1. MOTION TO FILE INSTANTER
      2. BEFORE THE ILLINOIS POLLUTION CONTROL BOARD
    1. ANALYTICAL COST FORM DRAFT
    2. ANALYTICAL COST FORM DRAFT
R04-22
(Rulemaking
-
~
JUN 21 2004
STATE OF ILLINOIS
Pollution Control Board
R04-23
(Rulemaking
—
UST)
Consolidated
To:
Dorothy M. Gunn, Clerk
Ms. Marie B. Tipsord
Illinois Pollution Control Board
Illinois Pollution Control Board
James R. Thompson Center
James R. Thompson Center
100 W. Randolph, Suite 11-500
100 West Randolph, Suite 11-500
Chicago, Illinois 60601
Chicago, IL 60601
MOTION TO FILE INSTANTER
Now comes CLAIRE
A.
MANNING, on behalfofthe Professionals ofIllinois for the
Protection ofthe Environment, PIPE, and respectfully requests that the Board, through its
Hearing Officer Marie Tipsord, accept the following documents instanter: PRE-FILED
TESTIMONY OF BILL FLEISHLI, PRE-FILED TESTIMONY OF JARRETT THOMAS,
SUPPLEMENTAL TESTIMONY OF JOSEPH M. KELLY and VARIOUS EXHIBITS to be
introduced at hearing. In support of said motion, the undersigned offers that no prejudice will
result from the admission, as the matters will be fully explored at public hearing and, in order to
be fully responsive to the matters presented by t JEPA at the last hearing, PWE-was unable to
coordinate this filing any earlier than this date.
Claire A. Maiming, Attorney
CLAIRE A. MANNING
Posegate & Denes, P.C.
111 N. Sixth Street, Suite 200
Springfield, Illinois 62701
(217) 522-6152
BEFORE THE ILLINOIS POLLUTION CONTROL BOARD
IN THE MATTER OF:
)
)
PROPOSED AMENDMENTS TO:
REGULATION PETROLEUM L~AK1NG
UNDERGROUND STORAGE TANKS
35
ILL. ADM. CODE 732
)
)
)
)
)
)
)
)
)
IN THE MATTER OF:
PROPOSED AMENDMENTS TO:
REGULATION PETROLEUM LEAKING
UNDERGROUND STORAGE TANKS
35 ILL. ADM. CODE 734
)
Printed on Recycled Paper in Accordance with 35111. Adm. Code 101.202 and 101. 302(g)
BEFORE THE ILLINOIS POLLUTION CONTROL BOARD
ERKS OFFICE
IN
THE MATTER OF:
).
STATE
JUN
OF
21ILLINOIS
2004
PROPOSED AMENDMENTS TO:
)
R04-22
Pollution Control Board
REGULATION PETROLEUM
LEAKING
)
(Rulemaking
- UST)
UNDERGROUND STORAGE TANKS
)
35 ILL.
ADM.
CODE. 732
)
iN THE MATTER OF:
)
)
PROPOSED AMENDMENTS TO:
)
R04-23
REGULATION PETROLEUM LEAKING
)
(Rulemaking
- UST)
UNDERGROUND STORAGE TANKS
)
Consolidated
35 ILL. ADM. CODE 734
)
TESTIMONY OF JARRETT THOMAS ON BEHALF OF THE PROFESSIONALS OF
ILLINOIS FOR THE PROTECTION OF THE ENVIRONMENT
AND
THE ILLINOIS
ASSOCIATION OF ENVIRONMENTAL LABORATORIES, INC.
My name is Jarrett R. Thomas. I am Vice President and co-owner ofSuburban
Laboratories, Inc., an IEPA accredited environmental testing laboratory located in
Hillside, Illinois. Suburban Laboratories has been in business since 1936 and has
performed analyses in support ofLUST remediations since the inception of the LUST
program.
In 2001, I was appointed by the Director of IEPA to be a member ofthe
Community Water Supply Testing Council, and the Environmental Laboratory
Certification Committee, ofwhich I am the Chairman. I am a current board member of
the Professionals ofIllinois for the Protection ofthe Environment (PIPE). PIPE is an
organization ofvarious businesses that perform remedial clean-ups ofunderground
storage tank sites as well as businesses that provide services to the remediation process,
such as landfills, laboratories, etc.
Printed on Recycled Paper in Accordance with 35 III. Adm. Code 101,202 and lOt. 302(g)
I am also a current board member, past President and co-founder of the Illinois
Association ofEnvironmental Laboratories, Inc. (IAETL). IAETL represents nearly
every IEPA accredited soil laboratory located in Illinois and our members perform an
estimated 90 ofLUST analyses in the State. I am here today to provide testimony on
behalfofPIPE and IAETL.
In October, 2002 I became aware of the existence ofthe Consulting Engineers
Council ofIllinois’ and the Illinois Petroleum Marketers Association’s Ad Hoc Work
Group on LUST Reimbursement Reform. A member ofthe Work Group provided me a
copy ofthe IEPA’s Analytical Cost Form Draft which proposed reimbursement limits for
laboratory analyses (Attachment A).
