organic compositions and
quantities that occur during the entire
averaging period due to normal variations in the
operating conditions for each process operating
mode identified for the source or process
generating the hazardous waste.
ii) When the facility owner or operator is not the
generator of the hazardous waste, a sufficient
number of VO concentration measurements for the
hazardous waste must be performed in accordance
with the requirements of subsection (a)(5)(D)
above to represent the complete range of
hazardous waste organic compositions and
quantities that occur in the hazardous waste as
received at the facility during the entire
averaging period.
iiiD) Calculations. The average VO concentration
of the
hazardous waste at the point of waste origination
(C)
on a mass-weighted basis
must be calculated by using
the results for all
VO measurements performed samples
analyzed in accordance with subsection (a)(
53)(DC)
above and the following equation:
288
=
T
j
j
C
1
Q
x
m
j = 1
( Q
x C
)
โ
C =
1
Q
x
n
i = 1
( Q
x C )
T
i
i
โ
Where:
C
ave
C =Average VO concentration of the hazardous
waste at the point of waste
origination on a mass-weighted
basis, in ppmw.
ji =
Individual discrete quantity sample "ji" of
the hazardous waste
for which a VO
concentration measurement is determined in
accordance with the requirements of
subsection (a)(5)(D) above
.
mn =
Total number of VO concentration
measurements determined in accordance with
the requirements of subsection (a)(5)(D)
abovesamples of the hazardous waste
collected (at least four)
for the
averaging period (not to exceed one year)
.
Q
j
Q
i
= Mass of the discrete quantity quantity of
the hazardous waste
stream
represented by C
j
C
i
, in kg /hr.
Q
T
=
Total mass quantity of the hazardous waste
forduring the averaging period, in kg
/hr.
C
j
C
i
= Measured VO concentration of
discrete
quantity sample "ji", as for the
hazardous waste determined in
accordance with the requirements of
subsection (a)( 53)(DC) above, in
ppmw.
E)
The quality assurance
progarm elements required under
subsections (a)(3)(C)(vi) and (a)(3)(C)(vii) above are
as follows:
i)
Documentation of site
-specific procedures to
minimize the loss of compounds due to
volatilization, biodegradation, reaction, or
sorption during the sample collection, storage,
preparation, introduction, and analysis steps.
ii)
Measurement of the overall accuracy and
precision of the specific procedures.
BOARD NOTE: Subsections (a)(3)(E)(i) and
(a)(3)(E)(ii) correspond with 40 CFR
289
265.984(a)(3)(iii)(F)(1), (a)(3)(iii)(F)(2),
(a)(3)(iii)(G)(1), and (a)(3)(iii)(G)(2), which
the Board has codified here to comport with
Illinois Administrative Code format
requirements.
6) Procedure for using knowledge of the waste to determine the
average VO concentration of a hazardous waste at the point
of waste origination.
A) The owner or operator shall identify and record the
point of waste origination for the hazardous waste.
All information used to determine the average VO
concentration of the hazardous waste must be based on
the hazardous waste composition at this point.
B) The owner or operator shall designate and record the
averaging period to be used for determining the
average VO concentration for the hazardous waste. The
averaging period must not exceed one year. An initial
waste determination must be performed for each
averaging period.
C) The owner or opera
tor shall prepare and record
sufficient information that documents the average VO
concentration for the hazardous waste. Information
may be used that is prepared by either the facility
owner or operator or by the generator of the hazardous
waste. Examples of information that may be used as
the basis for knowledge of the waste include: organic
material balances for the source or process generating
the waste; VO concentration measurements for the same
type of waste performed in accordance with the
procedure specified in subsection (a)(5)(D) above;
previous individual organic constituent test data for
the waste that are still applicable to the current
waste management practices; documentation that the
waste is generated by a process for which no
organics-
containing materials are used; previous test data for
other locations managing the same type of waste; or
other knowledge based on manifests, shipping papers,
or waste certification notices.
D) If test data other than VO concentration measurements
performed in accordance with the procedure specified
in subsection (a)(5)(D) above are used as the basis
for knowledge of the waste, then the owner or operator
shall document the test method, sampling protocol, and
the means by which sampling variability and analytical
variability are accounted for in the determination of
the average VO concentration. For example, an owner
or operator may use individual organic constituent
concentration test data that are validated in
accordance with Method 301 in 40 CFR 63, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, as the basis for knowledge of the waste.
4)
Use of owner or operator knowledge to determine average VO
concentration of a hazardous waste at the point of waste
origination.
290
A)
Documentation must be prepared that presents the
information used as the basis for the owner's or
operator's knowledge of the hazardous waste stream's
average VO concentration. Examples of information
that may be used as the basis for knowledge include
the following: material balances for the source or
process generating the hazardous waste stream;
constituent -specific chemical test data for the
hazardous waste stream from previous testing that are
still applicable to the current waste stream; previous
test data for other locations managing the same type
of waste stream; or other knowledge based on
information included in manifests, shipping papers, or
waste certification notices.
B)
If test data are used as the basis for knowledge, then
the owner or operator shall document the test method,
sampling protocol, and the means by which sampling
variability and analytical variability are accounted
for in the determination of the average VO
concentration. For example, an owner or operator may
use organic concentration test data for the hazardous
waste stream that are validated in accordance with
Method 301 in 40 CFR 63, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111, as the basis
for knowledge of the waste.
C)
An owner or operator using chemical
constituent -specific concentration test data as the
basis for knowledge of the hazardous waste may adjust
the test data to the corresponding average VO
concentration value which would have been obtained had
the waste samples been analyzed using Method 25D in 40
CFR 60, appendix A, incorporated by reference in 35
Ill. Adm. Code 720.111. To adjust these data, the
measured concentration for each individual chemical
constituent contained in the waste is multiplied by
the appropriate constituent
-specific adju stment factor
(f
m25D
).
D)
In the event that the Agency and the owner or operator
disagree on a determination of the average VO
concentration for a hazardous waste stream using
knowledge, then the results from a determination of
average VO concentration using direct measurement as
specified in subsection (a)(3) above must be used to
establish compliance with the applicable requirements
of this Subpart. The Agency may perform or request
that the owner or operator perform this determination
using direct measurement.
b)
Waste determination procedures for treated hazardous waste.
1)
An owner or operator shall perform the applicable waste
determination for each treated hazardous waste placed in a
waste management unit exempted under the provisions of
Section 725.983(c)(2) from using air emission controls in
accordance with standards specified in Section
s 725.985
through Section 725.988, as applicable to the waste
management unit.
291
2) The owner or operator shall perform a waste determination
for each discrete quantity of treated hazardous waste as
follows:
A) When the hazardous waste is treated by a continuous
process, the owner or operator shall:
i) Perform an initial waste determination for the
treated waste stream before the first time any
portion of the material in the waste stream is
placed in a waste management unit subject to
this Subpart, and thereafter update the
information used for the waste determination at
least once every 12 months following the date of
the initial waste determination; and
ii) Perform a new waste determination whenever
changes to the hazardous waste streams fed to
the process are reasonably likely to cause the
characteristics of the hazardous waste at the
point of waste treatment to change to levels
that fail to achieve the applicable conditions
specified in Section 725.983(c)(2).
B) When the hazardous waste is treated by a batch process
that is performed repeatedly but not necessarily
continuously, the owner or operator shall:
i) Perform an initial waste
determination for the
treated hazardous waste in one or more
representative batches treated by the process,
and thereafter update the information used for
the waste determination at least once every 12
months following the date of the initial waste
determination; and
ii) Perform a new waste determination whenever
changes to the hazardous waste treated by the
process are reasonably likely to cause the
characteristics of the hazardous waste at the
point of waste treatment to change to levels
that fail to achieve the applicable conditions
specified in Section 725.983(c)(2).
32)
The owner or operator shall designate and record the
specific provision in Section 725.983(c)(2)
forunder which
the waste determination is being performed. The waste
determination for the treated hazardous waste must be
performed using the applicable procedures specified in
subsections (b)( 43) through (b)( 109) below.
43)
Procedure to determine the average VO concentration of a
hazardous waste at the point of waste treatment.
A)
Identification.
The owner or operator shall identify
and record the point of waste treatment for the
hazardous waste. All waste samples used to determine
the average VO concentration of the hazardous waste
must be collected at this point.
B) The owner or operator shall designate and record the
292
averaging period to be used for determining the
average VO concentration for the hazardous waste. The
averaging period must not exceed one year. An initial
waste determination must be performed for each
averaging period.
C) The owner or operator shall identify each discrete
quantity of the material composing the hazardous waste
represented by the averaging period designated in
subsection (b)(4)(B) above.
D) The following procedure shall be used to measure the
VO concentration for each discrete quantity of
material identified in subsection (b)(4)(C) above:
i) A sufficient number of samples, but in no case
fewer than four samples, must be collected to
represent the organic composition for the entire
discrete quantity of hazardous waste being
tested. All of the samples must be collected
within a 1-hour period. Sufficient information
must be prepared and recorded to document the
waste quantity represented by the samples and,
as applicable, the operating conditions for the
process treating the hazardous waste represented
by the samples.
ii) Each sample must be collected in accordance with
the requirements specified in "Test Methods for
Evaluating Solid Waste, Physical/Chemical
Methods", incorporated by reference in 35 Ill.
Adm. Code 720.111.
iii) Each collected sample must be prepared and
analyzed in accordance with the requirements of
Method 25D in 40 CFR 60, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
iv) The measured VO concentration for the discrete
quantity of hazardous waste must be determined
by using the results for all samples analyzed in
accordance with subsection (a)(5)(D)(iii) above
and the following equation:
C =
1
n
x
n
i = 1
C
i
โ
Where:
C = Measured VO concentration of the
discrete quantity of hazardous
waste, in ppmw.
i = Individual sample "i" of the
hazardous waste collected in
accordance with the requirements of
SW-846.
293
n = Total number of samples of hazardous
waste collected (at least 4) within
a 1-hour period.
C
i
= VO concentration measured by Method
25D for sample "i", in
ppmw.
B)
Sampling. Samples of the hazardous waste stream must
be collected at the point of waste treatment in a
manner such that volatilization of
organics contained
in the waste and in the subsequent sample is minimized
and an adequately representative sample is collected
and maintained for analysis by the selected method.
i)
The averaging period to be used for determining
the average VO concentration for the hazardous
waste stream on a mass
-weighted average basis
must be designated and recorded. The averaging
period can represent any time interval that the
owner or operator determines is appropriate for
the hazardous waste stream but must not exceed
one year.
ii)
A sufficient number of samples, but no less than
four samples, must be collected for the
hazardous waste stream to represent the complete
range of compositions and quantities that occur
during the entire averaging period due to normal
variations in the operating conditions for the
process treating the hazardous waste stream.
Examples of such normal variations are seasonal
variations in waste quantity or fluctuations in
ambient temperature.
iii)
All samples must be collected and handled in
accordance with written procedures prepared by
the owner or operator and documented in a site
sampling plan. This plan must describe the
procedure by which representative samples of the
hazardous waste stream are collected such that a
minimum loss of organics occurs throughout the
sample collection and handling process, and by
which sample integrity is maintained. A copy of
the written sampling plan must be maintained
on-site in the facility operating
records. An
example of an acceptable sampling plan includes
a plan incorporating sample collection and
handling procedures in accordance with the
requirements specified in "Test Methods for
Evaluating Solid Waste, Physical/Chemical
Methods," EPA Publication No. SW
-846,
incorporated by reference in 35 Ill. Adm. Code
720.111, or in Method 25D in 40 CFR 60, appendix
A, incorporated by reference in 35 Ill. Adm.
Code 720.111.
C)
Analysis. Each collected sample must be prepared and
analyzed in accordance with one or more of the methods
listed in subsections (b)(3)(C)(i) through
(b)(3)(C)(ix) below, including appropriate quality
294
assurance and quality control (QA/QC) checks and use
of target compounds for calibration. If Method 25D in
40 CFR 60, appendix A is not used, then one or more
methods should be chosen that are appropriate to
ensure that the waste determination accounts for and
reflects all organic compounds in the waste with
Henry's law constant values at least 0.1 mole-
fraction-in-the-gas-phase/mole-fraction-in-the-liquid-
phase (0.1 Y/X) [which can also be expressed as 1.8 x
10
-6
atmospheres/gram-mole/m
3
] at 25 degrees Celsius.
Each of the analytical methods listed in subsections
(b)(3)(C)(ii) through (b)(3)(C)(vi) below has an
associated list of approved chemical compounds, for
which USEPA considers the method appropriate for
measurement. If an owner or operator uses EPA Method
624, 625, 1624, or 1625 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, to analyze one or more compounds that are not
on that method's published list, the Alternative Test
Procedure contained in 40 CFR 136.4 and 136.5,
incorporated by reference in 35 Ill. Adm. Code
720.111, must be followed. If an owner or operator
uses EPA Method 8260(B) or 8270(C) in "Test Methods
for Evaluating Solid Waste, Physical/Chemical
Methods", EPA Publication SW-846, incorporated by
reference in 35 Ill. Adm. Code 720.111, to analyze one
or more compounds that are not on that method's
published list, the procedures in subsection
(b)(3)(C)(viii) above must be followed. At the
owner's or operator's discretion, the concentration of
each individual chemical constituent measured in the
waste by a method other than Method 25D may be
corrected to the concentration had it been measured
using Method 25D by multiplying the measured
concentration by the constituent-specific adjustment
factor (f
m25D
) as specified in subsection (a)(4)(C)
below. Constituent-specific adjustment factors (f
m25D
)
can be obtained by contacting the USEPA, Waste and
Chemical Processes Group, Office of Air Quality
Planning and Standards, Research Triangle Park, NC
27711.
i)
Method 25D in 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
ii)
Method 624 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
iii)
Method 625 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111. Perform corrections to the compounds
for which the analysis is being conducted based
on the "accuracy as recovery" using the factors
in Table 7 of the method.
iv)
Method 1624 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
295
v)
Method 1625 in 40 CFR 136, appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111.
vi)
Method 8260(B) in "Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods", EPA
Publication SW-846, incorporated by reference in
35 Ill. Adm. Code 720.111. Maintain a formal
quality assurance program consistent with the
requirements of Method 8260(B). The quality
assurance program must include the elements set
forth in subsection (b)(3)(E) below.
vii)
Method 8270(C) in "Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods", EPA
Publication SW-846, incorporated by reference in
35 Ill. Adm. Code 720.111. Maintain a formal
quality assurance program consistent with the
requirements of Method 8270(C). The quality
assurance program must include the elements set
forth in subsection (b)(3)(E) below.
viii)
Any other EPA standard method that has been
validated in accordance with "Alternative
Validation Procedure for EPA Waste and
Wastewater Methods", 40 CFR 63, appendix D,
incorporated by reference in 35 Ill. Adm. Code
720.111. As an alternative, other EPA standard
methods may be validated by the procedure
specified in subsection (b)(3)(C)(ix) below.
ix)
Any other analysis method that has been
validated in accordance with the procedures
specified in Section 5.1 or Section 5.3, and the
corresponding calculations in Section 6.1 or
Section 6.3, of Method 301 in 40 CFR 63,
appendix A. The data are acceptable if they
meet the criteria specified in Section 6.1.5 or
Section 6.3.3 of Method 301. If correction is
required under Section 6.3.3 of Method 301, the
data are acceptable if the correction factor is
within the range 0.7 to 1.30. Other Sections of
Method 301 are not required.
E) The average VO concentration of the hazardous waste at
the point of waste treatment must be determined using
the following procedure:
i) When the facility owner or operator is the
generator of the hazardous waste, a sufficient
number of VO concentration measurements for the
hazardous waste must be performed in accordance
with the requirements of subsection (b)(4)(D)
above to represent the complete range of
hazardous waste organic compositions and
quantities treated by the process during the
entire averaging period.
iiD)
Calculations. The average VO concentration
of the
hazardous waste at the point of waste treatment
(C) on
a mass-weighted basis
must be calculated by using the
296
results for all VO measurements performed samples
analyzed in accordance with subsection (b)(
43)(DC)
above and the following equation:
ave
T
j
j
C
=
1
Q
x
m
j = 1
( Q
x C
)
โ
C =
1
Q
x
n
i = 1
( Q
x C )
T
i
i
โ
Where:
C
ave
C =Average VO concentration of the hazardous
waste at the point of waste
origination treatment on a
mass-weighted basis , in ppmw.
ji =
Individual discrete quantity sample "ji" of
the hazardous waste
for which a VO
concentration measurement is determined in
accordance with the requirements of
subsection (b)(4)(D) above
.
mn =
Total number of VO concentration
measurements determined in accordance with
the requirements of subsection (b)(4)(D)
abovesamples of the hazardous waste
collected (at least 4)
for the averaging
period (not to exceed 1 year)
.
Q
j
Q
i
= Mass of the discrete quantity of the
hazardous waste stream represented
by C
j
C
i
, in kg /hr.
Q
T
=
Total mass quantity of the hazardous waste
forduring the averaging period, in kg
/hr.
C
j
C
i
= Measured VO concentration of
discrete
quantity sample "ji", as for the
hazardous waste determined in
accordance with the requirements of
subsection (b)( 43)(DC) above, in
ppmw.
54)
Procedure to determine the exit concentration limit (C
t
) for
a treated hazardous waste.
A)
The point of waste origination for each hazardous
waste treated by the process at the same time must be
identified.
B)
If a sing le hazardous waste stream is identified in
subsection (b)( 54)(A) above, then the exit
concentration limit (C
t
) must be 100500 ppmw.
C)
If more than one hazardous waste stream is identified
297
in subsection (b)(
54)(A) above, then the
average VO
concentration of each hazardous waste stream at the
point of waste origination must be determined in
accordance with the requirements of subsection (a)
above. The exit concentration limit (C
t
) must be
calculated by using the results determined for each
individual hazardous waste stream and the following
equation:
t
x
x
y
x
y
C
=
m
x = 1
(Q
x C
)+
n
y = 1
( Q
x100ppmw)
m
x = 1
Q
+
n
y = 1
Q
โ
โ
โ
โ
Where:
C
t
=
Exit concentration limit for treated
hazardous waste, in
ppmw.
x =
Individual hazardous waste stream "x" that
has an average VO concentration less than
100500 ppmw at the point of waste
origination, as determined in accordance
with the requirements of
Section
725.984 subsection (a) above .
y =
Individual hazardous waste stream "y" that
has an average VO concentration equal to
or greater than 100500 ppmw at the point
of waste origination, as determined in
accordance with the requirements of
Section 725.984 subsection (a) above .
m =
Total number of "x" hazardous waste
streams treated by process.
n =
Total number of "y" hazardous waste
streams treated by process.
Q
x
=
Annual mass quantity of hazardous waste
stream "x", in kg/yr.
Q
y
=
Annual mass quantity of hazardous waste
stream "y", in kg/yr.
C
x
=
Average VO concentration of hazardous
waste stream "x" at the point of waste
origination, as determined in accordance
with the requirements of
Section
725.984 subsection (a) above , in ppmw.
65)
Procedure to determine the organic reduction efficiency (R)
for a treated hazardous waste.
A)
The organic reduction efficiency
(R) for a treatment
298
process must be determined based on results for a
minimum of three consecutive runs.
The sampling time
for each run must be one hour.
B) The point of eachAll hazardous waste stream
s entering
the process and eachall hazardous waste stream
s
exiting the treatment process that is to be included
in the calculation of the organic reduction efficiency
for the process must be identified.
The owner or
operator shall prepare a sampling plan for measuring
these streams that accurately reflects the retention
time of the hazardous waste in the process.
C)
For each run, the following information must be
determined for each hazardous waste stream identified
in subsection (b)(
65)(B) above, using the following
procedures:
i)
The mass quantity of each hazardous waste stream
entering the process (
Q
b
) and the mass quantity
of each hazardous waste stream exiting the
process ( Q
a
) must be determined.
ii)
The average VO concentration
at the point of
waste origination
of each hazardous waste stream
entering the process (
C
b
C
b
) during the run must
be measured determined in accordance with the
requirements of subsections (a)(
53)(D)(i)
through (a)(5)(D)(iv)
belowabove. The average
VO concentration
at the point of waste treatment
of each hazardous waste stream exiting the
process ( C
a
C
a
) during the run must be determined
in accordance with the requirements of
subsection (b)( 43)(D) belowabove. Samples must
be collected as follows: For a continuous
process, the samples of the hazardous waste
entering and samples of the hazardous waste
exiting the process must be collected
concurrently. For a batch process, the samples
of the hazardous waste entering the process must
be collected at the time that the hazardous
waste is placed in the process. The samples of
the hazardous waste exiting the process must be
collected as soon as practicable after the time
when the process stops operation or the final
treatment cycle ends.
D)
The waste volatile organic mass flow entering the
process ( E
b
) and the waste volatile organic mass flow
exiting the process (
E
a
) must be calculated by using
the results determined in accordance with subsection
(b)(65)(C) above and the following equations:
b
6
bj
bj
E
=
1
10
m
j = 1
( Q
x C
)
โ
299
a
6
aj
aj
E
=
1
10
m
j = 1
(Q
x C
)
โ
b
6
bj
bj
E
=
1
10
m
j = 1
( Q
xC
)
โ
a
6
aj
aj
E
=
1
10
m
j = 1
( Q
xC
)
โ
Where:
E
a
=
Waste volatile organic mass flow exiting
the process, in kg/hr.
E
b
=
Waste volatile organic mass flow entering
the process, in kg/hr.
m =
Total number of runs (at least 3)
j =
Individual run "j"
Q
bj
=
Mass quantity of hazardous waste entering
the process during run "j", in kg/hr.
Q
aj
=
Average mass quantity of waste exiting
the
process during run "j", in kg/hr.
C
aj
C
aj
=
Measured VO concentration of
hazardous waste exiting
the process
during run "j", as determined in
accordance with the requirements of
Section 725.984 subsection (b)(43)(D)
above, in ppmw.
C
bj
C
bj
=
Measured VO concentration of
hazardous waste entering
the process
during run "j", as determined in
accordance with the requirements of
Section 725.984 subsection 725.984
(a)(53)(D)(i) through (a)(5)(D)(iv)
above, in ppmw.
E)
The organic reduction efficiency of the process must
be calculated by using the results determined in
accordance with subsection (b)(
65)(D) above and the
following equation:
R =
E
- E
E
x100%
b
a
b
300
Where:
R =
Organic reduction efficiency,
in percent.
E
b
=
Waste volatile organic mass flow entering
the process as determined in accordance
with the requirements of subsection
(b)(65)(D) above, in kg/hr.
E
a
=
Waste volatile organic ma
ss flow exiting
the process as determined in accordance
with the requirements of subsection
(b)(65)(D) above, in kg/hr.
76)
Procedure to determine the organic
biodegradation efficiency
(R
bio
) for a treated hazardous waste.
A)
The fraction of organics biodegraded (
F
bio
) must be
determined using the procedure specified in 40 CFR 63,
Appendix C, incorporated by reference in 35 Ill. Adm.
Code 7 20.111.
B)
The organic biodegradation efficiency
(R
bio
) must be
calculated by using the following equation:
bio
bio
R
= F
x100%
Where
R
bio
= Organic biodegradation efficiency, in
percent.
F
bio
= Fraction of organic biodegraded
, as
determined in accordance with the
requirements of subsection (b)(
76)(A)
above.
87)
Procedure to determine the required organic mass removal
rate (RMR) for a treated hazardous waste.
A) The point of waste origination for
eachAll of the
hazardous waste treated bystreams entering the
treatment process at the same time
must be identified.
B) For each hazardous waste stream identified in
subsection (b)(8)(A) above,
theThe average VO
concentration of the hazardous waste stream at the
point of waste origination must be determined in
accordance with the requirements of subsection (a)
above.
C)
For each individual hazardous waste stream that has a
n
average volatile organic concentration equal to or
greater than 100500 ppmw at the point of waste
origination as determined in accordance with the
requirements of subsection (b)(8)(B) above
, the
average volumetric flow rate of hazardous waste
and
the density of the hazardous waste stream
at the point
of waste origination
and the density of the hazardous
waste stream must be determined.
301
D)
The required organic mass removal rate
(RMR) for the
hazardous waste must be calculated by using the
results determined for each individual hazardous waste
stream in accordance with the requirements of
subsections (b)(8)(B) and (b)(8)(C)
aboveaverage VO
concentration, average volumetric flow rate, and
density determined for each individual hazardous waste
stream, and the following equation:
RMR =
n
y = 1
V
x k
x
( C
-100ppmw)
10
y
y
y
6
โ
๏ฃฎ
๏ฃฐ
๏ฃฏ
๏ฃบ
๏ฃผ
๏ฃป
RMR =
n
y = 1
V
x k
x
( C
- 500ppmw)
10
y
y
y
6
โ
๏ฃฎ
๏ฃฐ
๏ฃฏ
๏ฃบ
๏ฃผ
๏ฃป
Where:
RMR =
Required organic mass removal rate, in kg/hr.
y =
Individual hazardous waste stream "y" that has
an average volatile organic
(VO) concentration
equal to or greater than
100500 ppmw at the
point of waste origination, as determined in
accordance with the requirements of
Section
725.984 subsection (a) above .
n =
Total number of "y" hazardous waste streams
treated by process.
V
y
=
Average volumetric flow rate of hazardous waste
stream "y" at the point of waste origination,
in m
3
/hr.
k
y
=
Density of hazardous waste stream "y", in kg/m
3
C
y
=
Average VO concentration of hazardous waste
stream "y" at the point of waste origination
, as
determined in accordance with the requirements
of Section 725.984 subsection (a) above , in ppmw.
98)
Procedure to determine the actual or
ganic mass removal rate
(MR) for a treated hazardous waste.
A)
The actual organic mass removal rate
(MR) must be
determined based on results for a minimum of three
consecutive runs. The sampling time for each run must
be one hour.
B)
The waste volatile organic mass flow entering the
process ( E
b
) and the waste volatile organic mass flow
exiting the process (
E
a
) must be determined in
accordance with the requirements of subsection
(b)(65)(D) above.
C)
The actual organic mass removal rate
(MR) must be
302
calculated by using the
results mass flow rate
determined in accordance with the requirements of
subsection (b)( 98)(B) above and the following
equation:
MR = E
- E
b
a
Where:
MR =
Actual organic mass removal rate, in
kg/hr.
E
b
=
Waste volatile organic mass flow entering
process, as determined in accordance with
the requirements of subsection (b)(
65)(D)
above, in kg/hr.
E
a
=
Waste volatile organic mass flow exiting
process, as determined in accordance with
the requirements of subsection (b)(
65)(D)
above, in kg/hr.
109)
Procedure to determine the actual organic mass
biodegradation rate (
MR
bio
) for a treated hazardous waste.
A)
The actual organic mass
biodegradation rate
(MR
bio
)
must be determined based on results for a minimum of
three consecutive runs. The sampling time for each
run must be one hour.
B)
The waste organic mass flow entering the process (
E
b
)
must be determined in accordance with the requirements
of subsection (b)(
65)(D) above.
C)
The fraction of organic biodegraded (
F
bio
) must be
determined using the procedure specified in 40 CFR 63,
Appendix C, incorporated by reference in 35 Ill. Adm.
Code 720.111.
D)
The actual organic mass
biodegradation rate
(MR
bio
)
must be calculated by using the mass flow rates and
fraction of organic biodegraded determined in
accordance with the requirements of subsections
(b)(109)(B) and (b)( 109)(C) above and the following
equation:
bio
b
bio
MR
= E
x F
Where:
MR
bio
=Actual organic mass
biodegradation rate,
in kg/hr.
E
b
=
Waste organic mass flow entering
the
process, as determined in accordance with
the requirements of subsection (b)(
65)(D)
above, in kg/hr.
F
bio
= Fraction of organic biodegraded, as
determined in accordance with the
303
requirements of subsection (b)(
109)(C)
above.
c)
Procedure to determine the maximum organic vapor pressure of a
hazardous waste in a tank.
1)
An owner or operator shall determine the maximum organic
vapor pressure for each hazardous waste placed in a tank
using air emission Tank Level 1 controls in accordance with
standards specified in Section 725.985(c).
2)
An owner or operator shall use either direct measurement, as
specified in subsection (c)(3) above, or knowledge of the
waste, as specified by subsection (c)(4) above, to determine
the maximum organic vapor pressure that is representative of
the hazardous waste composition stored or treated in the
tank.
3) To determine the maximum organic vapor pressu
re of the
hazardous waste by direct measurement, the following
procedure must be
used:Direct measurement to determine the
maximum organic vapor pressure of a hazardous waste.
A) Representative Sampling. A sufficient number of
samples of the waste contained in the tank
must be
collected to be representative of the waste contained
in the tank . Sampling All samples must be conducted
and handled in accordance with
written procedures
prepared by the owner or operator and documented in a
site sampling plan. This plan must describe the
procedure by which representative samples of the
hazardous waste are collected such that a minimum loss
of organics occurs throughout the sample collection
and handling process and by which sample integrity is
maintained. A copy of the written sampling plan must
be maintained on -site in the facility operating
records. An example of an acceptable sampling plan
includes a plan incorporating sample collection and
handling procedures in accordance with
the
requirements specified in "Test Methods for Evaluating
Solid Waste, Physical/Chemical Methods",
USEPA
Publication No. SW
-846, incorporated by reference in
35 Ill. Adm. Code 720.111
, or in Method 25D in 40 CFR
60, appendix A, incorporated by reference in 35 Ill.
Adm. Code 720.111
.
B)
Analysis. Any appropriate one of the following
methods may be used to analyze the samples and compute
the maximum organic vapor pressure
of the hazardous
waste, as appropriate :
i)
Method 25E in 40 CFR 60, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111;
ii)
Methods described in American Petroleum
Institute Publication 2517, incorporated by
reference in 35 Ill. Adm. Code 720.111;
iii)
Methods obtained from standard reference texts;
304
iv)
ASTM Method D 2879-92, incorporated by reference
in 35 Ill. Adm. Code 720.111
); or
v)
Any other method approved by the Agency
for this
use by the owner or operator
.
4) To determine the maximum organic vapor pressure of the
hazardous waste by knowledge, sufficient information must be
prepared and recorded that documents the maximum organic
vapor pressure of the hazardous waste in the tank. Examples
of information that may be used include: documentation that
the waste is generated by a process for which no
organics-
containing materials are used or that the waste is generated
by a process for which at other locations it previously has
been determined by direct measurement that the waste maximum
organic vapor pressure is less than the maximum vapor
pressure limit for the appropriate design capacity category
specified for the tank.
4)
Use of knowledge to determine the maximum organic vapor
pressure of the hazardous waste. Documentation must be
prepared and recorded that presents the information used as
the basis for the owner's or operator's knowledge that the
maximum organic vapor pressure of the hazardous waste is
less than the maximum vapor pressure limit listed in Section
725.985(b)(1)(A) for the applicable tank design capacity
category. An example of information that may be used is
documentation that the hazardous waste is generated by a
process for which at other locations it previously has been
determined by direct measurement that the waste maximum
organic vapor pressure is less than the maximum vapor
pressure limit for the appropriate tank design capacity
category.
d)
Procedure for determining no detectable organic emissions for the
purpose of complying with this Subpart:
1)
The test must be conducted in accordance with the procedures
specified in Method 21 of 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code 720.111.
Each potential leak interface (i.e., a location where
organic vapor leakage could occur) on the cover and
associated closure devices must be checked. Potential leak
interfaces that are associated with covers and closure
devices include, but are not limited to any of the
following: the interface of the cover and its foundation
mounting, the periphery of any opening on the cover and its
associated closure device, and the sealing seat interface on
a spring -loaded pressure relief valve.
2)
The test must be performed when the unit contains a
hazardous waste having an organic concentration
representative of the range of concentrations for the
hazardous waste expected to be managed in the unit. During
the test, the cover and closure devices must be secured in
the closed position.
3)
The detection instrument must meet the performance criteria
of Method 21 of 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111, except the
instrument response factor criteria in Section 3.1.2(a) of
305
Method 21 must be for the average composition of the organic
constituents in the hazardous waste placed in the waste
management unit, not for each individual organic
constituent.
4)
The detection instrument must be calibrated before use on
each day of its use by the procedures specified in Method 21
of 40 CFR 60, appendix A, incorporated by reference in 35
Ill. Adm. Code 720.111.
5)
Calibration gases must be as follows:
A)
Zero air (less than 10
ppmv hydrocarbon in air), and
B)
A mixture of methane in air at a concentration of
approximately, but less than, 10,000
ppmv.
6)
The background level must be determined according to the
procedures in Method 21 of 40 CFR 60, appendix A,
incorporated by reference in 35 Ill. Adm. Code 720.111.
7)
Each potential leak interface must be checked by traversing
the instrument probe around the potential leak interface as
close to the interface as possible, as described in Method
21 of 40 CFR 60, appendix A, incorporated by reference in 35
Ill. Adm. Code 720.111. In the case when the configuration
of the cover or closure device prevents a complete traverse
of the interface, all accessible portions of the interface
must be sampled. In the case when the configuration of the
closure device prevents any sampling at the interface and
the device is equipped with an enclosed extension or horn
(e.g., some pressure relief devices), the instrument probe
inlet must be placed at approximately the center of the
exhaust area to the atmosphere.
8)
The arithmetic difference between the maximum organic
concentration indicated by the instrument and the background
level must be compared with the value of 500
ppmv except
when monitoring a seal around a rotating shaft that passes
through a cover opening, in which case the comparison must
be as specified in subsection (d)(9) below. If the
difference is less than 500
ppmv, then the potential leak
interface is determined to operate with no detectable
organic emissions.
9)
For the seals around a rotating shaft that passes through a
cover opening, the arithmetic difference between the maximum
organic concentration indicated by the instrument and the
background level must be compared with the value of 10,000
ppmw. If the difference is less than 10,000
ppmw, then the
potential leak interface is determined to operate with no
detectable organic emissions.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.985
Standards: T anks
a) This Section applies to owners and operators of tanks subject to
this Subpart into which any hazardous waste is placed except for
the following tanks:
306
1) A tank in which all hazardous waste entering the tank meets
the conditions specified in Section 725.983(c); or
2) A tank used for biological treatment of hazardous waste in
accordance with the requirements of Section
725.983(c)(2)(D).
a)
The provisions of this Section apply to the control of air
pollutant emissions from tanks for which Section 725.983(b)
references the use of this Section for such air emission control.
b)
The owner or operator shall
place the hazardous waste into one of
the following tankscontrol air pollutant emissions from each tank
subject to this Section in accordance with the following
requirements, as applicable
:
1) A tank equipped with a cover (e.g., a fixed roof) that is
vented through a closed-vent system to a control device in
accordance with the requirements specified in subsection (d)
below;
2) A tank eq uipped with a fixed roof and internal floating roof
in accordance with the requirements of Section 725.991;
3) A tank equipped with an external floating roof in accordance
with the requirements of Section 725.991; or
4) A pressure tank that is designed to operate as a closed
system such that the tank operates with no detectable
organic emissions at all times that hazardous waste is in
the tank except as provided for in subsection (g) below.
c) As an alternative to complying with subsection (b) above
, an owner
or operator may place hazardous waste in a tank equipped with a
cover (e.g., a fixed roof) meeting the requirements specified in
subsection (d)(1) below when the hazardous waste is determined to
meet all of the following conditions:
1) The hazardous waste is neither mixed, stirred, agitated, nor
circulated within the tank by the owner or operator using a
process that results in splashing, frothing, or visible
turbulent flow on the waste surface during normal process
operations;
2) The hazar dous waste in the tank is not heated by the owner
or operator except during conditions requiring that the
waste be heated to prevent the waste from freezing or to
maintain adequate waste flow conditions for continuing
normal process operations;
3) The hazardous waste in the tank is not treated by the owner
or operator using a waste stabilization process or a process
that produces an exothermic reaction; and
4) The maximum organic vapor pressure of the hazardous waste in
the tank as determined using the procedure specified in
Section 725.984(c) is less than the following applicable
value:
1)
For a tank that manages hazardous waste which meets all of
the conditions specified in subsections (b)(1)(A) through
307
(b)(1)(C) below, the owner or operator shall control air
pollutant emissions from the tank in accordance with the
Tank Level 1 controls specified in subsection (c) below or
the Tank Level 2 controls specified in subsection (d) below.
A)
The hazardous waste in the tank has a maximum organic
vapor pressure that is less than the maximum organic
vapor pressure limit for the tank's design capacity
category, as follows:
Ai) If theFor a tank design capacity
is equal to or
greater than 151 m
3
(5333 ft
3
or 39,887 gal),
then the maximum organic vapor pressure
must be
less thanlimit for the tank is
5.2 kPa (0.75
psia or 39 mm Hg);
Bii) If theFor a tank design capacity
is equal to or
greater than 75 m
3
(2649 ft
3
or 19,810 gal) but
less than 151 m
3
(5333 ft
3
or 39,887 gal),
then
the maximum organic vapor pressure
must be less
thanlimit for the tank is
27.6 kPa (4.0 psia or
207 mm Hg); or
Ciii) If theFor a tank design capacity is less than 75
m
3
(2649 ft
3
or 19,810 gal),
then the maximum
organic vapor pressure then the maximum organic
vapor pressure must be less thanlimit for the
tank is 76.6 kPa (11.1 psia or 574 mm Hg).
d) To comply with subsection (b)(1) above, the owner or operator
shall design, install, operate, and maintain a cover that vents
the organic vapors emitted from hazardous waste in the tank
through a closed-vent system connected to a control device.
1) The cover must be designed and operated to meet the
following requirements:
A) The cover and all cover openings (e.g., access
hatches, sampling ports, and gauge wells) must be
designed to operate with no detectable organic
emissions when all cover openings are secured in a
closed, sealed position.
B) Each cover opening must be secured in a closed, sealed
position (e.g., covered by a
gasketed lid or cap) at
all times that hazardous waste is in the tank except
as provided for in subsection (f) below.
2) The closed-vent system and control device must be designed
and operated in accordance with the requirements of Section
725.988.
e) The owner and operator shall install, operate, and maintain
enclosed pipes or other closed systems for the transfer of
hazardous waste as described in subsection (e)(1) or (e)(2) below.
BOARD NOTE: U.S. EPA considers a drain system that meets the
requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
a "closed-system". The Board intends that this meaning be
included in the use of that term for the purposes of this Subpart.
308
1) Transfer all hazardous waste to the tank from another tank,
surface impoundment, or container subject to this Subpart,
except for those hazardous wastes that meet the conditions
specified in Section 725.983(c); and
2) Transfer all hazardous waste from the tank to another tank,
surface impoundment, or container subject to this Subpart,
except for those hazardous wastes that meet the conditions
specified in Section 725.983(c).
f) Each cover opening must be secured in a closed, sealed position
(e.g., covered by a
gasketed lid) at all times that hazardous
waste is in the tank except when it is necessary to use the cover
opening to:
1) Add, remove, inspect, or sample the material in the tank;
2) Inspect, maintain, repair, or replace equipment located
inside the tank; or
3) Vent gases or vapors from the tank to a closed-vent system
connected to a control device that is designed and operated
in accordance with the requirements of Section 725.988.
g) One or more safety devices that vent directly to the atmosphere
may be used on the tank, cover, closed-vent system, or control
device provided each safety device meets all of the following
conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the tank or the closed-vent system
connected to a control device; and
2) The safety device remains in a closed, se
aled position at
all times except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the tank, cover, closed-vent
system, or control device in accordance with good
engineering and safety practices for handling flammable,
combustible, explosive, or other hazardous materials. An
example of an unplanned event is a sudden power outage.
B)
The hazardous waste in the tank is not heated by the
owner or operator to a temperature that is greater
than the temperature at which the maximum organic
vapor pressure of the hazardous waste is determined
for the purpose of complying with subsection (b)(1)(A)
above.
C)
The hazardous waste in the tank is not treated by the
owner or operator using a waste stabilization process,
as defined in Section 725.981.
2)
For a tank that manages hazardous waste that does not meet
all of the conditions specified in subsections (b)(1)(A)
through (b)(1)(C) above, the owner or operator shall control
air pollutant emissions from the tank by using Tank Level 2
controls in accordance with the requirements of subsection
(d) below. Examples of tanks required to use Tank Level 2
controls include the following: a tank used for a waste
stabilization process and a tank for which the hazardous
309
waste in the tank has a maximum organic vapor pressure that
is equal to or greater than the maximum organic vapor
pressure limit for the tank's design capacity category, as
specified in subsection (b)(1)(A) above.
c)
Owners and operators controlling air pollutant emissions from a
tank using Tank Level 1 controls shall meet the requirements
specified in subsections (c)(1) through (c)(4) below:
1)
The owner or operator shall determine the maximum organic
vapor pressure for a hazardous waste to be managed in the
tank using Tank Level 1 controls before the first time the
hazardous waste is placed in the tank. The maximum organic
vapor pressure must be determined using the procedures
specified in Section 725.984(c). Thereafter, the owner or
operator shall perform a new determination whenever changes
to the hazardous waste managed in the tank could potentially
cause the maximum organic vapor pressure to increase to a
level that is equal to or greater than the maximum organic
vapor pressure limit for the tank design capacity category
specified in subsection (b)(1)(A) above, as applicable to
the tank.
2)
The tank must be equipped with a fixed roof designed to meet
the following specifications:
A)
The fixed roof and its closure devices must be
designed to form a continuous barrier over the entire
surface area of the hazardous waste in the tank. The
fixed roof may be a separate cover installed on the
tank (e.g., a removable cover mounted on an open
-top
tank) or may be an integral part of the tank
structural design (e.g., a horizontal cylindrical tank
equipped with a hatch).
B)
The fixed roof must be installed in a manner such that
there are no visible cracks, holes, gaps, or other
open spaces between roof Section joints or between the
interface of the roof edge and the tank wall.
C)
Each opening in the fixed roof must be either:
i)
Equipped with a closure device designed to
operate such that when the closure device is
secured in the closed position there are no
visible cracks, holes, gaps, or other open
spaces in the closure device or between the
perimeter of the opening and the closure device;
or
ii)
Connected by a closed
-vent system that is vented
to a control device. The control device must
remove or destroy
organics in the vent stream,
and it must be operating whenever hazardous
waste is managed in the tank.
D)
The fixed roof and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and which will maintain the integrity of
the fixed roof and closure devices throughout their
310
intended service life. Factors to be considered when
selecting the materials for and designing the fixed
roof and closure devices must include the following:
organic vapor permeability; the effects of any contact
with the hazardous waste or its vapors managed in the
tank; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
used for the tank on which the fixed roof is
installed.
3)
Whenever a hazardous waste is in the tank, the fixed roof
must be installed with each closure device secured in the
closed position, except as follows:
A)
Opening of closure devices or removal of the fixed
roof is allowed at the following times:
i)
To provide access to the tank for performing
routine inspection, maintenance, or other
activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample the
liquid in the tank, or when a worker needs to
open a hatch to maintain or repair equipment.
Following completion of the activity, the owner
or operator shall promptly secure the closure
device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues
from the bottom of tank.
B)
Opening of a spring
-loaded pressure -vacuum relief
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the tank internal pressure in accordance
with the tank design specifications. The device must
be designed to operate with no detectable organic
emissions when the device is secured in the closed
position. The settings at which the device opens must
be established such that the device remains in the
closed position whenever the tank internal pressure is
within the internal pressure operating range
determined by the owner or operator based on the tank
manufacturer recommendations; applicable regulations;
fire protection and prevention codes; standard
engineering codes and practices; or other requirements
for the safe handling of flammable, ignitable,
explosive, reactive, or hazardous materials. Examples
of normal operating conditions that may require these
devices to open are during those times when the tank
internal pressure exceeds the internal pressure
operating range for the tank as a result of loading
operations or diurnal ambient temperature
fluctuations.
C)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
311
4)
The owner or operator shall inspect the air emission control
equipment in accordance with the following requirements.
A)
The fixed roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the roof Sections or
between the roof and the tank wall; broken, cracked,
or otherwise damaged seals or gaskets on closure
devices; and broken or missing hatches, access covers,
caps, or other closure devices.
B)
The owner or operator shall perform an initial
inspection of the fixed roof and its closure devices
on or before the date that the tank becomes subject to
this Section. Thereafter, the owner or operator shall
perform the inspections at least once every year,
except under the special conditions provided for in
subsection (l) below.
C)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
D)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 725.990(b).
d)
Owners and operators controlling air pollutant emissions from a
tank using Tank Level 2 controls shall use one of the following
tanks:
1)
A fixed -roof tank equipped with an internal floating roof in
accordance with the requirements specified in subsection (e)
below;
2)
A tank equipped with an external floating roof in accordance
with the requirements specified in subsection (f) below;
3)
A tank vented through a closed
-vent system to a control
device in accordance with the requirements specified in
subsection (g) below;
4)
A pressure tank designed and operated in accordance with the
requirements specified in subsection (h) below; or
5)
A tank located inside an enclosure that is vented through a
closed -vent system to an enclosed combustion control device
in accordance with the requirements specified in subsection
(i) below.
e)
The owner or operator that controls air pollutant emissions from a
tank using a fixed
-roof with an internal floating roof shall meet
the requirements specified in subsections (e)(1) through (e)(3)
below.
1)
The tank must be equipped with a fixed roof and an internal
floating roof in accordance with the following requirements:
A)
The internal floating roof must be designed to float
312
on the liquid surface except when the floating roof
must be supported by the leg supports.
B)
The internal floating roof must be equipped with a
continuous seal between the wall of the tank and the
floating roof edge that meets either of the following
requirements:
i)
A single continuous seal that is either a
liquid -mounted seal or a metallic shoe seal, as
defined in Section 725.981; or
ii)
Two continuous seals mounted one above the
other. The lower seal may be a vapor
-mounted
seal.
C)
The internal floating roof must meet the following
specifications:
i)
Each opening in a
noncontact internal floating
roof except for automatic bleeder vents (vacuum
breaker vents) and the rim space vents is to
provide a projection below the liquid surface.
ii)
Each opening in the internal floating roof must
be equipped with a
gasketed cover or a
gasketed
lid except for leg sleeves, automatic bleeder
vents, rim space vents, column wells, ladder
wells, sample wells, and stub drains.
iii)
Each penetration of the internal floating roof
for the purpose of sampling must have a slit
fabric cover that covers at least 90 percent of
the opening.
iv)
Each automatic bleeder vent and rim space vent
must be gasketed.
v)
Each penetration of the internal floating roof
that allows for passage of a ladder must have a
gasketed sliding cover.
vi)
Each penetration of the internal floating roof
that allows for passage of a column supporting
the fixed roof must have a flexible fabric
sleeve seal or a
gasketed sliding cover.
2)
The owner or operator shall operate the tank in accordance
with the following requirements:
A)
When the floating roof is resting on the leg supports,
the process of filling, emptying, or refilling must be
continuous and must be completed as soon as practical.
B)
Automatic bleeder vents are to be set closed at all
times when the roof is floating, except when the roof
is being floated off or is being landed on the leg
supports.
C)
Prior to filling the tank, each cover, access hatch,
gauge float well or lid on any opening in the internal
313
floating roof must be bolted or fastened closed (i.e.,
no visible gaps). Rim space vents are to be set to
open only when the internal floating roof is not
floating or when the pressure beneath the rim exceeds
the manufacturer's recommended setting.
3)
The owner or operator shall inspect the internal floating
roof in accordance with the procedures specified as follows:
A)
The floating roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to
the following: when the internal floating roof is not
floating on the surface of the liquid inside the tank;
when liquid has accumulated on top of the internal
floating roof; when any portion of the roof seals have
detached from the roof rim; when holes, tears, or
other openings are visible in the seal fabric; when
the gaskets no longer close off the hazardous waste
surface from the atmosphere; or when the slotted
membrane has more than 10 percent open area.
B)
The owner or operator shall inspect the internal
floating roof components as follows, except as
provided in subsection (e)(3)(C) below:
i)
Visually inspect the internal floating roof
components through openings on the fixed
-roof
(e.g., manholes and roof hatches) at least once
every 12 months after initial fill, and
ii)
Visually inspect the internal floating roof,
primary seal, secondary seal (if one is in
service), gaskets, slotted membranes, and sleeve
seals (if any) each time the tank is emptied and
degassed and at least once every 10 years.
C)
As an alternative to performing the inspections
specified in subsection (e)(3)(B) above for an
internal floating roof equipped with two continuous
seals mounted one above the other, the owner or
operator may visually inspect the internal floating
roof, primary and secondary seals, gaskets, slotted
membranes, and sleeve seals (if any) each time the
tank is emptied and degassed and at least every five
years.
