ILLINOIS POLLUTION CONTROL BOARD

December 20,

1990

IN THE MATTER OF:

)

R90—1l

RCRA UPDATE, USEPA REGULATIONS

)

(Identical

in Substance Rules)

(4—1—90 THROUGH 6—30—90)

)

PROPOSAL FOR PUBLIC COMMENT

PROPOSED ORDER OF THE BOARD

(By J. Anderson):

Pursuant to Sections 22.4(a) of the Environmental Protection Act (Act),

the Board proposes amendments to the Resource Conservation and Recovery Act

(RCRA)

regulations.

Section 22.4(a)

provides for quick adoption of regulations which are

“identical

in substance” to federal regulations and that Title VII of the Act

and Section

5 of the Administrative Procedure Act (APA)

shall not apply.

Because this rulemaking is not subject to Section 5 of the APA, it

is not

subject to first notice or to second notice review by the Joint Committee on

Administrative Rules

(JCAR).

The federal RCRA regulations are found at 40 CFR

260 through 268.

This rulemaking updates RCRA rules to correspond with

federal amendments more fully outlined in the accompanying Opinion.

This Order

is supported by an Opinion adopted on the

same

day.

The

Board will receive public comment on the proposal for a period of 45 days

following

its publication in the Illinois Register.

The complete text of the

proposed rules follows.

IT IS SO ORDERED.

I,

Dorothy M.

Gunn,

Clerk of the Illinois Pollution Control Board,

hereby

certify that the above Order was adopted on the

______________

day of

______________

1990,

by a vote of

7

O

~~74

#/~

Dorothy M. ~

Clerk

Illinois Pol~htionControl Board

117—321

---

2

TITLE

35:

ENVIRONMENTAL PROTECTION

SUBTITLE G:

WASTE DISPOSAL

CHAPTER

I:

POLLUTION CONTROL BOARD

SUBCHAPTER b:

PERMITS

PART 703

RCRA PERMIT

PROGRAM

SUBPART A:

GENERAL PROVISIONS

SUBPART B:

PROHIBITIONS

Prohibitions in General

RCRA Permits

Specific Inclusions in Permit Program

Specific Exclusions from Permit Program

Discharges of Hazardous Waste

Reappiicatioris

Initial Applications

Federal Permits (Repealed)

SUBPART

C:

AUTHORIZATION BY RULE

AND

INTERIM STATUS

Purpose and Scope

Permits by Rule

Application by Existing HWM Facilities

QualificationB

Application by New

HWM

Facilities

Amended Part A Application

Qualifying for Interim Status

Prohibitions During Interim Status

Changes During Interim Status

Interim Status Standards

Grounds for Termination of Interim Status

Permits for Less Than an Entire Facility

Closure by Removal

Procedures for Closure Determination

SUBPART D:

APPLICATIONS

Scope and Relation to Other Parts

Purpose

References

Section

703. 100

703.101

703.110

Section

703. 120

703. 121

703.122

703. 123

703.124

703. 125

703. 126

703. 127

Section

703. 140

703. 141

703. 150

703. 151

703. 152

703. 153

703.154

703. 155

703. 156

703. 157

703. 158

703.159

703. 160

Section

703. 180

703. 181

703. 182

703. 183

703. 184

703.

185

703.186

703.187

and Interim Status

Applications in General

Contents of Part A

Contents of Part B

General Information

Facility Location Information

Groundwater Protection Information

Exposure Information

Solid Waste Management Units

117—32 2

---

3

703.188

Other Information

703.200

Specific Information

703.201

Containers

703.202

Tank Systems

703.203

Surface Impoundments

703.204

Waste Piles

703.205

Incinerators

703.206

Land Treatment

703.207

Landfills

703.209

Miscellaneous Units

SUBPART E:

SHORT TERM AND PHASED PERMITS

Section

703.221

Emergency Permits

703.222

Incinerator Conditions Prior to Trial Burn

703.223

Incinerator Conditions During Trial Burn

703.224

Incinerator Conditions After Trial Burn

703.225

Trial Burns for Existing Incinerators

703.230

Land Treatment Demonstration

703.231

Research,

Development and Demonstration Permits

SUBPART F:

PERMIT CONDITIONS OR DENIAL

Section

703.240

Permit Denial

703.241

Establishing Permit Conditions

703.242

Noncompliance Pursuant to Emergency Permit

703.243

Monitoring

703.244

Notice of Planned Changes

703.245

Twenty-four Hour Reporting

703.246

Reporting Requirements

703.247

Anticipated Noncompliance

SUBPART G:

CHANGES TO PERMITS

Section

703.260

Transfer

703.270

Modification

703.271

Causes for Modification

703.272

Causes

for Modification or Reissuance

703.273

Facility Siting

703.280

Permit Modification at the Request of the Permittee

703.281

Class

1 Modifications

703.282

Class

2 Modifications

703.283

Class

3 Modifications

Appendix A

Classification of Permit Modifications

AUTHORITY:

Implementing Section 22.4 and authorized by Section

27 of the

Environmental Protection Act (Ill. Rev.

Stat.

1989, ch.

111

1/2,

pars.

1022.4

and 1027).

SOURCE:

Adopted in R82-19,

53 PCB

131,

at

7

Ill. Reg.

14289, effective

October

12,

1983;

amended in R83—24 at 8

Ill. Reg.

206, effective December 27,

117—323

---

4

1983; amended

in R84—9 at

9

Ill.

Reg.

11899, effective July 24,

1985;

amended

in R85-22 at 10

Ill.

Reg.

1110, effective January

2,

1987;

amended in R85-23

at

10

Ill. Reg.

13284, effective July 28,

1986;

amended in R86-1 at 10

Ill.

Reg.

14093, effective August

12,

1986; amended in R86—19 at

10

Ill.

Reg.

20702, effective December

2,

1986;

amended in R86—28 at

11 Ill. Reg.

6121,

effective March 24,

1987;

amended in R86—46 at 11 Ill. Reg.

13543, effective

August

4,

1987;

amended in R87—5 at

11

Ill. Reg.

19383, effective November 12,

1987;

amended in R87—26 at

12

Ill. Reg.

2584,

effective January 15,

1988;

amended in R87—39

at

12

Ill. Reg.

13069, effective July 29,

1988;

amended in

R88-16 at

13

Ill.

Reg. 447, effective December 27,

1988; amended in R89—1

at

13

Ill.

Reg.

18477, effective November 13,

1989; amended in R89—9 at

14

Ill.

Reg.

6278,

effective April

16,

1990; amended in R90—2 at

14

Ill.

Reg.

14492,

effective August

22,

1990;

amended

in R90—11 at 15

Ill.

Reg.

,

effective

SUBPART D:

APPLICATIONS

Section 703.183

General Information

The following information is required in the Part

B application for all HWM

facilities,

except as

35

Ill. Adm. Code 724.101 provides otherwise:

a)

A general description of the facility;

b)

Chemical and physical analyses of the hazardous wastes to be

handled at the facility.

At a minimum,

these analyses must

contain all the information which must be known to treat,

store or

dispose of the wastes properly in accordance with 35 Ill.

Adrn.

Code 724;

c)

A copy of the waste analysis plan required by 35

Ill.

Adxn.

Code

724.113(b)

and,

if applicable,

35

Ill.

Adm. Code 724.113(c);

d)

A description of the security procedures and equipment required by

35

Ill. Adm.

Code 724.114,

or a justification demonstrating the

reasons for requesting a waiver of this requirement;

e)

A copy of the general inspection schedule required by 35

Ill.

Adm.

Code 724.115(b).

Include where applicable,

as part of the

inspection schedule,

specific requirements in 35

Ill.

Adxn. Code

724.274,

724.293(i),

724.295,

724.326,

724.354,

724.373, 724.403~

et~4724.702, 724.933,

724.952, 924.953 and 724.958

f)

A justification of any request for

a waiver of the preparedness

and prevention requirements of 35

Ill. Adm. Code 724.Subpart

C;

g)

A copy of the contingency plan required by 35

Ill. Adm. Code

724.Subpart D;

BOARD NOTE:

Include, where applicable,

as part of the contingency

plan,

specific requirements in 35

Ill. Adm. Code 724.327 and

724.355.

35

Ill. Adm. Code 724.355 has not yet been adopted.

117—324

---

5

h)

A description of procedures,

structures or equipment used at the

facility to:

1)

Prevent hazards in unloading operations

(for example,

ramps,

special forklifts);

2)

Prevent runoff from hazardous waste handling areas to other

areas of the facility or environment,

or to prevent flooding

(for example, berms, dikes,

trenches);

3)

Prevent contamination of water supplies;

4)

Mitigate effects of equipment failure and power outages; et~4

5)

Prevent undue exposure of personnel to hazardous waste

(for

example, protective clothing); ~

~j

Prevent releases to the atmosphere.

i)

A description of precautions to prevent accidental ignition or

reaction of ignitable, reactive or incompatible wastes as required

to demonstrate compliance with 35

Ill. Adm. Code 724.117 including

documentation demonstrating compliance with

35

Ill.

Adm. Code

724.117(c);

j)

Traffic pattern, estimated volume

(number, types of vehicles)

and

control

(for example,

show turns across traffic lanes and stacking

lanes

(if appropriate); describe access road surfacing and load

bearing capacity;

show traffic control signals);

k)

Facility location information as required by Section 703.184;

1)

An outline of both the introductory and continuing training

programs by owners or operators to prepare persons to operate or

maintain the HWM facility in a safe manner as required to

demonstrate compliance with 35

Ill.

Adin.

Code 724.116.

A brief

description of how training will be designed to meet actual job

tasks in accordance with requirements in 35 Ill.

Adxn.

Code

724. 116(a) (3);

m)

A copy of the closure plan and, where applicable, the post—

closure plan required by 35

Ill. Adm.

Code 724.212, 724.218 and

724.297.

Include where applicable, as part of the plans,

specific

requirements in 35

Ill. Adm. Code 724.278,

724.297,

724.328,

724.358,

724.380,

724.410, 724.451,

724.701 and 724.703;

n)

For

hazardous

waste

disposal

units

that

have

been

closed,

documentation that notices required under 35 Ill.

Adm

Code

724.219

have been filed;

117—325

---

6

0)

The most recent closure cost estimate for the facility prepared in

accordance with 35

Ill. Mm.

Code

724.242 and a copy of the

documentation required to demonstrate financial assurance under 35

Ill. Adm. Code 724.243.

For a new facility,

a copy of the

required documentation may be submitted 60 days prior to the

intitial receipt of hazardous wastes,

if

it

is later than the

submission of the Part B;

p)

Where applicable,

the most recent post—closure cost estimate for

the facility prepared in accordance with 35

Ill. Adm. Code 724.244

plus a copy of the documentation required to demonstrate financial

assurance under 35

Ill. Adm. Code 724.245; For a new facility, a

copy of the required documentation may be submitted 60 days prior

to the intitial receipt of hazardous wastes,

if

it is later than

the submission of the Part

B;

q)

Where applicable,

a copy of the insurance policy or other

documentation which comprises compliance with the requirements of

35

Ill. Adm. Code 724.247.

For a new facility, documentation

showing the amount of insurance meeting the specification

of 35

Ill.

Adm.

Code 724.247(a) and,

if applicable,

35 Ill.

Adm.

Code

724.247(b), that the owner or operator plans to have

in effect

before initial receipt of hazardous waste for treatment,

storage

or disposal.

A request for an alternative level of required

coverage,

for

a new or existing facility, may be submitted as

specified in 35

Ill. Adm.

Code 724.247(c);

s)

A topographic map showing a distance of 1000 feet around the

facility at

a scale of 2.5 centimeters

(1

inch)

equal to not more

than 61.0 meters

(200 feet).

Contours must be shown on the map.

The contour interval must be sufficient to clearly show the

pattern of surface water flow in the vicinity of and from each

operational unit of the facility.

For example,

contours with an

interval

of 1.5 meters

(5 feet),

if relief is greater than 6.1

meters (20 feet),

or an interval of 0.6 meters

(2 feet),

if relief

is less than 6.1 meters

(20 feet).

Owners and operators of HWM

facilities located

in mountainous areas shall use larger contour

intervals to adequately show topographic profiles of facilities.

The map must clearly show the following:

1)

Map scale and date;

2)

100—year floodplain area;

3)

Surface waters including intermittent streams;

4)

Surrounding land uses

(residential,

commercial,

agricultural,

recreational);

5)

A wind rose

(i.e., prevailing windspeed and direction);

6)

Orientation of the map (north arrow);

117—326

---

7

7)

Legal boundaries of the HWM facility site;

8)

Access control

(fences,

gates);

9)

Injection and withdrawal wells both on-site and off—site;

10)

Buildings; treatment,

storage or disposal operations;

or

other structures (recreation areas,

runoff control systems,

access and internal roadB,

8torm, sanitary and process

sewage systems,

loading and unloading areas,

fire control

facilities,

etc.);

11)

Barriers for drainage or flood control;

12)

Location of operational units within the HWM facility site,

where hazardous waste is

(or will be) treated,

stored or

disposed (include equipment cleanup areas);

BOARD NOTE:

For large HWM facilities, the Agency shall

allow the use of other scales on a case by case basis.

t)

Applicants shall submit such information as the Agency determines

is necessary for

it to determine whether to issue

a permit and

what conditions to impose

in any permit issued.

u)

For land disposal facilities,

if a case—by-case extension has been

approved under 35

Ill.

Adm.

Code 728.105,

or if a petition has

been approved under 35

Ill.

Adm. Code 728.106,

a copy of the

notice of approval of the extension or of approval of the petition

is required.

BOARD NOTE:

Derived from

40

CFR

270.14(b)

(1988),

as amended at

54

Fed.

Reg.

617, January 9,

1989.

(Source:

Amended at

15

Ill.

Reg.

,

effective

Section 703.210

Process Vents

Except

as otherwise provided in 35 111.

Adm. Code 724.101,

owners and

operators of facilities which have process vents to which 35

Ill.

Adm. Code

724.Subpart AA applies shall provide the following additional information:

~j

For facilities which cannot

install a closed—vent system and

control device to comply with 35

Ill.

Adm. Code 724.Subpart AA,

on

the effective date on which the facility becomes

sub-lect to that

Subpart or

35 Ill. Adm. Code 725.Subpart AA,

an implementation

schedule

as specified in

35

Ill. Adm. Code 724.933(aY(2).

~j

Documentation of compliance with the process vent standards

in

35

Ill.

Adm. Code 724.932,

includinQ:

117—32 7

---

8

fl

Information and data identifying all affected process vents,

annual throughput and operating hours of each affected unit,

estimated emission rates for the affected vent and for the

overall facility (i.e.,

the total emissions for all affected

vents at the facility)

and the a~~roximatelocation within

the facility of each affected unit (e.g..

identify the

hazardous waste management units on

a facility plot plan~.

~

Information and data su~~ortinaestimates of vent emissions

and emission reduction achieved by add—on control devices

based on engineering calculations or source tests.

For the

purpose of determining compliance, estimates of vent

emissions and emission reductions must be made using

operating parameter values

(e.g., temperatures,

flow rates

or concentrations) which represent the conditions which

exist when the waste management unit is operating at the

highest load or capacity level reasonably expected to occur.

~j

Information and data used to determine whether or not a

process vent

is subject to 35 Ill.

Adrn. Code 724.932.

çj

Where an owner or operator applies for permission to use a control

device

other

than a thermal vapor incinerator, catalytic vapor

incinerator,

flare, boiler,

process heater,

condenser or carbon

adsorption system to comply with 35

Ill.

Adm. Code 724.932,

and

chooses to use test data to determine the organic removal

efficiency or the total organic compound concentration achieved by

the control device,

a performance test plan as specified

in

35

Ill.

Adm.

Code 724.935(b) (3).

~j

Documentation of compliance with 35

Ill.

Adm.

Code

724.933,

including:

fl

A list of all information references and sources used in

preparing the documentation.

~J

Records

including the dates of each compliance test required

by 35

Ill. Adm. Code 724.933(k).

~j.

A design analysis, specifications,

drawings,

schematics,

and

piping and instrumentation diagrams based on the appropriate

sections of APTI Course 415,

incorporated by reference in 35

Ill. Adm. Code 720.111,

or other engineering texts approved

by the Agency which present basic control device design

information.

The design analysis must address the vent

stream

characteristics

and

control

device

parameters

as

sepcified in 35

Ill.

Adm.

Code

724.935(b)

(4) (CI.

~).

A statement signed and dated by the owner or operator

certifying that the o~eratina~arametere used in the design

analysis reasonably represent the conditions which exist

when the hazardous wapte management unit

is or would be

117—328

---

9

when

the

hazardous

waste

management

unit

is

or

would

be

operating at the highest load or capacity level reasonably

expected

to

occur.

~J.

A

statement

signed

and

dated

by

the

owner

or

operator

certifying that the control device

is designed to operate at

an

efficiency

of

95

weight

percent

or

greater

unless

the

total

organic

emission

limits

of

35

Ill.

Adm.

