TITLE 35: ENVIRONMENTAL PROTECTION
SUBTITLE B: AIR POLLUTION
CHAPTER II: ENVIRONMENTAL PROTECTION AGENCY
PART 278
PROCEDURES FOR MEASURING TRANSFER EFFICIENCY FOR
SURFACE COATING OPERATIONS IN WOOD FURNITURE COATING FACILITIES
SUBPART A: INTRODUCTION
Section
278.101
Purpose
278.103
Definitions of Terms
278.105
Interpretation of Symbols
278.107
General Rules for Conduct of Tests
278.109
Incorporation by Reference
SUBPART B: MEASUREMENT METHODS
Section
278.201
Foil Strip Film Transfer Efficiency Test
278.202
Mileage Film on Coating Object Transfer Efficiency Test
278.203
Production Record Mileage Transfer Efficiency Test
AUTHORITY: Implementing Sections 4(b), (e) and (g), 9(a), 30 and 5(b), and authorized by
Sections 4(h) and 39 of the Environmental Protection Act (Ill. Rev. Stat. 1985 and 1986 Supp.,
ch. 111 1/2, par. 1004(b), (e), (g) and (h), 1005(b), 1009(a), 1030, and 1039) and authorized by
35 Ill. Adm. Code 215.108(h).
SOURCE: Adopted at 11 Ill. Reg. 19105, effective November 10, 1987.
SUBPART A: INTRODUCTION
Section 278.101
Purpose
The purpose of this Part is to establish general procedures for measuring transfer efficiency from
surface coating operations to determine compliance. Sources which are subject to emission
limitations pursuant to 35 Ill. Adm. Code 215.204(1) shall comply with any applicable method
for measurement of transfer efficiency described herein.
Section 278.103
Definitions of Terms
"Coating Object": any object or combination of objects which is being produced at a
wood coating furniture facility.
"Mileage": the amount of square feet that a gallon of paint will cover at a standard film
thickness of 1 mil.
Section 278.105
Interpretation of Symbols
"Ai": square feet per individual coating object(Ft(2)).
"F": average film thickness during test as measured in mils (mils).
"Pi": number of coating objects produced for each combination of coating objects
painted.
"Vt": paint usage for the test period, as measured in gallons (gal).
Section 278.107
General Rules for Conduct of Tests
a)
A person planning to conduct a transfer efficiency test to demonstrate compliance with
35 Ill. Adm. Code 215.104(1) shall notify the Illinois Environmental Protection Agency
(Agency) of that intent not less than 30 days before the planned initiation of the tests so
that the Agency may observe the test.
b)
Any person conducting a transfer efficiency test to demonstrate compliance with 35 Ill.
Adm. Code 215.104(1) shall record parameters measured or calculated at the site and
observations on process operations either manually, by the observer and initiated, or by
means of electric or mechanical recording equipment.
Verification of a transfer efficiency test shall be demonstrated by supplying the following
information:
1)
Additional monitored information available to the owner or operator which
substantiates the recorded data;
2)
Evidence that the instrument has been certified by USEPA; or
3)
Calibration data which show that the equipment was operated within the
manufacturer's specifications.
c)
Samples taken for analysis by persons other than the owner or operator or employees of
the testing company shall be accompanied by a record of transfers and the identities of
holders so that persons responsible for preservation of the sample and analysis can be
known.
d)
Data and records submitted to the Agency may be claimed as confidential pursuant to 35
Ill. Adm. Code 161. However, emission information shall be available to the public in
accordance with Section 7(c) of the Environmental Protection Act (Ill. Rev. Stat. 1985,
ch. 111 1/2, par. 1001 et seq.) (the Act) and 35 Ill. Adm. Code 160.
e)
Laboratory analysis reports shall include the identity of the analyst and the procedure
used.
f)
A final report shall contain the following information:
1)
A summary of results;
2)
The company name and location, the test dates, a description of the process tested
and what test was conducted;
3)
Description of test conditions. This description shall include control equipment
and the portion of process tested including:
A)
Parameters monitored and values for each parameter. The parameters are
those listed in Sections 278.107(g)(2), (4), (6)-(9); 278.201(a), (h), (j), (k),
(n), (o), (q), and (r); and 278.203(a)-(d).
B)
Process samples taken or analyzed; and
C)
Instruments monitored and their calibrations.
4)
Data and calculations including:
A)
Copies of all raw filed data sheets;
B)
Record of any transfers and holders as described in Subsection 278.107(c)
above;
C)
Copies of all laboratory sheets showing any analyses;
D)
Copies of all calculations used to arrive at results;
E)
Data on equipment calibration;
F)
Process information including:
i)
Raw materials
ii)
Process rate
iii)
Mode of operation: manual or automatic; cleaning and auxiliary
systems; and process cycles.
G)
Conclusions which shall include results of the tests in the units of the
applicable standard and any additional information to assist the Agency in
interpreting the results in relaitonship to equipment performance.
g)
Any person conducting a transfer efficiency test to demonstrate compliance with 35 Ill.
Adm. Code 215.104(l) shall:
1)
Inspect all equipment to be used. All equipment and materials must meet the
requirements of the manufacturer's specifications;
2)
Set up paint supply and mass flow measurement equipment per manufacturer's
instructions;
3)
According to Section 9.8 of National Fire Code, No. 33 (NFPA 33), when using
fixed electrostatic apparatus, the resistance of the equipment to ground shall be
measured at a resistance of less than one million Ohms;
4)
If electrostatic equipment is being used, the gun-to-target distance should be at
least twice the sparking distance. This requirement is in accordance with Section
9-7 NFPA 33;
5)
Calibrate the mass flow measurement equipment once per week or each time that
it is moved, whichever occurs more frequently. The mass flow measurement
equipment is calibrated flow instrument or by a primary means of measuremnt
such as a stopwatch and a container of known weight.