D)
Prior to each inspection required by subsection
(e)(3)(B) or (e)(3)(C) above, the owner or operator
shall notify the Agency in advance of each inspection
to provide the Agency with the opportunity to have an
observer present during the inspection. The owner or
operator shall notify the Agency of the date and
location of the inspection as follows:
i)
Prior to each visual inspection of an internal
floating roof in a tank that has been emptied
and degassed, written notification must be
prepared and sent by the owner or operator so
that it is received by the Agency at least 30
314
calendar days before refilling the tank, except
when an inspection is not planned, as provided
for in subsection (e)(3)(D)(ii) below.
ii)
When a visual inspection is not planned and the
owner or operator could not have known about the
inspection 30 calendar days before refilling the
tank, the owner or operator shall notify the
Agency as soon as possible, but no later than
seven calendar days before refilling of the
tank. This notification may be made by
telephone and immediately followed by a written
explanation for why the inspection is unplanned.
Alternatively, written notification, including
the explanation for the unplanned inspection,
may be sent so that it is received by the
Regional Administrator at least seven calendar
days before refilling the tank.
E)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
F)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 725.990(b).
f)
The owner or operator that controls air pollutant emissions from a
tank using an external floating roof shall meet the requirements
specified in subsections (f)(1) through (f)(3) below.
1)
The owner or operator shall design the external floating
roof in accordance with the following requirements:
A)
The external floating roof must be designed to float
on the liquid surface except when the floating roof
must be supported by the leg supports.
B)
The floating roof must be equipped with two continuous
seals, one above the other, between the wall of the
tank and the roof edge. The lower seal is referred to
as the primary seal, and the upper seal is referred to
as the secondary seal.
i)
The primary seal must be a liquid
-mounted seal
or a metallic shoe seal, as defined in Section
725.981. The total area of the gaps between the
tank wall and the primary seal must not exceed
212 square centimeters (cm
2
) per meter (10.0 in
2
per foot) of tank diameter, and the width of any
portion of these gaps must not exceed 3.8
centimeters (cm) (1.5 inches). If a metallic
shoe seal is used for the primary seal, the
metallic shoe seal must be designed so that one
end extends into the liquid in the tank and the
other end extends a vertical distance of at
least 61 centimeters above the liquid surface.
ii)
The secondary seal must be mounted above the
primary seal and cover the annular space between
the floating roof and the wall of the tank. The
315
total area of the gaps between the tank wall and
the secondary seal must not exceed 21.2 cm
2
per
meter (1.0 in
2
per foot) of tank diameter, and
the width of any portion of these gaps must not
exceed 1.3 cm (0.5 inch).
C)
The external floating roof must meet the following
specifications:
i)
Except for automatic bleeder vents (vacuum
breaker vents) and rim space vents, each opening
in a noncontact external floating roof must
provide a projection below the liquid surface.
ii)
Except for automatic bleeder vents, rim space
vents, roof drains, and leg sleeves, each
opening in the roof must be equipped with a
gasketed cover, seal, or lid.
iii)
Each access hatch and each gauge float well must
be equipped with a cover designed to be bolted
or fastened when the cover is secured in the
closed position.
iv)
Each automatic bleeder vent and each rim space
vent must be equipped with a gasket.
v)
Each roof drain that empties into the liquid
managed in the tank must be equipped with a
slotted membrane fabric cover that covers at
least 90 percent of the area of the opening.
vi)
Each unslotted and slotted guide pole well must
be equipped with a
gasketed sliding cover or a
flexible fabric sleeve seal.
vii)
Each unslotted guide pole must be equipped with
a gasketed cap on the end of the pole.
viii)
Each slotted guide pole must be equipped with a
gasketed float or other device which closes off
the liquid surface from the atmosphere.
ix)
Each gauge hatch and each sample well must be
equipped with a gasketed cover.
2)
The owner or operator shall operate the tank in accordance
with the following requirements:
A)
When the floating roof is resting on the leg supports,
the process of filling, emptying, or refilling must be
continuous and must be completed as soon as practical.
B)
Except for automatic bleeder vents, rim space vents,
roof drains, and leg sleeves, each opening in the roof
must be secured and maintained in a closed position at
all times except when the closure device must be open
for access.
C)
Covers on each access hatch and each gauge float well
must be bolted or fastened when secured in the closed
316
position.
D)
Automatic bleeder vents must be set closed at all
times when the roof is floating, except when the roof
is being floated off or is being landed on the leg
supports.
E)
Rim space vents must be set to open only at those
times that the roof is being floated off the roof leg
supports or when the pressure beneath the rim seal
exceeds the manufacturer's recommended setting.
F)
The cap on the end of each
unslotted guide pole must
be secured in the closed position at all times except
when measuring the level or collecting samples of the
liquid in the tank.
G)
The cover on each gauge hatch or sample well must be
secured in the closed position at all times except
when the hatch or well must be opened for access.
H)
Both the primary seal and the secondary seal must
completely cover the annular space between the
external floating roof and the wall of the tank in a
continuous fashion except during inspections.
3)
The owner or operator shall inspect the external floating
roof in accordance with the procedures specified as follows:
A)
The owner or operator shall measure the external
floating roof seal gaps in accordance with the
following requirements:
i)
The owner or operator shall perform measurements
of gaps between the tank wall and the primary
seal within 60 calendar days after initial
operation of the tank following installation of
the floating roof and, thereafter, at least once
every five years.
ii)
The owner or operator shall perform measurements
of gaps between the tank wall and the secondary
seal within 60 calendar days after initial
operation of the tank following installation of
the floating roof and, thereafter, at least once
every year.
iii)
If a tank ceases to hold hazardous waste for a
period of one year or more, subsequent
introduction of hazardous waste into the tank
must be considered an initial operation for the
purposes of subsections (f)(3)(A)(i) and
(f)(3)(A)(ii) above.
iv)
The owner or operator shall determine the total
surface area of gaps in the primary seal and in
the secondary seal individually using the
procedure set forth in subsection (f)(4)(D)
below.
v)
In the event that the seal gap measurements do
317
not conform to the specifications in subsection
(f)(1)(B) below, the owner or operator must
repair the defect in accordance with the
requirements of subsection (k) below.
vi)
The owner or operator shall maintain a record of
the inspection in accordance with the
requirements specified in Section 725.990(b).
B)
The owner or operator shall visually inspect the
external floating roof in accordance with the
following requirements:
i)
The floating roof and its closure devices must
be visually inspected by the owner or operator
to check for defects that could result in air
pollutant emissions. Defects include, but are
not limited to any of the following: holes,
tears, or other openings in the rim seal or seal
fabric of the floating roof; a rim seal detached
from the floating roof; all or a portion of the
floating roof deck being submerged below the
surface of the liquid in the tank; broken,
cracked, or otherwise damaged seals or gaskets
on closure devices; and broken or missing
hatches, access covers, caps, or other closure
devices.
ii)
The owner or operator shall perform an initial
inspection of the external floating roof and its
closure devices on or before the date that the
tank becomes subject to this Section.
Thereafter, the owner or operator shall perform
the inspections at least once every year except
for the special conditions provided for in
subsection (l) below.
iii)
In the event that a defect is detected, the
owner or operator shall repair the defect in
accordance with the requirements of subsection
(k) below.
iv)
The owner or operator shall maintain a record of
the inspection in accordance with the
requirements specified in Section 725.990(b).
C)
Prior to each inspection required by subsection
(f)(3)(A) or (f)(3)(B) above, the owner or operator
shall notify the Agency in advance of each inspection
to provide the Agency with the opportunity to have an
observer present during the inspection. The owner or
operator shall notify the Agency of the date and
location of the inspection as follows:
i)
Prior to each inspection to measure external
floating roof seal gaps as required under
subsection (f)(3)(A) above, written notification
must be prepared and sent by the owner or
operator so that it is received by the Agency at
least 30 calendar days before the date the
measurements are scheduled to be performed.
318
ii)
Prior to each visual inspection of an external
floating roof in a tank that has been emptied
and degassed, written notification must be
prepared and sent by the owner or operator so
that it is received by the Agency at least 30
calendar days before refilling the tank except
when an inspection is not planned, as provided
for in subsection (f)(3)(C)(iii) above.
iii)
When a visual inspection is not planned and the
owner or operator could not have known about the
inspection 30 calendar days before refilling the
tank, the owner or operator shall notify the
Agency as soon as possible, but no later than
seven calendar days before refilling of the
tank. This notification may be made by
telephone and immediately followed by a written
explanation for why the inspection is unplanned.
Alternatively, written notification, including
the explanation for the unplanned inspection,
may be sent so that it is received by the
Regional Administrator at least seven calendar
days before refilling the tank.
D)
Procedure for determining gaps in the primary seal and
in the secondary seal for the purposes of subsection
(f)(3)(A)(iv) above:
i)
The seal gap measurements must be performed at
one or more floating roof levels when the roof
is floating off the roof supports.
ii)
Seal gaps, if any, must be measured around the
entire perimeter of the floating roof in each
place where a 0.32
-cm (_-inch) diameter uniform
probe passes freely (without forcing or binding
against the seal) between the seal and the wall
of the tank and measure the
circumferential
distance of each such location.
iii)
For a seal gap measured under subsection (f)(3)
above, the gap surface area must be determined
by using probes of various widths to measure
accurately the actual distance from the tank
wall to the seal and multiplying each such width
by its respective
circumferential distance.
iv)
The total gap area must be calculated by adding
the gap surface areas determined for each
identified gap location for the primary seal and
the secondary seal individually, and then
dividing the sum for each seal type by the
nominal perimeter of the tank. These total gap
areas for the primary seal and secondary seal
are then are compared to the respective
standards for the seal type, as specified in
subsection (f)(1)(B) above.
BOARD NOTE: Subsections (f)(3)(D)(i) through
(f)(3)(D)(iv) correspond with 40 CFR
319
265.1085(f)(3)(i)(D)(1) through (f)(3)(i)(D)(4),
which the Board has codified here to comport
with Illinois Administrative Code format
requirements.
g)
The owner or operator that controls air pollutant emissions from a
tank by venting the tank to a control device shall meet the
requirements specified in subsections (g)(1) through (g)(3) below.
1)
The tank must be covered by a fixed roof and vented directly
through a closed -vent system to a control device in
accordance with the following requirements:
A)
The fixed roof and its closure devices must be
designed to form a continuous barrier over the entire
surface area of the liquid in the tank.
B)
Each opening in the fixed roof not vented to the
control device must be equipped with a closure device.
If the pressure in the vapor
headspace underneath the
fixed roof is less than atmospheric pressure when the
control device is operating, the closure devices must
be designed to operate such that when the closure
device is secured in the closed position there are no
visible cracks, holes, gaps, or other open spaces in
the closure device or between the perimeter of the
cover opening and the closure device. If the pressure
in the vapor headspace underneath the fixed roof is
equal to or greater than atmospheric pressure when the
control device is operating, the closure device must
be designed to operate with no detectable organic
emissions.
C)
The fixed roof and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and will maintain the integrity of the
fixed roof and closure devices throughout their
intended service life. Factors to be considered when
selecting the materials for and designing the fixed
roof and closure devices must include the following:
organic vapor permeability; the effects of any contact
with the liquid and its vapor managed in the tank; the
effects of outdoor exposure to wind, moisture, and
sunlight; and the operating practices used for the
tank on which the fixed roof is installed.
D)
The closed -vent sys tem and control device must be
designed and operated in accordance with the
requirements of Section 725.988.
2)
Whenever a hazardous waste is in the tank, the fixed roof
must be installed with each closure device secured in the
closed position and the vapor
headspace underneath the fixed
roof vented to the control device except as follows:
A)
Venting to the control device is not required, and
opening of closure devices or removal of the fixed
roof is allowed at the following times:
i)
To provide access to the tank for performing
320
routine inspection, maintenance, or other
activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample
liquid in the tank, or when a worker needs to
open a hatch to maintain or repair equipment.
Following completion of the activity, the owner
or operator shall promptly secure the closure
device in the closed position or reinstall the
cover, as applicable, to the tank.
ii)
To remove accumulated sludge or other residues
from the bottom of a tank.
B)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air
emission control equipment in accordance with the following
procedures:
A)
The fixed roof and its closure devices must be
visually inspected by the owner or operator to check
for defects that could result in air pollutant
emissions. Defects include, but are not limited to
any of the following: visible cracks, holes, or gaps
in the roof sections or between the roof and the tank
wall; broken, cracked, or otherwise damaged seals or
gaskets on closure devices; and broken or missing
hatches, access covers, caps, or other closure
devices.
B)
The closed -vent system and control device must be
inspected and monitored by the owner or operator in
accordance with the procedures specified in Section
725.988.
C)
The owner or operator shall perform an initial
inspection of the air emission control equipment on or
before the date that the tank becomes subject to this
Section. Thereafter, the owner or operator shall
perform the inspections at least once every year
except for the special conditions provided for in
subsection (l) below.
D)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (k) below.
E)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 725.990(b).
h)
The owner or operator that controls air pollutant emissions by
using a pressure tank must meet the following requirements.
1)
The tank shall be designed not to vent to the atmosphere as
a result of compression of the vapor
headspace in the tank
during filling of the tank to its design capacity.
321
2)
All tank openings must be equipped with closure devices
designed to operate with no detectable organic emissions as
determined using the procedure specified in Section
725.984(d).
3)
Whenever a hazardous waste is in the tank, the tank must be
operated as a closed system that does not vent to the
atmosphere except in the event that a safety device, as
defined in Section 725.981, is required to open to avoid an
unsafe condition.
i)
The owner or operator that controls air pollutant emissions by
using an enclosure vented through a closed
-vent system to an
enclosed combustion control device shall meet the requirements
specified in subsections (i)(1) through (i)(4) below.
1)
The tank must be located inside an enclosure. The enclosure
must be designed and operated in accordance with the
criteria for a permanent total enclosure, as specified in
"Procedure T --Criteria for and Verification of a Permanent
or Temporary Total Enclosure" under 40 CFR 52.741, appendix
B, incorporated by reference in 35 Ill. Adm. Code 720.111.
The enclosure may have permanent or temporary openings to
allow worker access; passage of material into or out of the
enclosure by conveyor, vehicles, or other mechanical means;
entry of permanent mechanical or electrical equipment; or
direct airflow into the enclosure. The owner or operator
shall perform the verification procedure for the enclosure
as specified in Section 5.0 to "Procedure T
--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure" initially when the enclosure is first installed
and, thereafter, annually.
2)
The enclosure must be vented through a closed
-vent system to
an enclosed combustion control device that is designed and
operated in accordance with the standards for either a vapor
incinerator, boiler, or process heater specified in Section
725.988.
3)
Safety devices, as defined in Section 725.981, may be
installed and operated as necessary on any enclosure,
closed-vent system, or control device used to comply with
the requirements of subsections (i)(1) and (i)(2) above.
4)
The owner or operator shall inspect and monitor the
closed -vent system and control device, as specified in
Section 725.988.
j)
The owner or operator shall transfer hazardous waste to a tank
subject to this Section in accordance with the following
requirements:
1)
Transfer of hazardous waste, except as provided in
subsection (j)(2) below, to the tank from another tank
subject to this Section or from a surface impoundment
subject to Section 725.986 must be conducted using
continuous hard -piping or another closed system that does
not allow exposure of the hazardous waste to the atmosphere.
For the purpose of complying with this provision, an
individual drain system is considered to be a closed system
when it meets the requirements of 40 CFR 63, subpart RR,
322
"National Emission Standards for Individual Drain Systems",
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (j)(1) above do not apply
when transferring a hazardous waste to the tank under any of
the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the
point of waste origination.
B)
The hazardous waste has been treated by an organic
destruction or removal process to meet the
requirements in Section 725.983(c)(2).
k)
The owner or operator shall repair each defect detected during an
inspection performed in accordance with the requirements of
subsections (c)(4), (e)(3), (f)(3), or (g)(3) above as follows:
1)
The owner or operator shall make first efforts at repair of
the defect no later than five calendar days after detection,
and repair shall be completed as soon as possible but no
later than 45 calendar days after detection except as
provided in subsection (k)(2) below.
2)
Repair of a defect may be delayed beyond 45 calendar days if
the owner or operator determines that repair of the defect
requires emptying or temporary removal from service of the
tank and no alternative tank capacity is available at the
site to accept the hazardous waste normally managed in the
tank. In this case, the owner or operator shall repair the
defect the next time the process or unit that is generating
the hazardous waste managed in the tank stops operation.
Repair of the defect must be completed before the process or
unit resumes operation.
l)
Following the initial inspection and monitoring of the cover as
required by the applicable provisions of this Subpart, subsequent
inspection and monitoring may be performed at intervals longer
than one year under the following special conditions:
1)
Where inspecting or monitoring the cover would expose a
worker to dangerous, hazardous, or other unsafe conditions,
then the owner or operator may designate a cover as an
"unsafe to inspect and monitor cover" and comply with all of
the following requirements:
A)
Prepare a written explanation for the cover stating
the reasons why the cover is unsafe to visually
inspect or to monitor, if required.
B)
Develop and implement a written plan and schedule to
inspect and monitor the cover, using the procedures
specified in the applicable Section of this Subpart,
as frequently as practicable during those times when a
worker can safely access the cover.
2)
In the case when a tank is buried partially or entirely
underground, an owner or operator is required to inspect and
monitor, as required by the applicable provisions of this
Section, only those portions of the tank cover and those
323
connections to the tank (e.g., fill ports, access hatches,
gauge wells, etc.) that are located on or above the ground
surface.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.986
Standards: Surface
Impoundments
a)
The provisions of t
his Section appliesy to owners and operators
ofthe control of air pollutant emissions from
surface impoundments
subject to this Subpart into which any hazardous waste is placed
except for the following surface
impoundments: for which Section
725.983(b) of this Subpart references the use of this Section for
such air emission control.
1) A surface impoundment in which all hazardous waste entering
the surface impoundment meets the conditions specified in
Section 725.983(c); or
2) A surface impoundment used for biological treatment of
hazardous waste in accordance with the requirements of
Section 725.983(c)(2)(iv).
b)
The owner or operator shall
place the hazardous waste into a
surface impoundment equipped with a cover (e.g., an air-supported
structure or a rigid cover) that is vented through a closed-vent
system to a control device meeting the requirements specified in
subsection (d) below. control air pollutant emissions from the
surface impoundment by installing and operating either of the
following:
1)
A floating membrane cover in accordance with the provisions
specified in subsection (c) below; or
2)
A cover that is vented through a closed
-vent system to a
control device in accordance with the provisions specified
in subsection (d) below.
c) As an alternative to complying with subsection (b) above, an owner
or operator may place hazardous waste in a surface impoundment
equipped with a floating membrane cover meeting the requirements
specified in subsection (e) below when the hazardous waste is
determined to meet all of the following conditions:
1) The hazardous waste is neither mixed, stirred, agitated, nor
circulated within the surface impoundment by the owner or
operator using a process that results in splashing,
frothing, or visible turbulent flow on the waste surface
during normal process operations;
2) The hazardous waste in the surface impoundment is not heated
by the owner or operator; and
3) The hazardous waste in the surface impoundment is not
treated by the owner or operator using a waste stabilization
process or a process that produces an exothermic reaction.
d) To comply with subsection (b)(1) above, the owner or operator
shall design, install, operate, and maintain a cover that vents
the organic vapors emitted from hazardous waste in the surface
impoundment through a closed-vent system connected to a control
324
device.
1) The cover must be designed, installed, operated, and
maintained to meet the following requirements:
A) The cover and all cover openings (e.g., access
hatches, sampling ports, and gauge wells) must be
designed to operate with no detectable organic
emissions when all cover openings are secured in a
closed, sealed position.
B) Each cover opening must be secured in the closed,
sealed position (e.g., covered by a
gasketed lid or
cap) at all times that hazardous waste is in the
surface impoundment, except as provided for in
subsection (g) below.
C) The closed-v ent system and control device must be
designed and operated in accordance with Section
725.988.
e) To comply with subsection (c) above, the owner or operator shall
design, install, operate, and maintain a floating membrane cover
that meets all of the following requirements:
1) The floating membrane cover must be designed, installed, and
operated such that at all times when hazardous waste is in
the surface impoundment, the entire surface area of the
hazardous waste is enclosed by the cover, and any air spaces
underneath the cover are not vented to the atmosphere except
during conditions specified in subsection (h) below.
2) The floating membrane cover and all cover openings (e.g.,
access hatches, sampling ports, and gauge wells) must be
designed to operate with no detectable organic emissions
when all cover openings are secured in a closed, sealed
position.
3) Each cover opening must be secured in a closed, sealed
position (e.g., covered by a
gasketed lid or cap) at all
times that hazardous waste is in the surface impoundment
except as provided for in subsections (g)(1) through (g)(3)
below.
4) The synthetic membrane material used for the floating
membrane cover must be either:
A) High density polyethylene with a thickness no less
than 2.5 mm; or
B) A material or a composite of different materials
determined to have the following properties:
i) Organic permeability properties that are
equivalent to those of the material specified in
subsection (e)(4)(A) above; and
ii) Chemical an d physical properties that maintain
the material integrity for as long as the cover
is in use. Factors that must be considered in
selecting the material include: the effects of
325
contact with the waste managed in the
impoundment, weather exposure, and cover
installation and operation practices.
f) The owner or operator shall install, operate, and maintain
enclosed pipes or other closed systems for the transfer of
hazardous waste as described in subsection (f)(1) or (f)(2) below.
BOARD NOTE: U.S. EPA c
onsiders a drain system that meets the
requirements of 40 CFR 61.346(a)(1) or (b)(1) through (b)(3) to be
a "closed-system". The Board intends that this meaning be
included in the use of that term for the purposes of this Subpart.
1) Transfer all hazardous waste to the surface impoundment from
another tank, surface impoundment, or container subject to
this Subpart, except for those hazardous wastes that meet
the conditions specified in Section 725.983(c); and
2) Transfer all hazardous waste from the
surface impoundment to
another tank, surface impoundment, or container subject to
this Subpart, except for those hazardous wastes that meet
the conditions specified in Section 725.983(c).
g) Each cover opening must be secured in the closed, sealed position
(e.g., covered by a
gasketed lid or cap) at all times that
hazardous waste is in the surface impoundment except when it is
necessary to use the cover opening to:
1) Add, remove, inspect, or sample the material in the surface
impoundment;
2) Inspec t, maintain, repair, or replace equipment located
underneath the cover;
3) Remove treatment residues from the surface impoundment in
accordance with the requirements of 35 Ill. Adm. Code
728.104; or
4) Vent gases or vapors from the surface impoundment to a
closed-vent system connected to a control device that is
designed and operated in accordance with the requirements of
Section 725.988.
h) One or more safety devices that vent directly to the atmosphere
may be installed on the cover, closed-vent system, or control
device provided each device meets all of the following conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the surface impoundment or the
closed-vent system connected to a control device; and
2) The safety device remains in a closed, sealed position at
all times except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the cover, closed-vent system, or
control device in accordance with good engineering and
safety practices for handling flammable, combustible,
explosive, or other hazardous materials. An example of an
unplanned event is a sudden power outage.
c)
The owner or operator that controls air pollutant emissions from a
326
surface impoundment using a floating membrane cover must meet the
requirements specified in subsections (c)(1) through (c)(3) below.
1)
The surface impoundment must be equipped with a floating
membrane cover designed to meet the following
specifications:
A)
The floating membrane cover must be designed to float
on the liquid surface during normal operations and
form a continuous barrier over the entire surface area
of the liquid.
B)
The cover must be fabricated from a synthetic membrane
material that is either:
i)
High density polyethylene (HDPE) with a
thickness no less than 2.5 millimeters (mm)
(0.10 inch); or
ii)
A material or a composite of different materials
determined to have both organic permeability
properties that are equivalent to those of the
material listed in subsection (c)(1)(B)(i) above
and chemical and physical properties that
maintain the material integrity for the intended
service life of the material.
C)
The cover must be installed in a manner such that
there are no visible cracks, holes, gaps, or other
open spaces between cover Section seams or between the
interface of the cover edge and its foundation
mountings.
D)
Except as provided for in subsection (c)(1)(E) below,
each opening in the floating membrane cover must be
equipped with a closure device so designed as to
operate when that the closure device is secured in the
closed position there are no visible cracks, holes,
gaps, or other open spaces in the closure device or
between the perimeter of the cover opening and the
closure device.
E)
The floating membrane cover may be equipped with one
or more emergency cover drains for removal of
stormwater. Each emergency cover drain must be
equipped with a slotted membrane fabric cover that
covers at least 90 percent of the area of the opening
or a flexible fabric sleeve seal.
F)
The closure devices must be made of suitable materials
that will minimize exposure of the hazardous waste to
the atmosphere, to the extent practical, and will
maintain the integrity of the closure devices
throughout their intended service life. Factors to be
considered when selecting the materials of
construction and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the
liquid and its vapor managed in the surface
impoundment; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
327
used for the surface impoundment on which the floating
membrane cover is installed.
2)
Whenever a hazardous waste is in the surface impoundment,
the floating membrane cover must float on the liquid and
each closure device must be secured in the closed position
except as follows:
A)
Opening of closure devices or removal of the cover is
allowed at the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or
other activities needed for normal operations.
Examples of such activities include those times
when a worker needs to open a port to sample the
liquid in the surface impoundment, or when a
worker needs to open a hatch to maintain or
repair equipment. Following completion of the
activity, the owner or operator shall promptly
replace the cover and secure the closure device
in the closed position, as applicable.
ii)
To remove accumulated sludge or other residues
from the bottom of surface impoundment.
B)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
3)
The owner or operator shall inspect the floating membrane
cover in accordance with the following procedures:
A)
The floating membrane cover and its closure devices
must be visually inspected by the owner or operator to
check for defects that could result in air pollutant
emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the cover Section
seams or between the interface of the cover edge and
its foundation mountings; broken, cracked, or
otherwise damaged seals or gaskets on closure devices;
and broken or missing hatches, access covers, caps, or
other closure devices.
B)
The owner or operator shall perform an initial
inspection of the floating membrane cover and its
closure devices on or before the date that the surface
impoundment becomes subject to this Section.
Thereafter, the owner or operator shall perform the
inspections at least once every year except for the
special conditions provided for in subsection (g)
below.
C)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (f) below.
D)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 725.990(c).
328
d)
The owner or operator that controls air pollutant emissions from a
surface impoundment using a cover vented to a control device shall
meet the requirements specified in subsections (d)(1) through
(d)(3) below.
1)
The surface impoundment must be covered by a cover and
vented directly through a closed
-vent system to a control
device in accordance with the following requirements:
A)
The cover and its closure devices must be designed to
form a continuous barrier over the entire surface area
of the liquid in the surface impoundment.
B)
Each opening in the cover not vented to the control
device must be equipped with a closure device. If the
pressure in the vapor
headspace underneath the cover
is less than atmospheric pressure when the control
device is operating, the closure devices must be
designed to operate such that when the closure device
is secured in the closed position there are no visible
cracks, holes, gaps, or other open spaces in the
closure device or between the perimeter of the cover
opening and the closure device. If the pressure in
the vapor headspace underneath the cover is equal to
or greater than atmospheric pressure when the control
device is operating, the closure device must be
designed to operate with no detectable organic
emissions using the procedure specified in Section
725.984(d).
C)
The cover and its closure devices must be made of
suitable materials that will minimize exposure of the
hazardous waste to the atmosphere, to the extent
practical, and will maintain the integrity of the
cover and closure devices throughout their intended
service life. Factors to be considered when selecting
the materials for and designing the cover and closure
devices must include the following: the organic vapor
permeability; the effects of any contact with the
liquid or its vapors managed in the surface
impoundment; the effects of outdoor exposure to wind,
moisture, and sunlight; and the operating practices
used for the surface impoundment on which the cover is
installed.
D)
The closed -vent system and control device must be
designed and operated in accordance with the
requirements of Section 725.988.
2)
Whenever a hazardous waste is in the surface impoundment,
the cover must be installed with each closure device secured
in the closed position and the vapor
headspace underneath
the cover vented to the control device except as follows:
A)
Venting to the control device is not required, and
opening of closure devices or removal of the cover is
allowed at the following times:
i)
To provide access to the surface impoundment for
performing routine inspection, maintenance, or
other activities needed for normal operations.
329
Examples of such activities include those times
when a worker needs to open a port to sample
liquid in the surface impoundment, or when a
worker needs to open a hatch to maintain or
repair equipment. Following completion of the
activity, the owner or operator shall promptly
secure the closure device in the closed position
or reinstall the cover, as applicable, to the
surface impoundment.
ii)
To remove accumulated sludge or other residues
from the bottom of surface impoundment.
B)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
3)
The owner or operator shall inspect and monitor the air
emission control equipment in accordance with the following
procedures:
A)
The surface impoundment cover and its closure devices
must be visually inspected by the owner or operator to
check for defects that could result in air pollutant
emissions. Defects include, but are not limited to,
visible cracks, holes, or gaps in the cover Section
seams or between the interface of the cover edge and
its foundation mountings; broken, cracked, or
otherwise damaged seals or gaskets on closure devices;
and broken or missing hatches, access covers, caps, or
other closure devices.
B)
The closed -vent system and control device must be
inspected and monitored by the owner or operator in
accordance with the procedures specified in Section
725.988.
C)
The owner or operator shall perform an initial
inspection of the air emission control equipment on or
before the date that the surface impoundment becomes
subject to this Section. Thereafter, the owner or
operator shall perform the inspections at least once
every year except for the special conditions provided
for in subsection (g) below.
D)
In the event that a defect is detected, the owner or
operator shall repair the defect in accordance with
the requirements of subsection (f) below.
E)
The owner or operator shall maintain a record of the
inspection in accordance with the requirements
specified in Section 725.990(c).
e)
The owner or operator shall transfer hazardous waste to a surface
impoundment subject to this Section in accordance with the
following requirements:
1)
Transfer of hazardous waste, except as provided in
subsection (e)(2) below, to the surface impoundment from
another surface impoundment subject to this Section or from
a tank subject to Section 725.985 must be conducted using
330
continuous hard-piping or another closed system that does
not allow exposure of the waste to the atmosphere. For the
purpose of complying with this provision, an individual
drain system is considered to be a closed system when it
meets the requirements of 40 CFR 63, subpart RR, "National
Emission Standards for Individual Drain Systems",
incorporated by reference in 35 Ill. Adm. Code 720.111.
2)
The requirements of subsection (e)(1) above do not apply
when transferring a hazardous waste to the surface
impoundment under either of the following conditions:
A)
The hazardous waste meets the average VO concentration
conditions specified in Section 725.983(c)(1) at the
point of waste origination.
B)
The hazardous waste has been treated by an organic
destruction or removal process to meet the
requirements in Section 725.983(c)(2).
f)
The owner or operator shall repair each defect detected during an
inspection performed in accordance with the requirements of
subsection (c)(3) or (d)(3) above as follows:
1)
The owner or operator shall make first efforts at repair of
the defect no later than five calendar days after detection,
and repair must be completed as soon as possible but no
later than 45 calendar days after detection except as
provided in subsection (f)(2) below.
2)
Repair of a defect may be delayed beyond 45 calendar days if
the owner or operator determines that repair of the defect
requires emptying or temporary removal from service of the
surface impoundment and no alternative capacity is available
at the site to accept the hazardous waste normally managed
in the surface impoundment. In this case, the owner or
operator shall repair the defect the next time the process
or unit that is generating the hazardous waste managed in
the tank stops operation. Repair of the defect must be
completed before the process or unit resumes operation.
g)
Following the initial inspection and monitoring of the cover as
required by the applicable provisions of this Subpart, subsequent
inspection and monitoring may be performed at intervals longer
than one year in the case when inspecting or monitoring the cover
would expose a worker to dangerous, hazardous, or other unsafe
conditions. In this case, the owner or operator may designate the
cover as an "unsafe to inspect and monitor cover" and comply with
all of the following requirements:
1)
Prepare a written explanation for the cover stating the
reasons why the cover is unsafe to visually inspect or to
monitor, if required.
2)
Develop and implement a written plan and schedule to inspect
and monitor the cover using the procedures specified in the
applicable Section of this Subpart as frequently as
practicable during those times when a worker can safely
access the cover.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
331
Section 725.987
Standards: Containers
a)
The provisions of t
his Section appliesy to the owners and
operators ofcontrol of air pollutant emissions from
containers
having design capacities greater than 0.1 m
3
(3.5 ft
3
or 26.4 gal)
subject to this Subpart into which any hazardous waste is placed,
except for a container in which all hazardous waste entering the
container meets the conditions specified in Section 725.983(c).
for
which Section 725.983(b) references the use of this Section for
such air emission control.
b) An owner or operator shall manage hazardous waste in containers
using the following procedures:
1) The owner or operator shall place the hazardous waste into
one of the following containers, except when a container is
used for hazardous waste treatment as required by subsection
(b)(2) below:
A) A container that is equipped with a cover that
operates with no detectable organic emissions when all
container openings (e.g., lids, bungs, hatches, and
sampling ports) are secured in a closed, sealed
position. The owner or operator shall determine that
a container operates with no detectable emissions by
testing each opening on the container for leaks in
accordance with Method 21 in 40 CFR 60, Appendix A,
incorporated by reference in 35 Ill. Adm. Code
720.111, the first time any portion of the hazardous
waste is placed into the container. If a leak is
detected and cannot be repaired immediately, the
hazardous waste must be removed from the container and
the container not used to meet the requirements of
this subsection until the leak is repaired and the
container is retested.
B) A container having a desig
n capacity less than or
equal to 0.46 m
3
(16.2 ft
3
or 121.5 gal) that is
equipped with a cover and complies with all applicable
U.S. Department of Transportation regulations on
packaging hazardous waste for transport under 49 CFR
178, incorporated by reference in 35 Ill. Adm. Code
720.111.
i) A container that is managed in accordance with
the requirements of 49 CFR 178 for the purpose
of complying with this Subpart is not subject to
any exceptions to the 49 CFR 178 regulations,
except as noted in subsection (b)(1)(B)(ii)
above.
ii) A lab pack that is managed in accordance with
the requirements of 49 CFR 178 for the purpose
of complying with this Subpart may comply with
the exceptions for combination
packagings
specified in 49 CFR 173.12(b).
C) A container that is attached to or forms a part of any
truck, trailer, or
railcar and that has been
demonstrated within the preceding 12 months to be
332
organic vapor tight when all container openings are in
a closed, sealed position (e.g., the container hatches
or lids are gasketed and latched). For the purpose of
meeting the requirements of this subsection, a
container is organic vapor tight if the container
sustains a pressure change of not more than 0.75
kPa
(0.11 psig or 5.6 mm Hg) within 5 minutes after it is
pressurized to a minimum of 4.5
kPa (0.65 psig or 33.7
mm Hg). This condition is to be demonstrated using
the pressure test specified in Method 27 of 40 CFR 60,
Appendix A, incorporated by reference in 35 Ill. Adm.
Code 720.111, and a pressure measurement device that
has a precision of ยฑ 2.5 mm water and that is capable
of measuring above the pressure at which the container
is to be tested for vapor tightness.
2) An owner or operator treating hazardous waste in a container
by either a waste stabilization process, any process that
requires the addition of heat to the waste, or any process
that produces an exothermic reaction must meet the following
requirements:
A) Whenever it is necessary for the container to be open
during the treatment process, the container must be
located inside an enclosure that is vented through a
closed-vent system to a control device.
B) The enclosure must be a structure that is designed and
operated in accordance with the following
requirements:
i) The enclosure must be a structure that is
designed and operated with sufficient airflow
into the structure to capture the organic vapors
emitted from the hazardous waste in the
container and vent the vapors through the
closed-vent system to the control device.
ii) The enclosure may have permanent or temporary
openings to allow worker access, passage of
containers through the enclosure by conveyor or
other mechanical means, entry of permanent
mechanical or electrical equipment, or to direct
airflow into the enclosure. The pressure drop
across each opening in the enclosure must be
maintained at a pressure below atmospheric
pressure such that whenever an open container is
placed inside the enclosure no organic vapors
released from the container exit the enclosure
through the opening. The owner or operator
shall determine that an enclosure achieves this
condition by measuring the pressure drop across
each opening in the enclosure. If the pressure
within the enclosure is equal to or greater than
atmospheric pressure then the enclosure does not
meet the requirements of this Section.
C) The closed-vent system and control device must be
designed and operated in accordance with the
requirements of Section 725.988.
333
3) An owner or operator transferring hazardous wast
e into a
container having a design capacity greater than 0.46 m
3
(16.2 ft
3
or 121.5 gal) shall meet the following
requirements:
A) Hazardous waste transfer by pumping must be performed
using a conveyance system that uses a tube (e.g.,
pipe, hose) to add the waste into the container.
During transfer of the waste into the container, the
cover must remain in place and all container openings
must be maintained in a closed, sealed position except
for those openings through which the tube enters the
container and as provided for in subsection (c) below.
The tube must be positioned in a manner such that
either the:
i) Tube outlet continuously remains submerged below
the waste surface at all times waste is flowing
through the tube;
ii) Lower bottom edge of the tube outlet is located
at a distance no greater than two inside
diameters of the tube or 15.25 cm (0.50 ft or
6.0 in), whichever distance is greater, from the
bottom of the container at all times waste is
flowing through the tube; or
iii) Tube is connected to a permanent port mounted on
the bottom of the container so that the lower
edge of the port opening inside the container is
located at a distance equal to or less than
15.25 cm (0.50 ft or 6.0 in) from the container
bottom.
B) Hazardous waste transferred by a means other than
pumping must be performed such that during transfer of
the waste into the container, the cover remains in
place and all container openings are maintained in a
closed, sealed position except for those openings
through which the hazardous waste is added and as
provided for in subsection (d) below.
c) Each container opening must be maintained in a closed, sealed
position (e.g., covered by a
gasketed lid) at all times that
hazardous waste is in the container except when it is necessary to
use the opening to:
1) Add, remove, inspect, or sample the material in the
container;
2) Inspect, maintain, repair, or replace equipment located
inside the container; or
3) Vent gases or vapors from a cover located over or
enclosing
an open container to a closed-vent system connected to a
control device that is designed and operated in accordance
with the requirements of Section 725.988.
d) One or more safety devices that vent directly to the atmosphere
may be used on the container, cover, enclosure, closed-vent
system, or control device provided each device meets all of the
334
following conditions:
1) The safety device is not used for planned or routine venting
of organic vapors from the container, cover, enclosure, or
closed-vent system connected to a control device; and
2) The safety device remains in a closed, sealed position at
all times except when an unplanned event requires that the
device open for the purpose of preventing physical damage or
permanent deformation of the container, cover, enclosure,
closed-vent system, or control device in accordance with
good engineering and safety practices for handling
flammable, combustible, explosive, or other hazardous
materials. An example of an unplanned event is a sudden
power outage.
b)
General requirements.
1)
The owner or operator shall control air pollutant emissions
from each container subject to this Section in accordance
with the following requirements, as applicable to the
container, except when the special provisions for waste
stabilization processes specified in subsection (b)(2) below
apply to the container.
A)
For a container having a design capacity greater than
0.1 m
3
(26 gal) and less than or equal to 0.46 m
3
(120
gal), the owner or operator shall control air
pollutant emissions from the container in accordance
with the Container Level 1 standards specified in
subsection (c) below.
B)
For a container having a design capacity greater than
0.46 m
3
(120 gal) that is not in light material
service, the owner or operator shall control air
pollutant emissions from the container in accordance
with the Container Level 1 standards specified in
subsection (c) below.
C)
For a container having a design capacity greater than
0.46 m
3
(120 gal) that is in light material service,
the owner or operator shall control air pollutant
emissions from the container in accordance with the
Container Level 2 standards specified in subsection
(d) below.
2)
When a container having a design capacity greater than 0.1
m
3
(26 gal) is used for treatment of a hazardous waste by a
waste stabilization process, the owner or operator shall
control air pollutant emissions from the container in
accordance with the Container Level 3 standards specified in
subsection (e) below at those times during the waste
stabilization process when the hazardous waste in the
container is exposed to the atmosphere.
c)
Container Level 1 standards.
1)
A container using Container Level 1 controls is one of the
following:
A)
A container that meets the applicable U.S. Department
335
of Transportation (DOT) regulations on packaging
hazardous materials for transportation, as specified
in subsection (f) below.
B)
A container equipped with a cover and closure devices
that form a continuous barrier over the container
openings so that when the cover and closure devices
are secured in the closed position there are no
visible holes, gaps, or other open spaces into the
interior of the container. The cover may be a
separate cover installed on the container (e.g., a lid
on a drum or a suitably secured tarp on a roll
-off
box) or may be an integral part of the container
structural design (e.g., a "portable tank" or bulk
cargo container equipped with a screw
-type cap).
C)
An open-top container in which an organic
-vapor
suppressing barrier is placed on or over the hazardous
waste in the container such that no hazardous waste is
exposed to the atmosphere. One example of such a
barrier is application of a suitable organic-vapor
suppressing foam.
2)
A container used to meet the requirements of subsection
(c)(1)(B) or (c)(1)(C) above must be equipped with covers
and closure devices, as applicable to the container, that
are composed of suitable materials to minimize exposure of
the hazardous waste to the atmosphere and to maintain the
equipment integrity for as long as it is in service.
Factors to be considered in selecting the materials of
construction and designing the cover and closure devices
must include the following: the organic vapor permeability,
the effects of contact with the hazardous waste or its vapor
managed in the container; the effects of outdoor exposure of
the closure device or cover material to wind, moisture, and
sunlight; and the operating practices for which the
container is intended to be used.
3)
Whenever a hazardous waste is in a container using Container
Level 1 controls, the owner or operator shall install all
covers and closure devices for the container, as applicable
to the container, and secure and maintain each closure
device in the closed position except as follows:
A)
Opening of a closure device or cover is allowed for
the purpose of adding hazardous waste or other
material to the container as follows:
i)
In the case when the container is filled to the
intended final level in one continuous
operation, the owner or operator shall promptly
secure the closure devices in the closed
position and install the covers, as applicable
to the container, upon conclusion of the filling
operation.
ii)
In the case when discrete quantities or batches
of material intermittently are added to the
container over a period of time, the owner or
operator shall promptly secure the closure
devices in the closed position and install
336
covers, as applicable to the container, upon
either the container being filled to the
intended final level; the completion of a batch
loading after which no additional material will
be added to the container within 15 minutes; the
person performing the loading operation leaving
the immediate vicinity of the container; or the
shutdown of the process generating the material
being added to the container, whichever
condition occurs first.
B)
Opening of a closure device or cover is allowed for
the purpose of removing hazardous waste from the
container as follows:
i)
For the purpose of meeting the requirements of
this Section, an empty container, as defined in
35 Ill. Adm. Code 721.107(b), may be open to the
atmosphere at any time (i.e., covers and closure
devices are not required to be secured in the
closed position on an empty container).
ii)
In the case when discrete quantities or batches
of material are removed from the container but
the container does not meet the conditions to be
an empty container, as defined in 35 Ill. Adm.
Code 721.107(b), the owner or operator shall
promptly secure the closure devices in the
closed position and install covers, as
applicable to the container, upon the completion
of a batch removal after which no additional
material will be removed from the container
within 15 minutes or the person performing the
unloading operation leaves the immediate
vicinity of the container, whichever condition
occurs first.
C)
Opening of a closure device or cover is allowed when
access inside the container is needed to perform
routine activities other than transfer of hazardous
waste. Examples of such activities include those
times when a worker needs to open a port to measure
the depth of or sample the material in the container,
or when a worker needs to open a manhole hatch to
access equipment inside the container. Following
completion of the activity, the owner or operator
shall promptly secure the closure device in the closed
position or reinstall the cover, as applicable to the
container.
D)
Opening of a spring
-loaded, pressure
-vacuum rel ief
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the container internal pressure in
accordance with the design specifications of the
container. The device must be designed to operate
with no detectable organic emissions when the device
is secured in the closed position. The settings at
which the device opens must be established such that
the device remains in the closed position whenever the
337
internal pressure of the container is within the
internal pressure operating range determined by the
owner or operator based on container manufacturer
recommendations, applicable regulations, fire
protection and prevention codes, standard engineering
codes and practices, or other requirements for the
safe handling of flammable, ignitable, explosive,
reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to
open are during those times when the internal pressure
of the container exceeds the internal pressure
operating range for the container as a result of
loading operations or diurnal ambient temperature
fluctuations.
E)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 1
controls must inspect the containers and their covers and
closure devices as follows:
A)
In the case when a hazardous waste already is in the
container at the time the owner or operator first
accepts possession of the container at the facility
and the container is not emptied (i.e., does not meet
the conditions for an empty container as specified in
35 Ill. Adm. Code 721.107(b)) within 24 hours after
the container is accepted at the facility, the owner
or operator shall visually inspect the container and
its cover and closure devices to check for visible
cracks, holes, gaps, or other open spaces into the
interior of the container when the cover and closure
devices are secured in the closed position. If a
defect is detected, the owner or operator shall repair
the defect in accordance with the requirements of
subsection (c)(4)(C) below.
B)
In the case when a container used for managing
hazardous waste remains at the facility for a period
of one year or more, the owner or operator shall
visually inspect the container and its cover and
closure devices initially and thereafter, at least
once every 12 months, to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (c)(4)(C) below.
C)
When a defect is detected for the container, cover, or
closure devices, the owner or operator shall make
first efforts at repair of the defect no later than 24
hours after detection, and repair must be completed as
soon as possible but no later than five calendar days
after detection. If repair of a defect cannot be
completed within five calendar days, then the
hazardous waste must be removed from the container and
the container must not be used to manage hazardous
338
waste until the defect is repaired.
5)
The owner or operator shall maintain at the facility a copy
of the procedure used to determine that containers with
capacity of 0.46 m
3
(120 gal) or greater, which do not meet
applicable USDOT regulations as specified in subsection (f)
below, are not managing hazardous waste in light material
service.
d)
Container Level 2 standards.
1)
A container using Container Level 2 controls is one of the
following:
A)
A container that meets the applicable U.S. Department
of Transportation (USDOT) regulations on packaging
hazardous materials for transportation as specified in
subsection (f) below.
B)
A container that operates with no detectable organic
emissions, as defined in Section 725.981, and
determined in accordance with the procedure specified
in subsection (g) below.
C)
A container that has been demonstrated within the
preceding 12 months to be vapor
-tight by using 40 CFR
60, appendix A, Method 27, incorporated by reference
in 35 Ill. Adm. Code 720.111, in accordance with the
procedure specified in subsection (h) below.
2)
Transfer of hazardous waste in or out of a container using
Container Level 2 controls must be conducted in such a
manner as to minimize exposure of the hazardous waste to the
atmosphere, to the extent practical, considering the
physical properties of the hazardous waste and good
engineering and safety practices for handling flammable,
ignitable, explosive, reactive or other hazardous materials.
Examples of container loading procedures that the EPA
considers to meet the requirements of this subsection
include using any one of the following: a submerged
-fill
pipe or other submerged
-fill method to load liquids into the
container; a vapor
-balancing system or a vapor
-recovery
system to collect and control the vapors displaced from the
container during filling operations; or a fitted opening in
the top of a container through which the hazardous waste is
filled and subsequently purging the transfer line before
removing it from the container opening.
3)
Whenever a hazardous waste is in a container using Container
Level 2 controls, the owner or operator shall install all
covers and closure devices for the container, and secure and
maintain each closure device in the closed position except
as follows:
A)
Opening of a closure device or cover is allowed for
the purpose of adding hazardous waste or other
material to the container as follows:
i)
In the case when the container is filled to the
intended final level in one continuous
operation, the owner or operator shall promptly
339
secure the closure devices in the closed
position and install the covers, as applicable
to the container, upon conclusion of the filling
operation.
ii)
In the case when discrete quantities or batches
of material intermittently are added to the
container over a period of time, the owner or
operator shall promptly secure the closure
devices in the closed position and install
covers, as applicable to the container, upon
either the container being filled to the
intended final level; the completion of a batch
loading after which no additional material will
be added to the container within 15 minutes; the
person performing the loading operation leaving
the immediate vicinity of the container; or the
shutdown of the process generating the material
being added to the container, whichever
condition occurs first.
B)
Opening of a closure device or cover is allowed for
the purpose of removing hazardous waste from the
container as follows:
i)
For the purpose of meeting the requirements of
this Section, an empty container as defined in
35 Ill. Adm. Code 721.107(b) may be open to the
atmosphere at any time (i.e., covers and closure
devices are not required to be secured in the
closed position on an empty container).
ii)
In the case when discrete quantities or batches
of material are removed from the container but
the container does not meet the conditions to be
an empty container as defined in 35 Ill. Adm.
Code 721.107(b), the owner or operator shall
promptly secure the closure devices in the
closed position and install covers, as
applicable to the container, upon the completion
of a batch removal after which no additional
material will be removed from the container
within 15 minutes or the person performing the
unloading operation leaves the immediate
vicinity of the container, whichever condition
occurs first.