Code

724.932(a)

for

affected

process

vents

at

the

facility

can

be

attained

by

a

control

device

involving

vapor

recovery

at

an

efficiency

less

than

95

weight

percent.

(Source:

Added

at

15

Ill.

Reg.

,

effective

Section

703.211

Equipment

Except

as

otherwise

provided

in

35

Ill.

Adm.

Code

724.101,

owners

and

operators

of

facilities

which

have

equipment

to

which

35

Ill.

Ad.m.

Code

724.Subpart

BB

applies

shall

provide

the

following

additional

information:

~J

For

each

piece

of

equipment to which

35

Ill.

Adm.

Code

724.Subpart

BB

applies:

fl

Equipment

identification

number

and

hazardous

waste

management

unit

identification.

2.1

Approximate

locations

within

the

facility

(e.g.,

identify

the

hazardous

waste

management

unit

on

a

facility

plot

plan).

~j

Type

of

equipment

(e.g.,

a

pump

or

pipeline

valve).

j)

Percent

by

weight

total

organica

in

the

hazardous

wastestream

at

the

equipment.

.~j

Hazardous

waste

state

at

the

equipment

(e.g.,

gas/vapor

or

liquid).

QJ

Method

of

compliance

with

the

standard

(e.g.,

“monthly

leak

detection

and

repair”

or

“eguipped

with

dual

mechanical

seals”).

~j.

For

facilities

which

cannot

install

a

closed-vent

system

and

control

device

to

comply

with

35

Ill.

Adm.

Code

724.Subpart

BB

on

the

effective

date

that

facility

becomes

subiect

to

this

Subpart

or

35

Ill.

Adm.

Code

724.Subpart

BB.

an

implementation schedule

as

specified

in

35

Ill.

Mm.

Code

724.933(a)

(2).

~j

Where

an

owner

or

operator

applies

for

permission

to

use

a

control

device

other

than

a

thermal

vapor

incinerator,

catalytic

vapor

incinerator,

flare,

boiler,

process

heater,

condenser

or

carbon

adsorption

system

and

chooses

to

use

test

data

to

determine

the

117—32 9

---

10

concentration

achieved

by

the

control

device,

a

performance

test

plan

as

specified

in

35

Ill.

Adni.

Code

724.935(b)

(3).

~j

Documentation which demonstrates compliance with the equipment

standards in 35

Ill.

Adrn.

Code 724.952 or 724.959.

this

documentationmust

contain

the

records

re~uirad

under

35

Ill.

Adm.

Code 724.964.

The Agency shall request further documentation

if

necessary to demonstrate compliance.

Documentation to demonstrate

compliance with 35

Ill.

Adm.

Code 724.960m must include the

following information:

fl

A

list

of

all

information

references

and

sources

used

in

preparing

the

documentation.

21

Records including the dates of each compliance test required

by 35

Ill.

Adm. Code 724.933(1).

fl

A

design

analysis,

specifications,

drawings,

schematics,

and

piping

and instrumentation diagrams based on the appropriate

sections of APTI Course 415,

incorporated by reference

in

35

Ill.

Mm.

Code

720.111,

or

other

engineering

texts

appproved

by

the

Agency

which

present

basic

control

device

design

information.

The

design

analysis must address the vent

stream

characteristics

and

control

device

parameters

as

specified

in

35

Ill.

Adm.

Code

724.935(b)

(4) (C).

j).

A statement signed and dated by the owner or operator

certifying

that

the

operating

parameters

used

in

the

design

analvsis reasonably represent the conditions which exist

when

the

hazardous waste management unit

is or would be

operating

at

the

highest

load

or

capacity

level

reasonably

expected

to

occur.

~j

A

statement

signed

and

dated

by

the

owner

or

operator

certifying

that

the

control

device

is

designed

to

operate

at

an

efficiency

of

95

weight

percent

or

greater.

(Source:

Added

at

15

Ill.

Reg.

,

effective

)

117—330

---

11

Section 703.Appendix A

Classification of Permit Modifications

Class Modifications

A.

General Permit Provisions

1

1.

Administrative and informational changes.

1

2.

Correction of typographical errors.

1

3.

Equipment replacement or upgrading with functionally

equivalent

components

(e.g., pipes,

valves,

pumps,

conveyors,

controls).

4.

Changes in the frequency of or procedures for monitoring,

reporting, sampling or maintenance activities by the

permittee:

1

a.

To provide for more frequent monitoring, reporting or

maintenance.

2

b.

Other changes.

5.

Schedule of compliance:

1*

a.

Changes in interim compliance dates,

with prior

approval of the Agency.

BOARD NOTE:

“*“

indicates that prior Agency approval

is required.

3

b.

Extension of final compliance date.

1*

6.

Changes in expiration date of permit to allow earlier permit

termination, with prior approval of the Agency.

1*

7.

Changes in ownership or operational control of a facility,

provided the procedures of Section 703.260(b) are followed.

B.

General Facility Standards

1.

Changes to waste sampling or analysis methods:

1

a.

To conform with Agency guidance or Board regulations.

.1

b.

To incorporate chances associated with F039

(multi—

source leachate) sampling or analysis methods.

2

~.

Other changes.

2.

Changes to analytical quality assurance/control plan:

117—33 1

---

12

1

a.

To

conform

with

agency

guidance

or

regulations.

2

b.

Other changes.

1

3.

Changes in procedures for maintaining the operating record.

2

4.

Changes in frequency or content of inspection schedules.

5.

Changes

in the training plan:

2

a.

That affect the

type

or decrease the amount of

training given to employees.

1

b.

Other changes.

6.

Contingency plan:

2

a.

Changes in emergency procedures

(i.e.,

spill or

release response procedures).

1

b.

Replacement with functionally equivalent equipment,

upgrade or relocate emergency equipment listed.

2

c.

Removal of equipment from emergency equipment list.

1

d.

Changes

in name,

address or phone number of

coordinators or other persons or agencies identified

in the plan.

Note:

When a permit modification (such as

introduction of a new unit) requires a change in

facility plans or other general facility standards,

that change must be reviewed under the same procedures

as the permit modification.

C.

Groundwater Protection

1.

Changes to wells:

2

a.

Changes in the number,

location,

depth or design of

upgradient or downgradient wells of permitted

groundwater monitoring system.

1

b.

Replacement of an existing well that has been damaged

or

rendered

inoperable,

without

change

to

location,

design or depth of the well.

1*

2.

Changes in groundwater sampling or analysis procedures or

monitoring schedule, with prior approval of the Agency.

1*

3.

Changes in statistical procedure for determining whether a

statistically significant change in groundwater quality

117—332

---

13

between upgradient and downgradient wells has occurred,

with

prior approval of the Agency.

2*

4.

Changes in point of compliance.

5.

Changes in indicator parameters, hazardous constituents or

concentration limits

(including ACLa

(Alternate

Concentration Limits)):

3

a.

As specified in the groundwater protection standard.

2

b.

As specified in the detection monitoring program.

2

6.

Changes to

a detection monitoring program as required by 35

Ill.

Adm. Code 724.198(j), unless otherwise specified in

this Appendix.

7.

Compliance monitoring program:

3

a.

Addition of compliance monitoring program as

required

by 35

Ill. Adm.

Code 724.198(h)(4)

and 724.199.

b.

Changes to a compliance monitoring program as required

by 35

Ill.

Adni.

Code 724.199(k), unless otherwise

specified in this Appendix.

B.

Corrective action program:

3

a.

Addition of

a corrective action program as required by

35

Ill.

Adm.

Code

724.199(i)

(2)

and

724.200.

2

b.

Changes

to

a

corrective

action

program

as

required

by

35

Ill.

Adm.

Code

724.200(h),

unless

otherwise

specified

in

this

Appendix.

D.

Closure

1.

Changes

to

the

closure

plan:

1*

a.

Changes

in

estimate

of

maximum

extent

of

operations

or

maximum

inventory

of

waste

on—site

at

any

time

during

the

active

life

of

the

facility,

with

prior

approval

of

the

Agency.

1*

b.

Changes

in

the

closure

schedule

for

any

unit,

changes

in

the

final closure schedule for the facility or

extension

of

the

closure

period,

with

prior

approval

of

the

Agency.

1*

c.

Changes

in

the

expected

year

of

final

closure,

where

other

permit

conditions

are

not

changed,

with

prior

approval

of

the

Agency.

117—33 3

---

14

1*

d.

Changes

in

procedures

for

decontamination

of

facility

equipment

or

structures,

with

prior

approval

of

the

Agency.

2

e.

Changes

in

approved

closure

plan

resulting

from

unexpected

events

occurring

during

partial

or

final

closure,

unless

otherwise

specified

in

this

Appendix.

2

f.

Extension

of

the

closure

period

to

allow

a

landfill,

surface

impoundment

or

land

treatment

unit

to

receive

non—hazardous

wastes

after

final

receipt

of

hazardous

wastes

under

35

Ill.

Mm.

Code

724.213(d)

or

(e)..

3

2.

Creation

of

a

new

landfill

unit

as

part

of

closure.

3.

Addition

of

the

following

new

units

to

be

used

temporarily

for

closure

activities:

3

a.

Surface

impoundments.

3

b.

Incinerators.

3

c.

Waste

piles

that

do

not

comply

with

35

Ill.

Adin.

Code

724.350(c).

2

d.

Waste

piles

that

comply

with

35

Ill.

Adni.

Code

724.350(c).

2

e.

Tanks

or

containers

(other

than

specified

below).

1*

f.

Tanks

used

for

neutralization,

dewatering,

phase

separation

or

component

separation,

with

prior

approval

of

the

Agency.

E.

Post—Closure

1

1.

Changes

in

name,

address

or

phone

number

of

contact

in

post—

closure

plan.

2

2.

Extension

of

post—closure care period.

3

3.

Reduction

in

the

post—closure

care

period.

1

4.

Changes

to

the

expected

year

of

final

closure,

where

other

permit

conditions

are

not

changed.

2

5.

Changes

in

post—closure plan necessitated by eventB

occurring during the active life of the facility,

including

partial and final closure.

F.

Containers

117—334

---

15

1.

Modification

or

addition

of

container

units:

3

a.

Resulting in greater than 25

increase in the

facility’s container storage capacity, except as

provided in F(l)(c)

and F(4)(a).

2

b.

Resulting in up to 25

increase

in the facility’s

container storage capacity,

except as provided in

F(1)(c) and F(4)(a).

c.

Or treatment processes necessary to treat wastes that

are

restricted

from

land

disposal

to

meet

some

or

all

of

the

applicable

treatment

standards

or

to

treat

wastes

to

satisfy

(in

whole

or

in

part)

the

standard

of

“use

of

practically

available

technology

that

yields

the

greatest

environmental

benefit”

contained

in

40

CFR

268.8(a)(2)(ii),

incorporated by reference

in

35

Ill.

Adm.

Code

728.108,

with

prior

approval

of

the

Agency.

This

modification

may

also

involve

the

addition

of

new

waste

codes

or

narrative

description

of

wastes.

It

is

not

applicable

to

dioxin—containing

wastes

(FO2O,

F021,

F022,

F023,

F026,

F027

and

F028).

2.

2

a.

Modification

of

a

container

unit

without

increasing

the

capacity

of

the

unit.

b.

Addition

of

a

roof

to

a

container

unit

without

alteration

of

the

containment

system.

3.

Storage

of

different

wastes

in

containers,

except

as

provided

in

F(4):

3

a.

That

require

additional

or

different

management

practices

from

those

authorized

in

the

permit.

2

b.

That

do

not

require

additional

or

different

management

practices

from

those

authorized

in

the

permit.

Note:

See

Section

703.280(g)

for

modification

procedures

to

be

used

for

the

management

of

newly

listed

or

identified

wastes.

4.

Storage

or

treatment

of

different

wastes

in

containers:

2

a.

That require addition of units or change in treatment

process or management standards, provided that the

wastes are restricted from land disposal and are to be

treated to meet some or all of the applicable

treatment

standards,

or

are

to

be

treated

to

satisfy

117—335

---

16

(in whole or

in part)

the standard of “use of

practically available technology that yields the

greatest environmental benefit” contained in 40 CFR

268.8(a)(2)(ii),

incorporated by reference in 35 Ill.

Adm.

Code

728.108.

It

is

not

applicable

to

dioxin—

containing wastes

(F020,

F021,

F022, F023,

F026, F027

and F028).

b.

That do not require the addition of units or a change

in the treatment process or management Btandards, and

provided

that

the

units

have

previously

received

wastes of the same type (e.g., incinerator scrubber

water).

This modification is not applicable to

dioxin—containing

wastes

(F020,

F021,

F022,

F023,

F026, F027 and F028).

S.

Tanks

1.

3

a.

Modification or addition of tank units resulting in

greater than 25

increase in the facility’s tank

capacity,

except as provided in paragraphs G(1)(c),

G(1)(d)

and G(1)(e).

2

b.

Modification or addition of tank units resulting in up

to 25

increase in the facility’s tank capacity,

except as provided in paragraphs G(1)(d)

and G(1)(e).

2

c.

Addition of a new tank that will operate for more than

90 days using any of the following physical or

chemical treatment technologies:

neutralization,

dewatering,

phase separation or component separation.

1*

d.

After prior approval of the Agency,

addition of a new

tank that will operate for up to 90 days using any of

the following physical or chemical treatment

technologies:

neutralization, dewatering, phase

separation or component separation.

e.

Modification or addition of tank units or treatment

processes that are necessary to treat wastes that are

restricted from land disposal to meet some or all of

the applicable treatment standards or to treat wastes

to satisfy (in whole or in part)

the standard of “use

of practically available technology that yields the

greatest environmental benefit” contained in 40 CFR

268.8(a)(2)(ii),

incorporated by reference in 35

111.

Adm. Code 728.108, with prior approval of the Agency.

This modification may also involve the addition of new

waste codes.

It is not applicable to dioxin-

117—3 36

---

17

containing wastes (F020,

F021,

F022,

F023,

F026, F027

and F028).

2

2.

Modification of a tank unit or secondary containment system

without increasing the capacity of the unit.

3.

Replacement of a tank with

a tank that meets the same design

standards and has a capacity within

+1-

10

of the replaced

tank provided:

a.

The capacity difference is no more than 1500 gallons,

b.

The facility’s permitted tank capacity is not

increased and

c.

The replacement tank meets the same conditions in the

permit.

2

4.

Modification of

a tank management practice.

5.

Management of different wastes in tanks:

3

a.

That require additional or different management

practices, tank design,

different fire protection

specifications or significantly different tank

treatment process from that authorized in the permit,

except as provided in paragraph G(5)(c).

2

b.

That do not require additional or different management

practices,

tank design, different fire protection

specification or significantly different tank

treatment process than authorized in the permit,

except as provided in paragraph G(5)(d).

Note:

See Section 703.280(g)

for modification

procedures to be used for the management of newly

listed or identified wastes.

c.

That require addition of units or change in treatment

processes or management standards, provided that the

wastes are restricted from land disposal and are to be

treated to meet some or all of the applicable

treatment standards,

or that are to be treated to

satisfy (in whole or in part) the standard of “use of

practically available technology that yields the

greatest environmental benefit” contained in 40 CFR

268.8(a)(2)(ii), incorporated by reference in

35

Ill.

Adm. Code 728.108.

The modification

is not applicable

to dioxin—containing wastes

(F020,

F021, F022,

F023,

F026,

F027 and F028).

117— 33 7

---

18

d.

That do not require the addition of units or a change

in the treatment process or management standards,

and

provided that the units have previously received

wastes of the same type (e.g.,

incinerator scrubber

water).

This modification is not applicable to

dioxin—containing wastes (F020,

F021, P022,

P023,

F026,

F027 and P028).

H.

Surface Impoundments

3

1.

Modification or addition of surface impoundment units that

result in increasing the facility’s surface impoundment

storage or treatment capacity.

3

2.

Replacement of a surface impoundment unit.

2

3.

Modification of a surface impoundment unit without

increasing the facility’s surface impoundment storage or

treatment capacity and without modifying the unit’s liner,

leak detection system or leachate collection system.

2

4.

Modification of a surface impoundment management practice.

5.

Treatment,

storage or disposal of different wastes in

surface impoundments:

3

a.

That require additional or different management

practices or different design of the liner or leak

detection system than authorized in the permit.

2

b.

That do not require additional or different management

practices or different design of the liner or leak

detection system than authorized in the permit.

Note:

See Section 703.280(g)

for modification

procedures to be used for the management of newly

listed or identified wastes.

c.

That are wastes restricted from land disposal that

meet the applicable treatment standards or that are

treated to satisfy the standard of “use of practically

available technology that yields the greatest

environmental benefit” contained in 40 CFR

268.8(a)(2)(ii), incorporated by reference

in

35

Ill.

Adm.

Code 728.108,

and provided that the unit meets

the minimum technological reguirements stated in 40

CFR 268.5(h)(2),

incorporated by reference in

35

Ill.

Adm.

Code 728.105.

This modification is not

applicable to dioxin—containing wastes

(F020, F021,

F022, F023, P026,

F027 and F028).

117—338

---

19

d.