I forwarded this draft to the IEATL board of directors and on November 8, 2002,
on behalfof IAETL, I sent a letter to Mr. Doug Clay objecting to the maximum analytical
costs proposed by IEPA. Not only were the fees set much to low, they did not take into
account sample matrix, quality control requirements, methods ofanalysis, turnaround
time, deliverables, sampling tools, sample containers, shipping, sample disposal costs,
payment terms, costs of accreditation, etc...
I expressed concern that IEPA was commoditizing the analytical requirements of
the LUST program and that delays in processing LUST reimbursement payments were
hurting environmental labs. The letter concluded with an invitation to meet with IEPA
and a plea to be included in future workgroups.
In late November, 2002 several IAETL members, including myselfmet with
Doug Clay, Harry Chappel, Brian Baur, and Doug Oakly ofthe IEPA to discuss the
2
‘riffled on Recycled Paper in Accordance with 35
III. Adm, Code 101.2(12 and 101. 302(g)
laboratory industry’s concerns over the LUST reimbursement program and the Agency’s
draft lab fees.
I was primarily interested to learn how the Agency determined the draft fees. It
appeared that IEPA did not perform any formal surveys to obtain industry prices. Mr.
Baur indicated that he contacted a lab to obtain some pricing. To assist the Agency in
obtaining a more representative sampling of industry rates, I volunteered to collect price
lists from member laboratories, compile the data and submit it to the Agency for their
consideration.
Mr. Baur provided me the Analytical Cost Form Draft in a spreadsheet format to
be used for compiling the rates. Immediately following the meeting, I asked the IEATL
membership to forward me price lists for LUST analyses. Five laboratories responded to
the request and the results were tabulated (Attachment B). These five labs combined
perform an estimated 70 ofthe state’s LUST analyses.
On January 7, 2003 the survey information was provided to Mr. Clay and Mr.
Chappel via email along with a recommendation to accept the maximum rate. I made
several attempts to ascertain the status ofthe Agency’s proposal over then next twelve
months, but was unable to get an answer from Mr. Clay or Mr. Chappel, other than the
comments will be taken into consideration.
With the Agency’s original filing on January 13, 2004 I learned that that the rates
proposed in 732 Appendix D and 734 Appendix D, in nearly every case, were equal to
the average rate determined from the IAETL survey.
I understand the EPA’s need to control costs under the LUST reimbursement
program and the need to establish a cap on the lab rates, however, using the average rate
3
Printed on Recycled l’aper in Accordance with 35 III. Adm, Code 11)1.2(12 and 101. 302(g)
is not prudent. Assuming a normal distribution, using the average will result in 50 of
the rates falling above the reimbursement limit.
I recommend the original survey data compiled by IAETL be used to determine a
reimbursement cap for analytical laboratory testing. However, instead ofusing the
average rate, I recommend using the average plus one standard deviation or the maximum
rate, whichever is lower. The survey data and subsequent statistics are provided as
Attachment C.
I also recommend the following revisions to 732 Appendix D and 734 Appendix
D, most ofwhich are included in Attachment D:
1. Unit costs should be updated to reflect PIPE/IAETL recommendation;
2. Metals group costs should be clarified to reflect target analytes specified
in Appendix B of the applicable part;
3. Metals preparation costs should be clarified to reflect potential need to
analyze metals by more than one method;
4. Dry Weight Determination should be added to reflect IEPA reporting
requirements of soil samples;
5.
Delete reference to sampling devices and shipping costs. These costs are
not specific to analyses and should be moved to another location in the
Part.
6. IEPA should address how to handle potential tests requested by the
Agency and that are not listed in Appendix D.
7. LEPA should address costs for approved methods that are not specified in
Appendix D, For example BETX by method 8021 or PNAs by method
4
Printed on Recycled Paper in Accordance with
35
III. Adm. Code 101202 and 101. 302(g)
8310. Or the IEPA should remove all method references from Appendix
D when more than one method is approved.
I also recommend that Eligible Corrective Action Costs Section 732.625(4) and
734.625(4) be revised as follows:
Laboratory services necessary to determine site investigation and
whether the established remediation objectives have been met, including
but not limited to analyses, sample containers and collection devices such
as En Core ® samplers, purge-and-trap samplers or equivalentsampling
devices and shipping ofsample~
Finally, as costs ofsupplies and labor continue to escalate along with method and
certification requirements, I recommend that the costs be reviewed on a biannual basis
and adjusted if necessary. PIPE andlor IAETL would be honored to assist the agency in
this endeavor.
Thank you.
5
Printed on Recycled Paper in Accordance with 35 III. Adm, Code 101.202 and 101. 302(g)
ATTACHMENT A
ANALYTICAL COST FORM DRAFT
Laboratory Analysis — The laboratory analysis charge includes all costs associated with the transportation and/or
delivery, and
analysis
of each applicable sample. The charge includes but is not limited to costs associated with
laboratory
personnel,
samp~handling, transportation and/or delivery of samples to the laboratory,
sampling
equipment,
samplinu containers,
gloves,
and all aspects of the applicable laboratory analysis.