C)
Opening of a closure device or cover is allowed when
access inside the container is needed to perform
routine activities other than transfer of hazardous
waste. Examples of such activities include those
times when a worker needs to open a port to measure
the depth of or sample the material in the container,
or when a worker needs to open a manhole hatch to
access equipment inside the container. Following
completion of the activity, the owner or operator
shall promptly secure the closure device in the closed
position or reinstall the cover, as applicable to the
container.
D)
Opening of a spring
-loaded, pressure
-vacuum relief
340
valve, conservation vent, or similar type of pressure
relief device which vents to the atmosphere is allowed
during normal operations for the purpose of
maintaining the internal pressure of the container in
accordance with the container design specifications.
The device must be designed to operate with no
detectable organic emission when the device is secured
in the closed position. The settings at which the
device opens must be established such that the device
remains in the closed position whenever the internal
pressure of the container is within the internal
pressure operating range determined by the owner or
operator based on container manufacturer
recommendations, applicable regulations, fire
protection and prevention codes, standard engineering
codes and practices, or other requirements for the
safe handling of flammable, ignitable, explosive,
reactive, or hazardous materials. Examples of normal
operating conditions that may require these devices to
open are during those times when the internal pressure
of the container exceeds the internal pressure
operating range for the container as a result of
loading operations or diurnal ambient temperature
fluctuations.
E)
Opening of a safety device, as defined in Section
725.981, is allowed at any time conditions require
doing so to avoid an unsafe condition.
4)
The owner or operator of containers using Container Level 2
controls shall inspect the containers and their covers and
closure devices as follows:
A)
In the case when a hazardous waste already is in the
container at the time the owner or operator first
accepts possession of the container at the facility
and the container is not emptied (i.e., does not meet
the conditions for an empty container as specified in
35 Ill. Adm. Code 721.107(b)) within 24 hours after
the container arrives at the facility, the owner or
operator shall visually inspect the container and its
cover and closure devices to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (d)(4)(C) below.
B)
In the case when a container used for managing
hazardous waste remains at the facility for a period
of one year or more, the owner or operator shall
visually inspect the container and its cover and
closure devices initially and thereafter, at least
once every 12 months, to check for visible cracks,
holes, gaps, or other open spaces into the interior of
the container when the cover and closure devices are
secured in the closed position. If a defect is
detected, the owner or operator shall repair the
defect in accordance with the requirements of
subsection (d)(4)(C) below.
341
C)
When a defect is detected for the container, cover, or
closure devices, the owner or operator shall make
first efforts at repair of the defect no later than 24
hours after detection, and repair must be completed as
soon as possible but no later than five calendar days
after detection. If repair of a defect cannot be
completed within five calendar days, then the
hazardous waste must be removed from the container and
the container must not be used to manage hazardous
waste until the defect is repaired.
e)
Container Level 3 standards.
1)
A container using Container Level 3 controls is one of the
following:
A)
A container that is vented directly through a
closed -vent system to a control device in accordance
with the requirements of subsection (e)(2)(B) below.
B)
A container that is vented inside an enclosure which
is exhausted through a closed
-vent system to a control
device in accordance with the requirements of
subsections (e)(2)(A) and (e)(2)(B) below.
2)
The owner or operator shall meet the following requirements,
as applicable to the type of air emission control equipment
selected by the owner or operator:
A)
The container enclosure must be designed and operated
in accordance with the criteria for a permanent total
enclosure as specified in "Procedure T
--Criteria for
and Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111. The enclosure may have permanent or
temporary openings to allow worker access; passage of
containers through the enclosure by conveyor or other
mechanical means; entry of permanent mechanical or
electrical equipment; or direct airflow into the
enclosure. The owner or operator shall perform the
verification procedure for the enclosure as specified
in Section 5.0 to "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" initially when the enclosure is first
installed and, thereafter, annually.
B)
The closed -vent system and control device must be
designed and operated in accordance with the
requirements of Section 725.988.
3)
Safety devices, as defined in Section 725.981, may be
installed and operated as necessary on any container,
enclosure, closed
-vent system, or control device used to
comply with the requirements of subsection (e)(1) above.
4)
Owners and operators using Container Level 3 controls in
accordance with the provisions of this Subpart shall inspect
and monitor the closed
-vent systems and control devices, as
specified in Section 725.988.
342
5)
Owners and operators that use Container Level 3 controls in
accordance with the provisions of this Subpart shall prepare
and maintain the records specified in Section 725.990(d).
f)
For the purpose of compliance with subsection (c)(1)(A) or
(d)(1)(A) above, containers must be used that meet the applicable
U.S. Department of Transportation (USDOT) regulations on packaging
hazardous materials for transportation as follows:
1)
The container meets the applicable requirements specified in
49 CFR 178, "Specifications for Packaging", or 49 CFR 179,
"Specifications for Tank Cars", both incorporated by
reference in 35 Ill. Adm. Code 720.111.
2)
Hazardous waste is managed in the container in accordance
with the applicable requirements specified in 49 CFR 107,
subpart B, "Exemptions"; 49 CFR 172, "Hazardous Materials
Table, Special Provisions, Hazardous Materials
Communications, Emergency Response Information, and Training
Requirements"; 49 CFR 173, "
Shippers --General Requirements
for Shipments and Packages"; and 49 CFR 180, "Continuing
Qualification and Maintenance of
Packagings", each
incorporated by reference in 35 Ill. Adm. Code 720.111.
3)
For the purpose of complying with this Subpart, no
exceptions to the 49 CFR 178 or 179 regulations are allowed,
except as provided for in subsection (f)(4) below.
4)
For a lab pack that is managed in accordance with the
requirements of 49 CFR 178 for the purpose of complying with
this Subpart, an owner or operator may comply with the
exceptions for combination
packagings specified in 49 CFR
173.12(b), incorporated by reference in 35 Ill. Adm. Code
720.111.
g)
The owner or operator shall use the procedure specified in Section
725.984(d) for determining a container operates with no detectable
organic emissions for the purpose of complying with subsection
(d)(1)(ii) of this Section.
1)
Each potential leak interface (i.e., a location where
organic vapor leakage could occur) on the container, its
cover, and associated closure devices, as applicable to the
container, must be checked. Potential leak interfaces that
are associated with containers include, but are not limited
to: the interface of the cover rim and the container wall;
the periphery of any opening on the container or container
cover and its associated closure device; and the sealing
seat interface on a spring
-loaded pressure -relief valve.
2)
The test must be performed when the container is filled with
a material having a volatile organic concentration
representative of the range of volatile organic
concentrations for the hazardous wastes expected to be
managed in this type of container. During the test, the
container cover and closure devices must be secured in the
closed position.
h)
Procedure for determining a container to be vapor
-tight using
Method 27 of 40 CFR 60, appendix A for the purpose of complying
343
with subsection (d)(1)(C) above.
1)
The test must be performed in accordance with Method 27 of
40 CFR 60, appendix A, incorporated by reference in 35 Ill.
Adm. Code 720.111.
2)
A pressure measurement device must be used that has a
precision of ยฑ2.5 mm (0.10 inch) water and that is capable
of measuring above the pressure at which the container is to
be tested for vapor tightness.
3)
If the test results determined by Method 27 indicate that
the container sustains a pressure change less than or equal
to 750 Pascals (0.11 psig) within five minutes after it is
pressurized to a minimum of 4,500
Pascals (0.65 psig), then
the container is determined to be vapor
-tight.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.988
Standards: Closed-vent Systems and Control Devices
a)
This Section applies to each closed-vent system and control device
installed and operated by the owner or operator to control air
emissions in accordance with standards of this Subpart.
b)
The closed-vent system must meet the following requirements:
1)
The closed-vent system must route the gases, vapors, and
fumes emitted from the hazardous waste in the waste
management unit to a control device that meets the
requirements specified in subsection (c) below.
2)
The closed-vent system must be designed and operated in
accordance with the requirements specified in Section
725.933(j).
3) IfWhen the closed-vent system
contains one or moreincludes
bypass devices that could be used to divert
all or a portion
of the gas es, or vapors, or fumes from entering the control
device, the owner or operator shall meet the following
requirements: stream to the atmosphere before entering the
control device, each bypass device must be equipped with
either a flow indicator as specified in subsection (b)(3)(A)
below or a seal or locking device as specified in subsection
(b)(3)(B) below. For the purpose of complying with this
subsection, low leg drains, high point bleeds, analyzer
vents, open -ended valves or lines, spring
-loaded pressure
relief valves, and other fittings used for safety purposes
are not considered to be bypass devices.
A) For each bypass device except as provided for in
subsection (b)(3)(B) below, the owner or operator
shall either:
i) Install, calibrate, maintain, and operate a flow
indicator at the inlet to the bypass device that
indicates at least once every 15 minutes whether
gas, vapor, or fume flow is present in the
bypass device; or
ii) Secure the valve installed at the inlet to the
344
bypass device in the closed position using a
car-seal or a lock-and-key type configuration.
The owner or operator shall visually inspect the
seal or closure mechanism at least once every
month to verify that the valve is maintained in
the closed position.
B) Low leg drains, high point bleeds, analyzer vents,
open-ended valves or lines, and safety devices are not
subject to the requirements of subsection (b)(3)(A)
above.
A)
If a flow indicator is used to comply with subsection
(b)(3) below, the indicator must be installed at the
inlet to the bypass line used to divert gases and
vapors from the closed
-vent system to the atmosphere
at a point upstream of the control device inlet. For
the purposes of this subsection, a flow indicator
means a device which indicates the presence of either
gas or vapor flow in the bypass line.
B)
If a seal or locking device is used to comply with
subsection (b)(3) below, the device must be placed on
the mechanism by which the bypass device position is
controlled (e.g., valve handle or damper lever) when
the bypass device is in the closed position such that
the bypass device cannot be opened without breaking
the seal or removing the lock. Examples of such
devices include, but are not limited to, a car
-seal or
a lock -and-key configuration valve. The owner or
operator shall visually inspect the seal or closure
mechanism at least once every month to verify that the
bypass mechanism is maintained in the closed position.
4)
The closed -vent system must be inspected and monitored by
the owner or operator in accordance with the procedure
specified in Section 725.933(k).
c)
The control device must meet the following requirements:
1)
The control device
must be one of the following devices:
A)
A control device designed and operated to reduce the
total organic content of the inlet vapor stream vented
to the control device by at least 95 percent by
weight;
B)
An enclosed combustion device designed and operated in
accordance with the requirements of Section
725.933(c); or
C)
A flare designed and operated in accordance with the
requirements of Section 725.933(d).
2) The control device must be operating at all times when
gases, vapors, or fumes are vented from the waste management
unit through the closed-vent system to the control device.
2)
The owner or operator that elects to use a closed
-vent
system and control device to comply with the requirements of
this Section shall comply with the requirements specified in
345
subsections (c)(2)(A) through (c)(2)(G) below.
A)
Periods of planned routine maintenance of the control
device, during which the control device does not meet
the specifications of subsections (c)(1)(A),
(c)(1)(B), or (c)(1)(C) above, as applicable, must not
exceed 240 hours per year.
B)
The specifications and requirements in subsections
(c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
devices do not apply during periods of planned routine
maintenance.
C)
The specifications and requirements in subsections
(c)(1)(A), (c)(1)(B), and (c)(1)(C) above for control
devices do not apply during a control device system
malfunction.
D)
The owner or operator shall demonstrate compliance
with the requirements of subsection (c)(2)(A) above
(i.e., planned routine maintenance of a control
device, during which the control device does not meet
the specifications of subsections (c)(1)(i),
(c)(1)(B), or (c)(1)(C) above, as applicable, must not
exceed 240 hours per year) by recording the
information specified in Section 725.990(e)(1)(E).
E)
The owner or operator shall correct control device
system malfunctions as soon as practicable after their
occurrence in order to minimize excess emissions of
air pollutants.
F)
The owner or operator shall operate the closed
-vent
system so that gases, vapors, or fumes are not
actively vented to the control device during periods
of planned maintenance or control device system
malfunction (i.e., periods when the control device is
not operating or not operating normally), except in
cases when it is necessary to vent the gases, vapors,
or fumes to avoid an unsafe condition or to implement
malfunction corrective actions or planned maintenance
actions.
3)
The owner or operator using a carbon adsorptio
n system to
comply with subsection (c)(1) above shall operate and
maintain the control device in accordance with the following
requirements:
A)
Following the initial startup of the control device,
all activated carbon in the control device must be
replaced with fresh carbon on a regular basis in
accordance with the requirements of Section 725.933(g)
or 725.933(h).
B)
All carbon removed from the control device must be
managed in accordance with the requirements of Section
725.933( lm).
4)
An owner or operator using a control device other than a
thermal vapor incinerator, flare, boiler, process heater,
condenser, or carbon adsorption system to comply with
346
subsection (c)(1) above shall operate and maintain the
control device in accordance with the requirements of
Section 725.933(i).
5)
The owner or operator shall demonstrate that a control
device achieves the performance requirements of subsection
(c)(1) above as follows:
A)
An owner or operator shall demonstrate using either a
performance test, as specified in subsection (c)(5)(C)
below, or a design analysis, as specified in
subsection (c)(5)(D) below, the performance of each
control device except for the following:
i)
A flare;
ii)
A boiler or process heater with a design heat
input capacity of 44 megawatts or greater;
iii)
A boiler or process heater into which the vent
stream is introduced with the primary fuel;
iv)
A boiler or process heater industrial furnace
burning hazardous waste for which the owner or
operator has been issued a final permit
under 35
Ill. Adm. Code 702, 703, and 705 and that ishas
designed and operated operates in accordance with
the requirements of 35 Ill. Adm. Code
726.Subpart H; or
v)
A boiler or process heater industrial furnace
burning hazardous waste for which the owner or
operator has certified compliance designed and
operates in accordance
with the interim status
requirements of 35 Ill. Adm. Code 726.Subpart H.
B)
An owner or operator shall demonstrate the performance
of each flare in accordance with the requirements
specified in Section 725.933(e).
C)
For a performance test conducted to meet the
requirements of subsection (c)(5)(A) above, the owner
or operator shall use the test methods and procedures
specified in Section 725.934(c)(1) through (c)(4).
D)
For a design analysis conducted to meet the
requirements of subsection (c)(5)(A) above, the design
analysis must meet the requirements specified in
Section 725.935(b)(4)(C).
E)
The owner or operator shall demonstrate that a carbon
adsorption system achieves the performance
requirements of subsection (c)(1) above based on the
total quantity of
organics vented to the atmosphere
from all carbon adsorption system equipment that is
used for organic adsorption, organic
desorption or
carbon regeneration, organic recovery, and carbon
disposal.
6)
If the owner or operator and the Agency do not agree on a
demonstration of control device performance using a design
347
analysis, then the disagreement must be resolved using the
results of a performance test performed by the owner or
operator in accordance with the requirements of subsection
(c)(5)(C) above. The Agency may choose to have an
authorized representative observe the performance test.
7)
The control device must be inspected and monitored by the
owner or operator in accordance with the procedures
specified in Section 265.933(f)(2) and (k). The readings
from each monitoring device required by Section
265.933(f)(2) must be inspected at least once each operating
day to check control device operation. Any necessary
corrective measures must be immediately implemented to
ensure the control device is operated in compliance with the
requirements of this Section.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.989
Inspection and Monitoring Requirements
a) This Section applies to
anThe owner or operator
usingshall inspect
and monitor air emission control
s equipment used to comply with
this Subpart in accordance with the requirements
ofspecified in
Sections 725.985 through 725.988.
b) Each cover used in accordance with requirements of Sections
725.985 through 725.987 must be visually inspected and monitored
for detectable organic emissions by the owner or operator using
the procedure specified in subsection (f) below, except as
follows:
1) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in
subsection (f) below for the following tank covers:
A) A tank internal floating roof that is inspect
ed and
monitored in accordance with the requirements of
Section 725.991; or
B) A tank external floating roof that is inspected and
monitored in accordance with the requirements of
Section 725.991.
2) If a tank is buried partially or entirely underground, an
owner or operator is required to perform the cover
inspection and monitoring requirements specified in
subsection (f) below only for those portions of the tank
cover and those connections to the tank cover or tank body
(e.g., fill ports, access hatches, gauge wells, etc.) that
extend to or above the ground surface and can be opened to
the atmosphere.
3) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in
subsection (f) below for a container that meets all
requirements specified in either Section 725.987(b)(1)(B) or
(b)(1)(C).
4) An owner or operator is exempted from performing the cover
inspection and monitoring requirements specified in
subsection (f) below for an enclosure used to control air
348
emissions from containers in accordance with the
requirements of Section 725.987(b)(2).
b)
The owner or operator shall develop and implement a written plan
and schedule to perform the inspections and monitoring required by
subsection (a) above. The owner or operator shall incorporate
this plan and schedule into the facility inspection plan required
under Section 265.115.
c) Each closed-vent system used in accordance with the requirements
of Section 725.988 must be inspected and monitored by the owner or
operator in accordance with the procedure specified in Section
725.933(j).
d) Each control device used in accordance with the requirements of
Section 725.988 must be inspected and monitored by the owner or
operator in accordance with the procedure specified in Section
725.933(f).
e) The owner or operator shall develop and implement a written plan
and schedule to perform all inspection and monitoring requirements
of this section. The owner or operator shall incorporate this
plan and schedule into the facility inspection plan required under
35 Ill. Adm. Code 725.115.
f) Inspection and monitoring of a cover in accordance with the
requirements of subsection (b) above must be performed as follows:
1) The cover and all cover openings must be initially visually
inspected and monitored for detectable organic emissions on
or before the date that the tank, surface impoundment, or
container using the cover becomes subject to the provisions
of this Subpart and at other times as requested by the
Agency.
2) At least once every 6 months following the initial visual
inspection and monitoring for detectable organic emissions
required under subsection (f)(1) above, the owner and
operator shall visually inspect and monitor the cover and
each cover opening except for following cover openings:
A) A cover opening that has continuously remained in a
closed, sealed position for the entire period since
the last time the cover opening was visually inspected
and monitored for detectable emissions;
B) A cover opening that is designated as unsafe to
inspect and monitor in accordance with subsection
(f)(5) below;
C) A cover opening on a cover installed and placed in
operation before December 6, 1994 that is designated
as difficult to inspect and monitor in accordance with
subsection (f)(6) below.
3) To visually inspect a cover, the owner or operator shall
view the entire cover surface and each cover opening in a
closed, sealed position for evidence of any defect that may
affect the ability of the cover or cover opening to continue
to operate with no detectable organic emissions. A visible
hole, gap, tear, or split in the cover surface or a cover
349
opening is defined as a leak that must be repaired in
accordance with subsection (f)(7) below.
4) To monitor a cover for detectable organic emissions, the
owner or operator shall use the following procedure:
A) Method 21 in 40 CFR 60, appendix A, incorporated by
reference in 35 Ill. Adm. Code 720.111, to test each
cover seal and cover connection for detectable organic
emissions. Seals on floating membrane covers must be
monitored around the entire perimeter of the cover at
locations spaced no greater than 3 meters apart.
B) For all cover connections and seals except for the
seals around a rotating shaft that passes through a
cover opening, if the monitoring instrument indicates
detectable organic emissions (i.e., an instrument
concentration reading greater than 500
ppmv plus the
background level), then a leak is detected. Each
detected leak must be repaired in accordance with
subsection (f)(7) below.
C) For the seals around a rotating shaft that passes
through a cover opening, if the monitoring instrument
indicates a concentration reading greater than 10,000
ppmv, then a leak is detected. Each detected leak
must be repaired in accordance with subsection (f)(7)
below.
5) An owner or operator may designate a cover as an unsafe to
inspect and monitor cover if all of the following conditions
are met:
A) The owner or operator determines that inspe
ction or
monitoring of the cover would expose a worker to
dangerous, hazardous, or other unsafe conditions.
B) The owner or operator develops and implements a
written plan and schedule to inspect the cover using
the procedure specified in subsection (f)(3) above and
monitor the cover using the procedure specified in
subsection (f)(4) below as frequently as practicable
during those times when a worker can safely access the
cover.
6) An owner or operator may designate a cover installed and
placed in operation before December 6, 1994, as a difficult
to inspect and monitor cover if all of the following
conditions are met:
A) The owner or operator determines that inspection or
monitoring the cover requires elevating a worker to a
height greater than 2 meters (6.6 ft) above a support
surface; and
B) The owner and operator develops and implements a
written plan and schedule to inspect the cover using
the procedure specified in subsection (f)(3) above,
and to monitor the cover using the procedure specified
in subsection (f)(4) above at least once per calendar
year.
350
7) When a leak is detected by either of the methods specified
in subsection (f)(3) or (f)(4) above, the owner or operator
shall repair the leak in the following manner:
A) The owner or operator shall make a first attempt at
repairing the leak no later than 5 calendar days after
the leak is detected. Repair of the leak must be
completed as soon as practicable, but no later than 15
calendar days after the leak is detected. If repair
of the leak cannot be completed within the 15-day
period, except as provided in subsection (f)(7)(B)
below, then the owner or operator shall not add
hazardous waste to the tank, surface impoundment, or
container on which the cover is installed until the
repair of the leak is completed.
B) Repair of a leak detected on a cover installed on a
tank or surface impoundment may be delayed beyond 15
calendar days if the owner or operator determines that
both of the following conditions occur:
i) Repair of the leak requires first emptying the
contents of the tank or surface impoundment; and
ii) Temporary removal of the tank or surface
impoundment from service will result in the
unscheduled cessation of production from the
process unit or operation of the waste
management unit that is generating the hazardous
waste managed in the tank or surface
impoundment.
C) Repair of a leak determined by the owner or operator
to meet the conditions specified in subsection
(f)(7)(B) above must be performed at the next time the
process, system, or waste management unit that is
generating the hazardous waste managed in the tank or
surface impoundment stops operation for any reason.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.990
Recordkeeping Requirements
a)
Each owner or operator of a facility subject to requirements in
this Subpart shall record and maintain the
following information
specified in subsections (b) through (i) of this Section,
as
applicable : to the facility. Except for air emission control
equipment design documentation and information required by
subsection (i) below, records required by this Section must be
maintained in the operating record for a minimum of three years.
Air emission control equipment design documentation must be
maintained in the operating record until the air emission control
equipment is replaced or is otherwise no longer in service.
Information required by subsection (i) below must be maintained in
the operating record for as long as the tank or container is not
using air emission controls specified in Sections 264.984 through
264.987, in accordance with the conditions specified in Section
724.984(d).
1) Documentation for each cover installed on a tank in
351
accordance with the requirements of Section 725.985(b)(2) or
(b)(3) that includes information prepared by the owner or
operator or provided by the cover manufacturer or vendor
describing the cover design, and certification by the owner
or operator that the cover meets the applicable design
specifications as listed in Section 725.991(c).
2) Documentation for each floating membrane cover installed on
a surface impoundment in accordance with the requirements of
Section 725.986(c) that includes information prepared by the
owner or operator or provided by the cover manufacturer or
vendor describing the cover design, and certification by the
owner or operator that the cover meets the specifications
listed in Section 725.986(e).
3) Documentation for each enclosure used to control air
emissions from containers in accordance with the
requirements of Section 725.987(b)(2)(A) that includes
information prepared by the owner or operator or provided by
the manufacturer or vendor describing the enclosure design,
and certification by the owner or operator that the
enclosure meets the specifications listed in Section
725.987(b)(2)(B).
4) Documentation for each closed-vent system and control device
installed in accordance with the requirements of Section
725.988 that includes:
A) Certificatio n that is signed and dated by the owner or
operator stating that the control device is designed
to operate at the performance level documented by a
design analysis, as specified in subsection (a)(4)(B)
below, or by performance tests, as specified in
subsection (a)(4)(C) below, when the tank, surface
impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to
occur.
B) If a design analysis is used, then design
documentation as specified in Section 725.935(b)(4).
The documentation must include information prepared by
the owner or operator or provided by the control
device manufacturer or vendor that describes the
control device design in accordance with Section
725.935(b)(4)(C) and certification by the owner or
operator that the control equipment meets the
applicable specifications.
C) If performance tests are used, then a performance test
plan as specified in Section 725.935(b)(3) and all
test results.
D) Information as required by Sections 725.935(c)
(1) and
725.935(c)(2).
5) Records for all Method 27 tests performed by the owner or
operator for each container used to meet the requirements of
Section 725.987(b)(1)(C).
6) Records for all visual inspections conducted in accordance
with the requirements of Section 725.989.
352
7) Records for all monitoring for detectable organic emissions
conducted in accordance with the requirements of Section
725.989.
8) Records of the date of each attempt to repair a leak, repair
methods applied, and the date of successful repair.
9) Records for all continuous monitoring conducted in
accordance with the requirements of Section 725.989.
10) Records of the management of carbon removed from a carbon
adsorption system conducted in accordance with Section
725.988(c)(3)(B).
11) Records for all inspections of each cover installed on a
tank in accordance with the requirements of Section
725.985(b)(2) or (b)(3) that includes information as listed
in Section 725.991(c).
b) AnThe owner or operator
electing to useof a tank using air
emission controls
for a tank in accordance with the
conditions
specified inrequirements of Section 725.985 (c) shall record prepare
and maintain records for the tank that include
the following
information:
1) The date and time each waste sample is collected for direct
measurement of maximum organic vapor pressure in accordance
with Section 725.984(c).
1)
For each tank using air emission controls in accordance with
the requirements of Section 725.985 of this Subpart, the
owner or operator shall record:
A)
A tank identification number (or other unique
identification description as selected by the owner or
operator).
B)
A record for each inspection required by Section
725.985 that includes the following information:
i)
Date inspection was conducted.
ii)
For each defect detected during the inspection,
the following information: the location of the
defect, a description of the defect, the date of
detection, and corrective action taken to repair
the defect. In the event that repair of the
defect is delayed in accordance with the
provisions of Section 725.985, the owner or
operator shall also record the reason for the
delay and the date that completion of repair of
the defect is expected.
2) The results of each determination for the maximum organic
vapor pressure of the waste in the tank performed in
accordance with Section 725.984(c).
2)
In addition to the information required by subsection (b)(1)
above, the owner or operator shall record the following
information, as applicable to the tank:
353
A)
The owner or operator using a fixed roof to comply
with the Tank Level 1 control requirements specified
in Section 725.985(c) shall prepare and maintain
records for each determination for the maximum organic
vapor pressure of the hazardous waste in the tank
performed in accordance with the requirements of
Section 725.985(c). The records must include the date
and time the samples were collected, the analysis
method used, and the analysis results.
B)
The owner or operator using an internal floating roof
to comply with the Tank Level 2 control requirements
specified in Section 725.985(e) shall prepare and
maintain documentation describing the floating roof
design.
C)
Owners and operators using an external floating roof
to comply with the Tank Level 2 control requirements
specified in Section 725.985(f) shall prepare and
maintain the following records:
i)
Documentation describing the floating roof
design and the dimensions of the tank.
ii)
Records for each seal gap inspection required by
Section 725.985(f)(3) describing the results of
the seal gap measurements. The records must
include the date that the measurements were
performed, the raw data obtained for the
measurements, and the calculations of the total
gap surface area. In the event that the seal
gap measurements do not conform to the
specifications in Section 725.985(f)(1), the
records must include a description of the
repairs that were made, the date the repairs
were made, and the date the tank was emptied, if
necessary.
D)
Each owner or operator using an enclosure to comply
with the Tank Level 2 control requirements specified
in Section 725.985(i) shall prepare and maintain the
following records:
i)
Records for the most recent set of calculations
and measurements performed by the owner or
operator to verify that the enclosure meets the
criteria of a permanent total enclosure as
specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total
Enclosure" under 40 CFR 52.741, appendix B,
incorporated by reference in 35 Ill. Adm. Code
720.111.
ii)
Records required for the closed
-vent system and
control device in accordance with the
requirements of subsection (e) below.
3) The records specifying the tank dimensions and design
capacity.
354
c) An owner or operator electing to use air emission controls for a
tank in accordance with the requirements of Section 725.991 shall
record the information required by Section 725.991(c).
c)
The owner or operator of a surface impoundment using air emission
controls in accordance with the requirements of Section 725.986
shall prepare and maintain records for the surface impoundment
that include the following information:
1)
A surface impoundment identification number (or other unique
identification description as selected by the owner or
operator).
2)
Documentation describing the floating membrane cover or
cover design, as applicable to the surface impoundment, that
includes information prepared by the owner or operator or
provided by the cover manufacturer or vendor describing the
cover design, and certification by the owner or operator
that the cover meets the specifications listed in Section
725.986(c).
3)
A record for each inspection required by Section 725.986
that includes the following information:
A)
Date inspection was conducted.
B)
For each defect detected during the inspection the
following information: the location of the defect, a
description of the defect, the date of detection, and
corrective action taken to repair the defect. In the
event that repair of the defect is delayed in
accordance with the provisions of Section 725.986(f),
the owner or operator shall also record the reason for
the delay and the date that completion of repair of
the defect is expected.
4)
For a surface impoundment equipped with a cover and vented
through a closed -vent system to a control device, the owner
or operator shall prepare and maintain the records specified
in subsection (e) below.
d) An owner or operator electing not to
use air emission controls for
a particular tank, surface impoundment, or container subject to
this Subpart in accordance with the conditions specified in
Section 725.983(c) shall record the information used by the owner
or operator for each waste determination (e.g., test results,
measurements, calculations, and other documentation) in the
facility operating log. If analysis results for waste samples are
used for the waste determination, then the owner or operator shall
record the date, time, and location that each waste sample is
collected in accordance with applicable requirements of Section
725.984.
d)
The owner or operator of containers using Container Level 3 air
emission controls in accordance with the requirements of Section
725.987 shall prepare and maintain records that include the
following information:
1)
Records for the most recent set of calculations and
measurements performed by the owner or operator to verify
that the enclosure meets the criteria of a permanent total
355
enclosure as specified in "Procedure T
--Criteria for and
Verification of a Permanent or Temporary Total Enclosure"
under 40 CFR 52.741, appendix B, incorporated by reference
in 35 Ill. Adm. Code 720.111.
2)
Records required for the closed
-vent system and control
device in accordance with the requirements of subsection (e)
below.
e) An owner or operator electing to comply with requirements in
accordance with Section 725.983(c)(2)(E) or (c)(2)(F) shall record
the identification number for the incinerator, boiler, or
industrial furnace in which the hazardous waste is treated.
e)
The owner or operator using a closed
-vent system and control
device in accordance with the requirements of Section 725.988
shall prepare and maintain records that include the following
information:
1)
Documentation for the closed
-vent system and control device
that includes:
A)
Certification that is signed and dated by the owner or
operator stating that the control device is designed
to operate at the performance level documented by a
design analysis as specified in subsection (e)(1)(B)
below or by performance tests as specified in
subsection (e)(1)(C) below when the tank, surface
impoundment, or container is or would be operating at
capacity or the highest level reasonably expected to
occur.
B)
If a design analysis is used, then design
documentation, as specified in Section 265.935(b)(4).
The documentation must include information prepared
by the owner or operator or provided by the control
device manufacturer or vendor that describes the
control device design in accordance with Section
265.1035(b)(4)(C) and certification by the owner or
operator that the control equipment meets the
applicable specifications.
C)
If performance tests are used, then a performance test
plan as specified in Section 265.935(b)(3) and all
test results.
D)
Information as required by 40 CFR 265.1035(c)(1) and
Section 725.935(c)(2), as applicable.
E)
An owner or operator shall record, on a semiannual
basis, the information specified in subsections
(e)(1)(E)(i) and (e)(1)(E)(ii) below for those planned
routine maintenance operations that would require the
control device not to meet the requirements of Section
725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as
applicable.
i)
A description of the planned routine maintenance
that is anticipated to be performed for the
control device during the next six-month period.
This description must include the type of
356
maintenance necessary, planned frequency of
maintenance, and lengths of maintenance periods.
ii)
A description of the planned routine maintenance
that was performed for the control device during
the previous six -month period. This description
must include the type of maintenance performed
and the total number of hours during those six
months that the control device did not meet the
requirements of Section 725.988(c)(1)(A),
(c)(1)(B), or (c)(1)(C), as applicable, due to
planned routine maintenance.
F)
An owner or operator shall record the information
specified in subsections (e)(1)(F)(i) through
(e)(1)(F)(iii) below for those unexpected control
device system malfunctions that would require the
control device not to meet the requirements of Section
725.988(c)(1)(A), (c)(1)(B), or (c)(1)(C), as
applicable.
i)
The occurrence and duration of each malfunction
of the control device system.
ii)
The duration of each period during a malfunction
when gases, vapors, or fumes are vented from the
waste management unit through the closed
-vent
system to the control device while the control
device is not properly functioning.
iii)
Actions taken during periods of malfunction to
restore a malfunctioning control device to its
normal or usual manner of operation.
G)
Records of the management of carbon removed from a
carbon adsorption system conducted in accordance with
Section 725.988(c)(3)(B).
f)
The owner or operator of a tank, surface impoundment, or container
exempted from standards in accordance with the provisions of
Section 725.983(c) of this Subpart shall prepare and maintain the
following records, as applicable:
1)
For tanks, surface
impoundments, or containers exempted
under the hazardous waste organic concentration conditions
specified in Section 725.983 (c)(1) or (c)(2) of this
Subpart, the owner or operator shall record the information
used for each waste determination (e.g., test results,
measurements, calculations, and other documentation) in the
facility operating log. If analysis results for waste
samples are used for the waste determination, then the owner
or operator shall record the date, time, and location that
each waste sample is collected in accordance with applicable
requirements of Section 725.984 of this Subpart.
2)
For tanks, surface
impoundments, or containers exempted
under the provisions of Section 725.983(c)(2)(vii) or
Section 725.983(c)(2)(viii) of this Subpart, the owner or
operator shall record the identification number for the
incinerator, boiler, or industrial furnace in which the
hazardous waste is treated.
357
fg)
An owner or operator designating a cover as
"unsafe to inspect and
monitor " pursuant to Section
725.989(f)(5) 725.985(l) or difficult
to inspect and monitor pursuant to Section 725.989(f)(6)
shall
record in a log that is kept in the facility operating record the
following information:
the identification numbers for waste
management units with covers that are designated as "unsafe to
inspect and monitor", the explanation for each cover stating why
the cover is unsafe to inspect and monitor, and the plan and
schedule for inspecting and monitoring each cover.
1) A list of identification numbers for tanks with covers that
are designated as unsafe to inspect and monitor in
accordance with the requirements of Section 725.989(f)(5),
an explanation for each cover stating why the cover is
unsafe to inspect and monitor, and the plan and schedule for
inspecting and monitoring each cover.
2) A list of identification numbers for tanks with covers that
are designated as difficult to inspect and monitor in
accordance with the requirements of Section 725.989(f)(6),
an explanation for each cover stating why the cover is
difficult to inspect and monitor, and the plan and schedule
for inspecting and monitoring each cover.
g) All records required by subsections (a) through (f) above, except
as required in subsections (a)(1) through (a)(4) above, must be
maintained in the operating record for a minimum of 3 years. All
records required by subsections (a)(1) through (a)(4) above must
be maintained in the operating record until the air emission
control equipment is replaced or otherwise no longer in service.
h)
The owner or operator of a facility that is subject to this
Subpart and to the control device standards in 40 CFR 60, Subpart
VV, or 40 CFR 61, Subpart V, incorporated by reference in 35 Ill.
Adm. Code 270.111, may elect to demonstrate compliance with the
applicable Sections of this Subpart by documentation either
pursuant to this Subpart, or pursuant to the provisions of 40 CFR
60, Subpart VV or 40 CFR 61, Subpart V, to the extent that the
documentation required by 40 CFR 60 or 61 duplicates the
documentation required by this Section.
i)
For each tank or container not using air emission controls
specified in Sections 725.985 through 725.988 in accordance with
the conditions specified in Section 725.980(d), the owner or
operator shall record and maintain the following information:
1)
A list of the individual organic peroxide compounds
manufactured at the facility that meet the conditions
specified in Section 725.980(d)(1).
2)
A description of how the hazardous wast
e containing the
organic peroxide compounds identified pursuant to subsection
(i)(1) are managed at the facility in tanks and containers.
This description must include the following information:
A)
For the tanks used at the facility to manage this
hazardous waste, sufficient information must be
provided to describe each tank: a facility
identification number for the tank, the purpose and
placement of this tank in the management train of this
358
hazardous waste, and the procedures used to ultimately
dispose of the hazardous waste managed in the tanks.
B)
For containers used at the facility to manage this
hazardous waste, sufficient information must be
provided to describe
the following for
each
tankcontainer : a facility identification number for
the container or group of containers, the purpose and
placement of this container or group of containers in
the management train of this hazardous waste, and the
procedures used to ultimately dispose of the hazardous
waste managed in the containers.
B)
For containers used at the facility to manage these
hazardous wastes, sufficient information must be
provided to describe: A facility identification number
for the container or group of containers; the purpose
and placement of this container, or group of
containers, in the management train of this hazardous
waste; and the procedures used to ultimately dispose
of the hazardous waste handled in the containers.
3)
An explanation of why managing the hazardous waste
containing the organic peroxide compounds identified
pursuant to subsection (i)(1) above in the tanks or
containers identified pursuant to subsection (i)(2) above
would create an undue safety hazard if the air emission
controls specified in Sections 725.985 through 725.988 were
installed and operated on these waste management units.
This explanation must include the following information:
A)
For tanks used at the facility to manage this
hazardous waste, sufficient information must be
provided to explain: how use of the required air
emission controls on the tanks would affect the tank
design features and facility operating procedures
currently used to prevent an undue safety hazard
during the management of this hazardous waste in the
tanks; and why installation of safety devices on the
required air emission controls, as allowed under
Section 725.985(g)
this Subpart , would not address
those situations in which evacuation of tanks equipped
with these air emission controls is necessary and
consistent with good engineering and safety practices
for handling organic peroxides.
B)
For containers used at the facility to manage this
hazardous waste, sufficient information must be
provided to explain: how use of the required air
emission controls on the
tankscontainers would affect
the container design features and handling procedures
currently used to prevent an undue safety hazard
during management of this hazardous waste in the
containers; and why installation of safety devices on
the required air emission controls, as allowed under
Section 725.987(d)
this Subpart , would not address
those situations in which evacuation of containers
equipped with these air emission controls is necessary
and consistent with good engineering and safety
practices for handling organic peroxides.
359
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.991
Alternative Tank Emission Control Requirements
(Repealed)
a) This Section applies to owners and operators of tanks electing to
comply with Section 725.985(b)(2) or (b)(3).
1) The owner or operator electing to comply with Section
725.985(b)(2) shall design, install, operate, and maintain a
fixed roof and internal floating roof that meet the
following requirements.
A) The fixed roof must comply with the requirements of
Section 725.985(d)(1). The internal floating roof
must rest or float on the waste surface (but not
necessarily in complete contact with it) inside a tank
that has a fixed roof. The internal floating roof
must be floating on the waste surface at all times,
except during initial fill and during those intervals
when the tank is completely emptied or subsequently
emptied and refilled. When the roof is resting on the
leg supports, the process of filling, emptying, or
refilling must be
as continuous as possible, based on
the amount of waste and the nature of the waste
handling operation,
and must be accomplished as
rapidly as possible.
B) Each internal floating roof must be equipped with one
of the following closure devices between the wall of
the tank and the edge of the internal floating roof:
i) A foam- or liquid-filled seal mounted in contact
with the waste (liquid-mounted seal). A liquid-
mounted seal means a foam- or liquid-filled seal
mounted in contact with the waste between the
wall of the tank and the floating roof
continuously around the circumference of the
tank.
ii) Two seals mounted one above the other so that
each forms a continuous closure that completely
covers the space between the wall of the tank
and the edge of the internal floating roof. The
lower seal may be vapor-mounted, but both must
be continuous.
iii) A mechanical shoe seal. A mechanical shoe seal
is a metal sheet held vertically against the
wall of the tank by springs or weighted levers
and is connected by braces to the floating roof.
A flexible coated fabric (envelope) spans the
annular space between the metal sheet and the
floating roof.
C) Each opening in a
noncontact internal floating roof
except for automatic bleeder vents (vacuum breaker
vents) and the rim space vents is to provide a
projection below the waste surface.
D) Each opening in the internal floating roof except for
leg sleeves, automatic bleeder vents, rim space vents,
360
column wells, ladder wells, sample wells, and stub
drains is to be equipped with a cover or lid that is
to be maintained in a closed position at all times
(i.e., no visible gap), except when the device is in
actual use. The cover or lid must be equipped with a
gasket. Covers on each access hatch and automatic
gauge float well must be bolted, except when they are
in use.
E) Automatic bleeder vents must be equipped with a gasket
and are to be closed at all times when the roof is
floating, except when the roof is being floated off or
is being landed on the roof leg supports.
F) Rim space vents must be equipped with a gasket and are
to be set to open only when the internal floating roof
is not floating or at the manufacturer's recommended
setting.
G) Each penetration of the internal floating roof for the
purpose of sampling must be a sample well. The sample
well must have a slit fabric cover that covers at
least 90 percent of the opening.
H) Each penetration of the internal floating roof that
allows for passage of a column supporting the fixed
roof must have a flexible fabric sleeve seal or a
gasketed sliding cover.
I) Each penetration of the internal floating roof that
allows for passage of a ladder must have a
gasketed
sliding cover.
2) The owner or operator electing to comply with Section
725.985(b)(3) shall design, install, operate, and maintain
an external floating roof that meets the following
requirements:
A) Each external floating roof must be equipped with a
closure device between the wall of the tank and the
roof edge. The closure device is to consist of two
seals, one above the other. The lower seal is
referred to as the primary seal, and the upper seal is
referred to as the secondary seal.
i) The primary seal must be either a mechanical
shoe seal or a liquid-mounted seal. Except as
provided in subsection (b)(2)(D) below, the seal
must completely cover the annular space between
the edge of the floating roof and tank wall.
ii) The secondary seal must completely cover the
annular space between the external floating roof
and the wall of the tank in a continuous fashion
except as allowed in subsection (b)(2)(D) below.
B) Except for automatic bleeder vents and rim space
vents, each opening in a
noncontact external floating
roof must provide a projection below the waste
surface. Except for automatic bleeder vents, rim
space vents, roof drains, and leg sleeves, each
361
opening in the roof is to be equipped with a
gasketed
cover, seal, or lid that is to be maintained in a
closed position at all times (i.e., no visible gap),
except when the device is in actual use. Automatic
bleeder vents are to be closed at all times when the
roof is floating, except when the roof is being
floated off or is being landed on the roof leg
supports. Rim vents are to be set to open when the
roof is being floated off the roof leg supports or at
the manufacturer's recommended setting. Automatic
bleeder vents and rim space vents are to be
gasketed.
Each emergency roof drain is to be provided with a
slotted membrane fabric cover that covers at least 90
percent of the area of the opening.
C) The roof must be floating on the waste at all times
(i.e., off the roof leg supports), except during
initial fill until the roof is lifted off leg supports
and when the tank is completely emptied and
subsequently refilled. The process of filling,
emptying, or refilling when the roof is resting on the
leg supports must be continuous and must be
accomplished as rapidly as possible.
3) The owner or operator may elect to comply with Section
725.985(b)(2) or (b)(3) using an alternative means of
emission limitation for which U.S. EPA has published a
Federal Register notice in accordance with the requirements
of 40 CFR 60.114b permitting its use as an alternative means
for the purpose of compliance with 40 CFR 60.112b.
b) Monitoring and inspection of
the control equipment described in
subsection (a) above must be conducted as follows:
1) After installation, owners and operators of internal
floating roofs shall:
A) Visually inspect the internal floating roof, the
primary seal, and the secondary seal (if one is in
service), prior to filling the tank with waste. If
there are holes, tears, or other openings in the
primary seal, the secondary seal, or the seal fabric,
or defects in the internal floating roof, or both, the
owner or operator shall repair the items before
filling the tank.
B) For tanks equipped with a liquid-mounted or mechanical
shoe primary seal, visually inspect the internal
floating roof and the primary seal or the secondary
seal (if one is in service) through manholes and roof
hatches on the fixed roof at least once every 12
months after initial fill. If the internal floating
roof is not resting on the surface of the waste inside
the tank, or there is liquid accumulated on the roof,
or the seal is detached, or there are holes or tears
in the seal fabric, the owner or operator shall repair
the items or empty and remove the tank from service
within 45 days. If a failure that is detected during
inspections required in this subsection cannot be
repaired within 45 days and if the tank cannot be
emptied within 45 days, the Agency may grant the owner
362
or operator a provisional variance pursuant to Section
35(b) of the Act that extends this time for up to 30
days. Such a request for an extension must comply
with 35 Ill. Adm. Code 180, and it must document that
alternate capacity is unavailable and specify a
schedule of actions the owner or operator will take
that will assure that the control equipment will be
repaired or the tank will be emptied as soon as
possible.
C) For tanks equipped with a double-seal system as
specified in subsection (a)(1)(A)(ii) above:
i) Visually inspect the tank, as specified in
subsection (b)(1)(D) below, at least every 5
years; or
ii) Visually inspect the tank as specified in
subsection (b)(1)(B) above.
D) Visually inspect the internal floating roof, the
primary seal, the secondary seal (if one is in
service), gaskets, slotted membranes, and sleeve seals
(if any) each time the tank is emptied and degassed.
If the internal floating roof has defects; the primary
seal has holes, tears, or other openings in the seal
or the seal fabric; the secondary seal has holes,
tears, or other openings in the seal or the seal
fabric; the gaskets no longer close off the waste
surfaces from the atmosphere; or the slotted membrane
has more than 10 percent open area, the owner or
operator shall repair the items as necessary, so that
none of the conditions specified in this subsection
exist before refilling the tank with waste. In no
event may inspections conducted in accordance with
this provision occur at intervals greater than 10
years, in the case of tanks conducting the annual
visual inspection as specified in subsection (b)(1)(B)
above, or at intervals no greater than 5 years, in the
case of tanks specified in subsection (b)(1)(C) above.
E) Notify the Agency in writing at least 30 days prior to
the filling or refilling of each tank for which an
inspection is required by subsections (b)(1)(A) and
(b)(1)(D) above, to afford the Agency the opportunity
to have an observer present. If the inspection
required by subsection (b)(1)(D) above is not planned
and the owner or operator could not have known about
the inspection 30 days in advance of refilling the
tank, the owner or operator shall notify the Agency at
least 7 days prior to the refilling of the tank.
Notification must be made by telephone immediately
followed by written documentation demonstrating why
the inspection was unplanned. Alternatively, this
notification, including the written documentation, may
be made in writing and sent by express mail so that it
is received by the Agency at least 7 days prior to the
refilling.
2) After installation, the owner or operator of an external
floating roof shall:
363
A) Determine the gap areas and maximum gap widt
hs between
the primary seal and the wall of the tank and between
the secondary seal and the wall of the tank according
to the following frequency:
i) Measurements of gaps between the tank wall and
the primary seal (seal gaps) must be performed
during the hydrostatic testing of the tank or
within 60 days of the initial fill with waste
and at least once every five years thereafter.
ii) Measurements of gaps between the tank wall and
the secondary seal must be performed within 60
days of the initial fill with waste and at least
once per year thereafter.
iii) If any tank ceases to hold waste for a period of
one year or more, subsequent introduction of
waste into the tank must be considered an
initial fill for the purposes of subsections
(b)(2)(A)(i) and (b)(2)(A)(ii) above.
B) Determine the gap widths and areas in the primary and
secondary seals individually by the following
procedures:
i) Measure seal gaps, if any, at one or more
floating roof levels when the roof is floating
off the roof leg supports.
ii) Measure seal gaps around the entire
circumference of the tank in each place where a
0.32-cm diameter uniform probe passes freely
(without forcing or binding against the seal)
between the seal and the wall of the tank and
measure the circumferential distance of each
such location.
iii) Determine the total surface area of each gap
described in subsection (b)(2)(B)(ii) above by
using probes of various widths to measure
accurately the actual distance from the tank
wall to the seal and multiplying each such width
by its respective circumferential distance.
C) Add the gap surface area of each gap location for the
primary seal and the secondary seal individually and
divide the sum for each seal by the nominal diameter
of the tank and compare each ratio to the respective
standards in subsection (b)(2)(D) below.
D) Make necessary repairs or empty the tank within 45
days of identification in any inspection for seals not
meeting the following requirements:
i) The accumulated area
of gaps between the tank
wall and the mechanical shoe or liquid-mounted
primary seal must not exceed 212 cm
2
per meter
(10.0 in
2
per foot) of tank diameter, and the
width of any portion of any gap must not exceed
364
3.81 cm (1.50 in). One end of the mechanical
shoe is to extend into the waste contained in
the tank, and the other end is to extend a
minimum vertical distance of 61 cm (24.0 in)
above the waste surface. There are to be no
holes, tears, or other openings in the shoe,
seal fabric, or seal envelope.
ii) The secondary seal is to meet the following
requirements: The secondary seal is to be
installed above the primary seal so that it
completely covers the space between the roof
edge and the tank wall except as provided in
subsection (b)(2)(B)(iii) above. The
accumulated area of gaps between the tank wall
and the secondary seal must not exceed 21.2 cm
2
per meter (1.00 in
2
per foot) of tank diameter,
and the width of any portion of any gap must not
exceed 1.27 cm (0.500 in). There are to be no
holes, tears, or other openings in the seal or
seal fabric.