That

are

residues from wastewater treatment or

incineration,

provided the disposal occurs in a unit

that meets the minimum technological reguirements

stated in 40 CFR 268.5(h)(2),

incorporated by

reference in 35

Ill.

Adni. Code 728.105,

and provided

further that the surface

impoundment has previously

received wastes of the same type (for example,

incinerator scrubber water).

This modification is not

applicable to dioxin-containing wastes (F020, F02l,

F022,

F023,

F026,

F027 and P028).

I.

Enclosed Waste Piles.

For all waste piles, except those complying

with 35

Ill.

Adm.

Code 724.350(c), modifications are treated the

same as for a landfill.

The following modifications are

applicable only to waste piles complying with 35 Ill. Adm. Code

724.350(c).

1.

Modification or addition of waste pile units:

3

a.

Resulting in greater than 25

increase in the

facility’s waste pile storage or treatment capacity.

2

b.

Resulting in up to 25

increase in the facility’s

waste pile storage or treatment capacity.

2

2.

Modification of waste pile unit without increasing the

capacity of the unit.

3.

Replacement of

a waste pile unit with another waste pile

unit of the same design and capacity and meeting all waste

pile conditions in the permit.

2

4.

Modification of a waste pile management practice.

5.

Storage or treatment of different wastes in waste piles:

3

a.

That require additional or different management

practices or different design of the unit.

2

b.

That do not require additional or different management

practices or different design of the unit.

Note:

See Section 703.280(g)

for modification

procedures to be used for the management of newly

listed or identified wastes.

J.

Landfills and Unenclosed Waste Piles

3

1.

Modification or addition of landfill units that result in

increasing the facility’s disposal capacity.

3

2.

Replacement of a landfill.

117—339

---

20

3

3.

Addition or modification of a liner,

leachate collection

system,

leachate detection system,

run—off control or final

cover system.

2

4.

Modification of

a landfill unit without changing

a liner,

leachate collection system,

leachate detection system, run—

off control or final cover system.

2

5.

Modification of

a landfill management practice.

6.

Landfill

different

wastes:

3

a.

That

require additional or different management

practices,

different

design of the liner,

leachate

collection

system

or

leachate

detection system.

2

b.

That

do

not

require

additional

or

different

management

practices, different design of the liner,

leachate

collection

system

or

leachate

detection

system.

Note:

See

Section 703.280(g)

for modification

procedures

to

be

used

for

the management of newly

listed

or

identified

wastes.

c.

That

are wastes restricted from land disposal that

meet

the

applicable

treatment

standards

or

that

are

treated

to

satisfy

the

standard

of

“use

of

practically

available technology that yields the greatest

environmental benefit” contained in 40 CFR

268.8(a)(2)(ii),

incorporated by reference in 35 Ill.

Adm. Code 728.108,

and provided that the

landfill unit

meets the minimum technological reguirements stated in

40 CFR 268.5(h)(2),

incorporated by reference in 35

Ill. Adm.

Code 728.105.

This modification is not

applicable to dioxin—containing wastes

(F020, P021,

F022, F023, F026,

F027 and F028).

d.

That are residues from wastewater treatment or

incineration,

provided the disposal occurs in a

landfill unit that meets the minimum technological

reguirements stated in 40 CFR 268.5(h) (2),

incorporated by reference in

35

Ill.

Adm. Code

728.105,

and provided further that the landfill has

previously received wastes

of the same type

(for

example,

incinerator ash).

This modification

is not

applicable to dioxin—containing wastes (F020, P021,

F022,

P023,

P026, F027

and F028).

K.

Land Treatment

117—340

---

21

3

1.

Lateral expansion of or other modification of

a land

treatment unit to increase area extent.

2

2.

Modification of run—on control system.

3

3.

Modify run-off control system.

2

4.

Other modification

of land treatment unit component

specifications or standards required in permit.

5.

Management of different wastes in land treatment units:

3

a.

That

require

a

change

in

permit

operating

conditions

or

unit

design

specifications.

2

b.

That

do

not

require

a

change

in

permit

operating

conditions

or

unit

design

specifications.

Note:

See

Section

703.280(g)

for

modification

procedures

to

be

used for the management of newly

listed

or

identified

wastes.

6.

Modification

of

a

land

treatment

unit

management

practice

to:

3

a.

Increase

rate

or

change

method

of

waste

application.

1

b.

Decrease

rate

of

waste

application.

2

7.

Modification

of

a

land

treatment

unit

management

practice

to

change

measures

of

pH

or

moisture

content

or

to

enhance

microbial

or

chemical

reactions.

3

8.

Modification

of

a

land

treatment

unit

management

practice

to

grow

food

chain

crops,

to

add

to

or

replace

existing

permitted

crops

with

different

food

chain

crops

or

to

modify

operating

plans

for

distribution

of

animal

feeds

resulting

from such crops.

3

9.

Modification of operating practice due to detection of

releases from the land treatment unit pursuant to 35 Ill.

Adm. Code 724.378(g) (2).

3

10.

Changes in the unsaturated zone monitoring system resulting

in a change to the location,

depth, number of sampling

points

or replace unsaturated zone monitoring devices or

components of devices with devices or components that have

specifications different from permit requirements.

2

11.

Changes in the unsaturated zone monitoring system that do

not result

in a change to the location, depth,

number of

sampling points, or that replace unsaturated zone monitoring

117— 34

1

---

22

devices or components of devices with devices or components

having specifications different from permit requirements.

2

12.

Changes in background values for hazardous constituents in

soil

and

Boil-pore

liquid.

2

13.

Changes in sampling,

analysis or statistical procedure.

2

14.

Changes

in

land

treatment

demonstration

program

prior

to

or

during the demonstration.

1*

15.

Changes in any condition specified in the permit for

a land

treatment unit to reflect results of the land treatment

demonstration, provided performance standards are met,

and

the Agency’s prior approval has been received.

1*

16.

Changes to allow

a second land treatment demonstration to be

conducted when the results of the first demonstration have

not shown the conditions under which the wastes can be

treated completely, provided the conditions

for the second

demonstration are substantially the same as the conditions

for the first demonstration and have received the prior

approval of the Agency.

3

17.

Changes to allow a second land treatment demonstration to be

conducted when the results of the first demonstration have

not shown the conditions under which the wastes can be

treated completely, where the conditions for the second

demonstration are not substantially the same as the

conditions for the first demonstration.

2

18.

Changes

in vegetative cover requirements for closure.

L.

Incinerators

3

1.

Changes to increase by more than 25

any of the following

limits authorized in the permit: A thermal feed rate limit,

a waste feed rate limit or an organic chlorine feed rate

limit.

The Agency shall require a new trial burn to

substantiate compliance with the regulatory performance

standards unless this demonstration can be made through

other means.

2

2.

Changes to increase by up to 25

any of the following limits

authorized in the permit:

A thermal feed rate limit,

a waste

feed limit or an organic chlorine feed rate limit.

The

Agency shall require a new trial burn to substantiate

compliance with the regulatory performance standards unless

this demonstration can be made through other means.

3

3.

Modification of an incinerator unit by changing the internal

size or geometry of the primary or secondary combustion

117—342

---

23

units,

by adding

a primary or secondary combustion unit,

by

substantially changing the design of any component used to

remove HC1 or particulates from the combustion gases or by

changing other features of the incinerator that could affect

its capability to meet the regulatory performance standards.

The Agency shall require a new trial burn to substantiate

compliance with the regulatory performance standards,

unless

this demonstration can be made through other means.

2

4.

Modification of an incinerator unit in a manner that will

not

likely

affect

the

capability

of

the

unit

to

meet

the

regulatory performance standards but which will change the

operating conditions or monitoring requirements specified in

the permit.

The Agency may require a new trial burn to

demonstrate compliance with the regulatory performance

standards.

5.

Operating requirements:

3

a.

Modification of the limits specified in the permit for

minimum combustion gas temperature, minimum combustion

gas residence time or oxygen concentration in the

secondary combustion chamber.

The Agency shall

require a new trial burn to substantiate compliance

with the regulatory performance standards unless this

demonstration can be made through other means.

3

b.

Modification of any stack gas emission limitB

specified

in

the

permit,

or

modification

of

any

conditions in the permit concerning emergency shutdown

or automatic waste feed cutoff procedures or controls.

2

c.

Modification of any other operating condition or any

inspection or recordkeeping requirement specified in

the permit.

6.

Incineration of different wastes:

3

a.

If the waste contains

a POHC that is more difficult to

incinerate than authorized by the permit or

if

incineration of the waste requires compliance with

different regulatory performance standards than

specified

in the permit.,

the Agency shall require a

new trial burn to substantiate compliance with the

regulatory performance standards,

unless this

demonstration can be made through other means.

b.

If the waste does

not

contain

a

POHC that

is more

difficult to incinerate than authorized by the permit

and

if

incineration

of

the

waste

does

not

require

compliance

with

different

regulatory

performance

standards than specified in the permit.

117—34 3

---

24

BOARD NOTE:

See Section 703.280(g)

for modification

procedures to be used for the management of newly

listed

or

identified

wastes.

7.

Shakedown and trial burn:

2

a.

Modification of the trial burn plan or any of the

permit conditions applicable during the shakedown

period for determining operational readiness after

construction,

the trial burn period or the period

immediately following the trial burn.

1*

b.

Authorization of up to an additional 720 hours of

waste incineration during the shakedown period for

determining operational readiness after construction,

with the prior approval of the Agency.

1*

c.

Changes

in the operating requirements set in the

permit for conducting a trial burn,

provided the

change

is minor and has received the prior approval of

the Agency.

1*

d.

Changes

in

the

ranges

of

the

operating

requirements

set

in

the

permit

to

reflect

the results of the trial

burn,

provided the change

is minor and has received

the prior approval of the Agency.

8.

Substitution of an alternate type of fuel that

is not

specified in the permit.

BOARD NOTE:

Derived from 40 CFR 270.42, Appendix

I,

se

adopted

at

Z3 Fed.

Itcg.

37934, Ccptember

28,

1088

(1990).

(Source:

Amended

at

15

Ill.

Reg.

,

effective

)

117— 344

---

25

TITLE

35:

ENVIRONMENTAL

PROTECTION

SUBTITLE G:

WASTE DISPOSAL

CHAPTER

I:

POLLUTION CONTROL BOARD

SUBCHAPTER

c:

HAZARDOUS WASTE OPERATING REQUIREMENTS

PART 720

HAZARDOUS

WASTE

MANAGEMENT

SYSTEM:

GENERAL

SUBPART A:

GENERAL PROVISIONS

Section

720.101

Purpose,

Scope and Applicability

720.102

Availability of Information; Confidentiality of Information

720.103

Use of Number and Gender

SUBPART B:

DEFINITIONS

Section

720.110

Definitions

720.111

References

SUBPART C:

RULEMAKING PETITIONS AND OTHER PROCEDURES

Section

720.120

Rulemaking

720.121

Alternative Equivalent Testing Methods

720.122

Waste Delisting

720.130

Procedures for Solid Waste Determinations

720.131

Solid Waste Determinations

720.132

Boiler

Determinations

720.133

Procedures for Determinations

720.140

Additional

regulation

of

certain

hazardous

waste

Recycling

Activities on

a case—by—case Basis

720.141

Procedures for case—by—case regulation of hazardous waste

Recycling

Activities

Appendix A

Overview of

40

CFR,

Subtitle

C

Regulations

AUTHORITY:

Implementing Section 22.4 and authorized by Section 27 of

the

Environmental Protection Act

(Ill.

Rev.

Stat. 1989,

ch. 111

1/2,

pars.

1022.4

and 1027).

SOURCE:

Adopted

in R81—22,

43 PCB 427,

at 5 Ill. Reg.

9781,

effective as

noted

in 35 Ill.

Adm. Code 700.106;

amended and codified in R81—22, 45 PCB

317,

at

6 Ill. Reg.

4828, effective as noted in 35 Ill.

Adin.

Code 700.106;

amended

in R82—l9 at 7

Ill. Reg.

14015, effective Oct.

12, 1983;

amended in

R84-9,

53 PCB

131 at 9 Ill. Reg. 11819, effective July 24,

1985;

amended in

R85-22 at 10

Ill. Reg.

968, effective January

2,

1986;

amended in R86-1 at 10

Ill.

Reg.

13998, effective August

12,

1986;

amended in R86—19 at 10 Ill. Reg.

20630, effective December

2,

1986; amended in R86—28 at 11

Ill. Reg. 6017,

effective March 24, 1987;

amended in R86—46 at 11

Ill. Reg.

13435, effective

August

4,

1987;

amended in R87—5 at

11

Ill.

Reg. 19280,

effective November 12,

1987;

amended in R87—26 at

12 Ill.

Reg.

2450, effective January 15,

1988;

amended in R87—39 at

12

Ill.

Reg.

12999, effective July 29,

1988; amended in

R88-l6 at

13

Ill.

Reg.

362, effective December 27,

1988;

amended in R89—1 at

117—345

---

26

13

Ill.

Reg. 18278, effective November 13,

1989;

amended in R89—2 at

14 Ill.

Reg.

3075,

effective February 20,

1990;

amended in R89—9

at

14

Ill.

Reg.

6225,

effective April

16,

1990;

amended

in R90—10 at

14 Ill. Reg.

,

effective

September 25,

1990;

amended in R90—17 at

14

Ill. Reg.

,

effective

; amended in R90—ll at

15 Ill.

Reg.

,

effective

SUBPART B:

DEFINITIONS

Section 720.111

References

a)

The following publications are incorporated by reference:

ANSI.

Available from the American National Standards

Institute,

1430 Broadway,

New York, New York

10018,

(212)

354—3300:

ANSI

B31.3 and B31.4.

See

ASME/ANSI

B3l.3 and B31.4

API.

Available from the American Petroleum Institute,

1220

L Street, N.W., Washington,

D.C.

20005,

(202)

682—8000:

“Guide

for

Inspection

of

Refinery

Equipment, Chapter

XIII,

Atmospheric

and

Low

Pressure

Storage Tanks,” 4th

Edition,

1981,

reaffirmed December,

1987.

“Cathodic Protection of

Underground

Petroleum

Storage

Tanks and Piping Systems,” API Recommended Practice

1632, Second Edition, December,

1987.

“Installation of Underground Petroleum Storage

Systems,” API Recommended Practice 1615,

Fourth

Edition, November,

1987.

APTI.

Available from the Air and Waste Management

Association, Box 2861,

Pittsburg, PA

15230,

(412)

232—

3444:

APTI Course 415:

Control of Gaseous Emissions, EPA

Publication EPA—450/2—81—005, December,

1981.

ASME.

Available

from

the American Society of Mechanical

Engineers,

345 East 47th Street, New York, NY

10017,

(212)

705—7722:

“Chemical Plant and Petroleum Refinery Piping”,

ASME/ANSI

B3l.3—1987,

as supplemented by B31.3a—1988

and B31.3b—1988.

Also available from ANSI.

“Liquid Transportation Systems for Hydrocarbons,

Liquid Petroleum Gas, Anhydrous Ammonia,

and

117—346

---

27

Alcohols”, ASME/ANSI B31.4—1986,

as supplemented by

B31.4a—1987.

Also available from ANSI.

ASTM.

Available from American Society for Testing and

Materials,

1916 Race Street,

Philadelphia, PA 19103,

(215)

299—5400:

ACTII Standard Test Methods

for

Flash roint of

Liqui

Cetafla3h Closed Tester,”

ACTM

Standard

D

3828

87

ASTM D93-85.”ACTM Standard Test Methods for Flash

Point ~yPensky—Martens

Closed Tester,” ACTM Standard

D 03

70 or

D 03 80approved October 25,

1985.

ASTM D1946—90,

Standard Practice for Analysis of

Reformed Gas by Gas Chromatography, Approved March 30,

1990.

ASTM D2267—88,

Standard Test Method for Aromatics in

Light Naphthas and Aviation Gasolines by Gas

Chromatography,

approved November 17.

1988.

ASTM D2382-88,

Standard Test Method for Heat of

Combustion of Hydrocarbon Fuels by Bomb Calorimeter

(High Precision Method), approved October 31,

1988.

ASTM D2879-86,

Standard

Test

Method for Vapor

Pressure-Temperature Relationship and Initial

Decomposition Temperature

of Liquids by Isoteniscope,

approved October 31,

1986.

ASTM D3828-87,

Standard Test Methods for Flash Point

of Liquids by Setaflash Closed Tester,

approved

December

14,

1988.

ASTM El68-88,

Standard Practices

for General

Techniques of Infrared Quantitative Analysis,

approved

May 27,

1988.

ASTM E169—87,

Standard Practices for General

Techniques of Ultraviolet—Visible Ouantitative

Analysis,

approved February

1,

1987.

ASTM E260—85,

Standard Practice for Packed Column Gas

Chromatography, approved June 28,

1985.

GPO.

Available from the Superintendent of Documents, U.S.

Government Printing Office,

Washington,

D.C.

20401,

(202)

783—3238:

Standard Industrial Classification Manual

(1972),

and

1977 Supplement, republished in 1983

117—34 7

---

28

NACE.