Laboratory
Analysis
Number of
Cost per
Total
Chemical
Samples
analysis
per analysis
ArsenicTCLPSoil
x
$10.00
=
$
ArsenicTotalSoil
x
$20.00
=
S
ArsenicWater
x
$10.00
=
5
Barium
TCLP
Soil
.
x
$10.00
. =
S
Barium
Total Soil
x
$20.00
$
BariumWater
x
$10.00
=
5
BETX Soil with MTBE (EPA 8260)
x
$60.00
=
S
BETX
-
Water with MTBE (EPA 8260)
x
$60.00
S
BOD
(Biological
Oxygen Demand)
x
$18.00
S
Cadmium TCLP
Soil
x
$10.00
S
Cadmium Total Soil
x
$20.00
S
CadmiumWater
x
$10.00
=
S
ChromiumTCLP
Soil
x
$10.00
=
S
ChromiumTotal Soil
x
$30.00
=
S
ChromiumWater
x
$30.00
=
5
Corrosivity
x
$25.00
=
$
CyanideTCLP Soil
x
$28.00
=
s
CyanideTotal Soil
x
$35.00
=
5
CyanideWater
.
x
$35.00
=
5
Flash Point or Ignitability Analysis EPA 1010
x
$25.00
=
S
FOC (Fraction Organic Carbon)
x
$50.00
=
S
Fat, Oil, & Grease(FOG)
x
$30.00
=
S
IronTCLPSoil
x
$10.00
=
$
IronWater
x
$10.00
=
5
LeadTCLPSoil
x
$65.00
=
S
LeadTotalSoil
x
$20.00
=
5
LeadWater
.
x
$10.00
=
S
LUST (Priority) Pollutants Soil
x
$550.00
=
S
Mercury TCLPSoil
x
$25.00
=
S
Mercury Total Soil
x
$25.00
S________________
MercuryWater
x
$25.00
=
5
Metals TCLP Soil (a combination of all metals) RCRA
x
$150.00
=
Metals Total Soil (a combination ol’ all metals) RCRA
x
$190.00
=
S
Metals Water (a combination of all metals) RCRA
x
$100.00
=
Organic Carbon (ASTM-D 2974-87)
x
$30.00
=
5
Oxygen (Dissolved)
x
520.0()
=
Paint Filter(Free Liquids)
x
=
S
PCI3 / Pesticides (combination)
x
.5(~00
=
5
PCI3s
x
575.00
=
S
Pesticides
x
x
$125.00
S
1ill
=
S
l)l1Ct~0l
x
$3(~00
=
$
l’oly Nuclear Aromatics l’NA,
or PAH
SOIL EEA 8270
x
$1 3(L00
=
S
l’oly Nuclear Aroinatics PNA, or PAl-I WATER EPA 827()
x
SI 30.0()
5
I of2
ANALYTICAL COST FORM DRAFT
Reactivity
x
s~~.oo
=
$
SeleniumTCLPSoil
$10.00
=
S
SeleniumTotal Soil
x
$20.00
=
S
SeleniumWater
x
$10.00
=
$
SiIverTCLP
Soil
x
$10.00
=
5
SilverTotal
Soil
x
$20.00
=
5
SilverWater
x
S10.00
=
$
SVOC
- Soil (Semi
Volatile Organic
Compounds)
x
$225.00
=
S
SVOC
- Water (Semi Volatile Organic Compounds)
x
$225.00
=
S
TKN (Total Kjeldahl) “nitrogen”
x
$35.00
=
S
TOC (Total Organic Carbon) EPA 9060A
x
$33.00
=
$
TPH (Total Petroleum Hydrocarbons)
x
$75.00
=
S
VOC (Volatile Organic Compound)
-
Soil (Non-Aqueous)
x
$110.00
=
S
VOC (Volatile Organic Compound)
-
Water
x
$150.00
=
S
Waste Characterization (Landfill Analysis)
x
$250.00
=
S
Geo-Technical
Bulk Density ASTM D4292 / D2937
x
$45.00
=
5
Ex-Situ Hydraulic Conductivity / Permeability
x
$255.00
=
5
Moisture Content ASTM D22l6-90 / D4643-87
x
$9.00
=
S
Porosity
x
$30.00
=
S
Rock Hydraulic Conductivity Ex-situ
x
$350.00
=
S
Sieve / Particle Size Analysis ASTM D422-63 / Dl 140-54
x
$116.00
=
S
Soil Classification ASTM D2488-90/ D2487-90
x
$70.00
=
S
TOTAL SAMPLING ACTIVITIES:
$
L
2 of2
Laboratory Analysis
Propsed
Chemical
Note
LAB
1
LAB
2
LAB 3
LAB
4
LAB 5
Average
Rate
Arsenic
TCLP Soil
1
$
112.00
$
70.00
$
85.75
$
115.75
$
85.00
$
93.70
$
115.75
Arsenic
Total Soil
2
$
24.00
$
25.00
$
23.25
$
43.50
$
40.00
$
31.15
$
43.50
ArsenicWater
3
$
24.00
$
25.00
$
23.25
$
33.50
$
34.00
$
27.95
$
34.00
BariumTCLPSoil
1
$
112.00
$
70.00
$
78.00
$
107.75
$
72.00
$
87.95
$
112.00
Barium Total Soil
2
$
24.00
$
25.00