E) If a failure that is detected during inspections
required in subsection (b)(2)(A) above cannot be
repaired within 45 days and if the tank cannot be
emptied within 45 days, the Agency may grant the owner
or operator a provisional variance pursuant to Section
35(b) of the Act that extends this time for up to 30
days. Such a request for an extension must comply
with 35 Ill. Adm. Code 180, and it must include a
demonstration of the unavailability of alternate
capacity and a specification of a schedule that will
assure that the control equipment will be repaired or
the tank will be emptied as soon as possible.
F) Notify the Agency 30 days in advance of any gap
measurements required by subsection (b)(2)(A) above,
to afford the Agency the opportunity to have an
observer present.
G) Visually inspect the external floating roof, the
primary seal, secondary seal, and fittings each time
the vessel is emptied and degassed.
i) If the external fl
oating roof has defects, the
primary seal has holes, tears, or other openings
in the seal or the seal fabric, or the secondary
seal has holes, tears, or other openings in the
seal or the seal fabric, the owner or operator
shall repair the items as necessary so that none
of the conditions specified in this subsection
exist before filling or refilling the tank with
waste.
ii) For all the inspections required by subsection
(b)(2)(G), the owner or operator shall notify
the Agency in writing at least 30 days prior to
the filling or refilling of each tank to afford
the Agency the opportunity to inspect the tank
prior to refilling. If the inspection required
by this subsection is not planned and the owner
365
or operator could not have known about the
inspection 30 days in advance of refilling the
tank, the owner or operator shall notify the
Agency at least seven days prior to the
refilling of the tank. Notification must be
made by telephone immediately followed by
written documentation demonstrating why the
inspection was unplanned. Alternatively, this
notification, including the written
documentation, may be made in writing and sent
by express mail so that it is received by the
Agency at least seven days prior to the
refilling.
c) Owners and operators that elect to install and operate the control
equipment in subsection (a) above shall include the following
information in the operating record in accordance with the
requirements of Section 725.990(a)(1) and (a)(11):
1) Internal floating roof.
A) Document ation that describes the control equipment
design and certifies that the control equipment meets
the specifications of subsections (a)(1) and (b)(1)
above.
B) Records of each inspection performed as required by
subsections (b)(1)(A) through (b)(1)(D) above. Each
record must identify the tank on which the inspection
was performed and must contain the date the tank was
inspected and the observed condition of each component
of the control equipment (seals, internal floating
roof, and fittings).
C) If any of the conditions described in subsection
(b)(1)(B) above are detected during the annual visual
inspection required by subsection (b)(1)(B) above, the
records must identify the tank, the nature of the
defects, and the date the tank was emptied or the
nature of and date the repair was made.
D) After each inspection required by subsection (b)(1)(C)
above that finds holes or tears in the seal or seal
fabric, or defects in the internal floating roof, or
other control equipment defects listed in subsection
(b)(1)(B) above, the records must identify the tank
and the reason it did not meet the specifications of
subsection (a)(1) or (b)(1)(C) above and describe each
repair made.
2) External floating roof.
A) Documentation that describes the control equipment
design and certifies that the control equipment meets
the specifications of subsections (a)(2) and (b)(2)(B)
through (b)(2)(D) above.
B) Records of each gap measurement performed as required
by subsection (b)(2) above. Each record must identify
the tank in which the measurement was performed, the
date of measurement, the raw data obtained in the
366
measurement, and the calculations described in
subsections (b)(2)(B) and (b)(2)(C) above.
C) Records for each seal gap measurement that detects
gaps exceeding the limitations specified by subsection
(b)(2)(D) above that identifies the tank, the date the
tank was emptied or the repairs made, and the nature
of the repair.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 725.Appendix F
Compounds With Henry's Law Constant Less Than 0.1 Y/X
(At 25 degrees Celsius)
Compound name
CAS No.
Acetaldol
107-89-1
Acetamide
60-35-5
1-Acetyl -2-thiourea
591-08-2
3-Acetyl -5-hydroxypiperidine
2-Acetylaminofluorene
53-96-3
3-Acetylpiperidine
618-42-8
Acrylamide
79-06-1
Acrylic acid
79-10-7
Adenine
73-24-5
Adipic acid
124-04-9
Adiponitrile
111-69-3
Alachlor
15972-60
Aldicarb
116-06-3
Ametryn
4-Aminobiphenyl
92-67-1
4-Aminopyridine
504-24-5
Aniline
62-53-3
o-Anisidine
90-04-0
Anthraquinone
84-65-1
Atrazine
1912-24-9
Benzenearsonic acid
98-05-5
Benzenesulfonic acid
98-11-3
Benzidine
92-87-5
Benzo(a)anthracene
56-55-3
Benzo(a)pyrene
50-32-8
Benzo(ghi)perylene
191-24-2
Benzo(k)fluoranthene
207-08-9
Benzoic acid
65-85-0
Benzyl alcohol
100-51-6
gamma-BHC
58-89-9
bis(2-Ethylhexyl)phthalate
117-81-7
Bromochloromethyl acetate
Bromoxynil
Butyric acid
107-92-6
Caprolactam (hexahydro-2H-azepin-2-one)
105-60-2
Catechol
120-80-9
Cell wall
Cellulose (carboxymethylcellulose)
9000-11-7
2-Chloracetophe none
93-76-5
3-Chloro -2,5-diketopyrrolidine
Chloro -1,2-ethane diol
p-Chloro-m-cresol
59-50-7
Chloroacetic acid
79-11-8
p-Chloroaniline
106-47-8
367
p-Chlorobenzophenone
134-85-0
Chlorobenzylate
510-15-6
Chlorhydrin (3-Chloro-1,2-propanediol)
96-24-2
4-Chlorophenol
106-48-9
Chlorophenol polymers
1-(o-Chlorophenyl)thiourea
5344-82-1
Chrysene
218-01-9
Citric acid
77-92-9
Creosote
8001-58-
Cresol (mixed isomers)
1319-77-3
m-Cresol
108-39-4
o-Cresol
95-48-7
p-Cresol
106-44-5
4-Cumylphenol
27576-86
Cyanide
57-12-5
4-Cyanomethyl benzoate
Diazinon
Dibenzo(a,h)anthracene
53-70-3
3,5-Dibromo -4-hydroxybenzonitrile
1689-84-5
Dibutylphthalate
84-74-2
2,6-Dichloro -4-nitroaniline
99-30-9
2,5-Dichloroaniline (N,N-dichloroaniline)
95-82-9
2,6-Dichlorobenzonitrile
1194-65-6
2,5-Dichlorophenol
3,4-Dichlorotetrahydrofuran
3511-19
Dichlorvos
Diethanolamine
N,N-Diethylaniline
91-66-7
Diethyl phosphorothioate
126-75-0
N,N-Diethylpropionamide
15299-99
Diethylene glycol
111-46-6
Diethylene glycol dimethyl ether (dimethyl Carbitol)
Diethylene glycol monobutyl ether (butyl Carbitol)
112-34-5
Diethylene glycol monoethyl ether acetate (Carbitol acetate)
112-15-2
Diethylene glycol monoethyl ether (Carbitol Cellosolve)
111-90-0
Diethylene glycol monomethyl ether (methyl Carbitol)
111-77-3
N,N-Diethylhydrazine
Diethylthiophosphate benzo-m-ethyl-p-ether
Dimethoate
60-51-5
2,3-Dimethoxystrychnidin
-10-one
357-57-3
Dimethylcarbamoyl chloride
Dimethyl disulfide
624-92-0
Dimethylformamide
68-12-2
Dimethylphthalate
131-11-3
4-Dimethylaminoazobenzene
60-11-7
7,12-Dimethylbenz(a)anthracene
57-97-6
3,3-Dimethylbenzidine
119-93-7
1,1-Dimethylhydrazine
57-14-7
Dimethylsulfone
Dimethylsulfoxide
67-68-5
4,6-Dinitro -o-cresol
534-52-1
1,2-Diphenylhydrazine
122-66-7
Dipropylene glycol (1,1'-oxydi-2-propanol)
110-98-5
Endrin
72-20-8
Epinephrine
51-43-4
mono-Ethanolamine
141-43-5
Ethyl carbamate (urethane)
5-17-96
Ethyl morpholine (ethyl diethylene oxime)
Ethylene glycol
107-21-1
Ethylene glycol monobutyl ether (butyl Cellosolve)
111-76-2
368
Ethylene glycol monoethyl ether (Cellosolve)
110-80-5
Ethylene glycol monoethyl ether acetate (Cellosolve acetate)
111-15-9
Ethylene glycol monomethyl ether (methyl Cellosolve)
109-86-4
Ethylene glycol monophenyl ether (phenyl Cellosolve)
122-99-6
Ethylene glycol monopropyl ether (propyl Cellosolve)
2807-30-9
Ethylene thiourea (2-imidazolidinethione)
9-64-57
3-Ethylphenol
620-17-7
Fluoroacetic acid, sodium salt
62-74-8
Formaldehyde
50-00-0
Formamide
7-51-27
Formic acid
64-18-6
Fumaric acid
110-17-8
Glutaric acid
110-94-1
Glycerin (Glycerol)
56-81-5
Glycinamide
598-41-4
Glyphosate
Guthion
Gylcidol
556-52-5
Hexamethylene-1,6-diisocyanate (1,6-diisocyanatohexane)
822-06-0
Hexamethyl phosphoramide
680-31-9
Hexanoic acid
142-62-1
Hydrazine
302-01-2
Hydrocyanic acid
74-90-8
Hydroquinone
123-31-9
Hydroxy -2-propionitrile
109-78-4
Indeno(1,2,3 -cd)pyrene
193-39-5
Lead acetate
301-04-2
Lead subacetate (lead acetate, monobasic)
1335-32-6
Leucine
61-90-5
Malathion
121-75-5
Maleic acid
110-16-7
Maleic anhydride
108-31-6
Mesityl oxide
141-79-7
Methane sulfonic acid
75-75-2
Methomyl
16752-77
p-Methoxyphenol
150-76-5
1-Methyl -2-methoxyaziridine
Methylacrylate
96-33-3
4,4'-Methylene -bis-(2 -chloroaniline)
101-14-4
Methylene diphenyl diisocyanate (diphenyl methane diisocyanate)
101-68-8
4,4-Methylenedianiline
101-77-9
Methylene diphenylamine (MDA)
5-Methylfurfural
620-02-0
Methylhydrazine
60-34-4
Methyliminoacetic acid
Methylparathion
298-00-0
Methyl sulfuric acid
77-78-1
4-Methylthiophenol
106-45-6
Monomethyl formamide (n-methylformamide)
123-39-7
Nabam
alpha-Naphthol
90-15-3
beta-Naphthol
135-19-3
alpha-Naphthylamine
134-32-7
beta-Naphthylamine
91-59-8
Neopentyl glycol
126-30-7
Niacinamide
98-92-0
o-Nitroaniline
88-74-4
Nitroglycerin
55-63-0
2-Nitrophenol
88-75-5
369
4-Nitrophenol
100-02-7
N-Nitroso -n-methylurea
684-93-5
N-Nitrosodimethylamine
62-75-9
Nitrosoguanidine
674-81-7
N-Nitrosomorpholine (4-nitrosomorpholine)
59-89-2
Oxalic acid
144-62-7
Parathion
56-38-2
Pentaerythritol
115-77-5
Phenacetin
62-44-2
Phenol
108-95-2
Phenyl mercuric acetate
62-38-4
Phenylacetic acid
103-82-2
m-Phenylene diamine
108-45-2
o-Phenylene diamine
95-54-5
p-Phenylene diamine
106-50-3
Phorate
298-02-2
Phthalic anhydride
85-44-9
alpha-Picoline (2-methyl pyridine)
109-06-8
1,3-Propane sulfone
1120-71-4
beta-Propiolactone
57-57-8
Proporur (Baygon)
Propylene glycol
57-55-6
Pyrene
129-00-0
Pyridinium bromide
Quinoline
91-22-5
Quinone (p-benzoquinone)
106-51-4
Resorcinol
108-46-3
Simazine
122-34-9
Sodium acetate
127-09-3
Sodium formate
141-53-7
Strychnine
57-24-9
Succinic acid
110-15-6
Succinimide
123-56-8
Sulfanilic acid
121-47-1
Terephthalic acid
100-21-0
Tetraethyldithiopyrophosphate
3689-24-5
Tetraethylenepentamine
112-57-2
Thiofanox
39196-18
Thiosemicarbazide
79-19-6
2,4-Toluene diamine
95-80-7
2,4-Toluene diisocyanate
584-84-9
2,6-Toluenediamine
823-40-5
3,4-Toluenediamine
496-72-0
p-Toluic acid
99-94-5
m-Toluidine
108-44-1
1,1,2-Trichloro-1,2,2-trifluoroethane
76-13-1
Triethanolamine
102-71-6
Triethylene glycol dimethyl ether
Tripropylene glycol
24800-44-0
Warfarin
81-81-2
3,4-Xylenol (3,4-dimethylphenol)
95-65-8
(Source: Added at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 726
370
STANDARDS FOR THE MANAGEMENT OF SPECIFIC HAZARDOUS WASTE
AND SPECIFIC TYPES OF HAZARDOUS WASTE MANAGEMENT FACILITIES
SUBPART C: RECYCLABLE MATERIALS USED IN A MANNER
CONSTITUTING DISPOSAL
Section
726.120
Applicability
726.121
Standards applicable to generators and transporters of materials
used in a manner that constitutes disposal
726.122
Standards applicable to storers, who are not the ultimate users,
of materials that are to be used in a manner that constitutes
disposal
726.123
Standards Applicable to Users of Materials that are Used in a
Manner that Constitutes Disposal
SUBPART D: HAZARDOUS WASTE BURNED FOR ENERGY RECOVERY
Section
726.130
Applicability (Repealed)
726.131
Prohibitions (Repealed)
726.132
Standards applicab
le to generators of hazardous waste fuel
(Repealed)
726.133
Standards applicable to transporters of hazardous waste fuel
(Repealed)
726.134
Standards applicable to marketers of hazardous waste fuel
(Repealed)
726.135
Standards applicable to burners of hazardous waste fuel (Repealed)
726.136
Conditional exemption for spent materials and by-products
exhibiting a characteristic of hazardous waste (Repealed)
SUBPART E: USED OIL BURNED FOR ENERGY RECOVERY (Repealed)
Section
726.140
Applicability (Repealed)
726.141
Prohibitions (Repealed)
726.142
Standards applicable to generators of used oil burned for energy
recovery (Repealed)
726.143
Standards applicable to marketers of used oil burned for energy
recovery (Repealed)
726.144
Standards applicable to burners of used oil burned for energy
recovery (Repealed)
SUBPART F: RECYCLABLE MATERIALS UTILIZED FOR PRECIOUS METAL
RECOVERY
Section
726.170
Applicability and requirements
SUBPART G: SPENT LEAD-ACID BATTERIES BEING RECLAIMED
Section
726.180
Applicabi lity and requirements
SUBPART H: HAZARDOUS WASTE BURNED IN BOILERS
AND INDUSTRIAL FURNACES
Section
726.200
Applicability
726.201
Management prior to Burning
726.202
Permit standards for Burners
726.203
Interim Status Standards for Burners
726.204
Standards to Control Organic Emissions
726.205
Standards to control PM
726.206
Standards to Control Metals Emissions
726.207
Standards to control HCl and Chlorine Gas Emissions
726.208
Small quantity On-site Burner Exemption
371
726.209
Low risk waste Exemption
726.210
Waiver of DRE trial burn for Boilers
726.211
Standards for direct Transfer
726.212
Regulation of Residues
726.219
Extensions of Time
726.Appendix A
Tier I and Tier II Feed Rate and Emissions Screening Limits
for Metals
726.Appendix B
Tier I Feed Rate Screening Limits for Total Chlorine
726.Appendix C
Tier II Emission Rate Screening Limits for Free Chlorine and
Hydrogen Chloride
726.Appendix D
Reference Air Concentrations
726.Appendix E
Risk Specific Doses
726.Appendix F
Stack Plume Rise
726.Appendix G
Health-Based Limits for Exclusion of Waste-Derived Residues
726.Appendix H
Potential PICs for Determination of Exclusion of Waste-
Derived Residues
726.Appendix I
Methods Manual for Compliance with BIF Regulations
726.Appendix J
Guideline on Air Quality Models
726.Appendix K
Lead-Bearing Materials That May be Processed in Exempt Lead
Smelters
726.Appendix L
Nickel or Chromium-Bearing Materials that may be Processed
in Exempt Nickel-Chromium Recovery Furnaces
726.Appendix M
Mercury-Bearing Wastes That May Be
Processed in Exempt
Mercury Recovery Units
726.Table A
Exempt Quantities for Small Quantity Burner Exemption
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R85-22 at 10 Ill. Reg. 1162, effective January 2, 1986;
amended in R86-1 at 10 Ill. Reg. 14156, effective August 12, 1986; amended in
R87-26 at 12 Ill. Reg. 2900, effective January 15, 1988; amended in R89-1 at
13 Ill. Reg. 18606, effective November 13, 1989; amended in R90-2 at 14 Ill.
Reg. 14533, effective August 22, 1990; amended in R90-11 at 15 Ill. Reg. 9727,
effective June 17, 1991; amended in R91-13 at 16 Ill. Reg. 9858, effective
June 9, 1992; amended in R92-10 at 17 Ill. Reg. 5865, effective March 26,
1993; amended in R93-4 at 17 Ill. Reg. 20904, effective November 22, 1993;
amended in R94-7 at 18 Ill. Reg. 12500, effective July 29, 1994; amended in
R95-6 at 19 Ill. Reg. 10006, effective June 27, 1995; amended in R95-20 at 20
Ill. Reg. 11263, August 1, 1996
; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
________, effective ____________________
.
SUBPART F: RECYCLABLE MATERIALS UTILIZED FOR PRECIOUS METAL
RECOVERY
Section 726.170
Applicability and requirements
a)
The regulations of this subpart apply to recyclable materials that
are reclaimed to recover economically significant amounts of gold,
silver, platinum, paladium, irradium, osmium, rhodium, ruthenium,
or any combination of these.
b)
Persons whothat generate, transport or store recyclable materials
that are regulated under this Subpart are subject to the following
requirements:
1)
Notification requirements under Section 3010 of the Resource
Conservation and Recovery Act;
372
2)
35 Ill. Adm. Code 722.Subpart B (for generators), 35 Ill.
Adm. Code 723.120 and 121 (for transporters), and 35 Ill.
Adm. Code 725.171 and 725.172 (for persons
whothat store) .;
and
3)
For precious metals exported to or imported from designated
OECD member countries for recovery, 35 Ill. Adm. Code
722.Subpart H and 725.112(a)(2). For precious metals
exported to or imported from non-OECD countries for
recovery, 35 Ill. Adm. Code 722.Subparts E and F.
c)
Persons whothat store recycled materials that are regulated under
this Subpart shall keep the following records to document that
they are not accumulating these materials speculatively (as
defined in 35 Ill. Adm. Code 721.101(c);
1)
Records showing the volume of these materials stored at the
beginning of the calendar year;
2)
The amount of these mater
ials generated or received during
the calendar year; and
3)
The amount of materials remaining at the end of the calendar
year.
d)
Recyclable materials that are regulated under this Subpart that
are accumulated speculatively (as defined in 35 Ill. Adm. Code
721.101(c)) are subject to all applicable provisions of 35 Ill.
Adm. Code 722 through 725, and 35 Ill. Adm. Code 702, 703 and 705.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 728
LAND DISPOSAL RESTRICTIONS
SUBPART A: GENERAL
Section
728.101
Purpose, Scope and Applicability
728.102
Definitions
728.103
Dilution Prohibited as a Substitute for Treatment
728.104
Treatment Surface Impoundment Exemption
728.105
Procedures for case-by-case Extensions to an Effective Date
728.106
Petitions to Allow Land Disposal of a Waste Prohibited under
Subpart C
728.107
Waste Analysis and Recordkeeping
728.108
Landfill and Surface Impoundment Disposal Restrictions (Repealed)
728.109
Special Rules for Characteristic Wastes
SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION
AND ESTABLISHMENT OF TREATMENT STANDARDS
Section
728.110
First Third (Repealed)
728.111
Second Third (Repealed)
728.112
Third Third (Repealed)
728.113
Newly Listed Wastes
373
728.114
Surface Impoundment exemptions
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section
728.130
Waste Specific Prohibitions -- Solvent
Wastes
728.131
Waste Specific Prohibitions -- Dioxin-Containing Wastes
728.132
Waste Specific Prohibitions -- California List Wastes
728.133
Waste Specific Prohibitions: First Third Wastes
728.134
Waste Specific Prohibitions -- Second Third Wastes
728.135
Waste Specific Prohibitions -- Third Third Wastes
728.136
Waste Specific Prohibitions -- Newly Listed Wastes
728.137
Waste Specific Prohibitions -- Ignitable and Corrosive
Characteristic Wastes Whose Treatment Standards Were Vacated
728.138
Waste-Specifi c Prohibitions: Newly-Identified Organic Toxicity
Characteristic Wastes and Newly-Listed Coke By-Product and
Chlorotoluene Production Wastes
728.139 Statutory Prohibitions
Waste-Specific Prohibitions: End-of-pipe
CWA, CWA-Equivalent, and Class I Nonhazardous Waste Injection Well
Treatment Standards; Spent Aluminum Potliners; and Carbamate
Wastes
SUBPART D: TREATMENT STANDARDS
Section
728.140
Applicability of Treatment Standards
728.141
Treatment Standards Expressed as Concentrations in Waste Extract
728.142
Treatment Standards Expressed as Specified Technologies
728.143
Treatment Standards Expressed as Waste Concentrations
728.144
Adjustment of Treatment Standard
728.145
Treatment Standards for Hazardous Debris
728.146
Alternative Treatment Standards Based on HTMR
728.148
Universal Treatment Standards
SUBPART E: PROHIBITIONS ON STORAGE
Section
728.150
Prohibitions on Storage of Restricted Wastes
728.Appendix A
Toxicity Characteristic Leaching Procedure (TCLP)
728.Appendix B
Treatment Standards (As con
centrations in the Treatment
Residual Extract)
728.Appendix C
List of Halogenated Organic Compounds
728.Appendix D
Wastes Excluded from Lab Packs
728.Appendix E
Organic Lab Packs (Repealed)
728.Appendix F
Technologies to Achieve Deactivation of Characteristics
728.Appendix G
Federal Effective Dates
728.Appendix H
National Capacity LDR Variances for UIC Wastes
728.Appendix I
EP Toxicity Test Method and Structural Integrity Test
728.Appendix J
Recordkeeping, Notification, and Certification Requirements
728.Appendix K
Metal Bearing Wastes Prohibited From Dilution in a
Combustion Unit According to Section 728.103(c)
728.Table A
Constituent Concentrations in Waste Extract (CCWE)
728.Table B
Constituent Concentrations in Wastes (CCW)
728.Table C
Technology Codes and Description of Technology-Based
Standards
728.Table D
Technology-Based Standards by RCRA Waste Code
728.Table E
Standards for Radioactive Mixed Waste
728.Table F
Alternative Treatment Standards for Hazardous Debris
728.Table G
Alternative Treatm
ent Standards Based on HMTR
728.Table H
Wastes Excluded from CCW Treatment Standards
728.Table T
Treatment Standards for Hazardous Wastes
728.Table U
Universal Treatment Standards (UTS)
374
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R87-5 at 11 Ill. Reg. 19354, effective November 12, 1987;
amended in R87-39 at 12 Ill. Reg. 13046, effective July 29, 1988; amended in
R89-1 at 13 Ill. Reg. 18403, effective November 13, 1989; amended in R89-9 at
14 Ill. Reg. 6232, effective April 16, 1990; amended in R90-2 at 14 Ill. Reg.
14470, effective August 22, 1990; amended in R90-10 at 14 Ill. Reg. 16508,
effective September 25, 1990; amended in R90-11 at 15 Ill. Reg. 9462,
effective June 17, 1991; amendment withdrawn at 15 Ill. Reg. 14716, October
11, 1991; amended in R91-13 at 16 Ill. Reg. 9619, effective June 9, 1992;
amended in R92-10 at 17 Ill. Reg. 5727, effective March 26, 1993; amended in
R93-4 at 17 Ill. Reg. 20692, effective November 22, 1993; amended in R93-16 at
18 Ill. Reg. 6799, effective April 26, 1994; amended in R94-7 at 18 Ill. Reg.
12203, effective July 29, 1994; amended in R94-17 at 18 Ill. Reg. 17563,
effective November 23, 1994; amended in R95-6 at 19 Ill. Reg. 9660, effective
June 27, 1995; amended in R95-20 at 20 Ill. Reg. 11100, August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
SUBPART A: GENERAL
Section 728.101
Purpose, Scope and Appli
cability
a)
This Part identifies hazardous wastes that are restricted from
land disposal and defines those limited circumstances under which
an otherwise prohibited waste may continue to be land disposed.
b)
Except as specifically provided otherwise in this Part or 35 Ill.
Adm. Code 721, the requirements of this Part apply to persons that
generate or transport hazardous waste and to owners and operators
of hazardous waste treatment, storage, and disposal facilities.
c)
Restricted wastes may continue t
o be land disposed as follows:
1)
Where persons have been granted an extension to the
effective date of a prohibition under Subpart C or pursuant
to Section 728.105, with respect to those wastes covered by
the extension;
2)
Where persons have been granted an exemption from a
prohibition pursuant to a petition under Section 728.106,
with respect to those wastes and units covered by the
petition;
3) WA wastes that areis hazardous only because
theyit exhibit s
a hazardous characteristic of hazardous waste
and that areis
otherwise prohibited
from land disposal
under this Part
areis not prohibited from land disposal
if the waste s:
A)
Are disposed into a nonhazardous or hazardous waste
injection well, as defined in 35 Ill. Adm. Code
704.106(a); and
B)
Do not exhibit any prohibited characteristic of
hazardous waste identified in 35 Ill. Adm. Code
721.Subpart C at the point of injection; and
C) If, at the point of generation, the injected wastes
375
include D001 High TOC subcategory wastes or D012-D017
pesticide wastes that are prohibited under Section
728.117(c), those wastes have been treated to meet the
treatment standards of Section 728.140 prior to
injection.
4)
A waste that is hazardous only because it exhibits a
characteristic of hazardous waste and which is otherwise
prohibited under this Part is not prohibited if the waste
meets any of the following criteria, unless the waste is
subject to a specified method of treatment other than DEACT
in Section 728.140 or is D003 reactive cyanide:
A)
The waste is managed in a treatment system which
subsequently discharges to waters of the U.S. pursuant
to a permit issued under 35 Ill. Adm. Code 309; or
B)
The waste is treated for purposes of the pretreatment
requirements of 35 Ill. Adm. Code 307 and 310; or
C)
The waste is managed in a zero discharge system
engaged in Clean Water Act-equivalent treatment, as
defined in Section 728.137(a); and
D)
The waste no longer exhibits a prohibited
characteristic of hazardous waste at the point of land
disposal (i.e., placement in a surface impoundment).
d)
This Part does not affect the availability of a waiver under
Section 121(d)(4) of the Comprehensive Environmental Response,
Compensation, and Liability Act of 1980 (CERCLA) (42 U.S.C.
ยงยง 9601 et seq.).
e)
The following hazardous wastes are not subject to any provision of
this Part:
1)
Wastes generated by small quantity generators of less than
100 kg of non-acute hazardous waste or less than 1 kg of
acute hazardous waste per month, as defined in 35 Ill. Adm.
Code 721.105;
2)
Waste pesticides that a farmer disposes of pursuant to 35
Ill. Adm. Code 722.170;
3)
Wastes identified or listed as hazardous after November 8,
1984, for which USEPA has not promulgated land disposal
prohibitions or treatment standards;
or
4)
De minimis losses
of waste that exhibits a characteristic of
hazardous waste to wastewater s treatment systems of
commercial chemical product or chemical intermediates that
are ignitable (D001) or corrosive (D002) or that are organic
constituents that exhibit the characteristic of toxicity
(D012-D043) and that contain underlying hazardous
constituents, as defined in Section 728.102 of this Part,
are not considered to be prohibited waste
s and are defined
as follows: . "De minimis" is defined as l
A)
Losses from normal material handling operations (e.g.,
spills from the unloading or transfer of materials
from bins or other containers or leaks from pipes,
376
valves, or other devices used to transfer materials);
minor leaks of process equipment, storage tanks, or
containers; leaks from well-maintained pump packings
and seals; sample purging
s; relief device discharges;
discharges from safety showers and rinsing and
cleaning of personal safety equipment; and rinsate
from empty containers or from containers that are
rendered empty by that rinsing;
and laboratory waste
that does not exceed one per cent of the total flow of
wastewater into the facility's headworks on an annual
basis, or with a combined annualized average
concentration not exceeding one part per million (ppm)
in the headworks of the facility's wastewater
treatment or pretreatment facility; or
B)
Decharacterized waste that is injected into Class I
nonhazardous wells in which the decharacterized
waste's combined volume is less than one per cent of
the total flow at the wellhead on an annualized basis
and no greater than 10,000 gallons per day, and in
which any underlying hazardous constituents in the
characteristic waste are present at the point of
generation at levels less than 10 times the treatment
standards found at Section 728.148.
5)
Land disposal prohibitions for hazardous characteristic
wastes do not apply to laboratory wastes displaying the
characteristic of ignitability (D001), corrosivity (D002),
or organic toxicity (D012 through D043) that are mixed with
other plant wastewaters at facilities whose ultimate
discharge is subject to regulation under the CWA (including
wastewaters at facilities that have eliminated the discharge
of wastewater), provided that the annualized flow of
laboratory wastewater into the facility's headwork does not
exceed one percent or that the laboratory wastes' combined
annualized average concentration does not exceed one part
per million in the facility's headworks.
f)
A universal waste handler or universal waste transporter (as
defined in 35 Ill. Adm. Code 720.110) is exempt from Sections
728.107 and 268.150 for the hazardous wastes listed below. Such a
handler or transporter is subject to regulation under 35 Ill. Adm.
Code 733.
1)
Batteries, as described in 35 Ill. Adm. Code 733.102;
2)
Pesticides, as described in 35 Ill. Adm. Code 733.103; and
3)
Thermostats, as described in 35 Ill. Adm. Code 733.104.
g)
This Part is cumulative with the land disposal restrictions of 35
Ill. Adm. Code 729. The Environmental Protection Agency (Agency)
shall not issue a wastestream authorization pursuant to 35 Ill.
Adm. Code 709 or Sections 22.6 or 39(h) of the Environmental
Protection Act [415 ILCS 5/22.6 or 39(h)] unless the waste meets
the requirements of this Part as well as 35 Ill. Adm. Code 729.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.102 Definitions
377
When used in this Part, the following terms have the meanings given below.
All other terms have the meanings given under 35 Ill. Adm. Code 702.110,
720.102, or 721.103.
"Agency" means the Illinois Environmental Protection Agency.
"Board" means the Illinois Pollution Control Board.
"CERCLA" means the Comprehensive Environmental Respons
e,
Compensation, and Liability Act of 1980 (42 U.S.C. 9601 et seq.)
"Debris" means solid material exceeding a 60 mm particle size that
is intended for disposal and that is: a manufactured object;
plant or animal matter; or natural geologic material. However,
the following materials are not debris: any material for which a
specific treatment standard is provided in 728.Subpart D, namely
lead acid batteries, cadmium batteries, and radioactive lead
solids; process residuals, such as smelter slag and residues from
the treatment of waste, wastewater, sludges, or air emission
residues; and intact containers of hazardous waste that are not
ruptured and that retain at least 75% of their original volume. A
mixture of debris that has not been treated to the standards
provided by Section 728.145 of this Part and other material is
subject to regulation as debris if the mixture is comprised
primarily of debris, by volume, based on visual inspection.
"End-of-pipe" refers to the point where effluent is discharged to
the environment.
"Halogenated organic compounds" or "HOCs" means those compounds
having a carbon-halogen bond that are listed under Section
728.Appendix C.
"Hazardous constituent or constituents" means those constituents
listed in 35 Ill. Adm. Code 721.Appendix H.
"Hazardous debris" means debris that contains a hazardous waste
listed in 35 Ill. Adm. Code 721.Subpart D or that exhibits a
characteristic of hazardous waste identified in 35 Ill. Adm. Code
721.Subpart C.
"Inorganic metal-bearing waste" is one for which USEPA has
established treatment standards for metal hazardous constituents
that does not otherwise contain significant organic or cyanide
content, as described in Section 728.103(b)(1), and which is
specifically listed in Section 728.Appendix K.
"Inorganic Ssolid Ddebris" are nonfriable inorganic solids that
are incapable of passing through a 9.5 mm standard sieve and that
require cutting or crushing and grinding in mechanical sizing
equipment prior to stabilization, limited to the following
inorganic or metal materials:
Metal slags (either dross or scoria).
Glassified slag.
Glass.
Concrete (excluding cementitious or pozzolanic stabilized
hazardous wastes).
378
Masonry and refractory bricks.
Metal cans, containers, drums, or tanks.
Metal nuts, bolts, pipes, pumps, valves, appliances, or
industrial equipment.
Scrap metal, as defined in 35 Ill. Adm. Code 721.101(c)(6).
"Land disposal" means placement in or on the land, except in a
corrective action management unit, and includes, but is not
limited to, placement in a landfill, surface impoundment, waste
pile, injection well, land treatment facility, salt dome
formation, salt bed formation, underground mine, or cave or
placement in a concrete vault or bunker intended for disposal
purposes.
"Nonwastewaters" are wastes that do not meet the criteria for
"wastewaters" in this Section.
"Polychlorinated biphenyls" or "PCBs" are halogenated organic
compounds defined in accordance with 40 CFR 761.3, incorporated by
reference in 35 Ill. Adm. Code 720.111.
"ppm" means parts per million.
"RCRA corrective action" means corrective action taken under 35
Ill. Adm. Code 724.200 or 725.193, 40 CFR 264.100 or 265.93
(199496), or similar regulations in other States with RCRA
programs authorized by U
.S. EPA pursuant to 40 CFR 271 (19
9496).
"Stormwater impoundments" are surface impoundments that receive
wet weather flow and which receive process waste only during wet
weather events.
"Underlying hazardous constitue
nt" means any regulated constituent
listed in Section 728.Table U, "Universal Treatment Standards
(UTS)", except fluoride, vanadium , and zinc, that can reasonably
be expected to be present
, at the point of generation of the
hazardous waste , at a concentration above the constituent-specific
UTS treatment standard.
"U.S. EPA" or "USEPA" means the United States Environmental
Protection Agency.
"Wastewaters" are wastes that contain less than 1% by weight total
organic carbon (TOC) and less than 1% by weight total suspended
solids (TSS) , with the following exceptions:
F001, F002, F003, F004, and F005 solvent
-water mixtures that
contain less than 1% by weight TOC or less than 1% by weight
total F001, F002, F003, F004, and F005 solvent constituents
listed in Table A.
K011, K013, and K014 wastewaters (as generated) that contain
less than 5% by weight TOC and less than 1% by weight TSS.
K103 and K104 wastewaters that contain less than 4% by
weight TOC and less than 1% by weight TSS
.
379
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.103
Dilution Prohibited as a Substitute for Treatment
a)
Except as provided in subsection (b) below, no generator,
transporter, handler
, or owner or operator of a treatment,
storage , or disposal facility shall in any way dilute a restricted
waste or the residual from treatment of a restricted waste as a
substitute for adequate treatment to achieve compliance with
728.Subpart D of this Part , to circumvent the effective date of a
prohibition in 728.Subpart C of this Part , to otherwise avoid a
prohibition in 728.Subpart C of this Part , or to circumvent a land
disposal restriction imposed by RCRA section 3004
.
b)
Dilution of waste
s that areis hazardous only because
theyit
exhibit s a characteristic
of hazardous waste
in a treatment system
whichthat treats wastes subsequently discharged to a water of the
State pursuant to an NPDES permit issued under 35 Ill. Adm. Code
309, that treats wastes in a CWA-equivalent treatment system,
or
whichthat treats wastes for purposes of pretreatment requirements
under 35 Ill. Adm. Code 310 is not impermissible dilution for
purposes of this Section unless a method
other than DEACT
has been
specified in Section 728.140
as the treatment standard
in Section
728.142, or unless the waste is a D003 reactive cyanide wastewater
or nonwastewater.
c)
Combustion of waste designated by any of the USEPA hazardous waste
codes listed in Section 728.Appendix J is prohibited, unless the
waste can be demonstrated to comply with one or more of the
following criteria at the point of generation or after any bona
fide treatment, such as cyanide destruction prior to combustion,
(unless otherwise specifically prohibited from combustion):
1)
The waste contains hazardous organic constituents or cyanide
at levels exceeding the constituent-specific treatment
standard found in Section 728.148;
2)
The waste consists of organic, debris-like materials (e.g.,
wood, paper, plastic, or cloth) contaminated with an
inorganic metal-bearing hazardous waste;
3)
The waste has reasonable heating value, such as greater than
or equal to 5000 BTU per pound, at the point of generation;
4)
The waste is co-generated with wastes for which combustion
is a required method of treatment;
5)
The waste is subject to any federal or state requirements
necessitating reduction of organics (including biological
agents); or
6)
The waste contains greater than one percent Total Organic
Carbon (TOC).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.107
Waste Analysis and Recordkeeping
a)
Except as specified in Section 728.132, where a generator's waste
is listed in 35 Ill. Adm. Code 721.Subpart D or if the waste
exhibits one or more of the characteristics set out at 35 Ill.
380
Adm. Code 721.Subpart C, the generator shall test its waste, or
test an extract using the Toxicity Characteristic Leaching
Procedure, Method 1311, in "Test Methods for Evaluating Solid
Waste, Physical/Chemical Methods", U
.S. EPA Publication SW-846, as
incorporated by reference in 35 Ill. Adm. Code 720.111, or use
knowledge of the waste to determine if the waste is restricted
from land disposal under this Part. If the generator determines
that its waste displays the characteristic of ignitability (D001)
(and is not in the High TOC Ignitable Liquids Subcategory or is
not treated by CMBST or RORGS of Section 728.Table C
of this Part )
or the waste displays the characteristic of corrosivity (D002)
,
reactivity (D003), or organic toxicity (D012 through D043),
and
the waste is prohibited under Section
s 728.137, or the waste
displays the characteristic of organic toxicity (D012-D043) and is
prohibited under
Section 728.138,
and 728.139, the generator shall
determine what underlying hazardous constituents (as defined in
Section 728.102), are reasonably expected to be present in the
D001, D002, D003, or D012 through D043 waste.
1)
If a generator determines that it is managing a restricted
waste under this Part and the waste does not meet the
applicable treatment standards set forth in 728.Subpart D or
exceeds the applicable prohibition levels set forth in
Section 728.132 or 728.139, the generator shall
notify
thesend a one-time written notice to each
treatment or
storage facility
in writing with eachthe initial shipment of
waste. No further notification is necessary until such time
that the waste or facility change, in which case a new
notification must be sent and a copy placed in the
generator's file.
The notice must include the following
information:
A)
U.S. EPA hazardous waste number;
B)
The waste constituents that the treater will monitor,
if monitoring will not include all regulated
constituents, for wastes F001 through F005, F039,
D001, D002, D003, and D012 through D043
, and wastes
prohibited pursuant to Section 728.132 or Section
3004(d) of the Resource Conservation and Recovery Act,
referenced in Section 728.139
. The generator must
also include whether the waste is a nonwastewater or
wastewater (as defined in Section 728.102 (d) and (f))
and indicate the subcategory of the waste (such as
"D003 reactive cyanide") if applicable;
C)
The manifest number associated with the shipment of
waste;
D)
For hazardous debris, the contaminants subject to
treatment, as provided by Section 728.145(b), and the
following statement: "This hazardous debris is
subject to the alternative treatment standards of 35
Ill. Adm. Code 728.145
"; and
E)
Waste analysis data, where available
; and.
F) The date on which the waste is subject to the
prohibitions.
2)
If a generator determines that it is managing a restricted
381
waste under this Part and determines that the waste can be
land disposed without further treatment, with
eachthe
initial shipment of waste the generator shall submit a
one-
time written notice and a certification to
theeach
treatment, storage, or land disposal facility stating that
the waste meets the applicable treatment standards set forth
in 728.Subpart D and setting forth the applicable
prohibition levels set forth in Section 728.132 or RCRA
Section 3004(d), referenced in Section 728.139. A generator
of hazardous debris that is excluded from the definition of
hazardous waste under 35 Ill. Adm. Code 721.103(e)(2), 35
Ill. Adm. Code 728.103(f)(2), or 35 Ill. Adm. Code 720.122
(i.e. debris that is delisted), however, is not subject to
these notification and certififcation requirements.
If the
waste changes, the generator shall send a new notice and
certification to the receiving facility, and place a copy in
its files.
A)
The notice must include the following information:
i)
U.S. EPA hazardous waste number;
ii)
The waste constituents that the treater will
monitor, if monitoring will not include all
regulated constituents, for wastes F001 through
F005, F039, D001, D002,
D003, and D012 through
D043, and wastes prohibited pursuant to Section
728.132 or Section 3004(d) of the Resource
Conservation and Recovery Act, referenced in
Section 728.139 . The generator must also
include whether the waste is a nonwastewater or
wastewater (as defined in Section 728.102 (d)
and (f)) and indicate the subcategory of the
waste (such as "D003 reactive cyanide") if
applicable;
iii)
The manifest number associated with the shipment
of waste; and
iv)
Waste analysis data, where available.
B)
The certification must be signed by an authorized
representative and must state the following:
I certify under penalty of law that I personally have
examined and am familiar with the waste through
analysis and testing or through knowledge of the waste
to support this certification that the waste complies
with the treatment standards specified in 35 Ill. Adm.
Code 728.Subpart D and all applicable prohibitions set
forth in 35 Ill. Adm. Code 728.132, 728.139, or
Section 3004(d) of the Resource Conservation and
Recovery Act. I believe that the information I
submitted is true, accurate, and complete. I am aware
that there are significant penalties for submitting a
false certification, including the possibility of a
fine and imprisonment.
3)
If a generat or's waste is subject to an exemption from a
prohibition on the type of land disposal method utilized for
the waste (such as, but not limited to, a case-by-case
382
extension under Section 728.105, an exemption under Section
728.106, an extension under Section 728.101(c)(3), or a
nationwide capacity variance under 40 CFR 268.Subpart C
(199496)), the generator shall submit a
one-time written
notice with eachthe initial shipment of the waste to
theeach
facility receiving the generator's waste stating that the
waste is not prohibited from land disposal.
If the waste
changes, the generator shall send a new notice and
certification to the receiving facility, and place a copy in
its files. The notice must include the following
information:
A)
U.S. EPA hazardous waste number;
B)
The waste constituents that the treater will monitor,
if monitoring will not include all regulated
constituents, for wastes F001 through F005, F039,
D001, D002, D003, and D012 through D043. The
generator must also include whether the waste is a
nonwastewater or wastewater (as defined in Section
728.102 (d) and (f)) and indicate the subcategory of
the waste (such as "D003 reactive cyanide") if
applicable;
C)
The manifest number associated with the shipment
of waste;
D)
Waste analysis data, where available;
E)
For hazardous debris, when using the alternative
treatment technologies provided by Section 728.145:
i)
The contaminants subject to treatment, as
provided by Section 728.145(b);
ii)
An indication that these con
taminants are being
treated to comply with Section 728.145;
F)
For hazardous debris when using the treatment
standards for the contaminating waste(s) in Section
728.140: the requirements described in subsections
(a)(3)(A) through (a)(3)(D) above and subsection
(a)(3)(G) below; and,
G)
The date on which the waste is subject to the
prohibitions.
4)
If a generator is managing a prohibited waste in tanks,
containers, or containment buildings regulated under 35 Ill.
Adm. Code 722.134 and is treating such waste in tanks,
containers, or containment buildings to meet applicable
treatment standards under 728.Subpart D, the generator shall
develop and follow a written waste analysis plan that
describes the procedures the generator will carry out to
comply with the treatment standards. (A generator treating
hazardous debris under the alternative treatment standards
of Section 728.Table F, however, is not subject to these
waste analysis requirements.) The plan must be kept on-site
in the generator's records, and the following requirements
must be met:
383
A)
The waste analysis plan must be based on a detailed
chemical and physical analysis of a representative
sample of the prohibited wastes being treated, and it
must contain all information necessary to treat the
wastes in accordance with the requirements of this
Part, including the selected testing frequency.
B)
Such plan must be filed with the Agency a minimum of
30 days prior to the treatment activity, with delivery
verified.
C)
Wastes shipped off-
site pursuant to this subsection
must comply with the notification requirements of
Section 728.107(a)(2).
5)
If a generator determines whether the waste is restricted
based solely on the generator's knowledge of the waste, the
generator shall retain all supporting data used to make this
determination on-site in the generator's files. If a
generator determines whether the waste is restricted based
on testing the waste or an extract developed using the test
method described in Section 728.Appendix A, the generator
shall retain all waste analysis data on site in its files.
6)
If a generator determines, subsequent to the time of
generation, that it is managing a restricted waste that is
excluded from the definition of hazardous or solid waste or
exempt from regulation as a RCRA hazardous waste under 35
Ill. Adm. Code 721.102 through 721.106, the generator shall
place, in the facility's file, a one-time notice stating
such generation, the subsequent exclusion from the
definition of hazardous or solid waste or exemption from
regulation as a RCRA hazardous waste, and the disposition of
the waste.
7)
A generator shall retain on-site a copy of all notices,
certifications, demonstrations, waste analysis data, and
other documentation produced pursuant to this Section for at
least five years from the date that the waste that is the
subject of such documentation was last sent to on-site or
off-site treatment, storage, or disposal. The five year
record retention period is automatically extended during the
course of any unresolved enforcement action regarding the
regulated activity, or as requested by the Agency. The
requirements of this subsection apply to solid wastes even
when the hazardous characteristic is removed prior to
disposal, when the waste is excluded from the definition of
hazardous or solid waste under 35 Ill. Adm. Code 721.102
through 721.106, or when the waste is exempted from
regulation as a RCRA hazardous waste subsequent to the point
of generation.
8)
If a generator is managing a lab pack that
contains wastes
identified in Section 728.Appendix D and wishes to use the
alternative treatment standard under Section 728.142(c),
with each shipment of waste the generator shall submit a
notice to the treatment facility in accordance with
subsection (a)(1) above, except that underlying hazardous
constituents need not be determined. The generator shall
also comply with the requirements in subsections (a)(5) and
(a)(6) above and shall submit the following certification,
384
which must be signed by an authorized representative:
I certify under penalty of law that I personally have
examined and am familiar with the waste and that the lab
pack does not contain any of the wastes identified in 35
Ill. Adm. Code 728.Appendix D. I am aware that there are
significant penalties for submitting a false certification,
including the possibility of fine or imprisonment.
9)
This subsection corresponds with 40 CFR 268.7(a)(9), marked
"reserved" by U .S. EPA at 59 Fed. Reg. 48045 (Sept. 19,
1994). This statement maintains structural consistency with
federal regulations.
10)
Small quantity generators with tolling agreements pursuant
to 35 Ill. Adm. Code 722.120(e) shall comply with the
applicable notification and certification requirements of
subsection (a) above for the initial shipment of the waste
subject to the agreement. Such generators shall retain on-
site a copy of the notification and certification, together
with the tolling agreement, for at least three years after
termination or expiration of the agreement. The three-year
record retention period is automatically extended following
notification pursuant to Section 31(d) of the Environmental
Protection Act until either any subsequent enforcement
action is resolved or until the Agency notifies the
generator documents need not be retained.
b)
Treatment facilities shall test their wastes according to the
frequency specified in their waste analysis plans, as required by
35 Ill. Adm. Code 724.113 or 725.113. Such testing must be
performed as provided in subsections (b)(1), (b)(2), and (b)(3)
below.
1)
For wastes with treatment standards expressed as
concentrations in the waste extract (Section 728.141), the
owner or operator of the treatment facility shall test the
treatment residues or an extract of such residues developed
using the test method described in Section 728.Appendix A to
assure that the treatment residues or extract meet the
applicable treatment standards.