Available from the National Association of Corrosion

Engineers,

1400 South Creek Dr., Houston,

TX

77084,

(713)

492—0535:

“Control of External Corrosion on Metallic Buried,

Partially Buried,

or Submerged Liquid Storage

Systems”, NACE Recommended Practice RP0285-85,

approved March,

1985.

NFPA.

Available from the National Fire Protection

Association, Batterymarch Park, Boston, MA

02269,

(617)

770—3000 or

(800)

344—3555:

“Flammable and Combustible Liquids Code” NFPA 30,

issued July 17,

1987.

Also available from ANSI.

NTIS.

Available from the National Technical Information

Service,

5285 Port Royal Road,

Springfield, VA

22161,

(703)

487—4600:

“Generic Quality Assurance Project Plan for Land

Disposal Restrictjons Program”, EPA/530—SW—87—011,

March

15,

1987.

(Document

number

PB

88—170766.j

“Methods for Chemical Analysis of Water and Wastes”,

Third Edition, March,

1983.

(Document number PB 84—

128677)

“Petitions to Delist Hazardous Wastes

——

A Guidance

Manual”,

EPA/530—SW—85—003,

April,

1985.

(Document

Number PB 85—194488

“Procedures Manual for Ground Water Monitoring at

Solid Waste Disposal Facilities”, EPA—530/SW—6ll,

1977.

(Document number PB 84—174820)

“Test Methods for Evaluating Solid Waste,

Physical/Chemical Methods,” EPA Publication number SW-

846 (Second Edition, 1982 as amended by Update

I

(April,

1984)

and Update

II

(April,

1985))

(Document

number PB 87-120291)

STI.

Available from the Steel Tank Institute, 728 Anthony

Trail, Northbrook,

IL

60062,

(312)

498—1980:

“Standard for Dual Wall Underground Steel Storage

Tanks”

(1986).

USEPA.

Available from United States Environmental

Protection Agency,

Office of Drinking Water,

State Programs

Division,

WH 550

E, Washington,

D.C.

20460:

117—348

---

29

“Technical Assistance Document:

Corrosion,

Its

Detection and Control

in Injection Wells”,

EPA 570/9-

87—002, August,

1987.

b)

Code of

Federal Regulations.

Available from the Superintendent of

Documents,

U.S. Government Printing Office, Washington,

D.C.

20401,

(202)

783—3238:

10 CFR 20, Appendix B ~1089)(19901

40 CFR 60

(1990)

40 CFR 61, Subpart V

(19901

40 CFR 136 (1080)(1990)

40 CFR 142

(1989)(l990)

40 CFR 220

(1080)119901

40 CFR 260.20 (1989)11990)

40 CFR 264

.(l989) (1990)

40 CFR 302.4,

302.5 and 302.6 (1989)(1990)

40 CFR 761

(1089)(19901

C)

Federal Statutes

Section 3004 of the Resource Conservation and Recovery Act

(42

U.S.C.

6901 et seq.),

as amended through December 31,

1987.

d)

This Section incorporates no later editions or amendments.

(Source:

Amended at

15

Ill. Reg.

,

effective

117—349

---

30

TITLE 35:

ENVIRONMENTAL PROTECTION

SUBTITLE G:

WASTE DISPOSAL

CHAPTER

I:

POLLUTION CONTROL

BOARD

SUBCHAPTER

C:

HAZARDOUS

WASTE

OPERATING

REQUIREMENTS

PART

721

IDENTIFICATION AND LISTING OF

HAZARDOUS

WASTE

SUBPART A:

GENERAL

PROVISIONS

Purpose of Scope

Definition of Solid Waste

Definition of Hazardous Waste

Exclusions

Special Requirements for Hazardous Waste Generated by Small

Quantity Generators

Requirements for Recyclable Materials

Residues of Hazardous Waste in Empty Containers

PCB Wastes Regulated under TSCA

SUPBART

B:

CRITERIA FOR IDENTIFYING

THE CHARACTERISTICS

OF

HAZARDOUS

WASTE AND FOR LISTING HAZARDOUS WASTES

Criteria for Identifying the Characteristics of Hazardous Waste

Criteria for Listing Hazardous Waste

SUBPART C:

CHARACTERISTICS OF HAZARDOUS WASTE

SUBPART

D:

LISTS OF

HAZARDOUS

WASTE

General

Hazardous Wastes From Nonspecific Sources

Hazardous Waste from Specific Sources

Discarded Commercial Chemical Products, Off—Specification Species,

Container Residues and Spill Residues Thereof

Appendix A

Appendix B

Appendix C

Table A

Table B

Table

C

Appendix G

Appendix

H

Appendix

I

Table

A

Representative Sampling Methods

Method 1311 Toxicity Characteristic Leaching Procedure (TCLP)

Chemical Analysis Test Methods

Analytical Characteristics of Organic Chemicals

(Repealed)

Analytical Characteristics of Inorganic Species

(Repealed)

Sample Preparation/Sample Introduction Techniques

(Repealed)

Basis for Listing Hazardous Wastes

Hazardous Constituents

Wastes Excluded under Section 720.120 and 720.122

Wastes Excluded from Non—Specific Sources

Sect ion

721. 101

721.102

721.103

721.104

721. 105

721. 106

721. 107

721.108

Section

721.110

721.111

Section

721. 120

721.121

721. 122

721.123

721.

124

Section

721.130

721.131

721.132

721.133

General

Characteristic of Ignitability

Characteristic of Corrosivity

Characteristic of Reactivity

Toxicity Characteristic

117—350

---

31

Table

B

Wastes Excluded from Specific Sources

Table C

Wastes Excluded From Commercial Chemical Products,

Off—

Specification Species,

Container Residues,

and Soil Residues

Thereof

Appendix

J

Method of Analysis for Chlorinated Dibenzo—p—Dioxins and

Dibenzofurans

Appendix

Z

Table to Section 721.102

AUTHORITY:

Implementing Section 22.4 and authorized by Section 27 of the

Environmental Protection Act

(Ill.

Rev. Stat.

1989,

ch.

111 1/2, pars.

1022.4

and 1027).

SOURCE:

Adopted in R81—22, 43 PCB 427, at

5 Ill. Reg. 9781,

effective as

noted

in

35

Ill.

Mm.

Code

700.106; amended and codified in R81—22,

45 PCB

317,

at

6

Ill.

Reg.

4828,

effective

as

noted

in

35

Ill.

Mrs.

Code

700.106;

amended

in R82—18,

51 PCB 31, at

7

Ill. Reg. 2518,

effective February 22,

1983;

amended

in

R82—19,

53

PCB

131,

at

7

Ill.

Reg.

13999,

effective

October

12,

1983; amended in R84—34,

61 PCB 247, at

8 Ill.

Reg.

24562, effective

December

11,

1984;

amended

in

R84—9,

at

9

Ill.

Reg.

11834,

effective

July

24,

1985;

amended

in

R85—22

at

10

Ill.

Reg.

998,

effective

January

2,

1986;

amended

in R85—2 at 10 Ill. Reg. 8112,

effective May 2, 1986;

amended in R86—

1 at

10 Ill.

Reg.

14002, effective August

12,

1986;

amended in R86—19 at 10

Ill.

Reg. 20647, effective December

2,

1986;

amended in R86—28 at

11

Ill.

Reg.

6035,

effective March 24,

1987;

amended in R86—46 at 11 111. Reg.

13466,

effective

August

4,

1987;

amended

in

R87—32

at

11

Ill.

Reg.

16698,

effective

September 30,

1987; amended in R87—5 at

11 Ill. Reg. 19303,

effective November

12,

1987; amended in R87—26 at 12

Ill.

Reg.

2456, effective January

15, 1988;

amended

in R87—30

at

12

Ill.

Reg. 12070,

effective July 12,

1988;

amended in

R87—39 at

12

Ill.

Reg.

13006, effective July 29,

1988; amended in R88—l6 at

13

Ill. Reg.

382, effective December 27,

1988;

amended in R89—.

at 13

Ill. Reg.

18300, effective November 13,

1989;

amended in R90—2 at 14 Ill. Reg.

14401,

effective August 22,

1990;

amended in R90—10 at 14 Ill. Reg.

16472, effective

September 25,

1990;

amended in R90—17 at 14

Ill. Reg.

,

effective

amended in R90—11 at

15

Ill. Reg.

,

effective

SUBPART

A:

GENERAL PROVISIONS

Section 721.104

Exclusions

a)

Materials which are not solid wastes.

The following materials are

not solid wastes for the purpose of this Part:

1)

Sewage:

A)

Domestic sewage; and

B)

Any mixture of domestic sewage and other waste that

passes through

a sewer system to publicly—owned

treatment works for treatment.

“Domestic sewage”

means untreated sanitary wastes that pass through a

sewer

system.

117—35 1

---

32

2)

Industrial wastewater discharges that are point source

discharges with NPDES permits issued by the Agency pursuant

to Section 12(f)

of the Environmental Protection Act and 35

Ill.

Adm.

Code 309.

BOARD

NOTE:

This exclusion applies only to the actual

point

source discharge.

It does not exclude industrial

wastewaters while they are

being

collected,

stored or

treated before discharge, nor does it exclude sludges that

are generated by industrial wastewater treatment.

3)

Irrigation return flows.

4)

Source,

special nuclear or by—product material as defined by

the Atomic Energy Act of

1954, as amended

(42 U.S.C. 2011 et

seq.)

5)

Materials subjected to in—situ mining techniques which are

not removed from the ground as part of the extraction

process.

6)

Pulping liquors

(i.e., black liquor) that are reclaimed in a

pulping liquor recovery furnace and then reused

in the

pulping process,

unless accumulated speculatively as defined

in Section 721.101(c);

7)

Spent sulfuric acid used to produce virgin sulfuric acid,

unless

it

is accumulated speculatively as defined in Section

721.101(c).

8)

Secondary materials that are reclaimed and returned to the

original process or processes in which they were generated

where they are reused in the production process,

provided:

A)

Only tank storage is involved,

and the entire process

through completion of reclamation is closed by being

entirely connected with pipes or other comparable

enclosed means of conveyance;

B)

Reclamation does not involve controlled flame

combustion (such as occurs in boilers,

industrial

furnaces or incinerators);

C)

The Becondary materials are never accumulated in auch

tanks for over twelve months without being reclaimed;

and

D)

The reclaimed material

is not used to produce a fuel,

or used to produce products that are used in a manner

constituting disposal.

117—352

---

33

b)

Solid wastes which are not hazardous wastes.

The following solid

wastes are not hazardous wastes:

1)

Household waste,

including household waste that has been

collected,

transported,

stored,

treated,

disposed,

recovered

(e.g., refuse—derived fuel)

or reused.

“Household waste”

means any waste material (including garbage, trash and

sanitary wastes in septic tanks) derived from households

(including single and multiple residences, hotels and

motels,

bunkhouses, ranger stations,

crew quarters,

campgrounds,

picnic

grounds

and

day-use

recreation

areas).

A resource recovery facility managing municipal solid waste

shall not be deemed to be treating, storing, disposing of or

otherwise managing hazardous wastes for the purposes of

regulation under this Part,

if such facility:

A)

Receives and burns only:

i)

Household waste (from single and multiple

dwellings, hotels, motels and other residential

sources) and

ii)

Solid

waste

from

commercial

or

industrial

sources that does not contain hazardous waste;

and

B)

Such facility does not accept hazardous waste and the

owner or operator of such facility has established

contractural requirements or other appropriate

notification or inspection procedures to assure that

hazardous wastes are not received at or burned in such

facility.

2)

Solid wastes generated by any of the following and which are

returned

to

the

soil

as

fertilizers:

A)

The growing and harvesting of agricultural crops.

B)

The raising of animals, including animal manures.

3)

Mining overburden returned to the mine site.

4)

Fly ash waste,

bottom ash waste,

slag waste, and flue gas

emission control waste generated primarily from the

combustion of coal or other fossil fuels.

5)

Drilling fluids, produced waters, and other wastes

associated with the exploration, development,

or production

of crude oil, natural gas or geothermal

energy.

6)

Chromium wastes:

117—353

---

34

A)

Wastes which fail the test for the toxicity

characteristic (Section 721.124 and Appendix B)

because chromium is present or are listed in Subpart

D

due to the presence of chromium, which do not fail the

test for the toxicity characteristic for any other

constituent

or

are

not

listed

due to the presence of

any other constituent, and which do not fail the test

for any other characteristic,

if

it is shown by a

waste generator or by waste generators that:

i)

The chromium in the waste

is exclusively

(or

nearly exclusively) trivalent chromium; and

ii)

The waste is generated from an industrial

process which uses trivalent chromium

exclusively (or nearly exclusively) and the

process

does

not

generate

hexavalent

chromium;

and

iii)

The waste

is typically and frequently managed in

non—oxidizing environments.

B)

Specific

wastes

w1~ichmeet

the

standard

in

subsections

(b)(6)(A)(i),

(ii)

and

(iii)

(so long as they do not

fail the test for the characteristic of EP toxicity,

and do not fail the test for any other characteristic)

are

i)

Chrome

(blue) trimmings generated by the

following subcategories of the leather tanning

and finishing industry; hair pulp/chrome

tan/retan/wet finish;

hair save/chrome

tan/retan/wet finish;

retan/wet finish;

no

beaxnhouse; through—the-blue; and shearling.

ii)

Chrome

(blue)

shavings generated by the

following subcategories of the leather tanning

and finishing industry; hair pulp/chrome

tan/retan/wet finish;

hair gave/chrome

tan/retan/wet finish; retan/wet finish;

no

beamhouse; through-the-blue;

and ahearling.

iii)

Buffing dust generated by the following

subcategories of the leather tanning and

finishing industry:

hair pulp/chrome

tan/retan/wet finish; hair save/chrome

tan/retan/wet

finish; retan/wet finish; no

beamhouse; through-the-blue.

iv)

Sewer screenings generated

by

the

following

subcategories of the leather tanning and

finishing industry:

hair pulp/chrome

117—354

---

35

tan/retan/wet finish; hair save/chrome

tan/retan/wet finish; retan/wet finish;

no

beamhouge;

through-the-blue;

and

shearling.

v)

Wastewater treatment sludges generated by the

following subcategories of the leather tanning

and finishing industry:

hair pulp/chrome

tan/retan/wet finish; hair save/chrome

tan/retan/wet finish; retan/wet finish;

no

beamhouse; through—the—blue;

and shearling.

vi)

Wastewater treatment sludges generated by the

following subcategories of the leather tanning

and finishing industry:

hair pulp/chrome

tan/retan/wet finish; hair save/chrome

tan/retan/wet finish; and through—the-blue.

vii)

Waste

scrap

leather

from the leather tanning

industry, the shoe manufacturing industry, and

other leather product manufacturing industries.

viii) Wastewater treatment sludges

from

the

production

of titanium dioxide pigment using chromium-

bearing ores by the chloride process.

7)

Solid waste from the extraction, beneficiation and

processing of ores and minerals

(including coal),

including

phosphate rock and overburden from the mining of uranium

ore.

For purposes of

this

subsection, beneficiation of ores

and minerals

is restricted to the following activities:

crushing,

grinding,

washing,

dissolution,

crystallization,

filtration,

sorting, sizing,

drying,

aintering,

pelletizing,

briquetting, calcining to remove water or carbon dioxide,

roasting,

autoclaving or chlorination in preparation for

leaching

(except where the roasting or autoclaving or

chlorination)/leaching sequence produces a final or

intermediate product that does not undergo further

beneficiation

or

processing),

gravity

concentration,

magnetic separation, electrostatic separation, floatation,

ion exchange,

solvent extraction, electrowinning,

precipitation,

amalgamation,

and heap,

dump, vat Stank and in

situ leaching.

•For the purposes of this subsection,

solid

waste from the processing of ores and minerals will include

only

the

following wastes:

A)

Slag

from

primary

copper

processing;

B)

Slag from primary lead processing;

C)

Red and brown muds from bauxite refining;

D)

Phosphogypsum from phosphoric acid production;

117—355

---

36

E)

Slag from elemental phosphorus production;

F)

Gasifier ash from coal gasification;

G)

Process wastewater from coal gasification;

H)

Calcium sulfate wastewater treatment plant sludge from

primary copper processing;

I)

Slag tailings from primary copper processing;

J)

Fluorogypsum from hydrofluoric acid production;

K)

Process wastewater from hydrofluoric acid production;

L)

Air pollution control dust/sludge from iron blast

furnaces;

M)

Iron blast furnace slag;

N)

Treated residue from roasting/leaching of chrome ore;

0)

Process wastewater from primary magnesium processing

by the anhydrous process;

P)

Process wastewater from phosphoric acid production;

Q)

Basic oxygen furnace and open hearth furnace air

pollution control dust/sludge from carbon steel

production;

R)

Basic oxygen furnace and open hearth furnace slag from

carbon steel production;

5)

Chloride processing waste solids from titanium

tetrachloride production;

T)

Slag from primary zinc smelting;

and,

U)

Until June 30,

1991,

process wastewater, acid plant

blowdown

and

wastewater

treatment

plant

solids

from

primary zinc smelting and refining, except for

wastewater treatment plant solids which are hazardous

by characteristic and which are not processed.