$
15.50
$
35.50
$
27.00
$
25.40
$
35.50
Banum Water
3
$
24.00
$
25.00
$
15.50
$
25.50
$
22.00
$
22.40
$
25.50
BETX Soil
with
MTBE (EPA 8260)
4
$
90.00
$
82.00
$
91.25
$
87.00
$
70.00
$
8405
$
91.25
BEIX
-
Water with MTBE (EPA 8260)
4
$
90.00
$
70.00
$
85.00
$
87.00
$
70.00
$
80.40
$
90.00
BOD (Biological Oxygen Demand)
$
24.00
$
18.00
$
42.00
$
36.00
$
28.00
$
29.60
$
42.00
CadmiumTCLP Soil
1
$
112.00
$
70.00
$
85.75
$
115.75
$
85.00
$
93.70
$
115.75
CadmiumTotal Soil
2
$
24.00
$
25.00
$
23.25
$
43.50
$
40.00
$
31.15
$
43.50
CadmiumWater
3
$
24.00
$
25.00
$
23.25
$
33.50
$
34.00
$
27.95
$
34.00
ChromiumTCLP Soil
1
$
112.00
$
70.00
$
78.00
$
107.75
$
72.00
$
87.95
$
112.00
ChromiumlotalSoil
2
$
24.00
$
25.00
$
15.50
$
35.50
$
27.00
$
25.40
$
35.50
Chromium Water
3
$
24.00
$
25.00
$
15.50
$
25.50
$
22.00
$
22.40
$
25.50
Corrosivity
$
12.00
$
10.00
$
13.00
$
15.50
$
20.00
$
14.10
$
20.00
CyanideTCLPSoil
1
$
130.00
$
80.00
$
101.00
$
123.00
$
95.00
$
105.80
$
130.00
Cyanide Total Soil
$
30.00
$
35.00
$
38.50
$
30.75
$
35.00
$
33.85
$
38.50
CyanideWater
$
30.00
$
35.00
$
38.50
$
30.75
$
35.00
$
33.85
$
38.50
Flash Point or Ignitability Analysis EPA 1010
$
30.00
$
25.00
$
31.75
$
46.00
$
30.00
$
32.55
$
46.00
FOG (Fraction Organic Carbon)
$
24.00
-
$
24.25
$
51.25
$
50.00
$
37.38
$
51.25
Fat, Oil, & Grease (FOG)
.
$
36.00
$
50.00
$
100.00
$
61.50
$
50.00
$ 59.50 $
100.00
lionTCLP Soil
1
$
112.00
$
70.00
$
78.00
$
107.75
$
72.00
$ 87.95 $
112.00
IronWater
3
$
24.00
$
25.00
$
15.50
$
25.50
$
22.00
$
22.40
$
25.50
LeadTCLPSoil
1
$
112.00
$
70.00
$
86.00
$
115.75
$
85.00
$ 93.75 $ 115.75
Lead Total Soil
2
$
24.00
$
25.00
$
23.50
$
43.50
$
40.00
$
31.20
$
43.50
LeadWater
3
$
24.00
$
25.00
$
23.50
$
33.50
$
35.00
$ 28.20 $
35.00
LUST (Prionty) Pollutants Soil
5
$
660.00
$
710.00
$
656.25
$
711.75
$
725.00
$
692.60
$
725.00
Mercury
TCLPSoil
1
$
130.00
$
70.00
$
86.00
$
115.75
$
85.00
$
97.35
$
130.00
MercuryTotal Soil
$
30.00
$
25.00
$
23.50
$
23.50
$
25.00
$
25.40
$
30.00
Mercury Water
$
30.00
$
25.00
$
23.50
$
23.50
$
25.00
$
25.40
$
30.00
Metals TCLP Soil (a combination of all metals) RCRA
6
$
226.00
$
175.00
$
178.50
$
240.75
$
217.00
$
207.45
$
240.75
Metals Total Soil (a combination of all metals) RCRA
6
$
126.00
$
130.00
$
116.00
$
148.50
$
172.00
$
138.50
$
172.00
Metals Water (a combination of all metals) RCRA
6
$
126.00
$
130.00
$
116.00
$
148.50
$
167.00
$ 137.50 $ 167.00
Laboratory Analysis
$
18.25
$
35.00 $ 21.75 $
35.00
$
255.00
$
255.00
$
255.00
$
12.50
$
10.00
$
11.50
$
12.50
$
105.00
$
105.00
$
105.00
$ 350.00
$ 350.00 $
350.00
$
140.00
$ 150.00 $
145.00
$
150.00
Chemical
Note LAB 1
LAB 2
LAB 3
LAB 4
LAB 5
Propsed
AveraQe
Rate
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
$
Organic Carbon (ASTM-D 2974-87)
Oxygen (Dissolved)
Paint Filter (Free Liquids)
PCB
I
Pesticides (combination)
PCBs
Pesticides
pH
phenol
Poly Nuclear Aromatics PNA, or PAH SOIL EPA 8270
Poly Nuclear Aromatics PNA, or PAH WATER EPA 8270
Reactivity
Selenium TCLP Soil
Selenium Total Soil
Selenium Water
Silver TCLP Soil
Silver Total Soil
Silver Water
SVOC
-
Soil (Semi Volatile Organic Compounds)
SVOC
-