2)
For wastes prohibited under Section 728.132 or 728.139 that
are not subject to any treatment standards under 728.Subpart
D, the owner or operator of the treatment facility shall
test the treatment residues according to the generator
testing requirements specified in Section 728.132 to assure
that the treatment residues comply with the applicable
prohibitions.
3)
For wastes with treatment standards expressed as
concentrations in the waste (Section 728.143), the owner or
operator of the treatment facility shall test the treatment
residues (not an extract of such residues) to assure that
the treatment residues meet the applicable treatment
standards.
4)
A notice must be sent with
eachthe initial waste shipment to
theeach land disposal facility that includes the following
information, except that debris excluded from the definition
of the hazardous waste under 35 Ill. Adm. Code 721.103(e)
385
(i.e., debris treated by an extraction or destruction
technology provided by Section 728.Table F, and debris that
is delisted) is subject to the notififcation and
certification requirments of subsection (d) below rather
than these notification requirments
:. No further
notification is necessary until such time that the waste or
receiving facility change, in which case a new notice must
be sent and a copy placed in the treatment facility's file.
A)
U.S. EPA hazardous waste number;
B)
The waste constituents that the treater will monitor,
if monitoring will not include all regulated
constituents, for wastes F001 through F005, F039,
D001, D002, D003, and D012 through D043
, and wastes
prohibited pursuant to Section 728.132 or Section
3004(d) of the Resource Conservation and Recovery Act,
referenced in Section 728.139
. The generator must
also include whether the waste is a nonwastewater or
wastewater (as defined in Section 728.102 (d) and (f))
and indicate the subcategory of the waste (such as
"D003 reactive cyanide
") if applicable;
C)
The manifest number associated with the shipment of
waste; and
D)
Waste analysis data, where available.
5)
The treatment facility owner or operator shall submit a
certification with each shipment of waste or treatment
residue of a restricted waste to the land disposal facility
stating that the waste or treatment residue has been treated
in compliance with the treatment standards specified in
728.Subpart D and the applicable prohibitions set forth in
Section 728.132 or 728.139. Debris excluded from the
definiton of hazardous waste under 35 Ill. Adm. Code
721.103(e) (i.e., debris treated by an extraction or
destruction technology provided by Section 728.Table F, and
debris that is delisted), however, is subject to the
notififcation and certication requirements of subsection (d)
below rather than the certification requirements of this
subsection.
A)
For wastes with treatment standards expressed as
concentrations in the waste extract or in the waste
(Sections 728.141 or 728.143), or for wastes
prohibited under Section 728.132 or 728.139 that are
not subject to any treatment standards under
728.Subpart D, the certification must be signed by an
authorized representative and must state the
following:
I certify under penalty of law that I have
personally examined and am familiar with the
treatment technology and operation of the
treatment process used to support this
certification and that, based on my inquiry of
those individuals immediately responsible for
obtaining this information, I believe that the
treatment process has been operated and
maintained properly, so as to comply with the
386
performance levels specified in 35 Ill. Adm.
Code 728.Subpart D and all applicable
prohibitions set forth in 35 Ill. Adm. Code
728.132 or 728.139 or Section 3004(d) of the
Resource Conservation and Recovery Act without
impermissible dilution of the prohibited waste.
I am aware that there are significant penalties
for submitting a false certification, including
the possibility of fine and imprisonment.
B)
For wastes with treatment standards expressed as
technologies (Section 728.142), the certification must
be signed by an authorized representative and must
state the following:
I certify under penalty of law that the waste
has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.142. I am
aware that there are significant penalties for
submitting a false certification, including the
possibility of fine and imprisonment.
C)
For wastes with treatment standards expressed as
concentrations in the waste pursuant to Section
728.143, if compliance with the treatment standards in
728.Subpart D is based in part or in whole on the
analytical detection limit alternative specified in
Section 728.143(c), the certification also must state
the following:
I certify under penalty of law that I have
personally examined and am familiar with the
treatment technology and operation of the
treatment process used to support this
certification and that, based on my inquiry of
those individuals immediately responsible for
obtaining this information, I believe that the
nonwastewater organic constituents have been
treated by incineration in units operated in
accordance with 35 Ill. Adm. Code 724.Subpart O
or 35 Ill. Adm. Code 725.Subpart O, or by
combustion in fuel substitution units operating
in accordance with applicable technical
requirements, and I have been unable to detect
the nonwastewater organic constituents despite
having used best good faith efforts to analyze
for such constituents. I am aware that there
are significant penalties for submitting a false
certification, including the possibility of fine
and imprisonment.
D)
For characteristic wastes D001, D002,
D003, and D012
through D043 that are subject to the treatment
standards in Section 728.140 (other than those
expressed as a required method of treatment), that are
reasonably expected to contain underlying hazardous
constituents (as defined in Section 728.102(i)
), that
are treated on-site to remove the hazardous
characteristic, and that are then sent off-site for
treatment of underlying hazardous constituents, the
certification must state the following:
387
I certify under penalty of law that the waste
has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.140 to
remove the hazardous characteristic. This
decharacterized waste contains underlying
hazardous constituents that require further
treatment to meet universal treatment standards.
I am aware that there are significant penalties
for submitting a false certification, including
the possibility of fine and imprisonment.
E)
For characteristic wastes D001, D002, D003, and D012
through D043 that contain underlying hazardous
constituents, as defined in Section 728.102(i), and
which are treated on-site to remove the hazardous
characteristic and to treat underlying hazardous
constituents to levels set forth in the Sections
728.148 and 728.Table U Universal Treatment Standards,
the certification must state the following:
I certify under penalty of law that the waste
has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.140 to
remove the hazardous characteristic, and that
underlying hazardous constituents, as defined in
Section 728.102, have been treated on-site to
meet the Sections 728.148 and 728.Table U
Universal Treatment Standards. I am aware that
there are significant penalties for submitting a
false certification, including the possibility
of fine and imprisonment.
6)
If the waste or treatment residue will be further managed at
a different treatment or storage facility, the treatment,
storage, or disposal facility sending the waste or treatment
residue off-site must comply with the notice and
certification requirements applicable to generators under
this Section.
7)
Where the wastes are recyclable materials used in a manner
constituting disposal subject to the provisions of 35 Ill.
Adm. Code 726.120(b), regarding treatment standards and
prohibition levels, the owner or operator of a treatment
facility (i.e. the recycler) is not required to notify the
receiving facility pursuant to subsection (b)(4) above.
With each shipment of such wastes the owner or operator of
the recycling facility shall submit a certification
described in subsection (b)(5) above and a notice that
includes the information listed in subsection (b)(4) above
(except the manifest number) to the Agency. The recycling
facility also shall keep records of the name and location of
each entity receiving the hazardous waste-derived product.
c)
Except where the owner or operator is disposing of any waste that
is a recyclable material used in a manner constituting disposal
pursuant to 35 Ill. Adm. Code 726.120(b), the owner or operator of
any land disposal facility disposing any waste subject to
restrictions under this Part shall:
1)
Have copies of the notice and certification specified in
388
subsection (a) or (b) above and the certification specified
in Section 728.108, if applicable.
2)
Test the waste, or an extract of the waste or treatment
residue developed using the test method described in Section
728.Appendix A or using any methods required by generators
under Section 728.132, to assure that the waste or treatment
residue is in compliance with the applicable treatment
standards set forth in 728.Subpart D and all applicable
prohibitions set forth in Sections 728.132 or 728.139. Such
testing must be performed according to the frequency
specified in the facility's waste analysis plan as required
by 35 Ill. Adm. Code 724.113 or 725.113.
3)
Where the owner or operator is disposing of any waste that
is subject to the prohibitions under Section 728.133(f) but
not subject to the prohibitions set forth in Section
728.132, the owner or operator shall ensure that such waste
is the subject of a certification according to the
requirements of Section 728.108 prior to disposal in a
landfill or surface impoundment unit, and that such disposal
is in accordance with the requirements of Section
728.105(h)(2). The same requirement applies to any waste
that is subject to the prohibitions under Section 728.133(f)
and also is subject to the statutory prohibitions in the
codified prohibitions in Section 728.139 or Section 728.132.
4)
Where the owner or oper
ator is disposing of any waste that
is a recyclable material used in a manner constituting
disposal subject to the provisions of 35 Ill. Adm. Code
726.120(b), the owner or operator is not subject to
subsections (c)(1) through (c)(3) above with respect to such
waste.
d)
A generator or treater that first claims that hazardous debris is
excluded from the definition of hazardous waste under 35 Ill. Adm.
Code 721.103(e) (i.e., debris treated by an extraction or
destruction technology provided by Section 728.Table F, and debris
that has been delisted) is subject to the following notification
and certification requirements:
1)
A one-time notification must be submitted to the Agency
including the following information:
A)
The name and address of the RCRA Subtitle D (municipal
solid waste landfill) facility receiving the treated
debris;
B)
A description of the hazardous debris as initially
generated, including the applicable U
.S. EPA hazardous
waste numbers; and
C)
For debris excluded under 35 Ill. Ad
m. Code
728.103(f)(2) 721.103(e)(1) , the technology from
Section 728.Table F used to treat the debris.
2)
The notification must be updated if the debris is shipped to
a different facility and, for debris excluded 35 Ill. Adm.
Code 721.2(d)(1), if a different type of debris is treated
or if a different technology is used to treat the debris.
389
3)
For debris excluded under 35 Ill. Adm. Code
728.103(f)(2) 721.103(e)(1) , the owner or operator of the
treatment facility shall document and certify compliance
with the treatment standards of Section 728.Table F, as
follows:
A)
Records must be kept of all inspections, evaluations,
and analyses of treated debris that are made to
determine compliance with the treatment standards;
B)
Records must be kept of any data or information the
treater obtains during treatment of the debris that
identifies key operating parameters of the treatment
unit; and
C)
For each shipment of treated debris, a certification
of compliance with the treatment standards must be
signed by an authorized representative and placed in
the facility's files. The certification must state
the following: "I certify under penalty of law that
the debris has been treated in accordance with the
requirements of 35 Ill. Adm. Code 728.145. I am aware
that there are significant penalties for making a
false certification, including the possibility of fine
and imprisonment."
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.109
Special Rules for Characteristic Wa
stes
a)
The initial generator of a solid waste shall determine each U
.S.
EPA hazardous waste number (waste code) applicable to the waste in
order to determine the applicable treatment standards under
728.Subpart D. For purposes of this Part, the waste must carry
the waste code for any applicable listing under 35 Ill. Adm. Code
721.Subpart D. In addition, the waste must carry one or more of
the waste codes under 35 Ill. Adm. Code 721.Subpart C where the
waste exhibits a characteristic, except in the case when the
treatment standard for the waste code listed in 35 Ill. Adm. Code
721.Subpart D operates in lieu of the standard for the waste code
under 35 Ill. Adm. Code 721.Subpart C, as specified in subsection
(b) below. If the generator determines that its waste displays
thea characteristic of
ignitability (D001)
hazardous waste (and the
waste is not in the a D004 through D011 waste, a
High TOC Ignitable
Liquids Subcategory
D001 waste, orand is not treated by CMBST or
RORGS, as described in Section 728.Table C
), that its waste
displays the characteristic of corrosivity (D002) and is
prohibited under Section 728.137, or that its waste displays the
characteristic of toxicity (D012 through D043) and is prohibited
under Section 728.138,
the generator shall determine what
underlying hazardous constituents (as defined in Section 728.102)
are reasonably expected to be present
in the D001, D002, or D012
through D043 waste
above the universal treatment standards set
forth in Sections 728.148 and 728.Table U
.
b)
Where a prohibited waste is both listed under 35 Ill. Adm. Code
721.Subpart D and exhibits a characteristic under 35 Ill. Adm.
Code 721.Subpart C, the treatment standard for the waste code
listed in 35 Ill. Adm. Code 721.Subpart D will operate in lieu of
the standard for the waste code under 35 Ill. Adm. Code
721.Subpart C, provided that the treatment standard for the listed
390
waste includes a treatment standard for the constituent that
causes the waste to exhibit the characteristic. Otherwise, the
waste must meet the treatment standards for all applicable listed
and characteristic waste codes.
c)
In addition to any applicable standards determined from the
initial point of generation, no prohibited waste that exhibits a
characteristic under 35 Ill. Adm. Code 721.Subpart C shall be land
disposed unless the waste complies with the treatment standards
under 728.Subpart D.
d)
A waste s that exhibits a characteristic is also subject to Section
728.107 requirements, except that once the waste is no longer
hazardous, a one time one-time notification and certification must
be placed in the generator's or treater's files and sent to the
Agency , except for those facilities described in subsection (f)
below. The notification and certification that is placed in the
generator's or treater's files must be updated if the process or
operation generating the waste changes or if the subtitle D
facility receiving the waste changes. However, the generator or
treater need only notify the Agency on an annual basis if such
changes occur. Such notification and certification should be sent
to the Agency by the end of the year, but no later than December
31.
1)
The notification must include the following information:
A) TFor a characteristic waste other than one managed on
site in a wastewater treatment system subject to the
federal Clean Water Act (CWA), a zero-discharger
engaged in CWA-equivalent treatment, or a Class I
nonhazardous waste injection well, t
he name and
address of the RCRA Subtitle D (municipal solid waste
landfill) facility receiving the waste shipment; and
B) AFor a waste that exhibits a characteristic of
hazardous waste, a
description of the waste as
initially generated, including the applicable U
.S. EPA
hazardous waste numbers, the treatability group(s),
and the underlying hazardous constituents
(as defined
in Section 728.102(i)) in D001 and D002 wastes
prohibited under Section 728.137 or D012 through D043
wastes prohibited under Section 728.138
.
2)
The certification must be signed by an authorized
representative and must state the language found in Section
728.107(b)(5)(A). If treatment removes the characteristic
but does not treat underlying hazardous constituents, then
the certification found in Section 728.107(b)(5)(D) applies.
3)
For a characteristic waste whose ultimate disposal will be
into a Class I nonhazardous waste injection well, and for
which compliance with the treatment standards set forth in
Sections 728.148 and 728.Table U for underlying hazardous
constituents is achieved through pollution prevention that
meets the criteria set forth at 35 Ill. Adm. Code
738.101(d), the following information must also be included:
A)
A description of the pollution prevention mechanism
and when it was implemented if already complete;
391
B)
The mass of each underlying hazardous constituent
before pollution prevention;
C)
The mass of each underlying hazardous constituent that
must be removed, adjusted to reflect variations in
mass due to normal operating conditions; and
D)
The mass reduction of each underlying hazardous
constituent that is achieved.
e)
For a decharacterized waste managed on-site in a wastewater
treatment system subject to the federal Clean Water Act (CWA) or
zero-dischargers engaged in CWA-equivalent treatment, compliance
with the treatment standards set forth in Sections 728.148 and
728.Table D must be monitored quarterly, unless the treatment is
aggressive biological treatment, in which case compliance must be
monitored annually. Monitoring results must be kept in on-site
files for 5 years.
f)
For a decharacterized waste managed on-site in a wastewater
treatment system subject to the federal Clean Water Act (CWA) for
which all underlying hazardous constituents (as defined in Section
728.102) are addressed by a CWA permit, this compliance must be
documented and this documentation must be kept in on-site files.
g)
For a characteristic waste whose ultimate disposal will be into a
Class I nonhazardous waste injection well that qualifies for the
de minimis exclusion described in Section 728.101, information
supporting that qualification must be kept in on-site files.
(Source: Amended at 19 Ill. Reg. 9660, effective June 27, 1995)
SUBPART B: SCHEDULE FOR LAND DISPOSAL PROHIBITION
AND ESTABLISHMENT OF TREATMENT STANDARDS
Section 728.110
First Third (Repealed)
The Board incorporates by reference 40 CFR 268.10 (1991). This Section
incorporates no later editions or amendments.
(Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
Section 728.111
Second Thi rd (Repealed)
The Board incorporates by reference 40 CFR 268.11 (1991). This Section
incorporates no later editions or amendments.
(Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
Section 728.112
Third Third (Repealed)
The Board incorporates by reference 40 CFR 268.12 (1991). This Section
incorporates no later editions or amendments.
(Source: Repealed at 21 Ill. Reg. ________, effective ____________________)
SUBPART C: PROHIBITION ON LAND DISPOSAL
Section 728.139 Statutory Prohibitions
Waste-Specific Prohibitions: End-of-
392
pipe CWA, CWA-Equivalent, and Class I Nonhazardous Waste
Injection Well Treatment Standards; Spent Aluminum
Potliners; and Carbamate Wastes
No person shall cause, threaten or allow the land disposal of any waste in
violation of Section 3004 of the Resource Conservation and Recovery Act,
incorporated by reference in 35 Ill. Adm. Code 720.111.
a)
The wastes specified in 35 Ill. Adm. Code 721.132 as EPA Hazardous
Waste numbers K156-K159; and in 35 Ill. Adm. Code 721.133 as USEPA
hazardous waste numbers P127, P128, P185, P188 through P192, P194,
P196 through P199, P201 through P205, U271, U278 through U280,
U364, U367, U372, U373, U387, U389, 394, U395, U404, and U409
through U411 are prohibited from land disposal. In addition, soil
and debris contaminated with these wastes are prohibited from land
disposal.
b)
The wastes identified in 35 Ill. Adm. Code 721.123 as USEPA
hazardous waste number D003 are prohibited from land disposal,
other than those that are managed in a system whose discharge is
regulated under 35 Ill. Adm. Code:Subtitle C, one that injects
hazardous waste in Class I waste injection well regulated under 35
Ill. Adm. Code 702, 704, and 730, or one that is a zero discharger
that engages in federal Clean Water Act (CWA)-equivalent treatment
before ultimate land disposal. This prohibition does not apply to
unexploded ordnance and other explosive devices that have been the
subject of an emergency response. (Such D003 wastes are
prohibited unless they meet the treatment standard of DEACT before
land disposal (see Section 728.140)).
c)
The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA
hazardous waste number K088 are prohibited from land disposal. In
addition, soil and debris contaminated with these wastes are
prohibited from land disposal.
d)
Effective April 8, 1998, radioactive wastes mixed with waste
designated by any of USEPA hazardous waste numbers K088, K156
through K159, K161, P127, P128, P185, P188 through P192, P194,
P196 through P199, P201 through P205, U271, U278 through U280,
U364, U367, U372, U373, U387, U389, U394, U395, U404, and U409
through U411 are prohibited from land disposal. In addition, soil
and debris contaminated with these radioactive mixed wastes are
prohibited from land disposal.
e)
Until April 8, 1998, the wastes included in subsections (a), (b),
(c), and (d) above may be disposed in a landfill or surface
impoundment only if such unit complies with the requirements of
Section 728.105(h)(2).
f)
The requirements of subsections (a), (b), (c), and (d) of this
Section do not apply if:
1)
The wastes meet the applicable treatment standards specified
in 728.Subpart D;
2)
The person conducting the disposal has been granted an
exemption from a prohibition under a petition pursuant to
Section 728.106, with respect to those wastes and units
covered by the petition;
3)
The wastes meet the applicable alternative treatment
393
standards established pursuant to a petition granted under
Section 728.144; or
4)
The person conducting the disposal has been granted an
extension to the effective date of a prohibition pursuant to
Section 728.105, with respect to those wastes covered by the
extension.
g)
To determine whether a hazardous waste identified in this Section
exceeds the applicable treatment standards set forth in Section
728.140, the initial generator must test a sample of the waste
extract or the entire waste, depending on whether the treatment
standards are expressed as concentrations in the waste extract or
in the waste, or the generator may use knowledge of the waste. If
a waste contains constituents in excess of the applicable
728.Subpart D levels, the waste is prohibited from land disposal
and all requirements of this Part are applicable to the waste,
except as otherwise specified.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART D: TREATMENT STANDARDS
Section 728.140
Applicability of Treatment Standards
a)
A prohibited waste identified in Section 728.Table T, "Treatment
Standards for Hazardous Wastes", may be land disposed only if it
meets the requirements found in that Section. For each waste,
Section 728.Table T identifies one of three types of treatment
standard requirements:
1)
All hazardous constituents in the waste or in the treatment
residue must be at or below the values found in that Section
for that waste ("total waste standards");
2)
The hazardous constituents in the extract of the waste or in
the extract of the treatment residue must be at or below the
values found in that Section ("waste extract standards"); or
3)
The waste must be treated using the technology specified in
that Section ("technology standard"), which is described in
detail in Section 728.Table C, "Technology Codes and
Description of Technology-Based Standards".
b)
For wastewaters, compliance with concentration level standards is
based on maximums for any one day, except for D004 through D011
wastes for which the previously promulgated treatment standards
based on grab samples remain in effect. For all nonwastewaters,
compliance with concentration level standards is based on grab
sampling. For wastes covered by the waste extract standards, the
test Method 1311, the Toxicity Characteristic Leaching Procedure,
found in "Test Methods for Evaluating Solid Waste,
Physical/Chemical Methods", U
.S. EPA Publication SW-846,
incorporated by reference in Section 720.111, must be used to
measure compliance. An exception is made for D004 and D008, for
which either of two test methods may be used: Method 1311 or
Method 1310, the Extraction Procedure Toxicity Test, found in
"Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods", U .S. EPA Publication SW-846, incorporated by reference
in Section 720.111. For wastes covered by a technology standard,
394
the wastes may be land disposed after being treated using that
specified technology or an equivalent treatment technology
approved by the Agency pursuant to Section 728.142(b).
c)
When wastes with differing treatment standards for
a constituent
of concern are combined for purposes of treatment, the treatment
residue must meet the lowest treatment standard for the
constituent of concern.
d)
Notwithstanding the prohibitions specified in subsection (a)
above, treatment and disposal facilities may demonstrate (and
certify pursuant to 35 Ill. Adm. Code 728.107(b)(5)) compliance
with the treatment standards for organic constituents specified by
a footnote in Section 728.Table T, provided the following
conditions are satisfied:
1)
The treatment standards for the organic constituents were
established based on incineration in units operated in
accordance with the technical requirements of 35 Ill. Adm.
Code 724.Subpart O, or based on combustion in fuel
substitution units operating in accordance with applicable
technical requirements;
2)
The treatment or disposal facility has used the methods
referenced in subsection (d)(1) above to treat the organic
constituents; and
3)
The treatment or disposal facility may demonstrate
compliance with organic constituents if good-faith
analytical efforts achieve detection limits for the
regulated organic constituents that do not exceed the
treatment standards specified in this Section and Section
728.Table T by an order of magnitude.
e)
For characteristic wastes (U
.S. EPA hazardous waste numbers D001
,
D002, and D012 through D003 and D018 through
D043) that are
subject to treatment standards
set forth in Section 728.Table T,
"Treatment Standards for Hazardous Wastes", all underlying
hazardous constituents (as defined in Section 728.102(i)) must
meet the universal treatment standards,
foundset forth in Section s
728.148 and 728.Table U prior to land disposal
, as defined in
Section 728.102(c)
.
f)
The treatment standards for U
.S. EPA hazardous waste numbers F001
through F005 nonwastewater constituents carbon disulfide,
cyclohexanone, or methanol apply to wastes that contain only one,
two, or three of these constituents. Compliance is measured for
these constituents in the waste extract from test Method 1311, the
Toxicity Characteristic Leaching Procedure found in "Test Methods
for Evaluating Solid Waste, Physical/Chemical Methods", U
.S. EPA
Publication SW-846, incorporated by reference in Section 720.111.
If the waste contains any of these three constituents along with
any of the other 25 constituents found in U
.S. EPA hazardous waste
numbers F001 through F005, then compliance with treatment
standards for carbon disulfide, cyclohexanone, or methanol are not
required.
g)
This subsection corresponds with 40 CFR 268.40(g), added at 61
Fed. Reg. 43927 (Aug. 26, 1996), which has expired. This
statement maintains structural consistency with the federal rules.
395
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.144
Adjustment of Treatment Standard
a)
Where the treatment standard is expressed as a concentration in a
waste or waste extract and a waste cannot be treated to the
specified level, or where the treatment technology is not
appropriate to the waste, the generator or treatment facility may
petition to the Board for an adjusted treatment standard. As
justification, the petitioner shall demonstrate that, because the
physical or chemical properties of the waste differ significantly
from wastes analyzed in developing the treatment standard, the
waste cannot be treated to specified level or by the specified
methods.
BOARD NOTE: 40 CFR 268.44 refers to these as "treat
ability
variances". The Board has not used this term in its rules to
avoid confusion with the Board variances under Title IX of the
Environmental Protection Act. The equivalent Board procedures are
an "adjusted treatment standard" pursuant to sub
sections (a)
through (l), or a "treatability exception" adopted pursuant to
subsections (m) et seq. While the latter is adopted by "identical
in substance" rulemaking following a USEPA action, the former is
an original Board action which will be the only mechanism
following authorization to the State of this component of the RCRA
program.
b)
Each petition mu st be submitted in accordance with the procedures
in 35 Ill. Adm. Code 106.Subpart G.
c)
Each petition must include the following statement signed by the
petitioner or an authorized representative:
I certify under penalty of law that I have personally
examined and am familiar with the information submitted in
this petition and all attached documents, and that, based on
my inquiry of those individuals immediately responsible for
obtaining the information, I believe that the submitted
information is true, accurate and complete. I am aware that
there are significant penalties for submitting false
information, including the possibility of fine and
imprisonment.
d)
After receiving a petition for an adjusted treatment standard, the
Board may request any additional information or samples which are
necessary to evaluate the petition.
e)
The Board will give public notice and provide an opportunity for
public comment, as provided in 35 Ill. Adm. Code 106. In
conjunction with any updating of the RCRA regulations, the Board
will maintain, in this Part, a listing of all adjusted treatment
standards granted by the Board pursuant to this Section. A
LISTING OF ALL ADJUSTED STANDARDS GRANTED PURSUANT TO THIS SECTION
WILL BE PUBLISHED IN THE ILLINOIS REGISTER AND ENVIRONMENTAL
REGISTER AT THE END OF EACH FISCAL YEAR. (Section 28.1(d)(3) of
the Environmental Protection Act.)
f)
A generator, treatment facility or disposal facility that is
managing a waste covered by an adjusted treatment standard shall
comply with the waste analysis requirements for restricted wastes
found under Section 728.107.
396
g)
During the petition review process, the applicant is required to
comply with all restrictions on land disposal under this Part once
the effective date for the waste has been reached.
h)
Where the treatment standard is expressed as a concentration in a
waste or waste extract and a waste generated under conditions
specific to only one site cannot be treated to the specified
level, or where treatment technology is not appropriate to the
waste, the generator or treatment facility may petition the Board
for a site-specific adjusted treatment standard. The petitioner
shall demonstrate that, because the physical or chemical
properties of the waste differs significantly from the waste
analyzed in developing the treatment standard, the waste cannot be
treated to specified levels or by the specified methods.
i)
Each petition for a site-specific adjusted treatment standard must
include the information in 35 Ill. Adm. Code 720.120(b)(1) through
(4).
j)
After receiving a petition for a site-specific adjusted treatment
standard, the Board may request any additional information or
samples which the Board determines are necessary to evaluate the
petition.
k)
A generator, treatment facility or disposal facility which is
managing a waste covered by a site-specific adjusted treatment
standard shall comply with the waste analysis requirements for
restricted wastes in Section 728.107.
l)
During the petition review process, the petitio
ner for a site-
specific adjusted treatment standard shall comply with all
restrictions on land disposal under this Part once the effective
date for the waste has been reached.
m)
If USEPA grants a treatability exception by regulatory action
pursuant to 40 CFR 268.44 (19
9196) and a person demonstrates that
the treatability exception needs to be adopted as part of the
Illinois RCRA program because the waste is generated or managed in
Illinois, the Board will adopt the treatability exception by
identical in substance rulemaking pursuant to Section 22.4(a) of
the Environmental Protection Act.
BOARD NOTE: The Board will adopt the treatability exception
during a RCRA update Docket if a timely demonstration is made.
Otherwise, the Board will assign the matter to a separate Docket.
o)
The facilities listed in Table H are excluded from the treatment
standard under Section 728.143(a) and Table B, and are subject to
the constituent concentrations listed in Table H.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.148
Universal Treatment Standards
Section 728.Table U, "Universal Treatment Standards (UTS)", identifies the
hazardous constituents, along with the nonwastewater and wastewater treatment
standard levels, that are used to regulate most prohibited hazardous wastes
with numerical limits. For determining compliance with treatment standards
for underlying hazardous constituents, as defined in Section 728.102(i), these
treatment standards may not be exceeded. Compliance with these treatment
397
standards is measured by an analysis of grab samples, unless otherwise noted
in Section 728.Table U.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.Appendix K
Metal Bearing Wastes Prohibited From Dilution in a
Combustion Unit According to Section 728.103(c)
BOARD NOTE: A combustion unit is defined as any thermal technology subject to
35 Ill. Adm. Code 724.Subpart O, 725.Subpart O, or 726.Subpart H.
Waste code
Waste description
D004
Toxicity Characteristic for Arsenic.
D005
Toxicity Characteristic for Barium.
D006
Toxicity Characteristic for Cadmium.
D007
Toxicity Characteristic for Chromium.
D008
Toxicity Characteristic for Lead.
D009
Toxicity Characteristic for Mercury.
D010
Toxicity Characteristic for Selenium.
D011
Toxicity Characteristic for Silver.
F006
Wastewater treatment sludges from electroplating operations except
from the following processes: (1) sulfuric acid anodizing of
aluminum; (2) tin plating carbon steel; (3) zinc plating basis) on
carbon steel; (4) aluminum or zinc
-plating on carbon steel; (5)
cleaning/stripping associated with tin, zinc and aluminum plating
on carbon steel; and (6) chemical etching and milling of aluminum.
F007
Spent cyanide plating bath solutions from electroplating
operations.
F008
Plating bath residues from the bottom of plating baths from
electroplating operations where cyanides are used in the process.
F009
Spent stripping and cleaning bath solutions from electroplating
operations where cyanides are used in the process.
F010
Quenching bath residues from oil baths from metal treating
operations where cyanides are used in the process.
F011
Spent cyanide solutions from salt bath pot cleaning from metal
heat treating operations.
F012
Quenching waste water treatment sludges from metal heat treating
operations where cyanides are used in the process.
F019
Wastewater treatment sludges from the chemical conversion coating
of aluminum except from zirconium phosphating in aluminum car
washing when such phosphating is an exclusive conversion coating
process.
K002
Wastewater treatment sludge from the production of chrome yellow
398
and orange pigments.
K003
Wastewater treatment sludge from the production of molybdate
orange pigments.
K004
Wastewater treatment sludge from the production of zinc yellow
pigments.
K005
Wastewater treatment sludge from the production of chrome green
pigments.
K006
Wastewater treatment sludge from the production of chrome oxide
green pigments (anhydrous and hydrated).
K007
Wastewater treatment sludge from the production of iron blue
pigments.
K008
Oven residue from the production of chrome oxide green pigments.
K061
Emission control dust/sludge from the primary production of steel
in electric furnaces.
K069
Emission control dust/sludge from secondary lead smelting.
K071
Brine purification muds from the mercury cell processes in
chlorine production, where separately prepurified brine is not
used.
K100
Waste leaching solution from acid leaching of emission control
dust/sludge from secondary lead smelting.
K106
Sludges from the mercury cell processes for making chlorine.
P010
Arsenic acid H
3
AsO
4
.
P011
Arsenic oxide As
2
O
5
.
P012
Arsenic trioxide.
P013
Barium cyanide.
P015
Beryllium.
P029
Copper (I) cyanide Cu(CN).
P074
Nickel (II) cyanide Ni(CN)
2
.
P087
Osmium (VIII) tetroxide OsO
4
.
P099
Potassium silver cyanide KAg(CN)
2
.
P104
Silver cyanide AgCN.
P113
Thallic (III) oxide Tl
2
O
3
.
P114
Thallium (I) selenite Tl
2
SeO
3
.
P115
Thallium (I) sulfate Tl
2
SO
4
.
P119
Ammonium (V) vanadate NH
3
VO
3
.
399
P120
Vanadium (V) oxide V
2
O
5
.
P121
Zinc cyanide ZnCN.
U032
Calcium chromate CaCrO
4
.
U145
Lead phosphate.
U151
Mercury.
U204
Selenous acid H
2
SeO
3
.
U205
Selenium (IV) disulfide SeS
2
.
U216
Thallium (I) chloride TlCl.
U217
Thallium (I) nitrate TlNO
3
.
(Source: Added at 21 Ill. Reg. ________, effective ____________________)
Section 728.Table C
Technology Codes and Description of Technology-Based
Standards
Technology
code
Description of technology-based standard
ADGAS
Ventin g of compressed gases into an absorbing or reacting media (i.e.,
solid or liquid)--venting can be accomplished through physical release
utilizing valves or piping; physical penetration of the container; or
penetration through detonation.
AMLGM
Amalgamation of liquid, elemental mercury contaminated with radioactive
materials utilizing inorganic reagents such as copper, zinc, nickel,
gold, and sulfur that result in a nonliquid, semi-solid amalgam and
thereby reducing potential emissions of elemental mercury vapors to the
air.
BIODG
Biodegradation of organics or non-metallic inorganics (i.e., degradable
inorganics that contain the elements of phosphorus, nitrogen, and
sulfur) in units operated under either aerobic or anaerobic conditions
such that a surrogate compound or indicator parameter has been substan
-
tially reduced in concentration in the residuals (e.g., total organic
carbon (TOC) can often be used as an indicator parameter for the
biodegrada tion of many organic constituents that cannot be directly
analyzed in wastewater residues).
CARBN
Carbon adsorption (granulated or powdered) of non-metallic inorganics,
organo-metallics, or organic constituents, operated so that a surrogate
compound or indicator parameter has not undergone break
through (e.g.,
total organic carbon (TOC) can often be used as an indicator parameter
for the adsorption of many organic constituents that cannot be directly
analyzed in wastewater residues). Breakthrough occurs when the carbon
has become saturated with the constituent (or indicator parameter) and
substantial change in adsorption rate associated with that constituent
occurs.
CHOXD
Chemical or electrolytic oxidation utilizing the following oxidation
reagents (or waste reagents) or combinations or reagents:
1)
hypochlorite (e.g., bleach);
400
2)
chlorine;
3)
chlorine dioxide;
4)
ozone or UV (ultraviolet light) assisted ozone;
5)
peroxides;
6)
persulfates;
7)
perchlorates;
8)
permangantes; or
9)
other oxidizing reagents of equivalent efficiency, performed in
units operated so that a surrogate compound or indicator parameter
has been substantially reduced in concentration in the residuals
(e.g., total organic carbon (TOC) can often be used as an
indicator parameter for the oxidation of many organic constit
uents
that cannot be directly analyzed in wastewater residues).
Chemical oxidation specifically includes what is commonly referred
to as alkaline chlorination.
CHRED
Chemical reduction utilizing the following reducing reagents (or waste
reagents) or combinations of reagents:
1)
sulfur dioxide;
2)
sodium, potassium, or alkali salts of sulfites, bisulfites,
metabisulfites, and polyethylene glycols (e.g., NaPEG and KPEG);
3)
sodium hydrosulfide;
4)
ferrous salts; or
5)
other reducing reagents of equivalent efficiency, performed in
units operated such that a surrogate compound or indicator
parameter has been substantially reduced in concentration in the
residuals (e.g., total organic halogens (TOX) can often be used as
an indicator parameter for the reduction of many halogenated
organic constituents that cannot be directly analyzed in
wastewater residues). Chemical reduction is commonly used for the
reduction of hexavalent chromium to the trivalent state.
CMBST
Combustion in incinerators, boilers, or industrial furnaces operated in
accordance with the applicable requirements of 35 Ill. Adm. Code
724.Subpart O, 725.Subpart O, or 35 Ill. Adm. Code 726.Subpart H.
DEACT
Deactivation to remove the hazardous characteristics of a waste due to
its ignitability, corrosivity, or reactivity.
FSUBS
Fuel substitution in units operated in accordance with applicable
technical operating requirements.
HLVIT
Vitrification of high level mixed radioactive wastes in units in
compliance with all applicable radioactive protection requirements under
control of the federal Nuclear Regulatory Commission.
IMERC
Incineration of wastes containing organics and mercury in units operated
in accordance with the technical operating requirements of 35 Ill. Adm.
Code 724.Subpart O or 725.Subpart O. All wastewater and nonwastewater
401
residues derived from this process must then comply with the
corresponding treatment standards per waste code with consideration of
any applicable subcategories (e.g., high or low mercury sub
categories).
INCIN
Incineration in units operated in accordance with the technical
operating requirements of 35 Ill. Adm. Code 724.Subpart O or 725.Subpart
O.
LLEXT
Liquid-liquid extraction (often referred to as solvent extraction) of
organics from liquid wastes into an immiscible solvent for which the
hazardous constituents have a greater solvent affinity, resulting in an
extract high in organics that must undergo either incineration, reuse as
a fuel, or other recovery or reuse and a raffinate (extracted liquid
waste) proportionately low in organics that must undergo further
treatment as specified in the standard.
MACRO
Macroencapsulation with surface coating materials such as polymeric
organics (e.g., resins and plastics) or with a jacket of inert inorganic
materials to substantially reduce surface exposure to potential leaching
media. Macroencapsulation specifically does not include any material
that would be classified as a tank or container according to 35 Ill.
Adm. Code 720.110.
NEUTR
Neutralization with the following reagents (or waste reagents) or
combinations of reagents:
1)
acids;
2)
bases; or
3)
water (including wastewaters) resulting in a pH greater than 2 but
less than 12.5 as measured in the aqueous residuals.
NLDBR
No land disposal based on recycling.
PRECP
Chemical precipitation of metals and other inorganics as insoluble
precipitates of oxides, hydroxides, carbonates, sulfides, sulfates,
chlorides, fluorides, or phosphates. The following reagents (or waste
reagents) are typically used alone or in combination:
1)
lime (i.e., containing oxides or hydroxides of calcium or
magnesium;
2)
caustic (i.e., sodium or potassium hydroxides;
3)
soda ash (i.e., sodium carbonate);
4)
sodium sulfide;
5)
ferric sulfate or ferric chloride;
6)
alum; or
7)
sodium sulfate. Additional flocculating, coagulation, or similar
reagents or processes that enhance sludge dewatering
characteristics are not precluded from use.
RBERY
Thermal recovery of beryllium.
RCGAS
Recovery or reuse of compressed gases including techniques such as
reprocessing of the gases for reuse or resale; filtering or adsorption
402
of impurities; remixing for direct reuse or resale; and use of the gas
as a fuel source.
RCORR
Recovery of acids or bases utilizing one or more of the following
recovery technologies:
1)
distillation (i.e., thermal concentration);
2)
ion exchange;
3)
resin or solid adsorption;
4)
reverse osmosis; or
5)
incineration for the recovery of acid
--
Note: this does not preclude the use of other physical phase
separation or concentra
tion techniques such as decantation,
filtration (including ultrafiltration), and centrifugation, when
used in conjunction with the above listed recovery technologies.
RLEAD
Thermal recovery of lead in secondary lead smelters.
RMERC
Retorting or roasting in a thermal processing unit capable of volatiliz
-
ing mercury and subsequently condensing the volatilized mercury for
recovery. The retorting or roasting unit (or facility) must be subject
to one or more of the following:
a)
A national emissions standard for hazardous air pollutants
(NESHAP) for mercury (40 CFR 61, Subpart E);
b)
A best available control technology (BACT) or a lowest achievable
emission rate (LAER) standard for mercury imposed pursuant to a
prevention of significant deterioration (PSD) permit (including 35
Ill. Adm. Code 201 through 203); or
c)
A state permit that establishes emission limitations (within
meaning of Section 302 of the Clean Air Act) for mercury, includ
-
ing a permit issued pursuant to 35 Ill. Adm. Code 201. All
wastewater and nonwastewater residues derived from this process
must then comply with the corresponding treatment standards per
waste code with consideration of any applicable subcategories
(e.g., high or low mercury subcategories).
RMETL
Recovery of metals or inorganics utilizing one or more of the following
direct physical or removal technologies:
1)
ion exchange;
2)
resin or solid (i.e., zeolites) adsorption;
3)
reverse osmosis;
4)
chelation or solvent extraction;
5)
freeze crystallization;
6)
ultrafiltration; or
7)
simple precipitation (i.e., crystallization)
403
Note: this does not preclude the use of other physical phase separation
or concentration techniques such as decantation, filtration (including
ultrafiltration), and centrifugation, when used in conjunction with the
above listed recovery technologies.
RORGS
Recovery of organics utilizing one or more of the following technolo
-
gies:
1)
Distillation;
2)
thin film evaporation;
3)
steam stripping;
4)
carbon adsorption;
5)
critical fluid extraction;
6)
liquid-liquid extraction;
7)
precipitation or crystallization (including freeze
crystallization); or
8)
chemical phase separation techniques (i.e., addition of acids,
bases, demulsifiers, or similar chemicals).
Note: This does not preclude the use of other physical phase separation
techniques such as decantation, filtration (including ultrafiltration),
and centrifugation, when used in conjunction with the above listed
recovery technologies.
RTHRM
Thermal recovery of metals or inorganics from nonwastewaters in units
defined as cement kilns, blast furnaces, smelting, melting and refining
furnaces, combustion devices used to recover sulfur values from spent
sulfuric acid and "other devices" determined by the Agency pursuant to
35 Ill. Adm. Code 720.110, the definition of "industrial furnace".
RZINC
Resmelting in high temperature metal recovery units for the purpose of
recovery of zinc.
STABL
Stabilization with the following reagents (or waste reagents) or
combinations of reagents:
1)
Portland cement; or
2)
lime or pozzolans (e.g., fly ash and cement kiln dust)--this does
not preclude the addition of reagents (e.g., iron salts, sili
-
cates, and clays) designed to enhance the set or cure time or
compressive strength, or to overall reduce the leachability of the
metal or inorganic.
SSTRP
Steam stripping of organics from liquid wastes utilizing direct
application of steam to the wastes operated such that liquid and vapor
flow rates, as well as, temperature and pressure ranges have been
optimized, monitored, and maintained. These operating parameters are
dependent upon the design parameters of the unit such as, the number of
separation stages and the internal column design. Thus, resulting in a
condensed extract high in organics that must undergo either incinera
-
tion, reuse as a fuel, or other recovery or reuse and an extracted
wastewater that must undergo further treatment as specified in the
standard.
404
WETOX
Wet air oxidation performed in units operated such that a surrogate
compound or indicator parameter has been substantially reduced in
concentration in the residuals (e.g., total organic carbon (TOC) can
often be used as an indicator parameter for the oxidation of many
organic constituents that cannot be directly analyzed in wastewater
residues).
WTRRX
Controlled reaction with water for highly reactive inorganic or organic
chemicals with precautionary controls for protection of workers from
potential violent reactions as well as precautionary controls for
potential emissions of toxic or ignitable levels of gases released
during the reaction.
Note 1:
When a combination of these technologies (i.e., a treatment train)
is specified as a single treatment standard, the order of
application is specified in Section 728.Table T by indicating the
five letter technology code that must be applied first, then the
designation "fb." (an abbreviation for "followed by"), then the
five letter technology code for the technology that must be
applied next, and so on.
Note 2:
When more than one technology (or treatment train) are specified
as alternative treatment standards, the five letter technology
codes (or the treatment trains) are separated by a semicolon (;)
with the last technology preceded by the word "OR". This indi
-
cates that any one of these BDAT technologies or treatment trains
can be used for compliance with the standard.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.Table T
Treatment Standards for Hazardous Wastes
Note: The treatment standards that heretofore appeared in tables in Sections
728.141, 728.142, and 728.143 have been consolidated into this table.
Waste Code
Waste Des cription and Treat ment or Regulatory Sub
category
1
Regulated Hazardous Constituent
Wastewaters
Nonwaste waters
Common Name
CAS
2
Number
Concentration
in mg/l
3
; or
Technology
Code
4
Concentration
in mg/kg
35
un-
less noted as
"mg/l TCLP";
or Technology
Code
4
D001
9
Ignitable Characteristic Wastes, except for the Section 721.121(a)(1) High TOC
Subcategory , that are managed in non-CWA or non-CWA-equivalent or non-Class I
SDWA systems .
NA
NA
DEACT and meet
Section
728.148
standards;
8
or
RORGS; or
CMBST
DEACT and meet
Section
728.148
standards;
8
or
RORGS; or
CMBST
D001
Ignitable Characteristic Wastes, except for the Section 721.121(a)(1) High TOC
405
Subcategory, that are managed in CWA or CWA-equivalent or Class I SDWA systems
NA
NA
DEACT
DEACT
D001
9
High TOC Ignitable Characteristic Liquids Subcategory based on 35 Ill. Adm.
Code 721.121(a)(1) - Greater than or equal to 10% total organic carbon.
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
RORGS; or
CMBST
D002
9
Corrosive Characteristic Wastes
that are managed in non-CWA or non-CWA
equivalent or non-Class I SDWA systems
.
NA
NA
DEACT and meet
Section
728.148
standards
8
DEACT and meet
Section
728.148
standards
8
D002
Corrosive Characteristic Wastes that are managed in CWA, CWA equivalent, or
Class I SDWA systems.
NA
NA
DEACT
DEACT
D002, D004, D005, D006, D007, D008, D009, D010, D011
Radioactive high level wastes generated during the reprocessing of fuel rods.
(Note: This subcategory consists of nonwastewaters only.)
Corrosivity (pH)
NA
NA
HLVIT
Arsenic
7440-38-2
NA
HLVIT
Barium
7440-39-3
NA
HLVIT
Cadmium
7440-43-9
NA
HLVIT
Chromium (Total)
7440-47-3
NA
HLVIT
Lead
7439-92-1
NA
HLVIT
Mercury
7439-97-6
NA
HLVIT
Selenium
7782-49-2
NA
HLVIT
Silver
7440-22-4
NA
HLVIT
D003
9
Reactive Sulfides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
NA
NA
DEACT
DEACT
D003
9
Explosive subcategory based on 35 Ill. Adm. Code 721.123(a)(6), (a)(7), and
(a)(8).
NA
NA
DEACT and meet
Section
728.148
standards
8
DEACT and meet
Section
728.148
standards
8
D003
9
Unexploded ordnance and other explosive devices that have been the subject of
an emergency response.
NA
NA
DEACT
DEACT
D003
9
Other Reactives Subcategory based on 35 Ill. Adm. Code 721.123(a)(1).
NA
NA
DEACT and meet
Section
728.148
standards
8
DEACT and meet
Section
728.148
standards
8
D003
9
406
Water Reactive Subcategory based on 35 Ill. Adm. Code 721.123(a)(2), (a)(3),
and (a)(4).
(Note: This subcategory consists of nonwastewaters only.)
NA
NA
NA
DEACT and meet
Section
728.148
standards
8
D003
9
Reactive Cyanides Subcategory based on 35 Ill. Adm. Code 721.123(a)(5).
Cyanides (Total)
7
57-12-5
--
590
Cyanides (Amenable)
7
57-12-5
0.86
30
D004
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for arsenic based on the extraction procedure (EP) in SW-846 Method
1310.
Arsenic
7440-38-2
5.0
5.0 mg/l EP
Arsenic; alternat
ive
6
standard for
nonwastewaters only.
7440-38-2
NA
5.0 mg/l TCLP
D005
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for barium based on the extraction procedure (EP) in SW-846 Method
1310.
Barium
7440-39-3
100
100 mg/l TCLP
D006
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for cadmium based on the extraction procedure (EP) in SW-846 Method
1310.
Cadmium
7440-43-9
1.0
1.0 mg/l TCLP
D006
Cadmium -Containing Batteries Subcategory
(Note: This subcategory consists of nonwastewaters only.)
Cadmium
7440-43-9
NA
RTHRM
D007
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for chromium based on the extraction procedure (EP) in SW-846 Met
hod
1310.
Chromium (Total)
7440-47-3
5.0
5.0 mg/l TCLP
D008
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for lead based on the extraction procedure (EP) in SW-846 Method
1310.
Lead
7439-92-1
5.0
5.0 mg/l EP
Lead; alternat ive
6
standard for
nonwastewaters only
7439-92-1
NA
5.0 mg/l TCLP
D008
Lead Acid Batteries Subcategory
(Note: This standard only applies to lead acid batteries that are identified
as RCRA hazardous wastes and that are not excluded elsewhere from regulation
under the land disposal restrictions of this Part or exempted under other
regulations (see 35 Ill. Adm. Code 726.180).
This subcategory consists of
nonwastewaters only.
).
(Note: This subcategory consists of nonwastewaters only.)
407
Lead
7439-92-1
NA
RLEAD
D008
Radioactive Lead Solids Subcategory
(Note: These lead solids include, but are not limited to, all forms of lead
shielding and other elemental forms of lead. These lead solids do not include
treatment residuals such as hydroxide sludges, other wastewater treatment
residuals, or incinerator ashes that can undergo conventional pozzolanic
stabilization, nor do they include organo-lead materials that can be
incinerated and stabilized as ash.