8)

Cement kiln dust waste.

9)

Solid

waste

which

consists

of

discarded

wood

or

wood

products

which

fails

the

test

for

the

toxicity

characteristic solely

for arsenic and which is not

a

hazardous

waste

for

any

other

reason

or

reasons

if

the

waste

117—356

---

37

is

generated

by

persons

who

utilize

the

arsenical—treated

wood and wood products for these materials’

intended and

use.

10)

Petroleum-contaminated media and debris that fail the test

for

the

toxicity

characteristic

of

Section

721.124

(hazardous waste codes D018 throuah D043 only) and are

subject to corrective action regulations under 35

Ill.

Adm.

Code 731.

c)

Hazardous wastes which are exempted from certain regulations.

A

hazardous waste which is generated in a product or raw material

storage tank,

a product or raw material

transport

vehicle or

vessel,

a product or raw material pipeline,

or in a manufacturing

process unit or an associated non—waste—treatment manufacturing

unit,

is

not

subject

to

regulation

under

35

Ill.

Adxn.

Code 702,

703,

705

and

722 through 725 and 728 or to the notification

requirements of Section 3010 of RCRA until

it exits the unit in

which

it was generated, unless the unit is

a surface impoundment,

or

unless

the

hazardous waste remains in the unit more than 90

days after the unit ceases to be operated for manufacturing, or

for

storage

or

transportation

of

product

or

raw

materials.

d)

Samples

1)

Except

as provided in subsection

(d)(2),

a sample of solid

waste or a sample of water,

soil or air, which is collected

for the sole purpose of testing to determine its

characteristics or composition,

is not subject to any

requirements of this Part or

35

Ill.

Adm.

Code 702,

703, 705

and

722 through 728.

The sample qualifies when:

A)

The sample is being transported to a laboratory for

the

purpose

of

testing;

or

B)

The

sample

is

being transported back to the sample

collector

after testing;

or

C)

The

sample

is

being

stored

by

the

sample

collector

before transport to

a laboratory for testing; or

D)

The sample

is being stored in a laboratory before

testing;

or

E)

The sample is being stored in a laboratory for testing

but before

it

is returned to the sample collector;

or

F)

The sample is being stored temporarily in the

laboratory

after

testing

for

a specific purpose (for

example,

until conclusion of a court case or

enforcement

action

where

further testing of the sample

may

be

necessary).

117—357

---

38

2)

In order to qualify for the exemption in subsection

(d)(l)(A) and

(B),

a sample collector shipping samples to a

laboratory and

a laboratory returning samples to a sample

collector must:

A)

Comply with U.S. Department of Transportation (DOT),

U.S.

Postal Service (USPS) or any other applicable

shipping requirements;

or

B)

Comply with the following requirements if the sample

collector determines that DOT, USPS or other shipping

requirements do not apply to the shipment of the

sample:

i)

Assure that the following information

accompanies the sample:

The sample collector’s

name,

mailing address and telephone number;

the

laboratory’s name, mailing address and telephone

number;

the

quantity

of

the

sample;

the

date

of

the shipment; and a description of the sample.

ii)

Package the sample so that it does not leak,

spill or vaporize from its packaging.

3)

This exemption does not apply

if the laboratory determines

that the waste is hazardous but the laboratory is no longer

meeting any

of the conditions stated in subsection (d)(1).

e)

Treatability study samples.

1)

Except as is provided in subsection

(e)(2), persons who

generate or collect samples for the purpose of conducting

treatability studies,

as defined in 35

Ill.

Adm.

Code

720.110,

are

not

subject

to

any requirement of 35

Ill.

Adm.

Code 721 through 723 or to the notification requirements of

Section 3010 of the Resource Conservation and Recovery Act.

Nor are such samples included in the quantity determinations

of Section 721.105 and

35

Ill.

Mm.

Code

722.134(d)

when:

A)

The sample is being collected and prepared for

transportation by the generator or sample collector;

or,

B)

The sample

is being accumulated or stored by the

generator or sample collector prior to transportation

to a laboratory or testing facility;

or

C)

The sample

is being transported to the laboratory or

testing facility for the purpose of conducting a

treatability study.

117—358

---

39

2)

The exemption in subsection

(e)(1)

is applicable to samples

of hazardous waste being collected and shipped for the

purpose of conducing treatability studies provided that:

A)

The generator or sample collector uses

(in

“treatability studies”)

no more than 1000 kg of any

non—acute hazardous waste,

1 kg of acute hazardous

waste or 250 kg of soils, water or debris contaminated

with acute hazardous waste for each process being

evaluated for each generated wastestream; and

B)

The mass of each shipment does not exceed 1000 kg of

non—acute hazardous waste,

1 kg of acute hazardous

waste or 250 kg of soils, water or debris contaminated

with acute hazardous waste; and

C)

The sample must be packaged so that

it

does

not

leak,

spill or vaporize from its packaging during shipment

and the requirements of subsections

(i)

or

(ii)

are

met.

i)

The transportation of each sample shipment

complies

with

U.S.

Department

of

Transportation

(DOT),

U.S.

Postal Service (USPS) or any other

applicable shipping requirements;

or

ii)

If the DOT,

USPS or other shipping requirements

do not apply to the shipment of the sample,

the

following information must accompany the sample:

The name,

mailing address and telephone number

of the originator of the sample; the name,

address and telephone number of the facility

that will perform the treatability study; the

quantity of the sample; the date of the

shipment;

and,

a

description

of

the

sample,

including

its

USEPA hazardous waste number.

D)

The sample

is shipped to a laboratory or testing

facility which is exempt under

subsection

(f)

or has

an appropriate

RCRA

permit or interim status.

E)

The generator or sample collector maintains the

following records

for a period ending

3 years after

completion of the treatability study:

i)

Copies of the shipping documents;

ii)

A copy of the contract with the facility

conducting the treatability study;

iii)

Documentation showing:

The amount of waste

shipped under this exemption; the name,

address

117—359

---

40

and USEPA identification number of the

laboratory or testing facility that received the

waste; the date the shipment was made;

and,

whether or not unused samples and residues were

returned to the generator.

F)

The generator reports the information required in

subsection

(e)(2)(E)(iii)

in

itB

report under 35 Ill.

Adm. Code 722.141.

3)

The Agency may grant requests, on a case—by—case basis,

for

quantity limits

in excess of those specified in subsection

(e)(2)(A),

for up to an additional

500 kg of any non-acute

hazardous waste,

1 kg of acute hazardous waste and 250 kg of

soils, water or debris contaminated with acute hazardous

waste,

to conduct further treatability study evaluation

when:

-

There has been an equipment or mechanical failure

during the conduct of the treatability study;

there is need

to verify the results of a previously conducted treatability

study; there

is

a need to study and analyze alternative

techniques within a previously evaluated treatment process;

or, there is

a need to do further evaluation of an ongoing

treatability study to determine final specifications for

treatment.

The additional quantities allowed are subject to

all the provisions in subsections

(e)(1) and (e)(2)(B)

through

(F).

The generator or sample collector must apply

to the Agency and provide in writing the following

information:

A)

The reason why the generator or sample collector

requires additional quantity of sample for the

treatability study evaluation and the additional

quantity needed;

B)

Documentation accounting for all samples of hazardous

waste from the wastestrearn which have been sent for or

undergone treatability studies, including the date

each previous sample was shipped, the quantity of each

previous shipment,

the laboratory or testing facility

to which it was shipped, what treatability study

processes were conducted on each sample shipped,

and

the available results of each treatability study;

C)

A description of the technical modifications or change

in specifications which will be evaluated and the

expected results;

D)

If such further study is being required due to

equipment or mechanical failure, the applicant must

include information regarding the reason for the

failure or breakdown and also include what procedures

117—360

---

41

or equipment have been made to protect against further

breakdowns; and,

E)

Such other information as the Agency determines is

necessary.

4)

Final Agency determinations pursuant to this subsection may

be appealed to the Board.

f)

Samples undergoing treatability studies at laboratories or testing

facilities.

Samples undergoing treatability studies and the

laboratory or testing facility conducting such treatability

studies

(to the extent such facilities are not otherwise subject

to

RCRA

requirements)

are not subject to any requirement of this

Part,

or of 35

Ill. Adm. Code 702,

703,

705,

722 through 726,

and

728,

or to the notification requirements of Section 3010 of the

Resource Conservation and Recovery Act, provided that the

requirements of subsections

(f)(1) through (f)(11)

are met.

A

mobile treatment unit may qualify as a testing facility subject to

subsections

(f)(l) through (f)(11).

Where a group of mobile

treatment units are located at the same site,

the limitations

specified in subsections

(f)(1) through

(f)(11)

apply to the

entire group of mobile treatment units collectively as

if the

group were one mobile treatment unit.

1)

No less than 45 days before conducting treatability studies,

the facility notifies the Agency in writing that it intends

to conduct treatability studies under this subsection.

2)

The laboratory or testing facility conducting the

treatability study has

a USEPA identification number.

3)

No more than a total of 250 kg of “as received” hazardous

waste is subjected to initiation of treatability studies

in

any single day.

“As received” waste refers to the waste as

received

in the shipment from the generator or sample

collector.

4)

The quantity of “as received” hazardous waste stored at the

facility for the purpose of evaluation in treatability

studies does not exceed 1000 kg, the total of which can

include 500 kg of soils, water or debris contaminated with

acute hazardous waste or

1 kg of acute hazardous waste.

This quantity limitation does not include:

A)

Treatability study residues; and,

B)

Treatment materials

(including nonhazardous solid

waste)

added to

“as received” hazardous waste.

5)

No more than 90 days have elapsed since the treatability

study

for the sample was completed,

or no more than one year

117—361

---

42

has elapsed since the generator or sample collector shipped

the sample to the laboratory or testing facility, whichever

date first occurs.

6)

The treatability study does not involve the placement of

hazardous waste on the land or open burning of hazardous

waste.

7)

The facility maintains records for 3 years following

completion of each study that show compliance with the

treatment rate limits and the storage time and quantity

limits.

The following specific information mua be included

for each treatability study conducted:

A)

The name,

address and USEPA identification umber of

the generator or sample collector of each waste

sample;

B)

The date the shipment was received;

C)

The quantity of waste accepted;

D)

The quantity of “as received” waste in storage each

day;

E)

The date the treatment study was initiated and the

amount of “as received” waste introduced to treatment

each day;

F)

The date the treatability study was concluded;

G)

The date any unused sample or residues generated from

the treatability study were returned to the generator

or sample collector or,

if sent to a designated

facility, the name of the facility and the USEPA

identification number.

8)

The facility keeps,

on-site,

a copy of the treatability

study contract and all shipping papers associated with the

transport of treatability study samples to and from the

facility for a period ending

3 years from the completion

date of each treatability study.

9)

The facility prepares and submits

a report to the Agency by

March 15 of each year that estimates the number of studies

and the amount of waste expected to be used in treatability

studies during the current year,

and includes the following

information for the previous calendar year:

A)

The name,

address and USEPA identification number of

the facility conducting the treatability studies;

117—36 2

---

43

B)

The types

(by process)

of treatability studies

conducted;

C)

The names and addresses of persons for whom studies

have been conducted (including their USEPA

identification numbers);

D)

The total quantity of waste in storage each day;

E)

The quantity and types of waste subjected to

treatability studies;

F)

When each treatability study was conducted;

G)

The final disposition of residues and unused sample

from each treatability study;

10)

The facility determines whether any unused sample or

residues generated by the treatability study are hazardous

waste under Section 721.103 and,

if

so,

are subject to 35

Ill. Mm.

Code 702,

703 and 721 through 728, unless the

residues and unused samples are returned to the sample

originator under the subsection

(e)

exemption.

11)

The facility notifies the Agency by letter when the facility

is no longer planning to conduct any treatability studies at

the site.

(Source:

Amended at

15 Ill. Reg.

,

effective

)

Section 721.106

Requirements for Recyclable Materials

a)

Recyclable materials:

1)

Hazardous wastes that are recycled are subject to the

requirements for generators, transporters and storage

facilities of subsections

(b) and

(c), except for the

materials listed in subsections

(a)(2) and (a)(3).

Hazardous wastes that are recycled will be known as

“recyclable materials”.

2)

The following recyclable materials are not subject to the

requirements of this Section but are regulated under 35

Ill.

Adm. Code 726.Subparts C through G and all applicable

provisions in 35 Ill. Adm. Code 702,

703 and 705.

A)

Recyclable materials used in a manner constituting

disposal

(35 Ill. Adm.

Code 726.Subpart C);

B)

Hazardous wastes burned

for energy recovery in boilers

and industrial furnaces that are not regulated under

117—363

---

44

35

Ill. Adm. Code 724 or 725.Subpart 0

(35 Ill. Adm.

Code 726.Subpart D.)

C)

Used oil that exhibits one or more of the

characteristics of hazardous waste and is burned for

energy recovery in boilers or industrial furnaces that

are not regulated under 35

Ill.

Adrn.

Code 724 or

725.Subpart 0.

(35 Ill. Adm. Code 726.Subpart

E);

D)

Recyclable materials from which precious metals are

reclaimed

(35 Ill. Mm. Code 726.Subpart F);

E)

Spent lead-acid batteries that are being reclaimed

(35

Ill. Adm.

Code 726.Subpart G).

3)

The following recyclable materials are not subject to

regulation under 35 Ill. Adm. Code 722 through 726, 728, or

702,

703 or 705 and are not subject to the notification

requirements of Section

3010 of the Resource Conservation

and Recovery Act:

A)

Industrial ethyl alcohol that

is reclaimed except

that,

unless provided otherwise in an international

agreement as specified

in

35

Ill.

Adxn.

Code 722.158:

i)

A person initiating

a shipment for reclamation

in a foreign country, and any intermediary

arranging for the shipment, shall comply with

the requirements applicable to a primary

exporter in

35

Ill.

Adm. Code 722.153,

722.156(a)(1)

through (a)(4),

(a)(6) and

(b),

and 722.157,

shall export such materials only

upon consent of the receiving country and in

conformance with the USEPA Acknowledgement of

Consent as defined in

35 Ill. Adm. Code

722.Subpart

E,

and shall provide a copy of the

USEPA Acknowledgement of Consent to the shipment

to the transporter transporting the shipment for

export;

ii)

Transporters transporting a shipment

for export

shall not accept a shipment if the transporter

knows the shipment does not conform to the USEPA

Acknowledgement of Consent, shall ensure that

a

copy of the USEPA Acknowledgement of Consent

accompanies the shipment and shall ensure that

it is delivered to the facility designated by

the person initiating the shipment.

B)

Used batteries

(or used battery cells) returned to

a

battery manufacturer for regeneration;

117—364

---

45

C)

Used oil that exhibits one or more of the

characteristics of hazardous waste but is recycled in

some other manner than being burned for energy

recovery;

D)

Scrap metal;

E)

Fuels produced from the refining of oil—bearing

hazardous wastes along with normal process streams at

a petroleum refining facility if such wastes result

from normal petroleum refining,

production and

transportation practices;

F)

Oil reclaimed from hazardous waste resulting from

normal petroluem refining, production and

transportation practices, which oil

is to be refined

along with normal process streams at a petroleum

refining facility;

G)

Coke and coal tar from the iron and steel industry

that contains USEPA hazardous waste number K087

(decanter tank tar sludge from coking operations)

(Section 721.132) from the ironand steel production

process;

H)

Petroleum refining wastes.

i)

Hazardous waste fuel produced from oil—bearing

hazardous wastes from petroleum refining,

production or transportation practices,

or

produced from oil reclaimed from such hazardous

wastes, where such hazardous wastes are

reintroduced into

a process that does not use

distillation or does not produce products from

crude oil so long as the resulting fuel meets

the used oil specification under 35 Ill. Ada.

Code 726.140(e) and so long as no other

hazardous wastes are used to produce the

hazardous waste fuel;

ii)

Hazardous waste fuel produced from oil—bearing

hazardous waste from petroleum refining

production and transportation practices, where

such hazardous wastes are reintroduced into a

refining process after a point at which

contaminants are removed, so long as the fuel

meets the used oil fuel specification under 35

Ill. Ada. Code 726.140(e); and

iii)

Oil reclaimed from oil-bearing hazardous wastes

from petroleum refining, production and

transportation practices, which reclaimed oil

is

117—365

---

46

burned as a fuel without reintroduction to a

refining process,

so long as the reclaimed oil

meets the used oil fuel specification under 35

Ill.

Ada. Code 726.140(e); and

I)

Petroleum coke produced from petroleum refinery

hazardous wastes containing oil at the same facility

at which such wastes were generated, unless the

resulting coke product exceeds one or more of the

characteristics of hazardous waste in Subpart C.

b)

Generators and transporters of recyclable materials are subject to

the applicable requirements of

35 Ill. Ada. Code 722 and 723 and

the notification requirements under Section 3010 of the Resource

Conservation and Recovery Act, except as provided in subsection

(a).

c)

Storage and recycling:

1)

Owners or operators of facilities that store recyclable

materials before they are recycled are regulated under all

applicable provisions of 35

Ill. Ada.