Water (Semi Volatile Organic Compounds)
TKN (Total Kjeldahl) ~nitrogen”
TOC (Total Organic Carbon) EPA 9060A
TPH (Total Petroleum Hydrocarbons)
VOC (Volatile Organic Compound)
-
Soil (Non-Aqueous)
VOC (Volatile Organic Compound)
-
Water
Waste Characterization (Landfill Analysis)
Geo-Technical
Bulk Density ASTM D4292
I
02937
Ex-Situ Hydraulic Conductivity / Permeability
Moisture Content ASTM D221 6-90
I
04643-87
Porosity
Rock Hydraulic Conductivity Ex-situ
Sieve
I
Particle Size Analysis ASTM D422-63 / 01140-54
Soil Classification ASTM D2488-90
I
02487-90
$
24.25
•$
13.00
$
13.00
$ 212.75
$
90.25
$
122.50
$
13.00
$
39.75
$
126.00
$
126.00
$
78.00
$
86.00
$
23.50
$
15.50
$
78.00
$
15.50
$
15.50
$
281.25
$
281.25
$
38.50
$
33.00
$
87.50
$
170.00
$
154.50
10.00
240.00
100.00
140.00
10.00
25.00
210.00
210.00
65.00
70.00
25.00
25.00
70.00
25.00
25.00
350.00
350.00
35.00
25.00
160.00
192.00
180.00
24.00
24.00
12.00
180.00
120.00
120.00
12.00
30.00
150.00
150.00
60.00
112.00
24.00
24.00
112.00
24.00
24.00
300.00
300.00
48.00
30.00
100.00
180.00
180.00
12.00
12.00
$
$
36.00 $
$
15.50 $
$ 225.00 $
$
92.25 $
$ 138.25 $
$
15.50 $
$
36.00 $
$ 138.25 $
$ 138.25 $
$
66.75 $
$ 115.75 $
$
43.50 $
$
25.50 $
$ 107.75 $
$
35.50 $
$
25.50 $
$ 307.50 $
$ 307.50 $
$
56.00 $
$
36.00 $
$ 102.50 $
$ 179.50 $
$ 179.25 $
$
$
$
$
$
$
$
$
7$
7$
$
1$
2$
3$
1$
2$
3$
$
$
$
$
8$
$
$
9
$
$
$
$
$
$
50.00
20.00
15.00
250.00
150.00
175.00
15.00
35.00
135.00
135.00
70.00
85.00
40.00
35.00
72.00
27.00
22.00
325.00
325.00
40.00
30.00
160.00
150.00
150.00
$ 32.75
$ 23.25
$ 13.10
$ 221.55
$ 110.50
$ 139.15
$ 13.10
$ 33.15
$ 151.85
$ 151.85
$ 67.95
$ 93.75
$ 31.20
$ 25.00
$ 87.95
$ 25.40
$ 22.40
$ 312.75
$ 312.75
$ 43.50
$ 30.80
$ 122.00
$ 174.30
$ 168.75
$
50.00
$
36.00
$
15.50
$
250.00
$
150.00
$ 175.00
$
15.50
$
39.75
$
210.00
$ 210.00
$ 78.00
$ 115.75
$
43.50
$
35.00
$
112.00
$
35.50
$
25.50
$
350.00
$ 350.00
$
56.00
$
36.00
$
160.00
$
192.00
$
180.00
Laboratory Analysis
Propsed
Chemical
Note LAB 1
LAB 2
LAB 3
LAB 4
LAB 5
Average
Rate
Dry Weight Reporting (per sample)
10
$
10.00 $
12.50 $
8.00 $
10.00 $ 10.13 $ 12.50
Turnaround Surcharge
11
4Day
50
25
25
25
31
50
3Day
50
100
50
50
50
60
100
2Day
100
100
100
75
100
95
100
1Day
100
100
125
100
200
125
200
Note 1: Price incudes preparation at the rate of:
$ 100.00
$
62.50 $
92.25 $
60.00 $ 78.69 $
100.00
Note 2: Price incudes preparation at the rate of:
$
12.00
$
20.00 $
15.00 $ 15.67 $
20.00
Note 3: Price incudes preparation at the rate of:
$
12.00
$
10.00 $
10.00 $ 10.67 $
12.00
Note 4: BTEX by method 8021 approved but not listed
Note 5: Volatiles, semivolitiles, pesticides and PCBs
Note 6: Seven LUST Metals including all Preps
Note 7: PNAs by 8310 approved by not listed
Note 8: TPH indudes GRO and DRO
Note 9: Specific analyses not defined
Note 10: Only applys to soil samples
Note 11: Normal TAT is 5-7 work days
IAETL DRAFT
6/9/2004
Laboratory Analysis
Average Proposed
Chemical
Note Average
SD
Mm
Max
+
I SD
Rate
ArsenicTCLP Soil
1
$
93.70
19.50 $ 70.00
$115.75 $113.20
$
114.00
ArsenicTotal Soil
2
$
31.15
9.77 $ 23.25 $ 43.50 $
40.92
$
41.00
ArsenicWater
3 $
27.95
5.33 $
23.25
$ 34.00 $
33.28
$