This subcategory consists of
nonwastewaters only.
)
(Note: This subcategory consists of nonwastewaters only.)
Lead
7439-92-1
NA
MACRO
D009
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
1310; and contain greater than or equal to 260 mg/kg total mercury that also
contain organics and are not incinerator residues.
(High Mercury-Organic
Subcategory)
(High Mercury-Organic Subcategory)
Mercury
7439-97-6
NA
IMERC; or
RMERC
D009
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
1310; and contain greater than or equal to 260 mg/kg total mercury that are
inorganic, including incinerator residues and residues from RMERC.
(High
Mercury-Inorganic Subcategory)
(High Mercury-Inorganic Subcategory)
Mercury
7439-97-6
NA
RMERC
D009
Nonwastewaters that exhibit, or are expected to exhibit, the characteristic of
toxicity for mercury based on the extraction procedure (EP) in SW-846 Method
1310; and contain less than 260 mg/kg total mercury.
(Low Mercury
Subcategory)
(Low Mercury Subcategory)
Mercury
7439-97-6
NA
0.20 mg/l TCLP
All D009 wastewaters.
Mercury
7439-97-6
0.20
NA
D009
Elemental mercury contaminated with radioactive materials.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
AMLGM
D009
Hydraulic oil contaminated with Mercury Radioactive Materials Subcategory.
(Note: This subcategory consists of nonwastewaters only.)
Mercury
7439-97-6
NA
IMERC
D010
Wastes that exhibit, or are expected to exhibit, the characteristic
orof
toxicity for selenium based on the extraction procedure (EP) in SW-846 Method
1310.
Selenium
7782-49-2
1.0
5.7 mg/l TCLP
408
D011
Wastes that exhibit, or are expected to exhibit, the characteristic of
toxicity for silver based on the extraction procedure (EP) in SW-846 Method
1310.
Silver
7440-22-4
5.0
5.0 mg/l TCLP
D012
9
Wastes that are TC for Endrin based on the TCLP in SW-846 Method 1311.
Endrin
72-20-8
BIODG; or
INCINCMBST
0.13 and meet
Section
728.148
standards
8
Endrin aldehyde
7421-93-4
BIODG; or
INCINCMBST
0.13 and meet
Section
728.148
standards
8
D013
9
Wastes that are TC for Lindane based on the TCLP in SW-846 Method 1311.
alpha-BHC
319-84-6
CARBN; or
INCINCMBST
0.066 and meet
Section
728.148
standards
8
beta-BHC
319-85-7
CARBN; or
INCINCMBST
0.066 and meet
Section
728.148
standards
8
delta-BHC
319-86-8
CARBN; or
INCINCMBST
0.066 and meet
Section
728.148
standards
8
gamma-BHC (Lindane)
58-89-9
CARBN; or
INCINCMBST
0.066 and meet
Section
728.148
standards
8
D014
9
Wastes that are TC for Methoxychlor based on the TCLP in SW-846 Method 1311.
Methoxychlor
72-43-5
WETOX or
INCINCMBST
0.18 and meet
Section
728.148
standards
8
D015
9
Wastes that are TC for Toxaphene based on the TCLP in SW-846 Method 1311.
Toxaphene
8001-35-2
BIODG or
INCINCMBST
2.6 and meet
Section
728.148
standards
8
D016
9
Wastes that are TC for 2,4-D (2,4-Dichloro
phenoxyacetic acid) based on the
TCLP in SW-846 Method 1311.
2,4-D (2,4-Dichloro
-
phenoxy acetic acid)
94-75-7
CHOXD,;
BIODG,; or
INCINCMBST
10 and meet
Section
728.148
standards
8
D017
9
Wastes that are TC for 2,4,5-TP (Silvex) based on the TCLP in SW-846 Method
1311.
409
2,4,5-TP (Silvex)
93-72-1
CHOXD or
INCINCMBST
7.9 and meet
Section
728.148
standards
8
D018
9
Wastes that are TC for Benzene based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
Benzene
71-43-2
0.14 and meet
Section
728.148
standards
8
10 and meet
Section
728.148
standards
8
D019
9
Wastes that are TC for Carbon tetra
chloride based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Carbon tetra chloride
56-23-5
0.057 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D020
9
Wastes that are TC for Chlordane based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033 and
meet Section
728.148
standards
8
0.26 and meet
Section
728.148
standards
8
D021
9
Wastes that are TC for Chloro
benzene based on the TCLP in SW-846 Method 1311
and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Chloro benzene
108-90-7
0.057 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D022
9
Wastes that are TC for Chloro
form based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
Chloro form
67-66-3
0.046 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D023
9
Wastes that are TC for o-Cresol based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
o-Cresol `
95-48-7
0.11 and meet
Section
728.148
standards
8
5.6 and meet
Section
728.148
standards
8
D024
9
Wastes that are TC for m-Cresol based on the TCLP in SW-846 Method 1311
and
410
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
m-Cresol
(difficult to
distinguish from p-
cresol)
108-39-4
0.77 and meet
Section
728.148
standards
8
5.6 and meet
Section
728.148
standards
8
D025
9
Wastes that are TC for p-Cresol based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
p-Cresol
(difficult to
distinguish from m-
cresol)
106-44-5
0.77 and meet
Section
728.148
standards
8
5.6 and meet
Section
728.148
standards
8
D026
9
Wastes that are TC for Cresols (Total) based on the TCLP in SW-846 Method 1311
and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Cresol-mixed isomers
(Cresylic acid)
(sum of o -, m-, and p-
cresol con centrations)
1319-77-3
0.88 and meet
Section
728.148
standards
8
11.2 and meet
Section
728.148
standards
8
D027
9
Wastes that are TC for p-Dichloro
benzene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
p-Dichloro benzene (1,4-
Dichloro benzene)
106-46-7
0.090 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D028
9
Wastes that are TC for 1,2-Dichloro
ethane based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
1,2-Dichloro ethane
107-06-2
0.21 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D029
9
Wastes that are TC for 1,1-Dichloro
ethylene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
1,1-Dichloro ethylene
75-35-4
0.025 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D030
9
Wastes that are TC for 2,4-Dinitro
toluene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
2,4-Dinitro toluene
121-14-2
0.32 and meet
Section
728.148
standards
8
140 and meet
Section
728.148
standards
8
411
D031
9
Wastes that are TC for Heptachlor based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
Heptachlor
76-44-8
0.0012 and
meet Section
728.148
standards
8
0.066 and meet
Section
728.148
standards
8
Heptachlor epoxide
1024-57-3
0.016 and meet
Section
728.148
standards
8
0.066 and meet
Section
728.148
standards
8
D032
9
Wastes that are TC for Hexa
chloro benzene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Hexachloro benzene
118-74-1
0.055 and meet
Section
728.148
standards
8
10 and meet
Section
728.148
standards
8
D033
9
Wastes that are TC for Hexa
chloro butadiene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Hexachloro butadiene
87-68-3
0.055 and meet
Section
728.148
standards
8
5.6 and meet
Section
728.148
standards
8
D034
9
Wastes that are TC for Hexa
chloro ethane based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Hexachloro ethane
67-72-1
0.055 and meet
Section
728.148
standards
8
30 and meet
Section
728.148
standards
8
D035
9
Wastes that are TC for Methyl ethyl ketone based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Methyl ethyl ketone
78-93-3
0.28 and meet
Section
728.148
standards
8
36 and meet
Section
728.148
standards
8
D036
9
Wastes that are TC for Nitro
benzene based on the TCLP in SW-846 Method 1311
and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Nitrobenzene
98-95-3
0.068 and meet
Section
728.148
standards
8
14 and meet
Section
728.148
standards
8
D037
9
Wastes that are TC for Penta
chloro phenol based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
412
systems only .
Pentachloro phenol
87-86-5
0.089 and meet
Section
728.148
standards
8
7.4 and meet
Section
728.148
standards
8
D038
9
Wastes that are TC for Pyridine based on the TCLP in SW-846 Method 1311
and
that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA systems
only.
Pyridine
110-86-1
0.014 and meet
Section
728.148
standards
8
16 and meet
Section
728.148
standards
8
D039
9
Wastes that are TC for Tetra
chloro ethylene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Tetrachloro ethylene
127-18-4
0.056 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D040
9
Wastes that are TC for Trichloro
ethylene based on the TCLP in SW-846 Method
1311 and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Trichloro ethylene
79-01-6
0.054 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
D041
9
Wastes that are TC for 2,4,5-Trichloro
phenol based on the TCLP in SW-846
Method 1311 and that are managed in non-CWA or non-CWA equivalent or non-Class
I SDWA systems only
.
2,4,5-Trichloro phenol
95-95-4
0.18 and meet
Section
728.148
standards
8
7.4 and meet
Section
728.148
standards
8
D042
9
Wastes that are TC for 2,4,6-Trichloro
phenol based on the TCLP in
SW-846
Method 1311 and that are managed in non-CWA or non-CWA equivalent or non-Class
I SDWA systems only
.
2,4,6-Trichloro phenol
88-06-2
0.035 and meet
Section
728.148
standards
8
7.4 and meet
Section
728.148
standards
8
D043
9
Wastes that are TC for Vinyl chloride based on the TCLP in SW-846 Method 1311
and that are managed in non-CWA or non-CWA equivalent or non-Class I SDWA
systems only .
Vinyl chloride
75-01-4
0.27 and meet
Section
728.148
standards
8
6.0 and meet
Section
728.148
standards
8
F001, F002, F003, F004 & F005
413
F001, F002, F003, F004, or F005 solvent wastes that contain any combination of
one or more of the following spent solvents: acetone, benzene, n-butyl
alcohol, carbon disulfide, carbon tetra
chloride, chlorinated fluoro
carbons,
chloro benzene, o-cresol, m-cresol, p-cresol, cyclo
hexanone, o-dichloro
benzene,
2-ethoxyethanol, ethyl acetate, ethyl benzene, ethyl ether, isobutyl alcohol,
methanol, methylene chloride, methyl ethyl ketone, methyl isobutyl ketone,
nitrobenzene, 2-nitro propane , pyridine, tetra
chloro ethylene, toluene, 1,1,1-
trichloro ethane, 1,1,2-trichloro
ethane, 1,1,2-trichloro-
1,2,2-trifluoro -
ethane, trichloro
ethylene, trichloro
monofluoro methane, or xylenes (except as
specifically noted in other subcategories). See further details of these
listings in 35 Ill. Adm. Code 721.131
Acetone
67-64-1
0.28
160
Benzene
71-43-2
0.14
10
n-Butyl alcohol
71-36-3
5.6
2.6
Carbon disulfide
75-15-0
3.8
NA
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro benzene
108-90-7
0.057
6.0
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers
(Cresylic acid)
(sum of o -, m-, and p-
cresol con centrations)
1319-77-3
0.88
11.2
Cyclohexanone
108-94-1
0.36
NA
o-Dichloro benzene
95-50-1
0.088
6.0
Ethyl acetate
141-78-6
0.34
33
Ethyl benzene
100-41-4
0.057
10
Ethyl ether
60-29-7
0.12
160
Isobutyl alcohol
78-83-1
5.6
170
Methanol
67-56-1
5.6
NA
Methylene chloride
75-9-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Nitrobenzene
98-95-3
0.068
14
Pyridine
110-86-1
0.014
16
Tetrachloro ethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
1,1,2-Trichloro-1,2,2-
trifluoro ethane
76-13-1
0.057
30
Trichloro ethylene
79-01-6
0.054
6.0
Trichloro monofluoro -
methane
75-69-4
0.020
30
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
F001, F002, F003, F004 & F005
F003 and F005 solvent wastes that contain any combination of one or more of
the following three solvents as the only listed F001 through F005 solvents:
carbon disulfide, cyclo
hexanone, or methanol. (Formerly Section 728.141(c))
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
414
Methanol
67-56-1
5.6
0.75 mg/l TCLP
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Nitro
propane as the only list
ed F001 through
F005 solvent.
2-Nitro propane
79-46-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
F001, F002, F003, F004 & F005
F005 solvent waste containing 2-Ethoxyethanol as the only listed F001 through
F005 solvent.
2-Ethoxyethanol
110-80-5
BIODG; or
INCINCMBST
INCINCMBST
F006
Wastewater treatment sludges from electroplating operations except from the
following processes: (1) Sulfuric acid anodizing of aluminum; (2) tin plating
on carbon steel; (3) zinc plating (segregated basis) on carbon steel; (4)
aluminum or zinc-aluminum plating on carbon steel; (5) cleaning or stripping
associated with tin, zinc, and aluminum plating on carbon steel; and (6)
chemical etching and milling of aluminum.
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F007
Spent cyanide plating bath solutions from electroplating operations.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F008
Plating bath residues from the bottom of plating baths from electroplating
operations where cyanides are used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F009
Spent stripping and cleaning bath solutions from electroplating operations
where cyanides are used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
415
Silver
7440-22-4
NA
0.30 mg/l TCLP
F010
Quenching bath residues from oil baths from metal heat treating operations
where cyanides are used in the process.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.880.86
NA
F011
Spent cyanide solutions from salt bath pot cleaning from metal heat treating
operations.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F012
Quenching wastewater treatment sludges from metal heat treating operations
where cyanides are used in the process.
Cadmium
7440-43-9
NA
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
F019
Wastewater treatment sludges from the chemical conversion coating of aluminum
except from zirconium phosphating in aluminum can washing when such
phosphating is an exclusive conversion coating process.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
F020, F021, F022, F023, F026
Wastes (except wastewater and spent carbon from hydrogen chloride
purification) from the production or manufacturing use (as a reactant,
chemical intermediate, or component in a formulating process) of: (1) tri- or
tetrachloro phenol, or of intermediates used to produce their pesticide
derivatives, excluding wastes from the production of Hexa
chloro phene from
highly purified 2,4,5-trichloro
phenol (i.e., F020); (2) penta
chloro phenol, or
of intermediates used to produce its derivatives (i.e., F021); (3) tetra
-,
penta-, or hexa chloro benzenes under alkaline conditions (i.e., F022)
.
and Wwastes (except wastewater and spent carbon from hydrogen chloride
purification) from the production of materials on equipment previously used
for the production or manufacturing use (as a reactant, chemical intermediate,
or component in a formulating process) of: (1) tri- or tetra
chloro phenols,
excluding wastes from equipment used only for the production of Hexa
chloro -
phene from highly purified 2,4,5-trichloro
phenol (F023) ; or (2) tetra -,
penta-, or hexa chloro benzenes under alkaline conditions (i.e., F026).
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Penta
chloro -
NA
0.000035
0.001
416
dibenzo furans)
Pentachloro phenol
87-86-5
0.089
7.4
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
2,4,5-Tri chloro phenol
95-95-4
0.18
7.4
2,4,6-Tri chloro phenol
88-06-2
0.035
7.4
2,3,4,6-Tetra chloro -
phenol
58-90-2
0.030
7.4
Pentachloro phenol
87-86-5
0.089
7.4
F024
Process wastes, including but not limited to, distillation residues, heavy
ends, tars, and reactor clean-out wastes, from, the production of certain
chlorinated aliphatic hydrocarbons by free radical catalyzed processes. These
chlorinated aliphatic hydrocarbons are those having carbon chain lengths
ranging from one to and including five, with varying amounts and positions of
chlorine substitution. (This listing does not include wastewaters, wastewater
treatment sludges, spent catalysts, and wastes listed in Section 721.131 or
721.132.).
All F024 wastes
NA
CMBST
CMBST
2-Chloro -1,3-butadiene
126-99-8
0.057
0.28
3-Chloropropylene
107-05-1
0.036
30
1,1-Dichloroethane
75-34-3
0.059
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,2-Dichloropropane
78-87-5
0.85
18
cis-1,3-Dichloropropylen
e
10061-01-5
0.036
18
trans-1,3-Dichloro -
propylene
10061-02-6
0.036
18
bis(2-Ethylhexyl) -
phthalate
117-81-7
0.28
28
Hexachloroethane
67-72-1
0.055
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
F025
Condensed light ends from the production of certain chlorinated aliphatic
hydrocarbons, by free radical catalyzed processes. These chlorinated
aliphatic hydrocarbons are those having carbon chain lengths ranging from one
up to and including five, with varying amounts and positions of chlorine
substitution. F025
--Light Ends Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
1,2-Dichloroethane
107-06-2
0.21
6.0
1,1-Dichloroethylene
75-35-4
0.025
6.0
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F025
Spent filters and filter aids, and spent desiccant wastes from the production
of certain chlorinated aliphatic hydrocarbons, by free radical catalyzed
processes. These chlorinated aliphatic hydrocarbons are those having carbon
chain lengths ranging from one to and including five, with varying amounts and
positions of chlorine substitution. F025
--Spent Filters/A ids and Desiccants
Subcategory.
Carbon tetrachloride
56-23-5
0.057
6.0
417
Chloroform
67-66-3
0.046
6.0
Hexachlorobenzene
118-74-1
0.055
10
Hexachlorobutadiene
87-68-3
0.055
5.6
Hexachloroethane
67-72-1
0.055
30
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloroethane
79-00-5
0.054
6.0
Trichloroethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F027
Discarded unused formulations contianing tri
-, tetra -, or penta chloro phenol or
discarded unused formulations containing compounds derived from these chloro
-
phenols. (This listing does not include formulations containing hexa
chloro -
phene synthesized from prepurified 2,4,5-trichloro
phenol as the sole
component.)
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Penta
chloro -
dibenzo furans)
NA
0.000035
0.001
Pentachloro phenol
87-86-5
0.089
7.4
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
2,3,4,6-Tetra chloro -
phenol
58-90-2
0.030
7.4
Pentachloro phenol
87-86-5
0.089
7.4
F028
Residues resulting from the incineration or thermal treatment of soil
contaminated with USEPA hazardous waste numbers F020, F021, F023, F026, and
F027.
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Penta
chloro -
dibenzo furans)
NA
0.000035
0.001
Pentachloro phenol
87-86-5
0.089
7.4
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
2,3,4,6-Tetra chloro -
phenol
58-90-2
0.030
7.4
Pentachloro phenol
87-86-5
0.089
7.4
F024
Process wastes, including but not limited to, distillation residues, heavy
ends, tars, and reactor clean-out wastes, from the production of certain
chlorinated aliphatic hydro
carbons by free radical catalyzed processes. These
418
chlorinated aliphatic hydro
carbons are those having carbon chain lengths
ranging from one to and including five, with varying amounts and positions of
chlorine substitution. (This listing does not include wastewaters, wastewater
treatment sludges, spent catalysts, and wastes listed in 35 Ill. Adm. Code
721.131 or 721.132.)
All F024 wastes
NA
INCIN
INCIN
2-Chloro-1,3-buta
diene
126-99-8
0.057
0.28
3-Chloro propylene
107-05-1
0.036
30
1,1-Dichloro ethane
75-34-3
0.059
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,2-Dichloro propane
78-87-5
0.85
18
cis-1,3-Dichloro -
propylene
10061-01-5
0.036
18
trans-1,3-Dichloro
-
propylene
10061-02-6
0.036
18
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Hexachloro ethane
67-72-1
0.055
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
F025
Condensed light ends from the production of certain chlorinated aliphatic
hydrocarbons, by free radical catalyzed processes. These chlorinated
aliphatic hydro carbons are those having carbon chain lengths ranging from one
to and including five, with varying amounts and positions of chlorine
substitution.
F025 - Light Ends Subcategory
Carbon tetra chloride
56-23-6
0.057
6.0
Chloro form
67-66-3
0.046
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,1-Dichloro ethylene
75-35-4
0.025
6.0
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F025
Spent filters and filter aids, and spent desiccant wastes from the production
of certain chlorinated aliphatic hydro
carbons, by free radical catalyzed
processes. These chlorinated aliphatic hydro
carbons are those having carbon
chain lengths ranging from one to and including five, with varying amounts and
positions of chlorine substitution.
F025 - Spent Filters or Aids and Desiccants Subcategory
Carbon tetra chloride
56-23-5
0.067
6.0
Chloro form
67-66-3
0.046
6.0
Hexachloro benzene
118-74-1
0.055
10
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro ethane
67-72-1
0.055
30
Methylene chloride
75-9-2
0.089
30
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
F037
Petroleum refinery primary oil/water/solids separation sludge
--Any sludge
generated from the gravitational separation of oil/water/solids during the
storage or treatment of process wastewaters and oily cooling wastewaters from
petroleum refineries. Such sludges include, but are not limited to, those
generated in: oil/water/solids separators; tanks and impoundments; ditches
and other conveyances; sumps; and stormwater units receiving dry weather flow.
419
Sludge generated in stormwater units that do not receive dry weather flow,
sludges generated from non-contact once-through cooling waters segregated for
treatment from other process or oily cooling waters, sludges generated in
agressive biological treatment units as defined in 35 Ill. Adm. Code
721.131(b)(2) (including sludges generated in one or more additional units
after wastewaters have been treated in agressive biological treatment units)
and K051 wastes are not included in this listing.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
F038
Petroleum refinery secondary (emulsified) oil/water/solids separation sludge
or float generated from the physical or chemical separation of
oil/water/solids in process wastewaters and oily cooling wastewaters from
petroleum refineries. Such wastes include, but are not limited to, all
sludges and floats generated in: induced air floatation (IAF) units, tanks
and impoundments, and all sludges generated in DAF units. Sludges generated
in stormwater units that do not receive dry weather flow, sludges generated
from non-contact once-through cooling waters segregated for treatment from
other process or oily cooling waters, sludges and floats generated in
agressive biological treatment units as defined in 35 Ill. Adm. Code
721.131(b)(2) (including sludges and floats generated in one or more
additional units after wastewaters have been treated in agressive biological
units) and F037, K048, and K051 are not included in this listing.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
420
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
F039
Leachate (liquids that have percolated through land disposed wastes) resulting
from the disposal of more than one restricted waste classified as hazardous
under 728.Subpart D. (Leachate resulting from the disposal of one or more of
the following USEPA hazardous wastes and no other hazardous wastes retains its
USEPA hazardous waste numbers: F020, F021, F022, F026, F027, or F028.).
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
NA
Acetophenone
96-86-2
0.010
9.7
2-Acetyl aminofluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylonitrile
107-13-1
0.24
84
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
alpha-BHC
319-84-6
0.00014
0.066
beta-BHC
319-85-7
0.00014
0.066
delta-BHC
319-86-8
0.023
0.066
gamma-BHC
58-89-9
0.0017
0.066
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i) perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloro methane
75-27-4
0.35
15
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
4-Bromo phenyl phenyl
ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitro
-
phenol (Dinoseb)
88-85-7
0.066
2.5
Carbon disulfide
75-15-0
3.8
NA
Carbon tetra chloride
56-23-5
0.057
6.0
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033
0.26
p-Chloro aniline
106-47-8
0.46
16
Chloro benzene
108-90-7
0.057
6.0
Chloro benzilate
510-15-6
0.10
NA
2-Chloro-1,3-buta
diene
126-99-8
0.057
NA
Chloro dibromo methane
124-48-1
0.057
15
Chloro ethane
75-00-3
0.27
6.0
bis(2-Chloro ethoxy) -
methane
111-91-1
0.036
7.2
421
bis(2-Chloro ethyl) ether
111-44-4
0.033
6.0
Chloro form
67-66-3
0.046
6.0
bis(2-Chloro isopropyl) -
ether
108-60-1 39638-
32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
Chloro methane (Methyl
chloride)
74-87-3
0.19
30
2-Chloro naphthalene
91-58-7
0.055
5.6
2-Chloro phenol
95-57-8
0.044
5.7
3-Chloro propylene
107-05-1
0.036
30
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
Cyclohexanone
108-94-1
0.36
NA
1,2-Dibromo-3-chloro
-
propane
96-12-8
0.11
15
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
Dibromo methane
74-95-3
0.11
15
2,4-D (2,4-Dichloro
-
phenoxy acetic acid)
94-75-7
0.72
10
o,p'-DDD
53-19-0
0.023
0.0870.087
p,p'-DDD
72-54-8
0.023
0.087
o,p'-DDE
3424-82-6
0.031
0.087
p,p'-DDE
72-55-9
0.031
0.087
o,p'-DDT
789-02-6
0.0039
0.087
p,p'-DDT
50-29-3
0.0039
0.087
Dibenz (a,h)anthra cene
53-70-3
0.055
8.2
Dibenz(a,e)pyrene
192-65-4
0.061
NA
m-Dichloro benzene
541-73-1
0.036
6.0
o-Dichloro benzene
95-50-1
0.088
6.0
p-Dichloro benzene
106-46-7
0.090
6.0
Dichloro difluoro methane
75-71-8
0.23
7.2
1,1-Dichloro ethane
75-34-3
0.059
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,1-Dichloro ethylene
75-35-4
0.025
6.0
trans-1,2-Dichloro
-
ethylene
156-60-5
0.054
30
2,4-Dichloro phenol
120-83-2
0.044
14
2,6-Dichloro phenol
87-65-0
0.044
14
1,2-Dichloro propane
78-87-5
0.85
18
cis-1,3-Dichloro -
propylene
10061-01-5
0.036
18
trans-1,3-Dichloro
-
propylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethyl phthalate
84-66-2
0.20
28
2-4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
1,4-Dinitro benzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitro phenol
51-28-5
0.12
160
2,4-Dinitro toluene
121-14-2
0.32
140
422
2,6-Dinitro toluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
Di-n-propyl nitros amine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
NA12.0
170
Diphenyl amine (difficult
to distinguish from
diphenyl nitros amine)
122-39-4
0.92
13NA
Diphenyl nitros amine
(difficult to
distinguish from
diphenyl amine)
86-30-6
0.92
NA
1,2-Diphenyl hydrazine
122-66-7
0.087
NA
Disulfoton
298-04-4
0.017
6.2
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1-31-07-8 1031-
07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
Ethyl acetate
141-78-6
0.34
33
Ethyl cyanide (Propane
-
nitrile)
107-12-0
0.24
360
Ethyl benzene
100-41-4
0.057
10
Ethyl ether
60-29-7
0.12
160
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachloro benzene
118-74-1
0.055
10
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
Hexachloro ethane
67-72-1
0.055
30
Hexachloro propylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d)
pyrene
193-39-5
0.0055
3.4
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-8
0.0011
0.13
Methacrylo nitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
NA
Methapyrilene
91-80-5
0.081
1.5
Methoxychlor
72-43-5
0.25
0.18
3-Methyl cholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-
chloro aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methyl methacrylate
80-62-6
0.14
160
423
Methyl methan sulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
p-Nitro aniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
p-Nitro phenol
100-02-7
0.12
29
N-Nitroso diethyl amine
55-18-5
0.40
28
N-Nitroso dimethyl amine
62-75-9
0.40
NA
N-Nitroso-di-n-butyl
-
amine
924-16-3
0.40
17
N-Nitroso methyl ethyl-
amine
10595-95-6
0.40
2.3
N-Nitroso morpholine
59-89-2
0.40
2.3
N-Nitroso piperidine
100-75-4
0.013
35
N-Nitroso pyrrolidine
930-55-2
0.013
35
Parathion
56-38-2
0.014
4.6
Total PCBs
(sum of all PCB isomers,
or all Aroclors)
1336-36-3
0.10
10
Pentachloro benzene
608-93-5
0.055
10
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PcCDFs PeCDFs (All Penta -
chloro dibenzo furans)
NA
0.000035
0.001
Pentachloro nitrobenzene
82-68-8
0.055
4.8
Pentachloro phenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Phorate
298-02-2
0.021
4.6
Phthalic anhydride
85-44-9
0.055
NA
Pronamide
23950-58-5
0.093
1.5
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
2,4,5-T
93-76-5
0.72
7.9
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
1,1,1,2-Tetra chloro -
ethane
630-20-6
0.057
6.0
1,1,2,2-Tetra chloro -
ethane
79-34-6
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
2,3,4,6-Tetra chloro -
phenol
58-90-2
0.030
7.4
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Bromoform (Tribromo -
methane)
75-25-2
0.63
15
1,2,4-Trichloro benzene
120-82-1
0.055
19
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
Trichloro monofluoro -
75-69-4
0.020
30
424
methane
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
1,2,3-Trichloro propane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-
trifluoro ethane
76-13-1
0.057
30
tris(2,3-Dibromo propyl)
phosphate
126-72-7
0.11
NA
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers
(sum or o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
NA
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
NA
Fluoride
16964-48-8
35
NA
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
0.15
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
Sulfide
8496-25-8
14
NA
Thallium
7440-28-0
1.4
NA
Vanadium
7440-62-2
4.3
NA
K001
Bottom sediment sludge from the treatment of wastewaters from wood preserving
processes that use creosote or penta
chloro phenol.
Naphthalene
91-20-3
0.059
5.6
Pentachloro phenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.690.37 mg/l
TCLP
0.37 mg/l TCLP
K002
Wastewater treatment sludge from the production of chrome yellow and orange
pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K003
Wastewater treatment sludge from the production of molybdate orange pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K004
Wastewater treatment sludge from the production of zinc yellow pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
425
K005
Wastewater treatment sludge from the production of chrome green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.25
590
K006
Wastewater treatment sludge from the production of chrome oxide green pigments
(anhydrous).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K006
Wastewater treatment sludge from the production of chrome oxide green pigments
(hydrated).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
K007
Wastewater treatment sludge from the production of iron blue pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.25
590
K008
Oven residue from the production of chrome oxide green pigments.
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K009
Distillation bottoms from the production of acetaldehyde from ethylene.
Chloro form
67-66-3
0.046
6.0
K010
Distillation side cuts from the production of acetaldehyde from ethylene.
Chloro form
67-66-3
0.046
6.0
K011
Bottom stream from the wastewater stripper in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
1.838
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K013
Bottom stream from the acetonitrile column in the production of acrylonitrile.
Acetonitrile
75-05-8
5.6
1.838
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
K014
Bottoms from the acetonitrile purification column in the production of
acrylonitrile.
Acetonitrile
75-05-8
5.6
1.838
Acrylonitrile
107-13-1
0.24
84
Acrylamide
79-06-1
19
23
Benzene
71-43-2
0.14
10
Cyanide (Total)
57-12-5
1.2
590
426
K015
Still bottoms from the distillation of benzyl chloride.
Anthracene
120-12-7
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
85.0 mg/l TCLP
K016
Heavy ends or distillation residues from the production of carbon tetra
-
chloride.
Hexachloro benzene
118-74-1
0.055
10
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
Hexachloro ethane
67-72-1
0.055
30
Tetrachloro ethylene
127-18-4
0.056
6.0
K017
Heavy ends (still bottoms) from the purification column in the production of
epichloro hydrin.
bis(2-Chloro ethyl) ether
111-44-4
0.033
6.0
1,2-Dichloro propane
78-87-5
0.85
18
1,2,3-Trichloro propane
96-18-4
0.85
30
K018
Heavy ends from the fractionation column in ethyl chloride production.
Chloro ethane
75-00-3
0.27
6.0
Chloro methane
74-87-3
0.19
NA
1,1-Dichloro ethane
75-34-3
0.059
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
Hexachloro benzene
118-74-1
0.055
10
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro ethane
67-72-1
0.055
30
Pentachloro ethane
76-01-7
NA
6.0
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
K019
Heavy ends from the distillation of ethylene dichloride in ethylene dichloride
production.
bis(2-Chloro ethyl) ether
111-44-4
0.033
6.0
Chloro benzene
108-90-7
0.057
6.0
Chloro form
67-66-3
0.046
6.0
p-Dichloro benzene
106-46-7
0.090
NA
1,2-Dichloro ethane
107-06-2
0.21
6.0
Fluorene
86-73-7
0.059
NA
Hexachloro ethane
67-72-1
0.055
30
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
NA
Tetrachloro ethylene
127-18-4
0.056
6.0
427
1,2,4-Trichloro benzene
120-82-1
0.055
19
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
K020
Heavy ends from the distillation of vinyl chloride in vinyl chloride monomer
production.
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,1,2,2-Tetra chloro -
ethane
79-34-6
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
K021
Aqueous spent antimony catalyst waste from fluoro
methanes production.
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro form
67-66-3
0.046
6.0
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
K021
Aqueous spent antimony catalyst waste from fluoro
methanes production.
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro form
67-66-3
0.046
6.0
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
K022
Distillation bottom tars from the production of phenol or acetone from cumene.
Toluene
108-88-3
0.080
10
Acetophenone
96-86-2
0.010
9.7
Diphenylamine (difficult
to distinguish from
diphenyl nitros amine)
122-39-4
0.92
13
Diphenyl nitros amine
(difficult to
distinguish from
diphenyl amine)
86-30-6
0.92
13
Phenol
108-95-2
0.039
6.2
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K023
Distillation light ends from the production of phthalic anhydride from
naphthalene.
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
85-44-9
0.055
28
K024
Distillation bottoms from the production of phthalic anhydride from
naphthalene.
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
85-44-9
0.055
28
428
K025
Distillation bottoms from the production of nitro
benzene by the nitration of
benzene.
NA
NA
LLEXT fb SSTRP
fb CARBN; or
INCINCMBST
INCINCMBST
K026
Stripping still tails from the production of methyl ethyl pyridines.
NA
NA
INCINCMBST
INCINCMBST
K027
Centrifuge and distillation residues from the toluene diisocyanate production.
NA
NA
CARBN; or
INCINCMBST
CMBST
K028
Spent catalyst from the hydro
chlorinator rea ctor in the production of 1,1,1-
trichloro ethane.
1,1-Dichloro ethane
75-34-3
0.059
6.0
trans-1,2-Dichloro
-
ethylene
156-60-5
0.054
30
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro ethane
67-72-1
0.055
30
Pentachloro ethane
76-01-7
NA
6.0
1,1,1,2-Tetra chloro -
ethane
630-20-6
0.057
6.0
1,1,2,2-Tetra chloro -
ethane
79-34-6
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Cadmium
7440-43-9
0.69
NA
Chromium(Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K029
Waste from the product steam stripper in the production of 1,1,1-trichloro
-
ethane.
Chloro form
67-66-3
0.046
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,1-Dichloro ethylene
75-35-4
0.025
6.0
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
Vinyl chloride
75-01-4
0.27
6.0
K030
Column bodies or heavy ends from the combined production of trichloro
ethylene
and perchloro ethylene.
o-Dichloro benzene
95-50-1
0.088
NA
p-Dichloro benzene
106-46-7
0.090
NA
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro ethane
67-72-1
0.055
30
Hexachloro propylene
1888-71-7
NA
30
Pentachloro benzene
608-93-5
NA
10
Pentachloro ethane
76-01-7
NA
6.0
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
Tetrachloro ethylene
127-18-4
0.056
6.0
1,2,4-Trichloro benzene
120-82-1
0.055
19
429
K031
By-product salts generated in the production of MSMA and cacodylic acid.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K032
Wastewater treatment sludge from the production of chlordane.
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033
0.26
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
K033
Wastewater and scrub water from the chlorination of cyclo
pentadiene in the
production of chlordane.
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
K034
Filter solids from the filtration of hexa
chloro cyclopentadiene in the
production of chlordane.
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
K035
Wastewater treatment sludges generated in the production of creosote.
Acenaphthene
83-32-9
NA
3.4
Anthracene
120-12-7
NA
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
Dibenz (a,h)anthra cene
53-70-3
NA
8.2
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
NA
3.4
Indeno(1,2,3-cd) pyrene
193-39-5
NA
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
K036
Still bottoms from toluene reclamation distillaiton in the production of
disulfoton.
Disulfoton
298-04-4
0.017
6.2
K037
Wastewater treatment sludges from the production of disulfoton.
Disulfoton
298-04-4
0.017
6.2
Toluene
108-88-3
0.080
10
430
K038
Wastewater from the washing and stripping of phorate production.
Phorate
298-02-2
0.021
4.6
K039
Filter cake from the filtration of diethyl
phosphorodithioic acid in the
production of phorate.
NA
NA
CARBN; or
INCINCMBST
CMBST
K040
Wastewater treatment sludge from the production of phorate.
Phorate
298-02-2
0.021
4.6
K041
Wastewater treatment sludge from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K042
Heavy ends or distillation residues from the distillation of tetra
chloro -
benzene in the production of 2,4,5-T.
o-Dichloro benzene
95-50-1
0.088
6.0
p-Dichloro benzene
106-46-7
0.090
6.0
Pentachloro benzene
608-93-5
0.055
10
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
1,2,4-Trichloro benzene
120-82-1
0.055
19
K043
2,6-Dichloro phenol waste from the production of 2,4-D.
2,4-Dichloro phenol
120-83-2
0.044
14
2,6-Dichloro phenol
187-65-0
0.044
14
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
2,3,4,6-Tetra chloro -
phenol
58-90-2
0.030
7.4
Pentachloro phenol
87-86-5
0.089
7.4
Tetrachloro ethylene
127-18-4
0.056
6.0
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Penta
chloro -
dibenzo furans)
NA
0.000035
0.001
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
K044
Wastewater treatment sludges from the manufacturing and processing of
explosives.
NA
NA
DEACT
DEACT
K045
Spent carbon from the treatment of wastewater containing explosives.
NA
NA
DEACT
DEACT
K046
431
Wastewater treatment sludges from the manufacturing, formulation and loading
of lead-based initiating compounds.
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K047
Pink or red water from TNT operations.
NA
NA
DEACT
DEACT
K048
Dissolved air flotation (DAF) float from the petroleum refining industry.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Chrysene
218-01-9
0.059
3.4
Di-n-butyl phthalate
84-74-2
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-33
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K049
Slop oil emulsion solids from the petroleum refining industry.
Anthracene
120-12-7
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Carbon disulfide
75-15-0
3.8
NA
Chrysene
2218-01-9
0.059
3.4
2,4-Dimethyl phenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K050
Heat exchanger bundle cleaning sludge from the petroleum refining industry.
Benzo(a)pyrene
50-32-8
0.061
3.4
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
432
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K051
API separator sludge from the petroleum refining industry.
Acenaphthene
83-32-9
0.059
NA
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
Chrysene
2218-01-9
0.059
3.4
Di-n-butyl phthalate
105-67-9
0.057
28
Ethylbenzene
100-41-4
0.057
10
Fluorene
86-73-7
0.059
NA
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Cyanides (Total)
7
57-12-5
1.2
590
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K052
Tank bottoms (leaded) from the petroleum refining industry.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol
(difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol
(difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
2,4-Dimethyl phenol
105-67-9
0.036
NA
Ethylbenzene
100-41-4
0.057
10
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
Toluene
108-88-3
0.08
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
NA
Nickel
7440-02-0
NA
5.0 mg/l TCLP
K060
Ammonia still lime sludge from coking operations.
Benzene
71-43-2
0.14
10
Benzo(a)pyrene
50-32-8
0.061
3.4
Naphthalene
91-20-3
0.059
5.6
433
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K061
Emission control dust or sludge from the primary production of steel in
electric furnaces.
Antimony
7440-36-0
NA
2.1 mg/l TCLP
Arsenic
7440-38-2
NA
5.0 mg/l TCLP
Barium
7440-39-3
NA
7.6 mg/l TCLP
Beryllium
7440-41-7
NA
0.014 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
NA
0.16 mg/l TCLP
Silver
7440-22-4
NA
0.30 mg/l TCLP
Thallium
NA7440-28-0
NA
0.078 mg/l
TCLP
Zinc
7440-66-6
NA
5.3 mg/l TCLP
K062
Spent pickle liquor generated by steel finishing operations of facilities
within the iron and steel industry (SIC Codes 331 and 332).
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
NA
K069
Emission control dust or sludge from secondary lead smelting. - Calcium
sulfate (Low Lead) Subcategory
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K069
Emission control dust or sludge from secondary lead smelting. - Non-Calcium
sulfate (High Lead) Subcategory
NA
NA
NA
RLEAD
K071
K071 (Brine purification muds from the mercury cell process in chlorine
production, where separately prepurified brine is not used) nonwastewaters
that are residues from RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
K071
K071 (Brine purification muds from the mercury cell process in chlorine
production, where separately prepurified brine is not used) nonwastewaters
that are not residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
K071
All K071 wastewaters.
Mercury
7439-97-6
0.15
NA
K073
Chlorinated hydro
carbon waste from the purification step of the diaphragm cell
process using graphite anodes in chlorine production.
434
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro form
67-66-3
0.046
6.0
Hexachloro ethane
67-72-1
0.055
30
Tetrachloro ethylene
127-18-4
0.0580.056
6.0
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
K083
Distillation bottoms from aniline production.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
Cyclohexanone
108-94-1
0.36
NA
Diphenyl amine
(difficult to
distinguish from
diphenyl nitros amine)
122-39-4
0.92
13
Diphenyl nitros amine
(difficult to
distinguish from
diphenyl amine)
86-30-6
0.92
13
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
K084
Wastewater treatment sludges generated during the production of veterinary
pharmaceuticals from arsenic or organo-arsenic compounds.
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
K085
Distillation or fractionation column bottoms from the production of chloro
-
benzenes.
Benzene
71-43-2
0.14
10
Chloro benzene
108-90-7
0.057
6.0
m-Dichloro benzene
541-73-1
0.036
6.0
o-Dichloro benzene
95-50-1
0.088
6.0
p-Dichloro benzene
106-46-7
0.090
6.0
Hexachloro benzene
118-74-1
0.055
10
Total PCBs
(sum of all PCB isomers,
or all Aroclors)
1336-36-3
0.10
10
Pentachloro benzene
608-93-5
0.055
10
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
1,2,4-Trichloro benzene
120-82-1
0.055
19
K086
Solvent wastes and sludges, caustic washes and sludges, or water washes and
sludges from cleaning tubs and equipment used in the formulation of ink from
pigments, driers, soaps, and stabilizers containing chromium and lead.
Acetone
67-64-1
0.28
160
Acetophenone
96-86-2
0.010
9.7
bis(2-Ethyl hexyl)
phthalate
117-81-7
0.28
28
n-Butyl alcohol
71-36-3
5.6
2.6
Butylbenzyl phthalate
85-68-7
0.017
28
Cyclohexanone
108-94-1
0.36
NA
o-Dichloro benzene
95-50-1
0.088
6.0
Diethyl phthalate
84-66-2
0.20
28
Dimethyl phthalate
131-11-3
0.047
28
Di-n-butyl phthalate
84-74-2
0.057
28
Di-n-octyl phthalate
117-84-0
0.017
28
435
Ethyl acetate
141-78-6
0.34
33
Ethylbenzene
100-41-4
0.057
10
Methanol
67-56-1
5.6
NA
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
Methylene chloride
75-09-2
0.089
30
Naphthalene
91-20-3
0.059
5.6
Nitrobenzene
98-95-3
0.068
14
Toluene
108-88-3
0.080
10
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K087
Decanter tank tar sludge from coking operations.
Acenaphthylene
208-96-8
0.059
3.4
Benzene
71-43-2
0.14
10
Chrysene
218-01-9
0.059
3.4
Fluoranthene
206-44-0
0.068
3.4
Indeno l(1,2,3-cd) pyrene
193-39-5
0.0055
3.4
Naphthalene
91-20-3
0.059
5.6
Phenanthrene
85-01-8
0.059
5.6
Toluene
108-88-3
0.080
10
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K088
Spent potliners from primary aluminum reduction.
Acenaphthene
83-32-9
0.059
3.4
Anthracene
120-12-7
0.059
3.4
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
205-99-2
0.11
6.8
Benzo(k)fluoranthene
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Chrysene
218-01-9
0.09
34
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
Fluoranthene
206-44-0
0.068
3.4
Indeno(1,2,3 -c,d)pyrene
193-39-5
0.0055
3.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
0.014 mg/l
TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury
7439-97-6
0.15
0.025 mg/l
TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
436
Cyanide (Total)
7
57-12-5
1.2
590
Cyanide (Amenable)
7
57-12-5
0.86
30
Fluoride
16984-48-8
35
48 mg/l TCLP
K093
Distillation light ends from the production of phthalic anhydride from ortho-
xylene.
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
85-44-9
0.055
28
K094
Distillation bottoms from the production of phthalic anhydride from ortho-
xylene.
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
85-44-9
0.055
28
K095
Distillation bottoms from the production of 1,1,1-trichloro
ethane.
Hexachloro ethane
67-72-1
0.055
30
Pentachloro ethane
76-01-7
0.055
6.0
1,1,1,2-Tetra chloro -
ethane
630-20-6
0.057
6.0
1,1,2,2-Tetra chloro -
ethane
79-34-6
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
K096
Heavy ends from the heavy ends column from the production of 1,1,1-trichloro
-
ethane.
m-Dichloro benzene
541-73-1
0.036
6.0
Pentachloro ethane
76-01-7
0.055
6.0
1,1,1,2-Tetra chloro -
ethane
630-20-6
0.057
6.0
1,1,2,2-Tetra chloro -
ethane
79-34-6
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
1,2,4-Trichloro benzene
120-82-1
0.055
19
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
K097
Vacuum stripper discharge from the chlordane chlorinator in the production of
chlordane.
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033
0.26
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.0680.066
437
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
K098
Untreated process wastewater from the production of toxaphene.
Toxaphene
8001-35-2
0.0095
2.6
K099
Untreated wastewater from the production of 2,4-D.
2,4-Dichloro phenoxy-
acetic acid
94-75-7
0.72
10
HxCDDs (All Hexa chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexa chloro -
dibenzo furans)
NA
0.000063
0.001
PeCDDs (All Penta
chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Penta
chloro -
dibenzo furans)
NA
0.000035
0.001
TCDDs (All Tetra chloro -
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetra chloro -
dibenzo furans)
NA
0.000063
0.001
K100
Waste leaching solution from acid leaching of emission control dust or sludge
from secondary lead smelting.
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Lead
7439-92-1
0.69
0.37 mg/l TCLP
K101
Distillation tar residues from the distillation of aniline-based compounds in
the production of veterinary pharmaceuticals from arsenic or organo-arsenic
compounds.
o-Nitro aniline
88-74-4
0.27
14
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
K102
Residue from the use of activated carbon for decolorization in the production
of veterinary pharmaceuticals from arsenic or organo-arsenic compounds.
o-Nitro phenol
88-75-5
0.028
13
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Cadmium
7440-43-9
0.69
NA
Lead
7439-92-1
0.69
NA
Mercury
7439-97-6
0.15
NA
K103
Process residues from aniline extraction from the production of aniline.
Aniline
62-53-3
0.81
14
Benzene
71-43-2
0.14
10
2,4-Dinitro phenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
K104
Combined wastewater streams generated from nitro
benzene or aniline production.
Aniline
62-53-3
0.81
14
438
Benzene
71-43-2
0.14
10
2,4-Dinitro phenol
51-28-5
0.12
160
Nitrobenzene
98-95-3
0.068
14
Phenol
108-95-2
0.039
6.2
Cyanides (Total)
7
57-12-5
1.2
590
K105
Separated aqueous stream from the reactor product washing step in the
production of chloro
benzenes.
Benzene
71-43-2
0.14
10
Chloro benzene
108-90-7
0.057
6.0
2-Chloro phenol
95-57-8
0.044
5.7
o-Dichloro benzene
95-50-1
0.088
6.0
p-Dichloro benzene
106-46-7
0.090
6.0
Phenol
108-95-2
0.039
6.2
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine
production) nonwastewaters that contain greater than or equal to 260 mg/kg
total mercury.
Mercury
7439-97-6
NA
RMERC
K106
K106 (wastewater treatment sludge from the mercury cell process in chlorine
production) nonwastewaters that contain less than 260 mg/kg total mercury that
are residues from RMERC.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
K106
Other K106 nonwastewaters that contain less than 260 mg/kg total mercury and
are not residues from RMERC.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
K106
All K106 wastewaters.
Mercury
7439-97-6
0.15
NA
K107
Column bottoms from product separation from the production of 1,1-dimethyl
-
hydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
INCINCMBST; or
CHOXD fb
CARBN; or
BIODG fb CARBN
INCINCMBST
K108
Condensed column overheads from product separation and condensed reactor vent
gases from the production of 1,1-dimethyl
hydrazine (UDMH) from ca
rboxylic acid
hydrazides.
NA
NA
INCINCMBST; or
CHOXD fb
CARBN; or
BIODG fb CARBN
INCINCMBST
K109
Spent filter cartridges from product purification from the production of 1,1-
dimethyl hydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
INCINCMBST; or
INCINCMBST
439
CHOXD fb
CARBN; or
BIODG fb CARBN
K110
Condensed column overheads from intermediate separation from the production of
1,1-dimethyl hydrazine (UDMH) from carboxylic acid hydrazides.