Code 724.Subparta A

through L, AA and BB and 725.Subparts A through L,

AA and

~,

726, 728,

702,

703 and 705 and the notification

requirement under Section 3010 of the Resource Conservation

and Recovery Act, except as provided in subsection

(a).

(The recycling process itself is exempt from regu.ation~.

except

as provided

in subsection

(d).)

2)

Owners or operators of facilities that recycle recyclable

materials without storing them before they are recycled are

subject to the following requirements, except as provided in

subsection

(a).

A)

Notification requirements under Section 3010 of the

Resource Conservation and Recovery Act.

B)

35

Ill. Ada.

Code 725.171 and 725.172

(dealing with

the use of the manifest and manifest discrepancies)

Q~.

Subsection

(dl.

~j

Owners or operators of

facilities reguired to have a RCRA permit

pursuant to

35

Ill. Ada.

Code 703 with hazardous waste management

units which recycle hazardous wastes are subject to 35

Ill. Ada.

Code 724.Subpart AA and BE and 725.Subpart AA and BB.

(Source:

Amended at

15 Ill. Reg.

,

effective

117—366

---

47

SUBPART B:

CRITERIA FOR IDENTIFYING THE CHARACTERISTICS OF

HAZARDOUS WASTE AND FOR LISTING HAZARDOUS WASTES

Section 721.111

Criteria for Listing Hazardous Waste

a)

UOErA’e criteria for listing hazardous waste are given at 40 CFR

Cectjon 261.11.

USEPA lists

a solid waste as

p

hazardous

waste

only upon determining that the solid waste meets one of the

following criteria:

jj.

It exhibits any of the characteristics of hazardous waste

identified

in Subpart

C;

or

b~

2.).

“P” list;

Acutc hazardous wastes are listtd in Ccction

721.133(c).

Acute hazardous wastes are those which have

been found to be fatal.

Acute toxic wastes are those which

haveAcute hazardous waste.

It

has been found to be fatal to

humans in low doses or,

in the absence of data on human

toxicity,

it has been shown in studies to have an oral LD

50

toxicity (rat) of less than 50 mg/kg,

an inhalation LC 50

toxicity

(rat)

of less than 2 mg/*~,or

a dermal LD

50

toxicity

(rabbit) of less than 200 mg/kg or is otherwise

capable of causing or significantly contributing to an

increase

in serious irreversible or incapacitating

reversible,

illness.

BOARD NOTE:

+Waste listed

in accordance with these criteria

will bt~ designated Acute Hazardous Waste-)-.

~j

Toxic waste.

It contains any of the toxic constituents

listed

in A~~endix

H unless,

after considering any of the

following factors, USEPA concludes that the waste

is capable

of posing a substantial present or potential hazard to human

he&ltl-i or the environment when improperly treated,

stored,

transported or disposed of,

or otherwise managed:

~j

The nature of the toxicity presented by the

constituent.

~j

The concentration of the constituent in the waste.

~j.

The potential of the constituent or any toxic

degradation product of the constituent to migrate from

the waste into the environment under the tvtea of

improper management considered

in subsection

(al (3) (G).

~J

The persistence of the constituent or any toxic

degradation product

of the constituent.

117—36 7

---

48

~j

The potential for the constituent

or any toxic

degradation product of the constituent to dearade into

nonharaful constituents and the rate of degradation.

fi

The degree to which the constituent or any degradation

product of the constituent bioaccumulates in

ecosystems.

~).

The plausible tv~esof improper management to which

the waste could be subjected.

!U

The guantities of the waste generated at individual

generation sites or on

p

regional or national basis.

fl

The nature and severity of the human health and

environmental

damage

that

has

occurred

as

a result of

the

improper management of the

wastes

containing

the

constituent.

Qj

Action taken by other governmental agencies or

regulatory programs based on the health or

environmental hazard posed by the waste or waste

constituent.

~j

Such

other

factors

as

may

be

appropriate.

BOARD

NOTE:

Wastes

listed

in

accordance

with

these

criteria

are

designated

toxic

wastes.

ii

Substances

are

listed

in

Appendix

H

only

if

they

have

been

shown in scientific studies to have toxic,

carcinogenic,

mutagenic or teratogenic effects on humans or other life

forms.

~j

USEPA may list classes or

types

of solid waste as hazardous waste

if USEPA has reason

to

believe

that

individual

wastes,

within

the

class or

type

of waste, typically or freguently are hazardous

under

the

definition

of

hazardous

waste

found

in

Section

1004(5)

of the Resource Conservation and Recovery Act

(42 USC 6901 et

seg.)

c)

UCEt’A’s criteria for

~i~tn,i

haziardous waste are t1(ven at 40

cm

Cection 261.ll.USEPA will use the criteria for listing specified

in

this

Section

to

establish

the

exclusion

limits

referred

to

in

Section 721.105(c~.

(Source:

Amended at 15 Ill. Reg.

,

effective

)

117—368

---

49

SUBPART C:

CHARACTERISTICS OF

HAZARDOUS

WASTE

Section 721.120

General

a)

A solid waste,

as defined

in Section 721.102, which is not

excluded from regulation as a hazardous waste under Section

721.104(b),

is

a hazardous waste if it exhibits any of the

characteristics identified in this Subpart.

(Board NoteiBOARD NOTE:

35

Ill.

Ada. Code 722.111 sets forth the

generator’s responsibility to determine whether the generator’s

waste exhibits one or more characteristics identified in this

Subpart.-)-

b)

A hazardous waste which

is identified by ~ characteristic in this

Subpart,

but

is not listed as a hatardous wacte in Cubpart D,

is

assigned t~eeveryUSEPA Hazardous Waste Number which

is applicable

as

set forth in the respective charactcrietic in this Subpart.

This number must be used in complying with the notification

requirements of Section 3010 of the Resource Conservation and

Recovery Act and certainall applicable recordkeeping and reporting

requirements under

35

Ill.

Ada. Code 702,

703, 722 through 725

and

728.

c)

For purposes of this Subpart,

a sample obtained using any of the

applicable sampling methods specified in Appendix A is

a

representative sample within the meaning of

35

Ill.

Ada. Code 720.

(Board Note;BOARD NOTE:

Since the Appendix A sampling methods are

not being formally adopted,

a person who desires to employ an

alternative sampling method is not required to demonstrate the

equivalency of the person’s method under the procedures set forth

in 35

Ill.

Ada. Code 720.121.1-

(Source:

Amended at

15 Ill. Reg.

,

effective

)

Section 721.121

Characteristic of Ignitability

a)

A solid waste exhibits the characteristic of ignitability if a

representative sample of the waste has any of the following

properties:

1)

It is a liquid, other than an aqueous solution containing

less than 24 percent alcohol by volume, and has

a flash

point less than 60°C(140°F),as determined by

a Pensky-

Martens Closed Cup Tester,

using the test method specified

in the American Doeiety of Testing Materials

(AOTM) Ctandar~

D

03

70 or

D 03 80

(incorporated by refercnce,

see

5720. l11)ASTM D—93,

incorporated by reference in 35

Ill.

Adm. Code 720.111,

or a Setaflash Closed Cup Tester, using

the test method specified in ASTM Standard D-32283278 78

(incorporated by reference,

see 5720.111),

incorporated by

117—369

---

50

reference in 35

Ill.

Ada.

Code 720.111,

or as determined by

an equivalent test method approved by the Board

(S~35 Ill.

Adm. Code 720.120).

2)

It

is not a liquid and is capable, under standard

temperature and pressure,

of causing fire through friction,

absorption of moisture or spontaneous chemical changes and,

when ignited, burns

so vigorously and persistently that it

creates a hazard.

3)

It

is an ignitable compre8sed gas as defined in 49 CFR

173.300, incorporated by reference in 35

Ill. Ada. Code

720.111,

and as determined by the test methods described in

that regulation or equivalent test methods approved by the

Board (~35Ill. Ada. Code 720.120).

4)

It

is an oxidizer as defined in 49 CFR 173.151, incorporated

by reference

in

35

Ill.

Ada. Code 720.111.

b)

A solid waste that exhibits the characteristic of ignitability-r

but

is not listed as a hazardous waste

in Subpart

D, has the EPA

Hazardous Waste Number of D001.

(Source:

Amended at

15

Ill.

Reg.

,

effective

Section 721.122

Characteristic of Corrosivity

a)

A solid waste exhibits the characteristic of corrosivity if a

representative sample of the waste has either of the following

properties:

1)

It

is aqueous and has a pH less than or equal to

2

or

greater than or equal to 12.5,

as determined by a pH meter

using either an EPA test method or an equivalent test method

(S~35 Ill. Ada.

Code 720.121).

The EPA test method for pH is

specified as Method 5.2

in “Teat Methods for the Evaluation

of Solid Waste, Physical/Chemical Methods” -(-it~eorpcratedby

reference,

eec 5720.111), incorporated by reference in 35

Ill. Ada. Code 720.111.

2)

It

is a liquid and corrodes steel

(SAE

1020) at a rate

greater than 6.35 mm (0.250 inch) per year at a test

temperature of 55°C(130°F)as determined by the test method

specified in NACE (National Association of Corrosion

Engineers) Standard TM—01—69 as standardized in “Test

Methods for the Evaluation of Solid Waste,

Physical/Chemical

Methods”

(incorporated by reference,

ccc 572O.lll)L.

incorporated by reference in 35

Ill. Ada. Code

720.13.1, or

an equivalent test method (~35Ill. Adm. Code 720.121).

117—370

---

51

b)

A solid waste that exhibits the characteristic of corrosivity

,-

but

is not listed as a hazardous waste in

Cubpart

B,

has the EPA

Hazardous Waste Number of D002.

(Source:

Amended at

15

Ill.

Reg.

,

effective

Section 721.123

Characteristic of Reactivity

a)

A solid waste exhibits the characteristic of reactivity

if

a

representative sample of the waste has any of the following

properties:

1)

It

is normally unstable and readily undergoes violent change

without detonating.

2)

It reacts violently with water.

3)

It forms potentially explosive mixtures with water.

4)

When mixed with water,

it generates toxic gases,

vapors or

fumes

in a quantity sufficient to present a danger to human

health or the environment.

5)

It

is

a cyanide or sulfide bearing waste which,

when exposed

to pH conditions between 2 and 12.5 can generate toxic

gases,

vapors or fumes in a quantity sufficient to present

a

danger to human health or the environment.

6)

It

is capable of detonation or explosive reaction

if

it

is

subjected to

a strong initiating source or

if heated under

confinement.

7)

It

is readily capable of detonation or explosive

decomposition or reaction at standard temperature and

pressure.

8)

It is a forbidden explosiveas defined in 49 CFR 173.51,

or

a Class A explosive as defined

in 49 CFR 173.53 or

a Class B

explosive as defined in 49 CFR 173.88,

incorporated by

reference in 35

Ill. Ada. Code 720.111.

b)

A solid waste that exhibits the characteristic of reactivity

,

but

io not listcd as a hazardous waste in Subpart

D, has the EPA

Hazardous Waste Number of D003.

(Source:

Amended at

15

Ill.

Reg.

,

effective

Section 721.124

Toxicity Characteristic

a)

A solid waste exhibits the characteristic of toxicity

if, using

the test methods described in Appendix B or equivalent methods

approved by the Agency under the procedures

set forth in Sections

117—37 1

---

52

720.120 and 720.121, the extract from a representative sample of

the waste contains any of the contaminants listed in the table in

subsection

(b)

at a concentration equal to or greater than the

respective value given in that table.

Where the waste contains

less than 0.5 percent filterable solids, the waste itaelf, after

filtering using the methodology outlined in Appendix B,

is

considered to be the extract for the purpose of this Section.

BOARD NOTE:

Generators are required to use the TCLP test

for the

hazardous waste determination under

35

Ill.

Ada. Code 722.120 as

of September 25, 1990.

Provided, however,

that, as specified at

55 Fed. Reg.

11850, March 29, 1990,

small quantity generators of

100 to 1000 kg! month,

as defined in 35

Ill. Ada. Code 721.105,

may continue to use the EP toxicity test until March 29,

1991.

The EP toxicity test is Method 1310 in SW 846,

“Test Methods for

Evaluating Solid Wastes, Physical/Chemical Methods”,

incorporated

by reference in

35

Ill. Ada. Code 720.111.

The reference to the

“EP toxicity test” in 35

Ill. Ada.

Code 808.410(b)(4)

is to be

understood as referencing the test required by this Section.

b)

A solid waste that exhibits the characteristic of toxicity,

but

is

not

listed as a hazardous waste in Cubpart D,

has the USEPA

Hazardous Waste Number specified in the following table which

corresponds to the toxic cont~.minantcausing it to be hazardous.

MAXIMUM CONCENTRATION OF CONTAMINANTS

FOR THE TOXICITY CHARACTERISTIC

USEPA

Hazardous

CAS

Regulatory

Waste No.

Contaminant

Number

Note

Level(mg/L)

D004

Arsenic

7440—38—2

5.0

DOOS

Barium

7440—39—3

100.0

D018

Benzene

71—43—2

0.5

D006

Cadmium

7440—43—9

1.0

D019

Carbon tetra-

56—23-5

0.5

chloride

D020

Chlordane

57—74—9

0.03

D021

Chlorobenzene

108—90-7

100.0

D022

Chloroform

67—66—3

6.0

D007

Chromium

7440—47—3

5.0

D023

o—Cresol

95—48—7

4

200.0

D024

m—Cresol

108—39—4

4

200.0

D025

p—Cresol

106-44—5

4

200.0

D026

Cresol

4

200.0

D0l6

2,4—D

94—75—7

10.0

D027

1,4—Dichioro—

106—46—7

7.5

benzene

D028

1,2—Dichloroethane

107—06—2

0.5

D029

1,l—Dichloro—

75—35—4

0.7

ethylene

117—372

---

53

D030

2,4-Dinitrotoluene

121—14—2

3

0.13

D012

Endrin

72—20—8

0.02

D031

Heptachior (and its

76—44—8

0.008

epoxide)

D032

Hexachlorobenzene

118—74—1

3

0.13

D033

Hexachlorobuta—

87—68—3

0.5

diene

0034

Hexachloroethane

67-72—1

3.0

0008

Lead

7439—92—1

5.0

0013

Lindane

58—89—9

0.4

D009

Mercury

7439—97—6

0.2

D0l4

Methoxychior

72—43—5

10.0

D035

Methyl ethyl ketone

78—93—3

200.0

D036

Nitrobenzene

98—95—3

2.0

D037

Pentachlorophenol

87—86—5

100.0

D038

Pyridine

110—86—1

3

5.0

DOlO

Selenium

7782—49—2

1.0

DOll

Silver

7440—22—4

5.0

D039

Tetrachloro—

127—18—4

0.7

ethylene

D015

Toxaphene

8001—35—2

0.5

D040

Trichioroethylene

79—01-6

0.5

D041

2,4,5—Trichloro—

95—95—4

400.0

phenol

D042

2,4,6—Trichloro—

88—06—2

2.0

phenol

D017

2,4,5—TP

(Silvex)

93—72—1

1.0

D043

Vinyl chloride

75—01—4

0.2

Notes to Table:

3

Quantitation limit is greater than the calculated regulatory

level.

The quantitation limit therefore becomes the

regulatory level.

4

If

o—, a—, p—cresol concentrations cannot be differentiated,

the total

creso.

(D026) concentration is used.

The

regulatory level of total

creso.

is 200.0 mg/L.

(Source:

Amended at

15

Ill.

Reg.

,

effective

SUBPART D:

LISTS OF HAZARDOUS WASTE

Section 721.131

Hazardous Wastes From Nonspecific Sources

The following solid wastes are listed hazardous wastes from non—specific

sources unless they are excluded under

35

Ill.

Ada. Code 720.120 and 720.122

and listed

in Appendix

I.

117—37 3

---

54

EPA

Hazardous

Hazard

Waste No.

Industry and Hazardous Waste

Code

FOOl

The following spent halogenated solvents used in

(T)

degreasing:

tetrachloroethylene, trichloroethylene,

methylene chloride,

1,1,1—trichloroethane, carbon

tetrachloride and chlorinated fluorocarbons;

all

spent solvent mixtures and blends used in degreasing

containing, before use,

a total of ten percent or

more

(by volume)

of one or more of the above

halogenated solvents or those solvents listed in

F002,

F004 or F005;

and still bottoms from the

recovery of these spent solvents and spent solvent

mixtures.

F002

The following spent halogenated solvents:

tetra—

(T)

chloroethylene, methylene chloride, trichloro—

ethylene,

1,1,1—trichloroethane,

chlorobenzene,

1, 1, 2-trichloro-1,2 ,2—trifluoroethane,

orthodichlorobenzene, trichlorofluoromethane and

l,1,2-trichloroethane; all spent solvent mixtures

and blends containing, before use,

a total of ten

percent or more (by volume) of one or more of the

above halogenated solvents or those solvents listed

in FOOl,

F004 or F005; and still bottoms from the

recovery of these spent solvents and spent solvent

mixtures.