34.00
Barium TCLP Soil
I $
87.95
20.29 $ 70.00 $112.00 $108.24 $
109.00
BariumTotal Soil
2 $
25.40
7.15 $ 15.50 $ 35.50 $ 32.55 $
33.00
Barium Water
3 $
22.40
4.08 $ 15.50 $ 25.50 $ 26:48 $
26.00
BETX Soil with MTBE (EPA 8260)
4 $
84.05
8.62 $ 70.00 $ 91.25 $ 92.67 $
92.00
BETX
-
Water with MTBE (EPA 8260)
4 $
80.40
9.66 $ 70.00 $ 90.00 $ 90.06 $
90.00
BOD (Biological Oxygen Demand)
$
29.60
9.53 $ 18.00 $ 42.00 $ 39.13 $
40.00
Cadmium TCLP Soil
1 $
93.70
19.50 $ 70.00 $115.75 $113.20 $
114.00
Cadmium TotalSoil
2 $
31.15
9.77 $ 23.25 $ 43.50 $ 40.92 $
41.00
—~
Cadmium Water
3 $
27.95
5.33 $ 23.25 $ 34.00 $ 33.28 $
34.00
Chromium TCLP Soil
1 $
87.95
20.29 $ 70.00 $112.00 $ 108.24 $
109.00
ChromiumTotal Soil
2 $
25.40
7.15
$ 15.50 $ 35.50 $ 32.55 $
33.00
m
ChromiumWater
3 $
22.40
4.08 $ 15.50 $ 25.50 $ 26.48 $
26.00
Corrosivity
$
14.10
3.85 $ 10.00 $ 20.00 $ 17.95 $
18.00
a
Cyanide
TCLP Soil
1
$
105.80
20.54 $ 80.00 $ 130.00 $ 126.34 $
127.00
CyanideTotal Soil
$
33.85
3.49 $ 30.00 $ 38.50 $ 37.34 $
38.00
CyanideWater
$
33.85
3.49 $ 30.00 $ 38.50 $ 37.34 $
38.00
Flash Point or lgnitability Analysis EPA 1010
$
32.55
7.93 $ 25.00 $ 46.00 $ 40.48 $ 41.00
FOG (Fraction Organic Carbon)
$
37.38
15.31 $ 24.00 $ 51.25 $ 52.68 $
52.00
Fat, Oil,
&
Grease (FOG)
$
59.50
24.38 $ 36.00 $ 100.00 $ 83.88 $
84.00
Iron TCLP Soil
1 $
87.95
20.29 $ 70.00 $112.00 $ 108.24 $ 109.00
Iron Water
3 $
22.40
4.08 $ 15.50 $ 25.50 $ 26.48 $
26.00
Lead TCLP Soil
1 $
93.75
19.48 $ 70.00 $115.75 $113.23 $ 114.00
LeadTotalSoil
2
$
31.20
9.72 $ 23.50 $ 43.50 $ 40.92 $
41.00
LeadWater
3 $
28.20
5.57 $ 23.50 $ 35.00 $ 33.77 $
34.00
LUST (Priority) Pollutants Soil
5 $ 692.60
32.03 $656.25 $725.00 $ 724.63 $
725.00
MercuryTCLP Soil
1 $
97.35
24.67 $ 70.00 $130.00 $122.02 $
123.00
MercuryTotal Soil
$
25.40
2.68 $ 23.50 $ 30.00 $ 28.08 $
29.00
MercuryWater
$
25.40
2.68 $ 23.50 $ 30.00 $ 28.08 $
29.00
Metals TCLP Soil (a combination of all metals) RCRA
6 $ 207.45
29.31 $175.00 $240.75 $ 236.76 $
237.00
Metals Total Soil (a combination of all metals) RCRA
6 $
138.50
22.12 $116.00 $ 172.00 $ 160.62 $
161.00
~I
IAETL DRAFT
61912004
Laboratory Analysis
Average Proposed
Chemical
Note Average
SD
Miii
Max
+
1 SD
Rate
Metals Water (a combination of all metals) RCRA
6
$
137.50
20.26 $116.00 $167.00
$
157.76
$
158.00
Organic Carbon (ASTM-D 2974-87)
$
32.75
14.94
$
24.00
$
50.00
$
47.69
$
48.00
Oxygen (Dissolved)
$
23.25
9.64 $
13.00
$
36.00
$
32.89
$
33.00
Paint Filter(Free Liquids)
$
13.10
2.25 $ 10.00 $ 15.50 $ 15.35 $
16.00
PCB
I
Pesticides (combination)
$ 221.55
27.23 $ 180.00 $250.00 $ 248.78 $
249.00
PCBs
$ 110.50
25.02 $ 90.25 $150.00 $135.52 $
136.00
Pesticides
$ 139.15
21.97 $120.00 $175.00 $161.12 $
162.00
pH
$
13.10
2.25 $ 10.00 $ 15.50 $ 15.35 $
16.00
phenol
$
33.15
5.73 $ 25.00 $ 39.75 $ 38.88 $
39.00
Poly Nuclear Aromatics PNA, or PAH SOIL EPA 8270
7 $ 151.85
33.62 $126.00 $210.00 $ 185.47 $
186.00
Poly Nuclear Aromatics PNA, or PAH WATER EPA 8270
7 $ 151.85
33.62 $126.00 $210.00 $185.47 $
186.00
Reactivity
$
67.95
6.68 $ 60.00 $ 78.00 $
74.63
$
75.00
Selenium TCLP Soil
1 $
93.75
19.48 $ 70.00 $115.75 $ 113.23 $ 114.00
Selenium Total Soil