NA
NA
INCINCMBST; or
CHOXD fb
CARBN; or
BIODG fb CARBN
INCINCMBST
K111
Product washwaters from the production of dinitro
toluene via nitration of
toluene
2,4-Dinitro toluene
121-1-1
0.32
140
2,6-Dinitro toluene
606-20-2
0.55
28
K112
Reaction by-product water from the drying column in the production of
toluenediamine via hydro
genation of dinitro
toluene.
NA
NA
INCINCMBST; or
CHOXD fb
CARBN; or
BIODG fb CARBN
INCINCMBST
K113
Condensed liquid light ends from the purification of toluenediamine in the
production of toluenediamine via hydro
genation of dinitro
toluene.
NA
NA
CARBN; or
INCINCMBST
CMBST
K114
Vicinals from the purification of toluenediamine in the production of
toluenediamine via hydro
genation of dinitro
toluene.
NA
NA
CARBN; or
INCINCMBST
CMBST
K115
Heavy ends from the purification of toluenediamine in the production of
toluenediamine via hydro
genation of dinitro
toluene.
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
NA
NA
CARBN; or
INCINCMBST
CMBST
K116
Organic condensate from the solvent recovery column in the production of
toluene diisocyanate via phosgenation of toluenediamine.
NA
NA
CARBN; or
INCINCMBST
CMBST
K117
Wastewater from the reactor vent gas scrubber in the production of ethylene
dibromide via bromination of ethene.
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
Chloro form
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
K118
440
Spent absorbent solids from purification of ethylene dibromide in the
production of ethylene dibromide via bromination of ethene.
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
Chloro form
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
K123
Process wastewater (including supernates, filtrates, and washwaters) from the
production of ethylene
bisdithio carbamic acid and its salts.
NA
NA
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN)
INCINCMBST
K124
Reactor vent scrubber water from the production of ethylene
bisdithio carbamic
acid and its salts.
NA
NA
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN)
INCINCMBST
K125
Filtration, evaporation, and centrifugation solids from the production of
ethylene bisdithio carbamic acid and its salts.
NA
NA
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN)
INCINCMBST
K126
Baghouse dust and floor sweepings in milling and packaging operations from the
production or formulation of ethylene
bisdithio carbamic acid and its salts.
NA
NA
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN)
INCINCMBST
K131
Wastewater from the reactor and spent sulfuric acid from the acid dryer from
the production of methyl bromide.
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
K132
Spent absorbent and wastewater separator solids from the production of methyl
bromide.
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
K136
Still bottoms from the purification of ethylene dibromide in the production of
ethylene dibromide via bromination of ethene.
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
Chloro form
67-66-3
0.046
6.0
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
K141
441
Process residues from the recovery of coal tar, including, but not limited to,
collecting sump residues from the production of coke or the recovery of coke
by-products produced from coal. This listing does not include K087 (decanter
tank tar sludge from coking operations).
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-2-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
8.2
Indeno(1,2,3-cd) pyrene
193-39-5
0.0055
3.4
K142
Tar storage tank residues from the production of coke from coal or from the
recovery of coke by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
8.2
Ideno(1,2,3-cd) pyrene
193-39-5
0.0055
3.4
K143
Process residues from the recovery of light oil, including, but not limited
to, those generated in stills, decanters, and wash oil recovery units from the
recovery of coke by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
K144
Wastewater sump residues from light oil refining, including, but not limited
to, intercepting or contamination sump sludges from the recovery of coke by-
products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
442
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
8.2
K145
Residues from naphthalene collection and recovery operations from the recovery
of coke by-products produced from coal.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
6.28.2
Naphthalene
91-20-3
0.059
5.6
K147
Tar storage tank residues from coal tar refining.
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
8.2
Indeno(1,2,3-cd) pyrene
193-39-5
0.0055
3.4
K148
Residues from coal tar distillation, including, but not limited to, still
bottoms.
Benz(a)anthracene
56-55-3
0.059
3.4
Benzo(a)pyrene
50-32-8
0.061
3.4
Benzo(b)fluoranthene
(difficult to
distinguish from benzo
-
(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from benzo
-
(b)fluoranthene)
207-08-9
0.11
6.8
Chrysene
218-01-9
0.059
3.4
Dibenz(a,h)anthra
cene
53-70-3
0.055
8.2
Indeno(1,2,3-cd) pyrene
193-39-5
0.0055
3.4
K149
Distillation bottoms from the production of alpha- (or methyl-) chlorinated
toluenes, ring-chlorinated toluenes, benzoyl chlorides, and compounds with
mixtures of these functional groups. (This waste does not include still
bottoms from the distillations of benzyl chloride.)
Chloro benzene
108-90-7
0.057
6.0
443
Chloro form
67-66-3
0.046
6.0
Chloro methane
74-87-3
0.19
30
p-Dichloro benzene
106-46-7
0.090
6.0
Hexachloro benzene
118-74-1
0.055
10
Pentachloro benzene
608-93-5
0.055
10
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
Toluene
108-88-3
0.080
10
K150
Organic residuals, excluding spent carbon adsorbent, from the spent chlorine
gas and hydro chloric acid recovery processes associated with the production of
alpha- (or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional groups.
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro form
67-66-3
0.046
6.0
Chloro methane
74-87-3
0.19
30
p-Dichloro benzene
106-46-7
0.090
6.0
Hexachloro benzene
118-74-1
0.055
10
Pentachloro benzene
608-93-5
0.055
10
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
1,1,2,2- Tetra chloro -
ethane
79-34-5
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
1,2,4-Trichloro benzene
120-82-1
0.055
19
K151
Wastewater treatment sludges, excluding neutralization and biological sludges,
generated during the treatment of wastewaters from the production of alpha-
(or methyl-) chlorinated toluenes, ring-chlorinated toluenes, benzoyl
chlorides, and compounds with mixtures of these functional groups.
Benzene
71-43-2
0.14
10
Carbon tetra chloride
56-23-5
0.057
6.0
Chloro form
67-66-3
0.046
6.0
Hexachloro benzene
118-74-1
0.055
10
Pentachloro benzene
608-93-5
0.055
10
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
Tetrachloro ethylene
127-18-4
0.056
6.0
Toluene
108-88-3
0.080
10
K156
Organic waste (including heavy ends, still bottoms, light ends, spent
solvents, filtrates, and decantates) from the production of carbamates and
carbamoyl oximes. (This listing does not apply to wastes generated from the
manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Acetonitrile
75-05-8
5.6
38
Acetophenone
96-86-2
0.010
9.7
Aniline
62-53-3
0.81
14
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbaryl
63-25-21
0.006
0.14
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chlorobenzene
108-90-7
0.057
6.0
Chloroform
67-66-3
0.046
6.0
o-Dichlorobenzene
95-50-1
0.088
6.0
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
444
Methyl ethyl ketone
78-93-3
0.28
36
Naphthalene
91-20-3
0.059
5.6
Phenol
108-95-2
0.039
6.2
Pyridine
110-86-1
0.014
16
Toluene
108-88-3
0.080
10
Triethylamine
121-44-8
0.081
1.5
K157
Wastewaters (including scrubber waters, condenser waters, washwaters, and
separation waters) from the production of carbamates and carbamoyl oximes.
(This listing does not apply to wastes generated from the manufacture of 3-
iodo-2-propyl-n-butylcarbamate.)
10
Carbon tetrachloride
56-23-5
0.057
6.0
Chloroform
67-66-3
0.046
6.0
Chloromethane
74-87-3
0.19
30
Methomyl
16752-77-5
0.028
0.14
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
o-Phenylenediamine
95-54-5
0.056
5.6
Pyridine
110-86-1
0.014
16
Triethylamine
121-44-8
0.081
1.5
K158
Bag house dusts and filter/separation solids from the production of carbamates
and carbamoyl oximes. (This listing does not apply to wastes generated from
the manufacture of 3-iodo-2-propyl-n-butylcarbamate.)
10
Benomyl
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Carbenzadim
10605-21-7
0.056
1.4
Carbofuran
1563-66-2
0.006
0.14
Carbosulfan
55285-14-8
0.028
1.4
Chloroform
67-66-3
0.046
6.0
Methylene chloride
75-09-2
0.089
30
Phenol
108-95-2
0.039
6.2
K159
Organics from the treatment of thiocarbamate wastes.
10
Benzene
71-43-2
0.14
10
Butylate
2008-41-5
0.042
1.4
EPTC (Eptam)
759-94-4
0.042
1.4
Molinate
2212-67-1
0.042
1.4
Pebulate
1114-71-2
0.042
1.4
Vernolate
1929-77-7
0.042
1.4
K161
Purification solids (including filtration, evaporation, and centrifugation
solids), baghouse dust and floor sweepings from the production of
dithiocarbamate acids and their salts.
10
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
Arsenic
7440-38-2
1.9
5.0 mg/l TCLP
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Dithiocarbamates (total)
NA
0.028
28
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P001
Warfarin, & salts, when present at con
centrations greater than 0.3%
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
445
P002
1-Acetyl-2-thio urea
1-Acetyl-2-thio urea
591-08-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P003
Acrolein
Acrolein
107-02-6 107-
02-8
0.29
CMBST
P004
Aldrin
Aldrin
309-00-2
0.021
0.0680.066
P005
Allyl alcohol
Allyl alcohol
107-18-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
P006
Aluminum phosphide
Aluminum phosphide
20859-73-
620859-73-8
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
P007
5-Aminomethyl-3-isoxazolol
5-Aminomethyl-3-isoxa
-
zolol
2763-96-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P008
4-Aminopyridine
4-Aminopyridine
504-24-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P009
Ammonium picrate
Ammonium picrate
131-74-8
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
P010
Arsenic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P011
Arsenic pentoxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P012
Arsenic trioxide
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
446
P013
Barium cyanide
Barium
7440-39-3
NA
7.6 mg/l TCLP
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P014
Thiophenol (Benzen e thiol)
Thiophenol (Benzene
thiol)
108-98-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P015
Beryllium dust
Beryllium
7440-41-7
RMETL;or RTHRM
RMETL; or
RTHRM
P016
Dichloro methyl ether (Bis(chloro
methyl) ether)
Dichloro methyl ether
542-88-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P017
Bromoacetone
Bromoacetone
598-31-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P018
Brucine
Brucine
357-57-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P020
2-sec-Butyl-4,6-dinitro
phenol (Dinoseb)
2-sec-Butyl-4,6-dinitro
-
phenol (Dinoseb)
88-85-7
0.066
2.5
P021
Calcium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P022
Carbon disulfide
Carbon disulfide
75-15-0
3.8
INCINCMBST
Carbon disulfide;
alternate
6
standard for
nonwastewaters only
75-15-0
NA
4.8 mg/l TCLP
P023
Chloro acetaldehyde
Chloro acetaldehyde
107-20-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
447
INCINCMBST
P024
p-Chloro aniline
p-Chloro aniline
106-47-8
0.46
16
P026
1-(o-Chloro phenyl) thiourea
1-(o-Chloro phenyl) thio-
urea
5344-82-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P027
3-Chloro propionitrile
3-Chloro propio nitrile
542-76-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P028
Benzyl chloride
Benzyl chloride
100-44-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P029
Copper cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P030
Cyanides (soluble salts and complexes)
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P031
Cyanogen
Cyanogen
460-19-5
CHOXD; WETOX;
or INCINCMBST
CHOXD; WETOX;
or INCINCMBST
P033
Cyanogen chloride
Cyanogen chloride
506-77-4
CHOXD; WETOX;
or INCINCMBST
CHOXD; WETOX;
or INCINCMBST
P034
2-Cyclo hexyl-4,6-dinitro
phenol
2-Cyclo hexyl-4,6-
dinitro phenol
131-89-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P036
Dichloro phenyl arsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P037
Dieldrin
Dieldrin
60-57-1
0.017
0.13
448
P038
Diethyl arsine
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
P039
Disulfoton
Disulfoton
298-04-4
0.017
6.2
P040
O,O-Diethyl-O-pyrazinyl-phosphorothioate
O,O-Diethyl-O-pyrazinyl
-
phosphoro thioate
297-97-2
CARBN; or
INCINCMBST
CMBST
P041
Diethyl-p-nitro phenyl phosphate
Diethyl-p-nitrophenyl
phosphate
311-45-5
CARBN; or
INCINCMBST
CMBST
P042
Epinephrine
Epinephrine
51-43-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P043
Diisopropyl fluoro phosphate (DFP)
Diisopropyl fluoro -
phosphate (DFP)
55-91-4
CARBN; or
INCINCMBST
CMBST
P044
Dimethoate
Dimethoate
60-51-5
CARBN; or
INCINCMBST
CMBST
P045
Thiofanox
Thiofanox
39196-18-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P046
alpha,alpha-Dimethyl
phenethyl amine
alpha,alpha-Di methyl -
phenethyl amine
122-09-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P047
4,6-Dinitro-o-cresol
4,6-Dinitro-o-cresol
543-52-1
0.28
160
P047
4,6-Dinitro-o-cresol salts
NA
NA
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
449
P048
2,4-Dinitro phenol
2,4-Dinitro phenol
51-28-5
0.12
160
P049
Dithio biuret
Dithio biuret
541-53-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P050
Endosulfan
Endosulfan I
939-98-8
0.023
0.066
Endosulfan II
33213-6-5
0.029
0.13
Endosulfan sulfate
1031-07-8
0.029
0.13
P051
Endrin
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
P054
Aziridine
Aziridine
151-56-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P056
Fluorine
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb NEUTR
P057
Fluoro acetamide
Fluoro acetami de
640-19-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P058
Fluoro acetic acid, sodium salt
Fluoro acetic acid,
sodium salt
62-74-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P059
Heptachlor
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
P060
Isodrin
Isodrin
465-73-6
0.021
0.066
P062
Hexaethyl tetra phosphate
Hexaethyl tetra phosphate
757-58-4
CARBN; or
INCINCMBST
CMBST
450
P063
Hydrogen cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P064
Isocyanic acid, ethyl ester
Isocyanic acid, ethyl
ester
624-83-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P065
P065 (mercury fulminate) nonwastewaters, regardless of their total mercury
contant content , that are not incinerator residues or are not residues from
RMERC.
Mercury
7439-97-6
NA
IMERC
P065
P065 (mercury fulminate) nonwastewaters that are either incinerator residues
or are residues from RMERC; and contain greater than or equal to 260 mg/kg
total mercury.
Mercury
7339-97-6
NA
RMERC
P065
P065 (mercury fulminate) nonwastewaters that are residues from RMERC and
contain less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
P065
P065 (mercury fulminate) nonwastewaters that are incinerator residues and
contain less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
P065
All P065 (mercury fulminate) wastewaters.
Mercury
7439-97-6
0.15
NA
P066
Methomyl
Methomyl
16752-77-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P067
2-Methyl-aziridine
2-Methyl-aziridine
75-55-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P068
Methyl hydrazine
Methyl hydrazine
60-34-4
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED,
or CMBST
P069
451
2-Methyl lactonitrile
2-Methyl lactonitrile
75-86-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P070
Aldicarb
Aldicarb
116-06-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P071
Methyl parathion
Methyl parathion
298-00-0
0.014
4.6
P072
1-Naphthyl-2-thio
urea
1-Naphthyl-2-thio
urea
86-88-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P073
Nickel carbonyl
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
P074
Nickel cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
P075
Nicotine and salts
Nicotine and salts
54-11-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P076
Nitric oxide
Nitric oxide
10102-43-9
ADGAS
ADGAS
P077
p-Nitro aniline
p-Nitro aniline
100-01-6
0.028
28
P078
Nitrogen dioxide
Nitrogen dioxide
10102-44-0
ADGAS
ADGAS
P081
Nitroglycerin
Nitroglycerin
55-63-0
CHOXD; CHRED;
CARBN; BIODG
or INCINCMBST
CHOXD; CHRED;
or CMBST
P082
N-Nitroso dimethyl amine
452
N-Nitroso dimethyl amine
62-75-9
0.40
2.3
P084
N-Nitroso methyl vinylamine
N-Nitroso methyl vinyl-
amine
4549-40-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P085
Octamethyl pyrophosphoramide
Octamethyl pyrophosphor -
amide
152-16-9
CARBN; or
INCINCMBST
CMBST
P087
Osmium tetroxide
Osmium tetroxide
20816-12-0
RMETL; or
RTHRM
RMETL; or
RTHRM
P088
Endothall
Endothall
145-73-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
P089
Parathion
Parathion
56-38-2
0.014
4.6
P092
P092 (phenyl mercuric acetate) nonwastewaters, regardless of their total
mercury content, that are not incinerator residues or are not residues from
RMERC.
Mercury
7439-97-6
NA
IMERC; or
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are either incinerator
residues or are residues from RMERC; and still contain greater than or equal
to 260 mg/kg total mercury.
Mercury
7439-97-6
NA
RMERC
P092
P092 (phenyl mercuric acetate) nonwastewaters that are residues from RMERC and
contain less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
P092
P092 (phenyl mercuric acetate) nonwastewaters that are incinerator residues
and contain less than 260 mg/kg total mercury.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
P092
All P092 (phenyl mercuric acetate) wastewaters.
Mercury
7439-97-6
0.15
NA
P093
Phenyl thiourea
Phenyl thiourea
103-85-5
(WETOX or
INCINCMBST
453
CHOXD) fb
CARBN; or
INCINCMBST
P094
Phorate
Phorate
298-02-2
0.021
4.6
P095
Phosgene
Phosgene
75-44-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P096
Phosphine
Phosphine
7803-51-2
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
P097
Famphur
Famphur
52-85-7
0.017
15
P098
Potassium cyanide.
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P099
Potassium silver cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 mg/l TCLP
P101
Ethyl cyanide (Propanenitrile)
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
P102
Propargyl alcohol
Propargyl alcohol
107-19-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
P103
Selenourea
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P104
Silver cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
Silver
7440-22-4
0.43
0.30 mg/l TCLP
P105
Sodium azide
Sodium azide
26628-22-8
CHOXD; CHRED;
CARBN; BIODG;
CHOXD; CHRED;
or CMBST
454
or INCINCMBST
P106
Sodium cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P108
Strychnine and salts
Strychnine and salts
57-24-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P109
Tetraethyldithio pyrophosphate
Tetraethyldithio pyro-
phosphate
3689-24-5
CARBN; or
INCINCMBST
CMBST
P110
Tetraethyl lead
leadLead
7439-92-1
0.69
0.37 mg/l TCLP
P111
Tetraethylpyrophosphate
Tetraethylpyrophosphate
107-49-3
CARBN; or
INCINCMBST
CMBST
P112
Tetranitromethane
Tetranitromethane
509-14-8
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
P113
Thallic oxide
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P114
Thallium selenite
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
P115
Thallium (I) sulfate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
P116
Thiosemicarbazide
Thiosemicarbazide
79-19-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
P118
Trichloro methanethiol
Trichloro methane thiol
75-70-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
455
P119
Ammonium vanadate
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P120
Vanadium pentoxide
Vanadium (measured in
wastewaters only)
7440-62-2
4.3
STABL
P121
Zinc cyanide
Cyanides (Total)
7
57-12-5
1.2
590
Cyanides (Amenable)
7
57-12-5
0.86
30
P122
Zinc phosphide Zn
3
P
2
, when present at con
centrations greater than 10%
Zinc Phosphide
1314-84-7
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
P123
Toxaphene
Toxaphene
8001-35-2
0.0095
2.6
P127
Carbofuran
10
Carbofuran
1563-66-2
0.006
0.14
P128
Mexacarbate
10
Mexacarbate
315-18-4
0.056
1.4
P185
Tirpate
10
Tirpate
26419-73-8
0.056
0.28
P188
Physostigimine salicylate
10
Physostigmine salicylate
57-64-7
0.056
1.4
P189
Carbosulfan
10
Carbosulfan
55285-14-8
0.028
1.4
P190
Metolcarb
10
Metolcarb
1129-41-5
0.056
1.4
P191
Dimetilan
10
Dimetilan
644-64-4
0.056
1.4
P192
Isolan
10
Isolan
119-38-0
0.056
1.4
P194
Oxamyl
10
Oxamyl
23135-22-0
0.056
0.28
P196
456
Manganese dimethyldithiocarbamates (total)
10
Dithiocarbamates (total)
NA
0.028
28
P197
Formparanate
10
Formparanate
17702-57-7
0.056
1.4
P198
Formetanate hydrochloride
10
Formetanate hydro
-
chloride
23422-53-9
0.056
1.4
P199
Methiocarb
10
Methiocarb
2032-65-7
0.056
1.4
P201
Promecarb
10
Promecarb
2631-37-0
0.056
1.4
P202
m-Cumenyl methylcarbamate
10
m-Cumenyl methyl -
carbamate
64-00-6
0.056
1.4
P203
Aldicarb sulfone
10
Aldicarb sulfone
1646-88-4
0.056
0.28
P204
Physostigmine
10
Physostigmine
57-47-6
0.056
1.4
P205
Ziram
10
Dithiocarbamates (total)
NA
0.028
28
U001
Acetaldehyde
Acetaldehyde
75-07-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U002
Acetone
Acetone
67-64-1
0.28
160
U003
Acetonitrile
Acetonitrile
75-05-8
5.6
INCINCMBST
Acetonitrile; alternate
6
standard for
nonwastewaters only
75-05-8
NA
1.838
U004
Acetophenone
Acetophenone
98-86-2
0.010
9.7
U005
2-Acetylaminofluorene
457
2-Acetylaminofluorene
53-96-3
0.059
140
U006
Acetyl chloride
Acetyl chloride
75-36-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U007
Acrylamide
Acrylamide
79-06-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U008
Acrylic acid
Acrylic acid
79-10-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U009
Acrylonitrile
Acrylonitrile
107-13-1
0.24
84
U010
Mitomycin C
Mitomycin C
50-07-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U011
Amitrole
Amitrole
61-82-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U012
Aniline
Aniline
62-53-3
0.81
14
U014
Auramine
Auramine
492-80-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U015
Azaserine
Azaserine
115-02-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U016
Benz(c)acridine
458
Benz(c)acridine
225-51-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U017
Benzal chloride
Benzal chloride
98-87-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U018
Benz(a)anthracene
Benz(a)anthracene
56-55-3
0.059
3.4
U019
Benzene
Benzene
71-43-2
0.14
10
U020
Benzenesulfonyl chloride
Benzenesulfonyl chloride
98-09-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U021
Benzidine
Benzidine
92-87-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U022
Benzo(a)pyrene
Benzo(a)pyrene
50-32-8
0.061
3.4
U023
Benzotrichloride
Benzotrichloride
98-07-7
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U024
bis(2-Chloro ethoxy) methane
bis(2-Chloro ethoxy) -
methane
111-91-1
0.036
7.2
U025
bis(2-Chloro ethyl) ether
bis(2-Chloro ethyl) ether
111-44-4
0.033
6.0
U026
Chlornaphazine
Chlornaphazine
494-03-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U027
459
bis(2-Chloro isopropyl) ether
bis(2-Chloro isopropyl) -
ether
108-60-1 39638-
32-9
0.055
7.2
U028
bis(2-Ethyl hexyl) phthalate
bis(2-Ethyl hexyl) -
phthalate
117-81-7
0.28
28
U029
Methyl bromide (Bromo
methane)
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
U030
4-Bromo phenyl phenyl ether
4-Bromo phenyl phenyl
ether
101-55-3
0.055
15
U031
n-Butyl alcohol
n-Butyl alcohol
71-36-3
5.6
2.6
U032
Calcium chromate
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
U033
Carbon oxyfluoride
Carbon oxyfluoride
353-50-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U034
Trichloro acetaldehyde (Chloral)
Trichloro acetaldehyde
(Chloral)
75-87-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U035
Chlorambucil
Chlorambucil
305-03-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U036
Chlordane
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033
0.26
U037
Chloro benzene
Chloro benzene
108-90-7
0.057
6.0
U038
Chloro benzilate
Chloro benzilate
510-15-6
0.10
INCINCMBST
U039
460
p-Chloro-m-cresol
p-Chloro-m-cresol
59-50-7
0.018
14
U041
Epichloro hydrin (1-Chloro-2,3-epoxypropane)
Epichloro hydrin (1-
Chloro-2,3-epoxypropane)
106-89-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U042
2-Chloro ethyl vinyl ether
2-Chloro ethyl vinyl
ether
110-75-8
0.062
INCINCMBST
U043
Vinyl chloride
Vinyl chloride
75-01-4
0.27
6.0
U044
Chloro form
Chloro form
67-66-3
0.046
6.0
U045
Chloro methane (Methyl chloride)
Chloro methane (Methyl
chloride)
74-87-3
0.19
30
U046
Chloro methyl methyl e ther
Chloro methyl methyl
ether
107-30-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U047
2-Chloro naphthalene
2-Chloro naphthalene
91-58-7
0.055
5.6
U048
2-Chloro phenol
2-Chloro phenol
95-57-8
0.044
5.7
U049
4-Chloro-o-toluidine hydro
chloride
4-Chloro-o-toluidine
hydrochloride
3165-93-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U050
Chrysene
Chrysene
218-01-9
0.059
3.4
U051
Creosote
Naphthalene
91-20-3
0.059
5.6
Pentachloro phenol
87-86-5
0.089
7.4
Phenanthrene
85-01-8
0.059
5.6
Pyrene
129-00-0
0.067
8.2
Toluene
108-88-3
0.080
10
461
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U052
Cresols (Cresylic acid)
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
Cresol-mixed isomers
(Cresylic acid)
(sum of o -, m-, and p-
cresol con centrations)
1319-77-3
0.88
11.2
U053
Crotonaldehyde
Crotonaldehyde
4170-30-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U055
Cumene
Cumene
98-82-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U056
Cyclohexane
Cyclohexane
110-82-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U057
Cyclohexanone
Cyclohexanone
108-94-1
0.36
CMBST
Cyclohexanone;
alternate
6
standard for
nonwastewaters only
108-94-1
NA
0.75 mg/l TCLP
U058
Cyclophosphamide
Cyclophosphamide
50-18-0
CARBN; or
INCINCMBST
CMBST
U059
Daunomycin
Daunomycin
20830-81-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U060
DDD
o,p'-DDD
53-19-0
0.023
0.087
462
p,p'-DDD
72-54-8
0.023
0.087
U061
DDT
o,p'-DDT
789-02-6
0.0039
0.087
p,p'-DDT
50-29-3
0.0039
0.087
o,p'-DDD
53-19-0
0.023
0.087
p,p'-DDD
72-54-8
0.023
0.087
o,p'-DDE
3424-82-6
0.031
0.087
p,p'-DDE
72-55-9
0.031
0.087
U062
Diallate
Diallate
2303-16-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U063
Dibenz(a,h)anthracene
Dibenz(a,h)anthracene
53-70-3
0.055
8.2
U064
Dibenz(a,i)pyrene
Dibenz(a,i)pyrene
189-55-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U066
1,2-Dibromo-3-chloro
propane
1,2-Dibromo-3-chloro
-
propane
96-12-8
0.11
15
U067
Ethylene dibromide (1,2-Dibromo
ethane)
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
U068
Dibromo methane
Dibromo methane
74-95-3
0.11
15
U069
Di-n-butyl phthalate
Di-n-butyl phthalate
84-74-2
0.057
28
U070
o-Dichloro benzene
o-Dichloro benzene
95-50-1
0.088
6.0
U071
m-Dichloro benzene
m-Dichloro benzene
541-73-1
0.036
6.0
U072
p-Dichloro benzene
p-Dichloro benzene
106-46-7
0.090
6.0
U073
3,3'-Dichloro benzidine
463
3,3'-Dichloro benzidine
91-94-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U074
1,4-Dichloro-2-butene
cis-1,4-Dichloro-2-
butene
1476-11-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
trans-1,4-Dichloro-2-
butene
764-41-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U075
Dichloro difluoro methane
Dichloro difluoro methane
75-71-8
0.23
7.2
U076
1,1-Dichloro ethane
1,1-Dichloro ethane
75-34-3
0.059
6.0
U077
1,2-Dichloro ethane
1,2-Dichloro ethane
107-06-2
0.21
6.0
U078
1,1-Dichloro ethylene
1,1-Dichloro ethylene
75-35-4
0.025
6.0
U079
1,2-Dichloro ethylene
trans-1,2-Dichloro
-
ethylene
156-60-5
0.054
30
U080
Methylene chloride
Methylene chloride
75-09-2
0.089
30
U081
2,4-Dichloro phenol
2,4-Dichloro phenol
120-83-2
0.044
14
U082
2,6-Dichloro phenol
2,6-Dichloro phenol
87-65-0
0.044
14
U083
1,2-Dichloro propane
1,2-Dichloro propane
78-87-5
0.85
18
U084
1,3-Dichloro propylene
cis-1,3-Dichloro -
propylene
10061-01-5
0.036
18
trans-1,3-Dichloro
-
propylene
10061-02-6
0.036
18
U085
1,2:3,4-Diepoxybutane
464
1,2:3,4-Diepoxybutane
1464-53-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U086
N,N'-Diethyl hydrazine
N,N'-Diethyl hydrazine
1615-80-1
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U087
O,O-Diethyl -S-methyl dithio phosphate
O,O-Diethyl -S-methyl -
dithio phosphate
3288-58-2
CARBN; or
INCINCMBST
CMBST
U088
Diethyl phthalate
Diethyl phthalate
84-66-2
0.20
28
U089
Diethyl stilbestrol
Diethyl stilbestrol
56-53-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U090
Dihydro safrole
Dihydro safrole
94-58-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U091
3,3'-Dimethoxybenzidine
3,3'-Dimethoxybenzidine
119-90-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U092
Dimethyl amine
Dimethyl amine
124-40-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U093
p-Dimethyl aminoazobenzene
p-Dimethyl -
aminoazobenzene
60-11-7
0.13
INCINCMBST
U094
7,12-Dimethyl benz(a) anthracene
7,12-Dimethyl benz(a) -
anthracene
57-97-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U095
465
3,3'-Dimethyl benzidine
3,3'-Dimethyl benzidine
119-93-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U096
alpha, alpha-Dimethyl benzyl hydro
peroxide
alpha, alpha-Dimethyl
benzyl hydro peroxide
80-15-9
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U097
Dimethyl carbamoyl chloride
Dimethyl carbamoyl
chloride
79-44-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U098
1,1-Dimethyl hydrazine
1,1-Dimethyl hydrazine
57-14-7
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U099
1,2-Dimethyl hydrazine
1,2-Dimethyl hydrazine
540-73-8
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U101
2,4-Dimethyl phenol
2,4-Dimethyl phenol
105-67-9
0.036
14
U102
Dimethyl phthalate
Dimethyl phthalate
131-11-3
0.047
28
U103
Dimethyl sulfate
Dimethyl sulfate
77-78-1
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U105
2,4-Dinitro toluene
2,4-Dinitro toluene
121-14-2
0.32
140
U106
2,6-Dinitro toluene
2,6-Dinitro toluene
606-20-2
0.55
28
U107
Di-n-octyl phthalate
Di-n-octyl phthalate
117-84-0
0.017
28
U108
1,4-Dioxane
1,4-Dioxane
123-91-1
(WETOX or
CHOXD) fb
CMBST
466
CARBN; or
INCINCMBST
1,4-Dioxane; alternate
6
standard for
nonwastewaters only
123-91-1
NA
170
U109
1,2-Diphenyl hydrazine
1,2-Diphenyl hydrazine
122-66-7
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
1,2-Diphenyl hydrazine;
alternate
6
standard for
wastewaters only
122-66-7
0.087
NA
U110
Dipropyl amine
Dipropyl amine
142-84-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U111
Di-n-propyl nitros amine
Di-n-propyl nitros amine
621-64-7
0.40
14
U112
Ethyl acetate
Ethyl acetate
141-78-8 141-
78-6
0.34
33
U113
Ethyl acrylate
Ethyl acrylate
140-88-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U114
Ethylene bisdithio carbamic acid salts and esters
Ethylene bisdithio -
carbamic acid
111-54-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U115
Ethylene oxide
Ethylene oxide
75-21-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CHOXD; or
INCINCMBST
Ethylene oxide;
alternate
6
standard for
wastewaters only
75-21-8
0.12
NA
U116
Ethylene thio urea
Ethylene thio urea
96-45-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
467
U117
Ethyl ether
Ethyl ether
60-29-7
0.12
160
U118
Ethyl methacrylate
Ethyl methacrylate
97-63-2
0.14
160
U119
Ethyl methane sulfonate
Ethyl methane sulfonate
62-50-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U120
Fluoranthene
Fluoranthene
206-44-0
0.068
3.4
U121
Trichloro monofluoro methane
Trichloro monofluoro -
methane
75-69-4
0.020
30
U122
Formaldehyde
Formaldehyde
50-00-0
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U123
Formic acid
Formic acid
64-18-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U124
Furan
Furan
110-00-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U125
Furfural
Furfural
98-01-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U126
Glycidylaldehyde
Glycidylaldehyde
765-34-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U127
468
Hexachloro benzene
Hexachloro benzene
118-74-1
0.055
10
U128
Hexachloro butadiene
Hexachloro butadiene
87-68-3
0.055
5.6
U129
Lindane
alpha-BHC
319-84-6
0.00014
0.066
beta-BHC
319-85-7
0.00014
0.066
delta-BHC
319-86-8
0.023
0.066
gamma-BHC (Lindane)
58-89-9
0.0017
0.066
U130
Hexachloro cyclopentadiene
Hexachloro cyclopenta-
diene
77-47-4
0.057
2.4
U131
Hexachloro ethane
Hexachloro ethane
67-72-1
0.055
30
U132
Hexachloro phene
Hexachloro phene
70-30-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U133
Hydrazine
Hydrazine
302-01-2
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U134
Hydrogen fluoride
Fluoride (measured in
wastewaters only)
16964-48-8
35
ADGAS fb
NEUTR; or
NEUTR
U135
Hydrogen sulfide
Hydrogen sulfide
7783-06-4
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
U136
Cacodylic acid
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
U137
Indeno(1,2,3-c ,d)pyrene
Indeno(1,2,3-c ,d)pyrene
193-39-5
0.0055
3.4
U138
Iodomethane
Iodomethane
74-88-4
0.19
65
U140
Isobutyl alcohol
469
Isobutyl alcohol
78-83-1
5.6
170
U141
Isosafrole
Isosafrole
120-58-1
0.081
2.6
U142
Kepone
Kepone
143-50-8
0.0011
0.13
U143
Lasiocarpine
Lasiocarpine
303-34-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U144
Lead acetate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U145
Lead phosphate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U146
Lead subacetate
Lead
7439-92-1
0.69
0.37 mg/l TCLP
U147
Maleic anhydride
Maleic anhydride
108-31-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U148
Maleic hydrazide
Maleic hydrazide
123-33-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U149
Malononitrile
Malononitrile
109-77-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U150
Melphalan
Melphalan
148-82-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U151
U151 (mercury) nonwastewaters that contain greater than or equal to 260 mg/kg
total mercury.
Mercury
7439-97-6
NA
RMERC
470
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury
and that are residues from RMERC only.
Mercury
7439-97-6
NA
0.20 mg/l TCLP
U151
U151 (mercury) nonwastewaters that contain less than 260 mg/kg total mercury
and that are not residues from RMERC only.
Mercury
7439-97-6
NA
0.025 mg/l
TCLP
U151
All U151 (mercury) wastewater.
Mercury
7439-97-6
0.15
NA
U151
Element Mercury Contaminated with Radioactive Materials
Mercury
7439-97-6
NA
AMLGM
U152
Methacrylonitrile
Methacrylonitrile
126-98-7
0.24
84
U153
Methanethiol
Methanethiol
74-93-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U154
Methanol
Methanol
67-56-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
Methanol; alternate
6
set
of standards for both
wastewaters and
nonwastewaters
67-56-1
5.6
0.75 mg/l TCLP
U155
Methapyrilene
Methapyrilene
91-80-5
0.081
1.5
U156
Methyl chloro carbonate
Methyl chloro carbonate
79-22-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U157
3-Methyl cholanthrene
3-Methyl cholanthrene
56-49-5
0.0055
15
U158
4,4'-Methylene bis(2-chloro
aniline )
4,4'-Methylene bis(2-
chloro aniline)
101-14-4
0.50
30
471
U159
Methyl ethyl ketone
Methyl ethyl ketone
78-93-3
0.28
36
U160
Methyl ethyl ketone peroxide
Methyl ethyl ketone
peroxide
1338-23-4
CHOXD; CHRED;
CARBN; BIODG;
or INCINCMBST
CHOXD; CHRED;
or CMBST
U161
Methyl isobutyl ketone
Methyl isobutyl ketone
108-10-1
0.14
33
U162
Methyl methacrylate
Methyl methacrylate
80-62-6
0.14
160
U163
N-Methyl-N'-nitro-N-nitroso
guanidine
N-Methyl-N'-nitro-N-
nitroso guanidine
70-25-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U164
Methyl thiouracil
Methyl thiouracil
56-04-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U165
Naphthalene
Naphthalene
91-20-3
0.059
5.6
U166
1,4-Naphthoquinone
1,4-Naphthoquinone
130-15-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U167
1-Naphthylamine
1-Naphthylamine
134-32-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U168
2-Naphthylamine
2-Naphthylamine
91-59-8
0.52
INCINCMBST
U169
Nitrobenzene
Nitrobenzene
98-95-3
0.068
14
U170
p-Nitro phenol
472
p-Nitro phenol
100-02-7
0.12
29
U171
2-Nitro propane
2-Nitro propane
79-46-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U172
N-Nitroso di-n-butyl amine
N-Nitroso di-n-butyl amine
924-16-3
0.40
17
U173
N-Nitroso diethanolamine
N-Nitroso diethanolamine
1116-54-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U174
N-Nitroso diethyl amine
N-Nitroso diethyl amine
55-18-5
0.40
28
U176
N-Nitroso-N-ethyl
urea
N-Nitroso-N-ethyl
urea
759-73-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U177
N-Nitroso-N-methyl
urea
N-Nitroso-N-methyl
urea
684-93-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U178
N-Nitroso-N-methyl
urethane
N-Nitroso-N-methyl
-
urethane
615-53-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U179
N-Nitroso piperidine
N-Nitroso piperidine
100-75-4
0.013
35
U180
N-Nitroso pyrrolidine
N-Nitroso pyrrolidine
930-55-2
0.013
35
U181
5-Nitro-o-toluidine
5-Nitro-o-toluidine
99-55-8
0.32
28
U182
Paraldehyde
Paraldehyde
123-63-7
(WETOX or
CHOXD) fb
CMBST
473
CARBN; or
INCINCMBST
U183
Pentachloro benzene
Pentachloro benzene
608-93-5
0.055
10
U184
Pentachloro ethane
Pentachloro ethane
76-01-7
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
Pentachloro ethane;
alternate
6
standards for
both wastewaters and
nonwastewaters
76-01-7
0.055
6.0
U185
Pentachloro nitrobenzene
Pentachloro nitrobenzene
82-68-8
0.055
4.8
U186
1,3-Penta diene
1,3-Penta diene
504-60-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U187
Phenacetin
Phenacetin
62-44-2
0.081
16
U188
Phenol
Phenol
108-95-2
0.039
6.2
U189
Phosphorus sulfide
Phosphorus sulfide
1314-80-3
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
U190
Phthalic anhydride
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
100-21-0
0.055
28
Phthalic anhydride
(measured as Phthalic
acid or Terephthalic
acid)
85-44-9
0.055
28
U191
2-Picoline
2-Picoline
109-06-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U192
474
Pronamide
Pronamide
23950-58-5
0.093
1.5
U193
1,3-Propane sultone
1,3-Propane sultone
1120-71-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U194
n-Propyl amine
n-Propyl amine
107-10-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U196
Pyridine
Pyridine
110-86-1
0.014
16
U197
p-Benzo quinone
p-Benzo quinone
106-51-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U200
Reserpine
Reserpine
50-55-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U201
Resorcinol
Resorcinol
108-46-3
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U202
Saccharin and salts
Saccharin
81-07-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U203
Safrole
Safrole
94-59-7
0.081
22
U204
Selenium dioxide
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
U205
Selenium sulfide
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
475
U206
Streptozotocin
Streptozotocin
18883-66-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U207
1,2,4,5-Tetra chloro benzene
1,2,4,5-Tetra chloro -
benzene
95-94-3
0.055
14
U208
1,1,1,2-Tetra chloro ethane
1,1,1,2-Tetra chloro -
ethane
630-20-6
0.057
6.0
U209
1,1,2,2-Tetra chloro ethane
1,1,2,2-Tetra chloro -
ethane
79-34-5
0.057
6.0
U210
Tetrachloro ethylene
Tetrachloro ethylene
127-18-4
0.056
6.0
U211
Carbon tetra chloride
Carbon tetra chloride
56-23-5
0.057
6.0
U213
Tetrahydrofuran
Tetrahydrofuran
109-99-9
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
U214
Thallium (I) acetate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U215
Thallium (I) carbonate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U216
Thallium (I) chloride
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U217
Thallium (I) nitrate
Thallium (measured in
wastewaters only)
7440-28-0
1.4
RTHRM; or
STABL
U218
Thioacetamide
Thioacetamide
62-55-5
(WETOX or
CHOXD) fb
INCINCMBST
476
CARBN; or
INCINCMBST
U219
Thiourea
Thiourea
62-56-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U220
Toluene
Toluene
108-88-3
0.080
10
U221
Toluenediamine
Toluenediamine
25376-45-8
CARBN; or
INCINCMBST
CMBST
U222
o-Toluidine hydro
chloride
o-Toluidine hydro
-
chloride
636-21-5
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U223
Toluene diisocyanate
Toluene diisocyanate
26471-62-5
CARBN; or
INCINCMBST
CMBST
U225
Bromoform (Tribromo methane)
Bromoform (Tribromo -
methane)
75-25-2
0.63
15
U226
1,1,1-Trichloro ethane
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
U227
1,1,2-Tricloroethane
1,1,2-Tricloroethane
79-00-5
0.054
6.0
U228
Trichloro ethylene
Trichloro ethylene
79-01-6
0.054
6.0
U234
1,3,5-Trinitro benzene
1,3,5-Trinitro benzene
99-35-4
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U235
tris-(2,3-Dibromo
propyl)-phosphate
tris-(2,3-Dibromo
-
propyl)-phosphate
126-72-7
0.11
0.10
U236
477
Trypan Blue
Trypan Blue
72-57-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U237
Uracil mustard
Uracil mustard
66-75-1
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U238
Urethane (Ethyl carbamate)
Urethane (Ethyl
carbamate)
51-79-6
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U239
Xylenes
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene con centrations)
1330-20-7
0.32
30
U240
2,4-D (2,4-Dichloro
phenoxyacetic acid)
2,4-D (2,4-Dichloro
-
phenoxyacetic acid)
94-75-7
0.72
10
2,4-D (2,4-Dichloro
-
phenoxyacetic acid)
salts and esters
NA
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U243
Hexachloro propylene
Hexachloro propylene
1888-71-7
0.035
30
U244
Thiram
Thiram
137-26-8
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
INCINCMBST
U246
Cyanogen bromide
Cyanogen bromide
506-68-3
CHOXD; WETOX;
or INCINCMBST
CHOXD; WETOX;
or INCINCMBST
U247
Methoxychlor
Methoxychlor
72-43-5
0.25
0.18
U248
Warfarin, & salts, when present at con
centrations of 0.3% or less
Warfarin
81-81-2
(WETOX or
CHOXD) fb
CARBN; or
INCINCMBST
CMBST
478
U249
Zinc phosphide, Zn
3
P
2
, when present at con
centrations of 10% or less
Zinc Phosphide
1314-84-7
CHOXD; CHRED;
or INCINCMBST
CHOXD; CHRED;
or INCINCMBST
U271
Benomyl
10
Benomyl
17804-35-2
0.056
1.4
U278
Bendiocarb
10
Bendiocarb
22781-23-3
0.056
1.4
U279
Carbaryl
10
Carbaryl
63-25-2
0.006
0.14
U280
Barban
10
Barban
101-27-9
0.056
1.4
U328
o-Toluidine
o-Toluidine
95-53-4
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb CARBN
INCINCMBST; or
Thermal
Destruction
U353
p-Toluidine
p-Toluidine
106-49-0
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb CARBN
INCINCMBST; or
Thermal
Destruction
U359
2-Ethoxyethanol
2-Ethoxyethanol
110-80-5
INCINCMBST; or
CHOXD fb
(BIODG or
CARBN); or
BIODG fb CARBN
CMBST
U364
Bendiocarb phenol
10
Bendiocarb phenol
22961-82-6
0.056
1.4
U367
Carbofuran phenol
10
Carbofuran phenol
1563-38-8
0.056
1.4
U372
Carbendazim
10
Carbendazim
10605-21-7
0.056
1.4
U373
Propham
10
Propham
122-42-9
0.056
1.4
479
U387
Prosulfocarb
10
Prosulfocarb
52888-80-9
0.042
1.4
U389
Triallate
10
Triallate
2303-17-5
0.042
1.4
U394
A2213
10
A2213
30558-43-1
0.042
1.4
U395
Diethylene glycol, dicarbamate
10
Diethylene glycol,
dicarbamate
5952-26-1
0.056
1.4
U404
Triethylamine
10
Triethylamine
101-44-8
0.081
1.5
U409
Thiophanate -methyl
10
Thiophanate -methyl
23564-05-8
0.056
1.4
U410
Thiodicarb
10
Thiodicarb
59669-26-0
0.019
1.4
U411
Propoxur
10
Propoxur
114-26-1
0.056
1.4
Notes:
1
The waste descriptions provided in this table do not replace waste
descriptions in 35 Ill. Adm. Code 721. Descriptions of Treatment or
Regulatory Subcategories are provided, as needed, to distinguish between
applicability of different standards.
2
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts
or esters, the CAS number is given for the parent compound only.
3
Concentration standards for wastewaters are expressed in mg/l
and are
based on analysis of composite samples.
4
All treatment standards expressed as a Technology Code or combination of
Technology Codes are explained in detail in 35 Ill. Adm. Code 728.Table
C, "Technology Codes and Descriptions of Technology-Based Standards".
"fb" inserted between waste codes denotes "followed by", so that the
first-listed treatment is followed by the second-listed treatment. ";"
separates alternative treatement schemes.
5
Except for Metals (EP or TCLP) and Cyanides (Total and Amenable) the
nonwastewater treatment standards expressed as a con
centration were
established, in part, based upon incineration in units operated in
accordance with the technical requirements of 35 Ill. Adm. Code
724.Subpart O or 35 Ill. Adm. Code 725.Subpart O
, or based upon
combustion in fuel substitution units operating in accordance with
480
applicable technical requirements. A facility may comply with these
treatment standards according to provisions in 35 Ill. Adm. Code
728.140(d). All con
centration standards for nonwastewaters are based on
analysis of grab samples.
6
Where an alternate treatment standard or set of alternate standards has
been indicated, a facility may comply with this alternate standard, but
only for the Treatment or Regulatory Subcategory or physical form (i.e.,
wastewater or nonwastewater) specified for that alternate standard.
7
Both Cyanide s (Total) and Cyanides (Amenable) for nonwastewaters are to
be analyzed using Method 9010 or 9012, found in "Test Methods for
Evaluating Solid Waste, Physical or Chemical Methods", USEPA Publication
SW-846, as incorporated by reference in 35 Ill. Adm. Code 720.111, with
a sample size of 10 grams and a distillation time of one hour and 15
minutes.
8
These wastes, when rendered nonhazardous and then subsequently managed
in CWA or CWA -equivalent systems are not subject to treatment standards.
(See Section 728.101(c)(3) and (c)(4)).
9
These wastes, when rendered nonhazardous and then subsequently injected
in a Class I SDWA well are not subject to treatment standards. (See 35
Ill. Adm. Code 738.101(d)).
10
This footnote corresponds with note 10 to the table to 40 CFR 268.40,
which has already expired by its own terms. This statement maintains
structural consistency with the federal regulations.
NA
means not applicable.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 728.Table U
Universal Treatment Standards (UTS)
Regulated Con stituent-
Common Name
CAS
1
No.