F003

The following spent non—halogenated solvents:

(I)

xylene, acetone, ethyl acetate, ethyl benzene, ethyl

ether,

methyl isobutyl ketone,

n—butyl alcohol,

cyclohexanone and methanol;

all spent solvent

mixtures and blends containing, before use, only the

above spent non—halogenated solvents; and all spent

solvent mixtures and blends containing, before use,

one or more of the above non—halogenated solvents

and a total of ten percent or more

(by volume) of

one or more of those solvents listed in FOOl,

F002,

F004 or F005; and still bottoms from the recovery of

these spent solvents and spent solvent mixtures.

F004

The following spent non—halogenated solvents:

(T)

cresols and cresylic acid and nitrobenzene; all

spent solvent mixtures and blends containing, before

use,

a total of ten percent or more

(by volume)

of

one or more of the above non—halogenated solvents or

those solvents listed in FOOl,

F002 or F005; and

still bottoms from the recovery of these spent

solvents and spent solvent mixtures.

117—374

---

55

F005

The following spent non—halogenated solvents:

(I,

T)

toluene, methyl ethyl ketone,

carbon disulfide,

isobutanol,

pyridine, benzene, 2—ethoxyethanol and

2—nitropropane; all spent solvent mixtures and

blends,

containing, before use,

a total of ten

percent or more

(by volume)

of one or more of the

above non—halogenated solvents or those solvents

listed in FOOl,

F002 or P004;

and still bottoms from

the recovery of these spent solvents and spent

solvent mixtures.

F006

Wastewater treatment sludges from electroplating

(T)

operations except from the following processes:

(1)

sulfuric acid anodizing of aluminum;

(2) tin plating

on carbon steel;

(3)

zinc plating

(segregated basis)

on carbon steel;

(4) aluminum or zinc—aluminum

plating on carbon steel;

(5) cleaning/stripping

associated with tin,

zinc and aluminum plating on

carbon steel; and

(6)

chemical etching and milling

of aluminum.

F019

See Below

F007

Spent cyanide plating bath solutions from

(R,

T)

electroplating operations.

FOO8

Plating bath residues from the bottom of plating

(R,

T)

baths

from electroplating operations where cyanides

are used in the process.

F009

Spent stripping and cleaning bath solutions from

(R,

T)

electroplating operations where cyanides are used in

the process.

FOb

Quenching bath residues from oil baths from metal

(R,

T)

heat treating operations where cyanides are used in

the process.

FOll

Spent cyanide solutions from salt bath pot cleaning

(R,

T)

from metal heat treating operations.

F012

Quenching wastewater treatment sludges from metal

(T)

heat treating operations where cyanides are used in

the process.

F0l9

Wastewater treatment sludges from the chemical

(T)

conversion coating of aluminum except from zirconium

phosphating in aluminum can washing when such

phosphating

is

an exclusive conversion coating

process.

117—375

---

56

FO2O

Wastes (except wastewater and spent carbon from

(H)

hydrogen chloride purification)

from the production

or manufacturing use (as a reactant,

chemical

intermediate or component in a formulating process)

of tn— or tetrachlorophenol, or of intermediates

used to produce their pesticide derivatives.

(This

listing does not include wastes from the production

of hexachlorophene from highly purified 2,4,5-tn—

chlorophenol.)

F021

Wastes

(except wastewater and spent carbon from

(H)

hydrogen chloride purification)

from the production

or manufacturing use

(as a reactant,

chemical

intermediate or component in a formulating process)

of pentachlorophenol,

or of intermediates used to

produce

its derivatives.

F022

Wastes

(except wastewater and spent carbon from

(H)

hydrogen chloride purification)

from the

manufacturing use

(as a reactant, chemical

intermediate or component

in

a formulating process)

of tetra—,

penta— or hexachlorobenzenes under

alkaline conditions.

P023

Wastes

(except wastewater and spent carbon from

(H)

hydrogen chloride purification)

from the production

of materials on equipment previously used for the

production or manufacturing use (as a reactant,

chemical intermediate or component in a formulating

process)

of tn— and tetrachlorophenols.

(This

listing does not include wastes from equipment used

only for the production or use of hexachlorophene

from highly purified 2,4,5— tnichlorophenol.

F024

Process wastes including but not limited to,

(T)

distillation residues,

heavy ends,

tars,

and reactor

cleanout wastes,

from the production of certain

chlorinated aliphatic hydrocarbons by free radical

catalyzed processes.

These chlorinated aliphatic

hydrocarbons are those having carbon chain lengths

ranging from one to and including five, with varying

amounts and positions of chlorine substitution.

(This listing does not include wastewaters,

wastewater treatment sludges,

spent

catalysts and

wastes listed in this Section or Section 721.132.)

117—37 6

---

57

P025

Condensed light ends,

spent filters and filter aids,

(T)

and spent dessicant wastes from the production of

certain chlorinated aliphatic hydrocarbons by free

radical catalyzed processes.

These chlorinated

aliphatic hydrocarbons are those having carbon chain

lengths ranging from one to and including five, with

varying amounts and positions of chlorine

substitution.

F026

Wastes

(except wastewater and spent carbon from

(H)

hydrogen chloride purification)

from the production

of materials on equipment previously used for the

manufacturing use (as a reactant, chemical

intermediate or component in aformulating process)

of tetra—,

penta— or hexachlorobenzene under

alkaline conditions.

P027

Discarded unused formulations containing tn—,

(H)

tetra- or pentachlorophenol or discarded unused

formulations containing compounds derived from these

chlorophenola.

(This listing does not include

formulations containing hexachlorophene synthesized

from prepurified 2,4,5—tnichlorophenol as the sole

component).

F028

Residues resulting from the incineration or thermal

(T)

treatment of soil contaminated with hazardous waste

numbers P020,

F021,

F022, F023,

P026 and F027.

P039

Leachate resulting from the treatment, storage or

.Lfl

disposal of wastes classified by more than one waste

code under Subpart D,

or from a mixture of wastes

classified under Subparts C and D.

(Leachate

resulting from the management of one or more of the

following USEPA hazardous wastes and no other

hazardous wastes retains its hazardous waste

code(s):

P020,

P021, F022, F023,

P026, P027 or

F028.)

(Board Note:BOARD NOTE:

The primary hazardous properties of these materials

have been indicated by the letters T

(Toxicity), R (Reactivity),

I

(Ignitability),

and C

(Corrosivity).

The letter H indicates Acute Hazardous

Waste.-)-

(Source:

Amended at

15

Ill.

Reg.

,

effective

Section 721.132

Hazardous Waste from Specific Sources

The following solid wastes are listed hazardous wastes from specific sources

unless they are excluded under 35

Ill. Ada.

Code 720.120 and 720.122 and

listed

in Appendix

I.

117—377

---

58

EPA

Hazardous

Hazard

Waste No.

Industry and Hazardous Waste

Code

Wood Preservation:

KOOI

Bottom sediment sludge from the treatment of waste-

(T)

waters from wood preserving processes that use

creosote and/or pentachlorophenol.

Inorganic Pigments:

1(002

Wastewater treatment sludge from the production of

(T)

chrome yellow and orange pigments.

K003

Wastewater treatment sludge from the production of

(T)

molybdate orange pigments.

1(004

Wastewater treatment sludge from the production of

(T)

zinc yellow pigments.

K005

Wastewater treatment sludge from the production of

(T)

chrome green pigments.

K006

Wastewater treatment sludge from the production of

(T)

chrome oxide green pigments (anhydrous and

hydrated).

K007

Wastewater treatment sludge from the production of

(T)

iron blue pigments.

1(008

Oven residue from the production of

chrome oxide

(T)

green pigments.

Organic Chemicals:

1(009

Distillation bottoms from the production of

(T)

acetaldehyde from ethylene.

1(010

Distillation side cuts from the production of

(T)

acetaldehyde from ethylene.

1(011

Bottom stream from the wastewater stripper in the

(R,T)

production of acrylonitrile.

K013

Bottom stream from the acetronitnile column in the

(T)

production of acrylonitrile.

1(014

Bottoms

from the acetontnile purification column in

(T)

the production of acrylonitrile.

117—378

---

59

.1(015

Still bottoms from the distillation of benzyl

(T)

chloride.

K016

Heavy ends or distillation residues from the

(T)

production of carbon tetrachloride.

1(017

Heavy ends (still bottoms) from the purification

(T)

column in the production of epichlorohydrin.

1(018

Heavy ends from the fractionation column in ethyl

(T)

chloride production.

1(019

Heavy ends from the distillation of ethylene di—

(T)

chloride in ethylene dichloride production.

K020

Heavy ends from the distillation of vinyl chloride

(T)

in vinyl chloride monomer production.

K02l

Aqueous spent antimony catalyst waste from

(T)

fluoromethanes production.

1(022

Distillation bottom tars from the production of

(T)

phenol/acetone from cumene.

1(023

Distillation light ends from the production of

(T)

phthalic anhydride from naphthalene.

1(024

Distillation bottoms from the production of phthalic

(T)

anhydride from naphthalene.

1(093

Distillation light ends from the production of

(T)

phthalic anhydride from ortho—xylene.

1(094

Distillation bottoms from the production of phthalic

(T)

anhydride from ortho—xylene.

1(025

Distillation bottoms from the production of

(T)

nitrobenzene by the nitration of benzene.

K026

Stripping still tails from the production of methyl

(T)

ethyl pyridines.

1(027

Centrifuge and distillation residues from toluene

(R,T)

diisocyanate production.

K028

Spent catalyst from the hydrochlorinator reactor in

(T)

the production of l,1,l—trichloroethane.

1(029

Waste

from the product stream stripper in the

(T)

production of

1,1,1—trichioroethane.

117—37 9

---

60

1(095

Distillation bottoms from the production of 1,1,1—

(T)

trichloroethane.

1(096

Heavy ends from the heavy ends column from the

(T)

production of

1,1,1-trichloroethane.

1(030

Column bottoms or heavy ends from the combined

(T)

production of trichloroethylene and perchloro—

ethylene.

K083

Distillation bottoms from aniline production.

(T)

1(103

Process residues from aniline extraction from the

(T)

production of~aniline.

1(104

Combined wastewater streams generated from

(T)

nitrobenzene/aniline production.

1(085

Distillation or fractionation column bottoms

(T)

from the production of chlorobenzenes.

Kb05

Separated aqueous stream from the reactor product

(T)

washing step

in the production of chlorobenzenes.

1(107

Column bottoms from product separation from the

(C,T~

production of 1,1—dimethylhydrazine

(UDMH)

from

carboxilic

acid hydrazides.

1(108

Condensed column overheads from product separation

(I,T)

and condensed reactor vent gases from the production

of l,l-dimethylhydrazine

(UDMH)

from carboxilic acid

hydrazides.

1(109

Spent filter cartridges from the product

purification from the production of l,1-di—

methylhydrazine

(UDMH)

from carboxilic acid

hydrazides.

1(110

Condensed column overheads from intermediate

IT.).

separation from the production of 1,l—di-

methylhydrazine

(UDMH~

from carboxilic acid

hydrazides.

1(111

Product wastewaters from the production of di—

(C,T)

nitrotoluene via nitration of toluene.

K112

Reaction by—product water

from the drying column in

(T)

the production of toluenediaxnine via hydrogenation

of dinitrotoluene.

117—380

---

61

1(113

Condensed liquid light ends from the purification of

(T)

toluenediamine in the production of toluenediamine

via hydrogenation of dinitroluene.

K114

Vicinals

from the purification of toluene—diamine in

(T)

the production of toluenediamine via hydrogenation

of dinitrotolune.

1(115

Heavy ends from the purification of toluenediamine

(T)

in the production of toluenediamine via

hydrogenation of dinitrotoluene.

1(116

Organic condensate from the solvent recovery column

(T)

in the production of toluene diisocyanate via

phosgenation of toluenediamine.

1(117

Wastewater from the reactor vent gas scrubber in the

(T)

production of ethylene dibromide via bromination of

ethene.

K118

Spent adsorbent solids from purification of ethylene

(T)

dibromide

in the production of ethylene dibromide

via bromination of ethene.

1(136

Still bottoms from the purification of ethylene di—

(T)

bromide in the production of ethylene dibromide via

bromination of ethene.

Inorganic Chemicals:

1(071

Brine purification muds from the mercury cell

(T)

process in chlorine production, where separately

prepurified brine is not used.

K073

Chlorinated hydrocarbon waste from the purification

(T)

step of the diaphragm cell process using graphite

anodes

in chlorine production.

1(106

Wastewater treatment sludge from the mercury cell

(T)

process in chlorine production.

Pesticides:

K031

By-product

salts generated

in the production of MSMA

(T)

and cacodylic acid.

1(032

Wastewater treatment sludge from the production of

(T)

chlordane.

K033

Wastewater and scrub water from the chlorination of

(T)

cyclopentadiene in the production of chlordane.

117—38 1

---

62

1(034

Filter solids from the filtration of hexachloro—

(T)

cyclopentadiene in the production of chlordane.

K097

Vacuum atripper discharge from the chiordane

(T)

chlorinator

in the production of chlordane.

1(035

Wastewater treatment sludges generated in the

(T)

production of creosote.

1(036

Still bottoms from toluene reclamation distillation

(T)

in the production of disulfoton.

1(037

Wastewater treatment sludges from the production of

(T)

disulfoton.

1(038

Wastewater from the washing and stripping of phorate

(T)

production.

K039

Filter cake from the filtration of diethyl—

(T)

phosphorodithioic acid in the production of phorate.

1(040

Wastewater treatment sludge from the production of

(T)

phorate.

1(041

Wastewater treatment sludge from the production of

(T)

toxaphene.

1(098

Untreated process wastewater from the production of

(T)

toxaphene.

1(042

Heavy ends or distillation residues from the

(T)

distillation of tetrachlorobenzene in the production

of 2,4,5—T.

1(043

2,6—Dichlorophenol waste from the production of 2,4—

(T)

B.

1(099

Untreated wastewater from the production of 2,4—B.

(T)

1(123

Process wastewater

(including supernates,

filtrates

(T)

and washwaters)

from the production of ethylenebis—

dithiocarbamic acid and its salts.

1(124

Reactor vent scrubber water from the production of

(C,T)

ethylenebisdithiocarbamic acid and its salts.

Kb25

Filtration, evaporation and centrifugation solids

(T)

from the production of ethylenebisdithiocarbamic

acid and

its salts.

117—382

---

63

1(126

Baghouse dust and floor sweepings in milling and

(T)

packaging operations from the production or

formulation of ethylenebisdithiocarbamic acid and

its salts.

K131

Wastewater from the reactor and spent sulfuric acid

(C,T)

from the acid dryer from the production of methyl

bromide.

Kl32

Spent absorbent and wastewater separator solids from

(T)

the production of methyl bromide.

Explosives:

1(044

Wastewater treatment

sludges from the manufacturing

(R)

and processing of explosives.

1(045

Spent carbon from the treatment of wastewater

(R)

containing explosives.

1(046

Wastewater treatment sludges from the manufacturing,

(T)

formulation and loading of lead-based initiating

compounds.

1(047

Pink/red water from TNT operations.

(R)

Petroleum Refining:

KO48

Dissolved air flotation

(DAF)

float from the

(T)

petroleum refining

industry.

1(049

Slop oil emulsion solids from the petroleum refining

(T)

industry.

K050

Heat exchanger bundle cleaning sludge from the

(T)

petroleum refining industry.

K05b

API

separator sludge from the petroleum refining

(T)

industry.

1(052

Tank bottoms

(leaded) from the petroleum refining

(T)

industry.

Iron and Steel:

K061

Emission control dust/sludge from the primary

(T)

production of steel in electric furnaces.

1(062

Spent pickle liquor generated by steel finishing

(C,T)

operations of facilities within the iron and steel

industry

(SIC Codes 331 and 332)

(as defined in 35

Ill. Adm.

Code 720.110).

117—383

---

64

Primary Copper:

K064

Acid plant blowdown slurry or sludge resulting from

(T)

the thickening of blowdown slurry from primary

copper production.

Primary Lead:

1(065

Surface impoundment solids .contained in and dredged

(T)

from surface impoundments at primary lead smelting

facilities.

Primary Zinc:

1(066

After June 30,

1990,

sludge from treatment of

(T)

process wastewater or acid plant blowdown from

primary zinc production.

Primary Aluminum:

1(088

Spent potliners from primary aluminum reduction.

(T)

Ferroalloys:

K090

Emission control dust or sludge from

(T)

ferrochromiumsilicon production.

1(091

Emission control dust or sludge from ferrochromium

(T)

production.

Secondary Lead:

1(069

Emission control dust/sludge from secondary lead

(T)

smelting.

1(100

Waste leaching solution from acid leaching of

(T)

emission control dust/sludge from secondary lead

smelting.

Veterinary Pharmaceuticals:

1(084

Wastewater treatment sludges generated during the

(T)

production of veterinary pharmaceuticals from

arsenic or organo—arsenic compounds.