6)
Begin agitation of paint at least thirty minutes before any paint samples are taken;
7)
Using a small glass jar with an airtight lid, take a paint grab sample from the paint
pot;
8)
Record test run number on label jar (each pass of ten targets is a run); and
9)
Paint weight percent solids shall be determined by the person conducting the test
at the start of each day, at the end of each day and at any other time deemed
appropriate (e.g. new batch of paint, viscosity of paint changes, and physical
characteristics such as color change).
Section 278.109
Incorporation by Reference
The following materials are incorporated by reference. These standards do not include any later
amendments or editions.
a)
American Society for Testing and Materials (ASTM), 1916 Race Street, Philadelphia, PA
19103. ASTM Standards.
D-1005 - 1984 Measurement of Dry Film Thickness of Organic Coatings
D-1200 - 1982 Viscosity of Paints, Varnishes, and Lacquers by Ford Viscosity
Cup
D-1212 - 1985 Measurement of Wet Film Thickness of Organic Coatings
D-1475 - 1985 Density of Paint Varnish, Lacquer, and Related Products
D-2369 - 1982 Standard Test Method for Volatile Content of Coatings
D-3925 - 1981 Sampling Liquid Paints and Related Pigmented Coatings
(reapproved 1986)
b)
National Fire Codes, by National Fire Protection Association, Batterymarch Park,
Quincy, MA. NFPA No. 33 1986.
SUBPART B: MEASUREMENT METHODS
Section 278.201
Foil Strip Film Transfer Efficiency Test
This method is the preferred test method and is to be used except for the special conditions
described in Sections 278.202 and 278.203. When using this test method, the following steps
shall be followed in the order presented:
a)
Set up the conveyor speed measuring equipment consisting of photoelectric cells or limit
switches used in conjunction with a digital timer, or timing marks on the conveyor used
in conjunction with a stopwatch.
b)
Cut an appropriate number of strips of 0.0037 cm (1.5 mil) thick aluminum foil to
dimensions of 38.1 cm (15 in) by approximately 127 cm (50 in) for the testing.
c)
Consecutively number each precut foil strip on the dull side using a permanent marking
pen.
d)
Weigh each foil strip and record the foil number and mass.
e)
Attach preweighed labeled foil (dull side to the target) to six targets. Attach unlabeled
foil on four scavenger targets. All seams must face away from the spray equipment.
f)
Mount the foil-covered targets in consecutive order from right to left (facing the booth)
with the foil seam on each target facing away from the spray gun.
g)
Adjust all equipment operating parameters to the values desired for testing.
h)
Cure time and temperature of the oven should be set per manufacturer's instructions.
i)
Recheck operating parameters to ensure that they are correct.
j)
For electrostatic spray equipment, measure the operating voltage and adjust according to
manufacturer's instructions and record value.
k)
Inspect conveyor clock, stopwatch, and mass flow measurement equipment to assure that
all are prepared to operate.
l)
Turn on spray booth and conveyor. As the leading edge of the first scavenger target
passes in front of the gun, turn on paint spray equipment and simultaneously begin mass
flow measurement.
m)
As the trailing edge of the last scavenger target passes in front of the gun, stop the paint
spray equipment and mass flow measurement simultaneously.
n)
Record the mass flow measurement.
o)
Measure the wet film thickness on the trailing scavenger and record.
p)
Remove the painted targets from the conveyor and ensure that no paint is lost. Securely
hang the coated targets on oven racks so all painted surfaces are exposed for uniform
drying. Orient all targets in the same direction in the curing oven.
q)
Insert racks in oven and bake at manufacturer's recommended schedule. Oven door shall
be opened for minimum amount of time to prevent cooling.
r)
Remove targets from oven and record actual cure schedule on a separate data sheet. Cool
foil to room temperature. Remove foil from each target, weigh foil and record mass on
each foil and on a separate data sheet.
s)
After weighing, store foils in plastic bags, with the test run number labeled on each bag.
The laboratory shall retain all samples until data analyses are complete. Check all data
for correctness and completeness.
Section 278.202
Mileage Film on Coating Object Transfer Efficiency Test
This test may be used for very small or intricate parts which cannot be tested under the preceding
Sections 278.201. When using this test method, the following techniques shall be used:
a)
Each of the steps as set forth in the preceding Section 278.201 shall be followed, except
that no foil shall be used and the film shall be measured directly on the coating object.
b)
If a primer coat or coats have previously been applied, the film thickness of that coat or
coats shall be measured and averaged before topcoating. The measurment method for the
primer coat or coats shall be identical to that set forth in Section 278.201 herein.
Section 278.203
Production Record Mileage Transfer Efficiency Test
This test method utilizes the production records of a facility to determine the overall efficiency
of utilization of paint, including repainting of rejects, spillage, color change waste, etc. When
using this test method, the following steps shall be followed in the order presented:
a)
The square footage per coating object shall be measured, calculated and recorded as Ai
(square ft/coating object).
b)
The number of coating objects produced shall be counted and recorded for each
combination of coating objects produced and recorded as Pi.
c)
The paint and solvent usage shall be recorded during the measurement period (Vt
gallons).
d)
The film thickness shall be checked at least five times during the test at reasonable
intervals, and shall be averaged and recorded. (F mils)
e)
Mileage shall then be calculated according to the following formula:
mileage = F x Summation of (Pi)(Ai)/Vt
f)
The transfer efficiency shall be calculated according to the following formula:
T.E. = mileage/theoretical mileage at 100% application efficiency