Wastewater
Standard
Concentration
(in mg/l
2
)
Nonwastewater
Standard
Concentration
(in mg/kg
3
unless noted as
"mg/l TCLP")
A2213
6
30558-43-1
0.042
1.4
Acenaphthylene
208-96-8
0.059
3.4
Acenaphthene
83-32-9
0.059
3.4
Acetone
67-64-1
0.28
160
Acetonitrile
75-05-8
5.6
1.838
Acetophenone
96-86-2
0.010
9.7
2-Acetylamino fluorene
53-96-3
0.059
140
Acrolein
107-02-8
0.29
NA
Acrylamide
79-06-1
19
23
Acrylonitrile
107-13-1
0.24
84
481
Aldicarb Sulfone
6
1646-88-4
0.056
0.28
Aldrin
309-00-2
0.021
0.066
4-Aminobiphenyl
92-67-1
0.13
NA
Aniline
62-53-3
0.81
14
Anthracene
120-12-7
0.059
3.4
Aramite
140-57-8
0.36
NA
alpha-BHC
319-84-6
0.00014
0.066
beta-BHC
319-85-7
0.00014
0.066
delta-BHC
319-86-8
0.023
0.066
gamma-BHC
58-89-9
0.0017
0.066
Barban
6
101-27-9
0.056
1.4
Bendiocarb
6
22781-23-3
0.056
1.4
Bendiocarb phenol
6
22961-82-6
0.056
1.4
Benomyl
6
17804-35-2
0.056
1.4
Benzene
71-43-2
0.14
10
Benz(a)anthracene
56-55-3
0.059
3.4
Benzal chloride
98-87-3
0.055
6.0
Benzene
71-43-2
0.14
10
Benzo(b)fluoranthene
(difficult to
distinguish from
benzo(k)fluoranthene)
205-99-2
0.11
6.8
Benzo(k)fluoranthene
(difficult to
distinguish from
benzo(b)fluoranthene)
207-08-9
0.11
6.8
Benzo(g,h,i)perylene
191-24-2
0.0055
1.8
Benzo(a)pyrene
50-32-8
0.061
3.4
Bromodichloro methane
75-27-4
0.35
15
Methyl bromide (Bromo
-
methane)
74-83-9
0.11
15
4-Bromo phenyl phenyl
ether
101-55-3
0.055
15
n-Butyl alcohol
71-36-3
5.6
2.6
Butylate
6
2008-41-5
0.042
1.4
482
Butyl benzyl phthalate
85-68-7
0.017
28
2-sec-Butyl-4,6-dinitro
-
phenol (Dinoseb)
88-85-7
0.066
2.5
Carbaryl
6
63-25-2
0.006
0.14
Carbenzadim
6
10605-21-7
0.056
1.4
Carbofuran
6
1563-66-2
0.006
0.14
Carbofuran phenol
6
1563-38-8
0.056
1.4
Carbon disulfide
75-15-0
3.8
4.8 mg/l TCLP
Carbon tetrachloride
56-23-5
0.057
6.0
Carbosulfan
6
55285-14-8
0.028
1.4
Chlordane (alpha and
gamma isomers)
57-74-9
0.0033
0.26
p-Chloro aniline
106-47-8
0.46
16
Chloro benzene
108-90-7
0.057
6.0
Chloro benzilate
510-15-6
0.10
NA
2-Chloro-1,3-butadiene
126-99-8
0.057
0.28
Chloro dibromo methane
124-48-1
0.057
15
Chloro ethane
75-00-3
0.27
6.0
bis(2-Chloro -
ethoxy)methane
111-91-1
0.036
7.2
bis(2-Chloro ethyl)ether
111-44-4
0.033
6.0
2-Chloro ethyl vinyl
ether
110-75-8
0.062
NA
Chloro form
67-66-3
0.046
6.0
bis(2-Chloro -
isopropyl)ether
108-60-1 39638-
32-9
0.055
7.2
p-Chloro-m-cresol
59-50-7
0.018
14
2-Chloro ethyl vinyl
ether
110-75-8
0.062
NA
Chloro methane (Methyl
chloride)
74-87-3
0.19
30
2-Chloro naphthalene
91-58-7
0.055
5.6
2-Chloro phenol
95-57-8
0.044
5.7
3-Chloro propylene
107-05-1
0.036
30
483
Chrysene
218-01-9
0.059
3.4
o-Cresol
95-48-7
0.11
5.6
m-Cresol (difficult to
distinguish from p-
cresol)
108-39-4
0.77
5.6
p-Cresol (difficult to
distinguish from m-
cresol)
106-44-5
0.77
5.6
m-Cumenyl methyl -
carbamate
6
64-00-6
0.056
1.4
Cyclohexanone
108-94-1
0.36
0.75 mg/l TCLP
1,2-Dibromo-3-chloro
-
propane
96-12-8
0.11
15
Ethylene dibromide (1,2-
Dibromo ethane)
106-93-4
0.028
15
Dibromo methane
74-95-3
0.11
15
2,4-D (2,4-Dichloro
-
phenoxyacetic acid)
94-75-7
0.72
10
o,p'-DDD
53-19-0
0.023
0.087
p,p'-DDD
72-54-8
0.023
0.087
o,p'-DDE
3424-82-6
0.031
0.087
p,p'-DDE
72-55-9
0.031
0.087
o,p'-DDT
789-02-6
0.0039
0.087
p,p'-DDT
50-29-3
0.0039
0.087
Dibenz(a,h) anthra cene
53-70-3
0.055
8.2
Dibenz(a,e)pyrene
192-65-4
0.061
NA
1,2-Dibromo-3-chloro
-
propane
96-12-8
0.11
15
1,2-Dibromo -
ethane/Ethylene
dibromide
106-93-4
0.028
15
Dibromo methane
74-95-3
0.11
15
m-Dichloro benzene
541-73-1
0.036
6.0
o-Dichloro benzene
95-50-1
0.088
6.0
p-Dichloro benzene
106-46-7
0.090
6.0
Dichloro difluoro methane
75-71-8
0.23
7.2
484
1,1-Dichloro ethane
75-34-3
0.059
6.0
1,2-Dichloro ethane
107-06-2
0.21
6.0
1,1-Dichloro ethylene
75-35-4
0.025
6.0
trans-1,2-Dichloro
-
ethylene
156-60-5
0.054
30
2,4-Dichloro phenol
120-83-2
0.044
14
2,6-Dichloro phenol
87-65-0
0.044
14
2,4-Dichloro -
phenoxyacetic acid/2,4-D
94-75-7
0.72
10
1,2-Dichloro propane
78-87-5
0.85
18
cis-1,3-Dichloro -
propylene
10061-01-5
0.036
18
trans-1,3-Dichloro
-
propylene
10061-02-6
0.036
18
Dieldrin
60-57-1
0.017
0.13
Diethylene glycol,
dicarbamate
6
5952-26-1
0.056
1.4
Diethyl phthalate
84-66-2
0.20
28
p-Dimethylaminoazo
-
benzene
60-11-7
0.13
NA
2,4-Dimethyl phenol
105-67-9
0.036
14
Dimethyl phthalate
131-11-3
0.047
28
Dimetilan
6
644-64-4
0.056
1.4
Di-n-butyl phthalate
84-74-2
0.057
28
1,4-Dinitro benzene
100-25-4
0.32
2.3
4,6-Dinitro-o-cresol
534-52-1
0.28
160
2,4-Dinitro phenol
51-28-5
0.12
160
2,4-Dinitro toluene
121-14-2
0.32
140
2,6-Dinitro toluene
606-20-2
0.55
28
Di-n-octyl phthalate
117-84-0
0.017
28
p-Dimethylaminoazo
-
benzene
60-11-7
0.13
NA
Di-n-propylnitros
amine
621-64-7
0.40
14
1,4-Dioxane
123-91-1
NA12.0
170
485
Diphenylamine (difficult
to distinguish from
diphenylnitrosamine)
122-39-4
0.92
13
Diphenylnitros amine
(difficult to
distinguish from
diphenylamine)
86-30-6
0.92
13
1,2-Diphenylhydrazine
122-66-7
0.087
NA
Disulfoton
298-04-4
0.017
6.2
Dithiocarbamates
(total)
6
137-30-4
0.028
28
Endosulfan I
939-98-8 959-98-
8
0.023
0.066
Endosulfan II
33213-6-5 33213-
65-9
0.029
0.13
Endosulfan sulfate
1-31-07-8 1031-
07-8
0.029
0.13
Endrin
72-20-8
0.0028
0.13
Endrin aldehyde
7421-93-4
0.025
0.13
EPTC
6
759-94-4
0.042
1.4
Ethyl acetate
141-78-6
0.34
33
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
Ethyl benzene
100-41-4
0.057
10
Ethyl cyanide
(Propanenitrile)
107-12-0
0.24
360
Ethyl ether
60-29-7
0.12
160
bis(2-Ethylhexyl)
phthalate
117-81-7
0.28
28
Ethyl methacrylate
97-63-2
0.14
160
Ethylene oxide
75-21-8
0.12
NA
bis(2-Ethylhexyl)
phthalate
117-81-7
0.28
28
Famphur
52-85-7
0.017
15
Fluoranthene
206-44-0
0.068
3.4
Fluorene
86-73-7
0.059
3.4
Formetanate hydro
-
chloride
6
23422-53-9
0.056
1.4
486
Formparanate
6
17702-57-7
0.056
1.4
Heptachlor
76-44-8
0.0012
0.066
Heptachlor epoxide
1024-57-3
0.016
0.066
Hexachloro benzene
118-74-1
0.055
10
Hexachloro butadiene
87-68-3
0.055
5.6
Hexachloro -
cyclopentadiene
77-47-4
0.057
2.4
HxCDDs (All Hexachloro
-
dibenzo-p-dioxins)
NA
0.000063
0.001
HxCDFs (All Hexachloro
-
dibenzofurans)
NA
0.000063
0.001
Hexachloro ethane
67-72-1
0.055
30
Hexachloro propylene
1888-71-7
0.035
30
Indeno (1,2,3-c,d)
pyrene
193-39-5
0.0055
3.4
Iodomethane
74-88-4
0.19
65
Isobutyl alcohol
78-83-1
5.6
170
Isodrin
465-73-6
0.021
0.066
Isolan
6
119-38-0
0.056
1.4
Isosafrole
120-58-1
0.081
2.6
Kepone
143-50-8 143-50-
0
0.0011
0.13
Methacrylonitrile
126-98-7
0.24
84
Methanol
67-56-1
5.6
0.75 mg/l TCLP
Methapyrilene
91-80-5
0.081
1.5
Methiocarb
6
2032-65-7
0.056
1.4
Methomyl
6
16752-77-5
0.028
0.14
Methoxychlor
72-43-5
0.25
0.18
3-Methylcholanthrene
56-49-5
0.0055
15
4,4-Methylene bis(2-
chloro aniline)
101-14-4
0.50
30
Methylene chloride
75-09-2
0.089
30
Methyl ethyl ketone
78-93-3
0.28
36
Methyl isobutyl ketone
108-10-1
0.14
33
487
Methyl methacrylate
80-62-6
0.14
160
Methyl methansulfonate
66-27-3
0.018
NA
Methyl parathion
298-00-0
0.014
4.6
Metolcarb
6
1129-41-5
0.056
1.4
Mexacarbate
6
315-18-4
0.056
1.4
Molinate
6
2212-67-1
0.042
1.4
Naphthalene
91-20-3
0.059
5.6
2-Naphthylamine
91-59-8
0.52
NA
o-Nitro aniline
88-74-4
0.27
14
p-Nitro aniline
100-01-6
0.028
28
Nitrobenzene
98-95-3
0.068
14
5-Nitro-o-toluidine
99-55-8
0.32
28
o-Nitro phenol
88-75-5
0.028
13
p-Nitro phenol
100-02-7
0.12
29
N-Nitroso diethyl amine
55-18-5
0.40
28
N-Nitroso dimethyl amine
62-75-9
0.40
2.3
N-Nitroso-di-n-butyl
-
amine
924-16-3
0.40
17
N-Nitroso methyl ethyl-
amine
10595-95-6
0.40
2.3
N-Nitroso morpholine
59-89-2
0.40
2.3
N-Nitroso piperidine
100-75-4
0.013
35
N-Nitrosopyrrol idine
930-55-2
0.013
35
Oxamyl
6
23135-22-0
0.056
0.28
Parathion
56-38-2
0.014
4.6
Total PCBs (sum of all
PCB isomers, or all
Aroclors)
1336-36-3
0.10
10
Pebulate
6
1114-71-2
0.042
1.4
Pentachloro benzene
608-93-5
0.055
10
PeCDDs (All Pentachloro
-
dibenzo-p-dioxins)
NA
0.000063
0.001
PeCDFs (All Pentachloro
-
NA
0.000035
0.001
488
dibenzofurans)
Pentachloro ethane
76-01-7
0.055
6.0
Pentachloro nitrobenzene
82-68-8
0.055
4.8
Pentachloro phenol
87-86-5
0.089
7.4
Phenacetin
62-44-2
0.081
16
Phenanthrene
85-01-8
0.059
5.6
Phenol
108-95-2
0.039
6.2
o-Phenylenediamine
6
95-54-5
0.056
5.6
Phorate
298-02-2
0.021
4.6
Phthalic acid
100-21-0
0.055
28
Phthalic anhydride
85-44-9
0.055
28
Physostigmine
6
57-47-6
0.056
1.4
Physostigmine
salicylate
6
57-64-7
0.056
1.4
Promecarb
6
2631-37-0
0.056
1.4
Pronamide
23950-58-5
0.093
1.5
Propham
6
122-42-9
0.056
1.4
Propoxur
6
114-26-1
0.056
1.4
Prosulfocarb
6
52888-80-9
0.042
1.4
Pyrene
129-00-0
0.067
8.2
Pyridine
110-86-1
0.014
16
Safrole
94-59-7
0.081
22
Silvex (2,4,5-TP)
93-72-1
0.72
7.9
2,4,5-T (2,4,5-
Trichloro phenoxyacetic
acid)
93-76-5
0.72
7.9
1,2,4,5-Tetrachloro
-
benzene
95-94-3
0.055
14
TCDDs (All Tetrachloro
-
dibenzo-p-dioxins)
NA
0.000063
0.001
TCDFs (All Tetrachloro
-
dibenzofurans)
NA
0.000063
0.001
1,1,1,2-Tetrachloro
-
ethane
630-20-6
0.057
6.0
489
1,1,2,2-Tetrachloro
-
ethane
79-34-6 79-34-5
0.057
6.0
Tetrachloro ethylene
127-18-4
0.056
6.0
2,3,4,6-Tetrachloro
-
phenol
58-90-2
0.030
7.4
Thiodicarb
6
59669-26-0
0.019
1.4
Thiophanate-methyl
6
23564-05-8
0.056
1.4
Tirpate
6
26419-73-8
0.056
0.28
Toluene
108-88-3
0.080
10
Toxaphene
8001-35-2
0.0095
2.6
Triallate
6
2303-17-5
0.042
1.4
Bromoform ( Tribromo -
methane (Bromoform )
75-25-2
0.63
15
1,2,4-Trichloro benzene
120-82-1
0.055
19
1,1,1-Trichloro ethane
71-55-6
0.054
6.0
1,1,2-Trichloro ethane
79-00-5
0.054
6.0
Trichloro ethylene
79-01-6
0.054
6.0
Trichloro monofluoro -
methane
75-69-4
0.020
30
2,4,5-Trichloro phenol
95-95-4
0.18
7.4
2,4,6-Trichloro phenol
88-06-2
0.035
7.4
2,4,5-Trichloro phenoxy -
acetic acid/2,4,5-T
93-76-5
0.72
7.9
1,2,3-Trichloro propane
96-18-4
0.85
30
1,1,2-Trichloro-1,2,2-
trifluoro ethane
76-13-1
0.057
30
Triethylamine
6
101-44-8
0.081
1.5
tris-(2,3-Dibromo
propyl)
phosphate
126-72-7
0.11
0.10
Vernolate
6
1929-77-7
0.042
1.4
Vinyl chloride
75-01-4
0.27
6.0
Xylenes-mixed isomers
(sum of o -, m-, and p-
xylene concentrations)
1330-20-7
0.32
30
Antimony
7440-36-0
1.9
2.1 mg/l TCLP
490
Arsenic
7440-38-2
1.4
5.0 mg/l TCLP
Barium
7440-39-3
1.2
7.6 mg/l TCLP
Beryllium
7440-41-7
0.82
0.014 mg/l TCLP
Cadmium
7440-43-9
0.69
0.19 mg/l TCLP
Chromium (Total)
7440-47-3
2.77
0.86 mg/l TCLP
Cyanides (Total)
4
57-12-5
1.2
590
Cyanides (Amenable)
4
57-12-5
0.86
30
Fluoride
5
16964-48-
816984-48-8
35
NA
Lead
7439-92-1
0.69
0.37 mg/l TCLP
Mercury-Nonwastewater
from Retort
7439-97-6
NA
0.20 mg/l TCLP
Mercury-All Others
7439-97-6
0.15
0.025 mg/l TCLP
Nickel
7440-02-0
3.98
5.0 mg/l TCLP
Selenium
7782-49-2
0.82
0.16 mg/l TCLP
Silver
7440-22-4
0.43
0.30 mg/l TCLP
Sulfide
8496-25-8 18496-
25-8
14
NA
Thallium
7440-28-0
1.4
0.078 mg/l TCLP
Vanadium
5
7440-62-2
4.3
0.23 mg/l TCLP
Zinc
5
7440-66-6
2.61
5.3 mg/l TCLP
1
CAS means Chemical Abstract Services. When the waste code or regulated
constituents are described as a combination of a chemical with its salts
or esters, the CAS number is given for the parent compound only.
2
Concentration standards for wastewaters are expressed in mg/l are based
on analysis of composite samples.
3
Except for metals (EP or TCLP) and cyanides (total and amenable), the
nonwastewater treatment standards expressed as a concentration were
established, in part, based on incineration in units operated in
accordance with the technical requirements of 35 Ill. Adm. Code
724.Subpart O or 35 Ill. Adm. Code 725.Subpart O or on combustion in
fuel substitution units operating in accordance with applicable
technical requirements. A facility may comply with these treatment
standards according to provisions in 40 CFR 268.40(d). All
concentration standards for nonwastewaters are based on analysis of grab
samples.
4
Both Cyanides (Total) and Cyanides (Amenable) for nonwastewaters are to
be analyzed using Method 9010 or 9012, found in "Test Methods for
Evaluating Solid Waste, Physical/Chemical Methods", USEPA Publication
SW-846, incorporated by reference in 35 Ill. Adm. Code 720.111, with a
sample size of 10 grams and a distillation time of one hour and 15
491
minutes.
5 Vanadium and zinc
These constituents
are not "underlying hazardous
constituents" in characteristic wastes, according to the definition at
Section 728.102(i).
6
This footnote corresponds with note 6 to the table to 40 CFR 268.48(a),
which has already expired by its own terms. This statement maintains
structural consistency with the federal regulations.
Note: NA means not applicable.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 733
STANDARDS FOR UNIVERSAL WASTE MANAGEMENT
SUBPART A: GENERAL
Section
733.101
Scope
733.102
Applicability--Batteries
733.103
Applicability--Pesticides
733.104
Applicability--Mercury Thermostats
733.105
Applicability--Household and Conditionally Exempt Small Quantity
Generator Waste
733.106
Definitions
SUBPART B: STANDARDS FOR SMALL QUANTITY HANDLERS
Section
733.110
Applicability
733.111
Prohibitions
733.112
Notification
733.113
Waste Management
733.114
Labeling and Marking
733.115
Accumulation Time Limits
733.116
Employee Training
733.117
Response to Releases
733.118
Off-Site Shipments
733.119
Tracking Universal Waste Shipments
733.120
Exports
SUBPART C: STANDARDS FOR LARGE QUANTITY HANDLERS
Section
733.130
Applicability
733.131
Prohibitions
733.132
Notification
733.133
Waste Management
733.134
Labeling and Marking
733.135
Accumulation Time Limits
733.136
Employee Training
733.137
Response to Releases
733.138
Off-Site Shipments
733.139
Tracking Universal Waste Shipments
733.140
Exports
492
SUBPART D: STANDARDS FOR UNIVERSAL WASTE TRANSPORTERS
Section
733.150
Applicability
733.151
Prohibitions
733.152
Waste Management
733.153
Accumulation Time Limits
733.154
Response to Releases
733.155
Off-site Shipments
733.156
Exports
SUBPART E: STA NDARDS FOR DESTINATION FACILITIES
Section
733.160
Applicability
733.161
Off-Site Shipments
733.162
Tracking Universal Waste Shipments
SUBPART F: IMPORT REQUIREMENTS
Section
733.170
Imports
SUBPART G: PETITIONS TO INCLUDE OTHER WASTES
Section
733.180
General
733.181
Factors for Petitions to Include Other Wastes
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R95-20 at 20 Ill. Reg. 11291, effective August 1, 1996
;
amended in R96-10/R97-3/R97-5 at 21 Ill. Reg. ________, effective
____________________
.
SUBPART B: STANDARDS FOR SMALL QUANTITY HANDLERS
Section 733.120
Exports
A small quantity handler of universal waste that sends universal waste to a
foreign destination
other than to those OECD countries specified in 35 Ill.
Adm. Code 722.158(a)(1) (in which case the handler is subject to the
requirements of 35 Ill. Adm. Code 722.Subpart H)
shall:
a)
Comply with the requirements applicable to
a primary exporter in
35 Ill. Adm. Code 722.153; 722.156(a)(1) through (a)(4), (a)(6),
and (b); and 722.157;
b)
Export such universal waste only upon consent of the receiving
country and in conformance with the USEPA Acknowledgement of
Consent, as defined in 35 Ill. Adm. Code 722.Subpart E; and
c)
Provide a copy of the USEPA Acknowledgment of Consent for the
shipment to the transporter transporting the shipment for export.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART C: STANDARDS FOR LARGE QUANTITY HANDLERS
Section 733.140
Exports
A large quantity handler of universal waste that sends universal waste to a
493
foreign destination
other than to those OECD countries specified in 35 Ill.
Adm. Code 722.158(a)(1) (in which case the handler is subject to the
requirements of 35 Ill. Adm. Code 722.Subpart H)
shall:
a)
Comply with the requirements applicable to a primary exporter in
35 Ill. Adm. Code 722.153; 722.156(a)(1) through (a)(4), (a)(6),
and (b); and 722.157;
b)
Export such universal waste only upon consent of the receiving
country and in conformance with the USEPA Acknowledgement of
Consent as defined in 35 Ill. Adm. Code 722.Subpart E; and
c)
Provide a copy of the USEPA Acknowledgement of Consent for the
shipment to the transporter transporting the shipment for export.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART D: STANDARDS FOR UNIVERSAL WASTE TRANSPORTERS
Section 733.156
Exports
A universal waste transporter transporting a shipment of universal waste to a
foreign destination
other than to those OECD countries specified in 35 Ill.
Adm. Code 722.158(a)(1) (in which case the transporter is subject to the
requirements of 35 Ill. Adm. Code 722.Subpart H)
may not accept a shipment if
the transporter knows the shipment does not conform to the USEPA
Acknowledgment of Consent. In addition the transporter shall ensure the
following:
a)
A copy of the USEPA Acknowledgment of Consent accompanies the
shipment; and
b)
The shipment is delivered to the facility designated by the person
initiating the shipment.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART F: IMPORT REQUIREMENTS
Section 733.170
Imports
Persons managing universal waste that is imported from a foreign country into
the United States are subject to the applicable requirements of this Part
immediately after the waste enters the United States, as
follows indicated in
subsections (a) through (c) below
:
a)
A universal w aste transporter is subject to the universal waste
transporter requirements of 733.Subpart D.
b)
A universal waste handler is subject to the small or large
quantity handler of universal waste requirements of 733.Subpart B
or C, as applicable.
c)
An owner or operator of a destination facility is subject to the
destination facility requirements of 733.Subpart E.
d)
Persons managing universal waste that is imported from an OECD
country as specified in 35 Ill. Adm. Code 722.158(a)(1) are
subject to subsections (a) through (c) above, in addition to the
494
requirements of 35 Ill. Adm. Code 722.Subpart H.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER d: UNDERGROUND INJECTION CONTROL AND UNDERGROUND
STORAGE TANK PROGRAMS
PART 738
HAZARDOUS WASTE INJECTION RESTRICTIONS
SUBPART A: GENERAL
Section
738.101
Purpose Scope and Applicability
738.102
Definitions
738.103
Dilution Prohibited as a Substitute
for Treatment
738.104
Case-by-Case Extensions of an Effective Date
738.105
Waste Analysis
SUBPART B: PROHIBITIONS ON INJECTION
Section
738.110
Waste Specific Prohibitions - Solvent Wastes
738.111
Waste Specific Prohibitions - Dioxin-Containing Wastes
738.112
Waste Specific Prohibitions - California List Wastes
738.114
Waste Specific Prohibitions - First Third Wastes
738.115
Waste Specific Prohibitions - Second Third Wastes
738.116
Waste Specific Prohibitions - Third Third Wastes
738.117
Waste Specific Pr
ohibitions - Newly-Listed Wastes
738.118
Waste specific prohibitions
--Newly Identified Wastes
SUBPART C: PETITION STANDARDS AND PROCEDURES
Section
738.120
Petitions to Allow Injection of a Prohibited Waste
738.121
Required Information to Support Petitions
738.122
Submission, Review and Approval or Denial of Petitions
738.123
Review of Adjusted Standards
738.124
Termination of Adjusted Standards
AUTHORITY: Implementing Section 13 and 22.4 and authorized by Section 27 of
the Environmental Protection Act [415 ILCS 5/13, 22.4 and 27].
SOURCE: Adopted in R89-2 at 14 Ill. Reg. 3059, effective February 20, 1990;
amended in R89-11 at 14 Ill. Reg. 11948, effective July 9, 1990; amended in
R90-14 at 15 Ill. Reg. 11425, effective July 24, 1991; amended in R92-13 at 17
Ill. Reg. 6190, effective April 5, 1993; amended in R93-6 at 17 Ill. Reg.
15641, effective September 14, 1993; amended in R95-4 at 19 Ill. Reg. 9501,
effective June 27, 1995
; amended in R96-10/R97-3/R97-5 at 21 Ill. Reg.
________, effective ____________________
.
SUBPART A: GENERAL
Section 738.101
Purpose Scope and Applicability
a)
This Part identifies hazardous wastes that are restricted from
disposal into Class I
hazardous waste injection
wells and defines
those circumstances under which a waste, otherwise prohibited from
injection, may be injected.
495
b)
The requirements of this Part apply to owners or operators of
the
following Class I wells:
1)
hHazardous waste injection wells
that are used to inject
hazardous waste ; and
2)
Injection wells that are used to inject wastes which once
exhibited a prohibited characteristic of hazardous waste
identified in 35 Ill. Adm. Code 721.Subpart C, at the point
of generation, and which no longer exhibit the
characteristic at the point of injection
.
c)
Wastes otherwise prohibited from injection may continue to be
injected:
1)
If an extension from the effective date of a prohibition has
been granted pursuant to Section 738.104; or
2)
If an adjusted standard has been granted in response to a
petition filed under Section 738.120; or
3)
If the waste is generated by a conditionally exempt small
quantity generator, as defined in 35 Ill. Adm. Code 721.105.
d) WA wastes that areis hazardous only because
theyit exhibit s a
hazardous characteristic , and which of hazardous waste and which
areis otherwise prohibited from injection under this Part
or 35
Ill. Adm. Code 728
, areis not prohibited from injection if
the
following is true of
the waste s:
1) AreIt is disposed into a
Class I nonhazardous waste
injection well or a Class I hazardous waste injection well
that receives only non-prohibited hazardous wastes
, as such
are defined under 35 Ill. Adm. Code 730.106(a); and
2) DoIt does not exhibit any prohibited characteristic of
hazardous waste identified in 35 Ill. Adm. Code 721.Subpart
C at the point of injection.
BOARD NOTE: The exemption for injection of diluted
hazardous waste in this subsection was the subject of
litigation in Chemical Waste Management et al. v. USEPA, 976
F.2d 2 (D.C. Cir. 1992). The USEPA response to the mandate
in this litigation may result in the repeal or modification
of 40 CFR 148.1(d), from which this subsection is derived.
USEPA responded to the remand by issuing an interim final
rule on May 24, 1993, at 58 Fed. Reg. 29860, but that action
did not directly affect 40 CFR 148.1. The Board views any
federal court decision on the effectiveness or
enforceability of the USEPA rule as binding on this
subsection.
BOARD NOTE: Derived from 40 CFR 148.1 (199
26), as amended
at 57 Fed. Reg. 31963 (July 20, 1992)
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 738.103
Dilution Prohibited as a Substitute for
Treatment
The prohibition of 35 Ill. Adm. Code 728.103 shall apply to owners or
496
operators of Class I hazardous waste injection wells.
a)
The provisions of 35 Ill. Adm. Code 728.103 shall apply to owners
or operators of Class I wells used to inject a waste that is
hazardous at the point of generation whether or not the waste is
hazardous at the point of injection.
b)
Owners or operators of Class I nonhazardous waste injection wells
that inject waste formerly exhibiting a hazardous characteristic
which has been removed by dilution may address underlying
hazardous constituents by treating the hazardous waste, obtaining
an exemption pursuant to a petition filed under Section 738.120,
or complying with the provisions set forth in 35 Ill. Adm. Code
728.109.
BOARD NOTE: Derived from 40 CFR 148.3 (19
8896), as added at 53 Fed. Reg.
28155, July 26, 1988
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 738.104
Case-by-Case Extensions of an Effective Date
The owner or operator of a Class I hazardous
or nonhazardous waste injection
well may submit an application to
USEPA for an extension of the effective date
of any applicable prohibition established under Subpart B. (See 35 Ill. Adm.
Code 728.105.)
BOARD NOTE: Derived from 40 CFR 148.4 (19
8896), as added at 53 Fed. Reg.
28155, July 26, 1988
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
SUBPART B: PROHIBITIONS ON INJECTION
Section 738.117
Waste Specific Prohibitions - Newly-Listed Wastes
a)
The wastes specified in 35 Ill. Adm. Code 721.Subpart D by the
following U .S. EPA hazardous waste numbers are prohibited from
underground injection:
F037
F038
K107
K108
K109
K110
K111
K112
K117
K118
K123
K124
K125
K126
K131
K136
U328
U353
U359
497
b)
The wa stes specified in 35 Ill. Adm. Code 721.Subpart D by the
following U .S. EPA hazardous waste numbers are prohibited from
underground injection:
K141
K142
K143
K144
K145
K147
K148
K149
K150
K151
c) Effective September 19, 1995, the wastes specified in 35 Ill. Adm.
Code 721.Subpart C by the following U.S. EPA hazardous waste
numbers are prohibited from underground injection:
D001 (high TOC subcategory, as specified at 35 Ill.
Adm. Code 728.140)
D012
D013
D014
D015
D016
D017
c)
This subsection corresponds with 40 CFR 148.17(c), removed and
marked "reserved" by USEPA at 61 Fed. Reg. 15662 (Apr. 8, 1996).
This statement maintains structural consistency with USEPA rules.
d)
Effective June 30, 1995, the wastes specified in 35 Ill. Adm. Code
721.Subpart D by the following U
.S. EPA hazardous waste numbers
are prohibited from underground injection:
K117
K118
K131
K132
e)
The requirements of subsections (a) and (b) above do no
t apply:
1)
If the wastes meet or are treated to meet the applicable
standards specified in 35 Ill. Adm. Code 728.Subpart D; or
2)
If an adjusted standard has been granted in response to a
petition under 738.Subpart C; or
3)
During the period of extension of the applicable effective
date, if an extension is granted under Section 738.104.
BOARD NOTE: Derived from 40 CFR 148.17
, as added at 57 Fed.
Reg. 37263 (Aug. 18, 1992)
(1996) .
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
Section 738.118
Waste specific prohibitions
--Newly Identified Wastes
a)
The wastes specified in 35 Ill. Adm. Code 721.132 as having the
following USEPA hazardous waste numbers are prohibited from
498
underground injection:
K156
K157
K158
K159
K160
K161
P127
P128
P185
P188
P189
P190
P191
P192
P194
P196
P197
P198
P199
P201
P202
P203
P204
P205
U271
U277
U278
U279
U280
U364
U365
U366
U367
U372
U373
U375
U376
U377
U378
U379
U381
U382
U383
U384
U385
U386
U387
U389
U390
U391
U392
U393
U394
U395
U396
U400
U401
U402
U403
499
U404
U407
U409
U410
U411
b)
The wastes specified in 35 Ill. Adm. Code 721.132 as USEPA
Hazardous waste number K088 is prohibited from underground
injection.
c)
On April 8, 1998, the wastes specified in 35 Ill. Adm. Code 721 as
having the following USEPA Hazardous waste numbers and Mixed
TC/Radioactive wastes are prohibited from underground injection:
D018
D019
D020
D021
D022
D023
D024
D025
D026
D027
D028
D029
D030
D031
D032
D033
D034
D035
D036
D037
D038
D039
D040
D041
D042
D043
d)
On April 8, 1998, the wastes specified in 35 Ill. Adm. Code 721 as
having the following USEPA Hazardous waste numbers are prohibited
from underground injection:
D001
D002
D003
(Source: Added at 21 Ill. Reg. ________, effective ______________________)
SUBPART C: PETITION STANDARDS AND PROCEDURES
Section 738.120
Petitions to Allow Injection of a Prohibited Waste
a)
Any person seeking an exemption from a prohibition under Subpart B
for the injection of a restricted hazardous waste
into an
injection well or wells
, including a hazardous waste that exhibits
a characteristic of hazardous waste and which contains underlying
hazardous constituents at the point of generation, but which no
500
longer exhibits a characteristic of hazardous waste when injected
into a Class I injection well or wells,
shall submit a petition
for an adjusted standard to the Board, pursuant to 35 Ill. Adm.
Code 106.Subpart G, demonstrating that, to a reasonable degree of
certainty, there will be no migration of hazardous constituents
from the injection zone for as long as the waste remains
hazardous. This demonstration requires a showing that:
1)
The hydrogeological and geochemical conditions at the
site(s) and the physiochemical nature of the waste stream(s)
are such that reliable predictions can be made that:
A)
Fluid movement conditions are such that the injected
fluids will not migrate within 10,000 years:
i)
Vertically upward out of the injection zone; or
ii)
Laterally within the injection zone to a point
of discharge or interface with an Underground
Source of Drinking Water (USDW) as defined in 35
Ill. Adm. Code 730; or
B)
Before the injected fluids migrate out of the
injection zone or to a point of discharge or interface
with USDW, the fluid will no longer be hazardous
because of attenuation, transformation, or
immobilization of hazardous constituents within the
injection zone by hydrolysis, chemical interactions or
other means; and
2)
For each well the petition has:
A)
Demonstrated that the injection well's area of review
complies with the substantive requirements of 35 Ill.
Adm. Code 730.163;
B)
Located, identified, and ascertained the condition of
all wells within the injection well's area of review
(as specified in 35 Ill. Adm. Code 730.163) that
penetrate the injection zone or the confining zone by
use of a protocol acceptable to the Board that meets
the substantive requirements of 35 Ill. Adm. Code
730.164;
C)
Submitted a corrective action plan that meets the
substantive requirements of 35 Ill. Adm. Code 730.164,
the implementation of which shall become a condition
of any adjusted standard granted; and
D)
Submitted the results of pressure and radioactive
tracer tests performed within one year prior to
submission of the petition demonstrating the
mechanical integrity of the well's long string casing,
injection tube, annular seal, and bottom hole cement.
In cases where the petition has not been approved or
denied within one year after the initial demonstration
of mechanical integrity, the Board may require the
owner or operator to perform the tests again and
submit the results of the new tests.
BOARD NOTE: The requirements of subsection (a)(2)
501
need not be incorporated in a permit at the time the
Board grants an adjusted standard.
b)
A demonstration under subsection (a)(1)(A) must identify the
strata within the injection zone which will confine fluid movement
above the injection interval and include a showing that this
strata is free of known transmissive faults of fractures and that
there is a confining zone above the injection zone.
c)
A demonstration under subsection (a)(1)(B) must identify the
strata within the injection zone where waste transformation will
be accomplished and include a showing that this strata is free of
known transmissive faults or fractures and that there is a
confining zone above the injection zone.
d)
A demonstration may include a showing that:
1)
Treatment methods that reduce the toxicity or mobility of
the wastes, the implementation of which will become a
condition of any adjusted standard, must be utilized; or
2)
A monitoring plan, the implementation of which will become a
condition of any adjusted standard, must be utilized to
enhance confidence in one or more aspects of the
demonstration.
e)
Any person whothat has been granted an adjusted standard pursuant
to this Section may submit a petition for reissuance of the
adjusted standard to include an additional restricted waste or
wastes or to modify any conditions placed on that adjusted
standard by the Board. The Board will reissue the adjusted
standard if the petitioner complies with subsections (a), (b) and
(c).
f)
Any person whothat has been granted an adjusted standard pursuant
to this Section may submit a petition to modify that adjusted
standard to include an additional (hazardous) waste or wastes.
The Board may grant the modification if it determines, to a
reasonable degree of certainty, that the additional waste or
wastes will behave hydraulically and chemically in a manner
similar to previously included wastes and that it will not
interfere with the containment capability of the injection zone.
BOARD NOTE: Derived from 40 CFR 148.20 (19
8896), as added at 53
Fed. Reg. 28155, July 26, 1988
.
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)
TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE G: WASTE DISPOSAL
CHAPTER I: POLLUTION CONTROL BOARD
SUBCHAPTER c: HAZARDOUS WASTE OPERATING REQUIREMENTS
PART 739
STANDARDS FOR THE MANAGEMENT OF USED OIL
SUBPART A: DEFINITIONS
Section
739.100
Definitions
502
SUBPART B: APPLICABILITY
Section
739.110
Applicability
739.111
Used oil specifications
739.112
Prohibitions
SUBPART C: STANDARDS FOR USED OIL GENERATORS
Section
739.120
Applicability
739.121
Hazardous waste mixing
739.122
Used oil storage
739.123
On-site burning in space heaters
739.124
Off-site shipments
SUBPART D: STANDARDS FOR USED OIL COLLECTION CENTERS AND
AGGREGATION POINTS
Section
739.130
Do-it-yourselfer used oil collection centers
739.131
Used oil collection centers
739.132
Used oil aggregate points owned by the generator
SUBPART E: STANDARDS FOR USED OIL TRANSPORTER AND TRANSFER
FACILITIES
Section
739.140
Applicability
739.141
Restrictions on transporters that are not als
o processors
739.142
Notification
739.143
Used oil transportation
739.144
Rebuttable presumption for used oil
739.145
Used oil storage at transfer facilities
739.146
Tracking
739.147
Management of residues
SUBPART F: STANDARDS FOR USED OIL PROCESSORS
Section
739.150
Applicability
739.151
Notification
739.152
General facility standards
739.153
Rebuttable presumption for used oil
739.154
Used oil management
739.155
Analysis plan
739.156
Tracking
739.157
Operating record and reporting
739.158
Off-site shipm ents of used oil
739.159
Management of residues
SUBPART G: STANDARDS FOR USED OIL BURNERS THAT BURN
OFF-SPECIFICATION USED OIL FOR ENERGY RECOVERY
Section
739.160
Applicability
739.161
Restriction on burning
739.162
Notification
739.163
Rebuttable presumption for used oil
739.164
Used oil storage
739.165
Tracking
739.166
Notices
739.167
Management of residues
SUBPART H: STANDARDS FOR USED OIL FUEL MARKETERS
Section
739.170
Applicability
503
739.171
Prohibitions
739.172
On-specification used oil fuel
739.173
Notification
739.174
Tracking
739.175
Notices
SUBPART I: STANDARDS FOR USE AS A DUST SUPPRESSANT DISPOSAL OF USED OIL
Section
739.180
Applicability
739.181
Disposal
739.182
Use as a dust suppressant
AUTHORITY: Implementing Section 22.4 and authorized by Section 27 of the
Environmental Protection Act [415 ILCS 5/22.4 and 27].
SOURCE: Adopted in R93-4 at 17 Ill. Reg. 20954, effective November 22, 1993;
amended in R93-16 at 18 Ill. Reg. 6931, effective April 26, 1994; amended in
R94-17 at 18 Ill. Reg. 17616, effective November 23, 1994; amended in R95-6 at
19 Ill. Reg. 10036, effective June 27, 1995
; amended in R96-10/R97-3/R97-5 at
21 Ill. Reg. ________, effective ____________________
.
SUBPART B: APPLICABILITY
Section 739.110
Applicability
This Section identifies those materials which are subject to regulation as
used oil under this Part. This Section also identifies some materials that
are not subject to regulation as used oil under this Part, and indicates
whether these materials may be subject to regulation as hazardous waste under
Parts35 Ill. Adm. Code
702, 703, 720 through 726, and 728.
a)
Used oil. U .S. EPA presumes that used oil is to be recycled
unless a used oil handler disposes of used oil, or sends used oil
for disposal. Except as provided in Section 739.111, the
regulations of this Part apply to used oil, and to materials
identified in this Section as being subject to regulation as used
oil, whether or not the used oil or material exhibits any
characteristics of hazardous waste identified in 35 Ill. Adm. Code
721.Subpart C.
b)
Mixtures of used oil and hazardous waste.
1)
Listed hazardous waste.
A)
A mixture of used oil and hazardous waste that is
listed in 35 Ill. Adm. Code 721.Subpart D is subject
to regulation as hazardous waste under 35 Ill. Adm.
Code 703, 720 through 726, and 728, rather than as
used oil under this Part.
B)
Rebuttable presumption for used oil. Used oil
containing more than 1,000 ppm total halogens is
presumed to be a hazardous waste because it has been
mixed with halogenated hazardous waste listed in 35
Ill. Adm. Code 721.Subpart D. Persons may rebut this
presumption by demonstrating that the used oil does
not contain hazardous waste (for example, by using an
analytical method from SW-846, Edition III, to show
that the used oil does not contain significant
concentrations of halogenated hazardous constituents
504
listed in 35 Ill. Adm. Code 721.Appendix H). U
.S. EPA
Publication SW-846, Third Edition, is available from
the Government Printing Office, Superintendent of
Documents, P.O. Box 371954, Pittsburgh, PA 15250-7954,
(202) 783-3238 (document number 955-001-00000-1).
i)
The rebuttable presumption does not apply to
metalworking oils or fluids containing
chlorinated paraffins, if they are processed,
through a tolling arrangement as described in
Section 739.124(c), to reclaim metalworking oils
or fluids. The presumption does apply to
metalworking oils or fluids if such oils or
fluids are recycled in any other manner, or
disposed.
ii)
The reb uttable presumption does not apply to
used oils contaminated with chlorofluorocarbons
(CFCs) removed from refrigeration units where
the CFCs are destined for reclamation. The
rebuttable presumption does apply to used oils
contaminated with CFCs that have been mixed with
used oil from sources other than refrigeration
units.
2)
Characteristic hazardous waste. A mixture of used oil and
hazardous waste that exhibits a hazardous waste
characteristic identified in 35 Ill. Adm. Code 721.Subpart C
and a mixture of used oil and hazardous waste that is listed
in Subpart D of this Part solely because it exhibits one or
more of the characteristics of hazardous waste identified in
35 Ill. Adm. Code 721.Subpart C is subject to:
A)
Except as provided in subsection (b)(2)(C) of this
Section, regulation as hazardous waste under 35 Ill.
Adm. Code 703, 720 through 726, and 728 rather than as
used oil under this Part, if the resultant mixture
exhibits any characteristics of hazardous waste
identified in 35 Ill. Adm. Code 721.Subpart C; or
B)
Except as provided in subsection (b)(2)(C) of this
Section, regulation as used oil under this Part, if
the resultant mixture does not exhibit any
characteristics of hazardous waste identified under 35
Ill. Adm. Code 721.Subpart C.
C)
Regulation as used oil under this Part, if the mixture
is of used oil and a waste which is hazardous solely
because it exhibits the characteristic of ignitability
(e.g., ignitable-only mineral spirits), provided that
the resultant mixture does not exhibit the
characteristic of ignitability under 35 Ill. Adm. Code
721.121.
3)
Conditionally exempt small quantity generator hazardous
waste. A mixture of used oil and conditionally exempt small
quantity generator hazardous waste regulated under 35 Ill.
Adm. Code 721.105 is subject to regulation as used oil under
this Part.
c)
Materials containing or otherwise contaminated with used oil.
505
1)
Except as provided in subsection (c)(2) of this Section, a
material containing or otherwise contaminated with used oil
from which the used oil has been properly drained or removed
to the extent possible such that no visible signs of free-
flowing oil remain in or on the material:
A)
Is not used oil, and thus, it is not subject to this
Part, and
B)
If applicable, is subject to the hazardous waste
regulations of 35 Ill. Adm. Code 703, 705, 720 through
726, and 728.
2)
A material containing or otherwise contaminated with used
oil that is burned for energy recovery is subject to
regulation as used oil under this Part.
3)
Used oil drained or removed from materials containing or
otherwise contaminated with used oil is subject to
regulation as used oil under this Part.
d)
Mixtures of used oil with products.
1)
Except as provided in subsection (d)(2) below, mixtures of
used oil and fuels or other fuel products are subject to
regulation as used oil under this Part.
2)
Mixtures of used oil and diesel fuel mixed on-site by the
generator of the used oil for use in the generator's own
vehicles are not subject to this Part once the used oil and
diesel fuel have been mixed. Prior to mixing, the used oil
is subject to the requirements of Subpart C of this Part.
e)
Materials derived from used oil.
1)
Materials that are reclaimed from used oil that are used
beneficially and are not burned for energy recovery or used
in a manner constituting disposal (e.g., re-refined
lubricants) are:
A)
Not used oil and thus are not subject to this Part,
and
B)
Not solid wastes and are thus not subject to the
hazardous waste regulations of
Parts 35 Ill. Adm. Code
703, 720 through 726, and 728 as provided in 35 Ill.
Adm. Code 721.103(e)(1).
2)
Materials produced from used oil that are burned for energy
recovery (e.g., used oil fuels) are subject to regulation as
used oil under this Part.
3)
Except as provided in subsection (e)(4) below, materials
derived from used oil that are disposed of or used in a
manner constituting disposal are:
A)
Not used oil and thus are not subject to this Part,
and
B)
Are solid wastes and thus are subject to the hazardous
506
waste regulations of 35 Ill. Adm. Code 703, 720
through 726, and 728 if the materials are listed or
identified as hazardous waste.
4)
Used oil re-refining distillation bottoms that are used as
feedstock to manufacture asphalt products are not subject to
this Part.
f)
Wastewater. Wastewater, the discharge of which is subject to
regulation under either Section 402 or Section 307(b) of the Clean
Water Act (including wastewaters at facilities which have
eliminated the discharge of wastewater), contaminated with de
minimis quantities of used oil are not subject to the requirements
of this Part. For purposes of this subsection, "de minimis"
quantities of used oils are defined as small spills, leaks, or
drippings from pumps, machinery, pipes, and other similar
equipment during normal operations or small amounts of oil lost to
the wastewater treatment system during washing or draining
operations. This exception will not apply if the used oil is
discarded as a result of abnormal manufacturing operations
resulting in substantial leaks, spills, or other releases, or to
used oil recovered from wastewaters.
g)
Used oil introduced into crude oil pipelines or a petroleum
refining facility.
1)
Used oil mixed with crude oil or natural gas liquids (e.g.,
in a production separator or crude oil stock tank) for
insertion into a crude oil pipeline is exempt from the
requirements of this Part. The used oil is subject to the
requirements of this Part prior to the mixing of used oil
with crude oil or natural gas liquids.
2)
Mixtures of used oil and crude oil or natural gas liquids
containing less than 1% used oil that are being stored or
transported to a crude oil pipeline or petroleum refining
facility for insertion into the refining process at a point
prior to crude distillation or catalytic cracking are exempt
from the requirements of this Part.
3)
Used oil that is inserted into the petroleum refining
process before crude distillation or catalytic cracking
without prior mixing with crude oil is exempt from the
requirements of this Part, provided that the used oil
contains less than 1% of the crude oil feed to any petroleum
refining facility process unit at any given time. Prior to
insertion into the petroleum refining process, the used oil
is subject to the requirements of this Part.
4)
Except as provided in subsection (g)(5) below, used oil that
is introduced into a petroleum refining facility process
after crude distillation or catalytic cracking is exempt
from the requirements of this Part only if the used oil
meets the specification of Section 739.111. Prior to
insertion into the petroleum refining facility process, the
used oil is subject to the requirements of this Part.
5)
Used oil that is incidentally captured by a hydrocarbon
recovery system or wastewater treatment system as part of
routine process operations at a petroleum refining facility
and inserted into the petroleum refining facility process is
507
exempt from the requirements of this Part. This exemption
does not extend to used oil that is intentionally introduced
into a hydrocarbon recovery system (e.g., by pouring
collected used oil into the wastewater treatment system).
6)
Tank bottoms from stock tanks containing exempt mixtures of
used oil and crude oil or natural gas liquids are exempt
from the requirements of this Part.
h)
Used oil on vessels. Used oil produced on vessels from normal
shipboard operations is not subject to this Part until it is
transported ashore.
i)
Used oil containing PCBs.
In addition to the requirements of this
Part, a marketer or burner of used oil that markets used oil
containing any quantifiable level of PCBs is subject to the
requirements of 40 CFR 761.20(e).
(Source: Amended at 21 Ill. Reg. ________, effective ____________________)