1(101

Distillation tar residues from the distillation of

(T)

aniline-based compounds in the production of

veterinary pharmaceuticals from arsenic or organo—

arsenic compounds.

117—384

---

65

1(102

Residue from use of activated carbon for

(T)

decolorization in the production of veterinary

pharmaceuticals from arsenic or organo—arsenic

compounds.

Ink Formulation:

1(086

Solvent washes and sludges,

caustic washes and

(T)

aludg~s,or water washes and sludges from cleaning

tubs and equipment used

in the formulation of ink

from pigments, driers,

soaps and stabilizers

containing chromium and lead.

Coking:

1(060

Ammonia still

lime sludge from coking operations.

(T)

1(087

Decanter tank tar sludge from coking operations.

(T)

(Source:

Amended at

15

Ill. Reg.

,

effective

Section 721.133

Discarded Commercial Chemical Products,

Off—Specification

Species, Container Residues and Spill Residues Thereof

The following materials or items are hazardous wastes

if and when they are

discarded or intended to be discarded as described in Section

721.102(a)(2)(A), when they are mixed with waste oil or used oil or other

material and applied to the land for dust suppression or road treatment,

when

they are otherwise applied to the land in lieu of their original intended use

or when they are contained in products that are applied to land in lieu of

their original intended use,

or when,

in lieu of their original intended use,

they are produced for use as (or as

a component of)

a fuel,

distributed for

use as

a fuel,

or burned as a fuel.

a)

Any commercial chemical product,

or manufacturing chemical

intermediate having the generic name listed in subsections

(e) or

(f).

b)

Any off—specification commercial chemical product or manufacturing

chemical intermediate which,

if

it met specifications, would have

the generic name listed in subsections

(e)

or

(f).

C)

Any residue remaining in a container or inner

liner removed from a

container that has held any commercial chemical product or

manufacturing chemical intermediate having the generic name listed

in subsection

(e)

or

(f),

unless the container is empty as defined

in Section 72l.b07(b)(3).

BOARD

NOTE:

Unless the residue is being beneficially used or

reused, or

legitimately recycled or reclaimed,

or being

accumulated,

stored, transported or treated prior to such use,

117—385

---

66

reuse, recycling or reclamation,

the Board considers the residue

to be intended for discard, and thus a hazardous waste.

An

example of

a legitimate reuse of the residue would be where the

residue remains in the container and the container is used to hold

the same commercial chemical product or manufacturing chemical

intermediate

it previously held.

An example of the discard of the

residue would be where the drum is sent to a drum reconditioner

who reconditions the drum but discards the residue.

d)

Any residue or contaminated soil, water or other debris resulting

from the cleanup of

a spill,

into or on any land or water of any

commercial chemical product or manufacturing chemical intermediate

having the generic

name

listed in subsection

(a)

or

(f), or any

residue or contaminated soil,

water or other debris resulting from

the cleanup of

a spill,

into or on any land or water,

of any off—

specification chemical product or manufacturing chemical

intermediate which,

if

it met specifications, would have the

generic name listed

in subsection

(e)

or

(f).

BOARD NOTE:

The phrase “commercial chemical product or

manufacturing chemical intermediate having the generic name listed

in

...“

refers to

a chemical substance which is manufactured or

formulated

for commercial or manufacturing use which consists of

the commercially pure grade of the chemical,

any technical grades

of the chemical that are produced or marketed,

and all

formulations

in which the chemical

is the sole active ingredient.

It does not refer to a material,

such as

a manufacturing process

waste,

that contains any of the substances listed

in subsections

(e)

or

(f).

Where

a manufacturing process waste

is deemed to be a

hazardous waste because it contains a substance listed in

subsections

(e) or

(f),

such waste will be listed in either

Sections

721.131 or 721.132 or will be identified as a hazardous

waste by the characteristics set forth in Subpart C.

e)

The commercial chemical products,

manufacturing chemical

intermediates or off-specification commercial chemical products or

manufacturing chemical intermediates referred to in subsections

(a) through

(d),

are identified as acute hazardous waste

(H)

and

are subject to the small quantity exclusion defined in Section

721.105(e).

These wastes and their corresponding EPA Hazardous

Waste Numbers are:

BOARD NOTE:

For the convenience of the regulated community the

primary hazardous properties of these materials have been

indicated by the letters T (Toxicity), and R (Reactivity).

Absence of

a letter indicates that the compound only is listed

for

acute toxicity.

117—386

---

67

Chemical

Hazardous

Abstracts

Waste No.

No.

Substance

P023

107-20-0

Acetaldehyde, chboro—

P002

591-08-2

Acetamide, N—(aminothioxomethyl)

P057

640—19-7

Acetamide, 2—fluoro—

P058

62—74-8

Acetic acid,

fluoro—, sodium salt

P002

591—08-2

1—Acetyl—2—thiourea

P003

107—02—8

Acrolein

P070

116—06—3

Aldicarb

P004

309—00—2

Aidrin

P005

107—18—6

Allyl alcohol

P006

20859-73—8

Aluminum phosphide

(R,T)

P007

2763—96—4

5—(Aminomethyl

)

—3—isoxazolol

P008

504-24—5

4—Aminopyridine

P009

131-74—8

Ammonium picrate

(R)

P119

7803-55-6

Ammonium vanadate

P099

506—61-6

Argentate(1—), bis(cyano-C)—, potassium

P010

7778—39—4

Arsenic acid H3AsO4

P012

1327—53—3

Arsenic oxide As2O3

POll

1303—28—2

Arsenic oxide As205

P011

1303—28-2

Arsenic pentoxide

P012

1327—53—3

Arsenic trioxide

P038

692—42—2

Arsine, diethyl—

P036

696-28-6

Arsonous dichloride, phenyl-

P054

151—56—4

Aziridine

P067

75—55—8

Aziridine, 2—methyl

P013

542-62-1

Barium cyanide

P024

106-47—8

Benzenamine, 4-chloro—

P077

100-01-6

Benzenamine,

4—nitro—

P028

100-44-7

Benzene,

(chioromethyl)—

P042

51-43-4

l,2—Benzenediol, 4—(1—hydroxy—2—

(methylamino)ethyl-,

(R)-

P046

122-09-8

Benzeneethanamine, alpha,

alpha—di—

methyl-

P014

108-98-5

Benzenethiol

POOl

P81-81-2

2H—l-Benzopyran-2—one,

4-hydroxy-3—(3-

oxo-1-phenylbutyl)-, and salts, when

present at concentrations greater than

0.3

P028

100-44—7

Benzyl chloride

P015

7440-41—7

Beryllium

P017

598-31-2

Bromoacetone

P018

357-57—3

Brucine

P045

39196-18-6

2—Butanone, 3, 3—dimethyl—l—(methyl—

thio)-,

O-(methylamino)carbonyfl oxime

P021

592-01-8

Calcium cyanide

P021

592-01—8

Calcium cyanide Ca(CN)2

P022

75-15-0

Carbon disulfide

P095

75-44-5

Carbonic dichloride

P023

107-20—0

Chloroacetaldehyde

117—387

---

68

P024

106—47—8

p—Chloroaniline

P026

5344-82-1

1-(o-Chlorophenyl)thiourea

P027

542—76-7

3—Chloropropionitrile

P029

544-92-3

Copper cyanide

P029

544-92-3

Copper

cyanide CuCN

P030

Cyanides (soluble cyanide salts), not

otherwise specified

P031

460-19-5

Cyanogen

P033

506-77-4

Cyanogen chloride

P033

506-77-4

Cyanogen chloride

CNC1

P034

131-89-5

2—Cyclohexyl—4,6—dinitrophenol

P016

542-88-1

Dichloroaethyl ether

P036

696-28-6

Dichlorophenylaraine

P037

60—57—1

Dieldrin

P038

692—42—2

Diethylarsine

P041

311-45-5

Diethyl-p-nitropheriyl phosphate

P040

297-97-2

0,0—Diethyl 0-pyrazinyl

phosphorothioate

P043

55-91—4

Diisopropylfluorophosphate

(DFP)

P004

309—00-2

1,4,5,8—Dimethanonaphthalene,

1,2, 3,4,10, 10—hexachloro-

1,4,4a,5,8,Ba—hexahydro-,

(lalpha,

4alpha, 4abeta,

Salpha,

Balpha,

8abeta)-

P060

465-73-6

1,4, 5,8—Di—methanonaphthalene,

1,2,3,4,10, 1O—hexachloro—

1,4,4a,5,8,8a—hexahydro-,

(lalpha,

4alpha,

4abeta,

Sbeta,

Bbeta,

8abeta)—

P037

60-57-1

2,7:3,6—Dimethanonaphth(2,3—boxirene,

3,4,5,6,9,9—hexachloro-

la,2, 2a,3,6, 6a, 7, 7a—octahydro—,

(laalpha,

2beta, 2aalpha, 3beta,

6beta,

6aalpha, 7beta,

laalpha)—

P051

P72-20—8

2,7:3,6—Dimethanonaphth(2,3—boxirene,

3,4,5,6,9,9—hexachloro—

1a,2,2a,3,6,6a,7,7a—octahydro—,

(laalpha,

2beta, 2abeta,

3alpha,

6alpha,

6abeta,

7beta, 7aalpha)-,

and

metabolitea

P044

60-51-5

Dimethoate

P046

122-09-8

alpha,

alpha-Dimethylphenethylamine

P047

534-52—1

4,6—Dinitro—o-cresol and salts

P048

51-28—5

2,4—Dinitrophenol

P020

88—85—7

Dinoseb

P085

152-16-9

Diphosphoramide, octamethyl-

P111

107-49-3

Diphosphoric acid,

tetraethyl ester

P039

298—04—4

Disulfoton

P049

541—53-7

Dithiobiuret

P050

115—29—7

Endosulfan

P088

145—73—3

Endothall

P051

72—20—8

Endrin

P051

72-20-8

Endrin,

and metabolites

117—388

---

69

P042

51-43—4

Epinephrine

P031

460—19-5

Ethanedinitrile

P066

16752-77-5

Ethanimidothioic acid, N-((methyl—

amino)carbonyloxy)—,

methyl ester

P101

107-12-0

Ethyl cyanide

P054

151—56-4

Ethylenimine

P097

52-85-7

Famphur

P056

7782—41—4

Fluorine

P057

640—19-7

Fluoroacetamide

P058

62—74—8

Fluoroacetic acid,

sodium salt

P065

628—86-4

Fulminic acid, mercury

(2+)

salt

(R,T)

P059

76—44-8

Heptachlor

P062

757-58-4

Hexaethyl tetraphosphate

P116

79-19-6

Hydrazinecarbothioamide

P068

60-34-4

Hydrazine, methyl—

P063

74-90-8

Hydrocyanic acid

P063

74-90—8

Hydrogen cyanide

P096

7803—51-2

Hydrogen phosphide

P060

465—73-6

Isodrin

P007

2763—96—4

3(2H)—Isoxazolone,

5—(aininomethyl)—

P092

62—38-4

Mercury,

(acetato—O)phenyl—

P065

628—86—4

Mercury fulminate (R,T)

P082

62-75-9

Methanamine, N-methyl—N—nitroso—

P064

624—83-9

Methane,

isocyanato—

P016

542-88-1

Methane, oxybischloro—

P112

509-14-8

Methane, tetranitro-

(R)

P118

75-70-7

Methanethiol, trichloro—

P050

115-29-7

6,9—Methano—2,4,3—benzodioxathiepen,

6,7,8,9,10,10—hexachloro—1,5,5a,6,9,9a—

hexahydro—, 3-oxide

P059

76—44-8

4,7—Methano—1H—indene,

1,4,5,6,7,8,8—

heptachloro—3a, 4,7,7a—tetrahydro—

P066

16752-77—5

Methomyl

P068

60-34-4

Methyl hydrazine

P064

624-83-9

Methyl

isocyanate

P069

75—86-5

2—Methyllactonitrile

P071

298-00-0

Methyl parathion

P072

86-88-4

alpha—Naphthylthiourea

P073

13463—39—3

Nickel carbonyl

P073

13463—39-3

Nickel carbonyl Ni(CO)4,

(T—4)—

P074

557-19-7

Nickel cyanide

P074

557-19-7

Nickel cyanide Ni(CN)2

P075

54—11-5

Nicotine, and salts

P076

10102—43—9

Nitric oxide

P077

100—01—6

p—Nitroaniline

P078

10102-44—0

Nitrogen dioxide

P076

10102-43-9

Nitrogen oxide NO

P078

10102—44—0

Nitrogen oxide NO2

P081

55—63—0

Nitroglycerine

(R)

P082

62-75-9

N—Nitroaodimethylamine

P084

4549-40-0

N—Nitrosomethylvinylamine

P085

152-16-9

Octainethylpyrophosphoramide

117—389

---

70

P087

20816—12—0

Osmium oxide OSO4~ (T—4)—

P087

20816-12—0

Osmium tetroxide

P088

145-73-3

7—Oxabicyclo(2.2.1)heptane-2,3—di—

carboxylic acid

P089

56—38-2

Parathion

P034

131—89-5

Phenol,

2—cyclohexyl—4

,

6—dinitro—

P048

51-28—5

Phenol, 2,4—dinitro-

P047

P534-52-1

Phenol,

2—methyl—4,6—dinitro—,

and

salts

P020

88—85-7

Phenol,

2—(1—methylpropyl)—4,6-dinitro—

P009

131-74—8

Phenol,

2,4,6—trinitro—, ammonium salt

(H)

P092

62-38-4

Phenylmercury acetate

P093

103—85-5

Phenylthiourea

P094

298-02-2

Phorate

P095

75-44-5

Phosgene

P096

7803—51-2

Phosphine

P041

311—45-5

Phosphoric acid,

diethyl 4-nitrophenyl

ester

P039

298-04-4

Phosphorodithioic acid, O,O-diethyl S-

2—(ethylthio)ethyl)

ester

P094

298—02-2

Phosphorodithioic acid, O,O-diethyl S-

((ejhylthio)methyl

ester

P044

60-51-5

Phoaphorodithioic acid,

0,0-dimethyl

5-

2-

(methylarnino)—2-oxoethyl

ester

P043

55—91-4

Phosphorofluoridic acid,

bis(1—methyl—

ethyl)eater

P089

56-38-2

Phosphorothioic acid,

0,0-diethyl 0-

(4-nitrophenyl) ester

P040

297—97-2

Phosphorothioic acid, O,O-diethyl 0—

pyrazinyl ester

P097

52-85-7

Phosphorothioic acid, O—(4—

(dimethyl—

amino)sulfonyl) phenyl)

O,O-dimethyl

ester

P071

298-00-0

Phosphorothioic acid, O,O-dimethyl 0-

(4-nitrophenyl) ester

P110

78-00-2

Plumbane, tetraethyl—

P098

151-50-8

Potassium cyanide

P098

151-50-8

Potassium cyanide KCN

P099

506-61-6

Potassium silver cyanide

P070

116-06-3

Propanal, 2—methyl—2—(methylthio)—,

0-

((methylamino) carbonyl

3

oxime

P101

107-12—0

Propanenitrile

P027

542-76-7

Propanenitrile, 3—chloro-

P069

75-86-5

Propanenitrile, 2-hydroxy—2—methyl-

P081

55-63-0

1,2,3—Propanetriol, trinitrate-

(R)

P017

598-31—2

2—Propanone,

1—bromo—

P102

107—19-7

Propargyl alcohol

P003

107—02-8

2—Propenal

P005

107—18—6

2—Propen—1—ol

P067

75-55—8

1,2—Propylenimine

P102

107—19—7

2—Propyn—1—ol

117—390

---

71

P008

504—24—5

4—Pyridinamine

P075

P54—11—5

Pyridine,

3—(1—methyl—2—

pyrrolidinyl)-,

(S)— and salts

P114

12039—52—0

Selenioua acid, dithallium

(1+) salt

P103

630-10-4

Selenourea

P104

506-64—9

Silver cyanide

P104

506-64—9

Silver cyanide

AgCN

P105

26628—22—B

Sodium azide

P106

143-33—9

Sodium cyanide

P106

143-33-9

Sodium cyanide NaCN

P108

P57-24—9

Strychnidin—lO—one, and salts

P018

357-57-3

Strychnidin-lO-ona,

2,3—dimethoxy-

P108

P57—24—9

Strychnine and salts

P115

7446—18—6

Sulfuric acid,

dithalliunt

(1+)

salt

P109

3689—24-5

Tetraethyldithiopyrophosphate

P110

78-00-2

Tetraethyl lead

P111

107-49-3

Tetraethylpyrophosphate

P112

509—14-8

Tetranitromethane

(R)

P062

757-58-4

Tetraphoaphoric acid, hexaethyl ester

P113

1314—32—5

Thallic oxide

P113

1314—32—5

Thallium oxide Tl203

P114

12039—52—0

Thallium

(I)

selenite

P115

7446—18—6

Thallium

(I)

sulfate

P109

3689-24-5

Thiodiphosphoric acid, tetraethyl ester

P045

39196—18—4

Thiofanox

P049

541-53—7

Thioimidodicarbonic diamide

((H2N)C(S) ~2

P014

108-98-5