2 $
31.20
9.72 $ 23.50 $ 43.50 $ 40.92 $
41.00
SeleniumWater
3 $
25.00
6.92 $ 15.50 $ 35.00 $ 31.92 $
32.00
SilverTCLP Soil
1 $
87.95
20.29 $ 70.00 $112.00 $ 108.24 $
109.00
SilverTotal Soil
2 $
25.40
7.15 $ 15.50 $ 35.50 $
32.55
$
33.00
SilverWater
3 $
22.40
4.08 $ 15.50 $ 25.50 $ 26.48 $
26.00
SVOC
-
Soil (Semi Volatile Organic Compounds)
$ 312.75
26.08 $281.25 $350.00 $338.83 $
339.00
SVOC
-
Water (Semi Volatile Organic Compounds)
$ 312.75
26.08 $281.25 $350.00 $ 338.83 $
339.00
TKN (Total Kjeldahl) “nitrogen”
$
43.50
8.46 $ 35.00 $ 56.00 $ 51.96 $
52.00
TOC (Total Organic Carbon) EPA 9060A
$
30.80
4.09 $ 25.00 $ 36.00 $ 34.89 $
35.00
TPH (Total Petroleum Hydrocarbons)
8 $ 122.00
35.15 $ 87.50 $ 160.00 $ 157.15 $
158.00
VOC (Volatile Organic Compound)
-
Soil (Non-Aqueous)
$ 174.30
15.67 $150.00 $192.00 $ 189.97 $ 190.00
VOC (Volatile Organic Compound)
-
Water
$
168.75
15.i5 $150.00 $ 180.00 $ 183.90 $
180.00
Waste Characterization (Landfill Analysis)
9
Geo-Technical
Bulk Density ASTM D4292/D2937
$
21.75
11.89
$ 12.00 $ 35.00 $ 33.64 $
34.00
Ex-Situ Hydraulic Conductivity
I
Permeability
$ 255.00
$255.00 $255.00 $ 255.00 $
255.00
Moisture Content ASTM D2216-901 D4643-87
$
11.50
1.32 $ 10.00 $ 12.50 $ 12.82 $
13.00
Porosity
$ 105.00
$ 105.00 $ 105.00 $
105.00
$
105.00
Rock Hydraulic Conductivity Ex-situ
$
350.00
$350.00 $350.00 $ 350.00 $
350.00
2
IAETL
DRAFT
6/912004
Laboratory Analysis
$
21.75
$ 255.00
$
11.50
$ 105.00
$ 350.00
$ 35.00
$255.00
$ 12.50
$ 105.00
$350.00
$ 33.64
$ 255.00
$ 12.82
$
105.00
$ 350.00
$
34.00
$
255.00
$
13.00
$
105.00
$
350.00
Chemical
Note Average
SD
Miii
Max
Average
+
I
SD
Proposed
Rate
Metals Water (a combination of all metals) RCRA
6
$
137.50
20.26 $116.00 $167.00
$
157.76
$
158.00
Organic Carbon (ASTM-D 2974-87)
$
32.75
14.94 $
24.00
$
50.00
$ 47.69 $
48.00
Oxygen (Dissolved)
$
23.25
9.64 $ 13.00
$ 36.00 $
32.89
$
33.00
Paint Filter(Free Liquids)
$
13.10
2.25 $
10.00
$
15.50
$
15.35
$
16.00
PCB
I
Pesticides (combination)
$
221.55
27.23 $180.00 $250.00
$248.78
$
249.00
PCBs
$
110.50
25.02
$
90.25 $150.00 $135.52
$
136.00
Pesticides
$
139.15
21.97 $120.00 $175.00 $161.12
$
162.00
pH
$
13.10
2.25 $ 10.00 $ 15.50 $ 15.35 $
16.00
phenol
$
33.15
5.73 $ 25.00 $ 39.75 $ 38.88 $
39.00
Poly Nuclear Aromatics PNA, orPAH SOIL EPA 8270
7 $ 151.85
33.62 $126.00 $210.00 $185.47 $
186.00
Poly Nuclear Aromatics PNA, or PAH WATER EPA 8270
7 $ 151.85
33.62 $126.00 $210.00 $ 185.47 $ 186.00
Reactivity
$
67.95
6.68 $ 60.00
$ 78.00 $
74.63
$
75.00
SeleniumTCLPSoil
1 $
93.75
19.48 $ 70.00 $115.75 $113.23 $ 114.00
Selenium Total Soil
2 $
31.20
9.72 $ 23.50 $ 43.50 $ 40.92 $
41.00
Selenium Water
3 $
25.00
6.92 $ 15.50 $ 35.00 $ 31.92 $
32.00
SilverTCLP Soil
1
$
87.95
20.29
$ 70.00 $112.00 $
108.24
$
109.00
SilverTotal Soil
2 $
25.40
7.15 $
15.50
$ 35.50 $
32.55
$
33.00
SilverWater
3 $
22.40
4.08 $ 15.50 $ 25.50 $ 26.48
$
26.00
SVOC
-
Soil (Semi Volatile Organic Compounds)
$ 312.75
26.08 $281.25 $350.00 $ 338.83 $
339.00
SVOC
-
Water (Semi Volatile Organic Compounds)
$ 312.75
26.08
$281.25 $350.00 $ 338.83 $
339.00
TKN
(Total Kjeldahl) “nitrogen”
$
43.50
8.46
$ 35.00
$ 56.00 $ 51.96 $
52.00
TOG (Total Organic Carbon) EPA 9060A
$
30.80
4.09
$ 25.00
$ 36.00 $ 34.89
$ 35,00
TPH (Total Petroleum Hydrocarbons)
8
$
122.00
35.15
$ 87.50 $ 160.00 $
157.15
$
158.00
VOC (Volatile Organic Compound)
-
Soil (Non-Aqueous)
$
174.30
15.67
$ 150.00 $ 192.00 $ 189.97 $ 190.00
VOC (Volatile Organic Compound)
-
Water
$ 168.75
15.15
$150.00 $ 180.00 $
183.90
$
180.00
Waste Characterization (Landfill Analysis)
9
Geo-Technical
Bulk Density ASTM D4292 / D2937
11.89
$ 12.00
Ex-Situ Hydraulic Conductivity
I
Permeability
$255.00
Moisture Content ASTM D2216-90
I
D4643-87
1.32 $ 10.00
Porosity
$105.00
Rock Hydraulic Conductivity Ex-situ
$350.00
2
IAETL DRAFT
619/2004
Laboratory Analysis
Average Proposed
Chemical
Note Average
SD
Mm
Max
+
1
SD
Rate
Sieve / Particle Size Analysis ASTM D422-63
I
Dl 140-54
$ 145.00
7.07 $ 140.00 $ 150.00 $
152.07
$
150.00
Soil Classification ASTM D2488-90 / D2487-90
Dry Weight Reporting (per sample)
10 $
10.13
$ 12.50 $ 10.13 $
11.00
Turnaround Surcharge
11
4Day
31
50
3Day
60
100
2 Day
95
100
1 Day
125
200
Note 1: Price incudes preparation at the rate of:
$
78.69
$100.00 $ 78.69 $ 79.00
Note
2:
Price incudes preparation at the rate of:
$
15.67
$ 20.00 $ 15.67 $
16.00
Note 3: Price incudes preparation at the rate of:
$
10.67
$ 12.00 $ 10.67 $
11.00
Note 4: BTEX by method 8021 approved but not listed
Note 5: Volatiles, semivolitiles, pesticides and PCBs
Note 6: Seven LUST Metals including all Preps
Note 7: PNAs by 8310 approved by not listed
Note 8: TPH includes GRO and DRO
Note 9: Specific analyses not defined
Note 10: Only applys to soil samples
Note 11: Normal TAT is 5-7 work days
3
-
—~~~~—-—-—-—~----
I-
Section
732/734.
APPENDIX D Sample Analysis
Unit
of Production Description
Unit of Measure
Unit Cost
Barium TCLP Soil
EACH
$30.00
Barium Total Soil
EACH
$17.00
Barium Water
EACH
$15.00
Cadmium TCLP Soil
EACH
$35.00
Cadmium Total Soil
EACH
$25.00
Cadmium Water
-
EACH
$23.00
Chromium TCLP Soil
EACH
$30.00
-
Chromium Total Soil
-
EACH
$17.00
Chromium Water
EACH
$15.00
Cyanide TCLP Soil
EACH
$48.00
Cyanide Total Soil
EACH
$38.00
Cyanide Water
EACH
$38.00
Iron TCLP Soil
EACH
$30.00
Iron Total Soil
EACH
$17.00
Iron Water
EACH
$15.00
Lead TCLP Soil
EACH
$35.00
Lead Total Soil
EACH
$25.00
Lead Water
EACH
$23.00
Mercury TCLP Soil
EACH
$44.00
Mercury Total Soil
EACH
$29.00
Mercury Water
EACH
$29.00
Selenium TCLP Soil
EACH
$35.00
Selenium Total Soil
EACH
$25.00
Selenium Water
EACH
$21.00
Silver TCLP Soil
EACH
$30.00
Silver Total Soil
EACH
$17.00
Silver Water
EACH
$15.00
Metals TCLP Soil (a combination ofmetals listed in Appendix B
of this Part)
EACH
$158.00
Metals Total Soil (a combination of metals listed in Appendix B
of this Part)
EACH
$145.00
Metals Water (a combination of metals listed in Appendix B of
this Part)
EACH
$147.00
Soil prep. for Metals TCLP Soil (one fee per sample/per method)
EACH
$79.00
Soil prep. for Metals Total Soil (one fee per sample/per method)
EACH
$ 1 6.00
Water prep. for Metals Water (one fee per sample/per method)
EACH
5 11 .00
Soil Dry Weight Determination (one fee per soil sample)
EACH
$ 11.00

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